v+:l f)o(!oj--

DuPont Engineering

v+:l f)O(!oJ--/<rj, r/vrr ;(ICP {5/)J /'?O J.f{,PontEngineering

/

6324 Fairview Road Charlotte, NC 28210 Tel. 17041362-6630 Fax 17041362·6636

--March 7, 2006

Mr. Larry G. Stanley North Carolina Department of Environment

And Natural Resources Hazardous Waste Section 401 Oberlin Road- Suite !50 1646 Mail Service Center Raleigh, NC 27699-1646

. ~ -........ .., .... ___ _

Re: DuPont Kinston Plant, Lenoir County, EPA ID# NCD 003 190 Kinston Ash Landfill Year-End Letter Report April, 2005 and October, 2005 Sampling Events

Dear Mr, Stanley:

The following year-end report includes the analytical data from the April, 2005 and October, 2005 Kinston Ash Landfill groundwater sampling events. Samples were collected from the following six monitoring wells: MW-13, MW-14, MW-15, MW-16, MW-17A, and MW-18.

Figure I depicts monitoring well locations along with the location of the Ash LandfilL Data collected in the field from the April, 2005 and October, 2005 sampling events are presented on Tables I and Table 2. Table I provides the water quality field parameters and Table 2 provides the water level elevations. Analytical results from the April, 2005 and October, 2005 sampling events are shown on Tables 3 and Table 4, respectively. Data qualifier information along with the laboratory report_.and laboratory chains of custody are presented as Attachment I,

If you have any/questions or comments concerning this letter report, please do not hesitate to contact me at (704) 362-6634.

!

Sincerely, ·/ ,J------~

___....~.-V"'--------~---

Andrew Alcazar DuPont Corporate Remediation Group Consultant

cc: Mr. Sergio Maciera, Unifi Kinston Plant

E. I. duPont da Nemours and Company EN-3960 Rev. 06/00

Enclosures:

Figure I -Kinston Ash Landfill Sample Location Map

Table I -Monitoring Well Field Parameters

Table 2- Kinston Monitoring Well Groundwater Elevations

Table 3 -Kinston Ash Landfill First Half 2005 Analytical Results

Table 4 -Kinston Ash Landfill Second Half 2005 Analytical Results

Attachment I: Laboratory Data Report, Data Qualifier Information, Laboratory Chains of Custody (GW Sampling IH05, and GW Sampling 2H05)

Legend

• Monitor1ng Welt ~ Drainage Channel

--+- Railroad -Surface Water

Site Road

---Fence

'"""""""' Property Line

.....t._ Fau~ Line

CJ Site Structure

-Tank

CJ Ash landfill

Map Projection. NC Slale Plane Fee~ NAD 63 Map Scale: 1112,000

0 250 500 1 000 Feet

CORPORATE REMEDIATION GROUP An Alliance between

DuPont and URS Corporation • North Garolina 6324 Fairveiw Road Charlotte, NC 28210

TITLE: Kinston Ash Landfill 2005 Monitoring Well Sample Location Map DuPont Kinston Plant Kinston, North Carolina

\

Drawn:

ND Date:

1113012005

Figure No.:

1 18984211

File Name: G:/Kioston/GisJProject_figuresJAsh_LandfiiV 2005/Kin_Site_Layoutmxd

SAMPLE (WELL I D)

MW-13

MW-14

MW-15

MW-16

MW-17A

MW-18

IINM=not measured BGS=feet below ground surface; ft BTOC= feet below top of

IIC=degrees celsius mhos/cm=micromhos per centimeter; mg/l=milligrams per lite 1tu=national turbidity unit

Elevations reference feet above mean sea level = T,

...

EID

MW-13 MW-13 MW-13 MW-13 MW-13 MW-13 MW-13 MW-13 MW-13 MW-13 MW-13 MW-13 MW-14

MW-14 MW-14 MW-14

MW-14 MW-14 MW-15

MW-15

I DATE

Table 3 Kinston Ash Landfill

First Half 2005 Analytical Results

Aw~nns ALKALINITY, BICARB. AS CAC03 AT PH 4.5 ·BARIUM

I UNITS I MDL

'

IPQL

2.0 0.0050

:02<YGEN DEMAND (COD)

MG/LAS 40.6CACC 21.4 MG/L

33200 MG/L ~ 7 50.0 J HLORIDE

~-c4;:,/4::::/2"'o~o5"'F:;L-;::L 4/4/2005 MANGANESE 4

iiNITRATE ~TE

I4/4/20051TOTAL DISSOLVED SOLIDS >TOTAL

•ZINC ; 1

18700 MG/L 140 MG/L 20 MG/L

0.065 MG/L

0.40 0.030 0.00084

2.0 0.10 0.0050

0.000028 0.00020 TB 0.040 0.10 -1-J

6230QfMG/L 3.0 10.0 18900q[_ MG/L 9. 7 30.0

9500 MG/L 0.50 2.0 5.3 MG/L 0.0048 0:0200 IJ

5 UG/L 1 5 MG/LAS

14/4/20051ALKALINITY, BICARB. AS CAC03 AT PH 4.5 59.1 CAC03 0.41 2.0 l4141?nn51f'IARIUM 9.2 MG/L 0.00045 0.0050

EMICAL OXYGEN DEMAND (COD) 11400 MG/L 9.7 50.0 J 1 . 15000 MG/L 0.40 2.0 I

f4

>~I~E 'y HE

IUIAL

nTALC LVED souns

1

r,4-DII

4/4/?00'i ALKALINITY, BICARB. AS CAC03 AT PH 4.5

UG/L = micrograms per liter

MG/L as CAC03 = milligrams per liter as Calcium Carbonate

J = Analyte present. Recorded value may not be accurate or precise.

85 MG/L 0.030 0.10 J 231 MG/L 0.0495 0.200 B 7.1 MG/L 0.00084 0.0050

0.091 MG/L 84500 MG/L

~ MG/L 4000 MG/L

150 UG/L MWL A'<j

494 CAC03 0.41 12.0

IB

B

B = Not detected substantially above the level reported in the laboratory or field blanks.

MDL= Method Detection Limit

POL = Practical Quantitation Limit

;10

MW-15 MW-15 MW-15 MW-15 MW-15 MW-15 MW-15 MW-15 MW-11 MW-11

... ,AI -Ia

~ ~

IMW-17A jMW-17A

I DATE I ANAL YTE



RESULT UNITS

14 MG/L I MDL PQL

0.0050 I DEMAND (COD) 19.7 50.0 IJ

I 4/4/2005 CHLORIDE FLL IRON

1.6 8.0 176tMGtL To.o3o 0.10

41100jMG/L _10.0495 0.200 JESE 241 MG/L 0.00084 0.0050 t 4/4/20o5tMERCURY 0.091 MG/L 0.000028 0.00021)_JE3_

l4i4/?00~[TOTAL DISSOLVED SOLIDS 606000 MG/L 19.4 60.0 OTAL ORGANIC CARBON 12200 MG/L 0.50 2.0

I4/4/2005[TOTAL ORGANIC HALOGEN 58.1 UG/L 35.0 100 TJ I 511 ,4-DIOXANE 86 UG/L 1 5 I I

MG/LAS I I< ALINITY, BICARB. AS CAC03 AT PH ~.5 240 CAC03 0.41 2.0

l4i47200SIBARIUt.f DMIUM EM I CAL LORI DE

14/4/?00~IFLLJORinF ~IRON

5 M~ 5 ME

I [

TOTAL DISSOLVED SOLIDS TOTAL ORGANIC CARBON

4/4/2005 TOTAL ORGANIC HALOGEN

'w~nn" ALKALINITY, BICARB. AS 1\0C'La.llf"

>(COD)

ATPH4.5

19 MG/L 0.0047 0.0100 10.1 MG/L 0.00045 0.0050

1.1 MG/L 0.00076 0.0050 IJ 35600 MG/L 9.7 50.0 -1-J 13000 MG/L 0.80 4.0

170 MG/L 0.030 0.10 5980 MG/L 0.0495 0.200-216 MG/L 0.00084 0.0050

0.091 MG/L IB 30.0

tlf 43.1 UG/L

MG/LAS ??R r.Ar.n~

i 0 0

lo.41 N J

0 16[MG/L [0.0047 [0.0100

NOTE: UG/L = micrograms per liter




MDL = Method Detection Limit

POL= Practical Quantitation Limit

SAMPLEID DATE

MW-17A 4/4/2005 MW-17A 4/4/2005 MW-17A 4/4/2005 MW-17A 4/4/2005 MW-17A 4/4/2005 MW-17A 4/4/2005 MW-17A 4/4/2005 MW-17A 4/4/2005 MW-17A 4/4/2005 MW-17A 4/4/2005 MW-17A 4/4/2005 MW-17A 4/4/2005 MW-17A 4/4/2005

MW-18 4/4/2005 MW-18 4/4/2005 MW-18 4/4/2005 MW-18 4/4/2005 MW-18 4/4/2005 MW-18 4/4/2005 MW-18 4/4/2005 MW-18 4/4/2005 MW-18 4/4/2005 IMW-18 4/4/2005

ANALYTE

BARIUM CADMIUM CHEMICAL OXYGEN DEMAND (COD} CHLORIDE CHROMIUM FLUORIDE IRON MANGANESE MERCURY SULFATE TOTAL DISSOLVED SOLIDS TOTAL ORGANIC CARBON TOTAL ORGANIC HALOGEN



RESULT

10.1 2.7

977000 53800

3.9 62

17200 346 0.12

10500 550000 326000

49900

ALKALINITY, BICARB. AS CAC03 AT PH 4.5 35.7 BARIUM 25.3 CHLORIDE 4900 FLUORIDE 130 MANGANESE 27.9 MERCURY 0.091 NITRATE 1800 SULFATE 48200 TOTAL DISSOLVED SOLIDS 124000 TOTAL ORGANIC 3200

NOTE: UG/L = micrograms per liter





POL = Practical Quantitation Limit

UNITS MDL PQL QUALIFIER INHOUSE

MG/L 0.00045 0.0050 MG/L 0.00076 0.0050 J MG/L 19.4 100 J MG/L 2.0 10.0 MG/L 0.0025 0.0050 J MG/L 0.030 0.10 J MG/L 0.0495 0.200 MG/L 0.00084 0.0050 MG/L 0.000028 0.00020 B MG/L 3.0 10.0 MG/L 9.7 30.0 MG/L 12.5 50.0 UG/L 3500 10000 MG/LAS CAC03 0.41 2.0 MG/L 0.00045 0.0050 MG/L 0.40 2.0 MG/L 0.030 0.10 MG/L 0.00084 0.0050 MG/L 0.000028 0.00020 B MG/L 0.040 0.10 J MG/L 6.0 20.0 MG/L 9.7 30.0 MG/L 0.50 2.0 B

SAMPLEID

MW-13 MW-13 MW-13 MW-13 MW-13 MW-13 MW-13 MW-13 MW-13 MW-13 MW-13 MW-13 MW-13 MW-14

MW-14 MW-14 MW-14 MW-14 MW-14 MW-14 MW-14 MW-14 MW-14 MW-14 MW-14 MW-15

Table4 Kinston Ash Landfill

Second Half 2005 Analytical Results

DATE ANALYTE RESULT

10/13/2005 ALKALINITY, BICARB. AS CAC03 AT PH 4.5 40.1 10/13/2005 BARIUM 0.0236 10/13/2005 CHEMICAL OXYGEN DEMAND (COD) 37.7 10/13/2005 CHLORIDE 17.6 10/13/2005 FLUORIDE 0.16 10/13/2005 MANGANESE 0.0214 10/13/2005 NITRATE 0.35 10/13/2005 SILVER 0.0023 10/13/2005 SULFATE 51.6 10/13/2005 TOTAL DISSOLVED SOLIDS 179 10/13/2005 TOTAL ORGANIC CARBON 10.4 10/13/2005 TOTAL ORGANIC HALOGEN 48.7 10/13/2005 ZINC 0.0144 10/13/2005 1 ,4-DIOXANE 2

10/13/2005 ALKALINITY, BICARB. AS CAC03 AT PH 4.5 38.4 10/13/2005 BARIUM 0.0169 10/13/2005 CHEMICAL OXYGEN DEMAND (COD) 23.0 10/13/2005 CHLORIDE 27.5 10/13/2005 FLUORIDE 0.061 10/13/2005 MANGANESE 0.0210 10/13/2005 SILVER 0.0027 10/13/2005 SULFATE 146 10/13/2005 TOTAL DISSOLVED SOLIDS 341 10/13/2005 TOTAL ORGANIC CARBON 6.2 10/13/2005 TOTAL ORGANIC HALOGEN 46.2 10/13/2005 1 ,4-DIOXANE 200

UGJL = micrograms per liter

MG/L as CAC03 = milligrams per liter as Calcium Carbonate J = Analyte present. Recorded value may not be accurate or precise.

B = Not detected substantially above the level reported in the laboratory or field blanks. MDL = Method Detection Limit

PQL = Practical Quantitation Limit

UNITS MDL PQL QUALIFIER INHOUSE

MG/LAS CAC03 0.46 2.0 MG/L 0.00044 0.0050 MG/L 12.8 50.0 J MG/L 0.40 2.0 MG/L 0.030 0.10 J MG/L 0.00096 0.0050 MG/L 0.040 0.10 MG/L 0.0020 0.0050 J MG/L 3.0 10.0 MG/L 9.7 30.0 MG/L 0.50 2.0 UG/L 35.0 100 B MG/L 0.0053 0.0200 B UG/L 1 5 J MG/LAS CAC03 0.46 2.0 MG/L 0.00044 0.0050 MG/L 12.8 50.0 J MG/L 0.40 2.0 MG/L 0.030 0.10 J MG/L 0.00096 0.0050 MG/L 0.0020 0.0050 J MG/L 7.5 25.0 MG/L 9.7 30.0 MG/L 0.50 2.0 UG/L 35.0 100 B

~ 2 10 --- ---

OlD

MW-15 MW-1: MW-1: MW-1 MW-15 MW-15 MW-1: MW-1: MW-1: MW-15 MW-15 MW-1: MW-·

!IVIVV"

Table4 Kinston Ash Landfill


!DATE

0/13/2005 ALKALINITY, BICARB. AS CAC03 AT PH 4.5 0/13/2005 BARIUM 0/13/2005 CHEMICAL OXYGEN DEMAND (COD)

11 0/13/2005 CHL 10/13/2005 CC

10/13/2005 1,

AL ORGANIC HALOGEN c

10/13/2005 ALKALINITY, BICARB. AS CAC03 AT PH 4.5 10/13/2005 ARSENIC 1 0/13/2005 BARIUM 10/13/2005 CHEMICAL OXYGEN DEMAND (COD) 10/13/20n!; r.HI ORin!= 10/1J 1 0/13/2005!1ROII 10/13/2( 10/13/20051 SILVER 1 0/13/2005!1lJ_I_AL DISSOLVED ::;u_l,IDS

~ESUL!_

501 J.0332 54.7

142. )57

0103 10.267 ill

0.0045

l.24 19.5

10.177 iFo37

1248

NOTE; UG/L = micrograms per liter






UNITS !MDL

0.41 0.00044 12.1 1.6 0.0018 !0.030 J.0378 0.0084 <f6009i 0.040 0.0020 9.7 0.51 3( 0.0053 1

