re: diamond alkali superfund site passaic river study area

PPG Industries, loc. One PPG Place Pittsburgh, Pennsylvania 15272

.Joseph M. K .....ARisl8nl CounHIlaw 0ep0WnenIDIr8ct DI8I: (4'2) 434-2415Telecopy: (412) ~

VIA CERTIFIED HAIL/RETURN RECEIPT REQUESTEDSeptember 18, 1996

( Re: Diamond Alkali Superfund SitePassaic River Study Area

Dear Mr. Richman:

This is in response to USEPA"s request for information regarding the above-referencedsite. PPG previously submitted a partial response to this request, a copy of which is attachedhereto.

As a preliminary matter, PPG objects to the Agency's request for information to the extentthat it seeks infonnation or action which exceeds EPA's statutory authority. PPG also objects tothe request to the extent it seeks information which is not relevant to the release of hazardoussubstances at the above-referenced site, or is a privileged communication.

Notwithstanding these objections, PPG has conducted a diligent search for informationresponse to the questions contained in the request. Based upon that search, PPG's responses areattached hereto. These responses address conditions at the former PPG facility in Newark, NewJersey during the period that PPG operated at that location.

Please contact me if you have any questions.

Sincerely,

~~J~se~M~~asAssistant Counsel

Attachme~

cc: ~elia Wagner, Esq.T. J. Ebbert

jmk~doc

..'

853220001

TIERRA-B-004351

REQUEST FOR INFORMATION

Background

The United States Environmental Protection Agency ("EPA") is investigating the release of hazardoussubstances into the Passaic River. EPA has infonnation indicating that hazardous substances from yourfacility located at 29 Riverside Avenue inNewark, New Jersey from 1920 through 1971 may have beendischarged into the Passaic River.

Provide the information requested below, including copies of all available documentation that supportsyour answers.

1) How long has your company operated at the facility designated above? If your company nolonger operates at this facility. during what years did your company operate at the facility?

PPG operated a paint manufacturing facility at 29 Riverside Avenue in Newark, NJ fromapprOXimately 1902 to 1971. PPG no longer operates at thisfacility.

2) Did your company receive, utilize, manufacture, discharge. release or dispose of any materialscontaining the following substances:

YES NO2,3,7.8-tetrachlorodibenzo-p-dioxin

or other dioxin compounds2.4-dichlorophenoxyacetic acid2,4,S~trichlorophenoxyacetic acidNapthaleneAlkyd resinsPhenolic resinsCarbon disulfideChlorofonnCyanogenMethyl Ethyl KetoneTetrachloroethaneTolueneXyleneEthyl benzeneTrans-I,2-dichloroetheneArsenicCadmiumChromiumCopperLeadMercuryNickel

853220002

TIERRA-B-004352

'.

YES NOSilverTitaniumZincCyanidePCBsBasic Lead Carbonate (White Lead)

PPG manufactured paint, varnish, linseed oil, and resins at its Newark facility. Basic raw materialsincluded natural gums and resins, flax seed, non-chlorinated solvents and pigments, though thechemical constituents of some oj these materials changed over time. Relative to the chemicals listedabove:

• Alkyd resins were manufactured at the site. Theseproducts were used by PPG as raw materialsin paint and varnish manufacture. Phenolic resins were not manufactured but would have beenreceived at the site and used as raw materials in the manufacture of paints and varnishes.

Toluene, rylene, ethylbenzene. and methyl ethyl ketone would have been received at the siteand used as raw materials in the manufacture of paints and varnishes.

• Pigments would have been brought to the site and used in the manufacture oj paints. Thesewere often metallic chemicals and would have included compounds of cadmium, chromium,lead, titanium and zinc. Basic lead carbonate (white lead) would have been one of thepigments used as a raWmaterial. Mercury was used, probably as a preservative in certainpaints.

• Small amounts of flaJcenaphthalene reportedly were used in lacquer production and smallamounts of copper oride reportedly were used in paint production. .

• PCBs, diorins, 2,4-dichlorophenoxyacetic acid, and 2,4,5-trichlorophenoryacetic acid wouldnot have been received, utilized, manuJactured, discharged. released, or disposed of at theNewark site.

• PPG believes that carbon disulfide, chloroform, tetrachloroethane, trans-l,2-dichloroethene,arsenic, cyanogen or cyanide were likewise not present at the site, particularly since thesechemicals are not normally associated with the types of operations conducted by PPG at thesite.

PPG has no information relative to nickel or silver, erc:eptto note that these metals are notcommonly found inpigments.

2 853220003

TIERRA-B-004353

3). a)· Provide a description of the manufacturing processes for which all hazardous substances,including, but not limited to, the substances listed in response to item (2), were a product or by-product.Include in your answer the identity and quantity of the raw materials combined in each process; thetemperature, pH and pressure of each process; and any residues or by-products generated as a result ofthe process.

RESPONSE: PPG manufactured paint, varnish, linseed oil, and resins at its Newark Paint Plant.Raw materials, consisting of resins, solvents, and pigments were mixed to produce paints. Varnisheswere made from resins. Oils, and solvents. linseed oil was manufactured at this facility using flax seedas the principal raw material. Small amounts of caustic soda were used in processing the oiL Solventsfrom cleaning manufacturing equipment and off-spec products were recycled by reuse in theproduction process or reclaimed to recover solvents. Wastes from solvent recovery typically consistedof still sludge which was drummed and sent offsite for disposal. Finished products were shipped intankwagons, drums or smaller containers. PPG has information about the identity of compounds thatwere used in the processes as indicated in response to question 2; however. information about thequantities, temperatures, pH and pressures. residues and by-products is not available.

b) During what parts of the manufacturing processes identified in the response to item(3)(a), above, were hazardous substances, including, but not limited to, the substances listed in responseto item (2), generated?

An integral part of paint. varnish and resin manufacture involves the cleaning of equipment betweenbatches. Either organic solvents or a caustic water solution was used as the cleaning agent. When thesolvent was too dirty to continue to be used, it was recovered using a solvent still. Distillation residuesconsisting of solvent residues and pigments would have been waste and were drummed and sent offsitefor disposal. There is no information as to the amount of hazardous substances generated

i) Describe the chemical composition of these hazardous substances

Still sludge would have consisted or organic (nonchlorinated) solvents andpigments.

ii) For each process, what amount of hazardous substances was generatedper volume of finished product?

PPG has no information responsive to this question.

iii) Were the hazardous substances combined with wastes from otherprocesses? If so, wastes from what processes?

See response above.

4) Describe the methods of collection, storage, treatment, and disposal of all hazardous substances,including, but not limited to, the substances listed in response to item (2) and (3). Include infonnationon the following:

3 853220004

TIERRA-B-004354

a) How residues, by-products and off-spec products were disposed of

Solvents used for equipment cleaning were often recycled as Taw materials in making lower qualitycoatings as a cost effective substitute JOT virgin raw materials. Solvents wert; also recovered asdescribed in the response to Question 3(b). Materials that could not be recycled were drummed andlandfilled off-site. Ojf-spec products would have been recycled 10 maIce salable products or sent off-site jor disposal. With respect to caustic wastes, see the response to number 6.

b) What processes were used to treat your waste? What was done with the waste afterit was treated?

The plant had a solvent recovery system to reclaim dirty solvents. After solvents were reclaimed, theywere reused The reSidue was disposed of in drums ojf-site ..

c) Identify aU persons who arranged for and managed the processing, treatment, storage anddisposal of hazardous substances.

This plant closed 25 years ago. Throughout the facility's nearly seventy year operating history, anumber of persons had responsibility for making arrangements for the disposal of wastes. PPG hasbeen unable to locate any of these persons. Joseph Comeskey was the paint plant superintendent for anumber of years prior to the closure of the facility, and would have had this responsibility just prior tothe plant's closure in 1971. Mr. Comeskey died in 1990.

d) Ifhazardous substances were taken off-site by a hauler or transporter, provide the names andaddresses of the waste haulers and the disposal site locations.

Containerized wastes were transported off-site by a private contractor, the identity of which is notrelevant to this Requestfor Information.

S) Describe ill storage practices employed by your company with respect to all hazardoussubstances from the time operations commenced until the present. Include all on-site and off-sitestorage activities.

During its 70 year operating history, PPG's Newark facility used steel tanks, drums, barrels, pails,cans, bottles and bags to store materials used in the mmmfacturing process.

a) If drums were stored outside, were the drums stored on the ground or were they stored onareas that had been paved with asphalt or concrete? Please provide a complete description of thesestorage areas.

Some drums were stored outside. At least some oj these drums were stored on unpaved areas during aportion of the period that the plant operated It is unknown whether the drums stored in this mannerWere empty or what they may have contained One former employee recalled that empty harrels werestored outside.

4 853220005

TIERRA-B-004355

Sev.era/ of the largest buildings on the site were used for storage of drums of raw materials andfinished products. PPG does not have sufficient information to determine whether such materials werestored outside at any time during which the plant operated

b) When drums were stored outside, were empty drUmssegregated from full drums?

See response to 5a.

6. For process waste waters generated at the facility which contained any hazardous substances,including. but not limited to, the substances listed in response to items (2) and (3):

i) Was the waste stream discharged into a sanitary sewer and if so, during whatyears?

See response below.

ii) Was the waste stream treated before being discharged to the sanitary sewer and ifso, how? Please be specific.

See response below.

iii) If the waste waters were not discharged to the sanitary sewer, where were itdisposed of and during what years?

See response below

iv) Please provide the results of any analyses performed on any waste processstreams generated at the facility.

See response below.

PPG has insufficient information to answer this question. The plant was connected to a publicsewer system which we believe existed when thefacility was constructed in 1902. (See attached"Plumber's Specifications" from 1902 facility construction specificatiOns) However, it is notclear whether anything besides sanitary waste, was discharged to these sewers. No detailedmaps or records of analyses are available to PPG.

TanIcsused in the production of certain products,J.:g., water based painl, were rinsed with adilute caustic water solution for cleaning after use. The rinse from this cleaning possibly wasdischarged to the sanitary sewers. In addition, a caustic cleaning tank was used to cleanportable paint tanks. Periodically (1-2 months), the cleaning tank would be drained and itscontents possibly were discharged to the sanitary sewers.

Caustic water solutions were also used in the production of the linseed oil. Linseed oil wasproduced at the Newark plant from 1923 until /947. No informationwas found regarding thefinal disposition of the spent caustic water solution.

s 853220006

TIERRA-B-004356

PPG is not aware of any information that any sewered materials were treated before discharge.No records of any analyses performed on the waste streams werefound

b) For floor drains or other disposal drains at the facility:

PPG does not have information indicating that floor drains existed in any of thebuildings.

i) Did the drains connect to a sanitary sewer and if so, during what years?

See response above.

ii) If the floor drains or other disposal drains at the facility were not discharged tothe sanitary-sewer, where did they discharge and during what years?

See response above.

iii) (i) Did any storm sewers, catch basins or lagoons exist at any time at thefacility and if so, during what years?

PPG has no information that there are any catch basins or lagoons on theproperly. With regards to the storm sewers, refer to 8b.

a) If catch basins or lagoons existed, were they lined or un-lined?

Not applicable.

b) What was stored in the lagoons?

Not applicable.

c) Where was the discharge from any of these structures released and duringwhat years? Was this discharge treated before its release and if so. howand during what years? What was the chemical composition of any wastewaters released. and during which years?

Not applicable.

iv) Please provide maps andlor diagrams of any waste water collection. transport ordisposal systems on the property.

A 19S9 revision of a 1942 drawing (copy attached) shows an 8-inch sewer linerunning from BUilding 17southwest to the edge of the property. It apparentlyties in to a city sewer line at that point, although this is not definitively stated onthe drawing.

6 853220007

TIERRA-B-004357

'.

7) a) For each hazardous substance, including, but not limited to, the substances listed inresponse to item (2) or identified in the responses to item (3), above, provide the total amountgenerated during the operation of the facility on an annual basis.

PPG has no basis available on which to estimate quantities of hazardous substances generated by thisfaci/ity. Based upon available information, PPG believes only a limited amount of production relatedwaste, if any. was discharged to the sewers.

b) Were any hazardous substances, including, but not limited to, the substances listed inresponse to item (2) or identified in the responses to item (3), above disposed of in the Passaic River ordischarged to the Passaic River? If yes, identifY the hazardous substances, estimate the amount ofmaterial discharged to or disposed of in the Passaic River and the frequency with which this dischargeor disposal occurreC:l. Also please include any sampling of the river which you might have done afterany discharge or disposal.

PPG has no information that hazardous substances were disposed of in the Passaic River or directlydischarged to the Passaic River.

8) Please identify any leaks, spills, explosions, fires or other incidents of accidental materialdischarge that occurred at the facility during which or as a result of which any hazardous substances,including. but not limited to, the substances listed in response to items (2) or (3), were released on theproperty, into the waste water or storm drainage system at the facility or to the Passaic River. Provideany documents or information relating to these incidents, including the ultimate disposal of anycontaminated materials.

There was a fire at the Resin Plant (BUilding #17) in 1969. PPG has no information that anyhazardous substances were discharged into the storm drainage system or to the Passaic River.

a) Please provide the results of any sampling of the soil, water, air or other media after anysuch incident and before and after clean-up. Please provide in this information all sampling performedfor or by NJDEP.

PPG has no information about any sampling of soil, water, air or other media following this incident.

b) EPA has information that there were two "36" pipes at your facility that dischargeddirectly into the Passaic River. Please describe in detail how these outfalls were utilized, including, butnot limited to, whether storm water, process waste water. or any other material was ever dischargedthrough these outfalls. Provide any maps or diagrams showing the location of these outfalls.

PPG requests that EPA prOVide this information to PPG in response to our FOIA Request of July 22,1996. These outfalls may be regional storm sewers that originate Off of the former PPG site and passthrough a right of way. PPG has no information about tie-ins to the storm sewers on the PPG site

7 853220008

TIERRA-B-004358

'.

c) EPA has information that 4" to 6" pipes ran from each individual building on yourfacility directly to the Passaic River. Please describe in detail how these outfalls were utilized, includingbut not limited to, whether stonn water, process waste water, or any other material was ever dischargedthrough these outfalls. Provide any maps or diagrams showing the location of these outfalls.

PPG has no information which identifies or locates these pipes We request that EPA provide us withthe information it has on this subject in response to PPG 's FOIA request of July 22, /996.

d) EPA has information that a 100,000 gallon concrete underground tank was located atyour facility beneath building #7 adjacent to the Passaic River. Please provide all infonnationconcerning this tank, including but not limited to, what was stored in this tank, whether this tank waschecked for leaks and when, if ever, this tank was removed. Provide any maps Of diagrams showing thelocation of this tank.

In response to a FOIA request, PPG obtained from USEPA, Region 2, an October, /992 report by theNew Jersey Department oj Environmental Protection and Energy that describes such a tank However,former employees contacted did not recall its existence, and the drawings available do not identifysuch a tank. It is possible that the referenced structure was converted into a tank by a site operatorsubsequent to PPG's ownership of the site.

e) Please provide information relating to an explosion and fire which occurred at yourfacility on or about May 26, 1969. Please describe this incident and provide any and aU documentsrelating to the incident and clean-up, if any, or subsequent preventive measures taken.

According to a PPG employee, a vapor cloud was released from one of the resin reactors inBuilding 17. This vapor cloud migrated through the bUilding until an ignition source was found.The resulting explosion blew out sections of the walls and roof and ignited resin which had leaudout of one of the vessels. The burning resin spread throughout the building. Several other storagetanks and processing tanks jailed during the fire, releasing their contents into the building. A tanktruck which was being filled also caught fire and burned Newark City firefighters pumped waterfrom the river into the bUilding and nearby storage tanks to attempt to contain the fire.

The bUilding was damaged beyond repair during the fire and was later demolished

PPG has no information indicating that hazardous substances were released into the Passaic Riverduring this event.

9) Describe the use of the dock located on the Passaic River at your facility, including but notlimited to, the time period it was used, the identity and volume of material received, how the materialwas transported into your facility and whether any spills or accidents occurred during the handling ofthese materials at the dock.

The dock was used in the first half of the century to unload flax seed and coal for use in the factoryand to ship final products. Based on discussions with former employees, the dock was not used after/946.

8 853220009

TIERRA-B-004359

10) a) Was your facility ever subject to flooding. Ifoo, was the flooding due to:

i) overflow from sanitary" or storm sewer back~up, and/or

ii) flood overflow from the Passaic River?

Flooding from the Passaic river occurred at least once at the Newark plant in the 1960's. Thisflooding apparently did not cause significant damage to the faCility. Based on discussions withformer employees, this flood was the only one remembered

b) Please provide the date and duration of each flood event.

The date and duration of theflood in the 1960 's is not known.

11) Please provide a detailed description of any civil. criminal or administrative proceedings againstyour company for violations of any local, State or federal laws or regulations relating to water pollutionor hazardous waste generation, storage, transport or disposal. Provide copies of all pleadings anddepositions or other testimony given in these proceedings. !

PPG has no record of any such proceedings related to this plant.

12) Provide a copy of each document which relates to the generation, purchase, use, handling,hauling, and/or disposal of all hazardous substances, including, but not limited to, the substances listedin response to item (2) or (3): If you are unable to provide a copy of any document, then identify thedocument by describing the nature of the document (e.g. letter, file memo, invoice, inventory form,billing record, hazardous waste manifest, etc.) Describe the relevant information contained therein.Identify by name and job title the person who prepared the document. If the document is not readilyavailable, state where it is stored, maintained, or why it is unavailable.

PPG submitted a survey form covering this property to Congressman Eckhardt's subcommittee in1979. A copy of the completed Eckhardt survey for this plant is attached It has been redacted toeliminate the identity oj the company that hauled waste off-site, since that information is not relevantto this Request for Information.

13) a) Did you or anyone else sample the soil, ground water, surface water, ambient air or otherenvirorunental media at the facility for purposes other than those identified in questions above?

b) If so, please provide all other documents pertaining to the results of these analyses.

PPG has no information about any sampling oj SOil,water, air or other media, other than informationthat wasprOVided to PPG by USEI'A as part of a FOIA request related to another Superfund sile. ThaIinformation is contained in a 1992 report prepared by NJDEPE relative to the Frey Industriesfacility, which apparently occupies part of the former PPG site

9 853220010I'

TIERRA-B-004360

14) and (5) See PPG's partial response for this Site dated August 15, 1996, a copy afwhich isattached

16) Provide the name, address, telephone number, title and occupation of the person(s) answeringthis ''Request for Information" and state whether such person(s) has personal knowledge of theresponses. In addition, identify each person who assisted in any way in responding to the "Request forInformation" and specify the question to which each person assisted in responding. Please include thenames and addresses of former employees who were contacted to respond to any of the questions.

Joseph Karas:

Thomas Ebbert:

Greg Norman:

Bill Silvestri:

TomPrice

Pat Racioppi

TomRisch

jmk'pAc:I04.cIoc

Assistant CounselPPG Industries Inc., One PPG Place.. Pittsburgh, PA 15272412-434-141; No personal knowledgeEnvironmental Engineering A.ssociatePPG Industries, Inc., 4325 RDsanna Drive. Allison Park. PA /5/0/412-492-5478; No personal knowledgeProcess TechnicianPPG /ndustries,/nc., 15/ Colfax Street. Springdale, PA 15/44412-274-3454; No personal knowledgePPG's Cleveland Manager. Ohiofacility; 216-671-0050Questions 6,8 & 10;PPG's C&R Engineering Office, Allison Park, PA; 412-492-5477Question 8;Retired: Florida;Question 5, 6, 8 & 10Retired: Pittsburgh, PA; 412-487-6219Questions 2,5,6,8 &10.

10 853220011Ii

TIERRA-B-004361

UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION 2

290 BROADWAYNEWYORK. NY 10007-1866

SEP 1 5 2003

GENERAL NOTICE LETTERCERTIFIED MAIL-RETURN RECEIPT REQUESTED

Raymond LeBoeuf, PresidentPPG Industries, Inc.One PPG PlacePittsburgh, PeIUlSylvania 15272

RE: Diamond Alkali Superfund SiteNotice of Potential Liability forResponse Actions in the Lower Passaic River, New Jersey

Dear Mr. LeBoeuf:

The United States Environmental Protection Agency ("EP An) is charged with responding to therelease and/or threatened release of hazardous substances, pollutants, and contaminants into theenvironment and with enforcement responsibilities under the Comprehensive EnvironmentalResponse, Compensation, and Liability Act of 1980, as amended ("CERCLA"), 42 U.S.C. §9601et~. Accordingly, EPA is seeking your cooperation in an innovative approach toenvironmental remediation and restoration activities for the Lower Passaic River.

EPA has documented the release or threatened release of hazardous substances, pollutants andcontaminants into the six-mile stretch ofthe river, known as the Passaic River Study Area, whichis part of the Diamond Alkali Superfund Site ("Site'') located in Newark, New Jersey. Based onthe results of previous CERCLA remedial investigation activities and other environmentalstudies, including a reconnaissance study of the Passaic River conducted by the United StatesArmy Corps of Engineers ("USACE''), EPA has further determined that contaminated sedimentsand other potential sources of hazardous substances exist along the entire 17-mile tidal reach ofthe Lower Passaic River. Thus, EPA has decided to expand the Study to include the areal extentof contamination to which hazardous substances from the six-mile stretch were transported; andthose sources from which hazardous substances outside the six-mile stretch have come to belocated within the expanded Study Area.

By this letter. EPA is notifying PPG Industries, Inc. ("PPG'') of its potential liability relating tothe Site pursuant to Section 107(a) ofCERCLA, 42 V.S.C. §9607(a). Under CERCLA,potentially responsible parties ("PRPs'') include current and past owners of a facility, as well aspersons who arranged for the disposal or treatment of hazardous substances at the Site, or thetransport of hazardous substances to the Site.

851860001Internet Address (URl). http://www.epa.gov

R~IR.cyclabie • Prtnted wlth VegeUlble 0118Med Inb on Reqtcled p...... (MInimum 50% Poelloolwumer CWIU1n()

TIERRA-B-004362

In recognition of our complementary roles. EPA has formed a partnership with USACE and theNew Jersey Department of Transportation-Office of Maritime Resources C"OMR") ["thegovernmental partnership"] to identify and to address water quality improvement. remediation,and restoration opportunities in the 17-mile Lower Passaic River. This governmental partnershipis consistent with a national Memorandum of Understanding ("MOV'') executed on July 2, 2002between EPA and USACE. This MOU calls for the two agencies to cooperate, whereappropriate. on environmental remediation and restoration of degraded urban rivers and relatedresources. In agreeing to implement the MOU, the EPA and USACE will use their existingstatutory and regulatory authorities in a coordinated manner. These authorities for EPA includeCERCLA, the Clean Water Act. and the Resource Conservation and Recovery Act. TheUSACE's authority stems from the Water Resources Development Act ("WRDAU). WRDAallows for the use of some federal funds to pay for a portion of the USACE's approved projectsrelated to ecosystem restoration.

For the first phase of the Lower Passaic River Project, the governmental partners are proceedingwith an integrated five- to seven~year study to determine an appropriate remediation andrestoration plan for the river. The study will involve investigation of environmental impacts andpollution sources, as well as evaluation of alternative actions, leading to recommendations ofenvironmental remediation and restoration activities. This study is being conducted by EPAunder the authority ofCERCLA and by USACE and OMR, as local sponsor, under WRDA.EPA, USACE, and OMR are coordinating with the New Jersey Department of EnvironmentalProtection and the Federal and State Natural Resource Trustee agencies. EPA, USACE, andOMR estimate that the study will cost approximately $20 million, with the WRDA and CERCLAshares being about $10 million each. EPA will be seeking its share of the costs of the study fromPRPs.

Based on information that EPAevaluated during the course of its investigation of the Site. EPAbelieves that hazardous substances were being released from PPG's facility located at 29Riverside Avenue in Newark, New Jersey, into the Lower Passaic River. Hazardous substances,pollutants and contaminants released from the facility into the river present a risk to theenvironment and the humans who may ingest contaminated fish and shellfish. Therefore, PPGmay be potentially liable for response costs which the government may incur relating to the studyof the Lower Passaic River. In addition, responsible parties may be required to pay damages forinjury to. destruction of, or loss of natural resources, including the cost of assessing suchdamages.

Enclosed is a list of the other PRPs who have received Notice letters. This list represents EPA'sfindings on the identities ofPRPs to date. We are continuing efforts to locate additional PRPswho have released hazardous substances. directly or indirectly, into the Passaic River. Inclusionon. or exclusion from, the list does itot constitute a final determination by EPA concerning theliability of any party for the release or threat of release of hazardous substances at the Site. Beadvised that notice of your potential liability at the Site is being forwarded to all parties on thislist.

We request that you consider becoming a "cooperating party" for the Lower Passaic River

851860002

TIERRA-B-004363

Project. As a cooperating party, you, along with many other such parties, will be expected tofund EPA's share of the study costs. Upon completion of the study, it is expected that CERCLAand WRDA processes will be used to identify the required remediation and restoration programs,as well as the assi'gnment of remediation and restoration costs. At this time, the commitments ofthe cooperating parties will apply only to the study. For those who choose not to cooperate, EPAmay apply the CERCLA enforcement process, pursuant to Sections 106 (a) and I07(a) ofCERCLA, 42 U.S.C. §9606(a) and §9607(a) and other laws.

Pursuant to CERCLA Section 113(k), EPA must establish an administrative record that containsdocwnents that form the basis of EPA's decision on the selection of a response action for a site.The administrative record files, which contain the docwnents related to the response actionselected for this Site are located at EPA' s Region 2 office (290 Broadway, New York) on the 18*floor. You may call the Records Center at (212) 637-4308 to make an appointment to view theadministrative record for the Lower Passaic River Project.

EPA will be holding a meeting with all PRPs on October 29. 2003 at 10:00 AM inConferenceRoom 27A at the Region 2 office. At that meeting, EPA will provide information about theactions taken to date in the Lower Passaic River, as well as plans for future activities. After thepresentation, PRPs will be given the opportunity to caucus, and EPA will return to answer anyquestio~ that might be generated during the private session. Please be advised that due toincreased security measures, all visitors need to be registered with the security desk in the lobbyin order to gain entry to the office. In order to ensure a smooth arrival, you will need to provideEPA with a list of attendees no later than October 15,2003.

EPA recommends that the cooperating parties select a steering committee to represent thegroup's interest as soon as possible, since EPA expects a funding commitment for the financingof the CERCLA share of the $20 million study by mid-November 2003. If you wish to discussthis further, please contact Ms. Alice Yeh, Remedial Project Manager. at (212) 637-4427 or Ms.Kedari Reddy. Assistant Regional Counsel. at (212) 637-3106. Please note that allcommunications from attorneys should be directed to Ms. Reddy.

