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PHOS ACID JOB SAFETY HAZARD ANALISIS (JSHA) Table of Contents Clean Sluice Headers and Cloth Wash Sprays .................................................................................................................................................. 2 Catch Attack Sample .......................................................................................................................................................................................... 3 Clean Vacuum Scrubber Strainer ....................................................................................................................................................................... 4 Catching Filter Cake Sample .............................................................................................................................................................................. 5 Set Up Sulfuric to Evaporators ............................................................................................................................................................................ 6 Cutting Filter Cloths Off Pans ............................................................................................................................................................................. 7 Run Acid Sample ................................................................................................................................................................................................ 8 Cleaning Barometric Condensers ....................................................................................................................................................................... 9 Packing Change – Primary and Secondary Vacuum Scrubbers....................................................................................................................... 10 Clean Pond Water Strainers ............................................................................................................................................................................. 11 Cleaning Catchalls ............................................................................................................................................................................................ 12 Cleaning Slurry Distribution Boxes with Filter Down ......................................................................................................................................... 13 Clean Pump Impeller ........................................................................................................................................................................................ 14 Waterblasting Tubes or Piping .......................................................................................................................................................................... 15 Change Filter Cloths ......................................................................................................................................................................................... 16 Patching Filter Cloth.......................................................................................................................................................................................... 17 Packing Change on East & West Fume Scrubbers .......................................................................................................................................... 18 Clean Flash Cooler Nozzles ............................................................................................................................................................................. 19 Packing Change—Flash Cooler Vacuum Scrubber .......................................................................................................................................... 20 Opening and Closing All Manual Sulfuric Acid Valves ...................................................................................................................................... 21 Pressurizing a line with Sulfuric, Phos Acid, Scrub Water or Pond Water. ....................................................................................................... 22 Clean acid trap, receivers and vacuum scrubber seal tank .............................................................................................................................. 23 Clean filtrate seal tanks, hot wells, attack tanks ............................................................................................................................................... 24 Clean Flash Cooler Piping on Ground .............................................................................................................................................................. 25 Unplug Sample Ports ........................................................................................................................................................................................ 26 Mark Tubes in Evaporators ............................................................................................................................................................................... 27 Clean Inside Flash Coolers ............................................................................................................................................................................... 28 Clean Attack Agitators and 3 rd Flash Cooler Pumps on Ground ....................................................................................................................... 29 Packing Change on 3 rd Fume Scrubbers .......................................................................................................................................................... 30 Put New Floc Bag on Hopper ........................................................................................................................................................................... 31 Cleaning Slurry Distribution Boxes with Filter Running ..................................................................................................................................... 32 Clean Filter Crown ............................................................................................................................................................................................ 33

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PHOS ACID JOB SAFETY HAZARD ANALISIS (JSHA)

Table of ContentsClean Sluice Headers and Cloth Wash Sprays .................................................................................................................................................. 2Catch Attack Sample .......................................................................................................................................................................................... 3Clean Vacuum Scrubber Strainer ....................................................................................................................................................................... 4Catching Filter Cake Sample .............................................................................................................................................................................. 5Set Up Sulfuric to Evaporators............................................................................................................................................................................ 6Cutting Filter Cloths Off Pans ............................................................................................................................................................................. 7Run Acid Sample ................................................................................................................................................................................................ 8Cleaning Barometric Condensers ....................................................................................................................................................................... 9Packing Change – Primary and Secondary Vacuum Scrubbers....................................................................................................................... 10Clean Pond Water Strainers ............................................................................................................................................................................. 11Cleaning Catchalls ............................................................................................................................................................................................ 12Cleaning Slurry Distribution Boxes with Filter Down......................................................................................................................................... 13Clean Pump Impeller ........................................................................................................................................................................................ 14Waterblasting Tubes or Piping.......................................................................................................................................................................... 15Change Filter Cloths ......................................................................................................................................................................................... 16Patching Filter Cloth.......................................................................................................................................................................................... 17Packing Change on East & West Fume Scrubbers .......................................................................................................................................... 18Clean Flash Cooler Nozzles ............................................................................................................................................................................. 19Packing Change—Flash Cooler Vacuum Scrubber .......................................................................................................................................... 20Opening and Closing All Manual Sulfuric Acid Valves...................................................................................................................................... 21Pressurizing a line with Sulfuric, Phos Acid, Scrub Water or Pond Water. ....................................................................................................... 22Clean acid trap, receivers and vacuum scrubber seal tank .............................................................................................................................. 23Clean filtrate seal tanks, hot wells, attack tanks ............................................................................................................................................... 24Clean Flash Cooler Piping on Ground .............................................................................................................................................................. 25Unplug Sample Ports ........................................................................................................................................................................................ 26Mark Tubes in Evaporators............................................................................................................................................................................... 27Clean Inside Flash Coolers............................................................................................................................................................................... 28Clean Attack Agitators and 3rd Flash Cooler Pumps on Ground....................................................................................................................... 29Packing Change on 3rd Fume Scrubbers .......................................................................................................................................................... 30Put New Floc Bag on Hopper ........................................................................................................................................................................... 31Cleaning Slurry Distribution Boxes with Filter Running..................................................................................................................................... 32Clean Filter Crown ............................................................................................................................................................................................ 33

JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 001 Date written: 2/25/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Clean Sluice Headers and Cloth Wash SpraysApproval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out.

None. None.

2 Go inside gyp hopper. Slipping and falling. Watch footing and use hand holds. Wear gloves and safetyharness.

3 Roll spray bar end caps. Rod all sluice nozzles andremove and clean sprays.

Hand injury due to wrench slipping. Slipping andfalling.

Wear gloves and watch for pinch points. Wear face shield.Watch footing and wear safety harness. Pull wrench towardbody to prevent slipping.

4 Exit gyp hopper. Slipping and falling. Watch footing and use hand holds. Wear gloves.

5 Flush Sprays and sluice header. None. None.

6 Go back inside gyp hopper. Slipping and falling. Watch footing and use hand holds. Wear gloves and safetyharness.

7 Bolt end caps back together and install sprays. Hand injury due to wrench slipping. Slipping andfalling.

Wear gloves and watch for pinch points. Wear face shield.Watch footing and wear safety harness. Pull wrench towardbody to prevent slipping.

8 Exit gyp hopper. Slipping and falling. Watch footing and use hand holds. Wear gloves.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 002 Date written: 2/25/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Catch Attack SampleApproval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Walk out on top of attack. Tripping Eyes on Path

2 Fill sample cup to a few inches from top. Splash, Burn Wear acid jacket, rubber gloves and face shield when catchingsample.

3 a) Return to lab with lid on sample cup.b) If using cup without lid.

a) Trippingb) Tripping, Splash, Burn

a) Keep eyes on pathb) Keep eyes on path. Wear rubber gloves, face shield andlong acid jacket when transporting sample.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 003 Date written: 2/25/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Clean Vacuum Scrubber StrainerApproval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Valve out strainer and open drain. Hand injury on valve. Wear gloves.

2 Open the strainer, remove and clean. Water may spray out, pinch points, cut hand onstrainer. Hand injury due to wrench slipping.

Make sure drain is clear. Wear gloves. Pull wrench towardbody to prevent slipping.

3 Reinstall Strainer Pinch points, cut hand on strainer. Hand injury due towrench slipping.

Wear gloves. Pull wrench toward body to prevent slipping.

4 Open water valves. Hand injury on valve. Get sprayed with water. Wear gloves, make sure drain is closed, open valve slowly.checking for leaks

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 004 Date written: 2/25/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Catching Filter Cake Sample

Approval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Use shovel or dipper to scoop cake sample. Shovel or dipper getting caught on filter pan. Splintersfrom shovel.

Penetrate cake in front as far as possible. Wear gloves.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 005 Date written: 2/25/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Set Up Sulfuric to EvaporatorsApproval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Close all drains on sulfuric line to evaporators. Acid leaks, hand injury. Wear acid jacket with hood, acid pants, face shield, goggles,chemical gloves and boots Watch for pinch points.

2 Open the manual valves on the sulfuric line to theEvaporator

Acid leaks, hand injury. Wear acid jacket with hood, acid pants, face shield, goggles,chemical gloves and boots. Watch for pinch points.

3 Make sure evaporator is full of water. None. None.

4 Open auto valve to start flow of sulfuric. Acid leaks. Check line for leaks and secure line if it is leaking.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 006 Date written: 2/25/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Cutting Filter Cloths Off PansApproval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out.