0.46 0.0093

12.8 loAo !0.030

jQ,Q020

19.7

!PQL

2.0

J 0.10 J 0.200

J

0.10 J 0.0050 J 30.0 2.

1100 I~

~0 50.0 =±£

liD .1o IJ

).200 ).0050 ,~,J 30.0

OlD

MW-17A MW-17A MW-17A MW-17A

IMVV··I f 1\

MVV-1/A

MW-17A MW-17A

IVIVV- -1/ f\

MW-17A

IMW-18 MW-18 MW-1: MW-1:

-11

!DATE

10/1: 110/1: 10/1:

10/1 110/1: 10/1:.-

113/2( )/1~---

)/1: 110/1: 10/1:

13/2(

110/1:

10/1: 10/1: 10/1:

!10/1: ,,1: ,,1:

TE

I U I AL ORGANIC C

IUIAL ZINC



IRESULT IUNITS IMDL IPQL .8 MG/L 0.50 2.0

59.4 IUGIL 135.0 1100 IB I 0267 MG/L 0.0053 0. 0200 ~

MG/LAS LKALINITY, BICARB. AS CAC03 AT PH 4.5 ~IUM

207 CAC03 0.46 2.0 0.0217 MG/L 0.00044 0.0050

lUll

IICAL( RIDE

fOTAL ORGANIC

I (COD)

fOTAL ORGANIC HALOGEN

IKAI

.FAl

. AS CAC03 AT PH 4.5

923 MG/L 32.0 125 I 37.7 MG/L 1.6 8.0 I

MG/L 0.0048 0.0150 J 10.067 MG/L 0.030 0.10 J

~ MG/L 0.0378 10.200

!J MG/L 0.00096 +0.0050 MG/L 0.0020

111

MG/L 9.7 256 MG/L 12.5 922 UG/L 35.0

MG/LAS 11oo IJ

7.5 CAC03 0.46 MGIL 0.00044 0050

4.6 MGIL 0.40 0.25 MG/L 0.030 10.10 IJ 0.0635 MGIL 0.00096

!3.3 IMGIL 10.040 10.10 IJ 19.3 MGIL 6.0 20.0

VED SOLIDS T115 Ml;;/L ~.r ;lU.U 1 IC CARBON -1.2.4 MGIL 0.50 2.0 I

MG/L 0.0053 0.0200 B IIUIAL

NOTE: UG/L =micrograms per liter






ATTACHMENT 1

Memorandum

DATE:

TO:

FROM:

RE:

May 9, 2005

Marc Harder - URS Diamond Jerry Bailey- URS Diamond

Kelly Rinehimer

Analytical Data for Kinston

Enclosed please find the report for the GW SAMPLING-1H05 project.

Please call with questions.

Thanks Kelly

ADQM FINAL DATA REPORT NARRATIVE

Kinston

GWSAMPLING-lHOS

Sampling Dates April4-5 and April7-8, 2005

Laboratories Lancaster Laboratories (Lancaster) Lancaster, P A

Analytical Protocol

Parameterfs) Metals

AlkalinitY Chloride Fluoride Nitrate Sulfate

Total Dissolved Solids Total Oreanic Carbon Total Organic Halogen

Chemical Oxygen Demand 1,4-Dioxane

Site-Specific Volatiles

Sample Arrival & Receipt

Analvtical Method SW846 6010B/7470A

EPA 310.1 EPA 325.3 EPA 340.2 EPA 353.2 EPA 375.4 EPA 160.1 EPA 415.1

SW846 9020B EPA 410.4

SW846 8270C SW846 8260B

The groundwater samples collected for this project arrived at the laboratory intact and within temperature with the following exceptions: o Field personnel did not relinquish the samples listed on Lancaster COC 84889 to the

laboratory with a signature as required. o Field personnel did not sign Lancaster COCs 84888, 84895-96 upon receipt of the bottles in

the "Bottles Received by" box as required. He inadvertently signed on the line below the "Bottles Received by" box.

o The person who signed all of the Lancaster chains-of-custody (COCs) upon receipt of the bottles did not relinquish the bottles to the sampler with a signature as required.

o Equipment blank KIN-K-EQBLK-3 is listed on Lancaster COC 84943 but Lancaster did not receive the sample for analysis.

Significant QC Findings/Comments Overall the data is acceptable for use without qualification. None of the data is considered unusable. Some of the data is estimated due to blank contamination, low matrix spike and/or matrix spike duplicate recoveries, and results reported between the method detection limit (MDL) and practical quantitation limit (PQL ). The DDR Narrative Report lists the qualified samples and the reasons for qualification.

Kelly A. Rinehimer 05/09/05

L--------------------------------· --···

DuPont In-House Review (DDR)

The DDR is an automated internal review process used by the ADQM group to determine if the data is usable. The data is run through this automated program where a series of checks are performed on the data. The data is evaluated against hold time criteria, checked for blank contamination, assessed against matrix spike(MS)/matrix spike duplicate (MSD) recoveries, assessed against relative percent differences (RPDs) between these samples, assessed against laboratory control sample(LCS)/control sample duplicate (LCSD) recoveries, assessed against RPDs between these samples, assessed against RPDs between laboratory replicates, and assessed against surrogate spike recoveries. The DDR applies the following data qualifiers to analysis results, as warranted:

Qualifier Definition B Not detected substantially above the level reported in the laboratory

or field blanks. R Unusable result. Analyte may or may not be present in the sample.

J Analyte present. Reported value may not be accurate or precise. UJ Not detected. Reporting limit may not be accurate or precise.

Lancaster Laboratories Qualifiers

The laboratory may have applied one or more of the following data qualifiers to analysis results, as warranted:

J Estimated value; result falls between method detection limit (mdl) and practical quantitation limit(pql).

u Analyte was not detected at the specified reporting limit

These lab qualifiers are applied independent of DuPont In-House Data Review (DDR) qualifiers.

GW SAMPLING-1H05

DuPont Kinston

May9,2005

Prepared for

Marc Harder- URS Diamond Jerry Bailey - URS Diamond

Prepared by

URS Diamond Laboratory Services - Kelly Rinehimer

Barley Mill Plaza, Building 27 P.O. Box 80027

Wilmington, DE 19880-0027

Site: KIN- KINSTON Project: GW SAMPLING-1 HOS

Reporting Limit: MDL DDR Standards LABSTATS

Corporate Environmental Database DDR Narrative Report

5/9/200516:17:23 Page 1 of2

Contamination detected in Equipment Blank(s). Sample result does not differ significantly from the analyte concentration detected in the associated equipment blank(s).

Sample 10

KIN-G-MW-14 KJN-G-MW-14 KIN-G-MW-18

Date Lab Method Sampled 10 Code Analyte

4/4/2005 4495852-TOC I 415.1 TOTAL ORGANIC CARBON 414/2005 4495852-FE FS 60108 IRON 4/4/2005 4495857-TOC I 415.1 TOTAL ORGANIC CARBON

Result

4.0 0.231 3.2

Units

MGIL MGIL MGIL

MDL POL Qual

0.50 2.0 0.0495 0.200 0.50 2.0

B

B B

Contamination detected in Method Blank(s). Sample result does not differ significantly from the analyte concentration detected in the associated method blank(s).

Sample ID

KIN-G-MW-13 KIN-G-MW-14 KIN-G-MW-15 KIN-G-MW-16

KIN-G-MW-17A KIN-G-MW-17A-DUP KIN-G-MW-18

Date lab Method Sampled ID Code Analyte

4/4/2005 4495851-HG F! 7470A MERCURY 4/4/2005 4495852-HG F! 7470A MERCURY 4/4/2005 4495853-HG F! 7470A MERCURY 414/2005 4495854-HG F! 7470A MERCURY 414/2005 4495855-HG H 7470A MERCURY 414/2005 4495856-HG F~ 7470A MERCURY 414/2005 4495857·HG F~ 7470A MERCURY

Result Units

0.000065 MG/l 0.000091 MG/l 0.000091 MGJL 0.000091 MGJL 0.00012 MGJL 0.00011 MG/l 0.000091 MG/l

MDL PQL Qual

0.00002E 0.00020 B 0.00002E 0.00020 8 0.00002E 0.00020 8 0.00002E 0.00020 B

0.00002E 0.00020 8 0.00002E 0.00020 8 0.00002E 0.00020 8

The reported result is greater than/equal to the MDL and less than the PQL; it should be considered an estimated value.

Sample ID

KIN--G-MW·10 KIN·G·MW·13 KIN-G-MW-13 KIN·G--MW-14 KIN·G-MW-14 KIN-G-MW-15 KIN-G·MW·15 KIN-G--MW-16 KIN-G--MW-16 KIN·G-MW-16 KIN·G-MW-17A KIN-G-MW-17A KIN-G-MW·17A KJN-G--MW-17A·DUP KIN-G--MW-17A·DUP KIN-G--MW-17A·DUP KIN-G--MW·17A·DUP KIN-G-MW-23A KIN-G-MW-35 KIN-G-MW-56 KIN·K·EOBLK-DAY1 KIN·K·EOBLK-DAY1 KIN-K·E08LK-DAY1 KIN-K·E08LK-DAY1

Date Lab Method Sampled ID Code Analyte

4/512005 4496563--1 FS 8270C 41412005 4495851·ZN F~ 60108 414/2005 4495851-COO I 410.4 41412005 4495852·F FS 340.2 414/2005 4495852-COD I 410.4 414/2005 4495853--TOX F 90208 414/2005 4495853-COD I 410.4 4/4/2005 4495854--TOX F 90208 414/2005 4495854-COD I 410.4 4/412005 4495854-CD F~ 60108 4/4/2005 4495855-F FS 340.2 4/4/2005 4495855-CR F~ 601 DB 41412005 4495855-CD F! 601 OB 414/2005 4495856-804 F 375.4 41412005 4495856-F FS 340.2 414/2005 4495856-CR F~ 60108 414/2005 4495856-CD F~ 60108 415/2005 449657 4-1 FS 8270C 417/2005 4499832-1 FS 80218 4/5/2005 4496576-1 FS 8270C

1,4-DIOXANE ZINC CHEMICAL OXYGEN DEMAND FLUORIDE {DISTILLED) CHEMICAL OXYGEN DEMAND TOTAL ORGANIC HALOGEN CHEMICAL OXYGEN DEMAND TOTAL ORGANIC HALOGEN CHEMICAL OXYGEN DEMAND CADMIUM FLUORIDE (DISTILLED) CHROMIUM CADMIUM SULFATE (TURBIDIMETRIC) FLUORIDE (DISTILLED) CHROMIUM CADMIUM 1 ,4-DIOXANE CIS--1 ,2·DICHLOROETHEN E 1 ,4-DIOXANE

4/4/2005 4495861-TOC f 415.1 TOTAL ORGANIC CARBON 4/4/2005 4495861-HG El 7470A MERCURY 4/4/2005 4495861-FE EE 6010B IRON 414/2005 4495861-ALKP 310.1 ALKALINITY TO PH 4.5

Result

2 0.0053 33.2

0.085 11.4 58.1 47.8 43.1 35.6 0.0011 0.062 0.0039 0.0027 9.0 0.059 0.0038 0.0023 2 0.2 4

Units

UG/L MG/L MG/L MGIL MGIL UG/L MGIL UG/L MG/L MG/L MG/L MG/L MG/L MG/L MGIL MGIL MGIL UG/L UG/L UG/l

0.84 MG/L 0.000079 MG/L 0.107 MG/L 1.7 MG/l A

MDL PQL Qual

1 5 0.0048 0.0200 9.7 50.0 J

0.030 0.10 J 9.7 50.0 J 35.0 100 J

9.7 50.0 J 35.0 100 J 9.7 50.0 0.00076 0.0050 J

0.030 0.10 J 0.0025 0.0050 J 0.00076 0.0050 J 3.0 10.0 0.030 0.10 J

0.0025 0.0050 J 0.00076 0.0050 J 1 5 J 0.2 0.5 J 1 5 0.50 2.0 J 0.00002E 0.00020 J 0.0495 0.200 J

0.41 2.0 J

Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit but above 10%. The reported result may be biased low.

Sample ID

KIN--G-MW-13 KIN-G-MW-17A KIN·G--MW-17A-DUP KIN-G-MW-18


41412005 4495851-NOON 353.2 4/412005 4495855-COD I 410.4 41412005 4495856-COD I 410.4 414/2005 4495857-N03N 353.2

NITRATE CHEMICAL OXYGEN DEMAND CHEMICAL OXYGEN DEMAND NITRATE

Result

0.28 977 919 1.8

Units

MG/L MG/L MG/L MGIL

MDL

0.040 19.4 19.4 0.040

PQL Qual

0.10 100 100 0.10

J

J

J

Site: KIN - KINSTON Project: GW SAMPLING-1H05



5/9/200516:17:23 Page 2 of2

Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limil The actual detection limits may be higher than reported.

Date Lab Method Sample 10 Sampled ID Code Ana lyle Result Units MDL PQL

KIN-G-MW-14 4/4/2005 4495852-N03N 353.2 NITRATE < 0.040 MGIL 0.040 0.10 KIN-G-MW-15 414/2005 4495853-N03N 353.2 NITRATE < 0.040 MGIL 0.040 0.10 KIN-G-MW-16 4/4/2005 4495854-N03N 353.2 NITRATE < 0.040 MGIL 0.040 0.10 KIN-G-MW-17A 414/2005 4495855-N03N 353.2 NITRATE < 0.040 MGIL 0.040 0.10 KIN-G-MW-17 A-DUP 414/2005 449585S.N03N 353.2 NITRATE < 0.040 MGIL 0.040 0.10

Qual

UJ UJ UJ UJ UJ

Corporate Environmental Database

Lab Analysis Report Summary of Positive Results with In-House Qualifier

Site: KIN- KINSTON 5/9/200516:18:31

Project: GW SAMPLING-1H05 Page 1 of6

Reporting Limit: MDL

In Lab House

Analyte/Parameter Result Qual Qual Unit MDL PQL Method

Sampling Point: BW-1 Sampleno: KIN-G-BW-1

Date sampled: Apr 08, 2005 Sample type: Groundwater

Cl$-1 ,2-DICHLOROETHENE 780 UG/L 20 50 80216 TRICHLOROETHENE 3000 UG/L 20 50 80218


Date sampled: Apr 08,2005 Sample type: Groundwater

Cl$-1 ,2-DICHLOROETHENE 53 UG/L 2.0 5.0 80218 TRICHLOROETHENE 480 UG/L 2.0 5.0 80218


Date sampled: Apr08,2005 Sample type: Groundwater

CIS-1 ,2-DICHLOROETHENE 24 UGIL 1.0 2.5 80218 TRICHLOROETHENE 200 UG/L 1.0 2.5 80218

Sampling Point: 6W-4 Sampleno: KIN-G-BW-4


CIS-1,2-DICHLOROETHENE 180 UG/L 10 25 80216 TRICHLOROETHENE 2600 UG/L 10 25 80218

Sampling Point: BW-5 Sampleno: KIN-G-BW-5 Date sampled: Apr08, 2005 Sample type: Groundwater

TRICHLOROETHENE 2.4 UG/L 0.2 0.5 80218

Sampling Point: EQBLK-DAY1 Sampleno: KIN-K-EQBLK-DAY1

Date sampled: Apr 04,2005 Sample type: Blank Water

ALKALINITY TO PH 4.5 1.7 J J MG/L AS CAC03 0.41 2.0 310.1 TOTAL ORGANIC CARBON 0.84 J J MGIL 0.50 2.0 415.1 IRON 0.107 J J MGIL 0.0495 0.200 60108 MERCURY 0.000079 J J MGIL 0.000028 0.00020 7470A

