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Fast optical metrology of the hard x-ray optics for the High Energy Focusing Telescope (HEFT) Mario A. Jimenez-Garate, William W. Craig, Charles J. Hailey Columbia Astrophysics Laboratory, Columbia University 538 West 120 th street New York, NY 10027 ABSTRACT We describe a fast figure metrology system designed for the several thousand mirror quadrants in the High Energy Focusing Telescope (HEFT) balloon experiment. HEFT's multilayer coated hard x-ray optics will have ~ 1 arcminute HEW and operate at 20-80 keV. The optics are a conical approximation to the Wolter-I configuration. Our automated system can measure the axial figure error, in-phase and out-of-phase roundness errors of a mirror quadrant, and output their HEW contribution to the x-ray telescope. An optical laser scans a conical mirror in two cylindrical coordinate axes. A 2-D position sensitive diode (PSD) measures the reflected beam to ~ 4 arcseconds. The conical mirror can have 3 cm radius. We show the figure measurements of HEFT's aluminum foil and thermally formed glass substrates. Keywords: x-ray optics, surface metrology, x-ray telescopes, surface figure, optical testing, Wolter I optics, thin foil optics 1. INTRODUCTION The scanning apparatus we describe is designed to test the focusing hard x-ray optics for both the HEFT 1 balloon telescope and the proposed Hard X-ray Telescope (HXT) designs for the Constellation-X mission 2 . We are fabricating and testing x- ray optics for the HEFT telescope. HEFT will be the first focussing telescope in the 20-80 keV band, using graded d-spacing multilayer coatings to reflect hard x-rays by Bragg diffraction. To be launched in a balloon by the year 2001, it will perform an order of magnitude better than its predecessors in this energy band, outperforming even those in satellite platforms. The Constellation-X HXT requirements for the x-ray optic substrates are a factor of two tighter (0.5 arcsecond Half-Energy Width or HEW) than the HEFT goal (Table 1.) We are producing a new type of substrate by thermally forming glass 1,3 . X-ray scattering measurements indicate the microroughness is 3.5 Å, and multilayers deposited on these substrates have similar microroughness 4 . This translates to higher reflectivity in the hard x-ray band compared to epoxy-replicated foils. Large-scale figure measurements also satisfied the HEFT specifications 1 . However, we have observed that variations in the thermal processing of the substrate can introduce large-scale figure errors, in the order of 1 cm or greater wavelength. To control these large-scale figure errors of the substrate, we need a fast and efficient measurement apparatus. An interferometric measurement of the substrate is inadequate because the substrate is usually bowed before it is mounted, which makes it hard to compare to a cylindrical master. Typical interferometers do not span the desired correlation length and surface feature height scales needed for the HEFT optics (§3.1). Laser scanning has previously been used to measure the curvature of silicon wafers 5 . Long trace profilometer measurements have been performed on the XMM parabola-hyperbola shell mandrels using a 1-D stage that scans in a horizontal position while a mount rotates the mandrel 6 . AXAF mirrors were measured using separate axial and circularity setups 7 . Our design differs in that it profiles cylindrical-quadrant-shell mirrors, and can scan in axial and azimuthal directions, similar to the optical scanning setup for SODART 8,9 . It measures the different figure requirements of hard x-ray optics. We describe these figure requirements in §2 and a setup to verify them in §3 and §4. 2. X-RAY MIRROR REQUIREMENTS Correspondence: Mario A. Jimenez-Garate. [email protected] Telephone: (914)-591-2892 Fax: (914)-591-4906

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Page 1: Fast optical metrology of the hard x-ray optics for the High ...mario/public_html/papers/spie98...Fast optical metrology of the hard x-ray optics for the High Energy Focusing Telescope

Fast optical metrology of the hard x-ray optics for the High EnergyFocusing Telescope (HEFT) †

Mario A. Jimenez-Garate, William W. Craig, Charles J. Hailey

Columbia Astrophysics Laboratory, Columbia University538 West 120th street New York, NY 10027

ABSTRACT

We describe a fast figure metrology system designed for the several thousand mirror quadrants in the High Energy FocusingTelescope (HEFT) balloon experiment. HEFT's multilayer coated hard x-ray optics will have ~ 1 arcminute HEW andoperate at 20-80 keV. The optics are a conical approximation to the Wolter-I configuration. Our automated system canmeasure the axial figure error, in-phase and out-of-phase roundness errors of a mirror quadrant, and output their HEWcontribution to the x-ray telescope. An optical laser scans a conical mirror in two cylindrical coordinate axes. A 2-Dposition sensitive diode (PSD) measures the reflected beam to ~ 4 arcseconds. The conical mirror can have ≥ 3 cm radius.We show the figure measurements of HEFT's aluminum foil and thermally formed glass substrates.

Keywords: x-ray optics, surface metrology, x-ray telescopes, surface figure, optical testing, Wolter I optics, thin foil optics

1. INTRODUCTION

The scanning apparatus we describe is designed to test the focusing hard x-ray optics for both the HEFT1 balloon telescopeand the proposed Hard X-ray Telescope (HXT) designs for the Constellation-X mission2. We are fabricating and testing x-ray optics for the HEFT telescope. HEFT will be the first focussing telescope in the 20-80 keV band, using graded d-spacingmultilayer coatings to reflect hard x-rays by Bragg diffraction. To be launched in a balloon by the year 2001, it will performan order of magnitude better than its predecessors in this energy band, outperforming even those in satellite platforms. TheConstellation-X HXT requirements for the x-ray optic substrates are a factor of two tighter (0.5 arcsecond Half-Energy Widthor HEW) than the HEFT goal (Table 1.)