None. None.

2 Cut the filter cloths off. Cuts to hands and fingers. Falling off filter. Wear cut resistant gloves. Use only lock blade knife. Keepfree hand behind the knife during cutting. Wear safety harnessand lanyard when not in hand rail area.

3 Pull cloth and fold up for easy handling. Put them inthe basket.

Back strain or slipping hazard. Use good footing and proper lifting techniques.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 007 Date written: 2/25/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Run Acid SampleApproval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Run Sample Broken Glass, Burn, Splash in eyes. Use PyrexPlus glass ware, safety glasses or goggles.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 008 Date written: 2/25/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Cleaning Barometric CondensersApproval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out.

None. None.

2 Place scaffolding boards across downleg. Pinch points, hand injury, falling into condenser. Wear gloves, safety harness and be aware of surroundings.

3 Climb inside condenser. Falling in downleg and pinch points. Falling build-up. Make sure scaffolding boards are covering downleg properly.Check overhead for build-up. Wear gloves, face shield, acidjacket. Use safety harness and lanyard.

4 Air hammer build up. Falling in downleg. Noise. Falling build-up. Hosecoming apart.

Make sure scaffolding boards are covering downleg properly.Be aware of surroundings. Wear gloves, face shield, acidjacket, ear plugs and ear muffs. Use safety harness andlanyard. Use safety pins in air hose.

5 Shovel build-up out manway. Falling in downleg and pinch points. Back and musclestrains.

Make sure scaffolding boards are covering downleg properly.Be aware of surroundings. Wear gloves. Use safety harnessand lanyard. Use proper lifting techniques.

6 Exit condenser. Pinch points, hand injury, falling into condenser. Wear gloves, safety harness and be aware of surroundings.

7 Remove scaffolding boards. Pinch points, hand injury, falling into condenser. Wear gloves, safety harness and be aware of surroundings.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 009 Date written: 2/25/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Packing Change – Primary and SecondaryVacuum Scrubbers.

Approval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out.

None. None.

2 Remove top grid from scrubber. Pinching hand under grid. Wear gloves.

3 Remove packing. None. None.

4 Remove lower grid from scrubber. Pinching hand under grid. Wear gloves.

5 Climb down into scrubber for inspection. Falling into scrubber. Use ladder and maintain 3 points of contact. Wear harness incase of rescue.

6 Install lower grid from scrubber. Pinching hand under grid. Wear gloves.

7 Install packing. None. None.

8 Install top grid from scrubber. Pinching hand under grid. Wear gloves.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 010 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Clean Pond Water StrainersApproval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out. PRODUCTION-NO PERMIT REQUIRED

None. None.

2 Open drain on bottom of strainer. Splash from pond water. Wear acid jacket, face shield and chemical gloves.

3 Remove bolts from strainer lid. Splash from pond water. Hand injury. Wear acid jacket, face shield and chemical gloves. Use wrenchto hold bolts when using impact wrench. Pull wrench towardbody to prevent slipping.

4 Remove strainer. Splash from pond water. Muscle strain. Wear acid jacket, face shield and chemical gloves. Use hoist topull strainer if necessary.

5 Wash out strainer. Splash back. Wear acid jacket, face shield and chemical gloves.

6 Install strainer. Muscle strain. Use hoist to install strainer if necessary.

7 Bolt lid back in place. Hand injury. Use wrench to hold bolts when using impact wrench. Pullwrench toward body to prevent slipping.

8 Put strainer back in service. Blown gasket, spray from pond water. Wear acid jacket, face shield and chemical gloves.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 011 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Cleaning CatchallsApproval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out.

None. None.

2 Enter catchall. Could slip and fall. Falling build-up. Have watchman assist you. Inspect over head before entering.Wear safety harness and lanyard. Tie off outside of catchall.

3 Clean catchall. Could fall through the floor. Could easily slip on domefloor. Heat and fumes may be a hazard.

Wear safety harness and lanyard. Tie off outside of catchall. .Wear rubber boots and watch footing. Were respirator ifneeded. If you get hot, get out.