Sampling Point: MW-02 Sampleno: KIN-G-MW.()2 Date sampled: Apr 05, 2005 Sample type: Groundwater

1.4-DIOXANE 11 UG/L 5 8270C

Sampling Point: MW-10 Sample no: KIN-G-MW-1 0 Date sampled: Apr 05,2005 Sample type: Groundwater

1 ,4-DIOXANE 2 J J UGIL 5 8270C

Sampling Point: MW-11 Sampleno: KIN-G-MW-11 Date sampled: Apr OS, 2005 Sample type: Groundwater

1,4-DIOXANE 150 UG/L 5 24 8270C

Corporate Environmental Database Lab Analysis Report

Summary of Positive Results with In-House Qualifier

Site: KIN- KINSTON 5/9/2005 16:18:31

Project: GWSAMPLING-1H05 Page 2 of6 Reporting Limit: MDL

In Lab House

Analyte/Parameter Result Qual Qual Unit MDL PQL Melho<l

Sampling Point: MW-13 Sampleno: KIN-G-MW-13


TOTAL DISSOLVED SOLIDS 189 MG/L 9.7 30.0 160.1 ALKALINITY TO PH 4.5 40.6 MG/L AS CAC03 0.41 2.0 310.1 CHLORIDE (TITRIMETRIC) 18.7 MGIL 0.40 2.0 325.3 FLUORIDE (DISTILLED) 0.14 MGIL 0.030 0.10 340.2 NITRATE 0.28 J MG/L 0.040 0.10 353.2 SULFATE (TURBIDIMETRIC) 62.3 MGIL 3.0 10.0 375.4 CHEMICAL OXYGEN DEMAND 33.2 J J MGIL 9.7 50.0 410.4 TOTAL ORGANIC CARBON 9.5 MGIL 0.50 2.0 415.1 BARIUM 0.0214 MGIL 0.00045 0.0050 6010B MANGANESE 0.0200 MGIL 0.00084 0.0050 6010B

ZINC 0.0053 J J MG/L 0.0048 0.0200 6010B MERCURY 0.000065 J B MGIL 0.000028 0.00020 7470A

Sampling Point: MW-14 Sampleno: KIN-G-MW.14


TOTAL DISSOLVED SOLIDS 233 MGIL 9.7 30.0 160.1 ALKALINITY TO PH 4.5 59.1 MGIL AS CAC03 0.41 2.0 310.1 CHLORIDE (TITRIMETRIC) 15.0 MG/L 0.40 2.0 325.3 FLUORIDE (DISTILLED) 0.085 J J MG/L 0.030 0.10 340.2 SULFATE (TURBIDIMETRIC) 84.5 MGIL 6.0 20.0 375.4 CHEMICAL OXYGEN DEMAND 11.4 J J MGIL 9.7 50.0 410.4 TOTAL ORGANIC CARBON 4.0 B MGIL 0.50 2.0 415.1 BARIUM 0.0092 MGIL 0.00045 0.0050 6010B IRON 0.231 B MGIL 0.0495 0.200 6010B MANGANESE 0.0071 MGIL 0.00084 0.0050 6010B MERCURY 0.000091 J B MGIL 0.000028 0.00020 7470A 1.4-DIOXANE 5 UG/L 5 8270C



TOTAL DISSOLVED SOLIDS 606 MGIL 19.4 60.0 160.1 ALKALINITY TO PH 4.5 494 MGIL AS CAC03 0.41 2.0 310.1 CHLORIDE (TITRIMETRIC) 21.2 MGIL 1.6 8.0 325.3 FLUORIDE (DISTILLED) 0.17 MGIL 0.030 0.10 340.2 CHEMICAL OXYGEN DEMAND 47.8 J J MGIL 9.7 50.0 410.4 TOTAL ORGANIC CARBON 12.2 MGIL 0.50 2.0 415.1 BARIUM 0.0140 MGIL 0.00045 0.0050 6010B IRON 41.1 MGIL 0.0495 0.200 6010B MANGANESE 0.241 MGIL 0.00084 0.0050 6010B MERCURY 0.000091 J B MGIL 0.000028 0.00020 7470A 1.4-DIOXANE 150 UGIL 5 25 8270C TOTAL ORGANIC HALOGEN 58.1 J J UGIL 35.0 100 9020B



TOTAL DISSOLVED SOLIDS 298 MGIL 9.7 30.0 160.1 ALKALINITY TO PH 4.5 240 MGIL AS CAC03 0.41 2.0 310.1 CHLORIDE (TITRIMETRIC) 13.0 MGIL 0.80 4.0 325.3 FLUORIDE (DISTILLED) 0.17 MGIL 0.030 0.10 340.2



Site: KIN - KINSTON 5/9/2005 16:18:32 Project: GW SAMPLING-1H05 Page 3 of6


In Lab House

Analyte!Parameter Result Qual Qual Unit MDL PQL Method



CHEMICAL OXYGEN DEMAND 35.6 J J MG/L 9.7 50.0 410.4 TOTAL ORGANIC CARBON 8.7 MGIL 0.50 2.0 415.1 ARSENIC 0.0190 MG/L 0.0047 0.0100 60108 BARIUM 0.0101 MG/L 0.00045 0.0050 60108 CADMIUM 0.0011 J J MG/L 0.00076 0.0050 6010B IRON 5.98 MG/L 0.0495 0.200 60108 MANGANESE 0.216 MG/L 0.00084 0.0050 60108 MERCURY 0.000091 J B MG/L 0.000028 0.00020 7470A 1 ,4-DIOXANE 86 UGIL 5 8270C TOTAL ORGANIC HALOGEN 43.1 J J UG/L 35.0 100 90208

Sampling Point: MW-17A Sampleno: KIN-G-MW-17A


TOTAL DISSOLVED SOLIDS 550 MG/L 9.7 30.0 160.1 ALKALINITY TO PH 4.5 228 MG/L AS CAC03 0.41 2.0 310.1 CHLORIDE (TITRIMETRIC) 53.8 MG/L 2.0 10.0 325.3 FLUORIDE (DISTILLED) 0.062 J J MG/L 0.030 0.10 340.2 SULFATE (TURBIDIMETRIC) 10.5 MG/L 3.0 10.0 375.4 CHEMICAL OXYGEN DEMAND 977 J MGIL 19.4 100 410.4 TOTAL ORGANIC CARBON 326 MG/L 12.5 50.0 415.1 ARSENIC 0.0160 MG/L 0.0047 0.0100 60108 BARIUM 0.0101 MG/L 0.00045 0.0050 60108 CADMIUM 0.0027 J J MG/L 0.00076 0.0050 60108 CHROMIUM 0.0039 J J MGIL 0.0025 0.0050 6010B IRON 17.2 MGIL 0.0495 0.200 6010B MANGANESE 0.346 MGIL 0.00084 0.0050 6010B MERCURY 0.00012 J B MGIL 0.000028 0.00020 7470A TOTAL ORGANIC HALOGEN 49900 UG/L 3500 10000 9020B

Sampling Point: MW-17A Sample no: KIN-G-MW-17 A-D UP Date sampled: Apr 04,2005 Sample type: Groundwater

TOTAL DISSOLVED SOLIDS 544 MG/L 9.7 30.0 160.1 ALKALINITY TO PH 4.5 227 MG/L AS CAC03 0.41 2.0 310.1 CHLORIDE (TITRIMETRIC) 55.4 MG/L 2.0 10.0 325.3 FLUORIDE (DISTILLED) 0.059 J J MG/L 0.030 0.10 340.2 SULFATE (TURBIDIMETRIC) 9.0 J J MGIL 3.0 10.0 375.4 CHEMICAL OXYGEN DEMAND 919 J MG/L 19.4 100 410.4 TOTAL ORGANIC CARBON 323 MGIL 12.5 50.0 415.1 ARSENIC 0.0166 MG/L 0.0047 0.0100 6010B BARIUM 0.0098 MG/L 0.00045 0.0050 6010B CADMIUM 0.0023 J J MG/L 0.00076 0.0050 6010B CHROMIUM 0.0038 J J MG/L 0.0025 0.0050 6010B IRON 16.8 MG/L 0.0495 0.200 60108 MANGANESE 0.345 MG/L 0.00084 0.0050 6010B MERCURY 0.00011 J B MG/L 0.000028 0.00020 7470A TOTAL ORGANIC HALOGEN 34800 UG/L 7000 20000 9020B



Site: KIN - KINSTON 51912005 16:18:32

Project: GW SAMPLING-1H05 Page4of6


In Lab House

Analyte/Parameter Result Qual Qual Unit MDL POL Melhod



TOTAL DISSOLVED SOLIDS 124 MGIL 9.7 30.0 160.1

ALKALINITY TO PH 4.5 35.7 MG/L AS CAC03 0.41 2.0 310.1

CHLORIDE (TITRIMETRIC) 4.9 MG/L 0.40 2.0 325.3

FLUORIDE (DISTILLED) 0.13 MG/L 0.030 0.10 340.2 NITRATE 1.8 J MG/L 0.040 0.10 353.2 SULFATE (TURBIDIMETRIC) 48.2 MGIL 6.0 20.0 375.4 TOTAL ORGANIC CARBON 3.2 B MGIL 0.50 2.0 415.1 BARIUM 0.0253 MG/L 0.00045 0.0050 6010B MANGANESE 0.0279 MGIL 0.00084 0.0050 6010B MERCURY 0.000091 J B MG/L 0.000028 0.00020 7470A



1 ,4-DIOXANE 6 UG/L 5 8270C


Date sampled: Apr05, 2005 Sample type: Groundwater

1 ,4-DIOXANE 65 UG/L 5 8270C



1 ,4-DIOXANE 1700 UG/L 20 99 8270C

Sampling Point: MW-22 Sampleno: KIN-G-MW-22-DUP


1 ,4-DIOXANE 1500 UG/L 19 96 8270C



1 ,4-DIOXANE 2 J J UG/L 5 8270C



1 ,4-DIOXANE 6 UG/L 5 8270C



TRICHLOROETHENE 1.0 UG/L 0.2 0.5 8021B


Date sampled: Apr07, 2005 Sample type: Groundwater

TRICHLOROETHENE 2.5 UG/L 0.2 0.5 80218

r1es ·z~'i.., 1 <~J$0 '17 /'1...;'7-nn:~" ~ - ~o. s4a75 . ,-. -~--~....... . ...... ~'"'"-··-'-·'··· . . ~ .............. . 12..:25. L .... ster, PA 17605-2425 . . . .. .• -- .. ··- . ~- 7-mOIJ(Y' · ..,__

• ~

""*"'~ ~ar T · rHame·

Address

~ci'J!ISupwl!io<~ .·. · :.r SAMPLING-1H05. lt~:t --. - . - ... . ,;

.(~. t,Ji /t5U~ -Ill{. ' .-·

lot~~« Em_l_a l.· ~- pBlo .. iiie, i;ainple···· fil""l'_. ·. .•• .·. ~ily. ~f!it ox ~liOn · YP81- II""J, . .:;: · . JPe · ' . (JM.G.MW.I~ . . . WVY •I. s$ ,. 2 B ' • .

· · · . _,,. . •t . ;~r . · , . . 1 r .1 .1 ' : ... -' ·:~·;J ' ' .· .. , •':·1. _l

.:· ( . A " • c,·',;., i.: .· ;:,·,,' I·LJ.I: I/. Mn.--- ~6-,c, l'lo<, ;• :~i.,&;tedw£.,Qx,.-._._, • DcteJr ... I.[( I/~ Con ..... ofS-:-Unon~l;atl'ilal .. n r,,

Rein<M~Jed ~ ~ Dillefnme't-~-Of·\?CIII . I !Pi·--......... Date/T'~ \~;,.._j_ I~ · ·· · ~-~ . R ~- ' . • -............_ --....., , o(SU!ples \in Arr1vll /. C..0 c 0

R .···•· .. I bY ~ Dattmm~ . ":"< ~(. u ~i,_, ~ ,_ Dalell'lme :'#-S.Ji>~. 11 n rjl,t' }11'),,. loate u S ' -.... . . . __ ,.. 'J . ... . . u ·u . u 4t l

.. ,

(!oi?.p . '

; . :~;·· ·,,. . . '

if· " -~ ;;

·-·

'" ..-:

'i.:

···i :;l

,,- -----. ~-~.,..----~----, - No. $4888 ~ "'~ '3/ "3 8<N? I 'f¥'1$"5 n- r.. '-1

~-- 12 -- h2(}1i31e, ~..__._- . tT'?35-:o!!N720QO t ... ·-· b,.oa ~rl!i · hoM~ .

ighway 11 North Spot 21 g Kinston NC fagay Addren

:.·,to ·, T iit Nurnhat',. .........

-""" ··)

arc H•"'ler

~1 ; N03(353.2);

,,, ~~ii~-1H06 . . . . ~:~~=:.. I fProe.•• Pmcb*lg Sa::!;m~pltL,-:--,--;---'---,,---+- r:: .

~1;,..~t,, J k_, n.l'---~L I Special S!!DpinR I ;r,Cu,Fe,Pb,Mn,~,ny,~ Jlutl); Hg; i•F.t

~ ".d_l~ 15.11- COI'ill-410 "'

IOthor E . 'T'C

:\ U.ntlin !',

Jg!:n plate ime ample f'/oitHne PresOiYollie lQiiiliity llOfUe ype mQ • I _jfYP<

~ p lXV 1'- IM"IOOS roo fO.' fDS roc = ~20 .H3P04: t.• : Will,. H · Will . '

..... .,w.13\- -- WN 1 , .. _,,. -· 1-G-I\IW-1 :t . ·•;.. - WN Nario 1. P llCc •. ·

.· ', . :, i . . · .. ·

bt IX IX IX·''

. '\· '" •, ..•

' "' I ~ Bott~R :. 1tsi'/!'.'X .:A.' ~~Y;."~-~~ · ·'. me ..-of \JponanlvalatFlRoltle~-

- heolbv i;...o 'l£1'60: . . ~ '-i 'J'.t/!1'$ '-· ' •elibv ~ l.{A/()_j__ ( "' l I' .J. · i. '• '--.... - '"" 1'&,' ~ .. · . . . ... ~ a

o.tefTit1e · -~ ~ emp. of San1>\es on Armllol · • C

-~- dirt ---..._,Dalefrlme ~- ~~.; ~ ~ Cb,.._ lo.wrme 4'"5'.:;>abJii~e a~ 'J).,~ ~ Oo1l.ltJ..J-.l:)~~-{b ?Y&l,.. o u ~ ·· · a .,.. o ~

-~:

~.

··.-~--·--- -L . . .. . . {pfoLJ.3)"1~~o·o/'tYtf:>BS7-~~---. - . . :. -·· .. "'·~-- No. 84876 . ~- Lanc;a$r LaboJftorla... c .....•. ... , __ ., . . . . . .. ··~ r._201658 :· , 111 . 7-r"~ . 2425NowHolandl'b.PO 12425.1Jinoastor,PA1760S..2425 . . . · ~

. puPont Kindan Plant . Fr04..362-6825 : '.} . fader>ol !Oxpress I_ • . . FaclltvNamo T-•- ' 1i · Nome . Highway 11 North Spot 219 Kinslbn N() 28502,oeop, .

Fll<illly-s . . . T.......,.ner Addroft ·

Marc Harder . s Saver Fullilv ,· Molll!!!f_of~ ··. .·

GW SAMPLING-1H06 I· ProeeSs Produclno Sample . ' ... I Spedal SlippWJg

r~. sl8amolllo G-&r:·l 'K".stJ-. ; ' '

Olhor loHiandlina,

omplo pete im~f am~ it ~ai!Ye. P-'Y ['Ollie ox '¥ JPO (1!1{ . JPO

I(IN-G-IIW-14 lY'lS WN F ~ 2 Llf • .

