making neutrons and using them - nist · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100...

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MAKING NEUTRONS AND USING THEM Boualem Hammouda National Institute of Standards and Technology Center for Neutron Research neutron scattering neutron irradiation cold neutron source core region reflector region

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Page 1: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

MAKING NEUTRONS AND USING THEM

Boualem HammoudaNational Institute of Standards and Technology

Center for Neutron Research

neutron scatteringneutron

irradiation

cold neutron sourcecore region

reflector region

Page 2: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

1. MAKING NEUTRONS

Page 3: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

Hydrogen

Uranium

ChlorineSodium

Helium

PERIODIC TABLE OF THE ELEMENTS

The Hubbard Chart of the Atoms (1924) was developed at the National Institute of Standards and Technology as an early version of Mendeleev’s periodic table (1920).

Plutonium

Page 4: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

NUCLEUS INSIDE THE ATOM

Nucleus=10-13 cm

Electron (beta particle)

proton

Atom~1 Angstrom=10-8 cm

X-Ray ~ keV

Light ~ eV

Atomic and nuclear transitions.

neutronGamma-ray ~ MeV

Page 5: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

Alpha Helium-41836mm

electron

proton =

ElectronBeta

neutronproton m~m

ELEMENTARY PARTICLES

Proton Hydrogen nucleus

Neutron

Page 6: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

PHOTON WAVELENGTHS

Spectral ranges of various electromagnetic radiations and energy windows

X rays

Gamma rays

VisInfrared

UV

10-2 Å 1 Å 102 Å 104 Å 106 Å 108 ÅWavelength

1.2 eVEnergy1.2*106 eV 1.2*10-4 eV

Page 7: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

0

20

40

60

80

100

120

140

0 20 40 60 80 100 120 140

Num

ber o

f Pro

tons

(Z)

Ato

mic

Num

ber

Number of Neutrons (N)

alpha emission

N = Z line

betaemission

STABLE/UNSTABLE ELEMENTS

Points represent stable elements. Radioactive decay occurs above and below this band of stable elements.

isotopes

Page 8: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

STABLE/UNSTABLE ELEMENTS

Photo of the walkway area behind the Radiation Physics Building at the National Institute of Standards and Technology. The horizontal axis is the number of neutrons and the vertical axis is the number of protons.

Page 9: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

NUCLEAR FISSION

Fission Chain Reaction

fission fragment

2 to 3 fissionneutrons

gammasneutrons are slowed down in water

fissile nucleus(U-235, Pu-239)

incidentneutron

1 electron volt = 1.6 *10-19 joules

Neutrons are emitted with 2 MeV energiesThey are slowed down to 25 meV

Page 10: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

NUCLEAR FISSION

Cerenkov radiation characteristic of fission reactions (Light Water Reactor).

Page 11: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

MAJOR RESEARCH REACTORS IN THE US

National Labs:

-- Oak Ridge National Laboratory (HFIR). 85 Megawatts-- National Institute of Standards and Technology (NCNR). 20 Megawatts

University-Based:

-- University of Missouri-Columbia (MURR). 10 Megawatts-- University of Michigan (Phoenix Project). 2 Megawatts

Page 12: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

UNITS INTRODUCED

Length Unit:1 angstrom = 10-8 cm = 10-10 meters

Energy Unit:1 electron volt (eV) ~ 10-19 joules1 keV = 103 eV1 MeV = 106 eV1 meV = 10-3 eV

Force Unit:1 newton = 1 kg*m/s2

Force-Energy Relationship:1 joule = 1 newton*meter

Power:1 watt = 1 joule/s

Page 13: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

2. USING NEUTRONS

Page 14: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

Neutron Radiography

Neutron Activation Analysis

RadioisotopesApplications

USING NEUTRONS

Neutron Processing

neutron irradiation

core region

reflector region

Page 15: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

NEUTRON ACTIVATION ANALYSIS

Page 16: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

THE NEUTRON ACTIVATION ANALYSIS TECHNIQUE

1000

104

105

106

800 900 1000 1100 1200 1300 1400 1500 1600

Cou

nts

Energy (keV)

Sc

Fe

Sc

Rb

Co

Fe

Co Na

Eu

La

Ta Zn

Irradiated samples become radioactive (emit gamma rays).

Page 17: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

EXTINCTION OF THE DINOSAURS

A thin layer of iridium was detected by NAA. This layer was deposited by the impact of a huge meteorite and was related to the extinction of the dinosaurs some 65 million years ago.