We are producing a new type of substrate by thermally forming glass1,3. X-ray scattering measurements indicate themicroroughness is 3.5 Å, and multilayers deposited on these substrates have similar microroughness4. This translates tohigher reflectivity in the hard x-ray band compared to epoxy-replicated foils. Large-scale figure measurements also satisfiedthe HEFT specifications1. However, we have observed that variations in the thermal processing of the substrate canintroduce large-scale figure errors, in the order of 1 cm or greater wavelength. To control these large-scale figure errors ofthe substrate, we need a fast and efficient measurement apparatus. An interferometric measurement of the substrate isinadequate because the substrate is usually bowed before it is mounted, which makes it hard to compare to a cylindricalmaster. Typical interferometers do not span the desired correlation length and surface feature height scales needed for theHEFT optics (§3.1).

Laser scanning has previously been used to measure the curvature of silicon wafers5. Long trace profilometer measurementshave been performed on the XMM parabola-hyperbola shell mandrels using a 1-D stage that scans in a horizontal positionwhile a mount rotates the mandrel6. AXAF mirrors were measured using separate axial and circularity setups7. Our designdiffers in that it profiles cylindrical-quadrant-shell mirrors, and can scan in axial and azimuthal directions, similar to theoptical scanning setup for SODART8,9. It measures the different figure requirements of hard x-ray optics. We describe thesefigure requirements in §2 and a setup to verify them in §3 and §4.

2. X-RAY MIRROR REQUIREMENTS

† Correspondence: Mario A. Jimenez-Garate. [email protected] Telephone: (914)-591-2892 Fax: (914)-591-4906

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The HEFT optics consist of an array of 14 modules. Each module has a front and a rear section carrying 72 concentricconical shells that focus the x-rays onto the focal plane. This is the conical approximation to the Wolter-I configuration.Each section is put together from quadrant shells, fabricated and coated individually with a graded multilayer (Table 1).Constellation-X HXT optics will be similar, except more shells per section are desired and a longer substrate will be used.

Optics parameters HEFT1 Constellation-X HXT2

Type Conical approximationto Wolter-I (2 sectionsper module)

Conical approximation toWolter-I (2 sections permodule)

Angular resolution (HEW) 1-5 arcminutes 0.5-1 arcminuteField of view 17 arcminute 8-10 arcminutesNumber of optics modules 14 3 (for each of 6 satellites,

f=8.5 m)Number of shells per section 72 120 (f=8.5 m)Number of substrates per shell 4 TBDTotal number of substrates 8064 (> 4320 for f=8.5 m)Focal length 6 meters 8-12 metersModule tolerances: Conic approximation 0.4 arcminutes TBD Figure (axial figure and roundnesserrors included)

0.6 arcminutes TBD

Assembly 0.4 arcminutes TBD Scatter 0.1 arcminutes TBDMirror substrate parameters: Type of substrate Thermally formed glass Epoxy replicated foil or

thermally formed glass Thickness 300-500 µm 123-526 µm Radii 4-12 cm 3-14 cm Microroughness 3.5 Å ≤ 4.5 Å Length-diameter ratio (outer shell) 2 ~1.1 Graze angles 5-17 arcminutes 3-14 arcminutes (f=8.5 m)

Table 1. X-ray optics specifications for the modules, sections and individual shell substrates are shown. Note various otherdesigns are under analysis for the Constellation-X HXT2.

The constraints and specifications of a Wolter-I x-ray telescope are well-studied10,11,12,13. Point sources at the center of thefield-of-view produce a spot with some HEW due to imperfections in the optics system. The telescope’s HEW comes fromfigure errors, alignment errors, x-ray scattering, and the conical approximation to Wolter-I (Table 1). Our initial setup willmeasure figure errors, and we can derive their contribution to the HEW, termed (HEW)fig. Hard x-ray telescope HEWspecifications, although coarse compared to the current soft x-ray observatories, are challenging for the first generation ofhard x-ray optics which need to be quickly mass-produced at a low cost in order to obtain a significant effective area withvery small grazing angles.

The figure errors can be decomposed in several orthogonal error descriptors11,12,13. We mention three important descriptors.The axial figure or profile error consists of large wavelength slope imperfections along the cylindrical axis of the optic (1mmor greater correlation lengths in our case). Roundness errors are radius variations as a function of azimuthal angle thatremove the cylindrical piece from an ideal circular cross section. If these radii variations are consistent throughout theoptical axis of the piece, they are called in-phase roundness errors, and their contribution to the HEW is small because thegrazing angle at which photons reflect does not change from specification. If the radii variations change with axial position,they are called out-of-phase roundness errors and their contribution to the HEW is larger because they create slope variationsover the piece that change the grazing angle of the photons. We expect the axial figure error to dominate1.