Sincerely yours,

~~~------George Pavlou, DirectorEmergency and Remedial Response Division

Enclosure

cc: Joseph Karas, Esq.PPG Industries. Inc.

851860003

TIERRA-B-004364

PRPs in Receipt of Notice Letters:

IpRP ILegal Counsel

J. Roger Hid Paul W. Herring, Esq.President and Chainnan of the Board Andrews & KurthL.L.P.Occidental Chemical Co. 1717 Main Street. Suite 3700Occidental Tower Dallas. Texas 752015005 LBJ FreewayDallas, Texas 75244

Joseph Gabriel Philip Sellinger. Esq.Vice President of Operations Sills Cummis Zuckerman360 North Pastoria Environmental Corp. One Riverfront Plaza1100 Ridgeway Avenue Newark, NJ 07102Rochester, New York 14652-6280

Robert Ball. President Lawrence Salibra. Esq.Alcan Aluminum Corporation Alcan Aluminum Corporation100 Erieview Plaza. 29th Floor 6060 Parkland Blvd.Cleveland. Ohio 44114 Mayfield Hts., OR 44124

Mark Epstein. President Eric Aronson, Esq.Alden Leeds Inc. Whitman Breed Abbott & Morgan55 Jacobus Ave. One Gateway CenterKearny, New Jersey 07032 Newark, NJ 07102

Alan Bendelius, President Fredi L. Pearlmutter. Esq.Alliance Chemical, Inc. Cooper, Rose & English, LLPLinden Avenue 480 Morris AvenueRidgefield, New Jersey 07657 Summit, New Jersey 07901-1527

William Gentner. President A. Christian Worrell III. Esq.The Andrew Jergens Co. Head & Ritchey, LLP I

2535 Spring Grove Ave. 1900 Fifth Third CenterCincinnati. Ohio 45214 511 Walnut Street ICincinnati, OH 45202

-- -- -- ,

Gary Cappeline, President Stephen Leennakers, Esq.Ashland Specialty Chemical Co. Ashland Specialty Chemical Co. I

5200 Blazer Parkway 5200 Blazer ParkwayIDublin, Ohio 43017 . Dublin. OH 43017 il

Klaus Peter Loebbe. President Nan Bernardo, Esq. and Nancy Lake Martin, Esq. IIBASF Corporation BASF Corporation3000 Continental Drive North 3000 Continental Drive North

IIMount Olive, New Jersey 07828 Mount Olive. NJ 07828

851860004

TIERRA-B-004365

Joseph Akers, Vice President Gerard Hickel, Esq.Bayer Corporation Bayer Corporation100 Bayer Road 100 Bayer RoadPittsburgh, Pennsylvania 15205~9741 Pittsburgh, PA IS20S~9741

Yvan Dupay, President Arthur Schulz, Esq.Benjamin Moore & Co. Environmental Counsel51 Chestnut Ridge Road 4910 Massachusetts Ave., N.W. Suite 221Montvale, New Jersey 07645 Washington, DC 20016

Alberto Celleri, President Jim GiannottiChemical Compounds Inc. Chemical Compounds Inc.10 Baldwin Court 29- 75 Riverside AvenueRoseland, New Jersey 07086 Newark, NJ 07104

President Brian Kelly, Esq.Chris-Craft Industries, Inc. Chris-Craft Industries, Inc.767 Fifth Avenue, 46th Floor 767 Fifth Avenue, 46th FloorNew York, New York 10153 New York, NY 10153

John Guffey, President John R. Mayo, Esq.Coltec Industries, Inc. Coltee Industries, Inc.3 Coliseum Centre 430 Park Avenue2550 West Tyvola Road New York, NY 10022Charlotte, North Carolina 28217

Roger Marcus, President. Russell Hewit, Esq.Congoleum Corporation Dughi & Hewit3705 Quakerbridge Road 340 North AvenueMercerville, New Jersey 08619 Cranford, NJ 07016

Martin Benante, Chairman James Maher, Esq.Curtiss- Wright Corp. Curtiss-Wright Corp.4 Becker Farm Road 4 Becker Fann RoadRoseland, New Jersey 07068 Roseland, NJ 07068

Antonio Perez, President Elliot Stem, Esq.Eastman Kodak Company Eastman Kodak Company343 State Street 343 State StreetRochester, New York 14650 Rochester, NY 14650

Edgar Woolard, Chairman Bernard J. Reilly, Esq.E.I. du Pont de Nemours & Co. Corporate Counsel1007 Market Street E.I. du Pont de Nemours & Co.Wilmington, Delaware 19898 1007 Market Street

Wilmington. DE 19898

851860005

TIERRA-B-004366

David Weisman, CEO Je:ffiey Schwartz. Esq.Elan Chemical Company Sarber Schlesinger Satz & Goldstein268 Doremus Ave. One Gateway CenterNewark, New Jersey 07105 Newark, NJ 07102

Al Reisch, President NoneE M Sergeant Pulp & Chemical Co. Inc. I

6 Chelsea Road I

Clifton, New Jersey 07102

Mark Tucker, Esq. Kenneth Mack, Esq.Essex Chemical Corp. Fox, Rothschild, O'Brien & Frankel2030WMDC Princeton Pike Corp.CenterMidland, Michigan 48674 997 Lenox Drive, Building 3

LaWrenceville, NJ 08648

Todd Walker, President John Ix, Esq.Fairmount Chemical Co. Inc. Porzio Bromberg & Newman117 Blanchard St. 163 Madison Ave.Newark, New Jersey 07105 Morristown, NJ 07962

Bradley Buechler, President Robert M. Becker, Esq. ;

Franklin-Burlington Plastics Inc. Kraemer, Bwns, Mytelka & Lovell, P.A.113 Passaic Ave. 675 Morris Ave.Kearny, New Jersey 07032 Springfield, NJ 07081

Henry Benz, President Anne Conley-Pitchell, Esq.Hoescht Celanese Chemicals, Inc. Hoescht Celanese Corp.Route 202-206 Route 202·206P.O.Box 2500 P.O.Box 2500Somerville, New Jersey 08876 Somerville, NJ 08876

Francine Rothschild, President NoneKearny Smelting & Refining936 Harrison Ave #5Kearny, New Jersey 07032 _. _.

Henry Schact, CEO Ralph McMurry, Esq.Lucent Technologies, Inc. Hill, Betts & Nash LLP600 Mountain Avenue 1 Riverfront Plaza. Suite 327Murray Hill, New Jersey 07974 Newark, NJ 07102-5401

.

Richard Meelia, President Patricia Duft, Esq.Mallinckrodt, Inc. Mallinckrodt, Inc.675 McDonnell Blvd. 675 McDonnell Blvd.Hazelwood, Missouri 63042 Hazelwood, MO 63042

851860006

TIERRA-B-004367

Richard Mahoney, CEO i L.William Higley, Esq.Monsanto Company Monsanto Company800 N. Lindbergh Blvd. 800 N. Lindbergh Blvd.St. Louis. Missouri 63161 S1.Louis, MO 63167

Joseph Galli, President Peter Schultz, Director i

Newell Rubbermaid, Inc. Environmental Affairs I

29 E. Stephenson St. Newell Co.Freeport, Illinois 61032 4000 Auburn 8t.

Rockford. IL 61101

Jean~Pierre van Rooy. President Sarah Hurley. Esq.Otis Elevator Company Robinson & Cole LLPNorth American Operations 695 East Main Street10 Farm Springs Road Stamford, CT . 06904-2305Farmington. Connecticut 06032

Richard Ablon, President J.L. Effinger. Esq. I

Ogden Corporation Ogden CorporationTwo Pennsylvania Plaza, 25th Floor Two Pennsylvania Plaza., 25th FloorNew York, New York 10121 New York, NY 10121

Henry McKinnell, Chairman Michael McThomas, Esq.Pfizer Inc. Pfizer Inc.235 E. 42nd St. 235 E. 42nd St.New York, New York 10017 New York; NY 10017

Raymond LeBoeuf, President Joseph Karas, Esq.PPG Industries. Inc. PPG Industries. Inc.One PPG Place One PPG PlacePittsburgh, Pennsylvania 15272 Pittsburgh, PA 15272

Lawrence Codey. President Hugh Mahoney. Esq.PSE&GCo. PSE&GCo.P.O. Box 570 P.O. Box 570Newark, New Jersey 07101-0570 Newark. NJ 07101

Phillip D. Ashkettle, President Adam S. Walters, Esq.Reichhold Chemicals. Inc. Phillips, Lytle, Hitchcock, Blaine & HuberP.O. Box 13582 3400 Marine Midland CenterResearch Triangle Park, North Carolina Buffalo. NY 1420327709

Robert McNeeley, President Paul Rivers, DirectorReilly Industries. Inc. Corporate Environmental Affairs1510 Market Square Center Reilly Industries. Inc.151 North Delaware Street 1500 S. Tibbs AvenueIndianapolis, Indiana 46204 Indianapolis, IN 46242

851860007

TIERRA-B-004368

Robert Finn, President Howard Myers, Esq.RSR Corporation RSR Corporation2777 Stemrnons Freeway, Suite 1800 2777 Stemmons Freeway, Suite 1800Dallas, Texas 75207 Dallas, TX 75207

Christopher Connor, CEO Donald McConnell, Esq.The Sherwin-Williams Company The Sherwin-Williams Co.101 Prospect Avenue, N.W. 101 Prospect Ave., N.W.Cleveland, Ohio 44115-1075 Cleveland, OH 44115

George Barrett, President Kirsten E. Bauer, Esq.Teva Pharmaceuticals USA Inc. Teva North America1090 Horsham Road 1090 Horsham RoadNorth Wales, Pennsylvania 19454 North Wales, PA 19454

Robert Senior, President Robert DiLascio, Esq.Three County Volkswagen 30 Park Avenue, Suite 101701 Riverside Ave. Lyndhurst, NJ 07071Lyndhurst, New Jersey 07071

Michael Jordan, President Roger Willis, Esq.Westinghouse Electric Corp. Westinghouse Electric Corp.11 Stanwix Street 11 Stanwix StreetPittsburgh, Pennsylvania 15222 Pittsburgh, PA 15222

Isaac Weinberger, President NoneWiggins Plastics Inc.547 Maitland Ave.Teaneck, New Jersey 07666

851860008

TIERRA-B-004369

-

AntnAm OFWU,Lre MOORE

BrATE OF NEW JERSEY II

COUNTY OF VNJON I

'The witness, bavinl been duly 1WDrD, affirms as follows:

J. I, W1llie Moo~, am I former employee of tht PiUSbWJh Plare GWI (PPO) facility

fonnerly located at 29 Riverside Avenue, Newark, NI. J was eD1ployecfat the PPO facility

clurin& the period l~~l97J. Du.rin, this time J IaeJd Jevera] positionl, includina porter and

Itora&e lank attendant, as we1Ias IeI"Vin& as vice president of the union.I

2. PPG manulactured paints, Jac.quen, tmmell and wrnishea at the faciUty, in addition

to Jains aDd piaments. hw materiah used in theIe products included various JOlve:nrswhich

weft 1efC'md to by ~ Dumbers JUdJ as PXJ027, PXJ028, -PX.f2;-PK"3,-PX«. . _.and Dumber 260.

3. Durina my tl:nure at the fadlity l.bad' petSOnalJy witnessed OCher PPG employees

dllJDPin& CODtaiDets Jnto &be Passaic Rivtr. J am DOt knowJedacable ftPJ'dUaa the contents ofthole CIOIUaiDen.

4. Ewry IKdJdiD& at Ibe PPO &eDit)' had •• - 10 6- 8CWet pipe J'UMin& dUecUYIo the

-Vc. AJthoulh my boWled" u Jimfted I'eJlldinlIhe .. oflheae aewer line.s. adl buiJdina

'6Id floor draW lbat were CICWa'Cd by craw ...5. I JIIve Mtneaed PPG anployeea IWIepina raidue, incIudina IpiDI 01poducu and

aw 1IWcriaJs. dowD Ihae floor drains.

AHL000113853210009

TIERRA-B-004370

.,

,. I"~ Mines_ ftondiD,& or the Pusaic River at &he lite on IeYCnJ JDa.nces where''fICI'1iou of die fKility were 1IDde:rwaser.

STATE OF NEW JERSEy

COtJNTY OF VNlON

tIt

Before me, .1{£,,'i E:...· ....n..:.I....i2~sc~-::.IdI:.:..... t. notary publict

on this day

.-penonaIJy appeared Willie Mooret blown 10 ~ (or proved to me on the oath or Willie Moore)

10 be the penon wbose Dame is subscribed to the lorqoin& instrument and acknowledged to me

that he eucuted the lame lor the purposes and consideration tberdn expressccl.

Given UDder my band and teal of office this ", #' day of .5l/.),_L.,t 1994.

.--- --- --------JEFFREY F. McDeRMOTT

NOtARY pueuc OF NEW JERSEyIAr~n Expire, ~ ','1181

I1l1l?tt!kz >NotarY bJic =

-.. « 2

853210010AHL000114

TIERRA-B-004371

~tfn mtrstll ~tVadtutnf of ~nUirantuenfal 'raftdinn & ~ntrgll~itrisian of ~spansihlt 'ad\! 'He ~mt~iafian

~uteau of ~tuetgent1l ~spattse~gian Jf

INVESTIGATION

Case Number: 93-10-05-0736PAC:File:

Investigator: Bruce F DoyleJoe Hoyle

Time Arrived: 0730Time Departed: 1030

Location: Area of 29-75 Riverside AvenueAddress: Chemical Compounds Inc.

29-75 Riverside Ave.Newark, NJ

Responsible Party: Chemical Compounds Inc.Address: 29-75 Riverside Avenue

Newark, NJContact: Alberto CelleriPhone: (201)485-3211

Location Phone #: (201)485-3211

Health Dept. Rep: Not Present Phone#:

Origin of Complaint: Newark Fire Department Dispatch Phone #: (201)733-7400

Nature of Complaint: Fire at facility that makes dye. Chemicals involved in fire are not known or identifiedas of the request for assistance to BER.

Findings: Emergency Response Specialists Bruce Doyle and Joe Hoyle responded to Newark to assist NewarkFire Department with operations at the incident site. After arriving on the scene of Chemical Compounds Inc. itwas learned that the fire had been extinguished by the fire department, however, there was still no identificationof the materials involved. Newark FD Chief Anthony Apostolico stated that the fire appeared to be confined toone area of the facility and directed the attentions of the responders to a specific piece of machinery. Closerexamination of this apparatus revealed that it was a bladder press that would be used for the filtration of finishedproduct to remove particulate matter of specific size. It was the estimation of the DEPE Responders that thisapparatus, if not in operation, would not have sufficient material contained within to cause any sort of fire

TIERRA-B-004372

problem of the scope indicated by Chief Apostolico. Thus the area of investigation was broadened to thesurrounding machinery. Next to the press, a large roughly cubic device was observed. This device was paintedsilver (recently) and appeared from it's design to be a drier or cooker. The device was in fact still radiatingsignificant heat indicating it might still in operation. Closer inspection of the unit revealed that it had doors onboth ends, and that the seat of the anterior door had been breached from within possibly due to excessivepressure buildup. The door was observed to be missing the dogs (batten down bolts) on the bottom of the door,on both sides. The posterior door, closest to the loading bay, exhibited evidence of internal pressure build upalso, hut not to the extent noted on the anterior cloor. At first the re.,;;p0tlr:lers l1elieved thftt the bolts on the

anterior door were no longer apart of the unit, however, theywere found in the organicmass that had oozed from thedrier. It was also noted thatthe position of the door was inline with the press such that atthe point when the internalpressure exceeded the physicalcapability of the drier, itspewed the organic materialonto the press and ignited inthe ambient air. Furtherinspection of the inside of thebuilding revealed that inaddition to the press, otherapparatus was sprayed withthe organic mass, to a lesser

extent, in line with the seal of the anterior door. Also noted was the discoloration of portions of the buildingwhere the smoke (decomposing dye) billowed. Also noted during this inspection was the fact that apparatuswithin the building was still operating even though no one was at the facility overnight

After the arrival of Alberto Celleri,President of Chemical Compounds,it was learned that the apparatusinvolved in this incident was in facta drier that is used by the RP todesiccate an organic dye that is apolymer of nitrated aniline(C12H 19N30S) , this is themanufactured product. AlbertoCelleri stated that the drier is hotwater/steam fed from the boiler inthe basement and that the normaloperating temperature for this Door

apparatus is 2270F whichcorresponds to a boiler pressure of

Steam Coils

ShelVing

TIERRA-B-004373

20 PSIG. For this particular batch, Celleri stated that he increased the operating pressure to 30 PSIG, whichshould have corresponded to a temperature increase, within the unit, to 2500F. The dryer's function is similar tothat of a radiator; steam or hot water is pumped through coils beneath the shelves that hold the product to bedried. This radiated heat desiccates the dye and the moisture is drawn from the unit with an eductor fan (rated at90 CFM). Weather or not this increase in pressure produced too high a temperature within the drier, or a failureof the coils permittprl 1;""", steam to impinge on the dye; the dye was heated to a temperature in excess of 4000F.At this temperature, me dye produces ignitable vapors (flash point) and begins to decompose. This materialdecomposes to several organic and non organic molecules: including oxicies of nHrogerr. Th~ MSDS alsoindicate that oxides of nitrogen are produced in the combustion of this dye. Given the chemical properties ofnitrogen oxides, with particular focus on their Oxidizing capability, it is conceivable that the material built up inthe drier and either overcame or ignited under the vacuum of the eductor fan. Given the afore mentionedscenario, it would have been possible for a detonation to have taken place within the drier that may have beenresponsible for the damage to the door. This possibility can be speculated because of the chemical nature of thereactants that make up this product. As the material decomposes, aniline( reactant) is liberated as are oxides ofnitrogen. The oxidizing properties of these nitrogen oxides are well documented, and in particular, when heatedunder steam (Texas City, SS Grandcamp Explosion of 1947). Detonation can be initiated by excessive pressureof the nitrogen oxides alone. In the same space the reaction of the aniline would also contribute to the overallinstability of the atmosphere as aniline is volatile in the presence of steam and is incompatible with oxidizers. Ifsufficient concentrations of nitrogen oxides were present within the drier a violent decomposition (detonation)might have occurred due to the contact of the aniline (a decomposition product of the dye). Although thisscenario is possible, the specifics of the incident were not immediately evident from the evidence at the scene.It should be noted that the drier was not inspected by BER due to the extensive contamination of organic residuefrom the reaction (fire) on the inside. It should also be noted that the eductor was not functioning at the time ofBER's investigation; no determination was made as to weather this was an effect of the reaction/decompositionor a contributing factor.

After conferring with Alberto Celleri and Chief Anthony Apostolico, Newark FD, it was determined that thecause of the incident required further investigation by the RP to determine the exact cause to thus prevent itfrom happening again. While the organic mass did not exit the facility, thereby falling under Departmentaljurisdiction, the concern of the toxic combustion and decomposition by-products was addressed to Mr. Cellerias having the greatest potential for off site impact in the densely populated area ofNE Newark, E. Newark(Hudson County) and North Arlington (Bergen County). Celleri was directed by Newark Fire Department withthe concurrence of HER Personnel on scene, that the process could not be restarted until a full analysis of theincident could be made and further, that the drier could not be used until it's integrity could be certified.

Conclusions: BER 1 responded to the report of a chemical fire in the vicinity of 29 Riverside Avenue inNewark, Essex County. The fire was reported to the DEPE by Newark FD who also requested assistance.Initially, the fire was believed to have originated from the combustion of an unknown liquid in a bladder presson the main floor of the building owned by the RP. Subsequent BER investigation found that the fire originatedin a dryer where the final product was undergoing thermal desiccation. Pressure within the dryer built upsufficiently to break off two of the five bolts holding the door in place and cause the dye within to spew out inplane with the door seal. The temperature of the material was high enough to initiate decomposition and releaseoxides of nitrogen. The off gassing of the decomposing dye was enough to support combustion and result in thelow yield fire observed by Newark Fire Department. Subsequent analysis of the chemistry of the decompositionof this dye revealed that an explosive mixture could have formed in the drier and may have been responsible for

TIERRA-B-004374

the damage to the apparatus. The fire was found soon enough in its course to preclude excessive damage of thefacility however, the material did contaminated the main floor of the building. The material was found to be aNitrated Aniline dye which would be expected to decompose to oxides of nitrogen and carbon. Newark FDextinguished the fire and upon the arrival of the owner of the facility, the remediation of the facility wasundertaken.

Recommendations: Case Clnserl HER

Date

Su ervisor/I/~(,,hj

Date

TIERRA-B-004375

,Nm.; Jersey Department of Envi.ronmental Protection

COMMUNICATIONS CENTER NOTIFICATION REPORTReceived:10/05/93 TD Log # 16921Operator:ROGER Case # 93-10-5-1110-43._,._-----------~------_._--------_._-----------------------------------------------R'3ported By

B.DOYLEStreet Address

Notification Typl3: OtherAffiliation

NJIEPE·-DRPSR-BERMunicipality

Phone

Incident Location: Facility:::ite CHEMIC.l'.LS CC!'A~PO!JNDS INC 'H11 Ol;n 1/'j,<:"

,:..\I.J,-V."IU-."Z..tV

Street Address Hunic:ipality29-75 RIVERSIDE AVE NEWAHKLocation Type Industrial

countyESSEX

Incident Date 10/05/93State

NJTime 0700-------------~------_._-------------_._._-----_._._--------------------------_._-------

::.11bstanceReleased UNKNOWN SOLIDltl10untReleased ( )UNKNOWN

Ill: State So!id CAS# Release Is Continuous,..ddi'"ional Substances !i" BLUE 2

substance Contained? N Hazclrdous Hatl3ria17 U TCPA? U A310 LEltter? NCOMU CODE: 0714 REF CODE: 001

..--------- --- ---- --~~~.------ ............... _. __ .__ ._- .. ---- _._ ..-_ ...._-- ---- .......... -------- ..------ -_. --_ .._--Incident Description Fire/spill

Injuries? NPolice On Scene? Y

Public Evac::?N Fi~Gility Evac? NFiremen On Scen13? Y DEP Requested? Y

Public Exposure? YWind Sp/Dir

Contamination of Air ,Land Receiving WaterStatus At Scene FIRE AT ABOVE FACnPrY, INVOLVING NITRATED ANILINE

._._----------------------------------._---_._--_._---_._-----------------------------Responsible Party Known

:Party CHEMICALS COMPOUNDSConr.act ALBERTO CELLERI

Street Address:29-75 RIVERSIDE AVE

Phone 201-850-1436rritle PRES

Municipali t:rNEWARK

CountyESSEX

StateNJ:=:====================:===============::==~==~=:==~=================::==============

NAMEOFFIC I1\LS NOTI:?IED

'rn:LE PHONE DATE TIMEN,JSP :WJNIC: NEWARK CITYIyrHE? :

201-733-7400 10/05

.~-----~----------------------------~----_.__ ._--_._--._--------------------_._-------Name

B.DOYLEA.ffiliation

DRPSR ERlMethod Date Time T/MOffice/Faxed 10/05 1110 T

"l. •

~:====================::========::=~===::===:===:=:==:=========================:::=======COMl1ENTS

F:SFEP.TO CASE #93-10-5~0736-.38 TD 16901 FOR il.31.0Ix FURTHER INFORMATION.

TIERRA-B-004376

MATERIAL SAFETY DATA SHEET

MANUFACTURER'S NAME:CHEMICAL COMPOUNDS, INC.29-75 RIVERSIDE AVENUENEWARK, NEW JERSEY 07104

EMERGENCY PHONE NO:(2D~) 850-1436/485-3212REVISION DATE:

CAS# 33229-34-4CHEMICAL NAME: TRADE NAME: HC BLUE 22,2'-[4[-(2-Hydroxyethyl)amino)-2-nitro phenyl]imino]diethanolCHEMICAL FAMILY:Nitrated Aniline

FORMULA: C12H19N305

- ,..

*** HAZARDOUS INGREDIENTS ***INGREDIENT: PERCENT TLVHe Blue 2 90% none est.

*** PHYSICAL DATA ***

APPEARANCE:SPECIFIC GRAVITY:B")~-I.ING..POINT (DE-iF):VAPOR PRESSURE (romHg) :SOLUBILITY IN WATER:PERCENT VOLATILE BY VOLUME:EVAPORATION Rt:E:

Odorless deep purple powderNot ApplicableDecomposesNot ApplicableSlight0.1 - 1.0< 1

*** FIRE AND EXPLOSION HAZARD DATA ***FLASH POINT (METHOD USED) : 400 DEG F (COC)FLAMMABLE LIMITS: Not ApplicableEXTINGUISHING MEDIA: Foam, Dry Chemical. Carbon

Dioxide, Fog, ox water SpraySPECIAL FIRE FIGHTING PROCEDURES: NoneUNUSUAL FIRE AND EXPLOSION HAZARDS: Combustion liberates oxides

of nitrogen

*** HEALTH HAZARD DATA ***ORAL LD 50, RAT: 4120 mg/kgEFFECT OF OVEREXPOSURE: Not establishedEMERGENCY AND FIRST AID PROCEDURES: Eyes: Flush immediately with plenty ofcold water for 15 minutes. Get prompt medical attention. Skin: Wash

TIERRA-B-004377

CHEMICAL COMPOUNDS, INC.Riverside Industrial Park

29-75 Riverside Avenue • Newark, New Jersey 07104(201) 485-3211-2 • Fax: (201) 485-4870

Emergency and Remedial Response DivisionU.S. Environmental Protection Agency290 Broadway, 19th FloorNew York, New York 10007-1866

Januaty 28, 1997

To Mr. Lance R. Richman, P.G.,

As per request, please find enclosed a re-submittal to the following responsesto the "Request for Information" received on July 10, 1996 at Chemical CompoundsInc .. The reason for the re~submittal W"l.S to further verify specific responses whichour company regards confidential information. If you should have any furtherquestions or require additional information, please feel free to contact Jim Giannottiat (201) 485 - 3212.

Sincerely,

.....

/- ... ~( .,--:- ...

.-::-

Jim Giannotttijg/JGC.c: AC/SG

t CFl1nn O· 1~\1 L'Cl...:~1.}'

TIERRA-B-004378

.. .0.· .' ~.. '

ATTA.CHMENT AREQUEST FOR INFORMATION

BackgroundThe united states Environmental Protection Agency (ltEPA") isinvestigating the release of hazardous substances into thePassaic River. EPA has information indicating that hazardoussubstances from your facility located at 29-75 Riverside Avenuein Newark, New Jersey may have been discharged into the PassaicRiver.Please provide the information requested below, including copiesof all'available documentation that supports your answers.

1) How long has your company operated at the facilitydesigna~d above? If your company no longer operates at thisfacility, during what years did your company operate at the·facility?2) a) Does your company have or has it ih the past had a permitor permits issued pursuant to the Resource Conservption andRecovery Act, 42 U.S.C. §6901 .e..t ~.? If "yes", please providethe years" that your company held such a permit and its EPAIdentification Number.

b) D~es your company have or has it in the past had a permitor permits issued pursuant to the Federal Water Pollution ControlAct, 33 U.S.C. § 1251, g.t ~.? If "yes", please provide theyears that your company held such a permit.

3) Did your company receive, utilize, manufacture, discharge,release, store or dispose of any materials containing thefollowing substances:

Yes No2,3,7,8 tetrachlorodibenzo-p-dioxin

or other dioxin compoundsAcetic acidAdipic acidAmmonia.AnilineBenzeneBenzo(a) anthraceneBenzoic acidBenzyl chlorideButyl benzyl phthalateChlorobenzeneChloroethyleneChloroform1,2-dichloroetheneDi-n-butyl phthalateEthyl benzene

1

ACFOOOO?OTIERRA-B-004379

· . . .... ~~. .,

Yes NoFluorantheneMethanol'Methylene Chloride2-methylnapthaleneNaptha distillateNapthalene2-nitrophenolPetroleum etherPhenanthrenepyreneTetrachlorobenzeneTetrachloroethaneTetrachloroethyleneTrichloroethaneTrichloroethyleneToluene -XyleneArseniccadmiumChromiumCopperLeadMercuryNickelSilverzinccyanidePCBs

,--

4) a) Provide a description of the manufacturing processesfor which all hazardous substances, including, but not limitedto, the substances listed in response to item (3), were a productor by-product.

b) During what parts of the manufacturing processesidentified in the response to items (4)(a), above, were hazardoussubstances, including, but not limited to, the substances listedin response to item (3), generated?

i) Describe the chemical composition of thesehazardous substances.ii) For each process, what amount of hazardoussubstances was generated per volume of finishedproduct?iii) Were these hazardous substances combined withwastes from other processes? If so, wastes from whatprocesses?

2

'ACF000021TIERRA-B-004380

, . .' . . ,' ... '-

5) Describe the methods of collection, storage, treatment, anddisposal of all hazardous substances, including, but not limitedto, the substances listed in response to item (3) and (4).Include information on the following:

a) Identify all persons who arranged for and managed theprocessing, treatment, storage and disposal of hazardoussubstances.

b) If hazardous substances were taken off-site by a hauleror transporter, provide the names and addresses of ~he wastehaulers and the disposal site locations.

c)' Describe all storage practices employed by yourcompany with respect to all hazardous substances from the timeoperations commenced until the present. Include all on-site andoff-site ~torage activities.

i) If drums wereon the ground or were theywith asphalt or concrete?of these storage areas.

1i) When drums were stored outside, were empty drumssegregated from full drums?

stored outside, were the drums storedstored on areas that had been pavedPlease provide a comple~e description

d) What processes do you use to treat your waste? What doyou do with the waste after it is treated?6) a) For process waste waters generated at the facilitywhich contained any hazardous substances, including, but notlimited to, the substances listed in response to item (3) and( 4) :

i) Was the waste stream discharged into a sanitarysewer and if so, during what years?ii) Were they treated before being discharged to thesanitary sewer and if so, how? Please be specific.iii) If the waste waters were not discharged to thesanitary sewer, where were they disposed and duringwhat years?iv) Please provide the results of any ,analysesperformed on any waste process streams generated at thefacility.

b) For floor drains or other disposal drains at thefacility:

3

ACFooon??TIERRA-B-004381

i} Did the drains connect to a sanitary sewer and ifso, during what years?ii) If the floor drains or other disposal drains atthe facility were not discharged to the sanitary sewer,where did they discharge and during what years?

c} i) Did any storm' sewers, catch basins or lagoons existat any time at the facility and if so, during whatyears?ii) If catch basins or lagoons existed, were theylined or un-lined?iii) What was stored in the lagoons?

-iv) Where was the discharge from any of thesestructures released and during what years? Was thisdischarge treated before its release and if so, how andduring what years? What was the chemical compositionof any waste waters released, and during which years?

d} Please supply diagrams of any waste water collection,transport or disposal systems on the property.

e) Also, EPA has information relating to several instancesof discharge of process waste water into the sewer system in 1992and 1995. Please provide a detailed description of theseincidents.7) a} For each hazardous substance, including, but notlimited to, the substances listed in response to item (3) oridentified in the responses to item (4), above, provide the totalamount generated during the operation of the facility on anannual basis.

b} Were any hazardous substances, including, but notlimited to, the substances listed in response to item (3) oridentified in the responses to item (4), above, disposed of inthe Passaic River or discharged to the Passaic River? If yes,identify the hazardous sUbstances, estimate the amount ofmaterial discharged to or disposed of in the Passaic River andthe frequency with which this discharge or disposal occurred.Also please include any sampling. of the river which you mighthave done after any discharge or disposal.8) Please identify any leaks, spills, explosions, fires orother incidents of accidental material discharge that occurred atthe facility during which or as a result of which any hazardoussubstances, including, but not limited to, the substances listedin response to item (3) or (4), were releaseq on the property,into the waste water or storm drainage system at ~he facility or

4

A C F 0 0 OHE~~A-B-004382

· ' ..,:-." ..-..:.:..~.. - '. ~., : -. .. -". ~ • _0' •.. ' ••• ' ... :- .. " .. "

to the Passaic River. Provide any documents or informationrelating to these incidents, including the ultimate disposal ofany contaminated materials.

a) Please provide the results of any sampling of the soil,water, air or other media after any such incident and before andafter clean-up. Please provide in this information all samplingperformed for or by NJDEP.

b) Also, EPA has information that due to an industrial sewerline break in.1992, an unreported quantity of anili~e wasdischarged to the Passaic River. Please provide all informationrelating to this and any other discharges and any measures takento mitigate the impac~ of the discharges.9) a) Was your facility ever sUbject to flooding. If so, wasthe flooding due to:

i) overflow from sanitary or storm sewer back-up,and/or

b)event.

ii) flood overflow from the Passaic Rive~?Please provide the date and duration of each flood

10) Please provide a detailed description of any civil,criminal or administrative proceedings against your company forviolations of any local, state or federal laws or regulationsrelating to water pollution or hazardous waste generation,storage, transport or disposal. Provide copies of all pleadingsand depositions or other testimony given in these proceedings.

a) EPA has information that your facility has receivedseveral notices of violation for discharges of waste water intothe sewer system, including a NJDEPE Field Notice of Violationissued on January 7, 1992 and a PVSC Notice of Violation issuedon February 9, 1995. Please provide information on how theseviolations were resolved.11) Provide a copy of each document which relates to thegeneration, purchase, use, handling, hauling, and/or disposal ofall hazardous substances, including, but not limited to, thesubstances listed in response to item (3) or (4). If you areunable to provide a copy of any document, then identify thedocument by describing the nature of the document (e.g. letter,file memo, invoice, inventory form, billing record, hazardouswaste manifest, etc.). Describe the relevant informationcontained therein. Identify by name and job title the person whoprepared the document. If the document is not readilyavailable, state where it is stored, maintained, or why it isunavailable.

5

fCF:oonn011~ TIERRA-B-004383

....

12) a) Did you or anyone else sample the soil, ground water,surface water, ambient air or other environmental media at thefacility for purposes other than those identified in questionsabove?

b) If so, please provide all other documents pertaining tothe results of these analyses.13) a) Has your company owned the facility at the locationdesignated above? If so, from whom did your company purchase theproperty and in what year? If your company subsequently sold theproperty, to whom did your company sell it and in what year?Please provide copies of any deeds and documents of sale.

~ .

b) If your company did not own the facility, from whom didyour company rent the facility and for what years? Pleaseprovide copies of any rental agreements.

c) To the extent that you know, please ,provide the names ofall parties who owned or operated the facility during the periodfrom 1940 through the present. Describe the relat~onship, ifany, of each of those parties with your company.14) Answer the following questions regarding your business orcompany. In identifying a company that no longer exists, provideall the information requested, except for the agent for serviceof process. If your company did business under more than onename, list each name.

a) state the legal name of your company.b) state the name and address of the president or.the

chairman of the board, or other presiding officers ofyour company_

c) Identify the state of incorporation of your company andyour company's agent for service of process in thestate of incorporation and in New Jersey.

d) Provide a copy of your company's "Certificate ofIncorporation" and any amendments thereto.

e) If your company is a subsidiary or affiliate of anothercompany, or has subsidiaries, or is a successor toanother company, identify these related companies. Foreach related company, describe the relationship to yourcompany; indicate the date and manner in which eachrelationship was established.

f) Identify any predecessor organization and the datesthat such company became part of your company.

6

"'CFonnn')t::.h TIERRA-B-004384

.:.~., .... '. "-, • ".' :. ,60. .~ • .'.- ... t •.......... '.,:' , ;' -.'

g} Identify any other companies which were acquired byyour company or merged with your company.

h) Identify the date of incorporation, state ofincorporation, agents for service of process in thestate of incorporation and New Jersey, and nature ofbusiness activity, for each company identified in theresponses to items (14) (e), (f), and (g), above.

i) Identify all previous owners or parent companies,addressees), and the date change in ownership occurred.

15) Provide the name, address, telephone number, title andoccupation of the person(s) answering this "Request forInformation" and state whether such person(s} has personalknowledge of the responses. In addition, identify· each personwho assisted in any way in responding to the URequest forInformation" and specify the question to which each personassisted in responding. Please include the names and addressesof former employees who were contacted to respond to any of thequestions. •

7

t.C F 0 0 G-1~R~~-B-004385

CERTIFICATION QF ANSWERS TO REQUEST FOR INFORMATION

state of New Jersey

County of _EIOl..W.S.oOl.s.s::;eAx _

I certify under penalty of law that I have personally examinedand am familiar with the information submitted in this document(response to EPA Request for Information) and all documentssubmitted herewith, and that based on my inquiry of thoseindividuals immediately responsible for obtaining theinformation, I believe that the submitted information is true,accurate,-and complete, and that all documents submitted herewithare complete and authentic unless otherwise indicated. I amaware that. there are significant penalties for submitting falseinformation, including the possibility of fine and imprisonment.I am also aware that my company is under a continu'ing obligationto supplement its response to EPA's Request for Information ifany additional information relevant to the matters'addressed inEPA's Request for Information or the company's response theretoshould become known or available to the company.

AJ herto Cell eriNAME (print or type)

PresidentTITLE (print or t~e)

SI~~'

sworn to b~ me thisOJday of 1-q JeHt., 19....L.I.c:=-~~~--::Ja;;;=Ftm:t-i c~.

ACF000027TIERRA-B-004386

CONFIDENTIAL

INFORMA TION CONTAINED HEREIN RESPONSE TO QUESTION # (4a) CONCERNS PRODUCTS,MATERIALS AND PROCESSES IS PROPRIETARY AND CONFIDENTIAL AND MEETS THE

REQUIREMENTS OF 42 U.S.c. §9604(e)(7)(E)

CHEMICAL COMPOUNDS, INe.RESPONSE TO REQUEST FOR INFORMATION DATED JULY 9, 1996

The following are the responses of Chemical Compounds, Inc. to the Request forInformation from the United States Environmental Protection Agency, dated July 9, 1996.

1. Chemical Compounds, Inc. (CCI) has operated at the facility in Building #17 at 29-75Riverside Avenue since 1990. It acquired the facility in July, 1986 (See Deed -Attachment 1) and installed equipment through 1990. During the 1986-1990 period itcontracted with another entity for the manufacture of its products (See, TerminationNotice to Southwest Photo Chern., Inc. - Attachment 1).

2, (a) Yes, CCI has had a permit pursuant to the Resource Conservation and RecoveryAct since 1990. Chemical Compounds Inc. 's EPA Identification # is NJD 108661737.(See Acknowledgement of Notification of Hazardous Waste Activity - Attachment 2.)

(b) Yes, CCI has a permit pursuant to the Federal Water Pollution Control Act, itsamendments, the Clean Water Act and the Rules and Regulations of the Passaic ValleySewerage Commissioners. The Permit Number is 20407122 and CCI has had the permitsince July 20, 1992. (See copy of the Sewer Connection Permit with Passaic ValleySewerage Commissioners-Attachment 3.)


3. Yes, the following is eers response to question NO.3.

.::::··,::,,::.,:::::··':I~,::::::::·',:::·':::.,:::::

X2,3,7,8 Tetrachlorodibenzo-p-dioxin orother Dioxin CompowlCls

Acetic Acid X

Adipic Acid xAniline xBenzene x

xBenzo(a)anthracene

Benzoic Acid xBenzy Chloride X

Butyl Benzyl Phthalate xChlorobenzene xChloroethylene X

Chloroform x, .

Di-n-butyl phthalate X

Ethyl Benzene X IFluoranthene X

Methanol X

Methylene Chloride X

1 2-Dichloroethene X

2 -Methylnapthalene

Naptha distillate

Naphthalene

2-Nitrophenol

xX

Petrolewn Ether

Phenanthrene

X

X

xX

Pyrene

Tetrachlorobenzene

Tetrachloroethane xTetrachloroethylene X

Trichloroetlwle xxTrichloroethylene

Toluene X

Xylene x

t-,\(i'1

t

~.,

tt.

'I I X IArsenic ,

II

X. CadmiumXChromium

I v II

l"...

fC~N':r

I XLead

~X IMercnrv .,

J ANickel~ v~Silver .

"

XZincX tCyanide

J [ XJ PCBs

. ------~(8), CON F 1 DEN T I A L

I

"CFOOC030h TIERRA-B-004389

4(b) Attachment 4 contains a list of process waste water streams and their respectivehazardous waste components.

i) The hazardous components generated as by-products in the waste water streamdue to the impurity of the raw materials are detected in ppb concentrations, andare noted in Attachment 4.

ii) The amount of hazardous substances generated per volume of each finishedproduct is not available. The hazardous substances generated in the waste water.stream of various products are contained in the range of 500 - 1500 gallons of99.99 % water. Therefore, an estimated amount of hazardous substancesgenerated per volume of water is < 0.01 %. (See Attachment 4.)

t"lCFOGnn~1TIERRA-B-004390

iii) The hazardous substances located in the waste water stream are generated onbatch scale operations. The by-products are present in the waste water streamafter the separation of the product by filtration, After filtration, the waste waterstream is treated for regulated effluent exceedances. After treatment, the wastewater is stored in a 10,000 gallon tank. A number of process waste water streamswill combine in the 10,000 gallon storage tank,

5 (a) The following table is a list of employees at eer who were or are responsible for themanagement of hazardous substances:

I..' .... :, ....t __

.··t.".!'.?7.········ >::::'Title... .', I :!j)'¢$~Flptioribfl!~~ppg"m».(-I:'l·!::I :.'-.-. Harne ..... ', ..

.--:':-:.;0:' ...... :';.:.':-/:---'

IAlberto Celleri

ICo-President

1Overall Operations

IHarold Sullivan

ICo-President Overall Operations

Anura Celleri Chemical/EII\'i ronmentaJ Waste Water TreatmentlHazardous.Engineer Substance Storage

Jim Gi<Jllllalli Cbemica lIE l1\'i ronmental Waste Water TreaunenUlfazardousEngineer Substance Storage


5 (b) The following table is a list of transporters who were responsible for off-sitedisposal: including non-hazardous waste water:

Franks Vacuum Tmck Services,Inc.

NYD982792814

4500 Royal Ave. Research Oil Co.Niagra Falls, NY 14303 2655 Transport Rd.

Cleveland; OH 4415OHD004178612

Freehold Canage Inc.NJD054l26l64

P.O. Box 5010Freehold. NJ 07718

Systech Environmental11397 County Road 176

Paulding, OH 45879OHD005048947

Laidlaw Environmental ServicesMDD980554653

3517 Whisky Baltom RoadLaurel, l\.1D 20424

Laidlaw Environmental Services3527 Whisky Bottom Road

Laurel. l\.1D 20424

Maumee ExpressNJDlJ866tl7380

P.O. Box 178Somerville. NJ 08X76

Rineco Chemical Ind.1007 Vulcan Rd. - Haskell

Benton, AR 72015ARD981057870

Oldover CorporationVAD098443443

P.O. Box 68Rt. L State Rd. 652Arvonia, VA 23004

Oldover CorporationP.O. Box 68

Rt. I, State Rd. 652Arvonia. VA 23004

Freehold Cartage Inc.NJD054126164

Chemical Waste Management ofNJ

NJD08lJ2 16790


100 Lister A"enueNewark. NJ tl7\05

ECOFLO2750 Patterson Street

Greensboro: Maryland 27407NCD980842132


100 Lister AvenueNewark. NJ 07105

Tn-Slate MOlOrTransit Co.MOD095018998

P.O. II:;Joplin. MO (,4802

Rineco Chemical Ind.1007 Vulcan Rd. - Haskell

Benton, AR 72015ARD981057870

t~CFOOC033TIERRA-B-004392

5 (c) i)& ii) The following table is a list of storage practices for the hazardoussubstances Included in items (3) & (4) since the begmrung of operatIOns:

..:•..•:!••~ai~~~;;.~~~~dOUS.:•.•:.. ·•••:! •••:I:!il::::::.!jlm¥j~1~~~~.:I!II!I:i.!il!.!:i·i:iiJ:!li;Jji!.i.il:•••.::iii·

Raw Materials

or

Laboratol)'Supplies

Acetic Acid 55 gallon Plastic Drum< 4 L Glass Bottle - Laboratory Scale5.000 gallon Tanker Truck - Waste

Adipic Acid 50 lb. Bags I 2000 lb. Palates< 1 lb. Glass Bottle - Laboratory Scale

Ammonia

Benzoic Acid

150 lb. Cylinder

50 lb. Bags I 2000 lb. Palates< I lb. Glass Bottle - Laboratory Scale

Chloroform < 4 L. Glass Bottle - Laboratory Scale2 gal. Solvent Lab Disposal Container

55 gallon s/s drum - Waste5.000 gallon Tanker Truck - Waste

·LOOO gallon S/S Storage Tank - Waste

Metklllol 55 gallon Stainless Steel Drum250 gallon Plastic Totes

-1.000 gallon S/S Stora~e Tank - Waste5.000 gallon Tanker Truck - Waste< 4 L. Glass Jars - Laboratory Scale

2 gal. Solvent Lab Disposal Container55 gallon S/S drum - Waste

Methylene Chloride 55 gallon Stainless Steel Drum-1.000 gallon S/S Storage Tank - Waste

5.000 gallon Tanker Truck - Waste< 4 L. Glass Jars - Laboratory Scale

2 gal. Solvent Lab Disposal Container55 gallon s/s drum - Waste

Toluene 55 gallon Stainless Steel Drum-LOOO gallon S/S Storage Tank - Waste

5.000 gallon Tanker Truck - Waste< 4 L. Glass Jars - Laboratory Scale

2 gal. Solvent Lab Disposal Container55 gallon S/S drum - Waste

Xylen~_ ..

55 gallon S/S Drum250 gallon Plastic Totes

-1.000 gallon S/S Storage Tank - Waste5.000 gallon Tanker Truck - Waste

< 4 L. Glass Bottles - Laboratory Scale2 gal. Solvent Lab Disposal Container

55 gallon sls drum - Waste

Waste WaterStorage

(ppb Concentrations)Based on Allal~1jcal

Data

By·ProducL' found in the wastewat<.'f Slre;!ll1:

AnilirK B(llZ~ll(.

Benzoic Acid. Chl"rnbenzene.Chlorofonn. Elhyl B(llune.

Methanol. Melhyl~tl~ ChlorideNaphthal(ne.2-:\'ilroPhenol.

Tctra~hloro(thykn~. Toluene.Xylene. l...:ad. Zmc·. l\anide

55 gallon dnun - Waste

400 - 4,000 gallon S/S Storage Tank

10,000 gallon S/S Storage Tank

5.000 gallon Tanker Trucks - Waste

!,CFoonn7..1TIERRA-B-004393

(\

The 55 gallon drums or 250 gallon Plastic totes containing hazardous substances listedin items (3) & (4) are stored on wooden palates outside on either a paved area withasphalt or a concrete pad. (See Attachment 5 for a facility layout for the storage areas ofhazardous substances.)

In December 1993, a concrete diked area was constructed outside the building locatedon the southeast part of the building with a capacity of25,000 gallons. The diked area iswithin an 18 inch thick concrete berm approximately 4 feet high. Inside is the waste waterstorage area with (2) 4,000 gallon Above Ground S/S Storage tanks and (1) 10,000 gallonAbove Ground S/S Storage Tank on top of an 8 inch concrete slab In the past, the wastewater and or flammable solvents such as methanol, xylene, & toluene were stored in a5,000 gallon Tanker Truck in that same area. In addition, waste flammable liquids werestored in a 4,000 gallon Above Ground S/S Storage Tank in the diked area. SinceSeptember 1995, waste flammable liquids have been recycled. Currently, the 4,000 gallonS/S Storage Tank is being utilized for waste water storage.

Empty dmms are segregated from full drums. The empty drums are located at themost southeastern part of the proper1Y, adjacent to or in an enclosed sh~d.

5 (d) The waste water streams are treated by neutralization, chemical precipitation, orcarbon filtration. The process waste water streams are transferred to one of (2) 1,500gallon mixing tanks for the introduction of treatment. One treatment involvesneutralization by the addition of Sodium Hydroxide or Sulfuric Acid to meet dischargeregulations. Another treatment involves carbon filtration for the removal of organics. Thedrain water is collected in an Above Ground S/S Storage Tank located in the basementand treated for heavy metals. The treatment for the drain water involves chemicalprecipitation with the addition of lime followed by filtration. After treatment, the wastewater is transferred to a storage tank and analyzed.

If the treatments are effective, the waste water is transferred to a 10,000 gallon AboveGround S/S Storage tank. After the tank is full the waste water is combined with thesanitary waste water from the facility and pumped out of the building into the PVSCsanitary sewer which flows approximately 70 yards to an interceptor of the industrial park.The solid waste generated from treatment is non-hazardous and disposed off-site to aregulated facility. Carbon filtration and chemical precipitation treatment methods haveonly been used since October, 1995. Prior to that time, the waste water was treated byneutralization.

t,C F 0 0 nE~~;B-004394

,\

6 (a) i) From July 1992 to the present, the process waste water stream was dischargedinto a sanitary sewer connected with Passaic Valley Sewerage Commissioners.Before July, 1992, the process waste water stream was connected to a 5,000gallon tanker truck for off-site disposal.

ii) Yes, the waste water stream is treated before discharging into the sanitarysewer. The water is treated by neutralization, chemical precipitation, and carbonfiltration. (See 5 (d) for details of the treatment methods.)

iii) Before CCI obtained a permit for discharge to the sewer, the waste waterstream was collected in a 5,000 gallon tanker truck. When the tanker truckachieved maximum capacity, the water would be sent to a TSD facility fortreatment. CCI obtained a permit for discharging process waste water to thesewer on July 20, 1992. (See Attachment 11, for manifests.)

iv) Attachment 4 contains analytical results of process waste water streams.

6 (b) i) & ii) From 1986 - February, 1992, the main manufacturing floor at the facilitywas equipped with internal floor drains which were directly connected to thesanitary sewer. From February, 1992 through July, 1992, the drain water wascollected into an above ground storage tank located on the basement .floor and sentdirectly to a 5,000 gallon tanker truck. When the tanker truck became full, it wassent for off-site disposal. From July, 1992 - April, 1993, the drain water was sentto the 5,000 gallon Tanker Truck. then was combined with process waste waterand then transferred to an above ground storage tank in the basement. Aftersampling and analysis for effluent exceedances, the waste water was combined inthe basement with the sanitary waste water from the facility and pumped out of thebuilding into the sanitary sewer. In April, 1993 CCI replaced the 5,000 gallonTanker Truck with a 10,000 gallon above ground S/S Storage tank.

From 1995 to the present, the drain water has been transferred to an above groundS/S storage tank for the treatment of heavy metals by chemical precipitation. Aftertreatment, the drain water is transferred to another above ground storage tank foranalysis. If the treatment has been successful, the drain water is sent directly tothe 10,000 gallon Storage Tank, and mixed with the process waste water. Afterthe tank has accumulated to its maximum capacity, the waste water is combinedwith the sanitary waste water from the facility and pumped Ollt of the building intothe sanitary sewer which flows approximately 70 feet to an interceptor of theindustrial park.

6 (c) i) There have been no storm sewers, catch basins, or lagoons located at Building #17, 29-75 Riverside Ave, Newark, NJ since the beginning of operations ofCCI.

ii) N/A

iii) N/A

IV) N/A

6 (d) The facility layout for the collection, storage, and disposal ofwaste water can belocated in Attachment 6.

6 (e) On January 7, 1992 the Newark Fire Department and the New Jersey DEPresponded to a complaint of a discharge at the CCI facility. CCI's next door neighbor hadplugged up the sewer line, and when CCI'S personnel excavated the line to attempt toclear it, the contents of the line, including water colored purple with Red;; 3 and Blue # 2dye was disbursed into the excavation. This water was pumped out of the excavation ontothe ground where it was observed by the Fire Department and DEP. CCI was ordered toclean up the discharge, which was analyzed and shown to be non-hazardolls. (See analysisof soil and liquid samples - Attachment 8) CC I was charged with discha r'ging to theP\'SC sewer without a permit (See Attachment 7).

Subsequently, after CCl obtained a PYSC permit, it was cited by PVSC for havingdischarged waste water to the sewer which contained some volatile compounds and metalsin excess of permitted concentrations. These discharges exceedances ha\'e been resolved,and current treatment methods appear to be keeping wastewater discharges withinpermitted parameters.

7 (a) The total amount of hazardous substances generated during the opt'ration of thefacility on an annual basis can not be determined The hazardous substances which arecontained in the waste water stream are determined by the purity of the raw materials. Asa result, contaminant concentrations differ from one manufacturing batch to another.

7 (b) Chemical Compounds Inc. has not discharged any hazardous materials into thePassaic River.

8 (a) There have been no leaks, spills, explosive fires or other incidents that occurred atthe CCl facility that resulted in hazardous substances being released.

ACFonnn7Qh TIERRA-B-004396

8 (b) eCI did not discharge any hazardolls material into the Passaic River. (See answer to6(e) for description ofincidem.)

9 (a) Yes, CCl's facility is subject to flooding due to the close proximity of the PassaicRiver. Flooding does occur due to the overflowing of the Passaic River. As a result, thewater generated due to the flooding of the Passaic River is analyzed, treated and stored atour facility before discharging to the sewer.

9 (b) Flooding occurs during very bad storms, the dates of each occurrence are notknown

10 (a) In 1992. due to the discharge described in 6(e), Cel paid administrative costs to the.New Jersey Department of Environmental Protection for the discharge response. TheNJDEPE Case # is 92-01-07-1025. In addition, CCI was charged with violating theWater Pollution Control Act for negligently discharging a pollutant into a municipaltreatment works without possessing a valid industrial pretreatment permit issued by thePassaic Valley Sewerage Commission. CCl pled guilty to a fourth degree water pollutionviolation with a tine of $5,000 for the offense and had to provide a check in the amount of$1,76085 payable to the Otfice of the State Environmental Prosecutor to be used topurchase a one page advertisement in the Gloucester Times conveying a positiveenvironmental message.

CCl also paid for administrative costs when the Bureau of Emergency Responseresponded to a chemical fire at the facility on October 5, 1993. The case was closed. TheNJDEPE Case #' s are 93-10-05-0736 & 93- 10-05-1110.

On September 14, 1994. CCI had received a Notice of Violation from the Division ofFacility Wide Enforcement - NJDEP. The inspection identified a violation of the SolidWaste Management Act (N-lSA. 13: 1E-I et seq.) and Regulations (N.lA.C. 7:26-1 etseq.) promulgated thereunder. Remedial actions to correct the violations wereimplemented by CCI within days and no further enforcement was required thereafter.

With regard to violations of discharge permit limitations, eCI resolved the matter byentering into a Consent Order and Final Judgement with the Passaic Valley SewageCommissioner on November 24. 1994. by which it paid $6,000 to PVSC and entered intoa compliance schedule, which was subsequently extended to July I. 1996. (See ConsentOrder and Final Judgement and other relevant documents - Attachment 9 & 10.)

f,CF000038TIERRA-B-004397

11) For the purchasing of listed hazardous substances, such as raw materials, in item (3)or (4), the following table indicates CCl's suppliers since the beginning of operations.Documents such as invoices. bill of ladings. and a purchase order book for receiving thesehazardous substances are available .

..:.:}iazardoui(Su l}stancc-)} ·Ral~Mllte~il,i.··

. 1

Acetic Acid

Brown Chemical

Duso Chemical

302 West Oakland Ave.Oakland, N.J. 07436

Brown Chemical

Adipic AcidTextile Chemical

AmmOlll,l Jones Chemical

Benzoic Acid

Textile Chemical

Textile Chemical

JLM Industries

173 Smith StreetPoughkeepsie. N.Y. 12602

302 West Oakland Ave.Oakland. N.J. 07436

990 Jersey AveNew Brunswick. N.J. 08901

l 80 Munson StreetL7Roy. ~.Y. 144!2

BI'o\\'n ChemicalMeth:lllol

990 Jersey Ave.New Brunswick, N.J. 08901

8675 Hidden River ParkwayTampa, FL 33637


990 Jersey AveNew Brunswick. N.J. 0890 I

Brown Chemical

Methylene Chloride

Textile Chemical



BrowlI Chemical

TolueneTextile Chemical


990 Jersey AveNew Brunswick, N.J. 08901

-

Xylene Textile Chemical 990 Jersey AveNew Brunswick. N.J. 0890 I

f.CFoon039TIERRA-B-004398

For laboratory supplies, the following table provides information regarding suppliers:

Laboratory'1\1 ated<i1 Name

Acetic AcidAdipic Acid

Benzoic AcidChloroform

Melhylene ChlorideMethanolTolueneXylene

41 Plymouth StreetFairfield. N.J. 07004

PCI Scielllific Supply. Inc.

711 Forbes AvenuePittsburgh. PA 15219-4785

J.T. Baker 89 Newbury StreetSuire 103

Danvers. MA 01923

Fisher Scientific

For the hauling and disposal oflisted substances, such as waste water, plant andlaboratory solvents, in items (3) or (4), the following table indicates CCI's past and presenttransporters and disposal facilities. Documents, such as manifests. for the disposal of thesehazardous substances are in Attachment II.

<i.;llaia l;d olJs$t1.1Htii.nce < .," ... '... '!nlllspoI1crN]ame i'\••••••

<.TSD~l....Methanol. Xylene Freehold Cartage Inc ECOFLO

Waste Flammable Liquids 2700 Pallcrson St.Greensboro. NC 27407

Dye Waste Water Chemical Waste Management Chemical Waste ManagementNon-Hazardous 100 Lister Ave.

Newark. NJ 07105

Methanol. Xylene OldO\er Corporation Oldover CorporationWaste Flammable Liquids Route I. St:lte Road 651

Arvonia. V A 23004-- - _.

Chloroform. Methylene Chloride. Tri·Slal~ Motor Transit Co. RinecoXylene 1007 VUICaJl Rd. - Haskell

Laboratory Solvents Benton. AR 72015Waste Flammab[e Liquids

Dye Waste Water Laidlaw Environmental Services Laidlaw Environmental ServicesNon-Hazardous 3527 Whiskey Bonom Rd.

Laurel. rvID 20724

Dye Waste Water Maumee Express Ritl~cONon-Hazardous 11107Vulcall Rd. - Haskell

Beillon. AR 72015

Waste Dye Franks Vacuum Truck SClyice Research Oil Company(HC Yellow # 2) Inc. 2655 Transpon Rd.

Cleveland. OH 4415

M~thanol. Xylene Freehold Cartage Inc. Systech EnvironmentalWaste Flanunable Liquids 11397 County Rd. 176

Paulding. OH 45879

ACFoOOOt;nTIERRA-B-004399

12 a) & b) There has been no sampling of the soil. ground water, or surface water at thefacility for purposes other than those identified in the responses above. However, anOccupational Health Survey was conducted by CCl's insurance company to evaluateemployee exposure to possible various airborne contaminates. The survey included airsampling for xylene, methanol and others. As a result, none of the employees' exposuresexceeded the OSHA Permissible Exposure Levels for the above contaminatesAttachment 12 contains the report provided by CCI's insurance company.

13 a) Yes, CCI has owned the facility at 29-75 Riverside Ave. - Building # 17 since July1, 1986. Attachment 1 cOlltains a copy of the deed of sale. The property was purchasedfrom Industrial Development Associates. Inc ..

13 b) N/A

13 c) In 1888 the Freeholders of Essex County sold the property to Triton Boat Club ofNewark. This transaction is recorded in Essex County Deed Book K-24. Page 133. OnMay 16, 1902, Patton Paint Company acquired the property from the Triton Boat Club ofNewark, as recorded in Deed Book 1-35. Page 270. Patton Paint Company was amanufacturer of paint and varnishes.

Thereafter, Pittsburgh Plate Glass Co which manufactured paint and varnishes, tookthe subject property. The property was identified as Block 614, Lot 1. The currentfacility - Building # 17 - was constructed by the Pittsburgh Plate Glass Co as a chemicalresin manufacturing facilit~· for its operation PPG, Inc. which was formerly calledPittsburgh Plate Glass Co. purchased the property on January 31, 1941, and held theproperty to August 2, 1971.

In 1971, the site was sold to a developer, Riverside Ave. Properties, lnc .. Deed Book4382, Page 1023. Riverside Ave. Properties. Inc. thereafter leased the site. On October11, 1979, the property was sold to another developer, Industrial DevelopmentCorporation, which sold the property a month later to Industrial Development Associates.The principal ofIndustrial Development Associates is Anthony V. Pugliese, 1II. IndustrialDevelopment Associates leased the building to S.B.S. Chemicals, Inc. and Desachem Co.,Inc, manufacturers of chemicals and detergents. S.B.S. Chemicals and Desachem Co., Incoccupied Building # 17 pursuant to a lease agreement with Industrial DevelopmentAssociates, which argument expired on August 14, 1985. Thereafter. the building wasvacant and the lot and block numbers were changed and subdivided from Block 614, Lot I(partial) to Block 614, Lot 66. eel has 110 relationship with the past owners or tenants.

!I('Foonn.~1;~v TIERRA-B-004400

j

\14 (a) The legal name of the company is Chemical Compounds Inc ..

14 (b) The president of the company is :'\'Ir. Alberto Celleri. Mr. Celleri'~ address is 10Baldwin Court, Roseland, NJ 07068.

14 (c) Chemical Compounds Inc. is incorporated in the state of New Jersey.

14 (d) Attachment 13 contains a copy of the company's "Certificate ofIncorporation"and amendments thereto.

14 (e) CCI is not a subsidiary or affiliate of another company.

14 (f) Chemical Compounds Inc. has no predecessor organization

14 (g) Chemical Compounds lnc has not acquired nor merged with any other company.

14 (h) N/A

14 (i) There are no previous owners of eel.

15. The person answering this Request for Information is Alberto Celleri. President ofCCI, 10 Baldwin Court, Roseland, New Jersey 07068 (201) 364-0370. Mr. Cellen haspersonal knowledge of the responses. rvlr. Jim Giannotti, 72 Califon Drive. Colonia, NJ07067, (908) 382-5591, a Chemical Engineer at eCI, assisted with the preparation ofthese responses.

DATE OF VISIT: 1/7/92

COMPANY NAME: Chemical Compoun~s, Newark

COMPANY REPS: Harold Sullivan, PresidentAlbeI10 Celleri, Vice President

CRIMINAL JUSTICE: Frank BradleyVincent K. CinoFern Siegel

DEPE EMERGENCYRESPONSE: Matthew Garamone

NEW ARK HAZMA T: Battalin Chief, Anthony L. Aposrolico

ENSI: Fred Virazzi

PVSC REP: R. Quintieri

PURPOSE: Illegal Discharge

SUMMARY:

In response to a report by New Jersey Criminal Justice of an illegal dischargeby Chemical Compounds, [ was dispatched to investigate the situtation. Uponarrival [Cl the facility at 1:30 pm, I spoke to Mr. Cino, Criminal Justice, who toldme that the Maritime police had caught Chemical Compounds illegally dischargingwastewater to the river Lind to the groundwater at the side yard. At the time of myinvestigation the company hLid stopped production and an discharges.

I began my investigation by inspecting his process area. There was still traceliquid from his wastewater discharge at the noor drain, the pH was bewteen 2 & 3. Iinformed Mr. Sullivan, the president of Chemical Compounds, that it was illegal toJischarge any waste wastewater below 5.0. I also reminded him the ChemicalCompound is not allowed to discharge any of their wastewater because theCompany has elected to be considered a zero discharge regulated facility, and hasbeen filing zero discharge reports. Mr. Sullivan stated the company has recentlyadded an additional product line and was in the process of requesting an applicationto discharge.

TIERRA-B-004402

i\1r. Sullivan then referred me to Mr. Celleri 1 Vice President. Mr. CeJleristated that the spill in the process area was caused while the company wastransferring the spent acetic acid from their centifuge which is used to remove thespent acid from his product to the CWM tanker located in the yard outside of theprocess area.

We then proceeded to the stairs outside of the process area where two 5000gallon tank trailers are parked. Mr. Sullivan stated they pump their processwastewater to the tanker which is then shipped to Chemical Waste Management.

Examination of the yard showed several areas of surface water mixed withwaste product. There was also an excavation surrounding their sewer line. Mr.Sullivan stated that the sewer was blocked. (The cause of the blockage was found tobe a plug in the line by Napp Greco. The city directed Napp Greco to remove theplug).

The Criminal Justice Department required Chemical Compounds to hireENSI to immediately remove the surtace water and to make preparations to removethe contaminated soil. ENSI used a vaccum pump to pump the water into 55 gallondrums. When ENSI began pumping the wastewater, the Criminal Justices Officalsfelt thut the situation was under control and left the facility.

RECOMMEND ATION:

r recommend that Chemical Compounds be Gted for discharging effluentwaste below 5.0, discharging noxious odor and incorrectly reporting zero discharge.TIle company should also be directed to install a pH control system. I left a SewerConnection Application with Mr. Sullivan.

R. QuintieriRQ/mc

TIERRA-B-004403

,DEQ-1164/89

NEW JERSEY DEPARTMENT OF ENVIRONMENTAL PROTECTIONDIVISION OF ENVIRONMENTAL QUALITY

BUREAU OF EMERGENCY RESPONSE

FIELD NOTICE OF VIOLATIONS

CASE NO. 92-0/-07- Icrc2C DATE O;jof/92.-CASE NAME CIfet1£Y4[ COd/otlj/()S IJ4~,Tl!E61£ J)lfl1/!rYtPINCIDENT LOCATION filS S/trc 1ClJ~ et fJ.V137(s+/)T /f/~ m?9l(K

;>-

RESPONSIBLE PARTY ADDRESS CW/1':CC/lI- C0/1/0,fA/l)s- 21-71:: \1Vel'!' \ tiff ~ 49)

RESPONSIBLE PARTY REPRESENTATIVE CeUE r-<:......I""O:::::;--=-.=.::=-"'-----'--"'"'=---r-.J-"-L...+J.'-'--~'_____=_::....:.....;_"'_____=._~_

You are hereby NOTIFIED that during an investigation by DE? on the above date, the following violations of New Jersey

Statute and/or Regulation were observed. This violation has been recorded as part of a permanent enforcement history

file. In addition, this case is being forwarded to the appropriate Division with a recommendation that formal enforcementaction be taken.

~- NJSA 58:1 0-23.11 ----=~_

[21-NJSA~23:5·28

D NJAC -.7:26-7-

D_~ ,- _0----- _

c e SPILL COMPENSATION AND CONTROL ACT

POLLUTION AND OBSTRUCTION OF WATER

HAZARDOUS WASTE REGULATIONS

Within Ill1.Mtc10ftl;. 08ys-ef receipt of this notice, you shall submit in writing, to the address and investigator indicated

below, an account of the incident and corrective measures taken to attain compliance.

Investigator 11V1~ f!7ttn/rtO/)£-,

Address IY..J]!7j/E~611t:f7f?/ i<eptfVt2/fJ)/7 T:;z &k~c;f f0 ~rOh#e- dJ: 070S-~

COPlES: White· File Yellow. Investigator Pink - Responsible Party

TIERRA-B-004404

New Jersey Department of EnvironmentalCOMMUNICATIONS CENTJm NC~~IFICjWION

Received: 1/07/92Dperator:JIMH

ProtectionREPORT

TD LogCase #

r~/~7~r:-

# 3 ~:29 :1-1-7-1I) 25 - 3 3

._._-------------------------_._------_._--------_._--._._----~----------_ .._----_._------_.-R'3ported By

PICCITTOStreet Address

Notification Type: OtherAf:Eil.i.atio:1NJSP !'IARINEMunicipality

PhonE3201·-578-81.n

StatH

Incident Location: Other8ite NEXT TO J?hO)'lf3

Street Address Municipality1500 MCCAR'lHER HWY NEWARKLocation 'lype Industrial Incident Date

CountyESSEX1/07/92

StateNJ

Time 1016._._----------~-~--------------------_._----_._---_ ...._---------------_ .._--------------:3ubstance Released UNKNOWN LIQUID

Amount Released ( lUNKIn:UnknO\·m State Liquid CAS# Release I5 Continuous

Additional SubstancesSubstance Contained? N Hazardous Material? U TCPA? U A310 Letter? Y

COMU CODE: 0714 REF CODE: 001._._-------------------------_._-------.--------_._-_.---------------------_. __ ._------_.-Incident Description Illegal Dumping

Injuries? N·Police On Scene? Y

Public Evac? N FdCili ty Evac? N Public Exp0:i>ure?YFiremen On Scenl3? N DEP Hl3quested? Y Wind Sp/Dir

C'JntaminatiO.I1.,OfLand/Water Reeeivinq Water PASSAIC RIVERStatus At Scene DUt-1PINGFROM PIPE TO LOT lIND INTO RIVER

._._---------~---------------_._------------_._._--_.------------------------------_.-Responsible Party

:Party POLITICAL COMP.Contact·

Street AddressJ1CCARTHER HWY

KnownINC Phone

~P.i.tleMunicipa1ity

NEWARKCounty

ESSEXStateNJ:::=~=======~;;;==============:========::=====:=:::==:::=================::==========::=~=

NAMEN,JSP : OEMJ11JNIC:NEWARK CITYo'rHER:

OFFICIALS KOTIFIED'rITLE PHONE

609-882-2000201-733-7400

DATE 'rIME1/071/07 1034OPER 41

..._----------------------------------_._----_. __ ._-_ .._----------------~._--_._---------,-Name

1, C.GIBBONS2·,At,64a;J-frO'Jc?3.

AffiLLaticnDRPSR EHl.OEP McnitoringDFG HQl

MethodOfficeFaxedFaxed

Di~te1/071/071/07

'rime1030

=:================~==========:========::====~==::==::================~==========::===COMl1ENTS

TIERRA-B-004405

-;;J,' 'j,

New JE'r~_1 DepaTtmem. 0:E EnvironmlcmtalCOMMUNICATIONS CENTER NO~~IFICjV.rION

H'3ceived: 1/09/92Operator:RICH

Prc,--;tionREPORT

TD LogCase #

# 472n-1-9-1027-J.8

Hl3ported ByINV VINCE CINO

:)ueet Address

Notification Typ(3:._._--------------------------,-------_._----_._._,--~~-----------------_._---------_ ..__ .-

Othe~:A:::EiliationDIV CRIMINAL JUST.Municipality

Incident Location: FacilitySite CHEMICAL COMPOUNDS INC Phone

Street Address Municipality29-75 RIVERSIDE: AVE NEWARKLocation Type Industrial Incident Date

201-485-3211County

ESSEX1/09/92

PhonEl908-6:36-0364

Btatn

StateNJ

Tim'3 1015._--------------------------_._-----~------_._._._--,.-----------------------_._---~--_.-Substance Released UNKNOWN LIQUIDAmount Released ( )UNKNOWN

ID:Known State Liquid CASt Release Is ContinuousAdditional SubstancesSubstance Contained? N Hazardous Material? U TePA? U A310 Letter? Y

COMU CODE: 0714 REF CODE: 001Incident Description Illegal Dumping._._-------------------------_._-----~_._----_._._-_.-._----------~~---_ .._---,-_._------_.-