' : .,' .

I\ aottO .f.t . . I tD L . ;;>_~ "5'"'0~ sR..i.ed..<ig...J ,... ... ldal;ol[~ '1" (at' ~ . Uioon ·-., .... 1 Dostinolion

RolnQtdstoed~~ Oat :u-'t-of- noo R~lJY.,·'-......._ ~~ .

.l I _t

R~ohe<ibv"--., DlleiTine ~ R..etvedbv --- Date/Tine --......

l'""J': Df S8mpleS .. - --~ c•

R ~- Datemne ....... w,. 1\ ~(),,; oatenime '+--s~ li _Lf\ ~ lo.te Ll. '" . '.'~·: u u .~ . u u

'"·' d£1 ... ,. ".· ,.,

C. a /?:. r7 . ' -

.. '

... -·. .. -·-

~--

:?

.. .: . , r,A'fi~)"iJ'&t:Y:{?ft{'!:'!!fJI!:..~t .. ~-· ..c ;,;..,.., • · _ ... ·" . ' r ·· .,-. ··· . . - . :

r~; , .. ;. ___,__ na.-;:(,"J8QS:,d"· ·~·~1::.(/ . . . '. ··'

.s62..tll25 ederal ~" T..,. __ ........ _.._

1NC

rc Harder

~- ....

- ' -··-~or~ .4\·

I' f '·

Other

[ 'J --·.,. J, r :c

· L·· ', 1· . I 1· f . r- ··r

p p

,.-. -; saver

I Special !l!!pP!ns lnotnf!lon! .· .· · . . · . f ;r,Cu,F&;Pb,Mn,5e;Ag,Zn{3030C/6010B); H!i Cl-(325.3); F-(340.2); N03(353.2);. "'i.1\: Cbol410.4f.

oc

-·f.

IBottleoMO!ifWdbd[\j{~ 3·..l~---~¢·'><h·~ /I0¢·1§o!!eoR~~J:i ~~'tlJA.:--L - ''· ~£: .· . ,,~ ~M45-IS<nR..;;.w..J

• Upon an1vol f ( n~r..\--,

,, ,,

w-M'"':' ~lq~ d - ~.- Do =i.t~ b'), Date ·4¥6is ·. ~

.i 'i ..

b' '{ 3h 3 SDY7/Y!f7~8J/- b'(

'• ~ -

No, 84877 ' -~-- •--~- -·- -:~-,-;~!!_·;•""'-: r.20~ ~ I= ,,12000 -

,.;;,

;;;";;!";:,.; ~-;;;;.::;;~:-;;~; PA 1 .. 242;- • - . . . - tlbmer puPcnt K\nclon Plant . ~?4-36U62S . fadilritl Expres;~ I. . ' Foe , retep~Jono lllmber T..-_er~-'"'ighway 11_ North Spot 219 Kins~ NC 28502cOBOO' . Faa.yAd<hM , lr~..--·.

Marc Harder . ~pre$s saver · -··· ~-...

Molhoclof-.

GW SAMPLI . -!:: • I S!>edal SliDPlng I Proceot Pr<>G~omi. sa ·

s ,G. l a_d ilL be:<· .. ..., ' . . .. '· .'\

Other . ·--~)-..,. _.: _·

~-- pate ~ ampllf !"""!"• f"'W'al'ie F"''Y f>OI1Ie ox

~5 ... ype . (IIJ!' ype

'(•Y ... S ww 25CI .· S04JNa2 a 8 ,,.,

< - ' . .

... :· ·,

. ': ··- . f·::i ·' . - . ' __ [_[{'. . ~~-:>. . .Yr ~9!JY" 8olllos Re - · .r.:._&_.~ l ... lu.wf-..,. tJ ll df' sllDorurriwll at Filii · - - ·

~ed...r:. ~'IlL. ~·14irr--~~IMF noo RICI!illedby~ · Dat~ 'i 0\-1-er.+. . . ~

R~edliv- Da~~ R~by ~ oatemne --........ tre!l)p. or SIQ1llet onAn1val ) .;:[ c 0

R diN "--' D~o -~ I.CUU.O ~lf: b •• Dale~Rno~~~- JL" '-'l .=:RC £ Q, ":.Joat1:4-_5_--oS'.

'-

t~l2 '?7 f ·f:

i· ...

__ ,·~-~-

j ;

i I I I I I

~ I

··.--··--··

'~~·~~~h1'60'{(/'-f'-lt:f'JBJI-b'l . No. 84890 . ·-- . ···.····· . ..·. . . . ~- ··g:.;;, t;:~·:: .- , ·. ·-·-- l=::f-mooo- . -" .625 ' ~ederal Express . ' . r e Nwnber ~---..- ............ T .. llu!.liNur. .,._. ·

-·· ···-·-

'· PA 171105 k12425

.g, ~ Spot'219; KinstOn Nc .... .........__ __ ' . .

jMai\1! Harder · ~

1- .- s saver . ll.u..d

orrooess.rn~i.~~ 1~ ],~~~haJ• j

r. . " ' . ', -

Olhor E w• •:: I ' ' . f•• 'pie Dsl" . •- olhno '" •- "'~' Rnlllo LO.I< n "'"OC" JM•'·" •-· . "-· ~ --- ' I' ~ 1m• ~:c·· ... ;? creser<a.~ ,,_.lily :-· I . r-- ~- · , _ _, · ·---- .... ·-- · · --

3-Mw. 3-Mw. ~ ~

--

ype '""' .·. ype ,, I I I

I'" . /0) "' v. ~. ... = : e. . --t -L !Oro.. H2S04 . ···. 1 B ·

., 01)·. HN03- 1 . B ~ I 1 None 2 P X X

,.. Nona 1 · P I I I

l' I> .• I.. . I I I I I I I · .. : .

_,...,....,.....__,....._ __ ..___,..___. _ __...___. _ __. __ ., .. tl.,., .... '' IM~ .. ~ JIIJ ll!oltlosRocoiWod""':q__L- ···I 'I I,. ( I I I 'I =r r·--T"k ~t=a='::-¥2!!N!~~Y!s!!!!!.!~~~t..,-~~~-=--~~~~~E!!!!.!!!!!!:!!.!!!!~··

~~~~

tn?~9-c

Q co

1 ~ . . \(A !; t-1$'-t&l' . ~-Q~ttidDatelf; 't§,~=s~a~q. ~ · .u.3 · ,. · \,...) 0 '

'

Lancaster Labo~rles· ' ... 2426NowHolllndPice. PO 1if26.L@· "· "'~'"" .. ;.. -~

{§(,q3/ •nso~n/4'i9t8SJ-to.'t· .·,, • ·. ~ No: 84878 . . . - .. .... ..... .. . .... #E· p201~ -~~.,..mooo ·1 . /\ .. - . OrderJri -.. --~- ·,: Prnia.ot u. ...... ~.. . ~--:· -~--~uPont Kinston Plant · · ·;': FacRvNa~n• ·

~•gnway 11 North Spot219 Kin$ton NC :.!H:>U"L·UOOO Facilly Address · . · ·

arc Harder · · ·

I§VV: I Process.

_1-11-tUb ~.~.

I Stamnt.

.r,_2_J .... I ¥1<.l/l· ·. !CIIhet EIIIDio,..o/ol Holldlina

'----·- ~...,-~

L .•. p-pru~SaYer I U.thod J 01.

[-IShlliDinal-

~ox

.....

5~1& F~;~~~~m•\;:s€~~ I I ~ ... ·I · ' · -. ·•·I I· I I I I I I I I I II --

I I ..

e.t·::fib~ T A.·· .. ~ ~:J•~~~ t1qJ;;= L L=:::E~ I · ··· - .......... loA~. f:; ·· ·· I I . 1· -- _ I I · I·

~~r-~~ ~'::it-·;:=·:,;;_ I L.~ts:~ t='s: lm C Hen · 4i13ciiti L:: "7-oc~-E._.... 1-E , . 9:J i1? la. I ob oateLJ-s 1}S" I

-=IJ.(

'f:'

--.. __ __,_, ·•lt l:

No. 84891 Lanouter La · tdr!U,) .· ' ·~- - (.,(o '13/ ~ ~f$_0" ![l.f'-l7.) .JJ I• bY .; .. ·' t.;:; P-_20'1656":· - -- ,~·- 1. 7()35i604337-772000 2425 NaW Hlflnd Pi<o. PO 12425. i1i6ster, PA 1780i-2425 . · · · . ' --'-DuPont l(j,..ron Plant ' ' . Fr04-36Ul62!i:- ' . ""ederal Exp~

. I. Faciltv loi.mo · Telel)hono Nwnbor · · Tratl$11li!ru Name olUnb<tr -Highway 11 North Spilt 219 Kinston NC 28502-0800

Transporter AcldreB~ FocilityAddren •·

Marc Harder .. · "'xpress Saver Faeillv .. , IMelt>odot Sliooila GW SAMPUNG-1HQI?. ProcHs p.-.duclnQ SIII!'Oit . I~'" IMiruoiiO!IS

.•.. G. tJ.... I k_ i'S~tJl- ~~rs=As,Ba,Cd,Cr,Cu,Fg&~n,Se;Ag,Zn 41375.4\: TOCi41S.1i; ·· 410.4f ·

108); Hg; Cl-(325.3); F-(340.2); N03(353.2);

. :·. ' -- f •. . . . -0t11er E ·- w IS"""*' . .. palo ' . rnm• ample- ollme "'"'""lllivo ~ ~ p- poo ,..Ills f"'l' fAA ·'"' oc .

. .. ype

'"' KIN-G-MW-16 I 'I~ WN 120 H3P .1 B KIN-G-MW-111'· - WN 0 H2S( ~;. , . . f .. v

. ' KIN-G-Mw:t WN 1000' H2SC 1 a: Klli-G-Mw: 1 WNI HNC • t· B Klli-G-MW-1 WN 1 NOn 2 p KIN-G-MW- 3 >.--. ~ WN """' '

1 p

'

I :1 LIJ fJ ,>_, ~'{.,t I J}•(J. ra;.. Reeoled -~ (L ·]...., . Dale/Tint 4 ,, oS of ' Ibm llfl'ival at FNI Deotlnallon

R .~Y bl.VL "-'l-os~ t7MI- L - lb!!"-.. ' loaeJT~~~e >......_ .'ut::Lk~ :t::_

ReliQislled~ .::..' Rk•l'tt~Lb!! ~ 0 ~ fremp. of Samples an AnWil ,; .. c 0.

Re~Liished bv ......_.,.__ ' DBtetrm" ~ Jll'l. .. 1-0 :\R.;: .. ___k_ 0 n Dat~'::s1:1:~~ v. Jl . 1), {_,.~ ll o.IJ-5--os:. \_) L - \j u

Co ?9$)L 3 ,,

I

j

,/. . .. . - ' - : . -~- No. 84879 , Lane:* Labol)tories .. ·... '""...-. J;pl_.f!3/'1 380~l,':Llf~.r~[;.'f;;t ·_·_.· ·-~~~ ~~-··· ... -~I~?:: 7-·7lifl:ll'"-;r .·

2425 Ntw iuf!l Pb. PO B~if:12425. Lancoster'• PA 171105-2425 · · · : · · . ·,. c . r 111 · . ;<., litmm.r , : puPont Kinston Plant f104-362;8625 .. F""-rat Exp"'* · 1. . . . . · ·• · ·

. Facllv ,.,.,.,. . . ITel!ll!!!!!!!_ Number " r ... Mm.t ... Name. '. '-'"'ighway H. North Spot219' Kinmn NC 26502-0600 · ' FeclllyAdchu · Adchn

,':'v

~"!arc Harder· · · ~ress Saver ,, IF•ollll. · . , . Method of Slliooina · _:_

1 JGW SAMf>UNG-1H05 . . . . . . ' ·• Process Pro'*'CinQ Somple ·1 ~tsw-tn~

eii!PICYYIII$) G. 6« ~ l{'Y / ~·;~ <\W t . · · · I

·Other 'ol"'""""'

~. ·. pate . ime. . !"ample ....,. r-v- r-'lily r;::._ ve_ . ox ~~- ~ ~ r~~-KfN.G. I 'f· Wi'l 50M'Ia2 2 · 8 KIN-G-MW-17A- ___ .-,. Wi'l 511" SOMNa2~ 2'' . B

;.·· ....

. . .. f ' £ . ' '

l .lk./J r.t "- l~aU:o5" 09-!tS liri>tues Received rnh l>,. ;\<>.. D~ollP .Y J!/G't"' Condllon of Samolesll>on IITivalat Alai n

' R~cl:.f ~ o.teJr.ft-lf-o.t -17cW ~.ceived by----.... ( llltell"q~ I Vl-h-1 (' -1-; R ·' ' · "'- llalelTme~ Rec!!MdllY -.........__ llltefllne "" lr~;ofSIJrf!OsanAntlal _l ..5': C 0

' R f . ' "-....., oatetnne ~ Re_l/ll.lil '12 • • • H.1 Ji.emne ~~~~"' "· -0 -:P.,' . k.Oo 11at · 1 • r-

' l• • . G· . \J . ' U .~.....- -.Jt.l

C~;rar

:,:·-

.. ···...:-··---~-·---. --.

... LanGaster L!borl!torles. c, .. 'e'?"J/"7386_~7Lt.t_Y'7f8JI-fof.(_ ... ,~;.,. ~658"·''.· ~· 84813 ··- -r~ 4337- .-r~ ~~-·-·

2425 Newliollnd Pke. PO llali12425. La,.,.stor, PA 17605-2125 ·. . win . tbber ., puPont Kim;lion Plant . ~?'*-362-6625 fedenal Express

IT •

F~Nomo TailoollonoNimbor T"""""orNamo. ,-..,.. ~lghway 11 North Spot 219 Kinston NC 28502-0600 F•clfily Ackhst frran"f''''or Address

F-Aarc Harder ~ressSaver Fooili\1 MoiiKxlof SNooino

pw SAMPLING-1 H06 .

Prooess Samplo I $Dedi! Stllli>ln!llmllll<lions .. · slSmoftno G .&J~ J r_, c:_.-b~j-- :=l,s;~i~~iri5Cf{ggi~n,~,Ag,Zn(3030CI6010B); Hg; Cl-(325.3); F-(340.2); ~(&;3.2);

· 37 .4- T 4 .1 · 410.4 . · · If! . 'oll

. · .. ., . . '

• .. .

pa!e lllle ample ~ine freservaiive . puanlily p3<>1U. f'\1! Cl- COO-f. Me18s ~ ~ ~ oc ton ; . ype Pl>l . ype

17A ' ·~ WN 120· H3P04 1 . a.

II'" ···: . WN~

H2S04. 1 v 17A . ' -~· 1 •·

H2SOt! 1• B 17A . .. ;f.. IN)3'·. t B . ·· . p(

. . . :~. l,. 'NIV 100!1 None 2 p IX - .• WN m. -· . 1 p

.. ·. .• ., ..

. . . /1 ' .,

< .I ··,L ··,.·f. ~dl,l~_lllaltleoR ...... G . .&,~/11-'1.· · DateiiTnlo 411 'o!),~ .. of S-"•llaon O!rivol at Flilal ! •

. . . I bv fl::. .IJ~ ' . • '1/'t~S'-J~ . I~ . .·' Oate/T11110-...._ ' tn+at.-\-'

.·R~~ Oateffin&~ · >' R,ceJI,ea W ---- OoteJTn .. -.........._

. , )lf su..IK en Anival l ._r:;"' c• .·_, . ,.

R . IllY · =-=------- tl.teJTsne, )' ·. -........... R v ..... t\ -p,:r._ U1 Datem.;. J:'~ ~ 1 J. J\ .'t>. ~ $)o. tli.tH--~~

u \J . ' u $ . .. -!it ct9lU ·.•. ;. c

i .. · ! :-;-

?.

{f

• .->:

-·· .

··--

Lagcaster ~fli!er'!torlea ·~··- _ .. f.l~_tl ~4'73~0'{ 1 ('1'"'- -,_: <>-'' -~- L_;.··· p_201651J.- ---:-- ~tz~ -n~ 2425 Now Holand Pli PO llilit 12425. lancallltr. PA 17605-2425 ·· .: · · · ' • -_-·I~ '. -·-·· PuPont Kinston Plant ~04.362-8625 (Fadloral Exprasls I_ Faiillv N.,. - - ··- T~ .. ---Highway 11 North 6~219 Kinston NC 26502.()800

lr...........--1\ddrMoi F•Cilily Adctess ·

Marc Harder Express Saver _- ·.

Mettoodof- .

GW $AMPUNG-1 H05 . l'roceUPr- Samole. -'- . Spec:lal~lnstnK:llons: . .

Sarnolno ~.j:.;-j._y 'b:<..I. .... L- ~!&fs=As,Ba,Cd,Cr,Cu,Fe, .. Mn,se,Ag,zli~108); Hg; 0:.(325.3); F-(3110.2); N03(353.2); E Sd41375.4i: roci415.1i: co- 410.41 · · · · ·

~:~ l .· •... . -~ OCIIor

._, . . _:_ •

=liOn .·. f_ Date-- lme .. <*Jme Presemli'le PJOrlliiY llollle "" ~- f:OO MelliS ~ ~04 OS oc • )1)0

""' ypo

KI~MW-17.4-DUP ID =• • . 1 B KJN.G.MW-17.4-DUP ;. . I ..; H2 ' . f-. v

.MW-l7A-DUP . ww 11 •.· H< .. f B IX•

UW.17A-DUP ,,. .;c _'~!!~, .... ,. ft.l03 1 B MW-17.4-DUP ' .

il1tm - 2 p .· KIN.G.MW-17A-DUP " 1501!· . - 1 p .• .

~-..... ;r . '~ :."·

• ·• .•

.. ' [L[ ·_fL. ... · ~· '2..~-lft; /IV~I~JM'R · .... t,:J., DIIAITliM Lilt os:- · · of : 1.111<>n aRM~ at FNI ' .' ,>,

ttwK. .. ~ . _,~,. l'' ' ' ~r+ . j ... ' '.,/_.I ·• L · ~~~ ·· t .. '

~ ·' Oate/Tima~·:· R~w·· ............... . Nerliine --__ •IRI.-of~ lit on Anlolal • . • !=\""~ ' c:00 Re .,:_.

R .. !by --......_. iilteJT~· ·~ . ·. R.u ....... fi ~ ~ .. v.. 'It )'-;;:-. ·. u \J /1,_,., ___

! ••

/

............. _ .... __

Doltellime '"'r-, q--,[C' 11'.~ .. ~ I L IAL.. \.Q§i,

\... lt . Date I.J ~s~

. ~·'

4 'o;~

i "'i

II .I ··, l: .

,.~.

; i.

_ _.,,,

;'·

j ·~ '-;~

iii

.'·'\o;;

. (p, .. } "J~O ~~ 9

Sf- b.------. ---. . No. 84880 __, _Lancaster Laborato···' rla.St.,7 ..... · ... ,. ic-·~.,~ .. ~1.fJ[7 ~.':l'i ... ff?.,_ "~:-·!1' » •• n20~. . - - 1 7035<50.m1m~.

2425 Now Haiind Pica. PO B<iif24~~ PA 178~242$ brnion&. iord•r 10 ·.·. ~ ·. · '

puPont Ki~n Plant ; . . . · (704,3112-8625 "'e"'-1 ~. I Facllll Nome . ..·.·· · J Teh,_ Number r,.,;..,,, Nome ·· I. ~ighway 11 North Spot 219 Klrtsli'in NC 265Q2,0800• ·• · . ., Focay ~ . . · · ransp....,r Addrooo ·· · ·

[Marc Harder ~-ress Saver I c...... · I Metll<i!t_ot ~"' ""' _ pw SAMPUNG" 1H05 Pro<en SlfiiPle I SJ>ec:lll SlliPping lnstNotlono

EmoiOYet(s) SamDina b . .ec. 'lry I i. ~t : ..

Other Enlolowocl• ' · ' ' · jSom~ • ~ lm~i amfle ...,. fresar'lallve ~;;::Y:;;pl<>;:::ll~lo=. ;=::;;::=;:;;ox;:;==;-'~------:-----:____c_---------'