What are the requirements for the components of the surface normal unit vector n̂ ? HEFT’s surface-figure error tolerancegoal is 0.6 arcminutes, i.e. (HEW)fig = 0.6 arcminutes, including axial figure errors, in-phase roundness errors and out-of-

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phase roundness errors1. We will consider each error’s contribution to (HEW)fig independently so that we obtain a constraintto the n̂ of our cylindrical mirror shell substrate.

Let ⊥++= nnnn o

rrr||ˆ , Eq. 1

where onn

r=ˆ for the surface normal of a perfect cylindrical mirror. The axial figure constrains the surface normal component

parallel to the cylinder axis, ||n

r . Variations in the surface normal component perpendicular to the optical axis, ⊥nr , are a

signature of in-phase and out-of-phase roundness errors. We will measure ||n

r and ⊥nr in angular units with our apparatus.

The axial figure component ||n

r dominates the focusing of x-rays onto the detectors, and is constrained by:13

( )24

||figHEW

n ≤r axial figure, for 50% of the surface. Eq. 2

In general, constraints for ⊥nr are more relaxed than for

||nr . The out-of phase roundness contribution to the blur is (HEW)fig =

Lr /24 ∆ , while for the in-phase roundness (HEW)fig = fr /24 ∆ , where r∆± is the radius variation, L is the axial length of

the cylindrical shell, and f is the focal length of the telescope13. This sets the following constraints on ⊥nr :

( )ρ24

LHEWn

fig≤⊥

r out-of-phase roundness, and ( )ρ24

fHEWn

fig≤⊥

r in-phase, both for 50% of the surface, Eq. 3

where ∆r = ρ⊥n

r , ρ is the azimuthal correlation length of a feature on the mirror of angle ⊥n

r that produces a shift in radius

∆r. Since L << f, the out-of phase roundness error tolerance is smaller than for the in-phase roundness.

3. DESIGN OF SCANNING APPARATUS

Our design extensively modifies a previous one used on SODART9. That design consists of a scanning structure that movesindependently of the sample and reflects a laser beam from it to probe its surface profile.

The x-ray optics that we are characterizing initially have a cylindrical shape. Similar to SODART8, our mirror shells arefabricated as quadrants or thirds of cylinders to be bent into cones at mounting3. Thus, it is appropriate to use an apparatusthat scans in cylindrical coordinates, a “cylinderometer” that measures the deviations of the optic from a perfect cylinder.

Since we would like to optimize the substrate fabrication and improve yield, it is imperative to immediately have data on theshell substrate’s figure. Furthermore, once our substrate fabrication is optimal, we must ascertain the quality of a goodnumber of our optics before mounting begins.

3.1 Goals

The purpose of our initial setup is to measure individual cylindrical optic shells with (HEW)fig to 15 arcseconds. This isadequate for the HXT and HEFT HEW requirements. To accomplish this, we need to measure ~6 arcsecond deviations in thelaser beam, or ~3 arcsecond deviations of the surface normal (see below). We will measure surface features in the 1mm-200mm correlation length range, with local surface slopes of ~3 arcseconds to 1 degree. The angular dynamic range is 103

µrad. At 1mm correlation length, our surface height dynamic range is 12nm-17 µm, while at 200mm wavelength the heightrange is 2 µm-3mm. We would like to scan substrates of various masses and sizes without major modifications in our setup(axial length ≤ 300 mm, radius ≥ 30 mm). ). To make rapid measurements, we built a computer-controlled scanning system.The main components are shown in Figure 1.

Assuming axial figure and out-of-phase roundness errors each contribute 15 arcseconds to (HEW)fig, we calculate the requiredsensitivity of our n̂ measurement using Eqs. 2 and 3. Our setup must measure both

||nr to ±3 arcseconds and ⊥n

r to ±36

arcseconds.

HEFT requires a total of 8064 shell quadrants or 6048 shell thirds (Table 1). In a two-year production timetable, we mustproduce ~16 flight-quality quadrants per day. Assuming a 50% yield, our figure measurement system must measure one

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shell every ~15 minutes to scan all the shell substrates. Designs for the HXT also require similar numbers of shells. Thus,the aim of our optical figure measurement system is to measure a shell quadrant in ~15 minutes because our shell-productionyield, still unknown, will drive our shell figure sampling scale.

Figure 1. Mechanical setup of a laser scanning apparatus. The device measures the deviations of a cylindrical substratefrom a perfect cylinder by reflecting a laser beam and measuring its deflection angle. It is designed to map the substrate inone step, therefore performing quality control measurements for a large number of x-ray optics. LLF = laser line filter, BS =beamsplitter, PSD = position sensitive detector. A tilt table and stage align the substrate (η1 through η3).

3.2 Equipment configuration

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We bounce a laser beam off the top surface of the substrate. The laser beam originates from the cylindrical axis of the mirrorby the use of a beamsplitter. Thus, scanning a perfect cylinder over the azimuthal angle does not change the angle ofreflection since the laser beam is normally reflected from the cylindrical surface. Due to the one-dimensional (1-D) curvatureof the cylinder, the laser spot will be focused in 1-D at a focal length of r/2, r the radius of the cylinder (with someaberration). Further from the cylinder’s focal point, the beam diverges, crosses the beamsplitter, and is focussed back to around spot on a PSD detector by use of a cylindrical lens. To filter out stray light, we use a laser line filter and a tube baffle(Figure 2).