Injuries? N"Police On Scene? N Public Evac? N Fiieility Evac? N Public Expo::;:ure;;N

Firemen On Scen(~? N DK? Hequested? Y Wind Sp/DirContamination Of Land,Water Re·ee:l'Tin9Water PASSAIC RIVER:)tatus At Scene COM:PANY RESUJY\ING ILLEGAL DU11:?INGFROM ANOTHER POINT,

PtW::PINGFROM PIT INTO OPEN LOT._--------------------------_._------_._-------_._-_ ..----------------------_._--- .._--

Responsible Party Known:Party CHEMICAL COM:POUNDS IContact ALBERTO CELLERI

Street Address29-75 RIVERSIDE AVE

E~one 201-485-3211'l',itl e OWNER

Municipalit? CountyNEWARK ESSEX

NAMEN.JSP : OEMI1UNIC: NEIAlARKCITYO'rHER:

OFFICIALS NOTEI};])'rITLE

::===========================:=============::=::;:==~================::=============:=State

N~r

PHONE609-882-2000201-733-7400

DATE -rIME1/091/09

._._-------------------------_._------_._-----_ ...__ .-._---------------- .._----_._--------Name

1. CHRIS GIBBO:r-;-S2.?,J •

AffiLlation MethodDRPSR ERl Office,FaxedOEP Monitoring Faxed

Dilte 'rime1/09 10281/09

~:IN~;~:

COMHENTS:=========================================::====:::============================::===RE:SP 16 ENROUTE @ 1039 HRS

J At·! - 0 '3 - '~:2 T H I I .... TIERRA-B-004406

DATEt1L-~ er {(Mo) (Day) ~

Jf.1..p. PN..I}"1 off' -NEW JERSEY DEPARTMENT OF ENVIRONMENTAL PROTECTION (J L.> ~

DUTY OFFICER NOTIFICATION REPORT Y'pPCASE NO. q2.M. ()7-. /02S-

(Yr.) (Mo) (Day) (Time)

,ForA, DEP-001 C9/88

REC'D BY __ -=-- TIME _

IDENTITY OF SUBSTANCE(S) SPILLED, RELEASED, ETC.:Name of Substance(s) [GaS,@SOlid]: , IIn k-- I ,''1-' VI' JL.-_-,--_----'- _Amount Released/Spilled __ Actual ~ Potential

Type of Release/Spill: __ Terminated _/_ ,.C"'ontinuol'

__ Suspected __ Unknown

INCIDENT REPORT BY:

Name ')p.cf"'\~r £; ...I..c fit)Street _

City State _

AffiliationlTitle _

INCIDENT LOCATION:

Name (Site): / .500Street _

__ Transportation

mC C.-..,kr }-LghkJA.<..,\

__ Facility

Phone --:- _

__ Other: _

City '" ) f.vJ~J"iL-Date of Incident: QL-0 "":::J-_ ---.5l

(Mo) (Day) (Yr)

__ Estimated

___ Intermittent

Substance Contained y @J U

Hazardous Material Y N U

INCIDENT DESCRIPTION:__ Fire

__ Odors

__ Explosion

__ Sewage

__ Air Rei __ Spill __ MVA

__ Wildlife

_ ~~ent __ SmokelDust

_~_ 1II'''''eg'''allDumping __ Drums__ NJPDES __ Noise

__ Equip Start-Up/Shutdown, Equip Fait/Upset, etc. _

__ Other (specify) _

Injuries Y guFacitity Evacuation Y U

Population Evacuation Y . U ~

Potable Water Source Y N Y/Contamination of __ ~ __ ' _ Land __ Water

{ () ...Receiving Water .{\~\('" r.. /<- \ vZ'" Wind Direction/Speed I

Location Type: __ Residential __ Industrial __ Commercial __ Rural __ Sensitive Population (Hosp., SChool, Nurs. Home)

STATUS AT INCIDENT SCENE ()~, 'Y'p'/'.), ~~>/'('\' !J;,Vf \,' II fc Qio,'nd'-r- _r j /

PubliC Exposure (j)N U

Fire Department at Scene Y @ U

Police at Scene (Y;)N U

Assistance Requested @N U

Precipitation Y N U

__ Suspected __ Unknown,( c" f" ,I d

;-{f!"\

OFFICIALS NOTIFIED (Name/Title):

NJSP: / Phone _ DatelTime / __ ITIM\--- TIERRA-B-004407

New Jersey Department of Environmental Protection and EnergyDivision of Responsible Party site Remediation

Bureau of Emergency ResponseRegion I

INVESTIGATION

Case *= 92-1-9-1027-18 i'ile if: 0714PAC CODE:Date: 1/15/92

Investigator: Christopher Gibbons Time Arrived:

Location: Chemical Compounds Inc.Address: 29-75 Riverside Avenue

Newark, Essex CountyResponsible Party: Chemical Com~ounds Inc.Mailing Address: 29-75 Rivers1de Avenue

Newark, Essex County

Time Departed:

Location Phone f: 485-3211Health Dept. Rep: NoneOrigin of Complaint: Vince Cino, DCJ

Phone #

Phone # : 908-686-0364

Nature of Com~laint: Inspector Cino received call from Napp Greckocor~. of cont1nuing illegal dumping from Chemical Compounds Inc.Ass1stance is requested.Findin~s: Inspector Gibbons responded to the above location toinvest1gate illegal dumping from Chemical Compound Inc. (see reportcase nUmbers 92-01-07-1025 and 92-01-08-1147). This request for aresponse came from Investigator Vince Cino, DCJ who was notified byNapp Grecko Corp. of continuing illegal dumping at the ChemicalCompounds Inc. site.On site Inspector Gibbons met with Robert Penn, Newark OEM, Chief TonyApostilico, Newark HazMat and Vince Cino, and the situation wasdescribed as follows.Because the main sewer truck line runs under the Napp Grecko Corp.repair garage, and acetic acid odors were noticed, Napp Grecko Corp.reported the incident. On site at Chemical Compounds Inc. no illegaldumping was occurring. Discharging through the sanitary sewer linewas a acetic acid odor, pH3 water mixture. It was explained that thewater was non-contact cooling water. No odors were noticed inside theNapp Grecko varage, and no readings were detected by Drager tubes foracetic acid 1nside the garage. DCJ Water Pollution Task Force tooksamples, then all responders secured the site.

TIERRA-B-004408

..

Conclusions: BER I responded at the request of DCJ to a continuingillegal dumping problem at Chemical Compounds Inc. DCJ was notifiedby Management of Napp Grecko Corp. that since odors were noticed in arepair building directly over the main sewer truck line, ChemicalCompounds must be dumping. In the sewer line was a non-contactcooling water which had a pH of 3 for an unknown reason and positivevapors for acetic acid were detected utilizing a Drager tube for thespecific compound. No odors were detected in the Napp Grecko repairgarage. DCJ Water Pollution task force obtained samples, then allsecured the scene.Recommendations: This case was referred to OEP-Metro and DFG & w.NFA/BER I.

DateSupervisor Date

TIERRA-B-004409 '

DC003G

COUNSELLORS AT LAWRIJSSHL r KERBY" .lR •.J0fH'j W' COOPER.!!:RRY FITZGERALD ENGLISH:\RTHUR H GARYI), III

C."RY F DANIS. P E

~80 MORRIS AVENUE

RON/"LD.J TELL,TEYHI S GOLDENBERG'OF COUIJSEL

908-273-1212

FAX 908-273-8922'

FREDI L PE....RLMUTTER.KRIST! BEYER llRACC'STEPHEN R. CEllER'PETER W ULICNYDONNA M RUSSO"DANiEl JON KLEINMAN'"HOLLY ENGLISH ••••MARCAR£T R. KALAS"MARY T ZDANOWICZROBERT A. MEYERSRICH ....RD F. ICLIIR'

SUMMIT, NEW JERSEY 07901-l583

RICI·I.~RJ) C MOSER

1940'1992

~""'LSO ADMITTED IN N Y

"~"--'L.SOADMiITED IN 0 C

....•.....UO ADM-ITTfO IN P.t\

..···A.DMJTTf.D IN MA ONLY

May 25, 1993

John Ambrosio, Esq.464 Valley Brook AvenuePost Office Box 911Lyndhurst, New Jersey 07071

Re: Chemical Compounds, Inc.Compliance Schedule

Dear Mr. Ambrosio:

As we discussed recently by telephone, we are the attorneysfor Chemical Compounds, Inc., which SUbmitted its BaselineMonitoring Report Addendum for Mass Limitations to the PassaicValley Sewerage Commissioners (PVSC) on May 6, 1993.

As we also discussed, the sampling of Chemical Compounds'effluent has indicated the presence of toluene in its waste stream.So far the company has been unable to identify the source of thetoluene, despite investigatory efforts.

In order to cope with the toluene issue, and to better controlits effluent, Chemical Compounds is in the process of installing aholding tank at its facility. The effluent in the tank will besampled before discharge, and should there be problems with theeffluent, appropriate measures will be taken.

On behalf of Chemical Compounds we are hereby requesting acompliapce schedule for instituting the above described measuresand res9~ving the toluene problem. To this end, we think that itwould be:\helpful to set up a meeting to discuss a complianceschedule\J~nd a JUdicial Consent Order, which you indicated would benecessarYl:/'

(. ,'·)1

J ,.

I

. '.. ,

TIERRA-B-004410

IrII

,...... .

. John Ambrosio, Esq.May 25, 1993Page 2

Please advise us as to how you would like to proceed indetermining a compliance schedule, and in negotiating a JudicialConsent Orqer.

::J?:ruJJpr,-~~S~ller

SRG:pbkcc: Harold Sullivan

John SabaJerry Fitzgerald EnglishGary F. Danis

:\

TIERRA-B-004411

........ ~ ..... oIq

/~ANIEL f. BECHT. ESQ.CHAIRMAN

Passaic ValleySewerage Commissioners CARMINE T. PERRAPATO

EXECLJTIVE DIRECTORTHOMAS J. CIFELLIVICE CHAIRMAN 600 WilSON AVENUE

NEWARK, N.J. 07105(201) 344·1800

Fax: (201) 344-295'

ROBERTJ.DAVENPORTOEPUTY EXECLJTIVE OIRECTORROBERT M. BURKE, JR.

DOMINIC W. CUCCINELLORONALD W. GIACONI~JAMES KRONERAYMOND LUCHKOFRANK ORECHIOOONALD TUCKERCOMMISSIONERS

GABRIEL M. AMBROSIOCHIEF COUNSEL

LOUI S LANZllJ.O

CLERK

June 7,1994

Mr. Harold E. SullivanChemical Compounds29- 75 Riverside AvenueNewark, New Jersey 07104

Certified MailP 252571201

Dear Mr. Sullivan:

RE: NOTICE OF VIOLATIONPERMIT #: 20407122VIOLATION DATE: APRIL, 1994SECTION VIOLATED: 40 CFR 414 SV

You are put o? notice that your company is in violation of FederalRegulation 40 CFR 414 and Section 313.1 of the PVSC Rules and Regulations. Areview of your MR-I for Apri], 1994 revealed the following mass limitexceedances.

A sample for toluene taken by your company on 04/11/94 resulted in a massloading of 0.30590 grams/day, exceeding the monthly average limit of 0.29615grams/day.

Samples for total cyanide taken by your company on 04/11194 and 04/29/94resulted in mass loadings of 6.57693 grams/day and 0.76476 grams/dayrespectively. A sample for total cyanide taken on 04/27/94 by PVSC resulted in amass loading of 122.36148 grams/day, which exceeded the daily maximum limit of12.69196 grams/day. Additionally, the average of all three samples was 43.23438grams/day, exceeding the monthly average limit of 4.44219 grams/day by morethan 20%.

You should be aware that a monthly average of all samples taken either byyou or PVSC that is 20% or more above the monthly average limitation for ahazardous pollutant makes the violation a serious violation and that two (2) seriousviolations in any six month period would make a company a Significant NonComplier (SNC). In addition, four monthly average violations of any amount inany six month period would also make a company SNC. This would subject yourcompany to mandatory minimum fines under the Clean Water Enforcement A'TIERRA-B-004412(CWEA).

( RE: NOTICE OF VIOLATION - CHEMICAL COMPOUNDSJune 7, 1994Page 2

Based upon the explanation given above, your company has committed aserious violation as defined by the Clean Water Enforcement Act. In view of thet~lct that this matter is in litigation, a copy of this letter is being referred to thePVSC Counsel. Another item we must bring to your attention is that you must listyour permit requirements and sample measurements on the MR-I in five decimalplaces. Since this was not done on the April 1994 report, it appeared that toluenewas in compliance, when in fact it was not. If yOll have any questions, please callAndy Caltagirone a((20 1) 817-5723.

Very tmly yours,

PASSAIC VALLEY SEWERAGE COMMISSIONERS

~-=.:..c-~~---~~~ _

Caroline T. PerrapatoExecutive Director

CTP/mc

cc: Robert Davenport, Deputy Executive DirectorFrank P. D'AscensioCity of NewarkGabriel M. Ambrosio, Esq.

TIERRA-B-004413

'fI

Ir

./, .• 'j" 000046/

DANIEL F. BECHT, ESO.CHAIRMAN

Passaic ValleySewerage Commissioners

ROBeRT J. DAVENPORTEXECUTIVE DIRECTOR

THOMAS J. CIFel.L1VICE CHAIRMAN

ROBERT M. BURKE, JRDOMINIC W. CUCCINEUQRONALD W. GIACONIAJAMES KRONERAYMOND LUCHKOFRANK ORECHIODONALD TUCKERCOMMISSIONERS

600 WILSON AVENUENEWARK, N.J. 07105(201) 344-1800

Fax: (201) 344-2951

PETER G. SHERIDANCHIEF COUNSEL

l.OUlS l..ANZIUOCLERK

October 7) 1994

Mr. Alberto CelleriChemical Compounds29-75 Riverside AvenueNewark, New Jersey 07104

Certified Mailp 252 571 857

Dear Mr. Celleri:

RE: NOTICE OF VIOLATIONPERMIT #: 20407122VIOLATION DATE: AUGUST, 1994SECTION VIOLATED: 40 CFR 414 sv

You are put on notice that your company is in violation of FederalRegulation 40 CFR 414 and Section 313.1 of the PVSC Rules and RegUlations. Areview of your MR-] for August, 1994 revealed the fOllowing mass limitexceedances.

Samples for toluene taken by your company On 08/26194 and 08131194resu Ited in mass loadi ngs of 0 .09816 grams/day, and 2.29704 grams/dayre'pectively. The 08131/94 sample exceeded the daily maximum limit of 0.78267gram'/day. The average of the two samples, I. 19760 grams/day, exceeded themonthly average limit ofO.296J5 grams/day by more than 20%.

Samples for ethylbenzene taken by your company On08/26/94 and 08131194re,u Ited in mass loadings of o.09816 grams/day and 15.07799 grams/dayrespectively. The 08/31194 sample exceeded the daily maximum limit of 4.01912grams/day. Additionally, the average of both samples was 7.57826 gmms/day,exceeding the monthly average limit of 1.50188 gmmS/day by more than 20%.

A sample f9r lead laken by your company on 08/31194 resulled in a massloading of 4.5 I554 grams/day, which exceeded the monthly average limit of3.38452 grams/day by more than 20%.

A sample for zinc taken by your company On08/31/94 resulted in a massloadi ng of 13.

74296 grams/day, which exceeded the monthly average limit of TIERRA-B-00441411.10547 grams/day by 1l1000ethan 20%

RE: NOTICE OF VIOLATION - CHEMICAL COMPOUNDSOctober 7, 1994Page 2

You should be aware that a monthly average of all samples taken either byyou or PVSC that is 20% or more above the monthly average limitation for ahazardous po]]utant makes the violation a serious violation and that two (2) seriousviolations in any six month period would make a company a Significant NonComplier (SNC). In addition, four monthly average violations of any amount inany six month period would also make a company SNC. This would subject yourcompany to mandatory minimum fines under the Clean Water Enforcement Act(CWEA).

Based upon the explanation given above, your company has committed fourserious violations as defined by the Clean Water Enforcement Act. Since zinc andlead are covered in the upcoming Judicial Consent Order your company will enterinto with PVSC, additional penalties will not ensure for these parameters if thismatter is settled. However, since the toluene and ethylbenzene violations are notcovered in the lCO, your company is subject to CWEA fines. The CWEAstipulates a fine of $l ,000 for each parameter seriously violated. You may avoidfurther legal action if you remit $2,000 within 30 days of receipt of this letter.Please make the check payable to PVSC and forward it to the attention of CarmenDellaPia, Operations Coordinator. In view of the fact that this matter is inlitigation, a copy of this letter is being referred to the PVSC Counsel.

In a related matter, we have received your letter dated 09/16/94, wherein yourequested to have your OCPSF mass limits revised. (n support of your request, yousubmitted flow data from 03/94 through 08/94, which show a 51% increase overthe flow data submitted with the 1993 Baseline Monitoring Report, the basis ofyour current mass limits. A PVSC Inspector will visit your facility in the very nearfulure to discuss this matter with you.

As for your other request in the 09/16/94 letter we cannot make anymodified limits, if any are granted, retroactive to August I, and thereby reduce oreliminate the aforementioned violations. This is because any change to your SewerConnection Permit which might be considered would be subject to approval by theCommissioners at their next scheduled meeting, and would not take effect untiITI~F(RA-B-004415timp

October 7, 1994

If you have any questions, please call Andy Caltagirone at (201) 817-5723.

Very truly yours,

PASSAIC VALLEY SEWERAGE COMM:ISSIONERS

l1~d~~Robert J. DavenportExecutive Director

RID/me

cc: Frank P. D'AscensioCannen DellaPiaAndy CaltagironeGabriel M. Ambrosio, Esq.City of Newark

TIERRA-B-004416

- I

Passaic ValleySewerage Commissioners ROBERT J. DAVENPORT

EXECUTIVE DIRECTORD~~L F. BECHT, ESQ.

¢AiAMAN

.'.)

THOMAS J. CIFELLIVICE CHAIRMAN 600 WILSON AVENUE

NEWARK, N.J. 07105(201) 344-1800

Fax: (201) 344-29?1

PETER G. SHERIDANCHIEF COUNSEL

DOMINIC W. CUCCINELLORONALD W. GIACONIAJAMES KRONERAYMOND LUCHKOFRANK ORECHIODONALD TUCKERCOMMISSIONERS

LOUIS LANZILLOCLERK

Februaly9, 1995/

Mr. AlbeI10 CelleriChemical CompolLnds, Inc.29-75 Riverside AvenueNewark, New Jersey 07104

Certified MailP 258 625 759

RE: NOTICE OF VIOLATIONPERIVIIT #: 20407122VIOLATION DATE: DECEMBER, 1994SECTION VIOLATED: 40 CFR 414

SNC-ZINCSNC-TOLUENESNC-ETIlYLllENZEN ESV-CYANIDE

Dear Mr. Celleri:

You are put on notice that your company is in violation of Federal Regulation40 eFR 414 and Section 313.1 of the PYSC Rules and Regulations. A review ofyour MR-I for December, 1994 revealed the following mass limit exceedances:

A sample t()r zinc taken by your company on 12/14/94 resulted in a massloading 01'29.03672 g/day, exceeding the daily maximum limit of27.60502 g/day.Additionally, it exceeded the monthly average limit of 1 1.10547 g/day, by more than20[~·1l.

A sample {()to cyanide taken by your company on 12/14/94 resulted in a massloading of 5.58494 g/day. This exceeded the monthly average limit of 4.44219g/day, by more than 20%.

A sample for toluene taken by your cOIllpany on 12/14/94 resulted in a massloading of 5.747:17 g/day, exceeding the daily maximuIll limit of 0.78267 g1day.Additionally, it exceeded the monthly average limit of 0.2961 5 g/day, by more than:20%.

TIERRA-B-004417

RE: NOTICE OF VIOLATION - CHElVIICAL COlVIPOUNDS, INC.Fdmwry0,1905Page :2

A sample for 2-nitrophenol taken by your company on 12/14/94 resulted in alll:ISS loading of 0.74966 g/day. This exceeded the monthly average limit of0.68748 g/clay.

A sample for ethyl benzene taken by your company on 12114/94 resulted in amass loading of 2.99863 g/day. This exceeded. the monthly average limit of1.50188 g/day, by more than 20%.

YOli should be aware that a monthly average of all samples taken either byyou or PVSC that is 20% or more above the monthly average limitation for ahazardous pollutant makes the violation a seriolls violation and that two (2) seriousvioh!tiolls in any six month period would make a company a Significant NonComplier (SNC). In addition, four monthly average violations of any amount in anysix month period would also make a company SNC. This would subject yourcompany to mandatory minimum fines under the Clean Water Enforcement Act(CWEA). Based upon the explanation given above, your company has committedits third seriolls violation for zinc in a six month period (following those in Augustand November), as a defIned by the Clean Water Enforcement Act, making yourcompany SNC for this parameter. Chemical Compounds is also SNC for tolueneand ethylbenzene. There was also a serious violation for cyanide.

Tilis will also confIrm that Chemical Compounds is operating pursuant to theterms and conditions of a .!udicial Consent Order. The compliance date for lead,zinc and cyanide is IlO later than 04/01/95. Accordingly, so long as you adhere tothe cOlllpliilJ1Ce schedule and other conditions set forth in the .JCO, ChemicalClllllpounds will not be subject to additional enforcement action or civil penaltiesfor having violated the lead, zinc, and cyanide limitations of its pennit. Tolueneand ethyl benzene are not included in the lCO and are subject to additionalerll()J"cemcnt action. III view of these violations a copy of this letter is being/()rw<lrded to the PVSC attorney.

TIERRA-B-004418

HE: NOTICE OF VIOLATION - CHEIVIICAL COJ\-IPOUNDS, INC.February 9, 1995Page 3

if yUll have allY questions please call Andy Caltagirone at (20 I) 817-5723.

Very truly yours,


/"".- ..? -:. .--J10 ..·~--lj. .1'.,/ .......;

/' f5/;:I'I1 ;-'•.: ')'/'~'-'~'it)/-(-,;;y' t-~~~., I.. <. ._. ( //

.. !/Robert J, DavenportExecutive Director

RJD/mc

cc: Frank P. D'AscellsioGabriel M. Ambrosio, Esq.City of NewarkCarmen DeilaPia

TIERRA-B-004419

Form OWM.oSl" 1/B6

NEWJf:RS'r:.y DEPARTMENT or ENVIRONMENTAL PROTE2tr6NDIVISION OF WASTE MANAGEMENT

Page~~

CASE #:

INVESTIGATION

.,DWM FILE #: 02-/~-S-1 ~

.L TIME ARRIVED: ...-

DATE: 2/t!(fZ- TIME DEPARTED: -"

PROPERTY OWNER: eLect·?/ COJtk,#aLftrd.LMAILlNGADDRESS: ;:l..C(.?S- 8(i;... ...,..~.·deA..~

....,<%.". 'd<jc Ca. ,,4/, iT. 0 ,?, ()LfBLOCK: 6' /'1.. LOT: ~6LOCATION TELEPHONE #; tI?S:-3~'S-EPA ID #: _

RESPONSIBLE PARTY ~~~~ _

ADDRESS:

COPIES:. Whirt • D WM Fj{t Ye//ow. Locill Htillrh D,pI.

TIERRA-B-004420

For'm DWM<l51 A1/86

~;:'''-' \...../

NEW JERSEY DEPARTMENT OF ENVIRONMENTAL PROTECTIONDIVISION OF WASTE MANAGEMENT Page .-3:.. of z.:.

.1.'''-~.."'--.:.;r'~"

. .=....... :-'

INVESTIGA nON

CASE #

,'.

FINDINGS A."'IDSUMMARY:I

:..~,COP!ESJ~'" White· D WM File reI/ow· Local Health Dept. Pink ./nvtft;'l1tor

TIERRA-B-004421

Form OWM·051 C1/86

SKETCH

t

.NEW f-SEY DEPARTMENT OF ENY1RONMENTAL PRonb-rbN

DIVISION Of WASTE MANAGEMENT

INVESTIGATION

.....

-I

/_/

C' ~"...,,·,-,&~I

Co..",/CVYld. s

Oil

CASE # 1;2 -0 I-CJ7-10 ;LS-

]/1/11 ~DATE __ --.L_~=__~ _

0-- - - - - ."-;'.

SCALE: R.< !d >ci.r./""Include directional arrow.

'.

Supervisor Signarure Investigator SigNtturt

COPIES:'.-~"" .. -

Whitt· DWM Filt Ytllow • Local Htalth /Apt. Pink .Invtstigator

TIERRA-B-004422

TIERRA-B-004423


29-75 Riverside Avenue. Newark, New Jersey 07104(201) 485-3211-2 • Fax: (201) 485-4870

Emergency and Remedial Response DivisionU.S. EnvironmentaJProtection Agency290 Broadway, 17th FloorOffice ofR.egional CounselNew Yor~ New York 10007-1866

August 8, 1996

To Ms. Amelia Wagner,

Please find enclosed the following responses to the "Request fin Information"received on July 10, 1996 at Chemical Compounds Inc.. If you should have anyfurther questions or require additional information, please feel free to contact JimGiannotti at (201) 485 - 32)2.

Jim Giannotttijg.lJGC.c: AC/SG

RErr.:1\ICn.lUG 0 9 199G· .-

845340002

TIERRA-B-004424

__~ ATTACHMENT AREQUEST FOR INFORMATION

BackgroundThe united states Environmental Protection Agency (IIEPA")isinvestigating the release of hazardous substances into thePassaic River. EPA has information indicating that hazardoussubstances from your facility located at 29-75 Riverside Avenuein Newark, New Jersey may have been discharged into the PassaicRiver.Please provide the information requested beloW, including copiesof all available documentation that supports your answers.1) How long has your company operated at the facilitydesignated above? If your company no longer operates at thisfacility, during what years did your company operate at thefacility?2) a) Does your company have or has it in the past had a permitor permits issued pursuant to the Resource Conservation andRecovery Act, 42 V.S.C. §6901 ~ ~.? If 'tyes", please providethe years that your company held such a permit and its EPAIdentification Number.

~ b) Does your company have or has it in the past had a permitor permits issued pursuant to the Federal water Pollution ControlAct, 33 U.S.C. § 1251, sU. ~.? If lIyes'l, please provide theyears that your company held such a permit.3) Did your company receive, utilize, manufacture, discharge,release, store or dispose of any materials containing thefollowing substances: Yes No2,3,7,8 tetrachlorodibenzo-p-dioxin

or other dioxin compoundsAcetic acidAdipic acidAmmoniaAnilineBenzeneBenzo(a) anthraceneBenzoic acidBenzyl chlorideButyl benzyl phthalateChlorobenzeneChloroethyleneChloroforml,2-dichloroetheneoi-n-butyl phthalateEthyl benzene

1

845340003

TIERRA-B-004425

-- Yes NoFluorantheneMethanolMethylene Chloride2-methylnapthaleneNaptha distillateNapthalene2-nitrophenolPetroleum etherPhenanthrenePyreneTetrachlorobenzeneTetrachloroethaneTetrachloroethyleneTrichloroethaneTrichloroethyleneToluenexyleneArsenicCadmiumchromiumCopperLeadMercuryNickelSilverZinccyanidePCBs

4) a) Provide a description of the manufacturing processesfor which all hazardous substances, including, but not limitedto, the substances listed in response to item (3), were a productor by-product.

b) During what parts of the manufacturing processesidentified in the response to items (4)(a), above, were hazardoussubstances, including, but not limited to, the substances listedin response to item (3), generated?

i) Describe the chemical composition of thesehazardous substances.ii) For each process, what amount of hazardoussubstances was generated per volume of finishedproduct?

-iii) Were these hazardous substances combined withwastes from other processes? If so, wastes from whatprocesses?

2

845340004

TIERRA-B-004426

- 5) Describe the methods of collection, storage, treatment, anddisposal of all hazardous substances, including, but not limitedto, the substances listed in response to item (3) and (4).Include information on the following:


b) If hazardous substances were taken off-site by a hauleror transporter, provide the names and addresses of the wastehaulers and the disposal site locations.

c) Describe Qll storage practices employed by yourcompany with respect to all hazardous substances from the timeoperations commenced until the present. Include all on-site andoff-site storage activities.


stored outside, were the drums storedstored on areas that had been pavedPlease provide a complete description

ii) When drums were stored outside, were empty drumssegregated from full drums?

d) What processes do you use to treat your waste? What doyou do with the waste after it is treated?6) a) For process waste waters generated at the facilitywhich contained any hazardous substances, including, but notlimited to, the substances listed in response to item (3) and(4) :

i) Was the waste stream discharged into a sanitarysewer and if so, during what years?ii) Were they treated before being discharged to thesanitary sewer and if so, how? Please be specific.iii) If the waste waters were not discharged to thesanitary sewer, where were they disposed and duringwhat years?iv) Please provide the results of any analysesperformed on any waste process streams generated at thefacility.


,-3

845340005

TIERRA-B-004427

- i) Did the drains connect to a sanitary sewer and ifso, during what years?ii) If the floor drains or other disposal drains atthe facility were not discharged to the sanitary sewer,where did they discharge and during what years?

c) i) Did any storm sewers, catch basins or lagoons existat any time at the facility and if so, during whatyears?ii) If catch basins or lagoons existed, were theylined or un-lined?iii) What was stored in the lagoons?iv) Where was the discharge from any of thesestructures released and during what years? Was thisdischarge treated before its release and if so, how andduring what years? What was the chemical compositionof any waste waters released, and during which years?

d) Please supply diagrams of any waste water collection,transport or disposal systems on the property.

e) Also, EPA has information relating to several instances~ of discharge of process waste water into the sewer system in 1992

and 1995. Please provide a detailed description of theseincidents.7) a) For each hazardous sUbstance, including, but notlimited to, the substances listed in response to item (3) oridentified in the responses to item (4), above, provide the totalamount generated during the operation of the facility on anannual basis.

b) Were any hazardous substances, including, but notlimited to, the substances listed in response to item (3) oridentified in the responses to item (4), above, disposed of inthe Passaic River or discharged to the Passaic River? If yes,identify the hazardous substances, estimate the amount ofmaterial discharged to or disposed of in the Passaic River andthe frequency with which this discharge or disposal occurred.Also please include any sampling of the river which you mighthave done after any discharge or disposal.8) Please identify any leaks, spills, explosions, fires orother incidents of accidental material discharge that occurred atthe facility during which or as a result of which any hazardoussUbstances, including, but not limited to, the substances listedin response to item (3) or (4), were released on the property,into the waste water or storm drainage system at the facility or-

4

845340006

TIERRA-B-004428

- to the Passaic River. Provide any documents or informationrelating to these incidents, including the ultimate disposal ofany contaminated materials.

a) Please provide the results of any sampling of the soil,water, air or other media after any such incident and before andafter clean-up. Please provide in this information all samplingperformed for or by NJOEP.

b) Also, EPA has information that due to an industrial sewerline break in 1992, an unreported quantity of aniline wasdischarged to the Passaic River. Please provide all informationrelating to this and any other discharges and any measures takento mitigate the impact of the discharges.9) a) Was your facility ever subject to flooding. If so, wasthe flooding due to:

b)event.

i) overflow from sanitary or storm sewer back-Up,and/orii) flood overflow from the Passaic River?Please provide the date and duration of each flood

10) Please provide a detailed description of any civil,criminal or administrative proceedings against your company forviolations of any local, state or federal laws or regulationsrelating to water pollution or hazardous waste generation,storage, transport or disposal. Provide copies of all pleadingsand depositions or other testimony given in these proceedings.

a) EPA has information that your facility has receivedseveral notices of violation for discharges of waste water intothe sewer system, inclUding a NJDEPE Field Notice of Violationissued on January 7, 1992 and a PVSC Notice of Violation issuedon February 9, 1995. Please provide information on how theseviolations were resolved.

-

II} Provide a copy of each document which relates to thegeneration, purchase, use, handling, hauling, and/or disposal ofall hazardous substances, including, but not limited to, thesubstances listed in response to item (3) or (4). If you areunable to provide a copy of any document, then identify thedocument by describing the nature of the document (e.g. letter,file memo, invoice, inventory form, billing record, hazardouswaste manifest, etc.). Describe the relevant informationcontained therein. Identify by name and job title the person whoprepared the document. If the document is not readilyavailable, state where it is stored, maintained, or why it isunavailable.

5

845340007

TIERRA-B-004429

12) a) Did you or anyone else sample the soil, ground water,surface water, ambient air or other environmental media at thefacility for purposes other than those identified in questionsabove?

b) If so, please provide all other documents pertaining tothe results of these analyses.13) a) Has your company owned the facility at the locationdesignated above? If so, from whom did your company purchase theproperty and in what year? If your company subsequently sold theproperty, to whom did your company sell it and in what year?Please provide copies of any deeds and documents of sale.


c) To the extent that you know, please provide the names ofall parties who owned or operated the facility during the periodfrom 1940 through the present. Describe the relationship, ifany, of each of those parties with your company.14) Answer the following questions regarding your business orcompany. In identifying a company that no longer exists, provideall the information requested, except for the agent for service

~ of process. If your company did business under more than onename, list each name.

a) state the legal name of your company.b) state the name and address of the president or the

chairman of the board, or other presiding officers ofyour company.

c) Identify the state of incorporation of your company andyour company's agent for service of process in thestate of incorporation and in New Jersey.

d) Provide a copy of your company's "certificate ofIncorporationll and any amendments thereto.

e) If your company is a subsidiary or affiliate of anothercompany, or has subsidiaries, or is a successor toanother company, identify these related companies. Foreach related company, describe the relationship to yourcompany; indicate the date and manner in which eachrelationship was established.

f) Identify any predecessor organization and the datesthat such company became part of your company.-

6

845340008

TIERRA-B-004430

g) Identify any other companies which were acquired byyour company or merged with your company.

h) Identify the date of incorporation, state ofincorporation, agents for service of process in thestate of incorporation and New Jersey, and nature ofbusiness activity, for each company identified in theresponses to items (14)(e), (f), and (g), above.


15) Provide the name, address, telephone number, title andoccupation of the person(s) answering this "Request forInformation" and state whether such person(s) has personalknowledge of the responses. In addition, identify each personwho assisted in any way in responding to the "Request forInformation" and specify the question to which each personassisted in responding. Please include the names and addressesof former employees who were contacted to respond to any of thequestions.

- 7

845340009

TIERRA-B-004431

-

ATTACHMENT BINSTRUCTIONS FOR RESPONDING TO REQUEST FOR INFORMATION

1. A complete separate response must be made to each individualquestion in this "Request for Information".2. Precede each answer with the number of the question to whichit is addressed.J. In preparing your response to each question, consult withall current or former employees and agents of your company whomay be familiar with the matter to which the question pertains.4. Interpret "and" as well as "or" to include within the scopeof the question as much information as possible. If twointerpretations of a question are possible, use the one thatprovides more information.5. If you are unable to give a detailed and complete answer orto provide any of the information or documents requested,indicate the reasons for your inability to do so.6. If you have reason to believe that an individual other thanone employed by your company may be able to provide additionaldetails or documentation in response to any question, state thatperson's name, last known address, phone number and the reasonsfor your belief.7. For each document produced in response to this "Request forInformation", indicate on the document, or in some otherreasonable manner, the number of the question to which itapplies.8. If anything is deleted from a document produced in responseto this "Request for Information", state the reason for, and thesubject matter of, the deletion.9. Provide all documents that relate to each question. If adocument is requested but is not available, state the reason forits unavailability. In addition, to the best of your ability,identify any such document by author, date, sUbject matter,number of pages, and all recipients and their addresses.10. As used herein "relate to" or "relating to" means constit-uting, defining, containing, embodying, reflecting, identifying,stating, referring to, dealing with, or in any way pertaining to."Document" as used herein means any recording of information intangible form, inclUding memoranda, handwritten notes, invoices,checks, manifests, tape recordings, computer databases, or anytangible or physical objects however produced or reproduced uponwhich words or other information "are affixed or recorded or from

1

845340010

TIERRA-B-004432

-

-

which by appropriate transcription written matter or a tangiblething may be produced."11. Whenever in this l1Request for Information" there is arequest to identify a person or an entity other than a person,state the person or entity's full name, last known employment,present or last known home address, and telephone number.12. As used herein, the term "facility,1I "hazardous substance,1IIIperson,lIand IIrelease" shall have the meaning set forth insection 101(9), (14), (21) and (22) of CERCLA, 42 U.S.C.§9601(9), (14), (21), and (22), respectively.13. In answering these questions, every source of information towhich you have access should be consulted, regardless of whetherthe source is in your immediate possession or control. Alldocuments or other information, including records of all types ofmanUfacturing, treatment, transportation or disposal operations,in your possession or in the possession of the corporation shouldbe consulted. If you do not have access to certain informationand/or documents, state the nature of this information and/ordocuments, and indicate in whose possession they can be found.

.-2

845340011

TIERRA-B-004433

****RESPONS TO QUESTIONS 4A IS REDACTED****

-

,-..

845340012

TIERRA-B-004434

- Hi) The hazardous substances located in. the waste water stream are generated onbatch scale operations. The by-products are present in the waste water streamafter the separation of the product by filtration. After filtration, the waste waterstream is treated for regulated efJ]uent exceedances. After treatment, the wastewater is stored in a 10,000 gallon tank. A number of process waste water streamswill combine in the 10,000 gallon storage tank.

5 (a) The following table is a list ofempJoyees at eel who were or are responsible fortb.emanagement of hazardous substances:

-

.~ :·•.i··::~~.P.99P:9f.·&p9J1~~i~···:·····~·"'''C.:

Alberto Celleri Co-President Overall Operations

HarOld Sullivan Co-President Overall Operations•

Arturo Cel1eri Chemical/Bnvironmental Waste Water TreatmenllHazardousEngineer Substance Storage

Jim Giannotti Chemical/Environmental Waste Water Treatment/HazardousEngineer Substance Storage

845340013

TIERRA-B-004435

-

.-

-

5 (b) The following table is a Jist of transporters who were responsible for oJi.sitedisposal; including non-hazardous waste water:

:j··.;:lii~P911~jil~.I:'.1·;.·;:; ii;:;;DI~I_e!l·i:id~"··..~.'

v.-.

Franks Vacuum Truck Services. 4500 Royal Ave. Research Oil Co.Inc. Niagra Falls, NY 14303 2655 Transport Rd.

NYD982192814 Cleveland, OH 4415OHD004118612

Freehold Cartage Inc. P.O. Box SOlO Systecb EnvironmentalN1D054126164 Freehold, NJ 01728 11397 County Rood 176

. Paulding, OH 45819OHDOO5048941

Laidlaw Environmental Setvices 3521 Whisky Bottom Road Laidlaw Environmental ServicesMDD980554653 Laurel, MD 20424 3527 Whisky Bottom Road

Laurel, MD 20424

Maumee express P.O. Box 278 Rineco Chemical Ind.NJD986607380 Somerville. NJ 08876 1007 ,Vulcan Rd. - Haskell

Benton, AR 72015ARD981OS7870

Oldover Corporation P.O. Box 68 Oldover CorporationVAD098443443 Ri. I, StateRd 652 P.O. Box 68

Arvonia. VA 23004 Rt. I, StateRd 652Arvonia, VA 23004

Freehold Cartage Inc. P.O. Box: 5010 ECOFLON1D054126164 Freehold, NJ 07728 2750 Patterson Street

Greensboro. Maryland 27407NCD980842132

Chemical Waste Management of 100 Lister Avenue Chemical Waste Management ofNJ Newark:.,NJ 07105 NJ

NJOO892 16790 JOO Lister AvenueNewark, NJ 071 05

Tri-State Motor Transit Co. P.O. 113 Rineco Chemical Ind.MOD095038998 Joplin, MO 64802 1007 Vulcan Rd. - Haskell

Benton, AR 72015ARD9111057810

845340014

TIERRA-B-004436

-

-.

-

.\

5 (c) i)& ii) The fol1owing table is a list of storage practices for the hazardoussubstances included in items (3) & (4) since the bestinninR of oPerations:

!l;;:I[~••• !::I·I;' .:!·~il·;~ll·\·I;II!il~jl!:I~JJ.~'.~:'~ji!j:;·Irii!:..i~~i!i:..';,Acetic Acid 55 gallon Plastic Drum

<4 L Glass BoUle- Laboratory Scale5,000 gallon Tanker Truck - Waste

Adipic Acid 50 lb. Bag/l I 2000 lb. Palates< 1 lb. Glass Battle- Laboratory Scale

Ammonia 150 lb. Cylinder

Raw Materials Benzoic Acid 50 lb. Bags I 2000 lb. Palates- < 1 lb. Glass Bottle - Laboratory Scale

ChlorofolUl < 4 L. Glass Bottle .Laboratory Scale2 gal. Solvent Lab Disposal Container- 55 gallon slsdrum - Wasteor 5,000 gallon Tanker Truck .Waste

4,000 gallon SIS Storage Tank .Waste

Methanol 55 gallon Stain lea Steel Drum

Laboratory 250 gallon Plastic Totes

SUl?pli~4,000 gallon S/S Storage Tank - Waste

5,000 gallon Tanker Truck. - Waste< 4 L. Glliss Jars - Laboratory Scale

2 gal. Solvent Lab Disposal Container55 gallon sir.drum - Wasre

Methylene Chloride 55 gallon Stainless Steel Drum4,000 gallon S/S Storage Tank - Waste

5,000 galloo Tanker Truck.- Waste< 4 L. Glass Jars - Laboratory Scale

2 gal. Solvent Lab Disposal ContainerS5 gallon siB drum - Waste

Toluene 55 gallon Stainless Steel Drum4,000 gallon S/S Storage Tank - Waste

5,000 gallon Tanker Truck. - Waste< 4 L. Glass Jars .Laboratory Scale

2ga1. Solvent Lab Disposal Container5S ga1lon siB drum - Waste

Xylene 55 gallon SlS Drum250 gallon P1asticToteI

4,000 gallon S1S Storage Tank - Waste5,000 gallon Tanker Truck- Waste

<4 L. Glass Bottles - Laboratory Scale2 gal. Solvent Lab Disposal Container

55gnIlonsis drum .WasteBy-l'rochU fOl&ld in lho WIIIto 55 gallon drum- Waste--Waste Water ADiliac. Daualo,

400 4,000 gallon SIS Storage TankStorage llamIicAad, UlIcJrollal2alc, .

Q>lmdann,llIhyllltrl2llM,(ppb Coooeotratioos) ~.l4dhy1aloa.kridl> 10,000 gallon SlS Storage TankBased on Analytical ~2-NiCroA1a1"

Data T~cnc,T~Xy....... I..-I, ZDc, ~ 5,000 gallon Tanker Trucks - Waste

845340015

TIERRA-B-004437

-

--

The 55 gallon dnuns or 250 gallon Plastic totes containing hazardous substances listedin items (3) & (4) are stored on wooden palates outside on either a paved area withasphalt or a concrete pad. (See Attachrnmt 5 for a facility layout for the storage areas ofhazardous substances.)

In December 1993, a concrete diked area was constructed outside the bwlding locatedon the southeast part of the building with a capacity of25,Ooo gallons. The diked area iswithin an 18 inch thick concrete berm approximately 4 feet high. Inside is the waste waterstorage area with (2) 4,000 gallon Above Ground SIS Storage tanks and (1) 10,000 gallonAbove Ground SlS Storage Tank on top of an 8 inch concrete slab. In the past, the wastewater and or flammable soNents such as methanol. xylene, & toluene were stored in a5,000 gaJIon Tanker Truck in that same area. In addition, waste flammable liquids werestored in.a 4,000 gallon Above Ground SIS Storage Tank in the diked area. SinceSeptember 1995, waste flammable liquids have been recycled. Currently, the 4,000 gallonS/S Storage Tank is being utilized for waste water storage.

•Empty dnuns are segregated from full drums. The empty drums are located at the

most southeastern part of the property, alljacent to or in an enclosed shed.

5 (d) The waste water streams are treated by neutraJ~tion, chemical precipitation, orcarbon filtration. The process waste water streams are transferred to one of(2) 1,500gaDon mixing tanks for the introduction of treatment. One treatment involvesneutralization by the addition of Sodium HYdroxide or Sulfuric Acid to meet dischargeregulations. Another treatment involves carbon filtration for the removal of organics. Thedrain. water is collected in an Above Ground S/S Storage Tank located in the basementand treated for heavy metals. The treatment for the drain water involves chemicalprecipitation with the addition oflime followed by filtration. After treatment, the wastewater is transferred to a storage tank and analyzed.

If the treatments are effective, the waste water is transferred to a 10,000 gaDon AboveGround S1S Storage tank. After the tank is full the waste water is combined with thesanitary waste water from the facility and pumped out of the bwlding into the PVSCsanitary sewer which flows approximately 70 yards to an interceptor of the industrial park.The solid waste generated from treatment is non-haLUdous and disposed off-site to aregulated facility. Carbon fihration and chemical precipitation treatment methods haveonly been used since October, 1995. Prior to that time, the waste water was treated byneutralization.

845340016

TIERRA-B-004438

6 (a) i) From July 1992 to the present, the process waste water stream was dischargedinto a sanitary sewer connected with Passaic Valley Sewerage Commissioners.Before July, 1992, the process waste water stream. was connected to a 5,000gaDon tanker truck for off,.site disposal.


• iii) Before cel obtained a pennit for discharge to the sewer, the waste waterstream was conected in a 5,000 gaDon tanker truck.. When the tanker truckaooieved maximum capacity, the water would be sent to a TSD faCility fortreatment. cel obtained a pennit for discharging process waste water to thesewer on July 20, ] 992. (See Attachment 11, for manifests.)


6 (b) i) & ii) From 1986· February, 1992, the main manufacturing floor at the facilitywas equipped with internal floor drains which were directly connected to thesanitary sewer. FromFebroary, 1992 through July, 1992, the drain water wascollected into an above grOWl.d storage tank located on the basement floor and sentdirectly to a 5,000 gaDon tanker truck.. When the tanker truck became full, it wassent for ofl:site disposal From July, 1992 - April, 1993, the drain water was sentto the 5,000 gallon Tanker Truck, then was combined with process waste waterand then transferred to an above ground storage tank in the basement. Aftersampling and analysis for effluent exceedances, the waste water was combined inthe basement with the sanitary waste water from the facility and pumped out of thebuilding into the sanitary sewer. In Apnl, 1993 eCI replaced the :5,000 gaDonTanker Truck with a 10,000 gallon above ground S1S Storage tank.

From 1995 to the present, the drain water has been transferred to an above groundSIS storage tank for the treatment of heavy metals by chemical precipitation. Aftertreatment., the drain water is transferred to another above ground storage tank foranalysis. Ifthe treatment has been successfu]. the drain water is sent directly tothe 10.000 gallon Storage Tank, and mixed with the process waste water. Afterthe tank has accumulated to its maximum capacity. the waste water is combinedwith the sanitary waste water from the flCllity and pumped out of the bmlding intothe sanitary sewer which flows approximately 70 yards to an interceptor of theindustrial park.

-845340017

TIERRA-B-004439

-6 (c) i) There have been DO storm sewers, cateb basins, OT lagoons located at BUIlding #

17,29-75 Riverside Ave., Newark, N.J. since the beginning of operations orCCL

ii) N/A

iii) N/A

iv) N/A

,6 (d) The facility layout for the collection, storage, and disposal of waste water can belocated in Attachment 6.

6 (e) On January 6, 1992 the Newark Fire Department and the New Jersey DEPresponded to a complaint of a discharge at the CCI facility. CCl's ne~door neighbor hadplugged up the sewer line, and when ccrs personnel excavated the line to attempt toclear it, the contents of the line, including water colored purple with Red # 3 and Blue # 2dye was disbursed into the excavation. This water was pumped out of the excavation ontothe ground where it was observed by the Fire Department and DEP. (See Attachment 7)CCI was ordered to clean up the discharge, which was analyzed and shown to be nonw

hazardous. (See analysis of soil and liquid samples - Attachment 8). CCI was chargedwith discharging to the PVSC sewer without a permit.

Subsequently, after cel obtained a PVSC permit, it was cited by pvsc for havingdischarged waste water to the sewer which contained some volatile compounds and metalsin excess of permitted concentrations. These discharges exceedances have been resolved,and current treatment methods appear to be keeping wastewater discharges withinpermitted parameters.

7 (a) The total amount of hazardous substances generated during the operation of thefacility on an annual basis can not be determined. The hazardous substances which arecontained in the waste water stream are determined by tb.e purity of the raw materials. Asa result, contaminant concentrations differ from one manufactwing batch to another.

7 (b) Chemical Compounds Inc. has not disc1ulIged any hazardous materials into thePassaic River.

8 (a) There have been no leaks, spills, explosive fires or other incidents that occurred at- the eCI facility that resulted inhazardous substances being released.

845340018

TIERRA-B-004440

'.," '.,:"

-

.. ~,-. ~.'. ..;.- " ,..-" - ... "

8 (b) eCI did not discharge any hazardous material into the Passaic River. (See answer to6( e) for description of incident. )

9 (a) Yes. ecrs faCIlity is subject to flooding due to the close proximity of the PassaicRiver. Flooding does occur due to the overflowing of the Passaic River. As a result, thewater gen.erated due to the flooding of the Passaic River is analyzed, treated and stored atour facility before discharging to the sewer.

9 (b) Flooding occurs during very bad storms., the dates of each occurrence are notknown.

10 (a) In 1992, due to the discharge descn'bed in 6(e), eCI paid administrative costs to theNew Jersey {)q>artment of Environmental Protection for the discharge response. TheNJOEPE Case # is 92-01-07-1025. In addition, CCI was charged with. violating theWater PoDution Control Act for negligently discharging a poUutant into a municipaltreatment works without possessing a valid industrial pretreatment pennit issued by thePassaic Valley Sewerage Commission. cel pled gw1ty to a fourth degree water poUutionviolation with a fine of $5,000 for the offense and had to provide a check in the amount of$1,760.85 payable to the Office of the State Environmental Prosecutor to be used topurchase a one page advertisement in the Gloucester Times conveying a positiveenvironmental message.

CCI also paid for administrative costs when the Bureau of Emergency Responseresponded to a chemical fire at the facility on October 5, 1993. The case was closed. TheNJDEPE Case #'8 are 93-10-05-0736 & 93-10-05-1110.

On September 14, 1994, eCI had received a Notice of Violation from the Division ofFacility Wide Enforcement- NJDEP. The inspection identified a violation of the SolidWaste Management Act (N.J.S.A 13: IE-I et seq.) and Regulations (N.J.AC. 7:26-1 etseq.) promulgated thereunder. Remedial actions to correct the violations wereimplemented by eel within daysand no further enforcement was required thereafter.

With regard to violations of discharge permit limitations. eel resolved the matter byentering into a Consent Order and Final Judgement with the Passaic Valley SewageCommissioner on November 24, 1994, by which it paid $6,000 to PVSC and entered intoa compliance schedule, which was subsequently extended to July I, 1996. (See ConsentOrder and Final Judgement and other relevant documents - Attachment 9 & 10.)

845340019

TIERRA-B-004441

-

I]) For the purchasing of listed haL'U"dous substances. such as raw materials, in item (3)or (4), tbe following table indicates ccrs suppliers since the beginning of operations.Documents such as invoices, bitt of ladings, and a purchase order book for receiving thesehazardous substances are avatlable.

Brown Chemical

AA:eticAcid

Textile C.hemical

Duso Chemical


173 Smith StreetPoughkeepsie, N.Y. 12602

Brown Chemical

Adipic AcidTextile Chemical


990 Jersey AveNewBnmswick. N.J. 08901

Ammonia Jones Chemical

Textile Chemical

Benzoic AcidJLM Industries

80 Munson StreetLeRoy, N.Y. 14482

990 Jersey Ave.New Brunswick, N.J. 08901

8675 Hidden River ParkwayTampa, IlL 33637

Brown ChemicalMethanol

Textile Chemical


990 Jersey AveNew Brunswick. N.J. 0&901

Brown ChemicaJ.Methylene Chloride

Textile Chemical



Brown Chemical

TolueneTextile Chemical


990 Jersey AveNew Brunswick, N.J. 08901

Xylene 990 Jersey AveNew Bl1U1BWick,N.J. 08901

845340020

TIERRA-B-004442

For laboratory supplies, the following table provides information regarding suppliers:

Ac:etieA.c:idAdipicAeid

BeDZOicAcidChloroform

Methylene ChlorideMethanolTolueneXylene

89 Nev.buy StreetSuite 103

Danvers. MA 01923

·1:li~lljl'·t;!!iT.~.'!li~f~:IIIIII~.!~illl!~I:I'I:~::r'I\III'ltJi!:::i,jt\ti;PCI Scientific Supply.1.De. 41 Plymouth Street

Fairfield, N.J. 07004

J.T. Baker

Fisher Scientific 711 Forbes AvenuePittsburgh. PA 15219-4785

For the hauling and disposal ornsted substances, such as waste water. plant andlaboratory solvents, in items (3) or (4). the foJlowing table indicates CCl's past and presenttransporters and disposal facilities. Documents, such as manifests, for tlte disposal of thesehazardous substances are inAttachment ] 1.

.-

;;;,}#:~~r4~·~.~';;U!::;H:/~·'M'1I~;~f!~~:ti~·fM":::"':!@i @~i:;Hft;:lmgXg:~~\W·:;:I'.I·'it;·.:f::.::}Methanol, Xylene Freehold Cartage Inc. ECOFLO

Waste Flammable Liquids 2700 Patterson StGreensboro. NC 27407

Dye Waste Water Chemical Waste Management Chemical Waste ManagementNon-Hazardous 100 Lister Ave.

Newark. NJ 07105Methanol, Xylene Oldover Corporation OIdover Corporation

Waste Flammable Liquids Route 1. State Road 65]Arvonia.. VA 23004

Chloroform., Methylene Chloride, Tri-State Motor Transit Co. RinecoXylene .1007 Vulcan Rd - Haskell

LaboratOI}' Solvents Benton. AR 72015Waste Flammable Liquids

Dye Waste Warer Laidlaw Environmental Services Laidlaw Environmental ServicesNon-Hazardous 3527 Whiskey Bottom Rd

Laurel. MD 20724

Dye Waste WaIN Maumee Bxpress RinecoNon-Hazardous 1007 Vulcan Rd - Haskell

Benton, AR 72015

WarteI>ye Franks Vacuum Truck:Service Research Oil Company(HeYellow # 2) Inc. 2655 Transport Rtf.

Cleveland, OH 4415

Methanol. Xylene Freehold Cartage Inc. Systech EnvironmentalWaste Flammable Liquids 11397 County Rd 176

Paulding. OH45879

845340021

TIERRA-B-004443

.-

12 a) & b) There bas been no sampling of the soil, ground water, or surface water at thefacility for purposes other than. those identified in the responses above. However, anOccupational Health Survey was conducted by CCl's m.surance company to evaluateemployee exposure to pOSSlole various airborne contaminates. The survey included airsampling for xylene, methanol and others. As a result, none of the employees' exposuresexceeded the OSHA PenniSSlble Exposure Levels for the above contaminates.Attachment 12 contains the report provided by CCfs insurance company.

13 a) Yes, CCI has owned the facility at 29-75 Riverside Ave. - Building # 17 since July1, 1986. Attachment I contains a copy of the deed of sale. The property was purchasedfrom Industrial Development Associates, Inc ..

13 b) N/A

13 c) In 188S"the Freeholders of Essex County sold the property to Triton Boat Club ofNewark. This transaction is recorded inEssex County Deed Book K-24, Page 133. OnMay 16, 1902, Patton Paint Company acquired the property from the Triton Boat Club ofNewark, as recorded in Deed Book. 1-35, Page 270. Patton Paint Company was amanufacturer of paint and varnishes.

Thereafter, Pittsburgh Plate Glass Co. which manufactured paint and varnishes, tookthe subject property. The property was identified as Block 614, Lot 1. The currentfaCility - Building # 17 - was constructed by the Pittsburgh Plate Glass Co. as a chemicalresin manufacturing facility for its operation. PPG, Inc. which was formerly calledPittsburgbPlate Glass Co. purchased the property on January 31, 1941, and held theproperty to August 2, 1971.

In 1971, the site was sold to 11 developer, Riverside Ave. Properties, Ine .. Deed Book4382, Page 1023. Riverside Ave. Properties, Inc. thereafter leased the site. On. October11, 1979, the property was sold to another developer, Industrial DevelopmentCorporation, which sold the property a month later to lndustrial Development Associates.The principal of Industrial Development Associates is Anthony V. Pugliese, lll. IndustrialDevelopment Associates leased the bwlding to S.B.S. Chemicals, Inc. and Desachem Co.,Inc, manufacturers of chemicals and detergents. S.B.S. Chemicals and Desachem Co., Incoccupied Building # 17 pursuant to a lease agreement with Industrial DevelopmentAssociates, which argument expired on August 14, 1985. Thereafter, the building wasvacant and the lot and block numbers were changed and subdivided from Block 614, Lot 1(partial) to Block 6] 4, Lot 66. CCI has no relationship with the past owners or tenants.

845340022

TIERRA-B-004444

---

_.

14 (a) The legal name of the company is Chemical CompOlmds Inc ..

14 (b) 'The president of the company is Mr. Alberto Celleri. Mr. CeDeri's address is 10Baldwin Court, Roseland, NJ 07068.


14 (d) Attachment 13 contains a copy of the company's "Certificate oflncorporation"and amendments thereto.

14 (e) CCI is not a subsidiary or affiliate of another company.

14 (f) Chemical Compounds Inc. has no predecessor organization.

14 (g) Chemical Compounds Inc. has not acquired nor merged with any other company.

14 (h) N/A

14 (i) There are no previous owners orCCI.

15. The person answering this Request for Infonnation is Alberto Celleri, President ofCCI, 10 Baldwin Court, Roseland, New Jersey 07068 (201) 364-0370. Mr. Celleri baspersonal knowledge of the responses. Mr. Jim Giannotti, 72 Califon Drive, Colonia, NJ07067, (908) 382-5591, a Chemical Engineer at Cel, assisted with the preparation ofthese responses.

845340023

TIERRA-B-004445

--

CERTIFICATION OF ANSWERS TO REQUEST FOR INFORMATION

state of New Jersey

County of ....E....s'-"lsu;:e""x'-- _

I certify under penalty of law that I have personally examined'and am familiar with the information submitted in this document(response to EPA Request for Information) and all documentssubmitted herewith, and that based on my inquiry of thoseindividuals immediately responsible for obtaining theinformation, I believe that the submitted information is true,accurate,-and complete, and that all documents submitted herewithare complete and authentic unless otherwise indicated. I amaware,that there are significant penalties for sUbmittinq falseinformation, inclUding the possibility of fine and imprisonment.I am also aware that my company is under a continu'ing obligationto supplement its response to EPA's Request for Information ifany additional information relevant to the matters addressed in.EPA's Request for Information or the company's response theretoshould become known or available to the company.

Alberto CelleriNAME (print or type)

presidentTITLE (print or ty~e)

~

sworn to before me this yi-J-day of fil.fS 2( sl:- , 19...9b.-~p~s-rf

IRIS L. HERNANDezNOTARY PUBLIC OF NEW JERSE:

MY COMMISSION EXPIRES SEPT. e. :1189

845340024

TIERRA-B-004446

845340025

1

TIERRA-B-004447

-

-

.,-' -- -

'.

-.' ~" .... -'.: . -'~.::-.

...

. \

-.., '--' ,'\- ..---

• li._.

-" -' .

0.

DEEDJ !'~.":~U.!:iLrJAi I. Ueve} "IJllh:nt

J\s,:.;oci .'7aCt:s

OC.UIlU ••'I'll

ChClllj_C~I) Cumpo ..... I:.;. Inc.

Il,'<:\...,1 :.,,,1 ,,'Iu ..n III:

.7 ,;"t)l'gu Gilrrison. l';fOquil'CII J5 t:l j I Llln I.vCllUI1:

,:1ift\lll. ik~/Jursuy 111015

fir:ln ..:c.

... - ... ,..,;/..~..: .. -.-,.a::"-F"'.)".'

"':"".:':':--.!':"'!oo."

"

'--=r= .=-

.: "' . 845340026

TIERRA-B-004448

-

-

."-

1,0 104-DIED ..eAftGAINAHa SAl.il"~1II (;-. Aoil'QCOIl" fOlNO ()IICQIIIP.- ....... t .....

(""'" ..... 0 'UNlJ.. ..-.LsrAI£ t£GM, ..."..,yco0.,.. ('...... ,. Ut ..... c, ....... H.j aM'.

DEED.',L1y I ,1'1 11("This Iko:e1 is lIIaelo: on

BETWEEN UIUUS'I'IU hI. ImV&:;I,UI'HI::tI'I' t\l;;:iUl.:J.Nl'&:;S.Loll Lall:ta Avr.llul!GaJ:'! il:1d, ll~\~ Jl:Clmy

, ..ine ill ptino:ipal "m"" at;L CU'I~Uf"U.OU oj Ihe ,I ...IC' o{ lh:w J Ul:SCY

1,11 I•.,m:;] AVCIlUC, Gactic1cJ, r~cw JuJ:'scy,clO:f1o:c110;u Ibe u,an'o ••

A.ND ChCII,iC.:ll Compounds. llle,

hos<: flUS I oUi •.., aelel.e .. i. lU V.,ll,"y 1\,,,,.1, $li:lllou!JI:, 1I",\~ ,J""·I"'''Y-I'..:h:ll,.iLI hi ...'" di'l.: (~t,j;lnIL""C.!~lac wo,d -G,:uncc'" S.II"'. 111':.&1& aU (;"Inl':~::" h~t.,;iJ ahuvC'

Tr.n~fef or Ownc-mlip. -rhe (i&"'UE<JI K,:uU:li•.,ttJ l.:UlIVC)"l'i (Uall3ih:u. u","lIenlup ul' IlK: .,nl()CU)"

cJC$Cribcd b..:lnw In Ihe: (irn.,nla:. 'I hi", I.r ..... ,rc:r i" tU .. ~I.: tu.r ihC' :'\.11111ur One: lIun~lL·I:d ."i n~ty Fl '\Ie'l'hou~Olnd ($l!1~.O()O.lIlll l)uJl,II::' ,llId llll/lCIII--------- ...··-----------------

------------------------------------- Ilu: (i.au ..... .u;Lnuwh::'lII:Il.:~ lu;..:ifu nJ ,Jau, "'UIIC)'.

'1'... "·bp lI.rercllcc, (N.J,~.,\. ·lh.I)·!.11 1\1111"'"1",111)' "I NC\~a l"k0111".)( N... 614 l.", Nil. ,,(, ',,"CUUIlI r-;...o No prtlpcrlY E~" kJeUlui..:o4tiuH lIu ... ln:t il. .iI'\-:ailahh: un iI~~ d .....: .,1 lilii ()t;....d .• ("ald" ~." .c ....,-.........

I·rupcn,. TIe..:-1)1"'114,,':f4~'(111",.a.b ul Ihe ~••u~ OIIM! ;,IU UK.:hu~hJ'.Il!~ an,1 :IIUUI,.1illt:1lo oLHItilt.: b" .. i"lIho: Ci t:y "f tl~"'':ll'kCuunly uf Eli 5":< :",.1 ~IaIO: .... New J.ne)', fbo: leI:M1de",,,,'II"It ".

Dein9 knuwn .and d~ti(;l·jl."~lJ.u!i lJl,"ulJu:.,·d 1.f..... H'I.";U ..l1i I,.ill (.ut .llIdllescribQll on i1. '1..:1..:1 t'-l iu sutuli vi:.; i<J1I h .....~.. ~nt. i t.l ...: "'L"t·op""::i.....1 ~ul.uj 'JillionloOt 1 - 1110ck 1i14 N",will'k 'I';,x I-lill'" IiC"" .• r ...·.. h)' Ih"'1"j." I-I.:lcr,v,," 1.] ~Wiltsan. dated JUIIC 25. 1~84. "ud CiJ",1 in Ihe I";:.»ox CUllllly It~<JistQJ··sOffice on Pebruary 4, 19115 as I-I'lp Ho, J594. 'l'his conveyance is llleulesubject to Olnd ulcmq wi.l;h the ri<jllt 'tJl inql"USli Lind ..,,,r.:,s» i1Jon9.OVC.l -anu throuCJh lhe c.:.ll:ii.c:.hll:ill ....1'(:..1 1.1 ill uul olilli ".·U\' i..h.:d '0'- in Lhe.::afoJ:'QllIenliuned llulJui v i~j <.III .".'p.

See Schedule A attached harl:to for aJditional description.

~R. NVzt!1 hi ..llS

....

.~

TIERRA-B-004449

-

- '.

-

All tholia cereain trace <II: ",u·c...,] .. f .land. lit;d any iu.-now DC hereinafter cunsLrucL~d theruon lylng and b~-

prov~nhtS C t.y of Essex in the Cit.~·. "f Newiark and the Statein9 1.n t. e Dun • .• f 11of New JerS8)·. being further duscril.><!u .l~ c> qws:

aeine knawn and deslgnated a. Lot C in Block 61~ a. sho~ on Hap~ntlcled "Hap of Subdlvi.ion af Lat 1 - Blac.k 61~" fned Febl"U",ry4, 1985 in

the E...... County Reei.ter·. Off l"e .$ Hap Hu .... er 3594 •.

aeine further des~rlbcd a$ Callous:

BECltININCat A palnt .... ere the HorthcoSlerly boundary 11ne of Lot B1n Black 61~ •••• hown on the above lIu:ntluRed map. interseccs the UnitedState. P1erhead and BuH.head Llne Alon'l the ra.sal~ IllYer •• nd runnlnG; then~e:

(1) Alone said PlurhQ4d and lulkhud I.lne. Ilort" 38 degre ... 47 alnute.20 seconds E.st 82.94 Ceet to a point; thence:

(2) ContlnuinG alone said Pierhead "nd Bu]khead Line. North 31 desre ..09 ..inutes 20 seconds E",st 25.41 feat to '" polnt; thence:

(3) North 51 degree. IS ..lnutes 4(/,;"co"d5 West 100.00"Ceet to a point;chence:

'. (4) Norch 89 degrees 4J Minutes 30 scconda Uest 52.33 feet co a polnt;t.hcnce:

(5) South 36 delrees ~2 minutia to seconds Uust 19.00 feet to • pointin the Norchenater] y boundary 11"a of Lnt B; lhallce:

(6) "10111 said Nl)rche.ster]l' boundary J lne of I.ot B. Souel, 52 dacr ....31 ..buc •• 40 seconds East 141. 72 feet to " polnt ln lhe UnltedStat •• Plcrhaad and Bulkhead LIne ll"d tl,(' r<>lnt and place ofBECINNINC.

leU\; nlso known lIa I•." ~C> 1n 1I0ck 614 un lhe Tax Hap oC the Cley of N..war

845340028

TIERRA-B-004450

.•• ' .. ~ "+ ••• ~.

-

....

Tile convey ...n.:u (,f the r.:.....:'10 i Ill] cas""Qcnt for j n~/I:C5S c1nd eqrQss ismlldc exprc5>11y !lllbj,~C:L te. the C;r,..nt.~(· 'n "hI i9ilci(.n to IlIl1int"in 5l1me41 t it.s own c.:u;:,:.t and ~x(i~ns.J ill cUllun,.. , \'"i l:h ;\ 11 ut IIl:L-S \llIing SiUIIQ

and it is uncl.,~·!a:u(l<l l'h.'l: r.hn ';'",lnt.l1· !'h," I h:>\,(, "0 I'~s~,,"sibi Ii tyor ohli".ll:ioll ill t.h,.I, n'<J.:ln1 wh:.l.s, ..,v",'.

Thi s conveyance is mad~ SUbj-.!ct t(1 the l'n L Low i nl) covenant which shaflbe construe,l £IS a covenant running wit:h the l<1n<.l binding tha Grantee,its successors ~nd ~sslgnti.

The Gram:eo. i t5 sllee~SS(lrs .. nd as!! i '.Ins. sh::d l he obllq.:l tad to payth,. Grantor. its SIiCC'~"SO['5 <1'1<'1 .lsslgns, Cive (5'-1 l'areent of thecO,st of sn"w rt::anoval. \111.:1['(1 """v;cc;,' :m" .1xterinr jl.nicoric11 andmaintenance service .,rtl'jhllt:,hlol to th" I'rclliscs owned hy the Grantorof which the "remi 50S <:'"lv"V",1 h"rUIIII.I.,,' ronn,,<t .1 I';,rl;. The G ....anteeCOVQl1itnt:s t.o \I"Y <lny ur .011 .... t'I\(,; ~.(un::i.d,1 (:uHls within ten 1101 do1Ysuf the ....eceipt of t',he l:I-i1nl:ur's biJ 1 enl' lH.mc:, rl1 t.he event: that the ••.-'"G':l1n\;et! (uils to (lilY <IllY 0" ;,ll ur 1"1.. , ;'(''I'e501I0l costs within thirty(30) d.:lys of tit", ....CC(Jil't "f 1l,'ulll.Or'f: hill f'lI: mime, SOlid ::ost$ shall

'becollll! a lien against thesl:: prc,nsie:s ,.hir:h Uo::n shall Ik'! subordinateto any mortgage lien ilg.dnst LIt",se (ll"l,ni!i"s provhlccl that the proceedsof such mortq.,qc h.;lvC hO::(lIl i nv.',s,. .."l i lit" ..h,1 prqmiso:::s desc ....i bed above,

'rln! Grantee 01 J su coven .. nts wi Lit the C:",lntor to jCl in any prope ....tyowner's aS50cio1tion fa 1:10",,1Hub.H~qIlC'". r.u this convo::yance to administert.he tCl'ms (if the cClven.U\t. "h,~ G'::Jlltllr rcpl:.~sent.s that it shallcause c1ny of the remaining prDperty "wned hy it ill: 29-75 RiversideAvenue, t1ewa ....k. New .:rel·suy. of which t.hesE: p ....emises (armed c1 pal"t,to be cha ....ged with a similllr coven,lnl. :lncl that it sha~1.l fairly andevenly administer So1mc .. ~ to ~Il of tha premises c1ffected,

Thi4 conveyance is subjecc to eilllCRlents und rcstrictions of recordif any. z:oning ol'dinanccs, sto1t.C, c,,"nty ilnll mUlIicipoJl l<lws orordinances af feet ing tho promi sos oJ,,,I such sta te of facts as an accuratesurvey would revoa1,

845340029

t 1C)' J ... ~.') t "5""," . ,.h t~t.. ••

TIERRA-B-004451

- '.

,....'·1 ~I Ii, I'" '.:II ;

..'.

",u" .. i!li('7l loll)' c;, ....... ,. '11u: ti'Ool-mllt II.nun>\:", Ill I'h." (i'tudn, I...~ d oK: II" .. ,,·t I.... ~.....umllfotf die:luup.:rfy. Illi~ ,lflU'lIb': i,. "';i"k.·.~ -'"41\t"Uunt iI)' Ii'" 'uttn..u h"b

40

• N.J s.'" ·U ,••. nll~ ,"UUi.:Ilo1.: nn:;.I' ....fhalIh ..- t'.:,UIIII h .. !' Un' ;,"h",1\t·.1 ';111\ 11" "....... lu .oIohh.iu .lln ..·r u,· ...... "h .. "... ,lIt ...". th.· IIi.t, .."'" 1.,\1.. h ..... If)' ..1.. Li ••y..\ IUHU.~~· u, ;;;LU",,-ing .. fl•••,~m'·nl h" Ik' 'I.· .. h·h ...' .. ,:.11.... 1 ~t... '~'"U""')

Situ •• urn. TIU:i lk·cd i"li :!to1~1"'d.. lilt au ...,.u'd lu In .h..: (".mhll'" IIIUI'c, CUIIIU.:lL~ ....111"':':1' a,. u( the'•.hl.c:'~U.lhc tUI' or Uu: li'l\ol .. a~c .• 'S ':ilqkUOIh: ", .... I~ ..Uu.,·d

• IIIUllS'I'R L.\ I. UJ.VEI.CJJ'l.tr:::tl·l· ASSOCIATES. >.<~',I' i.' ~"":. . 11\': IIIIJII:;'I'I( I ,\ I. ~1-:VEll(H'~II::II'1; (;UIIPORA'l'rO.~ ...... ~U ....h:'l.1b)·:-: .... ". l;'·lIto •. d 1'.11 J.rl\':I~: i..: ·~,",i:.·(., :~~l';..\:, j

~.'.~ ~; :~. \- ~.r;:::~);.~.l.""L.,~ I

I \ ~ Crttrrfi;;9~i:re's'~""'"'"''''.~\~:!~.~:.:,+.~.\"~:':'

.•~"" ""t! If t, •

. STA'II, UF NEW j "usn'. I 'OIlN 1\' (II.

I l'Elnu:" Ih.1 "" .1uJ y 1P4triui~ Vuylicce

per:)iuuaUy C:DllliI: ht:lut\: 11M! .. ,,,I .h,) PCU~UII iIL·Ln .. ",,'k,tfM;d und,' ... aU •• II' III)' ....au"' ......;.,.... 111.:11'I.... '1"b.IIC"~1I1 i,. tl ..: ~~'''''''''')' .. , 1.lIh.':'.1 I' i ,11 Uc.:vt:luPJQcnt .Associ,)\:es 1100""'I,,,,;oli,,,, " ... ",11illlhi. 'X",<I;(ht .hPo pcrJl-clit .... he I!lIiL',;liltl "·.U.'''!'lo '" die :lI'l=lwn-.: .If I~II~ J)a,"" .... 111)'IlIoCP'~ .. "t."1"'uIIIIIUUC "Uk.:,,:, "bu it

r",nthony V. IJ'.yIJ.c:ln, III .,... 1 ,1,;'111 dl'l:'I'""I.ualfIHI:

,,'1 .'11,\ ·cI ... " "(-1M" •• 1''' •• 14'11\".,-,1 ~I' Ih'·.·u.,"u ........I .... ll'lo !l.· ..... Uf.4.'· .. 'L du')' "'.lluu"CI~ 1")... "t ....I,.;1u;"'.. ", " 'Ie 41~Ik .....d 4" 'h ....·,· ,; ..

hU lhi. 11CIMHlIL.n,."." d ..: INUIJCI :w. I '''t' ,· ,"'1 .. 1I411t \4.J.k"" " .. " ..dIu ...·" h' dlb I ",· .. d :C~I ,hi"" ,.:e""••• JiIl'I...." 1111.\ , ... U,,' h" aUL'hI lu d · UUII •• 11 11...........· ......:h: .111.1 ,-£;

III Illc lull antl .."n •• 1 "",.".t.:'.lilllll"' ..I b.: ' .... I Ii" lh"lr:tll"~r "II"'" i. S 195, UI)(I.,Q/.I ....... :••:.•.. '!j ..,Such c ".i<I~r.lil"' ;"lIdillc<! ill "' ..'.S.A .Jf"IS·5 I .. ' !- T ''1 :-;

Sittn,,-d 3.I0I.l ·unH"n lu 11ol:'1~tu'nil" un I"J. ..•... o~ ~ , .~. . .~, : ..'I ,luLy I :''11110 " i I .:; .•.... ,.~

_:!.!.~::r.._ _.~.;..:_._.;:;;.:.. - - _. . ..;r.~·~I,;,·;;'~-:;~;·~lj:aw;.~-;~.:...·...;., ~;.lIenry Pa",cr. ion At\u .... c:y .-.\: 1 10' uf L·,',trJClil PUCJ J G.~:i·J...j' ._.,:':-:.~.~~.:;~t:1Q St. .. t.C u! New JCL'SOy - .......:...~:?:~::.,

-~". • .. 11"

..' ··;t·····':"····· .;\ ...1\111 h"fly V;' L'u'J I j cre: .s".....·...·I·...r

I'~II.

.........I'R',,,,,,,,I bf: .

II.J.:l'A.:Ii'i."1II ......, ""If'U'lIttr.

845340030

TIERRA-B-004452

.'

-,

DIAGP~~1 OF THE BUILDING

-, :------------ ,,"-':'...._-------- •..:...----- j ~. ----'

.·:':~4.c. Lot:.:....,~

,,T

LA ...

...

".

~/~._-+---------------- --

--------II