~~~~---L=·~~··~~~~ . ~ KIN-G-MW-18 'f·'f""".·· 13~· ~~'NN · S041Na2S .• 2, . 8

G-MW-111--MS. t . . I ··. S04M12S .. __ Z. B ~MW-111- · ·.·. ~ . ' S041No2S ··,· 2 B

~==~~~~~~~~~~----.--.--.---r--r~.--.r--r-r ..._ ' ·. ' . ' . .. ,' ., . . ~ : ' .,

. . ' . ·• '· .

r .. A.. .

I. 1 ...... t.l · · n· .li' z..,. "1 ~ AO<Ir laattJes · 1 bY G.B,.;kJr I. 1H>-Of' · i.OI_Somnlo!l Llilor!.A.I1'iv!ll.at f!i!!!~on Rellncaished ~ ..t4riL:--, · · lo..t.m..e ~-4 -{):r"·tJ16l;l 1\ece!Ytd bv ~ ' ·. Dat ::_--... ln:ta .. t.t-Relixlliis~d~>~~ , . -~ ·.··••. Rot~lvedby ......__, Dalelllrne<.> ~ lromp.of~onAITMII /. ~ C 0

II • IDv .'----. , ' "-...,. II Lit\ ']1,[, \t.{jo o. ~~·~ 3 ..U. .:.._ • .f.<; ~{), Datet-/-S-oS' 1

I .' ·.~.·-: I'.···... . _·· \>7. u .' u ' 'J '--' -:/#I l l 4/ 't_ 0 ..

;;[: ,·.·

,.

,~., : ........

. Lancal! La~i!torl@:L. _ · _ 2425 NbW l'ike.ll!.ii•1242S. ~st. PA ·~ DuPont Kinston Plant :.

.. ,. .... ay 11 North Spot 219 Kinston NO Faeilty Addrwss

arc Harder ~2~ ....