A cylindrical scan requires the rotation axis of the scanning setup to be collinear with the center of curvature of thecylindrical mirror. A spool supports a rotation stage, and a mirror placed under the stage can reflect a horizontal laser beamonto a vertical beam. The vertical laser beam, positioned collinear to the rotation axis of the stage, is then deflected 45° bythe beamsplitter and onto the cylindrical mirror (Figures 1 and 2). The spool is machined so that its top and bottom surfacesare parallel to ~1 arcminute (§4.6).

A vertical linear stage holds a cantilevered aluminum beam that serves as an optical bench. The aluminum beam holds thebeamsplitter directly above the aperture of the rotational stage. Further towards the linear stage is the cylindrical lens. ThePSD is mounted on the vertical stage surface. The PSD measures the position of the centroid of the laser beam in 2-D,providing information on the cylindrical mirror surface normal. Following §3.1, our apparatus must resolve ±6 arcsecond

deflections in the PSD y direction and ±72 arcseconddeflections in PSD x (Figure 1).

The cantilevered beam must be stiff enough to have oscillationamplitudes smaller than the PSD resolution of ~4 µm, or anoscillation frequency higher than the surface sampling rate.We achieve this with a hollow rectangular beam made ofaluminum and two pairs of trusses connecting the beam to thetop of the vertical stage.

The vertical stage is mounted on a stiffened L-beam structure that connects it to the rotation stage. A wheel supports the L-beam on the far end and the rotational stage at the near end, as to minimize the forces on the rotational stage’s plate andmaximize the distance between the PSD and the beamsplitter. This distance, D, contributes linearly to the angular sensitivityof the apparatus, i.e. the precision to which we can measure the cylindrical mirror’s surface normals. The entire scanningapparatus rests on a vibration-isolated optical table.

Several types of scans are possible. Two useful scans are 1) a series of axial scans at different azimuthal angles and 2) agroup of azimuthal scans at different axial positions. The first will provide the best information on the axial figure error,while the second provides better information on the roundness errors. Measuring the laser deflection as a function of positionprovides information on how the surface normal changes throughout the mirror shell. The final output of the scan is thus theslope of the surface as a function of scanning position.

Figure 2. Top view schematic of the scanningoptical setup. A 10 mW CW 638 nm HeNe laserbeam is incident on the cylindrical mirror. Thescanning assembly (enclosed in dashed lines) canrotate around the center of curvature of thecylindrical mirror to perform azimuthal scans. Theassembly also scans in the axial direction,perpendicular to the page. The 1 mm laser spot iselongated after reflection on the substrate and isrestored to a circular spot on the PSD by acylindrical lens. The PSD reads out the intensity ofthe laser beam and its (x,y) coordinates.

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An alternative approach is to measure the curvature of the mirrors by using two slightly displaced beams incident on theglass. This means that only relative deflections are measured and many calibration problems eliminated. This addedcomplexity might pay off by increasing the sensitivity of the setup14.

3.2.1 Position sensitive detector (PSD) and analog-to-digital-converter card

The PSD is a Hamamatsu S1881, a 22mm x 22mm wafer diode that reads out the intensity of the incident light and thecentroid of the beam’s position (x,y). The position information is acquired by collecting a photocurrent with terminals at foursides of the wafer. The output range is 0-10 volts for the intensity readout and ±5.5 V for the x and y positions. The data isacquired and digitized with a Data Translation 16 bit DT16-EZ data acquisition PC-board in analog-to-digital-converter(ADC) mode running at 6 kHz, sufficient for a 103 µrad dynamic range. We achieve a ~4 µm resolution with this setup (see§4.1). Thus, for D = 600 mm, we can measure 6.7 µrad ≅ 1.5 arcsecond deflections. The PSD photosensitivity (currentproduced per incident luminous power) peaks at 900 nm, but it is only 30% smaller at 638 nm‡.

3.2.2 Motion control system

We use an Aerotech motion control system. We scan in cylindrical coordinates with the ART-320 rotating stage and theATS-15030-2-02B vertical stage. DC brush servo motors drive the stages, which include homing and limit switches and abrake for the vertical stage. A chassis with indicator LED’s and an emergency stop knob contains the BA-10 stage amplifiersand BB-501 interconnect board. An Aerotech U500 PC card controls the stages. The vertical stage has flatness, pitch andyaw tolerances of 4µm each, sufficient for our purposes. One advantage of having the scanning structure move (and not thesample) is that, with the working load constant, we adjust the servo loops only once for each stage.

3.2.3 Laser

We use a 10 mW, 638 nm CW He-Ne Uniphase laser in a cylindrical housing for rapid thermal stabilization. It has a 0.68mm spot size and 1.2 mrad divergence§. The power is sufficient to provide an adequate intensity for the PSD while scanningover an uncoated glass surface. This enables us to scan the thermally formed glass without modifying the PSD electronics, orapplying reflective coatings to the glass and potentially changing the microroughness of its surface. Our He-Ne laser has abetter pointing stability and smaller divergence than most other types (§4.1)15.

3.2.4 Optics

We use kinematic mirror mounts with a ~10 arcsecond resolution. This is important to co-align the laser beam with therotational axis (§4.6), but it is not strictly needed for single axial scans.