4 Exit catchall. Slip or fall. Have watchman assist you.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 012 Date written: 2/27/08 Date reviewed:

Approval (name): Date reviewed: 01/30/09Task:

Cleaning Slurry Distribution Boxes with FilterDown Approval signature: ______________ Approval (name): Mark Denz

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out.

None. None.

2 Remove lids. Falling through fume hood,. Fumes. Stand on I-Beams and grating. Do not stand on fume hood.Use respirator if necessary.

3 Clean boxes. Splash back. Falling through fume hood. Wear face shield and gloves. Stand on I-Beams and grating.Do not stand on fume hood.

4 Install lids. Falling through fume hood. Stand on I-Beams and grating. Do not stand on fume hood.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 013 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Clean Pump Impeller Approval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out.

None. None.

2 Clean lumps from impeller. Getting cut from sharp edges on impeller. Wear cut resistant gloves and use caution.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 014 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Waterblasting Tubes or PipingApproval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out.

None. None.

2 Inspect all blasting hoses before starting blaster. Being cut from metal braids sticking out of frayedhose.

Wear leather gloves and use caution.

3 Insert wand in tube or pipe. Hose turning around in pipe and coming back towardyou.

Make sure wand is at least twice as long as the pipe is wide.Example: A 6” pipe requires at least a 12” wand.

4 Begin water blasting. Ruptured hose, back spray, flying debris, hose comingout of tube or pipe.

Always have a watchman before water blasting. If hoseruptures, have watchman shut off water blaster. Wear rain suit,face shield, tall rubber boots, rubber gloves.

5 Release foot pedal. Foot pedal not releasing Have watchman shut off water blaster.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 015 Date written: 2/27/08 Date reviewed:

Approval (name): Date reviewed: 01/30/09Task:

Change Filter Cloths Approval signature: ______________ Approval (name): Mark Denz

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out.

None. None.

2 Climb up on filter. Falling off ladder or filter. Maintain 3 points of contact when climbing ladder. Use fallprotection if out of handrail area.

3 Knock pins out and clean rails. Hammer slipping, pinch points, hitting self or someoneelse. Flying debris.

Use dry gloves and good grip on hammer. Be aware of othersin area. Wear face shield.

4 Wash rails and pan. Splash back. Wear face shield.

5 Inspect/Install new rubber. Cutting hand. Wear gloves. Use proper cutting technique.

6 Install new cloth. Hammer slipping, pinch points, hitting self or someoneelse. Flying debris.

Use dry gloves and good grip on hammer. Be aware of othersin area. Wear face shield.

7 Climb down off filter. Falling off ladder. Maintain 3 points of contact when climbing ladder.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 016 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Patching Filter ClothApproval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out.

None. None.

2 Cut new patches from spare cloth. Cutting hand. Wear cut resistant gloves. Use proper cutting technique.

3 Climb up on filter. Falling off ladder or filter. Maintain 3 points of contact when climbing ladder. Use fallprotection if out of handrail area.

4 Patch filter cloth. Cutting hand. Getting poked with needle from taggergun.

Wear cut resistant gloves. Use proper cutting technique. Usecaution when working with tagger gun.

5 Climb down off filter. Falling off ladder. Maintain 3 points of contact when climbing ladder.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 017 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Packing Change on East & West FumeScrubbers

Approval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out.

None. None.

2 Remove lids from scrubber. Falling into scrubber. Pinched between handrail. Wear fall protection. Be aware of surroundings.

3 Open bottom doors on scrubber. Pond water splash. Pinch points. Wear face shield and rubber gloves. Use wrench on boltswhen using impact wrench.

4 Remove packing from scrubber. Falling into scrubber. Splash back. Wear fall protection when on top of scrubber and as you godown with the packing. Wear face shield.

5 Remove spray nozzles. Pond water splash. Slip or trip. Wear face shield, rubber boots and rubber gloves. Watchfooting on sloped floor. Be aware of surroundings.

6 Wash packing. Splash back. Wear face shield.

7 Clean nozzles. Hand injury. Wear gloves.

8 Install nozzles. Slip or trip. Watch footing on sloped floor. Be aware of surroundings.

9 Close bottom doors on scrubber. Pinch points. Wear gloves. Use wrench on bolts when using impact wrench.

10 Put packing back in scrubber. Falling into scrubber. Pinched between handrail. Wear fall protection. Be aware of surroundings.