~~~~ II

---l-.- __ ---Jl.

r.. .•

~~.... '£.(.

........... ":'7Cj'

I-I

:--------- .... __ . .,,-----._ -

r-- ..---------,! 4#~,,__ c .. -:-

: .t#CClI(.$1l

~---. ----- --- - j

TI

IiI 65'

"""--'--.J:l~r~- ,

i

1 JJ .. ,!I"'-

""

I

: ..z • .,..::._,. .. -Ii ...,.",,01[ ....I

•tL .. ~

.. - ... - ~'- .: ~~..• ,. 4~l.

~- .. -- ......

845340031

TIERRA-B-004453

-

-

-.

C H E M I ('~t' ~'\t.Ii""" lildi! ~,-, Ji.,-,;-, to·" ~Il I!F'''' '~" iiN ~. '" ;.\~JL. ~Il<,) ~'tf~ ~.iJ'~(;;~,:;,,1n"l:~:p)' /I . tt.,;>-...:~f\It~"'ij":I"Illtlil;.',,;.;l 1·',~r1.

END /°1''1'0-5eptBnber 10. 1990

Southwest Photo Clan. Inc.350 Electra StreetPcm::>na, california 91766

Attention: John Jeleniewski

Reference: Contract dated Dec€!11ber 20, 1983

Dear John:

Back in 1983. \v'e entered into a Contract dated Decarber 20; 1983 wherebyyou agreed to perfonn certain services for us. Paragra(il 8 of saidAgreement provided that the Contract \«>Uldextend for a period of five (5)years and annually thereafter tm1ess either party gave the other ninety (90)days notice of teJ:mination.

'!be purpose of this letter is to give you ninety (90) days notice oftennination of our lIgreaoonl: of flccc3'rtler20, 1983 an:i any subsequentcvnendments thereto. You arc advised that the restrictive covcnnnt. ~·()nti.lincdin the Agr03nent and the confidentiill infoxmation obtained under saidarrangement with us is protected in accordance with our Agreement.

Q..1r relationship hus been a gcxx1relationship, and we appreciate theassistance ycu have given us in the past. Our ~t is te:oni.'lated inaccordance with our AgJ:eeOent and this .letter .

Very truly yours,

CHEMICAL. c:a.1POlIIDS I INC.

845340032

TIERRA-B-004454

':.' .

~... - ;. .~:.

-.- ~:._--

·-0:0" _ 845340033

TIERRA-B-004455

-

1 of 22


SEWER CONNECTION PERMIT

PERMIT # 20407122

(Please use the Permit Number on any correspondence with PVSC)In compliance with the provisions of the Federal Water Pollution Control Act,its amendments, the Clean Water Act and-the Rules and Regulations of the

Passaic Valley Sewerage Commissioners:

1_----------1Chemical Compounds. Inc.

I I(herein, after referred to as the Pennittee)

is authorized to discharge from a facility located at

~9-75 Riverside Avenue - BUilding #17

----- ....... 1Newark. New Jersey 07104

to th~ Passaic VaHey Sewerage Commissioners T~eatment Works in accordancewith discharge limitations. monitoring requirements and other conditions set forthh~rein.

EFFECTIVE DATE -----,07/20/92

EXPIRATION DATE ____ ... 1[ 07/20/97

Rev: 02/96


- BV'~~'5L~ ~-- EXECUTI. ECTOR ~

845340034

TIERRA-B-004456

845340035

TIERRA-B-004457

-.. :". ~-. ""

. "-:-'...". '''''.. .. "- ..-.~' .. ..' ,~ - ...... ,

".,..-.".:.-..; ...' .~.

~.:..~ .

845340036

TIERRA-B-004458

845340037

TIERRA-B-004459

-

1 of 22



PERMIT # 20407122

(Please use the Permit Number on any correspondence with PVSC)In compliance with the provisions of the Federal Water Pollution Control Act,its amendments. the Clean Water Act and-the Rules and Regulations of tile

Passaic Valley Sewerage Commissioners:

I )Chemical Compounds, Inc.

,-----_1(herein. after referred to as the Pennittee)

is authorized to discharge from a facility located at29-75 Riverside Avenue - Building #17'. .

....._-------~Newark, New Jersey 07104

[0 the Passuic Valle\' Sewerac:e Commissioners Treatment Works in accorda.nce. - .with discharge limitations, monitoring requirements and other conditions set forthherein.

EFFECTIVE DATE I 07/20/92 II IEXPIRATION DATE 07/20/97

Rev: 02/96


BY~~~~~-'-' EXECUTI.ECT<i~ ~ ..

845340038~ ..... ~ .. ~~...... . ZW __ , _ .J, c .• i .•. hr_"'.

TIERRA-B-004460

845340039

TIERRA-B-004461

-CHl!:MlCAL COMPOUNDS me.

WASTE WATER POLLUTANTS

The following is a list of pollutants detected in each specific waste water stream. Thepollutants typed in BOLD face are detected regulated compounds in our waste water discharge. Theownbecs indicated in the table (and in parenthesis) are of an average coocentration anaIyz.ed in-house or at an accredited laboratory - throughout the years.

PRJORITY POLLUTANTS

HeavyMetab CyanideCoJu:.

VOACollC. BNA Conc.b

Metbylene Chloride Phenol (300)(38) 2-Nitrophenol (450)

COD - 450,000 Acetooe (13,200) NitrobeDzene (286)ppm Chlorororm (25) Aniline (2680)

1,2-DicbJoroethaDe (130) 2-Nitroaniline (800)Toluene (t650) 3-Nitroaniline (&70)

ChlorobenuDe (381).- Ethylbenzene (26)CblorometllaDe (550)

BeDzene (960)o-Xylene (4150)

m.p-Xylene (103)

HCBlue#2 <0.20 1.0 2.0 Tetrachloroethylene 2-Nitrophenol (650)(220) bis (2-Ch1oroeIhyl)Flher

COD - 60,000 ppm Chloroform (19) (440)

NHNFA <0.20 0.3 <0.10 Chloroform (22) PhenoJ (320)Methylene Chloride (25) 2-Nitrophenol (770)

COD - 42,000 pptn I.,2-Dicbloroetbane bis (2-CbJoroisopropyl)E:lher(1800) (7700)

Toluene (41.) NitrobeDUile (73)Chlorobenzene (57) 2-Nitroaniline (820)o-Xyleue (32,000) 3-Nitroaniline (&60)

NPD <0.20 0.35 0.20 BeIowMDL Phenol (26)2-Nitrophenol (155)

COD - 82,000 ppm lsophorone (180)2-Nitroaniline (300)3-Nitroaniline (980)

-.

845340040

TIERRA-B-004462

-

-

HC-Yellow#2

COD - 110,000, ppm

<0.20

<0.20 0.850

PRJORITY POLLUTANTS

VOA.Cone.II

ChlorobenzeDe (2810)Xylenes (49,100)

l,2-Dicblorobenzene(169)

BNA. COliC.

2-Cblorophenol (496)Nitrobenzene (159)

2-NitropbeDoJ (3380)2-Nitroaniline (5510)

HCYellow#4

COD- 190,000ppm

< O.OJ Methylene Chloride(5'4)

l,2-DiclJloruetbane(7200)

Acetone (8600)Chloroform (55)

Xylenes (260)

his (2-cWoroethyl) Ether(47,600)

bis (2-Ethylbexyl)phthalate (107)

DNHA 1.43 0.9 < 0.01 Below MOL 2,4-Dinitropbenol(12,100)

HCYellow#5 1.43 0.8 < 0.01 . 1,2,4-TricbloroIJeDune(44.2)

4-CWoroaniline (442)

BelowMDL

NOIlD

COD - 225,000ppm

0.269 0.277 < 0.05 Below MOL Below MOL

HC Red # 3 < G.20 < G.OI Methylene Chloride (32)adoroform (41)2-Buta.none (54)

Bromodichloromethane(31)

Toluellc (:17)m,p -Xylene (35)

l,2-Dicbloroetbane (50)

0.372 2-Nitmaniline (100)

.... MOL - Mean DetecliOD Limit

845340041

TIERRA-B-004463

·.. • r .•

ACCREDITED LA8~AllIRIES [1«:.UOLATILE IKANIC AtW..'tSI~ DATA

CASE IUIER J1B0 MATRIX AauepIII-:nu IIIIIER 9~AB9J6 DllUTl~F~ toqflLE )AJlj40 DATE OORACTED

....\00 NAI£ crt DATE lWl:aED tJ6a819~FIELD 10 jpre ANAlVZED BY lflRRY

...~._.................................................... ..........................................................CAS' ClI'flCl.N) tJ;1l IIX. CAS t C%J'fO.JG ~ I'D.............. ~............................................. .. ••••••• ................................ M ................