The major constraint for the optics in our scanning system is that they avoid introducing nonlinearities in the laser deviationduring a scan. Nonlinearities in the spatial laser deviation do exist, for example, as the beam transverses a flat piece of glass.If the angle of incidence is not zero, the transmitted beam is displaced with respect to the incident beam. The displacement ofthe beam changes as a function of the angle of incidence due to refraction, and there are nonlinearities of second order in theangle of incidence, as obtained with Snell’s law. These nonlinearities depend on the thickness of the optics and the angle ofincidence. For our 1 mm thick beamsplitter at 45°, there is a 0.2% nonlinear effect of the laser deflection at 20 arcseconds,and a 0.15% nonlinear effect for a 5 arcminute deflection. The fractional nonlinear effects through the cylindrical lens orlaser line filter are proportional to θ2, where θ = ±1° is the angle of incidence, giving 0.03%. The nonlinear refraction effectof the cylindrical lens and the laser line filter is very small because the laser beam is roughly at normal incidence, and it ispractically imperceptible by the PSD.

3.2.5 Software

To achieve a 15 minute scan per substrate we developed a customized scanning program that in one step synchronizes thestage motion with the PSD data acquisition and analyzes the data using Research Systems’ Interactive Data Language (IDL)package. Our program features a graphical user interface and a real-time graphical status of the laser position. The latter isespecially useful during alignment. ‡ Data from Hamamatsu Photonics§ Data from Newport Corporation

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Data acquisition proceeds as follows. The program requests the initial and final positions of the scan. The scan begins, andthe current laser spot position is displayed. The axial position of the vertical stage, azimuthal angle of the rotational stage,PSD spot position, and PSD intensity are continuously sampled from the ADC and stage controller cards and stored in a datafile. The PSD data is sampled at 6 kHz, but to reduce noise, we average every 100 data points for each of three channels(§4.1). Thus, we obtain PSD and stage position data at 20 Hz. After the scan is complete, the program calls an IDL code thatanalyzes the scan data. The necessary corrections and calibrations are performed in software.

For a single axial scan, a routine converts the slope information to a 1-D topographical map of the surface. Then a simplehalf-period sinusoid is fit to the topographical information to subtract any simple bending present in the cylindrical mirror.The residual topographical features are displayed and the HEW from axial figure is calculated (a single axial scan providesdata on the axial figure errors, and limited data on roundness out-of-phase errors).

The software for the azimuthal scans that measure the roundness errors is in development.

4. CALIBRATION AND ALIGNMENT

4.1 Laser and PSD stability

As a first step in our calibration, we verify the stability of both the laser and PSD. We measure the position resolution of oursystem, which determines the smallest angle to which we can measure deviations of the cylindrical mirror surface normal.The measurement consists of shining the laser directly on the PSD and monitoring the PSD position and intensity data for 1-4hours. A laser-line filter reduces the stray light intensity signal to less than ~0.2% of the laser intensity. We turn on thestages to provide good position stability through their servo loops, so we observe no linear drift in the position.

The PSD position and intensity standard deviations are larger if the laser is not allowed to warm up and reach thermalequilibrium. We know the laser reaches thermal equilibrium in ~2 hours or less. We measure the standard deviation of laserintensity, Iσ = 0.5 % over 30 minute measurements at thermal equilibrium (assuming a linear PSD response).

Instead of using the instantaneous position output from the PSD to make our laser deviation measurements, we takeadvantage of our 6 kHz ADC sampling rate to average a number of measurements and reduce the effect of electronic noise inour data. First, we collect n points of PSD data of value x and calculate their average xavg. We then calculate the standarddeviation of these averages (xavg)σ. So (xavg)σ ∝1/√n is expected (Table 2).

Number of datapoints in xavg (n)

(xavg)σσ

(mV)1σσ resolutionof PSD (µµm)

Expected value of (xavg)σσ

from statistics (mV)200 1.8 3.6 --500 2.4 4.8 1.13,333 0.84 1.68 0.44

Table 2. Data to determine the PSD resolution vs. data sampling rates. The measurements are also sensitive to laserstability. We obtained the data in 96 minute runs, except for n=200, which was a 34 minute run. Laser warm-up time is ~24hrs. Acquisition rate is 6 kHz.

There is no advantage in taking more than ~100 points of data for our average, so we choose n = 100. Taking even fewerpoints is incompatible with our current stage scanning rates and laser spot size. The PSD resolution improves with increasingphotocurrent (proportional to the light intensity incident on the PSD), so one must match the calibration’s photocurrent to theoperating photocurrent. The resolution is slightly better than our expectation for He-Ne lasers of 4-6 arcsecond laser pointinginstability for a 15-20 min warm-up (equivalent to 12-18 µm @ 600 mm for a 15 min warm-up) and 1% intensity stability15.