IGWSAMPl I ProeMs ·

_ NUO

1 Sample ---r.--;-

C. f?i.J:... 1 k_ . ._sU ,""':" 1-'

~~~3/~'?.~.~~~~(L(.~.qi-s.f-:t: b . . No. 84895 d ',,,_ .,,.,.'

17 _ _ .. : -6625- ede111l Express T~Nurnb- ,.-~-.. u...----

1~.--s-Saver -I u.thod Mt::!~. -

...,. 1 wY1~1\..ri 1VU1l >A\· Tl1r.IA15.1\:

~-

·~f 14\

- -

UlUts); Hg; -1: F-1340 7 .2)·

= P"'~- ~-- r''nYf; ~

B t+ ICl

'-· ..

rt /J A r ., §anl!os !.lpa!) anW at Filal .l.f/1/or -- ·:.~r~: ~[l· 't-5~\~ t~1i~n.JJU---- r.:• ---;.._,_ . lo. 19 dby ~ \ ~te/TIIlie ·\ d k'li±~'S!J:k .. ~(); a c:::r ---:- -!! s ...... u~- u \··

C~&IY~. ~ ~f ;~.- ..

}J; ,,

- --

..• - . ·-~------- NO. 84896

_ Lan . rlabonatarles."'"' .. ·."- .. J~.l.e93/'7J8Q9.:1}_LII/.9_£S.£Lc '-'1 . 12 ..... !!_2!n668' · ·.·:--:-" 1 7~7•1't'2000- • ~ 2425 Now INIId Plea. PO ~5. l.a$1iotw~,fA 1715lJ5.24:/.5 . . .· . k3raomt. . ~

...

DuPont Kinc!Dn Plant ' ' f704,'382-BB25 !Federal !;xp'*cc J. . F•olllv No1110 I T.aia&ono Nt.mbol- T,._or No,. lMIIll1tt. "'ighway 11 North Spot 219 Kinston NC 28502-0800 Foclllly-.. . , . !l'nlnsporter-. ~rc Harder t:xoress ~ver

. . . ~thadof~ pw SAMPiJNG-1H06 • Process · ' So...,. ' , Speclll SlippOig l11$1ructlon$

e . ~- una G.&.·} .. , .. fh d.. /J- ~~~,~\~~~r~f.ftg~r~o~·Aszn<3030CI001oa): Hg; cl-(325.3); F-(340.2); N03(353.2); . ' >; '

Other "· oolo ,;. .~ ' . . ·' ·. · '

~?'~"" !Jale ..,. · pamp'o !"""""' ~alive .. ~ potlle (VI' f-' (VOO . • Mehi!S !'fOO. j504 , [IU5 OC r""'ucn . .. , trype !1111) • · . :, . ype KIN-G-MW-1S..MS· •Ill'<!: .'f!i'J 120,:·. H3P04 ,,. 1 B

ION.G-MW-18-MIS' ~ 1£-'·"=t:· ~H2~SOig' nt: j'·~~v =~=~t:::::t=:t:=:l!==t=~b:==+~::t=+=+~ K ·. . ' ~ 1 !L H2SO.• 1·,. B IN.G-UW-111- • · ~ ·;,....i~HN03\~"-,· ~·,.._. ~f"+'·''·+-;;.B;_· .l--+-----'l'--l,...._-+-1.--f'-+--v-lv--1r--i !WN.G-MW-18- S . WN 10110 Nono,· · 2".' _: .p ~

KII'I'GIIW-18- · .'-> . , Oi!L· WN :i.-~-=~'' ..1· .,.....:1.,.;' '..I· r.-· ,:;;P-+-T-...ii---T-+--T--T--.lr-.....,i'--'T--T-""'r--;--, - - . l "

1 • I

.A./.. 0 ~·· · ·~/Orl"r"" t~~os ;- ' . . I. ot~U1>onlllrioalatrnal ,

· · , .:r: J-V'A.'·- .· .. ·· .tt/lks.~i~ .... u · '"'.,G.i..;l"'.".··, :.;,.r- · ~/oo 1'nkt+ ·.·.···.~·.··· ~<:.· R ~ · · · · -"' • ;: ;, ·Y. Re.....,."" '· ( · , ::·:·! ernp. of Saq>les on Arrival - ~: '•' C 0

(':.,'

Rem· ~ i. ·.•·· ...........__. R,J,..,.I\ 'R~~£1 Datelfme' .,.:.:l. u.,.,.rtl) ~tl.. J.L_5:~ . ,. · l: I \ J . • r I l' .

{ 0. /.J It~ "*5

'

~,

. ····-·-·

L_, 2425

1 1 . . PfO .. 84897 Copterybo&;ftorlat . l?bY319.38D'I)JL{lt.1B57~-:~.'l [ . ~···"--····· 17•6~7~

df'i!i. POI!P!12425.Lancaster,PA17805-2425 · · . no.,. '"111 Pn>lld""""'-' r .... '"'""'" """""c ,__ ,.......,._ r '· LiliOton Pla.nt .. _...... a:: I

...... """"'-<><>=

- - JTraMPDJt•r Name m,_ ,_.....:., -··

·-r---:ci Saver F_~§m;¥m ·-

v SAMPLING-I H06 .... -ss~S.mple .

I r;_t',..,L g .t.S~fh ~~h---~~-----.--~~~~~~---. -. Olhor Hli

omple

!" Non8 I Nonotc

1· -t---t--+-'""' I f . I · I

._...__ ....... ~ ...

·I~·-~~ ~ lJlucfl-tg; _, __ ,....,.,...,..,,w~Jr

' A): TOCI4 '!.§, 1\· ,.,--,~,j

Ld1

-.-

_;l;_ -

"\."1"" ____ ,

-·. I

i ffoc I

r· r·-

I

leol!tet dwl: s!L*i~ ~xf~I8GIIa>.R...-,.,G.€..· k-.. l0a1emme tth ~~---·--~ D.. ....... .,

·' Datll'llme c •.

n~A"" -\....UT"fi/5 ' -._ ... ~

:, ~;

{/

~·

Memorandum

DATE:

TO:

FROM:

RE:

November 18, 2005

Marc Harder - URS Diamond Jerry Bailey- URS Diamond

Kelly Rinehimer

Analytical Data for Kinston

Enclosed please find the report for the GW SAMPLING-2H05 project.

Please call with questions.

Thanks Kelly

ADQM FINAL DATA REPORT NARRATIVE

Kinston

GW SAMPLING-2H05

Sampling Dates October 11-14, 2005

Laboratories Lancaster Laboratories (Lancaster) Lancaster, PA

Analvtical Protocol ParameteriS)

Metals AlkalinitY Chloride Fluoride Nitrate Sulfate

Total Dissolved Solids Total Or~>anic Carbon Total Organic Haloeen

Chemical Oxygen Demand I ,4-Dioxane

Site-Specific Volatiles Sample Arrival & Recemt

Analvtical Method SW846 6010B/7470A

EPA 310.1 EPA 325.3 EPA 340.2 EPA 353.2 EPA 375.4 EPA 160.1 EPA 415.1

SW846 9020B EPA410.4

SW846 8270C SW846 8260B

The groundwater samples collected for this project arrived at the laboratory intact and within temperature with the following exceptions: • Field personnel did not include the date and time of collection on Lancaster COCs 88954 and

89252 for sample KIN-K-TBLK-1 as required. Since these are required fields for the Envista database, laboratory personnel entered the earliest date and time of collection ofthe associated samples as the date and time of collection of the trip blank samples.

Significant OC Findings/Comments Overall the data is acceptable for use without qualification. None of the data is considered unusable. Some of the data is estimated due to blank contamination, poor matrix spike and/or matrix spike duplicate recoveries, imprecision between the matrix spike and matrix spike duplicate samples and results reported between the method detection limit (MDL) and practical quantitation limit (PQL). The DDR Narrative Report lists the qualified samples and the reasons for qualification.

The reported results for total organic halogen (TOX) in samples KIN-G-MW-17A and KIN-GMW-17A-DUP may be biased high. The second column determinations were greater than 10% of the sum of the two column determinations for the TOX analysis.

Zinc was detected in the method blank associated with the samples in this project at a concentration of 0.0334 mg/L. Due to the 72-hour prep hold time, the laboratory was unable to redigest the samples. Therefore some of the samples were flagged with a "B" in the database due to method blank contamination.

Kelly A. Rinehimer 11/18/05


The DDR is an automated in temal review process used by the ADQM group to determine if the data is usable. The data is run through this automated program where a series of checks are performed on the data. The data is evaluated against hold time criteria, checked for blank contamination, assessed against matrix spike(MS)/matrix spike duplicate (MSD) recoveries, assessed against relative percent differences (RPDs) between these samples, assessed against laboratory control sample(LCS)/control sample duplicate (LCSD) recoveries, assessed against RPDs between these samples, assessed against RPDs between laboratory replicates, and assessed against surrogate spike recoveries. The DDR applies the following data qualifiers to analysis results, as warranted:



J Analyte present. Reported value may not be accurate or precise. UJ Not detected. Reporting limit may not be accurate or precise.



J Estimated value; result falls between method detection limit (mdl) and practical quantitation limit (pql).




The DDR is an automated internal review process used by the ADQM group to determine if the data is usable. The data is run through this automated program where a series of checks are performed on the data. The data is evaluated against hold time criteria, checked for blank contamination, assessed against matrix spike(MS)/matrix spike duplicate (MSD) recoveries, assessed against relative percent differences (RPDs) between these samples, assessed against laboratory control sample(LCS)/control sample duplicate (LCSD) recoveries, assessed against RPDs between these samples, assessed against RPDs between laboratory replicates, and assessed against surrogate spike recoveries. The DDR applies the following data qualifiers to analysis results, as warranted:



J Analvte present. Reported value may not be accurate or precise. UJ Not detected. Reporting limit may not be accurate or precise.



J Estimated value; result falls between method detection limit (mdl) and practical quantitation limit (pql).



GW SAMPLING-2H05

DuPont Kinston

November 18, 2005

Prepared for

Marc Harder- URS Diamond Jerry Bailey- URS Diamond

Prepared by

URS Diamond Laboratory Services - Kelly Rinehimer

Barley Mill Plaza, Building 19 P.O. Box 80027

Wilmington, DE 19880-0027


Reporting Limit MDL DDR Standards LABSTATS


11/18/200514:51:13 Page 1 of2

Contamination detected in Equipment Blank(s). Sample result does not differ significantly from the analyte concentration detected in the associated equipment blank(s).

SampleiD

KIN-G-MW-13

KIN-G-MW-14 KJN-G-MW-15 KIN-G-MW-16


1011312005 4624443-TOX f 90208

10/1312005 4624444-TOX F 90208 1011312005 4624445-TOX F 90208

1011312005 4624446-TOX f 90208

TOTAL ORGANIC HALOGEN




Result

48.7 46.2 83.1 59.4

Units

UG/l UG/L

UGIL UG/L

MDL

35.0

35.0 35.0 35.0

PQL Qual

100 100 100 100

B

B B 8

Contamination detected in Method Blank(s). Sample result does not differ significantly from the analyte concentration detected In the associated method blank(s).

Sample ID

KIN--G-MW-13 KJN-G-MW-15 KIN-G-MW-16

KIN-G-MW-16

KIN-G-MW-18

Date Lab Metl1od Sampled 10 Code Analyte

1011312005 4624443-ZN F~ 60108 ZINC 10/13/2005 4624445-ZN Fl: 60108 ZINC 10/13/2005 4624446-ZN FE 60108 ZINC 10/1312005 4624446-BA F~ 60108 10/1312005 4624449-ZN F~ 60108

BARIUM

ZINC

Result

0.0144 0.0110 0.0267

0.0050 0.0055

Units

MG/L

MGIL MG/L

MG/L

MG/L

MDL PQL Qual

0.0053 0.0200 B 0.0053 0.0200 8 0.0053 0.0200 8

0.00044 0.0050 8 0.0053 0.0200 8

Associated MS and/or MSD analysis had relative percent recovery (RPR) values higher than the upper control limit. The reported result may be biased high.

Sample ID

KIN-G-MW-17A-DUP KIN-K-EQ8LK-DAY1


10/1312005 4624448-TOX F 90208

10/1312005 4624453-TOX £ 90208



Result

916 39.0

Units

UG/L

UG/L

MDL

70.0

35.0

PQL Qual

200 100 J

High relative percent difference (RPD) observed between MS and MSD samples. The reported result may be imprecise.

Sample ID

KIN-G-MW-13 KIN-G-MW-14

KIN-G-MW-15 KIN-G-MW-16 KIN-G-MW-17A

KIN-G-MW-17A KIN-G-MW-17A-DUP KIN-G-MW-18

Date Lab Method Sampled ID Code

10/1312005 4624443-F FS 340.2 1011312005 4624444-F FS 340.2 10/1312005 4624445-F FS 340.2

10/1312005 4624446-F FS 340.2 10/1312005 4624447-TOX F 90208 10/1312005 4624447-F FS 340.2 10/13/2005 4624448-F FS 340.2

10/1312005 4624449-F FS 340.2

Ana lyle

FLUORIDE (DISTILLED) FLUORIDE (DISTILLED)

FLUORIDE (DISTILLED} FLUORIDE (DISTILLED) TOTAL ORGANIC HALOGEN FLUORIDE (DISTILLED)

FLUORIDE (DISTILLED) FLUORIDE (DISTILLED)

Result

0.16 0.061 0.25

0.24 922 0.067

0.081 0.25

Units

MG/L MG/L

MG/L

MG/L

UG/L MG/L

MG/L MG/L

MDL

0.030 0.030 0.030 0.030

35.0 0.030

0.030 0.030

PQL

0.10 0.10 0.10 0.10

100 0.10

0.10 0.10

Qual

J J J J

J J J J


Sample ID

KIN-G-MW-10 KIN-G-MW-13 KIN-G-MW-13

KIN-G-MW-14 KIN-G-MW-14 KJN-G-MW-14

KIN-G-MW-15 KIN-G-MW-15

KIN-G-MW-15 KIN-G-MW-16 KIN-G-MW-16 KJN-G-MW-17A

KIN-G-MW-17A

KIN-G-MW-17A-DUP KIN-G-MW-17 A-DUP KIN-G-MW-17A-DUP


1011112005 4622843-1 FS 8270C 1011312005 4624443-COD I 410.4 10/1312005 4624443-AG F~ 60108 10/1312005 4624458-1 FS 8270C

10/1312005 4624444-COD I 410.4 1011312005 4624444-AG F~ 60108

10/1312005 4624445-P8 F!: 60108 10/1312005 4624445-CU F~ 60108

10/13/2005 4624445-AG H 60108 10/1312005 4624446-COD I 410.4 10/1312005 4624446-AG F! 60108

10/1312005 4624447-CR F~ 60108 10/1312005 4624447-AG F! 60108

1011312005 4624448-CR H 60108 10/1312005 4624448-AS F~ 60108 10/1312005 4624448-AG H 60108

1 ,4-DIOXANE CHEMICAL OXYGEN DEMAND SILVER 1 ,4-DIOXANE

CHEMICAL OXYGEN DEMAND SILVER

LEAD

COPPER SILVER

CHEMICAL OXYGEN DEMAND SILVER CHROMIUM

SILVER CHROMIUM ARSENIC SILVER

Result

' 37.7

0.0023 2 23.0 0.0027

0.0103 0.0057 0.0045 37.7 0.0037 0.0069

0.0029

0.0075 0.0114 0.0025

Units

UG/L

MG/L

MG/L UG/L

MG/L MG/L

MG/L

MG/L

MG/L

MG/L MG/L MG/L

MG/L MG/L

MG/L MG/L

MDL PQL Qual

5 J 12.8 50.0 J

0.0020 0.0050 J 5

12.8 50.0 0.0020 0.0050 J 0.0084 0.0200 J 0.0018 0.0100 J 0.0020 0.0050 J

12.8 50.0 J 0.0020 0.0050

0.0048 0.0150 J 0.0020 0.0050 J 0.0048 0.0150 J 0.0093 0.0200 J 0.0020 0.0050 J




11118/200514:51:13 Page 2 of2


Date Lab Method Sample ID Sampled ID Code Ana lyle Result Units MDL PQL

KIN-G-MW-19 10/1212005 4622845-1 FS 8270C 1,4-DIOXANE 3 UG/L 5 KIN-G-MW-23A 10/11/2005 4822849-1 FS 8270C 1 ,4-DIOXANE 2 UG/L 5 KIN-G-MW-35 10/1412005 4625876-1 FS 82608 CIS-1,2-DICHLOROETHENE 0.4 UG/L 0.1 0.5 KIN-G-MW-36 10/1412005 4625881-1 FS 82608 TRICHLOROETHENE 0.2 UG/L 0.1 0.5 KIN-G-MW-36 10/1412005 4625881-1 FS 82608 CIS-1 ,2-DICHLOROETHEN E 0.1 UG/L 0.1 0.5 KIN-K-EQBLK-OAY1 10/1312005 4624453-BA EE 60108 BARIUM 0.0021 MG/L 0.00044 0.0050

Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit but above 10%. The reported result may be biased low.

Date Lab Method

Qual

J

J J

J J

J

SampleiD Sampled ID Code Analyte Result Units MDL PQL Qual

KIN-G-MW.15

KIN-G-MW-18

1011312005 4624445-N031\ 353.2 10113/2005 4624449-N031\ 353.2

NITRATE

NITRATE

0.12

3.3 MG/L

MG/L

0.040 0.040

0.10

0.10

Associated MS and/or MSD analysis had relative percent recovery (RPR) values less than the lower control limit The actual detection limits may be higher than reported.

Date Lab Method Sample ID Sampled ID Code Analyte Result Units MDL PQL

KJN~G-MW-16 10/1312005 4624446-N03N 353.2 NITRATE < 0.040 MG/L 0.040 0.10 KJN~G-MW-17A 10/13/2005 4624447~N03N 353.2 NITRATE < 0.040 MG/L 0.040 0.10 KIN~G-MW-17A~DUP 10/13/2005 4624448-N03N 353.2 NITRATE < 0.040 MGIL 0.040 0.10 KIN-K-EQBLK-OAY1 10/1312005 4624453-N03" 353.2 NITRATE < 0.040 MG/L 0.040 0.10

J

Qual

UJ UJ UJ UJ



Site: Kl N - Kl NSTON 11/18/200515:00:13 Project: GW SAMPLING-2H05 Page 1 of 5


In Lab House

Analyte/Parameter Result Qual Qual Unit MDL POL Method

Sampling Point: EQBLK-DAY1 Sampleno: KIN-K-EQBLK-DAY1

Date sampled: Oct 13,2005 Sample1ype: Blank Water

BARIUM 0.0021 J J MG/L 0.00044 0.0050 6010B ZINC 0.0386 MG/L 0.0053 0.0200 6010B TOTAL ORGANIC HALOGEN 39.0 J J UGIL 35.0 100 9020B

Sampling Point: MW-10 Sampleno: KIN-G-MW-1 0

Date sampled: Oct 11,2005 Sample 1ype: Groundwater

1,4-DIOXANE 3 J J UGIL 5 8270C



1 ,4-DIOXANE 140 UG/L 10 49 8270C


Date sampled: Oct 13, 2005 Sample type: Groundwater

TOTAL DISSOLVED SOLIDS 179 MG/L 9.7 30.0 160.1 ALKALINITY TO PH 4.5 40.1 MG/L AS CAC03 0.46 2.0 310.1 CHLORIDE (TITRIMETRIC) 17.6 MG/L 0.40 2.0 325.3 FLUORIDE (DISTILLED) 0.16 J MG/L 0.030 0.10 340.2 NITRATE 0.35 MG/L 0.040 0.10 353.2 SULFATE (TURBIDIMETRIC) 51.6 MG/L 3.0 10.0 375.4 CHEMICAL OXYGEN DEMAND 37.7 J J MGIL 12.8 50.0 410.4 TOTAL ORGANIC CARBON 10.4 MGIL 0.50 2.0 415.1 BARIUM 0.0236 MGIL 0.00044 0.0050 6010B MANGANESE 0.0214 MGIL 0.00096 0.0050 6010B SILVER 0.0023 J J MG/L 0.0020 0.0050 6010B ZINC 0.0144 J B MG/L 0.0053 0.0200 6010B TOTAL ORGANIC HALOGEN 48.7 J B UG/L 35.0 100 9020B

Sampling Point: MW-14 Sam plena: KIN-G-MW-14

Date sampled: Oct 13,2005 Sample type: Groundwater

TOTAL DISSOLVED SOLIDS 341 MG/L 9.7 30.0 160.1 ALKALINITY TO PH 4.5 38.4 MG/L AS CAC03 0.46 2.0 310.1 CHLORIDE (TITRIMETRIC) 27.5 MG/L 0.40 2.0 325.3 FLUORIDE (DISTILLED) 0.061 J J MG/L 0.030 0.10 340.2 SULFATE (TURBIDIMETRIC) 146 MG/L 7.5 25.0 375.4 CHEMICAL OXYGEN DEMAND 23.0 J J MG/L 12.8 50.0 410.4 TOTAL ORGANIC CARBON 6.2 MGIL 0.50 2.0 415.1 BARIUM 0.0169 MGIL 0.00044 0.0050 6010B MANGANESE 0.0210 MGIL 0.00096 0.0050 6010B SILVER 0.0027 J J MGIL 0.0020 0.0050 6010B 1 ,4-DIOXANE 2 J J UGIL 1 5 8270C TOTAL ORGANIC HALOGEN 46.2 J B UGIL 35.0 100 9020B


Date sampled: Del 13,2005 Sample type: Groundwater

TOTAL DISSOLVED SOLIDS 651 MG/L 9.7 30.0 160.1



Site: KIN- KINSTON 11/18/200515:00:13 Project: GW SAMPLING-2H05 Page 2 of 5


In Lab House




ALKALINITY TO PH 4.5 501 MGIL AS CAC03 0.46 2.0 310.1 CHLORIDE (TITRIMETRIC) 42.3 MGIL 1.6 8.0 325.3 FLUORIDE (DISTILLED) 0.25 J MGIL 0.030 0.10 340.2 NITRATE 0.12 J MG/L 0.040 0.10 353.2 CHEMICAL OXYGEN DEMAND 54.7 MG/L 12.8 50.0 410.4 TOTAL ORGANIC CARBON 13.8 MGIL 0.50 2.0 415.1 BARIUM 0.0332 MG/L 0.00044 0.0050 6010B COPPER 0.0057 J J MGIL 0.0018 0.0100 6010B IRON 19.4 MG/L 0.0378 0.200 6010B LEAD 0.0103 J J MGIL 0.0084 0.0200 6010B MANGANESE 0.267 MG/L 0.00096 0.0050 6010B SILVER 0.0045 J J MG/L 0.0020 0.0050 6010B ZINC 0.0110 J B MG/l 0.0053 0.0200 6010B 1 ,4-DIOXANE 200 UG/l 2 10 8270C TOTAL ORGANIC HALOGEN 83.1 J B UGIL 35.0 100 9020B

Sampling Point: MW-16 Sample no: KIN-G-MW-16


TOTAL DISSOLVED SOLIDS 248 MG/l 9.7 30.0 160.1 ALKALINITY TO PH 4.5 202 MG/l AS CAC03 0.46 2.0 310.1 CHLORIDE (TITRIMETRIC) 10.5 MG/l 0.40 2.0 325.3 FLUORIDE (DISTILLED) 0.24 J MGIL 0.030 0.10 340.2 CHEMICAL OXYGEN DEMAND 37.7 J J MG/L 12.8 50.0 410.4 TOTAL ORGANIC CARBON 9.8 MG/l 0.50 2.0 415.1 ARSENIC 0.0297 MG/L 0.0093 0.0200 6010B BARIUM 0.0050 J B MG/l 0.00044 0.0050 6010B IRON 49.5 MGIL 0.0378 0.200 6010B MANGANESE 0.177 MG/l 0.00096 0.0050 6010B SILVER 0.0037 J J MGIL 0.0020 0.0050 6010B ZINC 0.0267 B MGIL 0.0053 0.0200 6010B 1 ,4-DIOXANE 95 UG/l 1 5 8270C TOTAL ORGANIC HALOGEN 59.4 J B UG/l 35.0 100 9020B



TOTAL DISSOLVED SOLIDS 467 MG/L 9.7 30.0 160.1 ALKALINITY TO PH 4.5 207 MG/L AS CAC03 0.46 2.0 310.1 CHLORIDE (TITRIMETRIC) 37.7 MGIL 1.6 8.0 325.3 FLUORIDE (DISTillED) 0.067 J J MG/l 0.030 0.10 340.2 CHEMICAL OXYGEN DEMAND 923 MG/L 32.0 125 410.4 TOTAL ORGANIC CARBON 256 MG/L 12.5 50.0 415.1 BARIUM 0.0217 MG/L 0.00044 0.0050 6010B CHROMIUM 0.0069 J J MG/L 0.0048 0.0150 6010B IRON 181 MG/l 0.0378 0.200 6010B MANGANESE 0.311 MG/l 0.00096 0.0050 6010B SILVER 0.0029 J J MGIL 0.0020 0.0050 6010B TOTAL ORGANIC HALOGEN 922 J UG/L 35.0 100 9020B



Site: KIN - KINSTON 111181200515:00:14 Project: GW SAMPLING-2H05 Page 3 of 5


In Lab House


Sampling Point: MVV-17A Sampleno: KIN-G-MW-17 A-DUP


TOTAL DISSOLVED SOLIDS 448 MG/L 9.7 30.0 160.1 ALKALINITY TO PH 4.5 207 MG/L AS CAC03 0.46 2.0 310.1 CHLORIDE (TITRIMETRIC) 38.7 MG/L 1.6 8.0 325.3 FLUORIDE (DISTILLED) 0.081 J J MG/L 0.030 0.10 340.2 CHEMICAL OXYGEN DEMAND 990 MG/L 32.0 125 410.4 TOTAL ORGANIC CARBON 291 MG/L 12.5 50.0 415.1 ARSENIC 0.0114 J J MG/L 0.0093 0.0200 6010B BARIUM 0.0218 MG/L 0.00044 0.0050 6010B CHROMIUM 0.0075 J J MGIL 0.0048 0.0150 6010B IRON 176 MG/L 0.0378 0.200 6010B MANGANESE 0.304 MG/L 0.00096 0.0050 6010B SILVER 0.0025 J J MG/L 0.0020 0.0050 6010B TOTAL ORGANIC HALOGEN 916 J UG/L 70.0 200 9020B


Date sampled: Oct 13, 2005 Sample lype: Groundwater

TOTAL DISSOLVED SOLIDS 115 MGIL 9.7 30.0 160.1 ALKALINITY TO PH 4.5 7.5 MG/L AS CAC03 0.46 2.0 310.1 CHLORIDE (TITRIMETRIC) 4.6 MGIL 0.40 2.0 325.3 FLUORIDE (DISTILLED) 0.25 J MG/L 0.030 0.10 340.2 NITRATE 3.3 J MG/L 0.040 0.10 353.2 SULFATE (TURBIDIMETRIC) 49.3 MG/L 6.0 20.0 375.4 TOTAL ORGANIC CARBON 2.4 MG/L 0.50 2.0 415.1 BARIUM 0.0403 MG/L 0.00044 0.0050 6010B MANGANESE 0.0635 MG/L 0.00096 0.0050 6010B ZINC 0.0055 J B MG/L 0.0053 0.0200 6010B

Sampling Point: MW-19 Sampleno: KIN-G-MVV-19

Date sampled: Oct 12, 2005 Sample lype: Groundwater

1 ,4-DIOXANE 3 J J UGIL 5 8270C



1 ,4-DIOXANE 13 UG/L 5 8270C

Sampling Point: MVV-21 Sample no: KIN-G-MW-21


1 ,4-DIOXANE 100 UG/L 5 24 8270C



1 ,4-DIOXANE 760 UG/L 10 52 8270C

. , __ -'--... ::.~ .. ·.--;-;1---.......,-.. ···--'-::---- .. ,_.-. --~'"-': ~ ,.;.; .... ~-.. ""- ,_..., ..

Ol'et~3 Ctoc.plf:q(o?Sas-' No. 89244 LancaJler Laboratories; mnptelf-L/(J,')Lit.JLJ3-5LI . ~ j1207255 I 7Q35.~-mooo I 2425 NewHoHand Pike. PO Box 12425_ L•ncasler, PA 176[)5.2425 IG~ _Order tDPrl!!e; puPont Kinston Plant - -~ ~ - · --- - · r,04-362-6625 l=ederal Express 2nd lllay . I Facilitv Nome T~ Number ITrono-or Name . _ LT•

1-Jighway 11 North Spot 219 Kirilstan loiC :28502-0BOO fa.:Jity Ad<hoa IT~nsporter Adchoo

ndOay MetllodofS

2H05 Process Prodoi<iM Samole 1 'peciol Slipping 1151ruotions

Emolowe<sl Sitnollna M , U A/tiJI9/l.-OUter -- ' -- Handlina ....;,..,;_

~f IT OX ~:tion KIN-G-Mw: 13

Hie lme !Sample. ype

n""!;j WN

r ' Ll II

e Nwnber

~~•llei/;M/.J~j_~- ~~ '('-jb~ • ~· Ro~ _jDab!I[.,J{&Ilfo}- /ted lcordtion of Som>feslt!on anivaJ at Final OesmauDn ., ---------

.. by .• of SJ.iiiRfeS - c •. R~ _ ~'"I'- ~on _____ _

RelilcpsWby ~ lo~ ~Riii:~ b{ ill~ =<t~K- loatetrtne llllwl ffi:_ rliipt .. u;M . :Jvn L lo:ns /O}u,/,. <:'

c. d 971) . \ IT u - I J. - ! ,. . u I J · · · 0'110

~oi.v__ lp

' ~

-:-.--··

-·- !' ... ':"" _, -------

...... -~......_.__ ... .. . :;'~ _-,:.~--~---' .. ' ... ..._,_ _____ ,,_,_

aeetltfdt:U3 ~Jtq~ . No. 89257 Lancuter L · 2425 New Hollirnd Pike. P61 DuPont Kinston Plant I Facintv Name -

SAnp!etf:L/(d;)l.lt.N?r-51-f L p207255 17:=7-772000 I PII1761J5.2425 . . ·. ..'1'riPPraie:;;;;h:

2nd Day 1'. • NumiHir. -~

1 Nulnbar -~

I. ··a····-Y 11 North Spot 219 F•ctditv Address

NC -·~

t c:::::.... c; ~~~ ... ~~~~FtlhFI I t p "", ~ "f:eg ~ F ra• ros. roc

~

r· H2S04 1:" ~

:-·I= 100, -· u-

- -

r t l r· · F b !1 I I I I I I I 1 r I L, . .. .. . .. - -If I I I I . I I I I I I I IY L , .t.·., r r 1 II ' '""

c • ~==~~==~~~

~by . . :s;JQ.~6 :s;;JR~f~kMDj)t· lo.t;;I(P toJjfo; ls~~r~(1liM(r~ lc.Jb)Jtjot Oos~.5

Cho~3

':•;.

-----~~~~-

'" -··~·· ;.;~ . " _..._ --------'·· ___ ,_ ~.:.~---- -·

lt(o(py3Q-lWttq~'39C6 l&iica.;:e; liU\;ii:Ui"i.:~ _ .m;nptelfLt (,tJLILJt..l34-i ~ __ · c;~~255 ~~;;~ 2425 New Holond Pice. PO llox 12425. Lancaster, PA 176QI;.2425 _ . i':>ootm&.. dO I Numbor puPont Kins!Dn Plant 1704-362-8625 lFecN!ral Express 2nd Dar 1. .. _ · · IFocllltv lllame --'- IT• Nwni>M Tra-er Nome - • "''"'"'"' IH_ighwlly 11 North Spot 219 Kin:.tcn NC 28602-0800 Facility~ · IT"'"'Portor Address _

jMarc Harder !"nd Day IFaciltv • Meth9.!1:of -'''' · iGW SAMPLI~2H05, · Proeess . sarro>~o . _1_ • I Si>eclat-""' lnslnltllons

E :sl ~1111!1 · J..f, -RJII:._[){;; d , .

Other Em-..D(o)f:llndlkog

~mp. -· ·· pe1e me · arnplo 1/okJme Pn>ser~olve <lullllly !l"llle OX Do""~>IOO . l LL jpe (mO r ... - -· jpe

Klt-1-G-IIIIW-14 ,;y· WN 50 S04/Na2S< 2 6 · ·

_-_

..£ "' ·~~ ~ • .,.., ...... ~: ~ ,.,.,.,/~"" ··~ -··· ·-·--Relin<xisheci~Wl"~~ ' ~·111ru./o~ttr ~ Re<:~ ui?- . . . \ u... ~.J' r C- 0

RellnQlio""j;;;;f . · f' ~ Received by. ---- DltetTirne --- lrernp. of ~les on ArriYat _d._ ~. · C

111111q\h;hedby •• --... rnne• -........._ llecaiiiertMb..M ~~wr Oil.emneii-.I,J,t!N::""" ~ript.,._f ~ ~~ j&ro_Lo 1 "- ,_ •

- ' I u l'cJ9it> I c I I

C-oo~~-"

:-.. ;.

--------,

,,,: :~ .. ... i>·· , .......... . """" ·-·-..<······ • .,.:.. .. ,,,:..

~(f;ftl-rcp;-13 Utx.p*q(D~$'".

Lancuter Laboratories 50n1P1*' ... LfiO'JY44':>~'1 14 . n207255 1 7Q35.50~-772QOO 2425 New Holland Pice. PO Box 12425. Lancaster, PA 17805-2425 brn- lordor ID Jl'~ puPont Kinsloll Plant [704.3az,6625 Federal Express 2nd Day I FacillvNamo ITolooh-llll.mbor T.........,rtorNamo IT >Mi>LJ>...L Highway 11 North Spot 219 Kinston NC 28502-0800 Facility Adnn 1'111\Sflmtl!r Addren

Marc Harder ~nd Day r ·. --

pw SAMPLING-2H05 . . . . . Proe ... Pr-• a"'""'" I Sue<ia15Nollln!l-

.· · ·- I& l.a..l'.it\C:tz !'Jietals=As; Ba, Cd, cr, Cu, F'ei Pb, Mn, se, Ag, Zn(303CI50106r, Hg; Cl-(325.3); F-(340.2) EIIIIIIOIIt<!lsl S.~ l"f• ln~l- No3(353.2i: 804(375:4): T0Cf415:1l: Co0(410.4) .

Other E 'o\ . · •' :··. ,

h~e pate_ _ ime . !"'mplt I"'*""" l'reselvo!M_ ~ ~llle !\1(· p- f'"W Mel81s roo ~ [504 OS TOC ~-'"".fplm : . . 1 _ j ype (mO . ype !S!~MW-14 - · Wll 1211 H3P04 1 B KIN-G-MW-14 • r. VWI 140 None 1 V !;_

KIN-G-MW-14 BWN H2S04 1 v KIN-G-MW-14 -· 1 H2S04 1 B

I<IN-G-MW-14, ·. '-"'' ' . ;,--+-H'<fN::'0:'-3-+---.<-1-t~B+-t---+--t..---+--tv---f--+-+~-t;---[y-t----J KIN-G-MW-14 • . 1000 None 2 P ~

KIJ\I.G.MW-14" - · \J \ ' WIN. :::,_+..,:N~one=-+-1!.-,--\--!P-\.-+--r.---T---r--Lr-""""'Jr-"""'1.-"""'1-...,,_-"J--'r--T'--1 / '.": ·.· ' ; - ;

·,--:. .•. ; .1>. .-:

;:-..:..,-;:r/t~'::"'" ~:-t§# .. ·· ,~-W/IA ~-"t"-frZ:."~ R.tmuish~ u Da~ · IReeeNedbl - -· Oalefrme ._ ....._ Ire..,_ of~ onAnWBI , -/.I c.. c •

RelinQuished~ --........... Date/Time ,;---~oei<edb;f~kh';l,ilt_ . · oarelllme .LI Sti¥1aWtl~ -kab ~~~~ohtdn'l'

0 1 r U · 1 hun { I G ' "

&o~~

-

;~_' .

. '

.. ;

; .... ~~"-·."·-..f._,..,J ~-.-;··

........... , ........ -. ~'-~~----......... ~~-..:. .. -..,..-~.---~- . .:..,...,___ .,.·

Laneaater Labc 2425 New Helland Piko. PO !lox 12425. r, PA

(JC(lttt{du£ ~q (o?f;)r:£ 8:ftlplt tf lf (o~44lf 3-Sl/ Lr.

.. ____ . -···----' Planl • _ &2nd0ay 1 ·- . 1: ·-'NC ~-

-

._! l lou .. r 1)-..., • ·• 1/f. ~~~(4 EMlple __ ' rr;·re~ ~~m· IOJonily !Joll~

- I-- ~YP•

f35fo I WW -~~0- 2 ,-8

I I I I II 1. A- I I I I I .ll. . l#'

·-.-----rAck:

~ •. T~.-~

!fox

-

I I~·. -~~~~ jf)"i'#'t, ,~.F ~ ~Oat-~~ Ito? ~L .

-~_ -~

__ ::--,....._ " ~ I, ---I

11_1?}' ------.<_ bo/T1me ---......_ I. ~Yu~~rit·T~

Co~71'f I u

CJPW-~

_j

'()/J/~{/A

I - lr·~· • ulL'il ffl

1 O~io

• Nl/m.lltc_

No. 89246 17035-50433t-f I .t.UUU Proiect l«!mber

\: 'tt': ~Final Qeslinal~ .

ISOI1Arrlval eX. (,C c c

tk.o ~.D (_ loatl/o}Wcr' -· u l ,_.

'

.t:;.........,... ..~:...:.·-4--·-~···· ..... .., ..... -............ . ........ .--..-.-.... ·--'-··- ... _. ____ ,__.~ ...... _ . . -·-- ~ .. ~·

_.,·

No. 89259 ' LancaJter Latlratoriea

2425 New ltlland Pie. P Box 12425. La~ ~uPon! Kinston Planf

PA 176

acct-tt:~~ Vtteltq(owcsS/Xnf)Je.ff !./ ldc)Lt4 Cf'?>-54

~rN ... rr~~~~ I 035,504337-772000 !Unber

Faolay Nam• . .

j;~~~orth s~ 21_9