107028 Aerate in U 61 78875 l,2-Dichloropropene U 4.010'131 Acrylonitri Ie U 66 10861m cia-l,J-Dichlaropropene U 4.07487J Clloro.thane ~O W 20 "016 Tr ichloroethene U 4.0748J9 BraKl.thane 300 W 20 714J2 Benzene 9611 W 4.07;014 Uinyl Clloride U 20 124481 DibrolOchloro-ethene U 4.0i"im Chloroethanlt U 20 191DS 1,I,2-Trichloroethene U 4.07S092 Methylene Chloride U 10 1OU61026 trans-l,3-Dichloropropene U 4.067641 Acetone 24000 W 18 110i"i9 2-chloroethylvinylethllr U 20 .7'i1~O C4rbon DisuIFi'ae U 4.0 m~2 SrlllOfor. U 4.075694 TrichlorofluorOlllthane U 4.0 591786 2-HeK.none 110 9.11i"i~4 1,l-Dichlorllethene U 4.0 108101 4-Methyl-2-pentenone 68 7.07SJ4J 1,I-Dichloroeth.ne U 4.11 127184 Tetrachloroethene U 4.0156605 Iran,-l,2-0ichloroethene U 4.0 79J45 l,l,2,2-TDtrachlotoethane U &.a6]66J Cllorofo'" n 10I 4.0 10888J Toluene l~OO W 5.0107062 1,2-0ichloroeth~1 U 4.0 108987 Cbloroblnzenl 68 W 4.0789JJ 2-8utenone 18110 4.0 100414 EthylbenZllftll 26 1071;~6 1,I,I~Trichloroethane U 4.' 10047' Styrene U 4.0

.-!!62J5 Carbon Tetrachloride U 4.0 m0207 .,p-l(ylene J7 W 28'1l0~4 Uinyl Acet.te U 8.0 95476 o-l(ylene 250 W 21]4 BrolOdichlora.ethane U 4.0 1~6S92 cis-1,2-Dichloroethllf\ll U 4.0S!.RRtXjATE C!J!fWHIlS

1,2-Dichlorolthlne-d4Toluene-d8BrolOfluorobenzene

.JJ.!!!l.S...76-11498-110

.86-115

J - Indic.te. cllMpound concentration found below MOL.U - Indicates co~d analyzed for but not detected.

B - Indicates COMpound found in alsociated blenk.W - Result exceed, specific ground weter quelity criteri •• -

- Flaga are bas'd on Specific bround Water Quality Criteria fro_ HeN Jersey Register dated Februllry I, 199J.

-845340042

TIERRA-B-004464

CASE NJMIlERSAnIU tu1BER

-OATA FILElENT HAI'IE

IELO 10

ACCREDITED LA8ORAfUIUES, lit:.(jHA lRGflN I C AHALYSIS DATA

UBO9~01l9J6

0:1'!IIf!PA

CAS •...~~ .s•••••••••••••••••••••••• s••••••••••••••••••••••••••••••••

1089~295578954Q7I08J94llllJl;S105679120812111444S417J1lU611671001j16'I'';5Ul108601621647677219895378591658~0

-.111911'~01l21

20'11164;'8lJ76S'91S7677474~1'111788744131m208968\l9l1'J2833291J16496Q62112

Phenol2-Chlorophenol2-l'lethylphenol3&4-Methylpheno I2-Hi tropheno I2,4-0i-ethylphenol2,4-0ichlorophenalbis(-2-ChloroethyIIEther1,3-0ichlorobenlane1,4-0ichlorobenleneBenzyl Alcohol

'1,2-Dlchlorobenlenebis(2-ChlorolsopropylletherN-Hitro50-Ui-n-prapyla.lneHexachloroethaneNitrobenzeneIsopharaneBenZOIC Acidbis(-2-Chloraethoxy)Methane1,2,4-Trich)orabenzeneNaphthalene4-chlofoanilineHexachlarobutadiene2-nethylnephthllenehexachlorocyclopentadiene2-Chloranaphthllene2-H iIroan I1lneOi .. thyl PhlhaleleAceflaphthylene.HHtroand lneAcenephtheneDlbenzofuran2,6-0Initrotoluene

JOOJUUU

~OJUUUUUUUUUU

74 JWUUUUUUUUUU

8UO JuU

870 JUUU

~TE ctI!fWt)SHitrabenzene-d52-F)uorobIphenyITerpllenyl~d14Phenol-d52-f 1uoroph,no I2,4,6- Tr ibrOllOpheno 1

J - Indicates co-pound cOflcentrltiOfl found below MOl.U - Indicates tOlpound IfIllyzed for but not detected.

m500500508500500500SOU5005110

1000500500500500500SUO

2500500500500

11100m5UO508500

2500500m

2500500500500

MATRIXOILUTllJI FACTtR __ -:"~-::- _DATE EXTRACTEDDATE AlR..YlEDANll.YZED BY

Aqueous5806aB19S

CAS f:........................................................... ~ ~ .5~0788062959545128510002]'j)4l)21878651211420466270US72J867371000168630610155'11874185018120127847422064401290110115687919415655'11781721801911784U .2U599220708'1S0J18193m5m319174262m

4-Chloro-)- .. thylphenol2,4,6-Trlchlorophenol2,4,5-TrichlorophenoI2,4-Dinitrophlnol4-Hi trapheno I4,6-0in Itro-2-.ethylpheno 1Pentachlorophenol2,4-DlnitrotolueneO.lthylphlhalate4-Ch1orophenyl-phenyletherFluorene4-Ni troanliineN-HitrosodIPhenyla.ine4-8ro-aphenyl-phlnylether~xachlofobenzenePhenanthreneAnthraceneDi-n-8utylphthallteFluaranthen.Pyrene8utylbenzylpnthalate},J'-Dlchlofobenzldine8enla(aIAnthracenl8Is~2-Ethylhexyl)PhthlllteChrysen.Oi-nrOCtyl phthalateBenzolb)Fluoranth.n.Benzo(kIFluarant~ne8erJzo(a JPyreneIndeno(1,2,J-cdIPyreneDibenzo(l,hJAnthraceneBenzoI9,1l,1)PeryleneN-Hltrosodillthylaline

uuuuuuUUUUUUU

UUUUUUUUUUUUUUUUUUUU

10011SOd500

25002500250U250U560500SUO5UO

25UUSOU50U500SUU50U500500SOU5UU

lUUUSlIU,1IUSOd,00500'1UO50U~UU~OO,005Uu

~. Flags are based 0" Specific Ground Wlter QUllity Criteril Fro. Haw Jlrsey Register dated February 1, 199'.• J-/'1Itthylphenalend 4-""thylpllenol call not be M~ratld by the -ethod applied

REJ:DyERy J.ll!Ui. ~--B" 3'1-114 -L----!t , 4}-116 ~----i! " JJ~141 ~---!Z. " 111- 94 ..JIL~ " 21-100 -11----1J. " 10-123 --aL

B - Indicates cOlpound Found in Ilsociated blank.U - Reault exceeds speciFic 9r~nd NIter quality crlterla.-

845340043

TIERRA-B-004465

-.' ..'.INTEGRATED A!'R.. 'rT [Ci=L LAB TO01-15-1996 04:5:A1

--"".\i=J.srfRed.' .'. .1

. :Lab.-.. .IIi

7725898 P.05

I~egrated Analytical Laboratories, Inc.' (

273 Ft'lJn~lin ReadRandolph~ N. J. 07869

I,I .

:MOt ... B!ffiioD OETBCuON bArr

ANAL\'TlCAL DATA REPORTfor

CbemicaJ ComP9UncM fnc.Z9-75 Ri.-eqide A.-eoN~NJO'101

Project Nam~ I'VSC MONITOR.iNeLab Case Number: 10950.2904

201 381-4252Fax; 201 989.5286

! .f

< - LBSS THAN rnE •.fM:

.-

l.alj1D;:~C~tID:OOI I

M"rilllUaira : Aqucou - H(LPeatead..roimlre: 100 '

ICflI!Ipound .aar~~ViaYtCaJorideBromomilClwle

~TriehJoraftUOl'qmechano'l.l.biclloroetbeDeM~yJeae Ca1orid&tr'aai-1.2"Oic:hJOroetheDel.l.DichlorocchaaeCaIarofotlll1.I.j·Trichl~~ "'etrac~oride.1.2-()~~.

T~eae;1.2~di~

Cone:. Q< 10.0< 10.0

;< 10.0!: <: 10.0. < 10.0

< 10.0< 20.0< 10.0c:: 10.0

18.8< 10.0<: JO.O

~7 < lO.OI.I: < 10.0,. < 10.0

< 10.0

VOLATn.ESMechodQ4

MDL10.010.010.010.010.010.020.010.010.010.010.010.010.010.010.010.0

Compound

Bromodichlorompthane:z..ch.ICIftlOrbyl Vinyt Ether~"1.3-0ichlorop~Toluene .tQnl-l.J-OichJolopt'OptneJ .1.2·TrichfOl"Olltbai!eTctrlcbJoroedlcneDibromochloromett.aeCalotobcnleMEthylbeaz.MeTotal XylOQe$Bromo(onDI,J ,2.2-TetractaJoroedlane1,3·Dichlor~1,4-Dicblo~1,2-Dichlorobau.eac!

D,te Sampled: 12126195nme Sampled: 15:00Dite Aaalyu4: 1/2/96

•

Cone. Q MDL

< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< JO.O 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0

.< JO.O 10.0< 10.0 10.0

.-

TOTAL CYANIDEMethod 335.%

MOL0.05

D.~ Sampled: 12126195Time $aJaplod ~ 15:00D,te ADa!)'ZIId: 1/2196

These data have beeR reviewed and accepted by:

I Ie. • •. .Labotatoly Oirecto

Tbe.JJabilky oI~ ADal1ticaI ~. IDe. it limited to Che aaaf eosc ~tbo aaaJys.l*formed.

Hcwl~ CeniGi:dlaW' 1475t N_ YorkCercilicd Lab, IlW

TIERRA-B-004466

"..

\t~..·• n~r8Ced':.)..;1Ify~:~".

.- lII!

Integrated Analytical Laboratories, Inc.273 Franklin RoadRandolph, N.J. 07869 201 361·4~52

Fax: 201 989-5288

MRL J MWHOP DIITECTlON 4MIT

ANALYnCALDATA imPORTfor

Cbemk:aI Compounds. Inc.19·75 Riverside Ave.NcwarII. NJ 01101

Project Name : PVSC - MONITORINGLab Case Nwnber: 10950 _~

< - LESS iHAB THE M0la

TIERRA-B-004467

FROM INTEGRATED FtRYTICAL LAB TO 77258'38 P.03

.Integrated Analytical Labora~oriesJ 'nc.273 Franklin RoadRandolph.: N.J. 07869 201 361-4252

Fax: 201 989.5288

ANALYTICAL DATA REPORTfor

CheaticaJ CompoWlds, lnc.2f-7S Ri"cnide Aye.Newad, NJ 07181

Project Name : PVSc • MONITORINGLab Case Number: 10950- D03C : :;

Lab 10 ~29l?~-41Cleat JIP : 0El1~" ... !: AqlMoUS -ILIILPerceau ~Oi'-': 100Com i d~

!i .,

. LabID'~l, C1ieac m : 001

M.crwudi .. :!Aqaoou _1qiLPerceat ~ 100,CoatpoaaCI

! .: Lad :; ZJDc I

SEMlVOLA. TR.ES - ACIDSMethod'1S

Date S.mpled :Time Samplood :Cae. A.aaJyzed :,.

1212619515:001/11196

· Result Q MDL< 100< 100

'<100..: JOO

· <: 100,;-< tOO--- -.)

.... 20400...-./<: 100

·< 100< 100<: 100

:<: 100,< JOO'< 100kloo

100100100JOO100100

1000100100100100 .100100100100

METALSEPA Seriel200

. 121261951$:001111/96

Result Q

< 0.04iO.22

MDL0.04 .0.02

: Q - QuaJiBor! I'- ,i

: .... ~

!."

845340046

TIERRA-B-004468

FROM INTEGRATED AlRYTlCAL LAB TO 7'72~...g98, I

Integrated Analytical Laboratories, Inc.I ..; I .'

27~ FraqkfinRoad 201 361-4252Ra~dalp~;N.J. 076S9 Fax:201 989-5288

J 1 t"

ANAL \'TICAL DATA REPORTfor

Cbenic:al Compounds. Inc.Do1S !U"nde Aye.Newark, NJ 01101 ._

Project Name : PVSC - MONrrORINGLab Case Nwnbcr : 10950 - 2.9OJ'

MDt~ METHOP bmrnpN u~a• 1· .,

· . ,· ! < - LEss THAN THE MI5bLab ID ; ~3·<1lCUeot rD : E!O1 I

I . ,· Matrix/Vaic.: Aqueous. mclL :

P~t Moiimft:: 100 .,

GENERAL ANAL YTJCAL

Date S'Dlpled :Time Sampled :

l2l26/9515:00

I· CompoQnd (Method)

I •

. BiocJw:aaku :OXy~ Dczn-I (4Ols.1)- ~ 'i. I. -"'*&I S~ Soli. (160.2) ,. .

i Result Q MDL! 18600;< 10.0

NA10.0

JI2/96113/96

'Q - ~lifMr

• '. : I

·All NlOEP.Prot:ocol were (oJtpwed ~urinl analyses. These data have been revie",,~ and 4Ccepted by:· i

'-

TIERRA-B-004469

ACCREDITED LABOllATORIES. INC.-- VOLAnL£ ORGANIC ANAlYSIS DATA

CASE NlIIlIEJl 2616 MATRIX AgyeousSAMPLE NUMBER 9596616 DILUTIOIl FACTOR 1,0DATA FILE ~9813 01.IE EXTRACTEDCliENT NAME CCI DATE ANALY2ED 05ffi195fiELD ID .fA AIIALYlED BY LARR!

.._----------------_ ..-- - ••• = ._... •CAS 11 COlPWNO UG/L IIlL CAS' lXII'aJllll UG/L IIlL~._==.. ==_=_c===_-===_===== • .._;::QI=__ • .:II.__ ==___._

~.~.--- .... ~- __ ~k__ ____

107028 Acrolaln U 6.1 78875 '.2·0Ichlor~ U .4'07131 Acrylonitrile U 6.6 100610'5 cla-1.3-Dlchloropropene U .474873 Chlorllllllthana U 2.0 79016 Trlchloroeth_ U ,474839 Br_th_ U 2.0 71432 Ben:lene U .4750'4 Vinyl chloride U 2.0 '24481 Dlbromochloram.thane U .475003 Chloroeth_ U 2.0 7'9005 ',',2'Trlchloroethane U .475092 Methylene Chloride U 1.0 10061026 trens",3'Dichloropropene U .461641 Acetone U 1.8 210758 2·Chloroethyl vinylether U 2,075150 Carbon Disulfide U .4 75252 BrOllOforAI U .475694 TrlchlorofluoraBethane U .4 59'786 2·Hex_ U .975354 ','-Dichloroethene U .4 108'C:n 4-Methyl-2'pentanone U .775343 1,1-0lchloroethane U .4 '27184 Tetrachloroethefte U .4'56605 trans".2,Oichloroethene u .4 79345 l,'.2,2·Tetrachloroethane U .667663 ChlorofoMl 2.' .4 lQ8B83 Toluene U .5107062 ',2-0Ichlorotthane U .4 108907 Chloraben:lene U .478913 2·Butanone U .4 100414 Ethylbentene u '.071556 1,1. I-Trichloroethane U ,4 100425 Styr_ U .456235 Carbon Tetrechlorlde U .4 1330207 _,p'Xyl_ U 2,8- 108054 Vinyl Acetate 11 .8 95476 o-Xylene .a 2.175214 Bromodlchlora.ethane U .4 156592 cia'l,2'Olchloroethene U .4

SURROGATE ca1PaJNDS1.2-Dichloroethane-d4Toluene-dII'ra.ofluarobenzene

J - Indicates c~ concentration found below MDL.U ' Indicates clllllpDUndanalyzed for but not detected.

RECOVERY ...JJ!UIL. ....!I!nlL---l.2I" 16·214 ....z.....--19.1 " 88'1'0 --!!L--.1l!.1 " 86-115 ~

B ' Inc:liQtes coqlCUld found in ..aoclated blank.w - aesult exceeds specific ground water quality criteria ••

• Flags are based on Specific Grll\Rl lIater Quality Criteria frQllllIew Jersey lesllter dated February 1, 1993.

-845340048

TIERRA-B-004470

HtC~EDIT~J~ATCRI:~. IHC.cAA iJRl,FtliiC r.NALYSIS ~1ATH

t~'i'E tU'l8lQ-.. 'jAt"1lJt..£ Htnl£R

;AIA FILEell £liT NAI1£r!RD 10

CCI

MIRIXOILUT lorlrAC~ __ --'~ _DATE £<TRACTEDOIHE ANALyZ£DANAL.YZED BY

,C~/l,/Il';

.:.s••••••s.a•••••:aa•••s=~~=.aa.= ••••=.s••••••••••••••• ~~ s•••••••a••••••••aa••••••c•••••••cc.=••=•• s.~~~~~_~;~~s.~.

10~~,2 Phenol U ,U 9~9'" 2,~!'-Trlch.orophenol U 1~iJ'J"J8 2 -Ch 10ropheno 1 U 50 mllS 2,4-0Inltrophenol U Z~O··~48} 2-r.ethylphenoI U 50 lUUU1J 4-Hltropher.ol IJ 2~ai:;1I}94 J~4-r.ethylphenol U .;U " ..,21 ~16-0Inltro-2-~thylp~enol ~ 2~sJS~;-~lj 2-HI Iroohe"" I ~UU ~;J ll78~5 PentachiorophenoI ;J 2~i)ih"6i9 '1 !4-:'11 IIle l'hytche"o I U .,(/ 1Z1142 2,A-Olnitrotoluene 'J :'=iJ;~i.II~j2 2,A-OIChloropheno! U ,U 134Gb1 Olethylphthalate . ..:!14-'4 bl~(·2·Chloroe:hyl)tther U ~O }IIU,:'"D ..l-eh lcroc:-,el"!~~i-~ho!fJY~:!:l":'!!"

.,::'''ll~l 1,~-Olchlor6SenI,ne " 51J g67~7 F:uQi"l!r.e ,::Jo~? :~~-Olch~or~ben:ene " ~!) lU!j~~lD 4-NI~~o!nli1~! oj ".~;;

:~n'i:Q =-er::z.~; 1 Alcaho i " £;0 ncrj6 :I-I'h t :"Qsc~:~:.-!~,d~":ll"'1~ ;.:.:'

.';~~1j~ 1!2-Dichicr~ben:ene ~:j ~~:!::':3 ol"'~f':-ii.ao"'en:.:: -"~~!~'J~! ~~~... " ":q

:UHO'i ~ Jls~2-~~;~r~i~~p~OP:~:t~·~;.r .- . ~. ~.r_ ... ·-~/:=:L:-. ~':i,".;,: ':~:.-=~~!.':.,-":.-. ·~-·'h~i:;~·:-"';1-~'''?'''·1p;.,~;:!1-~ -'

; .~ ·':~!J~2 ~~~~!r--t~!"!~1! ., ~:J-'

~" ... ~ -~'(oc": ,j;,,~e!h~:,'! i..i ~:j 1~~12l ~.r::hr~C~!1t . ,."~,,~; N, ~~~be!1z!!ne J ~\l 311742 oJ·~-aut~ipht~~:a~e "":j

·-~~':tl IsopMranll ~U -;:U6~~ ncvr,~n :~ene " ..:,~li~u a'!nZ:lJ1C Acid " 7':U ~::9UUO P:Jr~l'ie J .".- .. ,1~':'11 blsi-2-1:hIQroethoAylr.e!~ane U ,i) 3%l!i' autylben~·...ic;;~~3.!~~ ..;.,;.. J~J~-Ol~~::~~b~~:~1~r~.;;:j321 1,2:~rrlchiorcten:llroe U ~O q, ..."'! ..1 :"::.:.... "..

~···.:7 ~ph:~alel'e il ,;,~ ~~:';3 e~n:~la~;nt~~~(=~e .. :;.....v ....

: ~:.. .;,:11 l " I , 'J ~~j 11.:'31.:' s,'! ~2-t·~;.1t~!:r~I!~~Ioo:t ... ~ ~!~'! .' • oJ.a._I ...; •• orocn1 ~H""·i"'~:~J ~e~acn,orn~u~3d:e~e U 5Q 21SU1Of O1r:J$tne W - ,

'l'.'~ i-~thylna~hthaler.e U ~!l llil14U ih-n-~ctyl phthaiat~ lj ~·i·~·"I.4l~ H~x~c~iorQeyc!openladlel'e !J '5iJ 2lJ,,9:.!, aento(b:~luQr3nthene :) ~~';l~ij] ~-IJ1loronaphthaienll U ,0 207GB? $enIo(k)~luor~nthene i'; ~iJ~11;.u ~·lil:1"l)antline IJ 2~~ ,1JJ29 [lenzota;~yr=ne '-j :.i'!."!;lll:, Ulllle:h~JI ~!tla late J 0;0 r~~::::, InG!not::~!J-~d>~~ren! :J ":.i~:11l~~i:1 Ilcenaj)hthylene 1I ,u "1)1J} Olbenzo(a.~}~l~raC!re .! ""I;

~'iIJn Hill troa", i,,,e ;j ,~l) 191'.:4;l oen.ol~,h~i)P,rylene 1J ,tl~}3~9 AcenaDntMne IJ 50 •• 'Io"~oJ- '~~ltro3Cdlmelhylemlne ~J'.)~/ ..· "L:~64'1 Olbenzohtren :) ,U 1H}29 2,~-Olnltrochlorooentenll 'j ~~IJ\l,,06202 2}Q-Olnltrotoluene .U 5u 229715 2.~-Dlnllroohenol :.J ::~iJiJ,~,!ll 4-lnioro-'-~thylphenol U ,g aalf\l! 'l~4:6-rrlnlirc?nenoi !j ~~iJa1d~J6l 1~~,a-irichlor~ph~nol IJ ,0

~L"r1'd'.\'~q; '~~'!1'I,,·;,it(!S:h I roben:,ne-o':''l-f!uOrtDlphenylTerphenyl-dl~Phenol-o!i2-Huoropheno 11,4,6-lrlbroaaphenol

!nClcetes c~mpo\lnd concentration round below ~.Indicates co~ound analyzed far but not detected.

ir::q.n.rc.'f{ Lin!~;i ':-:;;!;;;---ft , JH.:4 .....:.!----::! !C 015-116 -2-~ I }~-141 :JUT--&' 10- 94 --'L----l1 " 21-1011 ..J!L__ 1_6" 1U-123 ~

8 - Indlcate5 co~ound found In a&!oc!ate~ blank.~ - Mesult exceeds ~peclrlc ground water quality criteria .•

_.• ~lag5 are based on SpeCIfIC Ground Water Quality Criteria Fro_ Hew Jersey Regl&ter deted February 11 l~~J.•• J-nethylphenol and 4-Methylphenol can not be sepereted by the ..thod applied

845340049

TIERRA-B-004471

ti:NoUSTRIAL CORROS ION MANAGEMENT,. 1152 Route 10

'Ra;.ciOiph',NJ 07869h01.-584-0330

"'TOBER 11, 1995

Inc.

Certified for: NJ, PA, DE. CT, NY (DOH)NJ #14116 NY #11376US EPA CLP Lab

ANALYTICAL DATA REPORT PACKAGE

CHEMICAL COMPOUNDS, mc ,Waste waterCustomer

rD: MATRIXLAB

NUMBER

DATE "TIME

COLLECTED

ATLABDATE

,Aqueous 220698 09/21/95 08:30

Supervisor/Manager Signature:

~~' ~ '~Richard S. LeJine

pyright lCM, Inc., 1995.'.,.rights reserved.

_.4~,

Page #' 2

"845340050

TIERRA-B-004472

.... :-

INDUSTRIAL CORROSION MANAGEMENT,1152 Route 10Randolph, NJ 07869201-584·0330OCTOBER 4, 1995

INC.

Certified for: NJ, PA, DE, CT, NY'IDOH)NJ 114116 NY #11.376US EPA CLP Lab- PRIORITY POLLUTANT ACID FRACTION ANALYSIS BY GC/MS

Lw.. .,j'umber:Client:Sample source:Sample 10:Sample date:sailed by:At ab date:Matrix:

220698CHEMICAL COMPOUNDS, INC.Waste waterNPEl·MI,'.09/21/95 Extracted Date:CUstomer Analysis Date:09/22/95WATER

Data Pile: >I7063

09/26/9509/26/95 Column: 30m SPB-S

Dilution Factor: 10Init Sample vol_ 50ml Final volume_ 10m!

Conc. in Sample - ((Conc. on Quant Report/Initial Volume) *Pinal Volume) *1000

f?arameterMethodResult Blank

ug/l ug/l

t1 UU UU UU UU UU UU UU UU UU UU U

MinimumDetectionLimitug/l

2 -Chlorophenol2-Nitrophenol?henol2,4-Dimethylphenol2,4-Dichlorophenol2,4,6-Trichlorophenol?entachlorophenol!,4-Dinitrophenoll,6-Dinitro-2-methylphenolI-NitrophenolI-Chloro-J-methylphenol

200200360200200200200720200200200

- ug/l - micrograms/liter or ppbJ: Indicates a compound was analyzed for but not detected at the MOL.J: Indicates an estimated value. It is utilized when a reported valuemeets the identification criteria but the result is leS8 than thespecified detection limit but greater than zero.B: Indicates that the analyte was found in the blank as well as thesample. It indicates possible/probable blank contamination.NO: Not Determined.lNO: Indeterminable

Copyright ICM, Inc., 1995.~ reffJreserved.

-10 845340051

TIERRA-B-004473

,. nmtJSTRIAL CORROSI"" MANAGEMENT. DlC.1.152Route 10I Ra.n401ph, NJ 07869

I 201-584-0330OCTOBBR 4, 1.995

:-j PRIORITY" POLLUTANT BASE/NEUTRAL ANALYSIS BY GC/MS

I

•IIII'.ar....t.rIN-NitrosodimethYlaminebis(2-Chloroethyl)echerI 1,3-D1chlorobenzene1,4-Dichlorobenzene

1·1,2-DiChlorobenzene'bis(2-Chloroisopropyl)ether, N-Nitroso-di-n-propylamine

'

HexaChloroethaneNitrobenzeneIsophorone .'bis(2-Chloroetboxy)methane

. "1, 2,4 ~Trichlorobenzene", Naphthalenerxachlorobutadiene~chlorocyclopentadiene_ . ..1l:oronaphthaleneI D1methyl phthalate

Acenaphthylene112,6-Dinitrotoluene• Acenaphthene1-2,4-DinitrotolueneDiethyl phthalate

•4-ChloroPhenYl phenyl ether

Fluorene

r .N-Nitrosodiphenylamine1,2-Diphenylhydrazine (AzobenzeneJ

114-BromoPhenYl phenyl etherHexachlorobenzenePhenanthreneI-Anthracene

Di-n-butylphthalate

'

FluorantheneBenzidine.....PyrenaButyl benzylphthalate3,3'-DichlorobenzidineIIBenzo(aJanthracene~Bene

I"-bis(2-EthrlhexylJPhthalateDi-n-octy phthalate

IIIBenzo (b)fluoranthene

:."_ ug/1. micrograms/liter or ppbU: Indicates a compound was analyzed for but not detected at the MOL.J: Indicates an estimated value. It is utilized when a reported value

I-meets the identification criteria but the result is less than the" specified detection lilllitbut greater than zero._I B: Indicates that the analyte was found in the blank as well as the~ sample. It indicates possible/probable blank contamination.NO: Not Determined.

iI}-_ IND: IndeterminableCopyright 101, l:Dc.,1995.All rights reserved.

jM'M

Certified for: NJ, PA, DE, CT, NY (DOHINJ #14116 NY #11376US EPA CLP Lab

Lab Number:Client:Sample source:Sample ID:sample date:Sampled by:At lab date:Matrix:

220698CHEMICAL COMPOUNDS, IRC.Waste waterNPD MI.'s09/"1.1/95CUstomer09/22/95WATER

09/26/9509/26/95Extracted Date:Anal.yaia Date:

Data File: >.17063

Column: 30m SPB-5Dilution Factor: 10Init Sample vol. 50ml Final volume= 10m!

Cone. in Sample - «(Cone. on Quant Report/Initial Volume)*Final Volume)*1000

Resultug/l

MethodBlankug/l

uUUUUUUUoUUUUUUUUUUUUUUUoUUUUUUUUUUUUUUUU

uuuuuUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU

11


.'

200200480460.480240360580200200200460400200300400920300200380200460400340200200380380180160500120200100240200100100600200140

845340052

TIERRA-B-004474

,"I

INDUSTRIAL CORROSION MANAGEMENT,1152 Route 1.0Randolph, NJ 07869201-58470330OCTOBER ", 1995

INC.Certified for: NJ, PA, DE, CT, NY (DOH)NJ #1.41.16 NY #11376US SPA CLP Lab

- PRIORITY POLLUTANT BASE/NEUTRAL ANALYSIS BY GC/MS(Continued)Additional Base/Neutral Targeted CompoundsI

Lab Number:Client:Sample source:Sample :DJ:Sample date:sailed by;At ab date:Matrix:

09/26/9509/26/95 Column; 30m SPB-S

Dilution Factor: 10

220698CHEMICAL COMPOUNDS, INC.Waste waterDO ML'809/21/95 Extracted Date:Customer Analysis Date:09/22/95WATER

Data File: >17063

III

Init Sample vol_ SOml Final volume_ 10mlCone. in Sample. «Cone. on OUant Report/Initial Volume)*Final Volume)*lOOO

MinimumMethod DetectionResult Blank Limitug/l ug/l ug/l

u u 140U U 100U U 220U U 100U U 100.'

IParameter

Senzo(k)fluoranthene-. Benzo(a)pyrene

IIndeno (1.,2,3-ed)pyreneDibenzla,h)anthraceneBenzo{g,h,i)perylene

--1-

II

ug/l • microg~ams/liter or ppbU, Indicates a compound was analyzed for but not detected at the MOL.J: Indicates an estimated value. It is utilized when a reported valuemeets the identification criteria but the result is less than thespecified detection limit but greater than zero.

~ B: Indicates that the analyte was found in the blank as well as thesample. It indicates possible/probable blank contamination.ND: Not Determined.IND: Indeterminable

~opyright ICM, Inc., 1995.All rights reserved.

Jj

I

_J~-

12 845340053.ii£. ~~~!I!!!4l'!"'!:S""":J,!'"'!":".-,.-------------

TIERRA-B-004475

'..~:....12/13/1995 22:24 21317725898 El'NlRO CCH' INC

Ine.greied An8Iyclcell.8bor8torl ••• 'nc.273 FrwnUn RoedRandolph. N.J. 07869

201 361-4252Fex: 201 989-5289

ANAL 1'11CAL DATA REPORTfor

aa..aaI Com""-,2,." RI,,"* ,,"-Newutl. NJ 07111

~ N-.: INTERNAL MONITOaINCLab Cue NUllSbel': IIJ$O. ~

PAGE 07

..... 10: 2640-01-cn.tm: 001M.rrilllUlIi..: AqNou.t. ~IILPcK:eaI MoiICurc: 100

e-,....dQIoroIDltbllleViaJI daJvrideB1ViilUiDlldw-

COlI(.

<SO<SO<50<50<50<50< 100<50<SO<50<SO<50<50<50<50<50

Cbl~TridlI~1.1-DidII~Me4lI, __ chIori4Ie1nu·1.2·~J.l.1)~CII1orotOna1.1.1-T~c.nu. IItr1IdIIoriMl,2-Didl1OfOClCbaa....T~1.2·DidablJll'UlMDlJ

MOL CoaIpouAd

50 Bromodi~50 2~yIYiA,I"'"50 dl-l.'·DidlloropulptM50 TolueaeSO ..... 1.3-DichIot..,. ........50 1.1.1·TriehIoroeIbaeIOOT~50 DI~oromocbIDI50 0aJ0ma-- iC50 EIb,I""SO X,--. I:olIJ50 BI'OSDOfinISO 1,I.Z.2-T~50 1.3-D~50 1.4-DiddORlbeualeSO l.2·0idlJorobeueao

DUe SIImpIad: 11111J9S ..Ti_SuupW: 11:30DICe Aaalyud: 1112''"

c..:.<SO<50<SO<50<50<50<SO<502110<SO

-"100<50<50<50<50169

MDL

50SO50'050SO~5050SO

20005050SO50'0

Ye·llow -..

-845340054

TIERRA-B-004476

12/13/1995 22:24 2~1772S898 ENVlRO CCM" INC PtoGE HI

Integreted An.'ytic.' l.llboretori_. Inc.273 Frankfin AoedR.ndolph. N.J. 07869

ANALYTICAL DATA REPOItTlot

a.-ical C......... 1ac.DoT! Riy AYe.Newn.NJ me.

~ N-= INTERNAL MONlTOlUHGWIt e-N.-bcr. lllt5O...

201 361-4252Fax: 201 989·5288

< - LESSWAN M M&;OMOL c MijHoO DETECTION yMIT ;::: ___

~VOLATu.ES (BN3)LIb ED: 2640-01-Cliam: 00.MalrialUltitI; ~-IIIIL~ MoiIl:uR: 100

c........'-Nitr'olDiliMAOIGIIpIIdNM2•• ·Djaj~4-N"1b'opIMDoI2 .... Dia11rofokIeDeDibclofUnlDDiedaJlphtb.l.FllICIf-.

4-01onJph-,1

""'--"'N~4.6·Diaihv-2 ..... ylpbmalN-Nl~"'"1.2.-Di,...,..,....," ..... _4-BIOIDllpItco)'I.,.)'1cdlerH~~PbcuaIIaraIo~

eo..< 100< 100< 100< 100< 100<100< 100< 100< 100< 100< 100< 100< 100< 100< 100< 100< 100<100

MDL Coat,......IOO~100 Di...-htylpL ....100 PJuonadIeM100 8euidiae100 ~100 J.]'-DiIDIIIlylbeazid ..100 Butylt-Eylplllblhdit100 3.3'·D~100 1Har.o(.~100 CIuy_100 bit(2-Elbyl1lnrl)pbdlallcc100Di~100 B.m(bJft ........100 8cuo(k)ft1lOl'llllbelM100 8a11a(alm-100 IIIc1eDull.2.3.,...100' Di\Icu( ... )Iadu-100 Bauulr.".iJpa,1ato

0. &uapW: 11117195r.-s.mpW: 11:300-. ADal,..& : 11121f95

c... MDL<100 100< 100 100< 100 100< 100 100< 100 100< 100 100< 100 100< 100 100< 100 100< 100 100< 100 100< 100 100< 100 100< 100 100< 100 100<100 100< 100 100< 100 100

-845340055

TIERRA-B-004477

12/13/1995 22:24 21'117725898 E!'NlRO CCM" INC PAGE El9

Integrated Analytical Lebar8tarl.s. Inc.273 Ff'lInlclJnRoedRandolph, N.J. 07889

-

LIb 10: 2640-01-CIimt 10: 001MMmfUaica: ~. fAIIL..... MoiIIuro: 100

e.-pouIIlI

N-NiIroIodilOdh' ...."-olAaiIbIebi.I(2-a.JorOllth)1)1d.-2-a.loropbeaol1,:J-DkbIotObca-.1,4-Dic:hlOf'llbeazaleB.a&yllJoohol1,2·~2-Mecbylpbeaolbi.(2~i~I"'"4-Meda)'IJlIwaoIH·N~~2~_+4-~_~NiIrqh:p_IIopIaoroae,2-Nilfvpbeaol2,4-DilDKhyJflI-ol

c...< 100< 100< 100< 100496

< 100< 100< 100< 100< 100< 100< 100< 100< 100< 100m

< tOO)3SO

<100

201 361-4252Fax: 201 989-5288

MDLc ........100 bi.(2-cJa1otoc:cbox)')aIcIbaDe100 Jeugk:ci4tOO 2.... DimedaywuU-1002."D~100 1.2.4-Tric*Jocobeaz.cDe100 N.,.aw..lOO~lOOH~_100 4-OIIam-l..-hy1pMooJ100 2·.. "'yIaapIubeI ..100 HexlCblorocytlopcnCldicae100 2,4.6-T~100 1,4.SOTricUa ............loo~100 2~i~100 DUadh,IpbcW.100 2•• ·DiaiCnJtoI..100 Ac:aIIpbCIay....100

Dete s-pw: 11/11195T... SuapIed: ll:lO0. Aaalygd: 11121'"

e-c. MDL<100 100< 500 500< 100 100< 100 100< 100 100< 100 100< 100 100< 100 100< 100 100< 100 100< 100 100< 100 100<100 100< 100 1005$t0 100< 100 100< 100 100< 100 100

ANALYTICAL DATA REPORT-Owmit81 e-~-.D-7JRh .... " ...Hewatk. NJ 17101

PrvjId N-= IN1'EIlNAL MONITOllING.... c:.. NmaW; 1851·»18

MpL - MmL0[DEiE@o~ LIMrr=;:=;:===;;;;=::;;;===~<:-::JLiU TH"a m NDJaQMJVOUTILES (BNA.)

-

'f "-pUrr:

845340056

TIERRA-B-004478

12/13/1995 22:24 2017725898 ENVlRO aJlIP INC PAGE 62

Imegrllted Analytical L8borlltOri... Inc..-, 273 Fntnlclin Ro.cIR.ndolph. N•.J. 07869

201 3S1-42~2Fb: 201 989-5298

ANAL 'YTICAL DATA JUU"OIlTIiwo., ..c_ ...

D-75 Aft.Hewn. NJ 07111

.....,.. NuIe; I'YSC MONITOUIfG.....c..N..... :1""-2Qf

t.It ID : 263J.OOl- Date Sampled : 111lT,"ai.c1D:OOl n-Sulplod : &1:30ae.wullill :A.-. -".rL DaM AlllJy.d : 1JI2II95Pw-a~ 100O'pI.... ea-. Q MDL e-.paund .' c...Q MDL

Qb"''''I- <50 50 Bcomodk:bJoromedJane <50 50Y.)'J~ <30 so 1-C1a.1onMdayi Via,. Edl.- <so 50........-.- <50 50 ei.-1.3·Dic:hIoi ...... <so 50~ <50 50 Tol_ <50 50T~·"""'" <50 so ........ i.3-DicbIoc .......... <50 so- 1.1-DidIIol~I* <.50 .so l.l,2-T~ <so so- ~CWGridIr < 100 100 T~ <50 so..... l.2"Oalofort. <$0 50 DibroDxbJ~ <so so1.1~ <50 so ~ <so 50CIboIinI 53.1 ...-\, so Etbyl __ <so so1.1,1-TricIIIcIrori <50 \\\ 50 Tac.I Xyl- 260 50e.t- TIItl'IlcIIbiM <so 50 Ba-""iU <so so

~ ... 1,1-DidaIonlIdIIM_ noo- 200 l,1.2.2-T~ <50 so~ .... <50 50 1.J.DidaIoiobeu.o <so 50

TticIlIollDIdaJM <$0 $0 l,4-D~ <50 501.1-DicWus..,.utm <50 50 1,2·~ <so 50

• JlauItI rrom dihMd IImPIe anaIylb.

l.I'ID : 26~1ailIlIIlD : aolMeialUaiII : ....--IIIIIL...... NCIiIIJIN: 100

All NJDEP pruCDcDl were rollowed dutin& asWylll. T1lesc data have been reviewed and accepred by:

- ----!.Q1~.~~-LaborIIory D

1'111 Ulbility of~ "-I7tlaI ~ IDo. " I1adtId 10 a.1CQIaf COlI of ...... ,.. .... roaiiiid.N.w '''' CcftiIId a..b, 14151 .... Van c.-. t..b I 11_

845340057...,-;,,- .~---..:--.-. -::-

TIERRA-B-004479

12/13/1995 22:24 261772'5898 Ei'NlRO CD1F' INC PAGE 65

'ncegreted An.'ytlca' Labaratori •• Inc.

)ij5L - MEmoDDmCTIW LiMltSEMl\IoUflLd - lam < - lJss WAR WE PC

Metbodm1.11» ID : 2631-001Dlets-,w: UlI1I9!cu.am:OOJT_SlarpW; 1I:]()w.r.wu.r. : Acpoaa • "..n.o.te AMf)'lllllf: 11I2a.,s...... MoiiAbw: 100-

e-,.... "'t Q MOL...... < 100 1002-OIIonl,' ..<100

100 ..2....... ,,,.,...< 100 1004-Mc61I ...... <100 1002·Ni'ft.1pt II < 100 1002.4-D.... ,.,...< 100 100........ <500 500:z.4-DtcIIh CJ I Nl <100 1004.QIon).3..-"JP-ot < 100 100- 1.••~TriclaScroFt ... < 100 100..4.J·T~ < 100 1002.4-Diaicq' I < 100 1004-H1tm,' Elf < 100 1004.6-DiIIiII'O-z.-dI,."....,. < 100 100~ < 100 100

METALSEPA ___LIIb ID : 2631-001

n..a SaIpIad : 1111719.SCi..eJD rOOIr-.5ImpIld : 11:30M-WV ... : ~-1DIlL0... Aaal7IId ; 11122I9S....... M~loo

en, .. ..... Q MDLz.- 0.15 0.04ZiIIc:0.'. O.al

Q. QIIalia.

273 mnklin RoadRandolph, N.J. 01889

AHALYI1CAL D"TA.IlEPORTtw

o icoII e-I* r.:.2t-" ...."-vk.NJ 111.1

PrqJct N.... : I'VSC • MONlJ'ORINQLaIt Cue N..... : ._.101

201 3&1-4252Fex: 201 989-5288

All NJDEP protocoJ were followed durin& analyses. These data have

11w1iallil;,y of Jet p"" Aal1tie11 I.abae ....... __ .. "fed Il:I t6c1dull-e 0(" aul,.. PWlQ,iDid.-

845340058

TIERRA-B-004480

12/13/1995 22:24 2617725898 ENVIRO CCM' INC FAGE 64

Integrated An8lytica' I.8baratariee. Inc.273 Ff'entin FfoedRandolph, N.J. 07869

ANALYTICAL DATA IlEPORTtar

O .. dealc....-..-.D-7SlU ..... " ...N--*.NJmlI

ProJed ~: pvsc. MONIrOlUNGLab C_ N..... ; 1_·201

201361-4252F.~ 201989-5288

~ctEIIi1'1 ...;<;;;;.:;.,- aimAN me MoL

SDtIVOLA.TILI'.S -BASE NEDTIl.U.SMIdaodQ!

lib m : ]63 ... 1 DIlIt ...... : 11/17195ClMtID: 001 r......... : l1:lO.MItIWUaitII : ,......,..rr.. .,.,. AMI)'Dll : 111211'95.... MoiIMw: 100

c.apcIUIIII c-. Q MDL C_pouIIII C-. Q MDt.Diechyl .......... .'N-N"wn-wti"""'ylamiM < UXJ 100 < 100 100

AaiIIDe < 100 100 PI_ < 100 100biI(2-Qa1ondyo.ce-~. "411500 400 ~11-P-7W- < 100 1001.3-D~ < 100 . UIO 4-NitrolaiU. < 100 1001.4-DidaJolrolwII H < 100 100 N.NitnwvliplMay..... < 100 100JkuJll1co11al <100 100 1,1·Ci ... ylbydraiDel ...... _ < 100 100- I,%-Di~ < 100 100 ~rI1ll-)''''''' < 100 JOObI.(2~l)c:tbcr < Joo 100 H~ < lOCI 100""'~1aIIliM < 100 100 ........... < lOCI 100~ < 100 100 ~ < 100 100~ < 100 100 c..rbuM < 100 100~ < 100 100 Di.. ...,.I .. 1hIiII:e < 100 100N(Z-aa.IoroIdaoar....... < 108 100

F1____< 100 100

1,2,4-T~ <100 100 .. Mi... < 100 100N....... < 100 100 Pynae < 100 100~ < 100 100 3,3' -DimclaylbalzidiDr < 100 100~ < 100 100 lulJlbeur1 ..... < 100 1002-Madl' .... aw.. < 100 100 3,3 '-DIdaIOI'!"'-vid_ <100 100H~JCIopIa"" < 100 100 Beao(.~ < 100 1002~~ < 100 JOO au,- < 100 100Z·N~ < 100 100 biI(2.~yI)p'dltal'" 107 100Di.-laylph+,* < 100 100 IJi..tl.octJIpkh". < 100 1002,6oDiGiCtOli01ucDo < 100 100 1euo(1l]1IuocwIIbcDc < 100 100N-MpIIlhy'" < 100 100 8euD(i:)ft....,... < 100 1003-N-...w. <100 100 8eaal(.1P7- < 100 100.~ ... . < 100 100 ..... 1.2,3~ < 100 1001,~ < 100 JOO Da-z(.......... .< 100 100D11lIaIDfunIa < 100 100 BIazofI.hJlIer7I- < 100 100

Q - QgIIifiw• :- ..... t tn- diMDd "')'IIie.('cwd ......... _ .....

-Hew yadt CMiW lAb, 11_

.~... 845340059

TIERRA-B-004481

Integrated Analytical LabaMmJries.l Inc.273 Franldin RoadRandolph. N.J. 07868

ANALYTICAL DATA REPORT"for

Chemical Compounds Inc.2.9.75 Riverside An.Newark, Nl 07101

Project Name: SELF-MONITORINGLab Case Number: 10950-171'

201 361-4252Fax: 201 888-5288

MDL - METHOD DETEcrJON LIMIT < - LESS WAN WE MBE"

Date Sampled: 8/9195TlU10Sampled: 11:00Date Analyzed: Q715195

'" Cone. MDL< 100 100< 100 100<100 100< 100 100< 100 100< 100 100< 100 100<100 100<100 100< 100 100< 100 . 100< 100 100< 100 100.:::100 100< 100 100< 100 100

Lab ID: 1719-002C1i1lllt 10: 002MatrixlUnits: Aqueous - ,.alL

Compound

ChloromethaneVinyl chlorideBromomctbaaeChloroedwaoTricbloroflu.oromedJaae

• 1.1-Dichloroe~Methylene chloridetnlaa-l.2-Dichloroetheael.l-DichloroetbaDeChloroform••••• -TrichloroetbaDeCarboa tetrachloride1.2-DichloroetbaDeBeaz.eTrichlol'Oetbeoe••2-Dich10r0propaoo

Cone.