4.2 Position sensitive detector (PSD) and laser-line-filter (LLF) calibration

We perform a scan using the linear stage as a reference ruler to calibrate out the non-linear response of the PSD and LLFassembly. The calibration consists of detaching the PSD/LLF from the stage structure and replacing the cylindrical mirrorwith the PSD. In this way, the laser performs a series of linear scans on the PSD directly. The maximum nonlinearity on thePSD/LLF assembly occurs in scans through the entire PSD detector. This systematic error is generally in the shape of a pin-

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cushion distortion, producing some curvature in the slope measurements. That peak-to-valley nonlinearity is ~1.5arcminutes, but this error decreases in proportion to the fraction of PSD length used, so that if one tenth of the PSD is used,only ~0.15 arcminute error applies. Also, a scan through the center of the PSD will have a curvature error of ~50 arcsecondsin the scanning direction and a curvature of ~40 arcseconds in the perpendicular direction (for a scan over the 2° of the PSD).There are some local bumps with peak-to-valley amplitudes of as much as ~14 arcseconds over ~20 arcminutes of the PSD.

The LLF does not have a uniform spatial transmission coefficient, so that the intensity varies as much as 10% as the laserspot hits different points in the PSD/LLF assembly. Thus, the LLF could also be contributing to the nonlinearities in thepositioning response, so that every time the LLF is detached from the PSD, the system must be re-calibrated.

The calibration will produce three matrices that convert raw values of the PSD x, y and intensity I to the corrected values of x,y and I as a function of (x,y). As yet, this calibration is not finished, so for the time being we scan a piece in two differentspots in the PSD/LLF to estimate the systematic errors due to the PSD/LLF. Preliminary results indicate the PSD/LLF willbe calibrated to ≤ 6 arcseconds in (x,y).

4.3 Calibration of vertical stage straightness

We calibrate any repeatable flatness, pitch or yaw errors in the linear stage by using a reference flat. We use a λ/4 flat ofdiameter equal to the linear stage travel of 30 cm. The level of flatness errors is highly dependent on the mounting of thelinear stage, so every time the stage is repositioned, it must be re-calibrated. The maximum calibration corrections due to thevertical stage straightness range from 30-80 arcseconds and have been integrated into our software.

We do linear scans of the round reference flat at different angles and average the results in order to subtract any figure the flatmight have. After calibration of the linear stage, the error residuals for each of the PSD dimensions (x,y) have standarddeviations of σx = 5.1 arcseconds, σy = 5.2 arcseconds. Our flat was not coated on its front surface, so we used an anti-reflective coating on the rear part so the laser reflects only on the good part of the flat. The deviations σx and σy over-estimate the calibration errors by a factor of two or more since they include residual back-reflection effects (§4.5). The anti-reflective coating is not completely effective. Since the back surface is flat to several λ, interference fringes producesinusoidal intensity and position variations on the PSD. From the amplitude of these oscillations we estimate theircontribution to σx and σy, so we can isolate the straightness errors from the back reflection effects.

4.4 Measurement of linear stage vibration

The setup is the same as the PSD/LLF calibration. There are modulations on the position data of the PSD as it is scanned.The modulation amplitude is roughly proportional to the feedrate of the linear stage. Since these modulations are not presentin the measurements of the calibration flat, we conclude it is not a PSD effect but rather a stage vibration effect. The latteralso implies most vibrations do not come from beam deflections, since they would affect our slope measurements and shouldhave been observable while calibrating the flat. Thus, the stage structure as a whole is vibrating in the vertical direction, andthis will only affect the spot position on the mirror. Some of these vibrations come from the beamsplitter mounting, becausea change in the mounting changes the amplitude of the vibrations (Table 3). The frequency of the modulations is ≥ 20 Hz,the sampling rate of the PSD. The PSD was ~400 mm away from the beamsplitter, so each µm of

Linear stagefeedrate (mm/min)

Peak-to-valley amplitude ofvibrations (µµm)

Amplitude after beamsplittermounting adjustment (µµm)

10 6 ± 2 6 ± 125 16 ± 4 10 ± 250 30 ± 6 20 ± 6100 60 ± 16 --300 140 ± 30 --

Table 3. Vibration amplitudes in the vertical direction observed in the linear stage structure. The vibrations slightlyincrease the lower correlation length limit of the apparatus.

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vibration translates to 0.5 arcseconds in the case that the vibrations come from the end of the aluminum beam. Since our flatmeasurements did not detect such modulations to ~2 arcseconds at a feedrate of 100 mm/min, the beam deflection must belimited to ~4 µm.

The largest vibrations of the linear stage are only ~14% the size of the laser spot, which represents only a marginal sensitivitydegradation to our lower correlation length limit. It is possible that further tuning of the linear stage servo loop could reducevibrations at the highest feedrates.

4.5 Effects due to the back reflection in glass pieces.

Since the substrates will be coated with multilayers at the front surface, little or no treatment to the front surface is desired,since it could change the surface microroughness and thus the reflectivity of the optics in the x-ray band.

Hence, we intended to scan uncoated glass pieces. A laser beam incident on a clear glass sheet reflects both at the front andback surfaces. The two reflections have almost identical intensities, since they are both generated at an air/glass interface.We eliminate the back reflection with a low-cost removable anti-reflection coating at the back of the glass piece. The coatingconsists of a mixture of matte black watercolor and sugar, so it is soluble in water and easily removed. This coating’s indexof refraction matches that of the glass while absorbing entirely the transmitted light. With the coating, the back reflection is~4% of the incident intensity on the PSD. The residual position error due to the back reflection is ≤ 7 arcseconds.