~~~;,~ Harder

.- --'"""':'' :sS.m~·

NC

-

" I

1~--·· -"- ~. ~nt::'/l_ --.-

1~. ,\ l-laltdllrt

1'.- sOeli~U ;2nd Day -.. P.?_<!.. Da~

I Special stipping I "~' Ba, Cd, Cr, cu. Fe, PO; Mn, &1, "'J, -·. t ?\- ~1':17<;. .41· Tnr.t.415.1l: ...,....., •• n "

IIUI:>); Hg; -- _,

r:: .... - ~'i,fr SF I I r r F r r r E r E ~00

I 1 I

\Lll I ~IT~ l I -~T ,:_ ··. L.· ]X

I I I I I It II

No,.

•-•-~-•w -~lfi=l-"~ ~.!•;;.MWF..,...· . ""fll;-t-l~ . c--- s;:: ~ M i

·~

~~ I ~I ~-d-. Dttetrme ·

o.wnm.- 'RtceioedZ'J);AA ~niL "'rw.mmiolro]t,£/1"< co:ss13 '' o - -., ~'NtJ

C-oo~ Y l

lX

r o~Flnoll

~--of Ties on,<~,rr~ia~ (,f C: lT~- 2_~r 1. r "0

r

c• uf..J..-/7

......