< 100< 100< 100< 100< 100< 100<200< 100<100<100< 100< 100< 100< 100< 100< 100

VOLATILES

MDL Compound

100 Bromodichloromcthanc100 2-Chloroethylvinyl ether100 cis-I,3·DichJoropropene100 Tolueoe100 tnlDS-l.3-Dichioropropeoe100 l.l.Z-Trichloroethane200 Tetnchloroetheae100 Dibromochloromcthanc100 ChJorobenmae100 Ethylbeazeae100 Xylenes. JO(aI100 Bromoform100 1.1.2.2-Tetndlloroethuao100 1.3·Dicb1orobcnzene100 1.4-DichJorobeazeae100 1,2-DichlorobeDzeue

TENTATIVELY IDENTD'IED COMPOUNDSLab 10: 1719-002CIieut 10: 002MllrWUnits: Aqueous - ,.elL

COMPOUNDESTIMATED

CONCENTRATION

146000... -.;'; .:-::- - ~-._-_ ..... _~.- ._-

Date Sampled: 8/9/95Time Sampled: 11:00Daac AaIl)'Zlld: 8115195

RETENTION11MB

5.82

-

New .eney ee.tified 1.IbI·1415l.

845340060New Volt Cenified Lab I 114a1

TIERRA-B-004482

Integrated Analytical Laboratories, Inc.273 Franldin RoadRandolph. N•..!. 07869

201 361-4252Fax: 201 989-5288

"ANALYTICAL DATA REPORT·for

Chemical Compounds IDe.29-15 Riverside Aft..Newark, NI 07101

Project Name: SELF-MONITORINGLab Case Number: IOJSO -1119

MOL -= METHOD PETECTION LIMIT

-

Lab ID: 1719-002Clieut ID: 002MatrixlUaits: Aqueous - PIlL

Compound

N-Nitrosodimctb.ylaminoPhenolAniliaobis(24:hloroethyl)etber2-chloropheool

.• 1,3-DicbJoroboaz.eae1,4-DichlorobenzeaeBeazyl alcohol1,2-DicbJorobeozeoe2-MethylpbeDolbis(2-eh1oroisopropyl)ether4-MethylpheaolN-Nitroso-d.i-n-propylamiue2-Amioocolueao +4-AmiDotolueuoHeuchloroetbaneNitrobe&w:GeIsophoroae2-Nitropheaol2.4-Dimethylpbeaol

CODC.

< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0

BASE NEUTRALS ACIDS

MDL Compound

160.0 bis(2-Ch1oroethoxy)meChaoe160.0 Benzoic acid160.02,4-Dimetbylaaifule160.0 2.4-Dichlorophenol160.0 1.2.4-Trichlorobenzeac160.0 Naphlhaleno16O.04-ChloroaniliAc160.0 Hexachlorobntadieae160.0 4-Chloro-3-methylpbeool16O.02-Mctbylnaphtballllle160.0 Hexachloroc:yclopentadialc160.0 2,4,6-TriChloropbeaol160.0 2,4,5- Trichloropheaol16O.02-QJoronapbtbaieae160.0 2-Nitroaniliac160.0 Dimetbylpbtbalato160.0 2.6-Diaitrotolueae160.0 Acenaphthyleoo160.0

< - LESS THAN WE MOL

.'Date Sampled :

Time Sampled :Date Analyzed :

Cone.

< 160.0< 800.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0"S 160.0< 160.0< 160.0< 160.0< 160.0

8f919511:00ai1S195

MDL

160.0800.0160.0160.0160.0160.0160.0160.0160.0160.0

'"160.0160.0160.0160.0160.0160.0160.0160.0·

Continued OD aoxt pap.

845340061New York Certified Lab I 11402

TIERRA-B-004483

· ,

Integra~ed Analytical Labar_aries, Inc.273 FrankJin RoadRandolph. N.J. 07869

-ANALY1lCAL DATA REPORT-for

Cbanical Compounck lac.29-75RiYerside AYe.Newark, NJ 07101

Project Name: SELF-MONITORINGLab Cue Number: 10950 - 1719

201 361-4252Fax: 201 988-5288

MOL - METHOD DEIE£JJON UMIT < - LESSJHAN WE MDL

Labm: 171~Client m: 002MatrixlUaits: Aqueous - JIoIIL

Compound

3-NitroanilineAcenaphtbeae2.4-Diaitrophenol4-Nitl'opbeool2,4-Duutrotol_

.• DibeazofunaDietbylpbthalateFlllOreao4-Chloropbeoyl-pheDyletbet4-NitroloiliDe4.6-Diaitro-2-mctbylpbeaolN-NitrosodipbeoytamiDa1,2-0ipbmylbydtazine/ .Az.obeauae4-BromophClDyl-pbenyletberHeucblorobeazeoePentachloropbeaolPhenanthreDeAntbnceao

Cone.

< 160.0< 160.012100

< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0<:: 160.0< 160.0< 160.0

BASE NEUTRALS ACIDS

MOL Compound

160.0 Carbazole160.0 Oi-a-butylphtbalate160.0 FluorauthcDe160.0 Benlidine160.0 Pyreae160.0 3,3':Dimetbylbenzidine160.0 Butylbenzylphthalate160.0 3,3'·DicblorobeazidiDe160.0 Benzo(a)a.albrlceDe160.0 Chryseue160.0 bi~·EtbylbCll.yl)pblhalate160.0 Di-a-octylphthalate160.0 Benzo{b]Ouorantheao160.0 Bemo(k]Ouorautbeae160.0 Beazo(a]pyreae160.0 IDdeao{l.2,3-ed]pyreae160.0 Diben%ia.b]aathneeoe160.0 Bcoz.o[g,b.iJperyleac

"

Oate Sampled :Time Sampled :Date Analyzed :

COlIC.

< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0.: 160.0< 160.0< 160.0< 160.0

81919511:0011715195

MDL

160.0160.0160.0160.0160.0160.0160.0160.0160.0160.0

'·160.0160.0160.0160.0160.0160.0160.0160.0'

All NJDEP protocol were followed during analyses. These data have been reviewed and accepted by:

-'845340062

New Yort Certificcf 1M , 11402

TIERRA-B-004484

k="'. nti.ige"'c:ed_-' Labs

Integrated Analytical Laboratories, Inc.273 Franlc&n RoadRandolph.N.J. 07868

<\N'ALYJ'ICAL DATA REPORT"for

Chemical Compounds IJJc.29-75 R1.,erside Aye.Newark, N1 01101

Project Name: SELF.MONITORINGLab Cue Number: 10950 .1719

201361-4252Fax: 201 889-5288

MOL"" METHOD PETECTION LIMIT< • LESS THAN wi MDt

Date Sampled: 8/9195Time Sampled: 11:00Date Analyzed: 8115195

t Cone. MDL< 100 100<100 100<100 100< 100 100< 100 100< 100 100< 100 100< 100 100< 100 100< 100 100< 100 . 100<100 100< 100 100i:: 100 100< 100 100< 100 100

.-

Lab ID: 1719-001C1iCllt ID: 001M.uuIUDits: Aqueous - p.gIL

Compound

ChloromethaneVinyl cblorideBromomethaacChloroeibaneTricbJoroflllOrometbaoe1.I-DicbloroetbeDeMethyleoe chloridetnms-I.2-DichloroelbeoeI.I-DichloroethaDeChloroformI, I .1-TrichloroetbaDeCarbon tetracb10ridel,2-DicbJoroethaaeBea.zeneTrichloroetheae1.2-DichioroproplDCl

Cone.

< 100< 100< 100< 100< 100< 100< 200< 100< 100< 100<100< 100< 100< 100< 100< 100

VOLATILES

l\IDL Compound

100 Bromodichlorometbano100 2-ch1oroethylvioyl ether100 cis-l.3.0ichloropropene100 Tol_100 k1IILt-l,J-Dichloropropeac100 l,l,2-TricbJoroethaao200 Tetraehloroetheae100 Dibromochlorometbanc100 Chlorobeueae100 Ethylbenzeae100 Xyleaes. ~taI100 Bromoform100 1,I,2.2-Tetladdoroedulce100 1,3·Dichlorobenzeae100 l,4-Dichlorobeozenc100 1.2·Dichlorobeazeoe

TENTATIVELY IDENTIFIED COMPOUNDSLab ID: 1719-001C1ieat ID: 001MatrixlUDits: AqllClOU8- p.J!L

COMPOUNDESTIMATED

CONCENTRATION

158000

Date Sampled: 819195Time Sampled: 11:00Date Analyzed: 8/15195

RETENTIONTIME

5.76

- - Cootinued OG IICJlt a-p.

845340063New York Ccrti&cd Lab I U-4QZ

TIERRA-B-004485

'0 •• , ••••

I~~f:ed~

Integrated Analytical Labaramries, Inc.273 Franlcfin RoadRandolph.N.J. 07868

201 361-4252Fax: 201 988-5288

~ALYTICAL DATA REPORT"for

Chemical Compounds Inc.%9·75 RiYe:rslde Ave.Newark, NJ 01101

Project Name: SELF-MONITORINGLab Case Number: 10950 - 1719

MpL - METHOD DETECTION LIMIT < - LESSTHAN WE MRt

Lab ID: 1719-001.Client 10: 001MatrixlUnits: Aqueous - 1&&11..

CompoWld

N-NitrosodimcthylaminePhenolAnilinebis(2-ehJoroethyl)etber2-eh10r0pbeaol

~ 1.3-Dichlorobeazeue1.4-DichlorobeDzeDoBalzyl alcohol1.2-DichlorobeGzeae2-Methylpheaolbis(2..QJJoroisopropyJ)edIer4-MethylpheoolN-Nitroso-di-a-propyl&miDe2·Aminotolueao +4-Amiaotol_HexKhloroetlwaoNitrobenze:uelsopborone2-NitropheDol2.4-Dimethylpboao1

Cone.

< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0

BASE NEUTRALS ACIDS

MDL Compound .'

40.0 bis(2-CbJoroetholly)methane40.0 Benzoic acid40.0 2.4-Dimelhylanili.ae40.0 2.4-Dichloropheool40.0 1.2.4-Trichlorobenzcne40.0 Nllpf.thaleoo40.0 4-CbloroaniJiao40.0 Hexachlorobutadieno40.0 4-chJoro-3-mcthytphenol40.0 2·Melhylnaphthaleuo40.0 HexachJorocyclopeotadiene40.0 2.4,6-TrichJorophenoi40.0 2.4,S·Trichlorophenol40.0 2.Qdoronaphthalene40.0 2·NitrouiJiDo40.0 Dimethylpbthalate40.0 2.6-Diaitrotolueoe40.0 Acenapblhylene40.0

Date Sampled :Time Sampled :Date Analyzed :

Cone:.< 40.0< 200.0< 40.0< 40.044.2

< 40.0442

< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0<: 40.0< 40.0< 40.0< .w.0

8/919511:00AllSI9S

MDL

40.0200.040.040.040.040.040.040.040.040.0

-·40.040.040.040.040.040.040.040.0"

Coatinued on next paee.

-New Jaw)' C«tifiod LablJ47S1

845340064

New Yort Ccrtifiod Lab I 110402

TIERRA-B-004486

. ::". ....: ..

~. Lab.,-

'nt;egrated Analytical Labarataries, Inc.273 Frantnn RoadRandolph. N.J. 07869


Cbemic:al Compounds Ine.29-15 Riverside A"eoNewark. Nl 01101

Project Name: SELF-MONITORINGLab Case Nwnber: 10950. 17"

201 361-4252Fax: 201 989-5288

MOL,. METHOD DETEClJON yMlT < - LESSTHAN WE MDL

Ub 10= 1719.()()1Clicat 10: 001MatrhlUaits= Aqueous - IliILCompound

3-NitroanilideAceDlIphtheDe2,4-Dinitrophonol....NitropbolloJ2.4-DiaitrotoIUCIUI

• DibeozofunD'DietbylphtIWateFllIOreoe4-Qlorophenyl-pbeoylether4-Nitroaniliae .. -4.6-Diaitto-2-methylpbeoolN-NitrosodipheDylamiDe1.2-DiphraylhydraziDel Azoheazouo4-Bromophenyl~hraylothotHeuchlorobelwlaePentlclJloropbeaolPbcaaothraloADthraceoo

CODe.

< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< .w.0< 40.0< .w.O< 40.0< 40.0< 40.0

BASE NEUTRALS ACIDS

MDL Compound

40.0 Carbazole40.0 Di-o-hutylphtbalate40.0 Fluol'8lltbllDe40.0 Benzidine40.0 Pyrepe40.0 3.3'·Dimetbylbenzidino40.0 Butylbenzylphtha1ate40.0 3.3 ··Dichlorobenzidine40.0 Benzo(a]anthracoao40.0 Chrysoao40.0 bis(2-Etbylboxyl)phtbalate40.0 Di-o-oc:tyiphtbalato40.0 Beom(b]tIlIOrandaeno40.0 Benzo(k]tIuorantheoe40.0 Benm(a]pyreno40.0 Inde:llo[l.2.3-ed]pyreae40.0 Dibenz(a.h)anthraceae40.0 Benzo(g.h.i]poryleao

..Date Sampled :

Time Sampled =Date AnalyUld =

Cone.

< 40.0< 40.0<40.0< 40.0< 40.0< 40.0< 40.0<40.0< 40.0< 40.0< 40.0< 40.0< 40.0<:: 40.0< 40.0< 40.0< 40.0< 40.0

819195H:OO8/iSJ95

MDL

40.040.040.040.040.040.040.040.040.040.0

"40.040.040.040.040.040.040.040.0"

AJ) NJDEP protocol were followed during analyses. These data have been reviewed and accepted by:

-'-New 1eneY c'c1tifiod LaW: 14151. , "

845340065New Yorlc ~ LIb 111402

TIERRA-B-004487

Ii',·n~e9ret.d

elyt'cel_ . . Leba

Integrated Analytical Laboratories, Inc.273 Franklin RoadRandolph.N.J. 07869

201 361-4252Fax:201 989-5288

ANAL mCAL DATA REPORTfor

Chemical Compounds Inc.29-75 Riverside Ave.Newuk, NJ 07101

Project Name: IntemaJ MonitoringLab CllSe Nwnber : 10950 - 1439 NorD

VOLATILES - (601/602)< = LESS THAN WE MDLMOL = METHOD DETECTION lIMIT

Lab ID : 1439-001-Client ID: 001MatrixlUnits : Aqueous - ",glL

Compound Cone. MDL Compound "Chloromethane < 50.0 50.0 BromodichloromcthaneVinyl chloride < 50.0 50.0 2·Chloroethylvinyl etherBromomethane < 50.0 50.0 cis-I,3-0ichloropropeneChlorocthano < 50.0 50.0 TolueneTrichlorofluoromethane < 50.0 50.0 trans-! ,3-DichJoropropene

~ l,l-Dichloroethene < 50.0 50.0 1,1,2-TrichloroethaneMethylene chloride < 100.0 100.0 Telrachloroethenetrans-I,2-Dichloroethene < 50.0 50.0 DibromochloromelhaneI,l-Dicbloroethane < 50.0 50.0 Chlorobenzan"Chloroform < 50.0 50.0 Elhylbenzenel,l,l-Trichloroethane < 50.0 50.0 Xylenes, lolalCarbon tetrachlorido < 50.0 50.0 Bromoform1,2-Dichloroelhane < 50.0 50.0 1,1,2,2-TelrachloroelhaneBenane < 50.0 50.0 1,3-DichlorobeuzeoeTrichloroethene < 50.0 50.0 1,4-Dichlorobenzenel,2-Dichloropropane < 50.0 50.0 1,2-Dichlorobenzene

Date Sampled: 7n195TilDll Sampled: 14:00Date Analyzed: 7/12195

Cone:. MDL

< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0

TOTAL CYANIDE

Lab ID : 1439-001Client ID : OOt ~~MatrixlUDits : Aqueo 6

NOpp Date Sampled :

TUDe Sampled :Dale Analyzed :

7n19S14:007{12195

Result MDL

< 0.05 0.05 •


The liability of Integrated Analytical Laboratoria. Inc. is limiled to the actual cost of the analyses performed.

New Jorscy ~rtiticd Labl147S1 New Yolt Certified Lab , 11402

TIERRA-B-004488

Integrated Analytical Laboratories, Inc.273 Franklin RoadRandolph. N.J. 07888

201 361-4252Fax: 201 989-5288

ANALYTIC At. DATA REPORTfor

Chemical Compounds Inc.2'-75 Riferside Aye.Newark, NJ 01101

Project Name: Self-MonHorinlLab Cue Nwnber : 10950 • 1438

BASE NEUI'RALSMOL - METHOD DETECTION LIMIT < .. LESS THAN THE MOL

Lab 1D : 1438- 001Client 1D : 001MatrixlUnits : Aqueous - "IlL

CompoW1d

N-NitrosodimethylamineAnilioebis(2-CbJoroethyl)ether1,3-Dichloroben7.eae1,4-0ichlorobenzeaeBenzyl alcohol1,2 ·DichlorobeDZeDobis(2-eh1oroisopropyl}othorN-Nicroso-di-n-propylamineHexachloroethaneNitrobcuz.oneIsophoronobis(2-Cb.1oroethoxy)1DIlChane1,2,4- TrichlorobenzaleNaphtbalooo4-ChloroanilineHexachlorobutadiene2-Mechylnapbtba1eneHeuch1orocyclopeacadiene2-CbJorooaphthaiene2-NitroaoiliDoDimethylphthalace2,6-DinitrotolueneAconaphthyleae3-NitroaniliDeAcenaphtheno2,4-DinitrotolueoeDibemofuraa

Dace Sampled: 7n19STime Sampled: 14:00nate Analyzed: 7/tS/9S

Cone. MDL Compound .'

< 50.0 50.0 Diothylphtbalate< 50.0 50.0 Fluorene< 50.0 50.0 4-Cblorophenyl-phenylechor< 50.0 50.0 4-Nicroaniline< 50.0 50.0 N-Nicrosodipheaylamine< 50.0 50.0 1,2-DipbenylhydrazinelAzobenzeae< 50.0 50.0 4-Bromophenyl-phenylether< 50.0 50.0 Hexachlorobenzene< 50.0 50.0 Pbonanthmle< 50.0 50.0 Anthraceno< 50.0 50.0 Carbaml0< 50.0 50.0 Di-n-butylphthalaCc< 50.0 50.0 Fluoranthene< 50.0 50.0 Benzidine< 50.0 50.0 Pyreoe< 50.0 50.0 3,3'-DimethylbellZidine< 50.0 50.0 ButylbeazylphdJalate< 50.0 50.0 3,3'-Dichlorobeazidine< 50.0 50.0 Benz.o[a]aolhncea1e< 50.0 50.0 Chryseuo< 50.0 50.0 bis(2-Ethylhexyl)pbthalaCc< SO.O 50.0 Di-a-o<:lylphthalace< 50.0 50.0 Benzo[b)fluoranthene< 50.0 SO.O Beam[k]fluorantheao< 50.0 50.0 Beazo(a)pyreao< 50.0 50.0 IDdeao(l.2.3-cd]pyreoe< 50.0 50.0 Dibeozla,h]anchraccao< SO.O 50.0 Benzo{g,h.i]peryleae

Cone.

< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0

MDL

SO.O50.050.050.050.050.050.0SO.O50.050.050.050.050.050.050.050.050.0SO.OSO.O50.050.050.050.050.050.050.050.050.0

All NJDEP protocol werc followed during analyses. These data havc been reviewed and accepted by:

Ichac •Laboratory D'

The liability of Integrated Analytical Uboratories. IDe. is limited to the actual cost ofCho aoa.Iy_ performed.

New ler1C1CertiJiod Labl14'1S1 N_ York CertifH:d L.b , 11402

TIERRA-B-004489

Integrated Analytical Laboratories, Inc.273 Franklin RoadRandolph.N.J. 07869

201 361-4252Fax: 201 989-5288


Chemical Compounds Ine.29-75 Riyerside Aye.Newark, Nl 07101

Project Name: SeIf.MonitoringLab Case Nwnber : 10950 - 1438

MOL ... METHOD DETEcnON LIMIT

ACIDS< - LESS THAN MMpt:

Lab ID : 1438- If>1Client 10 : 001MatrilllUoits: Aqueous - PIlLCompound

Phenol2-ChJoropheool "2-Methylpheool4~Methylpbeuol2·Nitropbenol

.. 2,4-0imetbylpbenolBcazoic acid2,4-Dichlorophenol4-ehJoro-3-metbylpbenol2,4,6- Trichloropbenol2,4,5- Trichloropbenol2,4-0initropheool4-Nitrophcaol

.4.6-Dinitro-2-methylphenolPencaehloropheaol

Date Sampled: 7n195Time Sampled: 14:00Date Analyzed: 7/N19S

/

Lab m : 1438- 001Client m : 001M~ruuuoiu:~·J.l11LCompound

pH

Result Q MOL .'< 10.0 10,0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 50.0 50.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0

pHlCorrosivityDate Sampled : 7n195Time Sampled : 14:00nlte AnaI)'ZIld : 1/13195

Result MDL12.58 t.02

All NIDEP protocol were followed during analyses. These data have been reviewed and accepted by:

.-The liability of Intepted ADalytic:al Laboratories, Inc. is limited 10 the aceuat cost of the lDa1yses performed.

New Jersey CdrtirlOd Ub' 147'1 New York Certified Ub 111402

TIERRA-B-004490

.. ~t:;E NJIER- PlE NJIIER

fA FILE11.100 IW£FIElJ) tD

ACCREDITED l.ASCRAllRIES INC.UWlTlLE ~IC ~YSIS DATA

27139i0701l>AJ114a:I

CAS •....................................................................................................................107028107m7487374839]liQ14i".iODJ]Ii 092676417H50]li694]liJ"4m43156605676631070627893371556__ ~3"

'0'4.14

AcroleinAcrylonitril.OIloro.thlna8rOlOMthllleVinyl OIlarideO1laroethllleMethylene ChlorideAcetoneCarbon DilulfiiJeTrichlorofluoroMth.nel,l-Dichlora.thenel,l~ichloroethlnetrant-l,2-DichloroetheneChiara tor.l,2-Dichloroethlpe2-&tlllonel,I,I-TrichioroethaneCarbon TetrachlorideVinyl Acltate8rolOdichioroiethane

uuuuuU

32 WUUUUUU

41 W50 W54

UUU

J1 iii

SURBOGATE t:IJAlH)S1,2-Dichloroethene-d4Toluene-d88rolO'luorabenzene

J - Indicate. calpound concentration found below noLoU - Indicates CQlpound tnalyzed tor but not detected.

61

"202020201018

4.04.04.84.04.D4.0U4.84.0U8.04.0

/lATRIXDILUTlll4 FfCT(R __ -..111 _

OATE EXTRACTEDOAT£ ~VZEDA/oW. 'fZED BY

AgurpYI10

O6IQ2M

to. CAS t........................................................... .788i'510061815791167143212448179005100610261lO]li8]Ii~259178610810112718479J45108883101i907100414100425m0207'5476156592

1,2-Dichloropropanlcis-l,J-Dichloropropen.TrichloroetheneBenzeneOibrolGchloro .. than.1,I,2-Trichlora.thanetr.n.-l,J-Dichloropropene2-Chloroethylvinylether8rolOta ...2-Hexanon.4-Hethyl-2-pentinoneTetrachlotoethene~1,1,2,2-Tetrachloro.thaneTolueneChlorobenzeneEthylbenzen.Styrene.,p-XyI eneo-Xylenecil-l,2-0ichlotoethen.

LInus76-11488-110

.86-115

uuUUUUUUUUUUU

17UUU

"UU

4.04.04.04.04.04.04.020

4.09.07.04.06.05.04.0

104.02821

4.0

B - Indic.tes coapound found in al5aci.ted blink.W - Result exceedl specific ground water qUllity criteri •••

• Flag. ar. bal.d on Specific Ground Water Qu.lity Criteria fro. Hew Jert.y Register dated February 1, 199J •

.-845340069

TIERRA-B-004491

'lI5E IfJfIlER!:iAI1II.f ItJ'IlERDATA fiLEQ.I ENT HAI'£Flao 10

2m

ACCREDITED LAlmATlJUES, lit:.IIfA lRANlC lM-YSIS DATA

>F18?'i'JI'iU701l

0:1

..................• ~ ~ _ .

.................................... M .

11189S2'JlSS789,4117lU1U'.I481/}lj5lU'.i6791108J2111444,41nllU64/)711111516\lS~U110860162164767n1'IllY."~?i91.$1)5011191112UII'll~120J10647118768''JllS7677474"'IS871I117441311132181'68YYl1'J'llIm9U26496U62U2

Phenol2-01lorophenol2-l1et~~lphenol}&4-Methylphenol2-Nltrophenol2,4-0ilethylphenol2 ,4-Dlchlorepheno Ihis(-2-Chloroethyl)Ether1,,-Dlchlorobenz!"e1,4-0ichlorobenzeneSenzyl Alcotlol1,2-0ichlorobenzenebls(2-Chlorollo~ropyllether~itroao-Di-n~propyla.lneHexachloroethaneNitrobenzeneIsophoroneBenZOIC Acidbis(-2-ChloroethoxyIMethane1,2,4-TrlchlorobenzeneNaphtha lene4-thI oroani lineHexachlorobutadiene2-MelhylnaphthaleneHexachlorocyclopentadlene2-Ohloronaphthllene2-NI tr"ni IlneDiMethyl PhthalateAcen~ht hy I.ne'-NitroanJl illeAcene!1htheneDibenzofuren2!6-Dlnitrotoluene

uuuuuuuuuuuUlJUUUUUUUUUUUUU

100 JUUUUUU

AQu,ou,IlATRIXDIWT1l1l FACTtR __ ~~~ _IlATE EXTRj:CTEDDATE AHALVZEDAtW-YZED BY

,8504M06/17M

. .10.. ..

505050505850511,050500;0,U50

"505050

2'1U50'105111)0505050SO

25050150

2'iOSOSO50

m07BBD6295954mBS1011827S'4S21978651211429466270u572}8m7lOU0168630610155311B7418501812012784742206440129000856879194156553117817218019l1i'l140205"22070895mB19m5SJilGJ19124262Jl19

4-Chloro-J- .. thylphenol2,4,6-Trichlorophenol2,4,5-Trichlorophenol2,4-Oini trophenol4-Nit ropheno I4,6-Dinitro-2-18thylphenolPentachlorophenol2,4-0initrololueneOlethylphthalate4-Chlorophenyl~phenylelherFluorene •4-Hi troani Iin'N-Hitroacdiphenyla.ine4-8roMOP~enyl-phenyletherHexachlorobenzellePhenanthreneAnthreceneDi-n-ButylphthaleteFluoranthen.PyreneButylbenzylphthalete',"-DiehlorohenzidineBanzo(alAnthrlClne8i,(2-EthylhexyIIPhthelateChryaeneDi-n-octyl phthalate8enzo(bIf luorantheneBenzo(klFluotantheneBenzo(a)PyreneIndeno(1,2,J-cdIPyreneOibenzo(e,h)AnlhreceneBenzo(g,h,i)Peryl.neN-Ni trOlod i..thyla.ine

uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu

51SO

2S0no2502S0250,0

50SO50

2505050SO1)050501)01)050

10050,0505050505050SO5050

$IfflI5A1E C!J'f!J.HlSIIltrobenzene-d52-FluoroblphenylTerphlnyl-dl4Phenol-dS7-FluorO!JhenoI2,4,6-TribrD.aphenol

.-. J - Indicetl1l CllllpOllnd concentrehon found below 10.._ : _ 11141Icatea cOllpol,llldanelyzed for but not detected •

I!EtlWY .JJll1Ii. ...s:ra:wL~ , 35-114 ..IL--ll' 4J·116 -1IL-ll' H-141 ..J&lL--U " 11- 94 -L-UZ I 21-108 ....fIll...

.......... HOT DETECTED ....8 - Indicatel cOlpound found in aaaocieted blink •W • Reault exceeds epeci'ic ground weter quality criteria.-

• FlailS are bend on Specific Ground IMter lkJality CrIteria fro. New Jersey Regilter dated February 1, 199J... '-l1ethylphenol Ind 4-Methylphenol can not be ..pareled by the _thod applied

845340070

TIERRA-B-004492

-

ca.. ItS~l •• :Clfent 11_:FI.ld IIU111bert

ANAlnES

ACClEDlTED lABCIUTDIUES, INC.GENEIAL CIlatISTRY ANALYSIS DATA

zn325°7011eCI1Epf,J

IESULTS IIlL IIIfTS

...

tIIItrlx;D.t. ReceIved: -..lI:u.JIUJ:i- _

DILUTJDIIFACTOR

0'J112195

METIKD lLAIIIC1E5lI.TS IIlL

AIlALYSISDAn

Cyanide, Tat.l 05123195lID 0.01 IIWl 1.

..

lID 0.01

845340071

TIERRA-B-004493

845340072

TIERRA-B-004494

CONCRETEPAD .. ,.,- _- .ASPHALT

PAD HazJNon-Hu.Waste Storage

STORAGEAnA

STORAGEAREA I!

:IFilterPress

STORAGEAREAOFFICES

~

~BATHROOM

LAB 0/ -----.;..---

5RotaIy Vacuum

DryerElevator

TOSECONDFLOOR15001;310

TreatmentTank

oO lSoogal.10,000 gal. TreatmentW.Water Tank

Tank DikedArea

8o Shed-Location of

Empty Drums

cm;MICAL COMPOUNDS INC.29-75 Riverside Ave.Newark N.J. 07104

( ( {

TIERRA-B-004495

---"" - -._._---~-_._-_._--- ~-------~._.._-~~~~...... _-- ~-_._.--..._~._---~_... _---- ~

845340074

"TIERRA-B-004496

ConcretePad forStorage

OFFICES

BATHROOM

RAMP to Basement LAB

Loading&:Unloading

Pock .....................<.

DnfnWaterOut- Sat to10tOOO gallonStoraae Tank

CHEMICAL COMPOUNDS INC.29-75 Riverside Ave

S'

WASTE WATER PLANT

DraiD Water'It---Ia

StQrage Tank forAfter Treatment

PRODUCTION AREA

ALL PROCESS &: DRAIN WASTEWATERTRANSFER TO A HOLDING/STORAGE

TANK THEN TO SAMPLE POINT INBASEMENT AND THEN IS PUMPED our

OF BUllDING TO SEWER

Wastewater Out -to Samp.liD& Pointfor Discharge to

Sewn

ProcessWutewater ID -

from Production toStorageTaDk

After NecesuryTreatment

--:: 0:>.0Sanitary/'l

WasteMter 0Collection :

User Cha.rge~ [Pretreatment. *I&: Local Limit ~

SamplingPoint

To Manhole Tie-InApprox.70ft.

(4tOOOgal Storage

Tank for AfterTreatment PASSAIC RIV(

AcUacentBldg. #7

(

TIERRA-B-004497

-__ .•• .J<_. _ .••... _. .

845340076

TIERRA-B-004498

......

- ;.

~. ~~.

Jeruay Dop~rtmQnt ef Snviron~eDtAl Proteotion an~oivision or Re8p¢ns1ble Pa~ty site Re~edi~tionUureau or Emergency RespQnse

Region I

.;".;.. i: '.'.?-Q.1-()7-·'IJ·.2!".File;: 0714

P?\C CODE: 'l'F~" " .:\.

;:6

·":1·.. ,;:;ti9ator: "Natthe..., Garamona. Christopher Gibbons

.,Lcga~iQn: Chemical compounds, Inc.i\t1drS':)s:: '29-75 lUverside Avenue

:/" l'fewaX'K, NJ

Time ~rrive~: IllSTime Doparted: l~OO

•. .._., '""",..,;-.:

~~'1::1·.1n.~1.blepar"ty1.· Chemical com~ounds, Inc.:.~:: ':.'1'-; l'.ddress: 29-75 River.slde Avenue

tlel,,·a.rk, NJ

1)"L'pt:. Rep: Bob Swales - Newark OEM

of Complaint: Opet'"o Piccitto - NJSPN<I'l:ina Buteau

.i/i.t201-733-366"' .. "~It"201~5"a-a17J' ,..... I!:

.",',(f~.;:'; Ii:Cof Complaint; Unknown liquid tleinq cUscharged front pipe onto:'~~\~b::-~-..Fa;~d into Passaic River at incident locatioh. ,/~(~~~-;::,l~"

Phone /I

-=~~~iQn Phon~ I: 201-485-3211

Phone II

c-,- ,

to.. '. ~.....

,~.~~~.~;-~1~~~.:~;.... ":~I':" ~~.;')

TIERRA-B-004499

;....~,.

".: :':-'.'0: of; dark," : ~,.~:.'~ Ri ver,:;:~:.;hi:'~: \.1:) •

..,. .",:'" 1Compouhds, I no. manufa cturos hai r dYes, In 1>0rt i eur.r, th,",:

: j 2::r has bQen [Jl'odl.lcing red #'3 and He-blue '2 hair dyes, 'l'hQ dark,-.,'1·"' iquid obsa.t"vcd (Jf1 the qround around the outside of the,:,!;.r>:. '

.,-:i 1H:( 10 at t r.lbuted to tho. e t \{O dyes • The hc il ity • ~are 5 i ts ~?::.I". ',~uid frem tn.i. proce.se, in a 5,500 gallon cap.a.ty tanker:c

' :::~ In t)"l t"12.:.t't'of the f~lCility. Ois,posal of this material is ' .:',_";"1!: I.~l\emical hro:tsr.,~ l'l:ln,lgal1lent ......hich 10anifests the waste as a ' <,.

.... ~-:1I1::'''l"dOll':i pro(~,~S';; liqu.id n.<;>.$, Prior to recycling r.tElth~nol in,,r,':";'~'' .::' •. :).'·"':;Q;':S:OI;', the' f'M:llll:.y arso disposed Of waste methanol th1:'OU9h ',.' ":':.'\1 ['·,'J~·;tE! 1·1:,I1:II.1'.';:1r<l11: ilnd had an EPA generato!:' n~~mbtir:<"Jsslqnerdto" : :'''. ~!.tt,y (.jI!UD In ··l;<'3-:~ '1'37). The facility maintains tl tank(lr"-. ~.!,: ',1:' :netn(~n~_'l '?Il-:iilt..: with a c:a~acity of 4,000 qal!ons for their

., .:... FL·Jor drC\.iIl::l at. the faci1~ty dischar9Q into the sanitary,_. ":-l: ,·~vstem accor<:li119 to ~fr. Celleri. The facility, rowever', has no'

t;,,;t'lr.i t from pvsc to dlScharge any material (rom theit"l'rocessas into~:-:;:;!:l:'l:-:tarvline.

",,"" ~ndO~ff Ond Kir.ah<>or "ent to Clara Maa. Ho.pit.l in BeUevni.d~e to chernical~exposure at the incident location. In addition, 8 ,',';';:'01 !;""'d at he Hao -Greco Co. ad acent to the IncIaen€ "o_Gc"t ••• ieal attent.on for ChOh.ca .x a,ur. a r. .r •. edic'l~~

~=~U? 1n Pearny. nves gators from the Esaex County Prosecutor's .~'fJ~~ and the Division of Criminal Justice also perfor~ed ~n~~stigation of this incident. Invest ato ~ ..:.:':s::l~d a NOV to Chemical Com "i. , 'r:,-~n··::cl::1f cataon of a dlsc ar Of a I t uant to ...... .-~",--.,cdt act, Tho faci titv contnat.d ENSI , Inc, of Ne"erk to ' ..-..h',,. >: :"~'i" a clean-up Of ~ll, f.i:ee-stAndi1'19 1iq':lid on the property and to .,';':~'~)'.

.-.. " ,',,"?lo. for .naly ••• of tho stained ar.a. of grouM and .... '; ., . ,.' .;. '·."cllng liquid. Tne affected areaG were Covered ~ith plastio ;,. .',: :.

- .. ,.c·r,-J tho no.d to rehOVe .ny aontamin.ted .011 bosed on these ,.,.-' . :.,

..-;-

,~,

'.'

, ......

. "L . ~ .:,~:. q£! bng: HER Region r rGBpondel1 to Newark to invaetigat~ thfi . ';:),;..: .. :, ;,'/ tho OJ •• "arin. BUuau of the illegal dUJ>pingof an unknown,.:.'..;,-.:

,;.:- i" '.:' l"to th e '0.sai a Rive.. from tho Cho..ic~l comPQUnd.'tacH i ty "..'.iI[.t!}:~': .' ..., .-"seh>r90 of on unknown, dark pUrple liqtad containing aaetic acid;,' ..,,:,--/,.- a"ehc anhYd~ide oagurr.d onto the ground at tho faaility. .,~.,,,,..

. ·.r",. of "e".r-. was h.rad by the faaili~y to p.rform • ale.n-up, '1:,:,. ...:. ~a~ issued for thi$ discharge and th$ 1nci~ent is.under a ,~~:;:·:.:;'ha~ investigation by both the Statl4 and the County, ':';..

:,+ : ~ . " : ~;

" ~.:

I

:;:0'~ ~9S-i

-------

TIERRA-B-004500

.:~-:-.~..;:.'...;~r-~=-~--_._--- ..... ". . ~

•1iAEe •

D;sEo....

.. .". • :'''1=:: •• :. •• -;":1 •

,. .'

..... ~.... . ;.

... '

- " .:- .. "' .

O·j. ~ ..:.~.. ..-: - ~.'- ... -

... .._.:._-~

. _._--- .-._~..---._-.-- ..-.-- -'-' •.

- ...-._----~

845340079

TIERRA-B-004501

.-

-.... _..- "':"

." . .

NEWARK FIRE DEPARTMENTOFFICE OF BAZARDOUS MATERIALS188 Mulberry StreetNeWBrk.NewJeney 07102

STANLEY J. KOSSUP

(201) 733-7508 Fax (201) 73:J.7468

Chemical Compounds29·75 Riverside AvenueNewark, Nl 07104 January 10, 1992

attn: Mr. Harold Sullivan

On January 7, 1992, the Newark Fire Department's Hazardous Materials Unit respondedto your facility, Chemical Compounds at, 29 Riverside Avenue. The complaint regardedunidentified liquid flowing from a hose line on the second floor of your building, down a set ofexterior stairs, onto the ground and into the Passaic River.

nus action is a violation of me City of Newark's Hazardous Materials Regulations. Youare in violation of the following:

Section 8.4 Drainage from production facilities, including buildings, and other processareas shall be so engineered as to provide a means of secondarycontainment for spilled hazardous materials.

Process wastewater and cooling water pipes. plant drains and similarinstallations which drain into sewers, storm drains, public wastewatertreatment plants, watercourses or other routes which drain to waters of thestate shall be engineered so that spills of hazardous materials will notescape through them to waters of the State. Ifhazardous materials capturedin secondary containment systems drain into process wastewater lines,provisions must be made to treat or remove the hazardous materials beforethe water is discharged.

On January 7, 1992, you or one of your employees disconnected a hose line leading intoa waste recovery truck. The hose line was rerouted, enabling liquid to flow onto unprotectedearth, and into the Passaic River.

845340080.:.io

'. -.: ..;..~~... 4a.:,.__~.' .. ,

TIERRA-B-004502

-.'

Section to.tb It shall be unlawful to use or operate any bulk storage area or part thereofwithout:

(b) providing for the segregation of potentially reactive chemicals which 'I..materials or which may react so as to form hazardous materials, and whichpresent or cause a hazardous or dangerous condition.

It was noted that oxidizers, (M & T Chromic Acid) are stacked on top of corrosives.(Ethylene Cholorhydrin)

Section 12.2 All loading, unloading or transfer of hazardous materials shall take placeby a qualified person.

All vehicles and rail cars canying hazardous materials shall stand or beparked only in a secure area where they are under the care, custody, andcontrol of a Permit holder. l

A person who loads or unloads hazardous materials shall comply with theapplicable Federal laws and regulations, in addition to any local and staterequirements.

An unqualified person disconnected the hose leading to the waste container. If the person )!...was qualified he would have been required to know that the product he was discharging onto theground was hazardous.

Section 15.1 In the event of fire, explosion, structural failure, leakage or other dischargerelating to hazardous materials requiring notifications under Federal or Statelaw, the permit holder shall also notify the Director.

The permittee shall submit to the Director within ten days a copy of thewritten report pursuant to the Hazardous Substance Discharges: - Reportsand Notices Act, N.J.S.A. 13:IK-lS, and regulations promulgatedthereunder.

The permittee shall also provide information to the Director relating to the '"ability of the permittee to contain and dispose of the hazardous material, f'.

-the estimated time it will take to complete storage and disposal. the degreeof hazard created and the quantity and type of material released. TheDirector may verify that the hazardous material is being contained andappropriately disposed.

The appropriate agencies were not notified when the spill, leak or discharge occurred.A private citizen reported this incident to the State Police.

845340081

TIERRA-B-004503

"

Section 17.1c Failure to abate, correct or rectify any noncompliance with the provisionsof these Regulations any pennit conditions or any provisions of theHazardous Materials Management Plan with the time specified in the Noticeof Noncompliance;

Section 17.3 If the cause of the noncompliance is not abated. corrected. or rectifiedwithin the time specified in the Notice of Noncompliance, a Notice ofViolation shall be issued.

The Notice of Violation shall be in writing and shall include a referenceto the original Notice of Noncompliance, the unconditional right to ahearing and the remedial action to be undenaken.

Under conditions of imminent hazard the DireclOr.may issue a Notice ofViolation without issuing a Notice of Noncomplian~e.

Section 17.4 A request for a hearing by the penninee shall be given to the Director inwriting, setting forth in particular any defense the permittee might have inregard to the alleged violations, and a brief statement of the factual mattersin suppon thereof. The notice of the hearing date shall be given by theDirector at least ten (IO) days prior to the hearing date.

Section 18.4 Every Permit holder shall insure that a qualified person shall be in chargeat all times and at each and every place where hazardous materialsoperations are carried out. The. qualified person shall remain on thepremises as long as the manufacture. use processing. or handling ofhazardous materials is being carried out and shall return to the premiseswhen required under emergency circumstances. To be a qualified person,the individual shall be knowledgeable in the chemical and physicalprocesses utilized by the Pennit holder.

The Permit holder shall furnish to the Director a list of qualified persons \/with their addresses and telephone numbers to be contacted in the event ,"-of any emergency circumstance, to be updated annually. The director shallprovide said personnel with passes to be shown to City emergencypersonnel to allow the holder 10 pass through any manned emergencybarricades and enter the permittee facility in the event of an emergency.

The person who placed the hose leading from the building to the ground and into the riverdid not remain on the premises.-

845340082

TIERRA-B-004504

/, ,;

-.'-Section 20.2 Whenever in these Regulations any act is prohibited or is made or declared

to be unlawful, or whenever in these Regulations the performance of anyact is required or the failure to perform any act is made or declared to beunlawful, the commission of any such prohibited act or the failure toperform any such act, shall be punished by a finc or not more than$1,000.00 per day per violation or by imprisonment for a tcnn of not morethan 90 days, or by any combination of such fine and imprisonment. Eachday any violation of these Regulations continues shall be considered aseparate offense.

You have been found' to be in violation of five sections of the City of Newark'sHazardous Materials Regulations.

1(0

1YY"...1J..C1~1J}~~Jl

AA:lm

-845340083

TIERRA-B-004505

845340084_~............'_.' -, .~_._".---'-.,.......-~ ..-.................-.-.--..-~'-_ ..__........,..........-<-"-~~..-..-.

TIERRA-B-004506

.' •• 1 ~ •••• '<

TOTAL ANALYTICAL SERVICES FOR A SAFE ENVIRONMENT

nytest environmental he

January 31, 1992

Ens! Inc.194 Avenue LNew;u'k I NJ 07105

Attn:-:.Fred Virrazzi

~.-. Nytest is pleased to submit our Project No. __~9~21~861~~4~~~~Log.in No. 10097 on your sample (s) re~eived: 1109/92

Test s&IDple (s) associated with this project will be retainedfor a period of thirty (30) days, unless otherwise instruct-ed •.- ~ My staff is available to answer any questions concerning ourreport and we look forward to serving your future analyticalneeds.Very truly yours,c:;t;;:::r;;talRemo GiganteExec. VP

Inc.

RG:" .Enc.

SHIPPED VIA: UPS RED

845340085

box 15180 60 seaview blvd., port washington. ny 11050 0 (516) 625-5500:"" fax (516)625-1274

TIERRA-B-004507

-'. nytest environmentoloc

""''1,1" Icf."Hif;cntion and Rosults.-._..~-- -:. __ ~_ " - .

--_ ..-

-

-----~.---.

S"l1'ple No: 1Lab Sample 10 No.: 1099~OI

Rc~ul~s

pH OJ :!O Cron;tabi~ty, F PKCorrosivi tv, inches/yenr~~nct;v;ty to Cyanide, PPK

f~.:octivity to Sulfide, PPHTotal Solids, XP"t,olcun Hydrocarbons, PPH COry lit.)

FCo's ,PPK COry wT.l"

liD " None Detected

< " Less than

Log In No.: 10997

Max.Allowable Levels

2 • 12.5140

0.250

..

4.35> 212

< 0.01< 1.0< 1.0

49.35350< Z.O

00010

845340086

TIERRA-B-004508

- - - - ----\.""' .~TEClQlION INC.