4.6 Alignment

The alignment required depends on the type of scan one performs. A single axial scan requires the least alignment.The stage axis and the laser beam need only be aligned to < 1º so that the laser beam reflected off the cylindrical mirror fallswithin the PSD area. However, the cylindrical mirror axis must be aligned with respect to the axis of the scan to minimizedisplacements on the PSD detector. This misalignment limits the apparatus’ ability to measure simple bows in the piece towithin the amount of the misalignment, since linear shifts in our surface normal measurement correspond to parabolic surfacefeatures. The cylindrical mirror has five DOF. For an axial scan, only the two rotational DOF are important. The η1 degreeof freedom is the most important (Figure 1). As we scan, a misalignment in η1 can produce linear displacements in the both xand y coordinates of the PSD. A misalignment in η3 creates shifts in PSD y. Call these angular displacements δx and δy. Tolowest order in η1 and η3, the x and y coordinate angular shifts are

rx 1ρη

δ ≅ Eq. 4 ,( ) ( )

rDry

++≅

23

21 ηρηρ

δ Eq. 5

where ρ is the axial distance from the η1 rotation axis, r is the radius of the cylindrical mirror and D is the distance from thebeamsplitter to the PSD. Shifts in the PSD y coordinate correspond to bows in the cylindrical mirror, unless there is somemisalignment causing δy. For example, to detect a 15 arcsecond simple bow, δy must be less than 15 arcseconds, so thecylindrical mirror must be aligned to 13 arcminutes in η1 and to 52 arcminutes in η3. Note η3 need only be roughly alignedto be able to measure small bows. Fortunately, alignment of η1 is simplified by observing δx, which is linear in η1. Thecylindrical lens, though, focuses the δx and leaves δy unchanged. The transformation of angular deviations by the cylindricallens can be expressed as

yy δδ =′ ,Q

xx

δδ =′ , ( )rsD

DsQ

−=

2Eq. 6

where Q is the compression factor, the unprimed coordinates are deflections before the cylindrical lens while the primed after(the observable deviation on the PSD), s equals the distance from the cylindrical-lens to the focal line of the cylindricalmirror, r is the radius of the cylinder, and D is the distance from the PSD to the focal line of the cylindrical mirror (Figure 2).For our current setup, Q ~ 8. Using Eq. 6 and Eq. 8, aligning η1 to 13 arcminutes requires aligning δx’ to ~4 arcminutes inthe worst case scenario (cf. aligning δy to 15 arcseconds). Thus, to be able to measure bows in the piece accurately, we mustminimize the δx’ of the scan. To easily minimize δx’, shine the laser on the substrate with the stages static and move η1 untilan extremum in the x’ coordinate is reached. Then measure δx’ through a vertical scan of the substrate to verify alignment.

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To do a series of axial scans throughout the piece in different azimuthal angles, mapping the surface in one step, furtheralignment is necessary. The upward laser beam, vertical stage axis and optical table surface normal must be parallel to withinthe minimum tolerance required of η1 and η3. Following the previous example, measuring 15 arcsecond bows on each ofseveral scans through the piece requires the laser beam, stage axis and optical table normal to be parallel to ~13 arcminutes.We achieve this alignment in two steps with a penta prism replacing the beamsplitter, so that the laser is incident on the PSDand it does not leave the scanning structure. First, we rotate the stage with the scanning assembly. If the upward laser beamis collinear to the rotation axis, no displacement will be observed in the PSD. This aligns the laser beam with the rotationaxis. Second, we move the vertical stage. If the vertical stage axis is parallel to the laser beam, no displacement of the laserbeam on the PSD is observed. The parallelism is then limited by the performance of the penta prism and the error circle inwhich the spot lies on each calibration scan. We use a penta prism that bends a ray to 90º ±10 arcseconds. The error circleswe obtain are < 3 arcminutes for each case, currently limited by the wheel bounce (of ± 200 µm).

Once the alignment above is done, more stringent constraints apply to the cylindrical mirror positioning. For azimuthalscans, the two translational DOF of the cylindrical mirror become important in addition to η1 and η3. Both produce shifts inthe PSD x coordinate (δx), so the cylindrical mirror must be translated to minimize these shifts.

The beamsplitter must be roughly aligned to 45°, with the laser beam at its center. It should be rotated such that reflectedrays can be bounced back and transmitted through the beamsplitter casting a “shadow” roughly centered on the PSD, which isa distance D away.

Non-parallelism of the cylindrical-lens axis with respect to the scanned cylindrical-mirror’s axis creates a deformed spotshape on the PSD. This deformation does not affect the scan unless the spot changes shape through the scan, so that the lensdoes not need fine positioning. The distance s (Figure 2) should be adjusted to form a round spot on the PSD. That way, the

cylindrical lens does not compress δy, whichcarries information about

||nr . Future calibration

with a cylindrical master will verify the alignmentand calibration and should reveal nonlinear effectsdue to the cylindrical lens, if any.

To successfully align the optical system, the ruleis to have as many easily adjustable DOF aspossible for not only the optical parts but also thevertical stage. A set of nuts adjust the height ofthe L beam which holds the vertical stage, whichin turn adjust one rotational DOF of the verticalstage. The other DOF has to be manually adjustedby unscrewing the stage. The beamsplitter andcylindrical lens have practically all DOFadjustable conveniently through knobs and slots.The cylindrical mirror being measured has 2rotational DOF adjustable though a tilt table, anda third rotational DOF through a small rotationstage, forming 3 orthogonal rotational DOF. Thetranslation DOF of the stage will be adjusted inthe future with corresponding stages.