" ~----;_,_.

Cle(!.t-~4'3 Cra..prJ:q(o?i)CA No. 89247 Lanca•ter Laboratories 8}"ffprt . ..- '1CI'.:fLf'-ll.f'~-sc.t 2425 ~ lt>lland Pi<e. PO lox 12425. Lancaslo<, PA 17605-2425 - ~ .. ~~~~ lp?:J-504337-772000

t1l!m!l!lir' -

'"·<· '«· ~· ' ;\

::~

puPont Kinston Plant ~04-362.e625 Fecleml Express 2nd Day I. F•cililll- Toloobo .. Numbor Tra11<1>0rtor-~ighwfty 11 North Spot 219 Kin;allon NC 28502-0800 FacililyA<ktess

-ramporter AdchiSt!l

~arc Harder ' ~nd Day F ,... . Method Ill' Sl!i>Pinlt~ -pw SAMPLING,.2H05 '--' .. ,_; .. Prooe.. • 51111!1>1• · t'; I Ss>etia1 S11iwi1!1 liiitructions - -

EmDIOvu(s) fiA, ~ "~OFtt -

Olho.:Erno>lovooolol~na . -- · · ___:_

F>•mple · -: DolO -- ime omplo ~ J>reseMJIIve ouantlly Bol1lo ox p.xi;pnon I'* -ypo 1'"9 ype KIN-G-MW-16 .- ~I' ~1!'1- WN 250 S041Na2S 2 8

- /) -':

>- n~& L. ,r~~ -#if~ I ~~~

lo.,.rr..,P{~d" llRl ~"" ·- ru .1::- Du.mr:.te~/nkL!Led r;;:-- - --- lb..

.. , -_ -----=---,RellnQullhe~ 11 - · · ~-- ·· __ · : • · Recehred llv ~ Dlllemne

1\oln<lulshiKII>Y ~ loaemme ~ l\ocotveca(f"n2"Y ~~ d.,/<1~

_ t---- u-- - I cf9;o C_ 0">77y

c#{p

~

\ . . 't

--·----- ------ ::·-·

llMnUr_

-

-

-

-

Condilion of SII!IDieB Uoon arrival al. Final Destinltior1•

\~ J-.of 011 M1val cZ_" e. co

:t, {1&,_~);... _loae/omla>"

I (_; / I -

"~

~ /

.. .. ,:~.----............. ,."'~.,-··' •··.

Lancaster Laboratories. , . 2425 New HOlland Pke. PO Box 12425. Lane-. PA

uPont Kinston Plant

. ·- -~· ·- - .;.:. -- ~-...·-~-- ............ ~-- ..... --·~

aeef-~ Gctptt:. q~WD1 . No. 89260 · &JmpleiFI./fo~44Ll?rSt( ~ . r,2oi266 J7035-~7-mooo

;rmd nm.,- Jn · Prn~ect Pbnltir

,.Numb .. • &2nd Day

"" 1

-r;!"··

•• ., .... gy 11 North spot 2'\s Kinston NC trra"'""""' -.. .. F .. illy-s.

arc Harcl-·

""" ~W SAMPLING·2H05, D..----- Prnduc S !' . kmruc:tions

ftt__

-· I Lf ..;:.·

M• lJ I ' • ·J JJI/.

' l11c111os Re~~ b.JJr VfJ --·

i!!!!!! ' Upon arrival at F"ml -

\ll..kd ~~~~.i..VIu

bv..-. -----.;.;.;__ ~emp. of Sa.all>les on Arrival I . I e..:_ c '

dby ~ ~ Ii.1___ . llv 1'1l..M ~" ~ . t lbhl//n'\ isvwUJ ([JAil ~;),(_ !Date 111/.(//r/-

dt>.ssyy i ,.- (} ' hf:lto Tr- o · ' ' •

~olv.._ ~

(

. i· .

---~

..........,._:,. >-· • '-·····--·-·-·- ____ : --· . ... ~-.. ........... ~ . ....:.-..... ..

'

La. 2425

QCC;t-~lf'3i Q-ol,pltQ~. No. 89248 · La~ratorie$. S»~pte1f4~Yll4'3-5Y ~ · .. r.:o7255 17035-504337-772000' 1

d Pike-. PO Box 12425. lancaster, PA 176()5..2425 -~n'· . :tier tpPrcie,.t Nllnber t Kinston Plant r,o4.-~~~~ · ··

Ta~an•~

' I

....

IO!hor ·• ,1 Hoodfto -- ......

I ref·--...... _ TOX

<~\--~' I I I JP0 ~mq 1 ype G-liJW.17A -~ fg!.? WW 125D S041Na2& 2 8

fiiKIN-G-MW-17A-OUP ~ p:t::lq WW SIJ' S041Na2_l"" 2 B

I .. ,_.:. _c I I 1-l..J..ll I I

fTI

~~· r

---••n~:~

,·;·, Cl '· . c •·

DatefllJie' oate!Time lb J · • (O<'r

7\.t \r· ·u----- 1JW/6 b"OttP4 4bng; l~tokyr·

\) . ""II' . 0'/IZJ I . .. I

Cvof& ~

~~ :li

------~--------

"'"'""';-~-l: .. ...;..-. ~, _ _._ _ __. .......... ;,;;..:o •.••.•..

·-t .. ,,,

Lanc:;aster Laboratories . 1425 New Holand Pike. PO Box 12421! LolliH!er. PA ~,.. .DuPont Kin&ton Ptanf .

Ol!e*.t(D(ol8 Crc-ffl:q{tJ~ 9Jmple"hf(o~L14~~s.l ·.

Fa Namo 1~ ighway 11 North;Spot 219 Kin""n NC Facillty~ss ·.'·

aro Halder Fae'*v L'>--... _ !Process

---~-aSaDie

t: EmalowuJ~~:l U.ndlir: liS ..

crjllion

-------

'!' I~AI .,.,,..

..,.;......;.;: . ~

~~~ !Time &I"'*-'I L llmt .

WN - • - • . vwr14o WN 140 WN 1000 WN 500

............... .......... . . c-E·

""""'' I:Xpress ~ II' NaJnt. -

F .. '!~~--I Sp!ctal Silipplng

<:""; Ba, Cd, cr. CU; Fe, Pb, Mn, se, Ag, Zn1 3.21: S041375.4); TQ:l415.1\: CODl410.4l

.-r~ t"" ~-'Fro t'-

None .· H2S04

H2S04 11>103, -

1-

B v

WN 1000 y ww 15110 -+....._~_,'¥~"' I IV I ww 15oo I None

I .. --!··· .• •_jl,._._-./_l I I I 1-.-.l-4l.---.t-----IP.illf~_ > j J.

~

• Nl.ombar

JIUOJ; Hg;

No. 89261:

1 . --~ -~··I I ~\lftU.'\

Pmil!cl Nimh..,. · · •

!Melds !'fu fldl ~04 JlOO roc

1X

-

ui..JJA./'/Jif.. ·-~

~. ftM1Jo ~ I -~-1iJ[Z~os=~~s-~ft;_1 c.J\l)3. ~~=£ ~10 ~rLcJDb lo~·rojip> dbv . ----....

Co33tf3

~ , ... L

Coo~3

}:. __

~~?'

-------~----

., .•

~------·

i-·- ~-- ··----··-~-·-

Lancaster Laboratorh 2425 New HOIIond Pike. PO 110>: 12425. ~Pont KinSton Plant F::~cilitv t.h

. •• Q •• •• -Y 11 North Spot 219 FocllilyAdlfnls•'·

rc Harder

I Sample

• PA 171

INC

-4-i'!•--,<. ··-····- ' . :... ......... ~-............ ·~·~--- •.. -•---- 7>••• "'· ·----

Ol!Ct~~?)aa.p#q~ 9Xnptt*LUD'J-l/Lll.}?> ~:r-1 . ~

------. ·L---L-

II -"U./ tt.;J..J l'll .... lnrriN"tn

r~~~~ress 2nd Day

find Day •• • •-..!..

... AflllffL--.. c ·J·.~

.----~--

No. 89262

I . ~-~· -772000 Proiert Nl""-i-

.u .. -J. .

~~~-· fi ,· .. rM ~ ~:m• F••ve F~ ~:~· I I r r F r· IM~ r r r04 r roc I

rx IX ~ .

~

I' r I , I . .. . . - . -.

. . - . TT. I I -

-

. OM(rhl~~~wp¢~ I . ~ ls~1r fiLl\ (f ~- 4! /i) C033'{3 CD0~:5

~ --=:::::::: 1 Zal ...., v---- - .... AITMI, ;. oe-- co Allt:l!ivNt '+I ..ft_ Ill\. """5rr.. ;\: 1._

---------

It

·-~ .................... ,. ... -·-

. ~ QruJ"C?(b.0:>oS' Lancaster Laberatories t:t'ilnllle.ff4h~t./l/l.h-st1 2425 N.wHoland Pke. PO Box.12425. I,......,..,._. 04 4'7Lm.C. ru~.c_~~,., ~uPont Kinston PIRnt· Facilllv Nam. I'; IT~

No. 89249 ~ Pc20L

u~ Ortf.-r 1n. 1 035-504337-mooo

~ ........... 2ndDay I_

'' · p-!ighway 11 North S'* 219 Kinston NC

... - ~ .. ~ I

'il-

~Ry Address . ·.A...J...t...

f3W SAMPLING-21-1JS' .~lho4'of§hippinq !luc!ng Sample .··. ·· ·

Marc Haraer ~s.

AJt-1 --··-

~ . . ··'· ti:· I ~ . . ·. ' . I . ·. ''-· ..... · ~=.. . ·... . .. ~- J#:j ·. .· I .. · . £L ~ ~~Rec~ ~~. ~ifp~fh?tR:::;~ L===:__~ =R~. ,~ ...

_ lnv.m... ~[Rece-6fdw D"~

c 0 '5I "-? y

le.telli l:s: t.f

T.; _

~ok~

'

I

' !lnof~'JtDnttom

--_ I· . .,,,. ... · . ..........._, lremo. nt ~!l nn Arriltal

ffl.r.itJJ'"WJo

·fi=4lreb;-, «·r~ ~ali4'l 910 . . . · I V

··-··· ,'..,.:"' , .. ~-' -~~-

~~~-i:tlr...~~ ... ~-~-.tqeo~~Y' . . 89263 ~-I.WM...., No.

Langaster Laboratori• 2425 NOw Hoiand Pike. PO Box 12425. Lancaster. PA

,, . Pont KiR&ton Plant

SJmfl'"c./tfJ<JLI' ... ~ t..... ;:",;' I~ 772000, I

I' ~.-.-u........... f .._......,..,.., .... lit''"'"" 2nd Day_ .'. ~ To!IM.fthona ~.c.r TN~IHV\ttar J.lsrna T~ ...... r ·

·-;

... _,-'

VJarc HaraeJ . -.· . -. .

F SA~NG-2HQS . . .. •.

PTod!ltilg s.mp~elQ}· -,..," nt8.R .~'!<>cess . • . Nlfl .

'

I Special S!jpplng illstnlt1ton$. I ~As, Ba, Cd, Cr, Cu, Fe, Pb, Mn, S4t Ag, Zn(303CIOO'I08); Hg; Cl-(325.3); F·(340.2) ':<!. ?\· ~ild/::!75 41· TOCI415.1\: C()f)(410.4l .

"

~I ~""· ~~ ~m·r-· rxr; 1 I r r roo r e· r r r04 r toc I

-Tf

h I

_V-NV V-NV IMN - ~·· -· ~-. .; V-NV 10Qa WN 500 V-NV 1080 WN 500 r

f..

Dillolrma . of~· oo PmwaJ c c

e.tt;; ~~ t£14/l~?wb ~~omnlllD),tJas- ls;;ab;'I}J.M=?..~t . L ... ALZ . ....-1: ·d by llilel't1milr ·

cvo&o Po · ' I u- -r;Jq,?J t r-- ·· o ·· 1 1

-Coo~ d--

..

.• :~·· . .KiJ:li¥

_aster Labetatorles "~ "··u Hobnd Pile. PO SO. 12425. Lon•

, "'" Kins!Dn Pia~· I Faoiltv Jhrna·

__ ..,..}_

---

Qllet-tf(o(plj3 Cr~-fq(o39oS' ..9'fllple 14-LIVJ:I-1./1./ q3-s4

·, PA 17815..'~~"'~11:

. . I'U4~0.L·OO.Gl . .,;: . -T•Iecbono MJmb .

, t-lr--~

~ Pt207250 -if'lll.,. Or.Wr 1n

----·-----

~2nd Day

_ ......... y tt Nortt, SPot 219 . -··--·· . ·- ----.,---- 1... I Facility Addnmf ' · ' ' · ---~-- • •

..... ndDay

No. 89264 j7Q35.50037-772000 Preiect Nonl!oir

•lh•Mk•

.. , Prooess l'li>duoi'IQ Somule- 111 :1111 lnstrvotlons

A fldl C' n etals=As, Ba, Cd, Cr, Cu, Fe, Pb, Mn, Se, Ag, Zn(303C/60108); Hg; Cl-(325.3); F-(340.2).

• I~VP.f4- 03(353.2}: S041375.4l: TOCf415.J}; COD{410.4l

9!!!!!:.! . ;;

I)Ho ... ng

1-MS ~MS

~,.-,r,8-MS

~MWa· ;...MW-· 1-MW.· ;..uw .. :

~it --

' I

1'1' . p !COO r- ~elms jil02 fill ~04 ~DS ~oc I

-:•,.

R' )()

t,!•" ---r

I

f." .. ,c •

Cnlio 9o - 1 r ·{r!( 1 %1/k I f?.~~o(!6 loat~!ljrif~-

Cooltu__ cr-

.)

;:~ ···~

·• ~-:;~-~- ..... .. ; .. -

'"""aster Laboratorh Holland Pille. PO liox 12425. La"""ster. PA"'

'

Du. Pont Kinston Plant . FacQity N.:am.

~·

-~-- .. _,., ____ ,_ ··--~- ~ . ..,.,.....,.-

oeet~ an.pfU/0W.oS"' .5b'n~~1t-t.J~LI3-5Y C ~~-I'~ --... "' "'"1".,..; 2nd Day I

r N=lma ·

I.>W ~AMI-'LING-2HOS ·•

PmcM•~oo~~s~~r-~~------------------~~~~~~~~~~~~ 1;,: ~tz__

' .

No. 89265

1 7030~ Prni~r.tNu....,

I 1:.!\JUU

...... .....~..

JU10B); Hg; ; F-{340.2)

. I:_· · am~ 1me ample ~ reset'f81Ye OC Do>Criplion ype (mt

W.G-MW-1~MSD I I 0 . WN 120. HJ~ IN-G-MW-11!-MSD ·''. I WN 0 Net

:o .:' 0 H2S ~ . -·--

IX

-

I,_. t I I I I ; ll . M?·~ I·'· ~I l .,. ''tl .. I I; . .• . ·.. '1 t-of' . ' . . . It h JL{i\)1. terrmo , t:>&"lf !Ballios Ro ~ · lo.n.m. ___ 0::~ __ .:_• ~ol!loc'

('Oto?o \I u· I bttD (I 0 T/

C:oola-0 d--.-

c.

v+:l f)o(!oj--

Documents