11 Put lids on scrubber. Falling into scrubber. Pinched between handrail. Wear fall protection. Be aware of surroundings.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 018 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Clean Flash Cooler Nozzles Approval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out.

None. None.

2 Remove cover from clean out shoot. Muscle strain, pinch points. Get help removing cover and be aware of surroundings.

3 Begin air hammering nozzle. Flying debris, falling off scaffolding. Pinch points.Hose coming apart.

Wear face shield and fall protection. Be aware of surroundings.Watch footing. Use safety pins in air hose.

4 Put cover back over clean out shoot. Muscle strain, pinch points. Get help installing cover and be aware of surroundings.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 019 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Packing Change—Flash Cooler VacuumScrubber

Approval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out.

None. None.

2 Rake packing out through bottom door. Pinch points. Keep eyes on task.

3 Enter scrubber to clean grating. Awkward positioning. Falling through loose grating. Keep eyes on task. Use proper body positioning. Check forloose grating before entering.

4 Clean grating with hammer. Pinch points. Flying debris. Keep eyes on task. Use proper body positioning. Wear faceshield and gloves.

5 Exit scrubber. Awkward positioning. Keep eyes on task. Use proper body positioning.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 020 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Opening and Closing All Manual Sulfuric AcidValves

Approval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Open or close valve Piping, flange, valve ect… leaking sulfuric acid. Wear acid jacket with hood, acid pants, face shield, goggles,chemical gloves and boots.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 021 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Pressurizing a line with Sulfuric, Phos Acid,Scrub Water or Pond Water.

Approval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Start acid pump. Line blowing out, line leaking andsplash from acid, scrub water, orpond water.

Verify that all drains and sample ports areclosed and all valves on the line are open.Make sure that all people in the area,including pipe racks, are clear when startingpump and establishing flow. Check line forleaks after flow is established.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 022 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Clean acid trap, receivers and vacuumscrubber seal tank

Approval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out.

None. None.

2 Climb into vessel. Slip, fall. Use correct body positioning. Be aware of surroundings.

3 Air hammer build-up. Pinch points, flying debris and noise. Hose comingapart.

Be aware of surroundings. Wear face shield, ear muffs andgloves. Use safety pins in air hose.

4 Wash vessel. Splash back. Wear face shield.

5 Climb out of vessel. Slip, fall. Use correct body positioning. Be aware of surroundings.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 023 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Clean filtrate seal tanks, hot wells, attacktanks

Approval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out.

None. None.

2 Enter tank. Product build up overhead ,and slipperyconditions.

Look overhead for build up and wear rubber boots.*If a Permit Required Class “A” Entry-Must wear safetyharness and lanyard unless entanglement becomes ahazard then lanyard not required.

3 Clean tank. Slippery conditions, splash back, and loudnoise. Hose coming apart.

Watch footing, wear face shield, acid suit, rubbergloves, rubber boots. Wear ear plugs and ear muffswhen using air hammer. Use safety pins in air hose.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 024 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Clean Flash Cooler Piping on GroundApproval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Secure piping. Pipe rolling due to sloped surface or from build-upbeing removed.

Chalk piping.

2 Air hammer build-up in piping. Flying debris. Large pieces of build-up falling from topof piping. Hose coming apart.

Wear face shield. Cut build-up off top of pipe before entering.Use safety pins in air hose. Use ear muffs when inside pipe airhammering.

3 Wash piping. Splash back, others being splashed. Wear face shield. Barricade area.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 025 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Unplug Sample PortsApproval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Shut down pump. Getting sprayed from around seal. Wear long acid jacket(or full acid suit) face shield, goggles andchemical gloves.

2 Rod out sample port. Line of fire. Getting sprayed when sample port clears. Stand to the side. Wear long acid jacket(or full acid suit) faceshield, goggles and chemical gloves

3 Start pump. Line blowing out, acid leaking. Verify that all valves on the line are open. Make sure that allpeople in the area, including pipe racks from Phos Acid toClarification and battery limits, are clear when starting pumpand establishing flow

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 026 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Mark Tubes in EvaporatorsApproval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out.

None. None.

2 Mark tubes in top. Falling off ladder. Maintain 3 points of contact.

3 Mark tubes in bottom. Slippery surface. Acid dripping from tubes. Lay platform over lump screen for better footing. Wear faceshield, acid jacket and gloves.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 027 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Clean Inside Flash CoolersApproval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out.