L. Alvarez

240

245

250

255

260

265

270

275

1 10 100 1000 104

Dep

th (m

eter

s)

Iridium Abundance (parts per trillion)

240

245

250

255

260

265

270

275

0.1 1 10 100 D

epth

(met

ers)

Pollen/Spore Ratio

Page 18: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

VOLCANIC ERUPTIONS HISTORY FROM TREE RINGS ANALYSIS

Trace amounts of gold are detected in tree rings and related to documentedvolcanic eruptions over the past 500 years.

Page 19: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

Ele

men

t 2Element 1

APPLICATIONS IN ARCHEOLOGY

statistical clusters

NAA is used to determine the provenance of art objects. A Greek vase is shown on the left and statistical clusters corresponding to different pottery periods are mapped out on the right.

Page 20: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

FORENSIC SCIENCE

NAA is used to detect trace elements of gun powder.

Page 21: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

“Saint Rosalie Interceding for the Plague-Stricken of Palermo” painted by the Flemish painter Anthony van Dyck in 1624 on the left. Autoradiography unraveled the self portrait of the painter underneath shown on the right.

ART HISTORY

Page 22: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

RADIOISOTOPES APPLICATIONS

Page 23: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

RADIODATING

Radioisotope C-14 has a half life of 5,730 years. The ratio of C-12 to C-14 is used for radiodating very old organic matter.

U-234 has a half life of 233,000 years. The U-234/Th-230 ratiois used to date rock formations on a long time scale.

The Rb-87/Sr-87 ratio is used to date igneous and metamorphic rocks over billions of years time scale…

Page 24: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

RADIOISOTOPE GENERATOR

A radioisotope generator uses the continuous decay of a long half-life parent to produce a short half-life product. Cows that are milked on site.

)hours 67(T Technicium givesMoly 21 =

)hours 6(T decays 99-echniciumT 21 =

Page 25: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

BONE CANCER THERAPY AND IMAGING

89Strontium − 50 days Bone cancer therapy

Half-life Radioisotope UseElement

Page 26: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

MEDICAL APPLICATIONS OF GAMMA RAY IMAGING

125Iodine− 59 days Lexiscope imaging

Half-life Radioisotope UseElement

Page 27: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

INDUSTRIAL APPLICATIONS OF GAMMA RAY IMAGING

55-Iron 2.7 years Lexiscope imaging

Half-life Radioisotope UseElement

Page 28: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

MORE RADIOISOTOPES APPLICATIONS

Smoke detector uses Nickel-63.

Heart pacemaker uses Plutonium-238.

Page 29: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

COBALT–60 MEDICAL IRRADIATION FACILITY

The Cobalt-60 cancer radiation therapy machine.

The “gamma knife” is used for localized radiation treatment of the brain.

Page 30: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

NEUTRON RADIOGRAPHY

Page 31: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

RADIOGRAPHY OF A CAMERA

Neutron radiograph

X-ray radiograph

D. Jacobson

Page 32: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

HYDROGEN FUEL CELL

hydrogen + oxygen water + electricity

Page 33: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

NEUTRON RADIOGRAPHY OF HYDROGEN FUEL CELL

Real time radiography of water flow inside the fuel cell

Page 34: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

NEUTRON PROCESSING

Page 35: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

PRODUCTION OF NUCLEOPORE FILTER

A roll of polycarbonate film is made to pass next to a fission plate. Fission fragments create uniform pores on the film changing it to Nucleopore filter material.

Nucleopore filters (submicron pores) are used in chemistry and molecular biology. They are able to trap cells.

Page 36: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

TRANSMUTATION DOPING OF SILICON SEMICONDUCTOR

Ingots of high purity single crystal silicon are irradiated in nuclear reactors to produce semiconductor. Phosphorus-31 acts as an electron donor.

Silicon is the second most abundant element in the earth’s crust after oxygen. It is obtained from sand (silicon oxide) and is widely used as a semiconductorin the computer and electronics industries.

Used to make transistors, integrated circuits, IR detectors, power rectifiers, in energy production and storage applications.

Page 37: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

COLORATION OF GEMSTONES

Topaz is mined in Australia, Brazil, India, Nigeria, and Sri Lanka.

Neutron irradiation produces color centers in gemstones.

Some 13,000 pounds of Topaz are irradiated every year worldwide, 40 % of which is done in the US.

Page 38: Making Neutrons and Using Them - NIST · 2011. 5. 19. · 40 60 80 100 120 140 0 20 40 60 80 100 120 140 Number of Protons (Z) Atomic Number Number of Neutrons (N) alpha emission

SUMMARY

Neutron Radiography

Neutron Activation Analysis

RadioisotopesApplications

Neutron Processing

NEUTRONS ARE FUN

LEARN MORE ABOUT WHAT THEY CAN DO