250 Delawanna AvenueClifton, New Jersey 07014

201-773-5013FAX h 201-773-4788

_.

LAB DEP .: 07190

CLIENT: Chemical Compounds Inc.CLIENT REF: 22592

MATERIAL: One (1) composite fromeleven {II} drums

DATE:TECHNION REP:

DATE RECEIVED:LAB ID:

2-27-92160312-25-920122T

.~:~.(."'.- .: ,..;; .

ANALYSIS REQ: RCRA Waste characteristics I•.I.,

:..-The above samples were as received on 2-25-92 and analyzed

as requested. '

ANALYST: Sam Yart, Mara Fishman I.t:-.I::".,'":.:- ..."

CERTIFICATE OF ANALYSIS

r:EST RESULTS:_ 1

All test results are as attached..'','

'.J,' 7·.

Respectfully SUbmitted,/"

.<~..;/" ~ /L "-i/~,,- ./~ C-v";' I 7' !/it":-<-.-

(00, 'Susan Baturay, D.Sc.Laboratory Director

~." .....

SB/sn16031 1.. '~"

;~'." .

- _._- .._._---.

. • ~'.,~ ~ .. ",:l,,' ',: •......,

"845340087 ', ..

:.:"..

TIERRA-B-004509

- "~~HN:IOH IHC.,250 De~aw~na Avenue

Clifton, New Jersey 07014Lab Dap .: 07190

CLIENT: Chemica1 compounds :Inc.

RUN DATE/TIME: 2-27-92/10:00

SAMPLE TYPE: Liquid

SAMPLE DATBD: 2-25-92

SAMPLE I.O.~ Composite

TEST RESULTS FOR TCLP METALS

MAX. ALLOWABLEHETALS RESULTS BLANR MDL LIMITS

Arsenic N.D. <0.01 0.01 5.0Barium N.D. <0.01 0.01 100.0Cadmium N.D. <0.01 0.01 •• 1.0Chromium N. D. <0.01 0.01 5.0Lead N.D. <0.01 0.01 5.0:..rercury . N.D. <0.002 0.002 0.2 .,

Selenium N.D. <0.01 0.01 1.0Silver N.D. <0.01 0.01 5.0.- "'"'~.

-r;estresults are in mg/l, unless specified.

N. D. : Not DetectedM.D.L.: Minimum Detection Limit

i:!:.'.

..<,

"

845340088

TIERRA-B-004510

-

" .'. >.: '.~~'..

-...t'

TE~:ION :INC.,250 De~wanpa Avenue

Clifton, New Jersey 07014Lab Dep i: 07190

----CLIENT:.Chemical Compounds Inc.RUN DATE: 2-27-92

HAZARDoqs WASTE CHARACTERIST:ICS

WASTE CHA~CTERISTICS RESULTSPCB (mg/l) N.D.Reactivity for CN-(mg HCN/)1) N.D.Reactivity for S-(mg H2S/l) N.D.'rotal Pet.Hydc. (TPHC) (mg/l) 3.0Ignitability (oF) Not IgnitableCcrrosivity as pH 4.5

SAMPLE TYPE: Liquid

DATE SAMPLED: 2-25-92

SAMPLE I.D.: Composite

BLANKN.D.N. ri.N.D.N. O.N/AN/A

Test re~ults are in rnq/l, unless specified.N/A: Not ApplicableN.D.: Not DetectedMDL: Minimum Detection Limit

..-,',

MAX. ALLOWABLEMDL LIMITS Cppm)

0.365.Q,

10.0'0.10N/AN/A

...... ,

(mg/kg) 5,-50.250500

30000>140

2<pH < 12~5

845340089

TIERRA-B-004511

. ,.'

.-"~

TEC~.ION INC.,250 Delawanna Avenue

clifton, New Jersey 07014Lab Dep 't 07190

CLIENT; Chemical Compounds Inc. SAMPLE TYPE: LiquidDATE SAMPLED: 2-25-92RUN DATE: 2-26-92

SAMPLE ID12J456i

8"91011-

.-

...--

RESULTS FOR pH MEASUREMENTSRESULTS· (uni tl

5.25.14.95.14.25.84.35.74.14.24.2

•.

845340090

~:..~ ..

f 'I·.

;.;.....

j••••.

TIERRA-B-004512

I' ..

TU:I·~Njnli, , )"'"T f~:iti.. , .11~.J I ','::i' ;,l! loll •.. ,.1" JI, I t\:j /

,:,"" J~I~l\'j'Lllilli.L 1f~\ttL:lllh.:

C;i:;.;n~ N(~VI J';I ;;i.';,Y % 1·1

))LP.B ro II :

ILt}) T.'~\.501]"ff\X IIr (201),773.,...4700';:

",

l'ItOJECT 110,

. l;'19""UrcJ~!.::l1 n:L.. -----

"'IlUIJUCT I/flll( C.HGMIUlL 'e..oMI'OIJVO.5

r, Oll ECIE 0 "r. {1I',,0} .:J.v....-k ~w-==- _

':' Cllfll II Of CUSTODY

.:.: . '# :.".;1-;;:

Si le 10

.. ." .,

SaUlf,lo Utile T illle SiIllll)llng Point ~·i1:d SOlllpllog Hl!thou Sample"'0. 0' Sl,lll Spill Description Hateria} {In,)ly~ls lll!lllolrks "

(J..vM#I/ I,J.;lq. 1"t ILIOn /)£.11/,,,$ II j- / / ' L;QVID IG-n.t:lI3J '

~ l' 1/ t I

f?UI'II '" l-~tt·qJ ,

...vf'\ 1=1) I' " II:J,.,J. ,,~o . .

(l..1I1"l"~ " I' I I ,;; .j'l.9; .

. .#.5 ' ' I' II It . I

ItM J.~'!-1J.... tot Jt.f:, ;.J ,/.lfJ. " ,.t I

" ' , ..,t? ......,J:fl I' ,. ,-

,2.}I/".z

~~II . "

I()-;l '1-~:J

,

-Il(l 111(1\1 I SilEO 111 OIlGi\t11 Z1\T ION 1)11TE IT I/1E nECE1~EO~3Y . OIlGfllif ZJ\ HOIl OJ\T(ITII-IE 1lHJ,\III~SJ;;jJ J,.;.7f1f. ~

...........-. ~- . = • - == - - ,~W"/rtjO #i* *1;.1,1'110

. =m:

.. Ht:f"'IICi4L eo",.,. ....,.... , ["rreM IoN .PJC.....' 1 .." , ,

.. '

.-845340091 ...... '..' ---~... - ... -;

oiJ

~

oDl.~

J)

f?!

I":.

lo,.

TIERRA-B-004513

)

'r c:ii,i' I {u~ut ~u~'~lii 'I- ,II I....''''·' .• -.• I

,.' ,I) Oel,J.wanl' . '.'(iIlUU

'>,,1I, /'1(:.:: ," ),";0\.1

Lf.R In 1.= .~._-----:----._--\ )

, .

t:: ,:.1'/7 ~L..::-,~;:~".\

, . 1;'7\::. Ii t' C::Wll Tn,·XlOU:

. :1'nUI1UCIT liME Ch<"M'r,...~ I . CUfI:(2.lJvr)O< 1'1l0:H:C: :1'0.

'CUlllC1EUIIT,\ .,,,.1 j.gb}>J1c*(l,./ '-, ':'" '"..is),,no'u" J,....:;;==vf4:--b6...,..Al~, ~f.l.I_·Jf~.k-:~--------

::9!ill OF CUST,OOY " ?Site Trill! Sile IU

'~

-"

Silll1llll! U;llP. l illll! Saolll'iog roi nt ~a'ild s'illllpl ing ~Iuthod Silmp\e

Ho... Sllld Spld. Descri I>ti on !-1ateri a) (loaly~is

I\enlarl; s

NO') = .. -= :- 7,·,.

J-)~-1~ 14bo J7tl Vrt"S 1J. I- II L/~IIIP,

I ..

1)t...ll'l"f...ll,a 1J.5

'fI!.'

(){l II/"'" Itr llJ( l I"

..

J..)1(.tf2/-

-- ,

Oe.\J/"IrJjJ" "

I-

"-l,,~CfJ.

IV'S\M nt~~f"\~\ \

(lc.tJ.. '\NUTIt'

O<lA ("\ r~(1.A~

~r=/t.Jr-rplJ

... j •

•

'.,

'-' ,

-:

- j

~~

--lIf.llllqU I $11(11 Irt 0I1GMII Z,\"fl Otl IlATElTI"'E flECE1VEO OY onGAtu It\TI orl OATE/Tlm IIHlAnl~S

LL1.·~~0']1,--' 0,:--~Hf1i1it;oC .............~.'"'. pJlf ~

=rl/;{jqj Il/~

=....='1"'..-:-:-"

1·0.....-, ..."....s ' Yl.1Jr). /'/10 1ttHIJ1'A.! 'fN( •

. \ --'I . ' J

I

.' -\ -.'

..

- -845340092

~':~'~~r.'',.

~~~,:~T:~;:·:r~::;~~:'\;::,.,~,,;:·';~:m\;"l:." f.;: ~Sl':'::~':,:'\:;.>:.. ,

.

'.

'.!:'.;:'~~;:'~<..~'~;"~":'~~.: - ~;.':.':'::::~-:~''.~.c:~~:~.:.::,,~~.;,':".....:~::....:,.>.. '~:~ :•. ~.~.. "......... ",' -="" ~._' ....... --

" _:'~:~':.~{~:

........

'.' . '."

'::>~::..~:': ..." ...:

TIERRA-B-004514

SAMPLE LOG'lIN SHEET '"- ~~

Technion Inc.'\0'; Page { of..L.., .

iJ l.,: ~J ',: ~)7190

.: :·I··...~....~ =:. (Pr:nt ;-;'ame): ~_j~~~I'I,cL~ - L?g-in Dale: 2 - ;l '5- q '2...'~dil"

. '

:!!·.·.;c S:: ;Sign:llure}:

-. 0'" 1'":;.,::~i)L1b :~#: ____. .i.~ (;" CORRESPONDING

.~.".~...c k.e.,.\..v1 'uvi- SAMPLE ASSIGNED ANALYSIS \ REMARKS' ..~...,......... I

:0 '::Ut~~: L"" f 0 V\v1 ~

TAG LAB REQUESTED . CONDITION OF'" ~,.# # SAMPLE SHIPMENT,ETC.

~OOs,~1e i"'--... -rt. L..p f~ ~.J.. 12... ..:-j~• .:i.: 'I' •~

j:ilr-!um./Ab." -..Jo

- "1/ "\ Pl'. Rt:nr:u::r:l!ttllten

.: ~: .:,.'. -::-l' _".: ... ' . 1/ '/ I'P He .,", r-·j·.,-·" .-... r;~,o.;~It.'..\ll"cnl I! -S 9 J:) r'JJ1 l, .,.q' /}.~ lS )

':~'':; :.!;s c) \ e £}/It-i- \/'I1fll'f ( l.J\) T,-.":~t .'!~~)(,.."(lI: :!I~iCtu/Abec:nt

: ;,: -.;~. _t"\ I r'J J\ 1'1 -'/..,/l~ .A

'/

. ~. Ilf Ir- "

·:iA;I~1'lr"S.(.",-kll!r ) 77.4(1(\0 t1vC'~t~CftIlA'UCnl

/1- -v -ct.k'

,:,:,,:;-;·~7. _" ~~"ol'nt!'Atn(rtC

.

,.:."\"'" '''':4C~f''''0( Li&t"d

.. :r:';'~!'J.:.,ClhIi"..ol-

C~,;m/"~. .

'.•':"'.:'r ~•.. < i,· .•• :~',;l.c\'·i'\r..ttlln'l

t ....· ...;.;,inl

:' :-n.;'.: -,':::,1-,,'1"""".

~; .. o .... J..,· r~.-......: ...!:":Ioln~

~: ,.0::" :::-.': !:":r.l:;:e

.·~:l-f:r-:-c!......m ••

~~.):. :\.cC"C","c¢ ,~11..,~;

.:-:;';I .. lU-':~""-t:..!:

-

Sample Transfer

fr:.«i4n:.

Arc#:

., ..

8\'(,~I'I:

I

.-.'~,

..1<

f· .

,<'.

,t'·

,

'}?-O-<; vi \ \- ~ k,if .2-z7 JI. t~n <J;1.,

rf}n ~ C""'£05":k :ra·<M I' I-e. ..Oh~/n.e t/. 1'0.,..., II D /,um 5::t",,~,

845340093

TIERRA-B-004515

845340094--" ",,"'-*-..------_ ..---_._'- .., _-_._- ,_.._._-~

TIERRA-B-004516

-

.-

GABRIEL M~ AMBROSIO, ESQ.464 Valley Brook AvenueP.O. Box 911Lyndhurst, New Jersey 07071(201) 933-8844Attorneys for Plaintiff

'1rV\~ 1 A. MARGOUSf'.J. t:11

SUPERIOR COURT OF NEW JERSEYCHANCERY DIVISION - ESSEX COUNTY

PASSAIC VALLEY SEWERAGECOMMISSIONERS, a body politicand corporate.of the state ofNew Jersey,

DOCKET NO: C-338-93Civil Action

plaintiff, CONSENT ORDER ANDFINAL JUDGMENT

v.

CHEMICAL COMPOUNDS, INC.,Defendant.

This matter having been opened to the Court by Gabriel M.Ambrosio, Esq. (John T. Ambrosio, Esq., appearing) on behalf of theplaintiff, the PASSAIC VALLEY SEWERAGE COMMISSIONERS ("PVSC"),alleging that the defendant, Chemical Compounds, Inc. ("ChemicalCompounds"), violated the provisions of N.J.S.A. 58:14-1 ~ seg. by

discharging pollutants in excess of Sewer Connection permit No.20407122 ("permit"), the rules and regulations of the PVSC and theCategorical Pretreatment Regulations promulgated by the UnitedStates Environmental Protection Agency ("USEPA") at 40 C.F.R. §

414, and the defendant, without admitting any fact, liability orfault as to any or all of the allegations of the complaint, havingconsented to the entry of the within Consent Order and FinalJudgment, and for good cause thus shown;

845340095

TIERRA-B-004517

-

-

-

IT IS on thisORDERED that:

day of December 1994;

Civil Penalties1. within lO days of the date hereof, the defendant,

Chemical Compounds, shall pay to the PVSC the sum of six~thousanddollars ($6,000.00) (the "Settlement Amount") in settlement of allcivil penalties that could have been assessed against the defendantfor allegedly having violated the provisions of N.J.S.A. 58:14-1 etseg. -by discharging pollutants in excess of the CategoricalPretreatment effluent limitations promulgated at 40 C.F.R. !i 414and incorporated by reference in the Permit between July 1, 1991and th~ present, including, but not limited to, those allegedviolations set forth in the complaint filed by the plaintiff inthis action. All settlement payments shall be made payable to the"passaic valley Sewerage Conunissioners."

Compliance Schedule2. Chemical Compounds shall comply with the following

schedule for the purpose of controlling and eliminating dischargesin excess of the Lead, Zinc and Cyanide limitations of the !i 414categorical Pretreatment Regulation and the Permit:

(a) Chemical Compounds shall iImnediately conunenceand implement a study program for the purpose ofidentifying possible raw materials and in-plant processeswhich may be the source of Lead and Zinc entering itswastewater system.

- 2 -

845340096

TIERRA-B-004518

-

-

-

(b) On or before December 1, 1994, ChemicalCompounds shall submit a First Interim Report to the PVSCdetailing its compliance with the discharge limitationsfor Lead, Zinc and cyanide. If the results of the FirstInterim Compliance Report indicate that no additionalpretreatment control equipment is required, Chemicalcompounds shall be in compliance with the limitations forthe discharge of Lead and zinc on or before December 1,~994. If the results of the First Interim ComplianceReport indicate that :additional pretreatment controlequipment is required to achieve compliance with thedischarge limitations for Lead, Zinc and Cyanide,Chemical Compounds shall retain the services of aqualified environmental consultant who shall evaluate itsexisting wastewater pretreatment system and makenecessary recommendations for the purposes of controllingand eliminating discharges in_excess of the Lead, Zincand Cyanide discharge limitations of the Permit.

(C) In no event shall final compliance with thedischarge limitations for Lead, Zinc and Cyanide be

extended past April 1, 1995.

Progress Reports3. Chemical Compounds shall submit to the PVSC monthly

progress reports concerning its compliance with the requirements

and obligations of this Order.

- 3 -

845340097

TIERRA-B-004519

-

-

-

Final Report4. Within ninety (90) days of completing the corrective

action described in paragraph 12, the defendant shall submit to thePVSC a final report concerning its compliance with all applicablepretreatment standards.

Force Majeure5. The completion date for the corrective action described

in paragraph .2 or for the submission of any report required bythis -Order, shall be extended for the period of time that thedefendant or its agent is prevented by a Force Majeure event fromproceeding with the corrective action or subm~tting the requiredreport. As used in this Order, a Force Majeure event shall mean anevent which is beyond the reasonable control of the defendantincluding, but not limited to, such events as fire, explosion,inclement weather condi tiona (that create unforeseen delays), labordisputes, inability to obtain or unavoidable delay in the deliveryof materials, inability to obtain or unavoidable delay in securingmunicipal approvals and/or work permits, inability to obtain orunavoidable delay in securing State approvals and/or TreatmentWorks Approval and unforeseen subsurface conditions. If theoccurrence of a Force Majeure event causes or may cause delay inmeeting any completion or SUbmission date set forth above,defendant shall notify the PVSC in writing within ten (10) days ofthe occurrence of such event, the precise cause of the delay, themeasures taken or to be taken by the defendant to prevent orminimize the delay, an estimate of the date by which such measures

- 4 -

845340098

TIERRA-B-004520

-

-

-

I:'- ....

will be completed or such report will be submitted, and an estimateof the duration of the delay. The defendant shall promptlyimplement all reasonable measures to prevent or minimize any suchdelays, prevent or minimize any adverse impact on the PVSC systemas a result of such delays; and to comply with all requirements ofthis Order as soon as possible;

6. If the PVSC finds that: (a) the defendant has compliedwith the notice requirements of the preceding paragraph and; (b)the d~lay or anticipated delay has been or will be caused by aForce Majeure event, the PVSC shall extend the time for performanceunder this Order no longer than the delay resul~ing from the ForceMajeure event. If the PVSC determines that: (a) the defendant didnot comply with the notice requirements of the preceding paragraphor; (b) the event causing the delay does not constitute a ForceMajeure event, failure to complete the corrective action underparagraph #2 or to submit any report required hereunder shall be aviolation of the requirements of this Order and subject thedefendant to sanctions under the applicable statutes andregulations. The burden of establishing that any delay is causedby a Force Majeure event rests with the defendant;

General Provisions7. The corrective action undertaken by the defendant

pursuant to this Order shall constitute the penalty for anyviolations of the Categorical Pretreatment effluent limitations

-promulgated at 40 C.F.R. It 414 during the period covered by thecompliance schedule. In the event that the defendant completes all

- 5 -

845340099

TIERRA-B-004521

-

-

-

corrective action on or before the completion dates set forth inthe compliance schedule, and as modified by any Force Majeureevent, any such exceedances experienced during this period shallnot be subject to additional penalty.

8. The defendant further understands that any exceedance ofthe effluent limitation for discharges of Lead, zinc and/orCyanide experienced after the final completion date set forth inthe "compliance schedule, shall be subject to further enforcementproce~dings and civil penalties.

9. Nothing in this Order shall preclude the PVSC from takingenforcement action against the defendant for matters not set forthherein or in the complaint.

10. All provisions of the permit shall remain in full forceand effect and are not modified by this Order. The defendantexpressly understands that the compliance requirements contained inthis Order do not modify any provisions of the Permit or any dutiesor liabilities of the defendant thereunder.

11 • This Order shall be binding on the defendant, itsassignees and any trustee in bankruptcy or receiver appointedpursuant to a proceeding in law or equity.

12. Defendant shall perform all work conducted pursuant tothis Order in accordance with prevailing professional standards.

13. This Order shall not relieve the defendant from obtainingand complying with all applicable federal, state and local permits,as well as all applicable statutes and regulations while -carryingout the obligations imposed by this Order.

- 6 -

845340100

TIERRA-B-004522

-

-

.-

14. The obligations and civil penalties of this Order areimposed pursuant to the police powers of the State for theenforcement of law and the protection of public health, safety,welfare and are not intended to constitute a debt or debts whichmay be limited or discharged in a bankruptcy proceeding.

15. In addition to the PVSC's statutory and regulatory rightsto enter and inspect, the defendant shall allow the PVSC and itsauthorized repres~ntatives access to its facility at all times forthe p~rpose of monitoring defendant's compliance with this Order;

16. The defendant shall make available to the PVSC alltechnical records and contractual documents ma}ntained or createdby the defendant or its contractors in connection with this order.

17. The PVSC reserves the right to require the defendant totake additional actions as authorized by law should the PVSCdetermine that such actions are.necessary to protect human health,the environment or the PVSC system. Nothing in this Order shallconstitute a waiver of any statutory right of the pvsc to requirethe defendant to undertake such additional measures should the PVSCdetermine that such measures are necessary, subject to thedefendant's rights under this Order, applicable statutes andregulations.

18. The defendant shall not construe any informal advice,guidance, suggestions or comments by the PVSC or by person (s)acting on behalf of the PVSC, as relieving the defendant of itsobligation to obtain written approvals as may be required herein,unless such advice, guidance, suggestions or comments by the PVSC

- 7 -

845340101

TIERRA-B-004523

--

-

.-.

shall be submitted in writing to the defendant.19. The defendant shall give written notice of this Order to

any successor in interest. prior to transfer of ownership of thefacility which is the sUbject of this Order and shallsimultaneously verify to the PVSC that such notice has been given.

20. No modification or waiver of this Order shall be validexcept by written amendment duly executed by the defendant and thepvsc.

21. The Court shall retain jurisdiction over the parties tothis action solely for the purpose of enforcing the provisions ofthis Order.

22. The PVSC reserves the right to reopen this case in theevent the Commissioners of the PVSC, at their next available publicmeeting, do not accept the recommendations of the chief counsel toenter into this Consent Order and Final Judgment.

23. This Order does not constitute, nor shall it be used asevidence of the findings of any fact or the admission of any facts,fault or liability on the part of the defendant, nor shall any ofthe alleged violations settled herein be utilized in any way as

-prior violations for the purposes of characterizing any otherviolations, alleged or actual, existing or hereinafter committed.

,./ --""1

~h~L .~,....... '/yv-'j" ..~ ..;..,~

Hon. Harry A. Margolis, P.J.Ch •

- 8 -

845340102

TIERRA-B-004524

-

--

The undersigned hereby consent to the entry of the foregoingorder, both as to substance and form.

Dated: ';/)!9r

JTA: jaChemical Compounds.con

GABRIEL M. AMBROSIO, ESQ.

-"by0 ,"\.Iohn T. Ambrosio,

Attorneys for theEsq.PVSC

CHEMICAL COMPOUNDS, INC.

Print Name

Print Title & position

- 9 ~

845340103

TIERRA-B-004525

845340104......... -.- -'--.-------.--~_ _ ....--.-- _- -.~_.-------....

TIERRA-B-004526

VI()LATION NOTICEHAZARDOUS MATERIALS REGULATIONS

CITY C~ NEWARKFIRE DEPARTMENT

1010 HUhA~';. Newark,N.J. 07106(20 l) 733-7495

o NON COMPLIANCE o COURT ACTION REaUlflEO

LOC~;ION: .1.9 Ri.ver:sJ.de Avenue Bloele: .~ lot: _'~_, __

OW~F.R: AGENT:

NaMa .--tkICQ1Q SuB iYaO ._.- ..•. -.,,. ...Address 29-75 Rivecside Avenue __ . _Town/Slate'Zrp N(3....al:'j(~ 07104 .__. __. _

,\dd($H -19.-7 5 R~er;s.id@ A"enI,lH

Towl1/Sllto{Zp _ New,'lrk I NJ Q71Q4

"t·"'!'" Permit 'I:

----------~---------,- ..........-.~-_._-----_._-~---"

~~~~,C~'-· CGMP\J'NCEDUEDAfE' PAreO""'P€CTION, ~-_.-

- TAKE NOT1CEU1atyou have been found [0 be in violation of the City of Newark Ordinance (BS&FE amended M~rch21, 1990) govcmfng hazardous materials: .

•SCctiol\ 3.-\

Scc'.:ion li).l G

Sect:.ion 12.2Se:::I:.~..m 15.1

Section 18.4

II you have any questions concerning this matlor. please call: ....{...20.....1..,.I .....z""'33....:.... 7L.:41>9....5'-- __ ~~ --

DOlOHlUtnal Officer

Date

845340105

TIERRA-B-004527

-NE\VARK FIRE DEPARTMENTOFFICE OF HAZAROOUS MATERIAI.S1sa Mulberry StreetN("""·IUII;. NewJersey 07102

STANLEY J. KOSSUP

(201 J. 733·7306 Fax (201) 733.7468................ _ .. ~i.oo ._ - " t~t:_ -.:;o..:.~, ,

(:hcm;(:al Compounds1;:·::5 Riwrsid..: AVCIIll~

,':n.;:rk, NJ 07104JIU1UlUY 10. 1992

t

On January 7. 1992, the Newark Fire Depurtment's Hazllrdous Materials Unit respondedl(\ Yll\ll' facility, Chemical Compollnds nt, 29 River:-;ide Avenue. The cOlllphJint regardedill1id,·~l·':···.·d li~lujtf /lowing r.'ol1l il hose line (1Il the :-;ccolld floor of yOlll' b~l'ilding, UClWII 1Iset ofl~xl~'riilr.,wini, onto the ground and into the Passilic River.

This ;lctioll ili a violation of the City of Ncwllrk'~ HM.llrUOlill MlIlcrinls RegullltiollS. You:1t'Cill violation of the fol\owillg:

- Section 8.4 Drainage fmm procl~lcrion facilities. includh\g buildings. llnd ocher processllre:lS shall be so engineered as to provide a means of secondaryconlainment for spilled hazardous materials .....Process wastewater ~lnl;l cooling witter pipes. plant drains nnd similarinsl~lliations which drain into sewers. lHOI';1l drains. public wI'stewuterIrearnlent planu, walercourses or other routCli which dmin to waters of thest;lte shall be '.:ngineered so lhut spins of hRzardo~IS materials wiII notescape through them to waters of the State. If hazardous materials capturedill secondary contllinm~nt systems "drain into r"()Ccss wastCWlIler lines.provisiOlls must be mnde to treat or remove the hazardous materials beforelhe w:lCer is discharged.

Oil j;1ll1l:1ry 7, I~n,you or One of your employee.'l disconnected a hose Hne leading imo·1 ···le recov.~ry tnlck. The hose line WIIS rerouted, enabling liquid to now onto unprotected<:a: 'd huo the Plu:~:licRiver .

. ----

845340106

TIERRA-B-004528

~::~Tti\lllHUh It shall be lIll1nwfui to llS~or opcnlle ,tny hulk stornge Ill'eaur part thereof

""il!l\l\lt;

II was noted that oxidi;l.ers. (M & T Chl'omic Add) nr~ stacked 011 tOp of corrosives.

(lLlh)'lcnc Cholurhydrin)

(h) prnvidil1g for the s¢~r.:;g'Hi{)n of potentially rem:livc chemit::nlli whichm:ltcri(11s or which may react so ns \0 runn b;.\1.nrdOtI1lIl1illcrillls. tinct whichpresent ()r cmlSC ,I h.t7.ardo\ls 01' dilllgcrmis conditioll.

,-

~;eclioll (2.2 All londlng. 1It1ioauing or rnlllsfcr of bi\7.arlloUli JOllle-I'julsshall take placoby a qualified pCI'l;un.

All v~hicles and mil enrs carrying hlll-,u'dollS lililleri'l1s lIhall Slltl\d or beparked 01\1)' in a secure I\rea where they al'e under"rhe cure, custody, lU\d1,,;{)IHfolIII a Permit holder.

An unqualified person disconnected the hose leading to the wal;te container, If the pei'sonwas qualified he would have been required to know that the product he was discharging onto the

_ S!'()'lII\J wll'l h~7:\rclotlS. .

A pC"I'~OIl ,,,ho l<lads 01' \lnloatls hl\Zanlolls :l1llterh\ls shall comply with theapplicable focdcl'a\ laws l\nd I'c~ult\lions. ii' addition ;0 !lily locnl und !ltnte r

require,mellls.

Seclion 15.1 In the event of fire. explosion, str\1cturnl fallure, leakage or other dischargerelating to hazardous materials requiring notifications under Federal or Statelaw. thc p~rtl\it I~\der shllll ulso I\oliry the Direclor.

The penl\\uee shall sttbmit to the Director within ten days a copy of thewritten report purS\lAnt to the Hl\znrdullS S\lbstllnCe Discharges: • Reportsand Notices Act. NJ .S.A. 13: 1K·1S, l\nd regulations promulgated

thereunder. ," .The pennillcc shl\l! also provide informl\tion to lhc Director reh\ting to theability of the pemlillee to contain and dispose of the hazlIrdous ffil\terial.lhe estimll\cd time it willtllkc 10 cumplete lil()l"llg~,\lld dil;pusII1. the degreeof hazard crealed and the quantity and type ot' material released. TheDb'eclot' may verify that the hazardous material is being contained and

apprupri"lcly disposed,

The .\pproprime ,\gcncies were not nOlifie(.l. when the spill. leak or discharge occurred.

'ri";\lc cllllen reporred this Incident to the Sulte Police:.

-845340107

...,. I ~ ....... ~ ... ."..,-

TIERRA-B-004529

-:l\TlicIII 17.1c Failure \ll :lh:llL:. correct or rectify IIny IIUIlCCllllplillltCC'wilh the provisions

of these Regulations uny permit conditiMS or any provhiiotls of tIle['Ia".ardulls Malt::ri"ls MlInngement Plan with the lime specified in the Noticeof Noncon:pliallce;

So;;dioll 17.3 If the calise of the noncompliance is nm llbatcd, correcled, or rectitiedwithin the. time :\pecified in the Notice of Noncomplh,ncc, a Notice ofVil\lal inn shall ilL: i!iMlcd.

The Notice of Violation ShAll be in writing Ilnd shall include a referenceto the miginnl Notice or Noncompliance, the ul\conditlonlll right to II

he,lring and the remedial action to be undenaken.

Undt:.r condilions of imminent hnzard rhe Director may issue a Notice ofViolation without billuing a Nmice of Noncompliance,

';\'diOll 17.4 A request rO!' a hearing by the pcrmillcc shull be given to Ihe Director inwriting, selting forrh in PlIl'tic\llar any defense rhe penniuee might have int'egard ro the alleged violations, and 1\brief statement of the factual matterSin support lhereof. The nolice: of the healing dnrc shall be given by theDirector at least ten (10) days prior to the hearing date .

,

-.

Section 18..1 Every Pel'mil holder shall ins\l1'C that a qualified person shall be in chargeat nil times and at each l\J1d every place where hazardous materialsoperations tire cm'l'ied om. The qunlified person shall remain on thepremises ill! long Ill',the munllf~lchlre, \I~e proc.:;ssing. or huncHing ofhaziu'dou$ lllHt¢ri"ls is being carried Ollt and shall return to the premiseswhen required under emergency circumslilllccS, To be 1\quu1ified person,the individulll shall be knowledgeable ill the chemical and physicalVITlCeSlieS utilil.CU by the Permit holder.

.~ •• -+ .. -'

The Permit holde.}' shall furnish to the ·Director a list of qualified personswith their addresses and telephone nUlnbers to be contacted in the event()f :lOy emergency circumstllncc, to be \Ipdtltcd llnnually. The director shall[.>mville :;~lid pCI'llOllllCI wirh I't\liltCS 10 be shown to City emergencypersonnel to allow the holder to palls through any manned emergencybarricades and enler the permitree facility in the event of an emergency.

The PC'~OIl who placed the hose leading fl'om the building LOIhe ground and into the river.1iJ !1(\!. r.:m.\in on the premises. .

-845340108

s:e' .,j

TIERRA-B-004530

SI'~'1inn 211.2 Whcncv~~1'ill Ihese l~cl.ttl\lIli<IIIN any :Iel is pmhll>ilctl OJ'Is tlllKh:: or <h.:c!arcd_ to be ul1Jl\wful, or whenever in thell"CReguilltion~ the pcrfolTImllce of lIny

net j:; required or the fuihll'e to perron'l (lny liCI is made or declared 10 beunlawful. Ihe C()ll1l1li~~donof lilly :meh prohihiled lIe\ or the failure '10jll..:rfonll :III)' lllll;h :Icl, slmll be punished hy n fille or not more thull$1 ,()OO.OO pCI'day pCI'violation or by i!l1prisollmC111 for:l [crill of 1101morethan 90 tlays, or by any combinnlioll of such fine llnc.l impl'isonmcm. Each~/ay allY Vi~llHlioll of these Rcguhllions cOlltinllCs ~halt bc considered n

~cpi\n\lc olTcllllC.

Y',III !lave' been found to be ill violalioll of five :;ecriolls of the CilY of Newark's~! '! 'I.,'r,!nus Mal~.ril\ls Regulall()n~.

- ,VA: 11\\

~ .'...

I.'

-845340109

TIERRA-B-004531

-I~. "

-

" -j

.d

-

NEWARK FIRE DEPARTMENT

Omce of Hazardous Materials188 Mulberry StreetNewark,NJ 07102

Stanley J. KossupDirector/Fire Chief

(201) 733-7506 Fax (201) 733-7468

Chemical Compounds, Inc.29 Riverside AvenueNewark, NJ 07104

Jamtaly 31, 1992

ann: Mr.1Jarold Sullivan

•On January 31, 1992, a reinspection was conducted at your' facility on 29 Riverside

Avenue. The purpose of this was to check on the violations issued on January 10. [992. Theconclusions·.of this reinspection are as follows:

Section 8.4 Drainage from production facilities, including buildings, and other process an~asshall be so engineered as to provide a means of secondary containment tor spiiledhazardous materials. Process wastewater and cooling water pipes, plal1! Jr:rin:;and similar installations which drain into sewers, storm drains, public waste'.vatertreatment plants, watercourses or ciller routes which drain to waters of the stateshall be engineered so that spills of h~zardous mmerials will not escape throughthem to waters of [he State. If hazardous materials capwred in secondarycontainment systems drain into process wastewater lines, provisions must be madeto treat or remove the hazardous materials before the water is discharged.

THIS VIOLATION HAS BEEN ABATED.

All internal dr'dins in the building from the first fl<xlrhave been re-pipel1, enubling themto drain into a 1,000 gallon tank located on the ground floor. After the material ha~ been PHtested, it is pumped into a hazardous waste trailer.

Section lO.lb providing for the segregation of potentially reactive chemicals which arehazardous materials or which may react so as [0 fonn hazardous mutcli.l!s. andwhich reaction may present or cause a hazmuous or dangerous condition.


The oxidizers, M & T chromic acid, have been relocated [0 a different [ocutioll ;lllU ,Ireno longer stacked on top of corrosives, ethylene C~OlOrhYdrin,.;,.~.'~~

1: 845340110! .• !.".

-.."'..;.: .....

TIERRA-B-004532

·,

- Section 12.2 All loading, unloading or transfer of hazardous rnmerials shall tuke place by aqualified person~

All vehicles and rail cars carrying hazardous materials shall stand or be parkedonly in a SCCUl'C area where they are under the care, custody, and control of aPennil holder.

A person who loads or unloads hazardous materials shall comply with the. applicable Federal laws and regulations. in addition to any local and state

requirements.


Mr. Sullivan explained that his employees have been trained on the unloading and transferof hazardous materials. Mr. Sullivan also stated that in the event of a leak: spill or accident hisemployees will know what to do. I instructed Mr. Sullivan to send me a letter documenting this,to which he agreed:

...Mr. Sullivan was also informed that flammable liquids with a flammable rating of three

,)r more should q,e stacked no more than two drums high, as we found three drums stacked on

_ topof eachoili~ inilie frontof ilie bUUdi:j;;Z;; (}r /r4Battalion Chief Anthony Apostolico

AA:lm

-_.- 845340111

TIERRA-B-004533

--:;.----.:- ... --:",.'",~,.;-"j" . :-_-w.

TIERRA-B-004534

-- ., " ..Scott A. WeinerCommtssJoner

Sua of New JeneyDepu1ment of EnvIronmeDtal Prcnecdoa and Enel'J)'

DMslon of RespoNtble Party Site RemediationMetro Regional 0tBce

I 8abcodc PlaceWest Orange. NJ 07052

Tel. t 609-669-3955Fax.' 201-669--3993

ICatIJ. DelaneyDJredOr

Chemical compounds Inc.29-75 Rivers1de AvenueNewark, NJ 07104Attn: Alberto Celleri

February 26, 1992

Dear Mr. Celleri, "The New Jersey Department of Environmental Protection and Energyis authorized~ pursuant to the New Jersey spill Compensation andcontrol Act, ·~.J.S.A. 58:10-23.11 et seq. to collect all costsassociated with a discharge and incurred by the state in the removalof hazardous substances or mitigation of damages. Accordingly,oversight costs (salary~ materials and indirect costs), in the amountof $708.60 were 1ncurrea by the Department when the Bureau of~ .Emergency Response responded to an illegal dumping of aceticacid/anhydride which resulted in contam1nation of the ground and thePassaic River on 1/7/92 in Newark, Essex County. CEPE case number

92-01-07-1025.Payment of this amount will not relieve the company from potentialliabi11ty for civil or administrative penalties, adait10nal costsincurred by the Department, nor any other responsibility or obligationunder the law, including responsib1lity for damages Which may havebeen caused by the discnarge. Your payment of this amount merelysatisfies the Bureau's interest in recovering its actual costs or the

above referenced response action.You must submit a check to the Department payable"Treasurer State of New Jersey" with1.n30 days afternotice. piease se.ndyour check and.the white copy of

DEP-062A to:New Jersey Department of Environmentalprotection & EnergyBureau of RevenueeN 417Trenton, NJ 08625-0417

You may contact Walter Janicek of the Bureau of EmergencyResponse at 201-669-3955 if you have any questions or require furtherinformation. •

to thereceipt of thisattached fOr:!

-Very truXy yours,

J! I~ .' - . . I'_T/t: t....J.:.._~i:l-e CJ tF ..d_ •../ ~- -stanley De~likat ,'-

845340113

TIERRA-B-004535

\

}

.',

"~"";'-_ • ..11;f;· :':.:.,"p'~'j:t~ ,

"'~.J;~I, ~,,- r ":- ...,.• ..-... ,~, ............. ..,;. ..!.- ........... _ .•

1{l19lNew Jersey Departm9l11 of Envlronmenlal ProlllCtloo and Energy

oCheck her. If Revised Billing (ENFORCEMENT INVOICE)~umenl~ _Dale Rec'd _

Amounti·P•S•R•

F.MEBGEt¥'Y RESPONSE TYPE: 0 FlneIP.nalty (]J Cosl RlICOveryFACIlITV 10 NO,. ' ,""",..,,-,-,·""1-. -." ,:-,---PROGRAM 10 NO, ' l't2:';01-'p7-1025

Cas&'CompanYt:~~ I"eti'emica'l' Co'nJ()ounaa'"'' ;", ;';'1";1', ,. ,,',U\t'''".''ltJ ""- _ '" _": 0,' "

Al:Idt4l'.h!29l.,.75 Riveceida 'Avenue'Newac:k,NJ 07104

. l"" ,t I::"'~il:':"::.=..:::..;~!.:-:=:..:-~.w~~ __ -:- _

Pl•••• ,Id.ntlfy .appropriate. category: .. 'j, j

o CoUnty , Authority:'" ,""'; 0 Industrlal'.lo Local • l 0Reglonali' 0Colrlm8rdalo PrIvate 0 Local ·0OtMr •; I:· 11111 ' " - ~: ""'lS=~iU:-:---"-

1:~~f~.t:~~~~H~'t::..;;:t,:·\{~;t; .'

2/7/92 lI00HUSTRA.'l'lVE COS'l' RECOVERY $708.60$708.60AMOUNT DUE:

COPY D1STRIBrnIO/V;

Mail to: NJDEPE. Bureau of Revtll'lueeN 417, Trenton, N.J. 08625-0417

Wlaile - Remulance Copy fellow· Comp411y PjuJc • Bi/reau of Re.emit! Goldenrod· Divisi",/:.. - ..... _ ....... , ... '- ... , ..

, /

),

!i.

I'

, "

TIERRA-B-004536

J< ~". , .......

-NEW JERSEY DEPARTMENT OF ~IRONMENTAL PROTECTION AND ENERGY

BUREAU OF EMERGENCY RESPONSEADMINISTRATIVE COST RECOVERY WORK SHEET

PROJECT ACTIVITY # ~

Case Name: Chemical compoundsCASEI.D.NO. 92-01-07-1025-33

COST CALCULATION: $708.60

REGULAR OVER'l'IMERESPONPER DATE RATE HOURS AMOUNT RATE HOURS

M. Garamone 1/'9/92 52.20 4.0 208.80

C. Gibbons 1/7/92 52.20 3.5 182.70

--M. Garamone 1/9/92 52.20 2.0 104.40

M. Garamone 1/8/92 52.20 1.0 52.20

M. Garamone 1/9/92 52.20 2.5 130.50Total 678.60

AMOUNT

(Report)

Equipment:4 Drager Air sampling tubes - (Acetic Acid) - 4 x 7.50 ea/ = $30.00

-845340115

TIERRA-B-004537

-~Ubpl1f"a lutts Ufttum

~uperior <!lourt of NrUt ~trst!JStaft of N,wJrrsIllQtoutdy Df Sbrrtr

I) ..)

Custodian of RecordsChemical Compound, Inc.29-75 Riverside AvenueNewark, SJ

TO: _------------:~~=:---;-----::~~---:;:--........-~--R.J. Hughes Justiee Complexyouvehen~commandccfto1ppullt 2S Market St" 4th floor. Friday .

lntfle-CltyolJ'renton Oft January 24th at 11:30 AM- .

10 &lve tvtdenu before the Slue Grand Jury Ind you an Oldeted to appear wI&hout plcp~ymenc

of whncss fee and brIne wilh you the foUowin, (<<aIds: -------------:See Attached Schedule "All

If you f~ 10 appear ~d p,odu~. the saId lecords, I wunnt may be Issued ror your atTC$C

and you may be ~'eed with ~tcmpL

.WlTNESS. the JJaxrrable sanuel D. -terx:Dc, 3r., ~ of the aJperlor Q:A1rt.

tM. 13th ~ 01 January ~ U~.

7

~~ • assen,~609) 984-4470 /

.L4.~~~- ;,. ,/1119+ and on ,I,'f. fJ-

:tJ:..#.,.~~~Wl,jl.t-L!iJ..m.I.JL.- , served It on the withIn named ll.!?:.l,Jj )Jk~. Ii .

by denver n, acopy 10 ,,~--

TIERRA-B-004538

- custodial of RecordsChemical compound, Inc.29-75 Riverside AvenueNewark, NJ

--------------------------------SCHEDULE A

1. In answer to this subpoena, the records shall:a. Be delivered in the same condition and order as they are kept

in the ordinary course of business:b. a complete inventory shall accompany the records as to

exactly what records are contained in each carton or-envelope; and

c. the records shall be delivered in a secured carton orenvelope as to protect the records and keep them in proper'order. •

d. The term "document" shall mean any ORIGINAL WRITING .(handwritten, typed or otherwise reproduced) formal orinformal, in your possession, custody, or control, regardlessof where located and includes, but is not limited to,contracts, agreements, communications, letters, telegrams,regulations, memoranda, surveys, studies, summaries, reports,manifests, brokerage agreements, bills of lading, testanalysis results, notices, announcements, transcripts, fieldnotes, weigh tickets, telephone memoranda, purchase orders,instructions, charges, manuals, brochures, photographs,schedules, price lists, messages, records, invoices, taperecordings, notes of interviews or communications, calendarentries, records of meetings, applications, newspaper andadvertisements, video tapes, information retrieval systems,and any other method of electronic storage, and materialprepared for circulation to any past or present division,affiliate, officer, director, employee or agent. In allcases where originals are not available "documents· also meancopies of original writings and non-identical copies thereof.Without limitation of the term "control" as used in thepreceding sentence, a document is deemed to be in yourcontrol if yOU have the right to secure the document or acopy thereof from another source or pUblic or private entityhaving actual possession thereof.

.-

2. All documents reflecting the procedures or instructions foroperating the centrifuge located on the second floor of ChemicalCompound, Inc., 29-75 Riverside Avenue, Building 117.-

845340117

TIERRA-B-004539

- 3. All documents reflecting the procedures or instructions for thecleaning and draining of the centrifuge located on the secondfloor of Chemical Compound, Inc., 29-75 Riverside Avenue, Building'17.

4. All documents or records reflecting the Chemicals or other ,substances which were either mixed in, processed by, or used inthe centrifuge (located on the second floor of Chemical Compound,Inc., 29-75 Riverside Avenue, Building 117) between December 1,1991 and on or before January 7, 1992. Also included in thisdemand are documents reflecting the schedule that this unit iscleaned, including the date immediately prior to January 7, 1992.

5. All documents reflecting the disposal of waste for the periodDecember 1, 1991 to January 8, 1992.

6. All documents pertaining to discharges from Chemical Compound,Inc. or any of it's facilities, into the Passaic Valley Sewerage.Authority, including but not limited to analysis, correspondenceand operating procedures. •

-845340118

TIERRA-B-004540

0- - .-'

- •••

-.-.£ .-iJ .

ROBERT J. DEL TUFO., fOANEY GENERAl.