None. None.

2 Enter flash cooler. Slip and fall (flash cooler has slopped floor). Fallingbuild-up.

Watch footing. Wear fall protection. Look over head beforeentering.

3 Air hammer nozzles. Pinch points. Noise. Flying debris. Be aware of surroundings. Wear ear muffs, face shield andgloves.

4 Shovel build up out of cooler. Slip and fall (flash cooler has slopped floor), musclestrain.

Watch footing. Wear fall protection, Use Proper bodypositioning.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 028 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Clean Attack Agitators and 3rd Flash CoolerPumps on Ground

Approval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Remove buildup with sledge hammer and airhammer.

Flying debris. Getting cut by pump or agitator blades.Large falling lumps.

Wear face shield, long welding sleeves and cut residentgloves. Do not work under any large build-up. Cover bladeswith welding blanket finished.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 029 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Packing Change on 3rd Fume ScrubbersApproval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out.

None. None.

2 Remove lids from scrubber. Falling into scrubber. Pinched between handrail. Wear fall protection. Be aware of surroundings.

3 Open bottom doors on scrubber. Pond water splash. Pinch points. Wear face shield and rubber gloves. Use wrench on boltswhen using impact wrench.

4 Remove packing baskets from scrubber. Falling into scrubber. Pinched between handrail. Wear fall protection. Be aware of surroundings.

5 Remove spray nozzles. Pond water splash. Slip or trip. Wear face shield, rubber boots and rubber gloves. Watchfooting on sloped floor. Be aware of surroundings.

6 Wash packing. Splash back. Wear face shield.

7 Clean nozzles. Hand injury. Wear gloves.

8 Install nozzles. Slip or trip. Watch footing on sloped floor. Be aware of surroundings.

9 Close bottom doors on scrubber. Pinch points. Wear gloves. Use wrench on bolts when using impact wrench.

10 Put packing baskets back in scrubber. Falling into scrubber. Pinched between handrail. Wear fall protection. Be aware of surroundings.

11 Put lids on scrubber. Falling into scrubber. Pinched between handrail. Wear fall protection. Be aware of surroundings.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 030 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Put New Floc Bag on HopperApproval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Inspect hoist before using. None. None.

2 Cut plastic wrapping off bag. Getting cut. Wear gloves. Use proper cutting technique.

3 Raise Floc bag over hopper. Bag fallen due to various reasons. Ensure bag is properly hooked to hoist and aligned properly.Inspect straps on bag. Never stand below a suspended load.

4 Set bag on holding frame. Bag fallen due to various reasons. Hand injury. Keep hands out from underneath bag until bag rest on frame.

5 Reach under frame and open Floc bag. Spilling Floc. Proper alignment with hopper.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 031 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Cleaning Slurry Distribution Boxes with FilterRunning

Approval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Remove lids. Falling through fume hood,. Fumes. Stand on I-Beams and grating. Do not stand on fume hood.Use respirator if necessary.

2 Clean boxes. Splash back. Falling through fume hood. Getting Rodcaught on filter.

Wear face shield and gloves. Stand on I-Beams and grating.Do not stand on fume hood. Do not use rod that will go throughholes in bottom of slurry box.

3 Install lids. Falling through fume hood. Stand on I-Beams and grating. Do not stand on fume hood.

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JOB SAFETY HAZARD ANALYSIS

INITIAL REVIEWED

Area: Phos Acid Prepared by: Steve McAfee Prepared by:

Facility: New Wales Reviewed: Reviewed:

JSA No.: 032 Date written: 2/27/08 Date reviewed: 01/30/09

Approval (name): Approval (name): Mark DenzTask:

Clean Filter CrownApproval signature: ______________ Approval signature: ______________

Step Work Step Potential Hazards Corrective Actions

1 Verify that all equipment is properly isolated andlocked out.

None. None.

2 Raise filter crown Pinch points. Raising to high. Be sure that everyone is clear. Have some watch if needed socrown doesn’t get raised to high.

3 Clean crown Crown lowering. Pinch points. Use blocks to chalk crown.

4 Lower crown Pinch points. Be sure that blocks are removed and everyone is clear beforelowering crown.

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