5. RESULTS

We have successfully analyzed axial scans from various cylindrical shell quadrant substrates using the setup in Figure 3. Forcomparison, we scan aluminum foil pieces produced for SODART and measured by their scanning apparatus8,9. Our primaryresult is the (HEW)fig from the axial figure errors. These results are consistent with the SODART measurements. We alsoscan thermally formed glass substrates.

We position cylindrical shell quadrants on a plane by freely sitting the pieces on three wires, with the cylindrical axisperpendicular to the table. Our first piece is a 300 µm-thick glass shell quadrant with a 62 mm radius of curvature. We scan

Figure 3. Laser scanning apparatus.

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the substrate over its 200 mm axial length near its azimuthal center. We cut about 20mm on each side of the axial scan datato focus on the central features. The laser deflection vs. scan position is our raw data. Note the surface normal deviation is afactor of two smaller than the laser deflection. We integrate the surface normal slope to obtain an axial surface profile(Figure 4a), and we smooth out the noise in the ≤ 1 mm correlation length scale. The height of the simple bow shape in thesubstrate is 15 ±2 µm. We fit a simple sinusoidal bow shape to the profile so that we can observe the features that willremain after mounting (Figure 4b). We differentiate the surface height residuals to get the residual laser deflections (Figure5a), and we find the width of slopes that include 50% of the data, termed W50.9 W50 equals the (HEW)fig of the axial figureerrors for a one-bounce focusing system. The mirror shell contribution to (HEW)fig in a Wolter-I configuration is (W50)√2,shown in Figure 5a, and we obtain (HEW)fig = 0.7 ±0.1 arcminutes. We measure (HEW)fig for pieces with larger bows to ±0.2

(4a) Glass (4b) Glass

Figure 4. Central axial scans over a glass piece. (a) Surface height profile, shown in a solid line, the dash-dotted line isa sinusoidal fit to this bow. (b) Residual obtained from the measured bow and its fit. The edges of the 200 mm-longpiece are cut out to show details of the central region. From the residual height we obtain the slope profile in Figure 4a.

(5a) Glass (5b) Aluminum foil

Figure 5. Central axial scans of the above glass piece and aluminum foil compared. (a) Residual laser deflections forone scan. The glass substrate had 62 mm radius and the scan was done within 20 degrees from the azimuthal center ofthe piece. (b) Aluminum foil laser deflection profile for a scan along the azimuthal center. The foil has a 45 mm radius.

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arcminute. The measured (HEW)fig holds only on the scanned region, an azimuthal line ~20° from the center and the central80% of the axial length. Including the full axial length in our (HEW)fig calculation, though, will not change the result bymore than 0.1 arcminutes. We repeat the procedure with a 400 µm thick aluminum foil substrate of 45 mm radius ofcurvature (Figure 5b). The makers of the SODART optics manufactured the aluminum substrate. The (HEW)fig we obtain isconsistent with previous SODART measurements of substrates with radius > 8 cm, where W50 ~ 0.7 arcminutes8,9. Our erroris dominated by uncalibrated PSD nonlinearities, but future calibrations will decrease our error bars by a factor of ~2.

Preliminary measurements indicate the roundness out-of-phase (HEW)fig ≤ 0.9 arcseconds in the 1 mm correlation length (ρ)only, but larger values of ρ will likely increase this (HEW)fig result. These measurements are subject to stage straightnesserrors in the PSD x direction that are more difficult to remove than those in the y direction. To estimate the out-of phaseroundness error from a single axial scan, we look for nonlinearities in the PSD x coordinate as a function of vertical scanningposition. Using Eq. 3 with ρ = 1 mm, we calculate the (HEW)fig contribution of the out-of-phase roundness error. Definitiveroundness measurements will be obtained by performing an azimuthal scan of the substrate or a large enough number of axialscans so that neighboring scans have ~1 mm separation. More measurements of the glass substrates can be found in acompanion paper3.

6. ACKNOWLEDGEMENTS

This project was funded under NASA grant NAG5-5129. Separate funding for the metrology hardware was provided byColumbia University through the Office of the Provost Strategic Initiative Program. We appreciate engineering support fromTodd Decker and Irwin Rochwarger of the Columbia Astrophysics Laboratory and contributions from Ralph Gardner, PaulBetts and David Thomas, of Columbia University Nevis Laboratories.

7. REFERENCES

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4. P. H. Mao et al., “Development of grazing incidence multilayer mirrors for hard x-ray focusing telescopes,” SPIE Proc.3114, pp. 526-534, EUV, X-Ray, and Gamma-Ray Instrumentation for Astronomy VIII, 1997.

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13. Aschenbach et al., “The High-Throughput X-ray Spectroscopy mission, report of the telescope working group”, ESASP-1084, pp. 22-25, Feb. 1987.

14. P. Glenn, “Lambda-over-one-thousand metrology results for steep aspheres using a curvature profiling technique,” SPIEProc. 1531, Advanced Optical Manufacturing and Testing II, 1991.

15. J. Hecht, The laser guidebook, McGraw-Hill, New York, 1986.