~tuft of ~tf1J Jler£it\[DEPARTMENT OF LAW AND PUBLIC SAFETY

DIVISION OF CRIMINAL JUSTICECNOU

'''CHARD J. HUGHES JUSTICE CDMPLEXTRENTON.. NEW JERSEY 08125·0085

TEI.EPHONE: IW9·ge.·e50G

ROBERT T. WINTERDIRECTOR

August 18, 1992

Jonathan B. Roth, Esq.129 Washrngton StreetP.0 • Box 1779Hoboken, NJ 087030Dear Mr. Roth:

-Enclosed please find copies of the draft Waiver of Indictment

and Trial by Jury and Accusation prepared in accordance with yourJuly 13, 1992 letter. Advise me if you have any changes and I willthen file them and obtain a date with the Court for the plea.

The terms of the plea, pursuant to our recent discussions, arethat Chemical Compounds, Inc. plead guilty to a fourth degree waterpollution violation, N.J.S.A. 58:10A-I0f(3), as contained in theenclosed. The State will accept a fine of $5,000 for the offenseand Chemical Compounds, Inc.·will provide a check in the amount of$1,760.85 payable to the.Office of the state EnvironmentalProsecutor to be used to purchase a one page advertisement in theGloucester Times conveying a positive environmental message. Thedefendant will not be identified in the advertisement.

As soon as I determine from you that this is satisfactory, Iwill schedule a date with the Court.

~e~ ••

~ ~~es w. Glassen

JWG/dkEnclosure

.-845340119

New Je'$ey Is An Equal Opportunity Employer

TIERRA-B-004541

..'

-

--

SUPERIOR COURT OF NEW JERSEYCOUNTY OF ESSEXLAW DIVISION - CRIMINAL

STATE OF NEW JERSEY

v. WAIVER OF INDICTMENT ANDTRIAL BY JURY

CH~MICAL COMPOUNDS, INC.

CHEMICAL COMPOUNDS, INC., the above named defendant,charged with unlawful discharge of a pollutant, contrary toN.J.S.A. 58:10A-IOf(3) and N.J.S.A. 58:10A-6a; being advisedthrough its agents of the nature of the charges against themand of their right to indictment and trial by jury, herebywaives prosecution by indictment and trial by jury and requeststo be tried by the Court.

Dated in Newark, New Jersey, this day of, 1992.

Signed and deliveredin the presence of. CHEMICAL COMPOUNDS, INC.

By:

Reported By: Approved and accepted on thisday of , 1992,

in the presence of thedefendants and in open court.James W. Glassen

Deputy Attorney General

The HonorableJudge of the Superior Court

845340120

TIERRA-B-004542

-

_.

-


STATE OF NEW JERSEY ACCUSATIONv.


CHEMICAL COMPOUNDS, INC. having been charged underoath with violating the water_pollution control Act and havingin writing waived indictment and trial by jurx and havingrequested that the Defendant be tried by Accusation by theCourt, and the request having been granted;

DEPUTY ATTORNEY GENERAL JAMBS W. GLASSEN, for theState of New Jersey, alleges that

COUNT ONE(Unlawful Discharge of a Pollutant - Fourth Degree)


on or about January ,7" 1992, at the City of Newark, in theCounty of Essex, elsewhere, and within· the jurisdiction of thisCourt, did negligently discharge a pollutant into a municipaltreatment works, namely the Passaic Valley Sewerage Commissionsewer system in the area of 29-75 Riverside Avenue, Newark,without possessing a valid industrial pretreatment permitissued by the Passaic Valley Sewerage commission, that is,CHEMICAL COMPOUNDS, INC. did negligently release, spill, leak,pump, pour, emit, empty or dump into the Passaic ValleySewerage Commission sewer system, which leads to the Passaic

845340121

TIERRA-B-004543

",

.-

-

Valley Sewerage Commission sewage treatment works, which thenflows into waters of the State, a pollutant, namely industrialwastes, without possessing an industrial pretreatment programpermit issued to CHEMICAL COMPOUNDS, INC. by the Passaic Vall~ySewerage Commission, contrary to the provisions of N.J.S.A.58:10A-IOf, N.J.S.A. 58:10A-6a, and N.J.S.A. 2C:2-7, andagainst the peace of this State, the government and dignity ofthe same.

-ROBERT J. DEL TUFOATTORNEY GENERAL OF NEW JERSEY ;

By:-:J:-am_e_s--::w=-.~G:-:l:-a_s_s_e_n-Deputy Attorney General

- 2 - 845340122

TIERRA-B-004544

-LAW OFFICES

JONATHAN H. ROTH129 Washington Street

P.O. Box 1779Hoboken, New Jersey 07030

]ONATIiAN H. ROlliAdmitted in N]. NY, MA

(201) 792-0870Fax:(201) 6'9-1088

O/CoWISIIIMAlUSA Y. PARADISO

Mmitted in NJ. NY, CO

August 28, 1992

Mr. Ba~old E. Sullivan, PresidentChemical Compounds, Inc.29-75 RLverside AvenueNewark, New Jersey 07104Mr. Alberto CelleriChemical Compounds, Inc.29-75 Riverside AvenueNewark, New Jersey 07102

-Damon R. Sedita, Esq.Schwartz, Tobia & Stanziale22 Crestmont RoadMontclair, New Jersey 07042

RE: State of Hew Jersey v. Chemical Compounds, Inc./DraftWaiver of Indictment and Trial by Jury andAccusation

Gentlemen:I enclose herewith correspondence from James W. Glassen,

D.A.G. in addition to Draft Waiver of Indictment and Trial by Juryand Accusation. Kindly review the e~e and provide me with thebenefit of your comments andlor questions as soon as possible. Theterms of the plea are set forth in Mr. Glassen's letter and are asfollows:

1. Chemical Compounds, Inc. will plead guilty to a 4thDegree water pollution violation under N.J.S.A. 58:10A-10£(3) as contained in the enclosed;

2. Chemical Compounds, Inc. will pay a $5,000 fine and$1,760.85 for an environmental advertisement in theGloucester Times.

-845340123

TIERRA-B-004545

-

-

THE LAW OFFICES OF JONATHAN B. ROTHMr. Harold E. Sullivan, PresidentMr. Alberto CelleriDamon R. Sedita, Esq.August 28, 1992Page 2

I look forward to hearing from you.

JHR:slkEncs.

Roth

845340124

TIERRA-B-004546

).,

CHEMICAL COMPOUNDS, INC.2975 RIVERSIDE AVENUENEWARK, NJ 07104

6235

September 9 ~9_92I

PAY ~TO THEOROEROF ~

1$5,000.00Five thousand and 00/00 '..... , . .......... " DOLLARS

iII-=--....a.a ...... r-..-~-~~---.:IFOR_______________ . ...............

I:O~~~000251: ll31 ll?2~- ' ..-'.

CHEMICAL COMPOUNDS, INC.2975 RIVERSIDE AVENUENEWARK. NJ 07104

6236

Sep.t.ember9 19--92-

PAYTO THE I $ORDEROF._--=:...:..:--=...Jl..:...:.....:.-..:..-=.~..:...:...~:.-....:....::-.:..--:....:------------- 1,760.85•I One thousand seven hundred sixty and 85/00 .....................

----FOR _

'.

H-2/112138

6·2/112138

)

TIERRA-B-004547

,-

-

rII MP 71647

~~Coun.cf _

~ Court. SpedoI PIn'" ,z:" ':"~-c"..

eo-4 Ro<:.Ipt.i...- ,lor(.$, _

-"'-.-- I .. SUMMONS /"-;L"~Ccu1IJcf ~S~~ I

VOll AAe'"HERt:aY""SUMMONEO10 APPEAR PERSONALLY BeFORE THSCOURT AT lliE lWE AND fII.ACE SPEClFtED SELOW 10 NlSWEFl lliEF<ll.l.OWlNG VIOl.ATlONIS):

i

1

I

rl .... hlJoICIPIlIlv 01 • •iC CoonlyGl ..'

Ooc. "Rog. " f><l>.a-- -- ClIy -Fort Length

FlqUoIon 'I',ope COOr

NOTIC!: ~ YOU N1END 10 PILOO I<QT GUI.JY _ 10 COH1llST 1HE 0W0ClE lIPEC-..eJ .. 'IMSSULIYClMl. .. LEAST 3 ""'8 PllIOR '10 .... DAft fl><£D FOIl YOJR ~ II coum. 'lOI 00lU$T1OO1IFY1lE=,",-_ """""'SS _1EU!PHOHE~ IS_ON ... _t;tF'IO.ANIa<T1CIl, ~ 'I'CU_ 10 SO NOnfV 1HEC\,I!IIK IT _lIE NECt_~OA 't(lU~_ l\Oll eo<...-

-........-. y,JU l.<J/~~ be .Ccut~~O / jiJo.,-// /6"0Ccut~ 0.;01 18 111 M.

_01 Ccut _

CcutTolop/lOnlI ---; _

J~/-- ? ~?SUMMONS ,.

845340126

TIERRA-B-004548

·, •$ute of New JerseyDep..unent of EnvIronmentalProtection~d bUSY

DMslon of ~ponslble party Site RanedlatlonCN02.8

Trenton. NJ08625-0028 .

-Jeanne M. fox.Acting Commissioner

Karl J. DelaneyDIrector

November 30, 1993

Chemical compounds Inc.29-75 Rivers~de AvenueN~wark, NJ ~7102 ,..Attn: Alberto CelleriDear Mr. Celleri,

The New Jersey Department of Environmental Frotection and Energyis authorized, pursuant to the New Jersey Spill compensation andControl Act, N.J.S.A. 58:10-23.11 et seq. to collect all costsassociated wieh a discharge and incurred by the State in the removalof hazardous substances or mitigation of damages. Accordingly,oversight costs (salary(,materials and indirect costs), in -theamountof $866.47 were ~ncurrea by the Department when the Bureau ofEmergency Response responded to a chemical fire at Chemical CompoundsInc. on 10/5/93 in Newark, Essex County. DEFE case' 93-10-05-0736 &93-10-05-1110.

Pa~ent of this amount will not relieve the company from potentialliabil~ty for civil or administrative penalties, adait~onal costsincurred by the Department, nor any other responsibility or obligationunder the law, including responsib~lity for damages which may havebeen caus~d by the discfiarge. your payment of this amount merelysatisfies the Bureau's interest in recovering its actual costs or theabove referenced response action.

You must submit a check to the Department payable to thet1Treasurert state of New Jersey" within 30 days after receipt of thisnotice. F ease send your check and the white copy of attached formDEF-062A to:

New Jersey Department of EnvironmentalProtection , Energy CBureau of RevenueCN 417Trenton, NJ 08625-0417

You may contact Walter Janicek of the Bureau of EmergencyResponse at 201-669-3955 if you have any questions or require furtherinformation.

-.

Sincerely,

~.t?4f~ureau of Emergency Response

845340127

TIERRA-B-004549

DEPE·062A\0- oCheck here If Revised BllingDIVISION R • P • S. R. , \ FACIU'TY 10 NO. -----:----:-PROGRAMEMERGENCY RE SPONSE = ITYPE, 0F'''iP,,'''' r;] CoOt "_"" - D NO. 93-1 a-aS-Ill a

New Jersey Department of Environmental ProtectiOOand Energy

C ENFORCEMENT lNVOICE~

Docwnent ,,_---Dale Rcc'd __ --

Amount

DATE,· .ASSESSED·.'·"

Chemical Compounds Inc.29-75 Riverside Avenue

11/12/93ADMINIS~RATIVE COST RECOVERY

$866.47

DATE DUE:Malle check payable to: TrGasurer, State of New Jersey

" Mail to: NJDEPE. Bureau 01 RevenUee", 417, Trenton, M.J. 08625-0417

COpy DISTRIBUTION: Wl.itt' • Rt'mirranCt' Copy YdlolV· Company PillA: • Bureau oj Rt"'t'l/Ilt G(>/dt'nrod• Di,'j,sion

DECEMBER 30, 1993 ,... . AMOUNT DUE: S866.47

845340128

TIERRA-B-004550

NEW JERSEY DEPARTMENT OF ENVIRONMENTAL PROTECTION AND ENERGY~ BUREAO OF EMERGENCY RESPONSE

ADMINISTRATrvE COST RECOVERY WORK SHEET

CASE NAME: Chemical Compounds

PAC • V35RCASE t 93-10-05-0736

93-10-05-1110


REGULAR a.T.RESPONDER DATE RATE HOURS liMO RATE HOURS AMOUNT

8. Doyle l"g/5/93 64.43 3. 0" 193.29 104.03 0.5 52.01

J. Hoyle 10/5/93 60.66 3.0 '181.98 97.95 0.5 48.97••

.-

Req. Total = 375.27 O.T. Total = 100.98

REPORT:B. Doyle ~ 10/5/93 64.43 4.0 257.72

Report Total = 257.72

EQUIPMENT:Item: Amount c

HazCatOVADrager Tubes

75.0050.00

7.50

Equipment Total = 132.50

- TOTAL AMOUNT DUE = $B66.47

845340129

TIERRA-B-004551

- ...... .,i.-:': 1' ...

.,

... i·f

.~..~. -

New J8l'$ay Department of Environmental Protection and EnergyDivision of Facirl1y Wide Enforcement

Metra Bureau of Water & Hazardous Waate Enforcement2 Babcock Place, Wast Orange, N.J•. 070~

. (201) 669-3900

FWE.009_.:-: .11f1)2r

- "

\,

NOTICE OF VIOLATION:~;i~~.

':·":'10 NO. DATE >tip. Ilf. 1y.NAME 0 FACILITY C4:F--Mi Ct}--e- Cofl1{Jo lI\N I) s,T-~

~~OCATION ~F FACILlTYJ'- 7r r?i' .Iri.R.SII) ti... fh'. rJ ~~A1tt< tvt· tJ 7 I 0 c,L}

NAME OF OPERATOR A-L-Q 6:12..7" Ce:..L-i-U ~ - rl~€- S:b~-tJ-;--

-'You are he;by NOTIFIED that during my inspedlon of your facility on the above date, the follOwing

alleged violatlon(s) of the Solid Waste Management Act, tN.J.S.A. 13:1E-1 et seq.) and Regulations

(N.J.A.C.7:26-1 et seq.) promulgated thereunder were observed. These violatiQn(s) have been reooroed

as part of the permanent enforcement history of your facility.

......

'.

FacUIIyReceiP{J 7"..:,.. • d.

--:' ..:- 845340130

.. ..~~.~':

TIERRA-B-004552

New Jersey Department of Environmental Protection and EnergyDivision of Facil/ly Wide Enforcement

Metro Bureau of Water & Hazardous Waste Enforcement2 Babcock Place. West Orange, N.J. 07052

(201) 669-3900'"

'.. ,

,.r . .'

NOllCE OF VIOLATION

10 NO.t:.-l-D 1OJ: C' /"7 '37 . OAT~ 5'£P. I¥:9 V.NAME O~ FACILITYCM-~~CA-i- Co~POLt tJ~. kr .

LOCATION OF FACILlTY~ -7";- ~'I J.i4-S~ DC. J~. / fI/~~'f( ,..J ()7/ v ~I ()

NAME OF OPERATOR 1h..'!2~(l:i 0 efi<u""U~ - P,gf<;:/)';,J,--

You are herGbY NOTIFIED that during my inspection of your facility on the above date. the following

alleged violation(s) of the Solid Waste Management N::t. (N.J.S.A. 13:1E·1 at seq.) and Regulations

(N.J.A.C. 7:26-1 et seq.) promulgated thereunder were observed. These Ylolatl~n(s) have been recolded

as part of the permanent enforcement hlstolY of your facility.

'.,-

Remedial ac1lon to correc1 these violations must be initiated immediately and be colll>!eted by

o c-1'". I4- . '=t lI- : Wlhin Meen (15) days of receipt of this Notice of Violation, you

shall submit in writing. to the investigator Issuing this notice at the above address. the corrective measures

you have taken to attain compliance. The issuance of this doa.Iment serves as notice to)'Ou that a violation

has occurred and does not preclude the State of New Jersey, or any of its agencies from initiating further --

administratIVe or legal ac1ion. or from assessing penallles. with respect to this or other violatlo':!S. Violations

of these regulations are punishable by penalties of up to $50,000 per violation.

845340131.--_._-- - _ .... _ ...... _. __ •. u' __ ~ ._~...-_---_ .• --.-._ ..- ._- •._--_ •• - " ••• --.

TIERRA-B-004553

845340132

TIERRA-B-004554

·.· .. ·I,,,,....,M*:z.-.'·l;

~."

Slale of New JerseyDepartment of Environmental Protection

DivisIon of Hazardou, Wute ManagementManlle,t Section

/ . eN 028, Trenton; NJ08625..... bklclcIel'- (ponn dnl1lMd lor UN on elite (12-pltch) Iy~wn"r I-,

2. P.lli 1 /intormillon, in thl Ihlded .....of I l:w.not required by FIGlral

I~

iI-;:•e.iiIjI"i

1"'z -,1oS

If..IJ-II'Ia-

tII

III'11

I.!!

.-

--'

:'. s"'NMJanilAlltt ~mentNum~~''';';i~ ..(·,,;.:, ·~ur""~~:J,~;;:

B st.te <>-rate ... 10 '.-"':,'0;<_. ',' ""~'" ':

1-;:-~:;;:~::;~====,:,::=~--:;"';;:"'---:--";;;;;if----ii'C;""i:irrin::;.::=::-----1·".:~;':':' "~;·)~;~~·~):';~~~1f11·c. 51.tl Tran .. 10 oJ..•.t. "l~ J ~,c . (

I7. Tran$PQttlt :l ~mpany Naml 8. US E;PA10 Nutnblt

I I I I I I I I I I , Io.,Tnoll$poner"a Phollt t:;:,;;.; .. ~:, ;;~~~'Eo 5latl Tran •. IO '. ",' "' I,"'l:-" ·"r~';p

.~:'..... :.

~',.-. t·· • ,.

I 11, US DOT O.scr:ptIOo.(:r.cJuding Ptcpttf Shipping Name, HUlItC CUu, MId /0 Numt:~) j 12. C~nta,n.J3 i r~~alHM - t No. !Tyee: C:..:anHl'/

.' 'I. .,WasllNo.'

I i1-" ,""'.&\' ,-~ iL ~ 1-:' . "

.~,~'.,::: If/f.'iff y ~ ......,",,r-..::.",.rvil~J;'/e .!... ~ '- i W ,-£ Ie. i~r~~~~~·§1

I I' ,.~;'1.; I'i I.'~ ': I\"l'i· I

I .. I',.:... ·"'}-.. ~~,. .. 'olo..~ ...

I I I ·I~;~·(.}t

Q a, .... """N.h--+-......,! ---:::.....::-:...~~.:._;~~_=__.l...::::.....L:......l...=::':L:::::::l_=_l

~ ~'.I ..1;j: ~.l I

;

1I I ! !

! 1 i :

Ii I I

c.

IIId.i b." .. ,.. ... ...", d... b.

1$. Speci.' HaMling In$truCllons and Aaoitlonalinformatlon

A-

'I Sign.luno .. ' . '" ;,. ",: .'•• J I',...,.. ...... ~ ; ../ '.,-

'~~(,..'"

'Acnrll DIy YNI

J : I ' J t.0# ._ .....

;j ~T·:.:.. ...;7{:.:a:::n=SIl;:o;~~,'::.r~~~A;C::-~e::.c::"'.:.'.::.:c::.:~:.:• .:."';;:._n.:..rO;.,l_"I_• .:..C.;.,',;.~t.:.O.:..f_M:..a;.,te,;.r_'a_IS.:.... ,7i::::::::::_:--'-------~-:_- ==:-=-:--;;:~.lIl Print,....rTyped N&m8 " , .\fcnrll ~IIY Y."~N I -T' ,I _ " --:,.J"s ~,_,t~ \-", :.~":".:" t" _ If) ;1,":1;I~.

~ J.-:1:;8';...:.T:.:",:::n;;.PQ:.:,:tt;:..::,t:;2.;.A.::c;:Kn::._::.:.:;'.:,.d:::9:;8tn;::..:.;;.",;.t.:,of:..A_8C=Oi;;:P,;.I;;.of_""_I_1*l_·a_l_a---- .... -:c----:--; .....-----------------~.,....-__=-....,.,....-Jj ..: Pt,ntltdlTyped ~. Mom/l c.y Y.M Cr" I I I I I·! ~

lISi;n.tupi

~9. Discrepancv :nd:cal:cn 5paci _. ..

,;..) I ;.~I ;:. - r: .. i::' - ;-:.:- ,r: .... ':: ~ ! "="I,'. 845340133f (';ert:t.:.Au::t':"'-~·LD ~CT'"'])~~ 20. F.ci/ity 0_ or Operator: C.rIlficlllon of receipt 01 hezardous ma .. tlala colleflld by!hIs mantfMI8XC8pt u nOled i/llte/ll '8.

Y Pit;}}!-;'.Na,< _ • :..~ _, .' ; ::. ISlllnattuw -j-fr:;:':.,1'.. .. ' "::' - i~ •. '.'.w

EP,l For'" 8701J.-22(Rov.lIJU) P,..iau. lId'UOno"'_3 - TSD MAIL TO - GENERATOR

SIQNATU~( AND INFORMATION .vUSTBE L£GIBU! ON ALL COPIES

TIERRA-B-004555

I

fiII1

JiI

f5~IIi

.,;;··.~.·r

.-

.. - TSD fACILITY COPY

845340134

TIERRA-B-004556

9-4854870 P.03

845340135

TIERRA-B-004557

TO 9-48548'70 P.04

r-

=jI.I:j;

!Ij!if~o!

"1 GI.. t

I Ie

•I fl

i" ..T0.. ..

1~i1.!.;.::,

....iI~I•'If.IiII

II..I~.5s

o-a~.hdlll)' Name IHld t.Add"'" .' .

C/lJtI4IcAi- tl)AJ7'e.. ,VA.J?Jt::1'4 r.NTp elV .:fiE i&.i ~Y. J:..1 ;:..... (/

,,-1" ..t· ...p .... ~ .r. .. !""'"

11. US DoT Oeeenplion {~1Idi,.,.1'topIN Sllipping Na1rr'I, iiu.rt1 ClaD, Ifnd fO NurrrbM}HM . '.

b;

I/!JT ;f!.};!4 /;';1> ,,';,j r p;!,-:"/1. .'. :~ i .;..-: : oJ or ."

;,'t- O:\r'" ,.J,

f .....''''''''e~2Z,& - TSO f:AClllTY COPY

845340136

TIERRA-B-004558

t. T~lW~Com,p&nyN.m.e-::','.-.

·11,

c; L

r. ........II"tR II.

"T0

" It

D.£CA'JL· ~. 0?:J fw/HTE ,l'-'f4A-..n;:-·4-;;:' i.;} .n.#· ..~3·:

845340137

TIERRA-B-004559

AUG-07-199G FROM

Ir··IJII1.

fI•iIi

1i'

\;}'\ .. ::.... ' .,.':',1 . ·.:4 !

_ ,.", ~.. .. .;' ._~:4'." MoMh. '. r.... ~~~' . ~'I. ~(i·/.~ ;~~.-.:-,j _ .r~ /"/""".""

-845340138

TIERRA-B-004560

Stale of New JerserDepartment of EnvIronments Protectlon

CIvI.'on of Hazardou. Wa.te ManagemenlManlf •• 1 Section

CN 028, Trenton. NJ 08625_ Ple_ ryp. or prlnt InblockleltHL (Fo"" dul;n" lor 11M on ... Ie (U-pllchl typewrlt .. ,)

UNIFORM HAZARDOUS 1. Genlr.lor's US EPA to No.WASTE MANIFEST k:Ii J It!',a I I

5. T,anlportlr 1 Com pany Nam ..

I~ ,~'£1'--1 :0....::.:... A~'A~r.~J

L Tra"sporta, 2 Company Naml

G. Siale Facility'. 10 ...• .; :::.r.- .' t,:) H. ractllly'a Phon, 'I D

: 1. US DOT O•• c"pllon (fncludi"fl P!rIPM Shipping Miff"', HUJird CflJU. IIlId 10 NvmbBr/HM

12. C"ncaon .... I '3. '14, I •. ,.' I ., I ;olal i Umt . ,. .1

No. j ~"Il.i O"anlllY ;'NV'/ol' WII3te No;I

I ;, I

"1-1

J.

"",':"~. ·f •

b: b.15.

'6. GEHE1<ATOIl'S CERTIFICATION: I hl"by aecla'l1hal tn. conlents of Ihl, con,ignment arelllily Ind 1ccu,at.ly a.serite<: ~l:0Vtt oyprop.( 111Iopin\l n.ma ano a" c' .... fied, plICked.mlfl<ao. a"o libeled. and .rl In III ' •• pecl, in ptOpef ~onditlan lar ,r.:Jn.port ~y h:;:" .... yIccarding la applicabl. Intlmallonlland nalional oovemmanl reoul4tlono.III am • lorgo qllantity Olno"lar,1 cer1lty thetllUow a program in pllco to ntdllcolhe YQlumeand ~OXICity01WISlo oanlrate<l to tM dll9n." J ha .... ~"I"rmi"ec to oeeconamlcally Pf1lctic:able Ind thlll MV" .. lected lhe pract1C8.ote metnQd of treatmlnt. ~tarIO •. OfltllPClli cu'rently a.I"II:II. ta me wnlch ml"""l~"" Ih" prtnenl andfUlll" thr.etlO humlll hMllh end lhe ff1vitonment; OR, if I am I smail quentity Olnarator. Ihave maoe a 0°00 faith effort:o m,n,m,ZlI my w,ute 90nll'3t,on a"" ... 'ee!Ihe besl weste manl<,leme<11methQd lhet i. a\l1lilabla to ma aM tnall can a«oro.

:domn

:'l' '7. r'I~,po'r!"r 1 >,cknowledgemanl of Receipl of Melenals

A P~lnll<l1Tyt:8d Name·; ,- C t. 1="~ 18. T,an'llorter Z ACknowledgem'-nt QIReceipt of "'ellfil"~ PrlntadlTyped NameI!A

ISj;natc~.,.! /,::::.,;t>

r/

Month Day

:ll. Oiscrapency Inoicallan Spec.

845340139

Mont" Dsy YHI'

, fEPA Form 8700-22 (R... ~381 P<oviou. edi'loN ... _

8 - GENERATOR'COPYSIGNATURE AND INFORMATION MUSTSE l.EGISLE ON AU COPIES

TIERRA-B-004561

1.

us oor De~C11puoo..[lncluding PtopK s,~/ppi;,gNllm., Huard Cia.,., Vld 10 Numb,,'tH~ ;'

(.,/.~. /;,./. " .....1. ::4A,·-·':'~.-f::O'J5 ~"l}~);.~ .:~.;./-l j:i'~' ~~"-..4 ,'",:.:""••~,.;

11.

Qa.

EN

"R b.II.

T<)

A-:.

II

d.I

I'1

.'; -.;':.

~e. GENERATOR'S CERTIFICAnON: I he",Oy dec,erelhallhe contents of Ihla con,ignment a lIy and aecuralely described above byDroper shipping name and are cl.a.ified, peeked, marke<l, end labeted, and are in aU respecb In pre par condition lor transport by highwayaceercllng to <>ppllcable Intemalional and nbllenal governmenl regulations. .It lem elarge quantify generalbr, Icertify Ihall haye e pr~tam In place 10 reducell1eyolume and loxlclty of wa.t. genereled to the degr ... 1have delermined 10beeconomlcelly preclicabte andlhell haye .electad lI1e practicable method o1lrea,men!, ~Iorag., or disposal currently ... lIablelo me which minimll •• lhe presen.endlulur. Ihralll :e humen he.llh and the environment; OR, If Iam a amall quantify generelOt,' haye m.de a good '.lth eltort 10minimize my we.laganaralion and ",le<:1lhe be.t weste management med'Iod lI1ell' eYenable 10 me and thaI I c;an a,fQRI,' ..' .

;;

Ii';;

i.Ii

TIERRA-B-004562

Stat, of New Jene,Department of Envlronmenta Protectlon

DivIsion of Hazardous Waite Management. Manifest SectioneN 028, Trenfon, NJ 08525

,>;"~,,u ~[;'" \I' prl"tl" block lelte'" (Form d•• III"..1 f\lr .... on ellle (12·pllc"llyp ... rll.r.)_ .....-: 1. Generator'. US EPA 10 No.

;, :i ~•

. ...._ '1_·:'74~.~t~·.~~:,Form Appta>M1 OMS No. ~:,!XpltN ~

Informallon'ln tl"'flclfl:Jrl

"'::~2,.~~~~~~;""=~_.l!~::.LI~.I£..u:2l:.U~l6ll.!..uw.~'-~~:J.:~~£1h';'h...,.,..J,"'::I:W."OI re.~;U,l{~~Ar~.:

[;'1 ' :.1\ '! d

I I;! II

:f it wfhti, t<-o • 0 T AC:d.\lOnBIO- P.I one r a' a ' •

~;l 1::.l/;;H/£.!t!Jt1;;'~~~ ; ~ n - ~.~~~i~ii*~~.-~,,-: ;\ "'.1l ,,'; ~t~·..: : Cia. \l~ee ..,1 Handling InotrlJctlOlJo ond A

1:1 ~::t{~;:~.- -I !r

t3. CF.t-IE/1ATOR"S CERTlfICAnON: I "I "by declare Ihllthe contenle olthll cona1llnmentare 1~lly and accur.toly dttCllbed above by.' .':

• . prepel $hlpplnll name Ind ate CII.. IlIed, pICked. merked. and l.b.led. Ind arl In all reapeets In proper condition for Iranlport by highwayI ,"~,,,diIl1l10 applicable InternaUon.1 .nd nlUonal government rogulatlone. :. . • .•

III P,rTl a lorgo QUlnllly genetetor, I certify 1~111"Ive I progrlm In pilei to red ..ce t/ll volume Ind toxicity 01waale oo".rall" to Ihe degtle I hivi determined to !, ~~onomlcally practlcebl. and Illati "eVllliee1ecl the pllctk:able m.thod oflreltmen~ .torege. ordlapoul currenUy a.llllbll 10me which mlnlmlzOI Ih. preH"1 ae

i, \ IUI~rllhre.llohum.n h.. lthand the.nvlronment: OR, Illam .amlnQuentlty,fcdt18r.tor,IIIIVllMde I good IlltheHort to mlnlmtzl my wllte generallon and aeloi-- IhI>bul waote mlnallement method that II a.llIeblelo 1M and that I can a old. ' , ' .' .' . " "/ :,' '.: ,;' "'i',',' ·,(~i~-1,';

'.

I

" .' '. ...!~..-M .• ':"f'

,P)$J:i7 ISlg"~A lJc': ..AI I~........iA' .......Motlth; ...o.y \

I £. Su LL,'VA0 "'~ ·",·':·~';f~i'("i1017.- ,,,,,sporte, 1 Acknowledgement 01 Receipl 01 Mellnlll

, -,'~';~;i: '-"::'~~-f,.:

17.

~.. _~".; ,

H !'rinta::JT IPId Name ISionanu--.. Motllh DJty ,

l~.. - '( :.i ','j \' I

;.

ii1<.1. TroMportor 2 Acknowledgement of ReceIpt of M•• eril"

,. . ~:';1":..,._~:~;_. -

, Prin~YP~ N~e1Sl9natu·e

.",' ,: ' .. ::.'l-~'==~,l~I!J)OIY

..," " ",,~(~:.lf,.•r,' i I

I 19, Discrepancy Indication Spac;lJ

~ 845340141Ac

.I , . , . ,;,.._..._...~:-::~;;cr';~:1.~-.

l. . '-..

.-:.~

I,20 .. Facility, Owner Of Operllor: CMtIfieatlon of reeelpi of haurdoul mll.,lall CoYlred by thlo mlit\lIelle~coplea noted In 111m 18, '\'~""':['~~ei1'll~-

Tr ._~}~~ir~~.~'~:·'~J~~:~t~:'

\ Slgnllure'~ ' •. " ',' :," i7~~Month-«DJty

...;, ''='',~ .. .' ~', 't-O'.,~ • •..~.. '~. •- ... , .... ~ .,;Mt"o\~t~ .. ~~" I

" .'

.". , ..._. ."",,"f , .. ,-.."~~.~'",!~I~;~,~ odI~ ~~.. SIGN.&TURE AfoIO INfORMATION MUSTSE LEGIBL£OH~COPr~JS.o .M~IL;:,!,O·='~SD·S.STATE . ' ':'~~>' ..;P~;·~:~~(';p''{/

. ~.......__ ~__ .• _ , ._ ~_ • .............- --r' - -,- --- - -- - - - - -.-- _ ...--.---. _.-.-

--...--- ....

TIERRA-B-004563

.... '..

11. t;S.OOT Description (("eluding Propsr Sh(ppir.r,/. Nsm8, HSl!8ro Class, and ;D Numosr)11,...,"':.. --~. ',:-'~::: ~-".",~.

G

ENE '.

RJ.

raR 1-_~_-I----,!..-_.......... --:'_--------+J...:J...:+...l-f:-L-.L.-LcL...;.~~

..

...... J

j/jz..A it I!)C/~

. . //II-~>/I':~b.

c.

II.-:--!---+----~-----+-J-l-~.J....:_+_:_I·

.-

<l. i

I 1>.

1S.

,.i.\ ' i-i:- / 2...,0. GENERATOR'S CERTIFICAnON: I herllby d"clere that the conlents ollhl. consignment are tully and accurately rlesclibed above by

proper .h:;>olng m.m" and are claS3ilrltO, packed. markea. and laoeled. ami ~re in all r".peelS in proper condition for transporllly highwayaccording to applicable internallonal and nauonel govefllm.nt regulatIOns. .'111 am a large Quantity generator;1 certify that I heve a progrem In place to reducethll volume and toalclty of waste generated to the degre" I have detennfned to b.economically praclicable aM that I hevel s"llJCted th" practicable methoc 01 trealment, storage. or dlspo8a1 currenlly available to m& which ml~imiz .. the preeent a(l(llulur8 Ihre.1 to human he.Uh and the environm"nt; OR, if I am a small quantlty~erator.1 havel made a gOOd faith elfort to minimlra my wasla ganaratlon and Hlac:lIIa best wasle managemant m!,thod thatls available 10 me and thall can a. - .' ...•..: ., '. '. .'

~.."...;..;.~~;;~?,:~'.'.'.' ;,.,--"-

19. Oiscr.parn;y h'di(;ll~onSpace' '.' .... .', . - .... , " c~.. ' .,":,:'~ .. :'j·'>~~t4,~~~::>fi·'~·:~;·l:·::·:-.jJh.~t,:la;e·."~"'--""'-<<<~~"" ...•

paratQr;e..rti~cellon .ofrecelpt~f ll~rd~!1'8tarlals COVtlfedlly.lhfrlllaleaty,i;&ilt,.8 noted I/lllem

~~gmit~~.,//.~..~..~~V.·..~·:~:'~~;.~-::7-;..... '.~>'";';--'.".._..~t' .~- Y - /~.< ··f

. SIGNATURE AND INFORMATION'MUSriurl ..EGlat.EON ALL'COP1E:

~'i . ....,.~-•. '~'-':"" .. ;.-:> - .

:j.;r£~~ii:~;1:·j;:;~ 845340142

TIERRA-B-004564

----' -~_. • - 'fi~~- ~:"fi":"""'-~· __ ~

:6_ GENERATOR'S CERTIFICATION; I hereby declere lhat lhe conlenls at lhis consignmMt are tully and aCCljrale!y describod abov<I b-(: I .,cper '~'Pr.ir'il n""'d at1<;1are cla •• ,liM. packed, mafl<ed, aM laDeled, and are in all respects in properCol\dilion lor transport by highwayi according to applicable inlernational an<! nallonal govarnment regulations.

"

If I am a largo quanHly generator, Icertlly Ihall have a program in placalo reduca Ihe voiume and toxlcily 01 wasla genarated 10Ihe degree Ihave determined 10be"",onomlcally practicable and Ihall hava selecled the practicable melhod 01trealment. storage. or disposal CLlrrenllyavailabie to me whicn minimizes the present andfuture Ihre.llo human Mallh and Ihe environment; OR,lf I am a sm.1I quanlily generator,l have mede e good faith eflort 10minimiza my waste generation aM .el.,;tthe besl waSle management meltlcd IhallS available to me and Ihat I can alford. - _ -

. ,-

TIERRA-B-004565

~:

....·::-i.,,:goment of R.~.ipl 01 Malotlafs., :1_

.;:;;:-;,::;::;.:; ;"""cw!odgamenl01 Recelpt of.Matarlals .,

..; - ..'-<.-

. ~.,~~utooJUon, .if. obIottto.; • TSD;S'STATE . ..

TIERRA-B-004566

3.

7/~'~1. V$ Oc;i De::::;np:ma 1;;,C:(/!1li1; Fr:;.psr $.'fi;;;;;:1g .J.~(3:nO.Hutira ~f;:$':. ,1r:c';;; Num!':~~:l·

HM - o. fPe uan! .,

-;fA zA I~d e-t.l S. r:J.- ,-I U.--- .LJ 0' -

a, A/ .::;/.'/ ~. " -' , ..,.

1 .:::..,'''' "-'.

f) ,i ,:; 1/1/ ..1 S r6 vl':Ai5.f\ ;~!O,r -rrf 0151010,0 & xi;r,;itJ:;',

Ib, I !

I t..~·::.-1''''t - ,.) :-.,- r~-\i.' - .. ~ ~I :-',.'';/ -'l- i ....... ''';'

j i I I I I I t ",;j',.! :'-1I

I

'1 c. I ! I I I .

f

Ge-N

AA

ToR

I

i! I,

1.Ii

IGg

Iii".:Ii

'3..)i~

f•Ii,.:II=

j

I I I I I i I

..I.·:I~"';' "r:;:

, .,...:'{t-.t .I::, ....']. ~-z:;.,'.--'

Mon,h 031 \,~c

I :.,;;, 2k1/'

'/.cNamil1A,;"'~

Transporter 2 Acknowledgement of Receipl-pf Materials

P,inla<IfTyped Name:'.· f' 0:. ." :.:c:, Month Day Ye~:ISignatureI

19. Oiscrepa",.~/lndicatlon Space

'F''';·5~· ,..... A;:',J;,,~,,c".<!",.,,: t l-,,"""-::-...,,~"::""--:--:~::::==~::::;:::::i=:-::~:::-:;;:::::::;:...-::-::=::;:::::-:':':':::::::-::~~r:::Z::::===~::::::-~:::;'i-":~"';';;"";""''';';':'''"''"'~----~r::;:t\-":='':';'=~;':':''';'::~~i:-~===":::':'e:-:=i''::"''c_;''''--_'':'''''''';''-'''-;::--'-:''''''';'';'''::'':;,;...f:::--;:4.:..:;,-'--:-;''''--:'':'':'_':'''':':':':'''';:':'''':-_--:''''':--.."..---

c~:.}L..I-.~-:'l!;"''':::::~-+'~:-:-....A~~~ ... ~_;'';'~ __ ...!l:=:;''''_....i__ '';:';__ ';'''-=;';;''';;;;;';;_'':'' __ '-;''' ':''''''::::!....J.:...;L...lo:.:..l::..~

845340145.-~ _.;.:

.,.--~~,:..;};-.i~.~;';~~~1.~.~,:.~...~\lOItth Oii]J..,,-¥";;'/' I) '\ " r-o

~..V~.l ,J \ f J_SIGNATURE AN!> INFORMATION MU$rBElEGIBLE ON All CCPIE::

____ ... __ 11 '_.II! _ ......_u

TIERRA-B-004567

---"!''',~llllEV._f'. -~.' .~.'R '/' ~Iate of New Jerse,'1,;'" .'~ • : Department of Environments Protection

~ t: OlV,lsion of. Aazardoul Watte Management

'_ -". .::./-T... " ," .; ,,~- cit~~::\;:.c~~~8625-. "l.... ty ... 'C;',poMI In block le«erw.IFormdollgn.d ter UP on .111. (12·j>llchi ty ... writer.)

....UNIFORM HAZAROOUS 1: Generator's \JS .EPA fP ~o.'." :WASTE MANifEST ,-." .... ;.' . ". ' .

3., G..en~raIO(' Nameand.Me'ling Addr.~~ .,'::' ..:

.:...C~:C.OMPO~ ,.~c.'"'''' .<-. ·.:,c:.~·.::'..; %9~j5·1UWRSI.CE AVE~.1!LOG.l.l,N:EWARX,NJ 0710'4-4:'Ge~r3io";s FI10ne (.. } f::" ; . . .

~~.,!l~as£•.1tAnaqcmfJn~ ..::t:f'C. 6.""" :. - . ~". .

\JS EPA 10NU"'''''f

I I9.' Casl\:nated Facility Name and Sile Address'clmMICAL WASTE Mrt.~AGEMENT. lo6t.ISnR AVs:., '. .

~.-ii'..JiK,' NEW m,.ggy 07105

10. USEi'A 10Nu",!)"ror }.-z:w n:RSE.Y:tfl::.. F. Trensportor'3 Phone ( .

G. Stale Fa£illr(. 10, 'H.• ::ac:tit'{s Phcr:s t

1'" US OCT OesC':'iplj~ ;Ji.c!u:1ing Pr;;~er $h:t;;lr.g Ns.~e. ,<":'.e..zardC:asf:. ~nr: if) Numb~')HM ",

'12. G:vntalr.tHs 't 3.I T~tal

I'~J. '7,pa i :~3rti:-!

l!l'AFo<"'!7~~l...~;~88I!'~':l""iti"'''''~_'' SIGNAT\1iU;'AND INFORMATION MUSTBE LEGIBLE ON ALlICOPIES3 - TSO MAIL TO· GENERATOR

..-

a. iI

Ib. I

I

NON-lL,\1AP.ooU$ .Dn WASH WATERNOT R3GOLA:rED BY 49CPR

c.

l·d.

10' '.,~cll',>:. {

;:;. SpGClal Handling 1~51ructio~. and Acoitionallnformalion

DECAL MO.:5. GENERATOR'S CERTIFICATION: I hereby decla,~<5l It.etenlents of Ihis cens,,,nmenl are lully a1'0 .cc::r31ely cesc,'bl1d doc'Je::;y

proper shipping name and ara claS3itied. pacl<ed. marked, and labeled, and are in all ",.p~IS in proper condilion tor transport by highwayaccoro:ng 10 applicable !"temalional md national goyernment regulations.. .'. •If Ia~ a large quantitY9"""taIOf,1 certify that I heve a program In place to f1!!luce the volume aM !O,ciclty ot wUle genaralad 10 thed.gree I have determined to beeconorn,,:aHy precticaDloaM!IllIt Iha.". selllcl"d Ihe practicable method of treatment, lIo,ag&, Of dISposal cllrranliy aYailable tome-which mlniml~'" the present sndtutll'.mraal10 human health ano!llll environment OR,:f I am a smell quanllty genaralOr,l have mades geod faith effort to mimmile my wosle generation and seleetIlle best '~asle man:lgo",er.t ,,-:.thod ~~~t il ava.:aole to me ."0 thaI I can afford,

Pnnleo;Typeo Name

I.Sig~a!l:(e .. .MonrJ1 OilY. Y"lIr

19. O,screp .."c:y Indication Spa.:e

TIERRA-B-004568

I.Wasla No.

Special Hnndling Inslruc:lons and ACllitional InformatiO(l

~iAS'::E ~RCFILE NO.

'6, CENERATOR'S CERT;FIC.l.TlON: I ~ereby eclere t~al :he.:ontantsottnis cons;gnrrenu,&fuliy and aoo~r!.I.'y oescri""c acove bv;;rc.pat $tuopin; ~Sr.HJ ana are c'l.Siified . .pack ad. rnarl<:ed. and lat9-ted! anQ ar9 in -lit ,es.peels in prc~er <:onCI~:on fQr transport by hignwayaccorll,ng to ap?li~ol. internationel aM nalional go .. ,:,:,ment rogulatlcns .. ' .~~If I am a large c;uanlity gen"ralor.1 certify that I ha"e a program in ~lac8lo r!duce Ihe vo!um'tlIr.d tcxicity of waste gan.rated 10the degree! have delermlned to :-eeconomIcally pracliable and :hat I h.v. ,.lactO<! the pracllcable melllCXlof !to.lment, sIPrage. "r dispo •• , cutfently ovailabl. to '"" ....hlch mihmlzes Ihe present andlulure ,nreat to numan heallh ana the environment OR,if lam a sm.lI q"ar.tity. generator. Ih.ve m.dee good lilith effort to minimize my waste generation and selectIhlj be,t wille management me!tlOdlhalls ... 1181>1810 me and 'hat Icanalfora.

I S'~r.Q!~re ,. Mor.rh ;;~y '1<13.-,

• ;/rf 1:11 ~ ~:4 i

".10f1ff! O~y

845340147

en. fQ...e'1lio-~~ 1~"'.jI8lll P,.. lO\A ~;ti""""_3 - TSD MAIL TO. GENERATOR

TIERRA-B-004569

'"V '. SI.",'N•• J."",~,~" Department of Envli'onmentaf Protection~' Division 01 Hazardous Waste Management

\~ Mamfest SecUon"', .. '\ . eN 028, Trenton, NJ 08625

1'1•••• typo orprl ... I.. block I.tl.n. (Fonndo.lg ..... 'or u.o 0" 0111. (1:Z·pllohllyp ... rll.r.) Form Approve<J.OMS No. 2050-0039. £.<;;ir".9-:

,II

tk,,.

--I..iIie..I...~ I(j I

¥QE !

;II N

I eRA

! T0.. R

l~~~

UNIFORM HAZARDOUS I T. G8nerato(s us EPA 10 No. ' Mani'.$!WASTE MANIFEST ! .u:T1'1\1/1 "'I1..<'1...;,·i..1 J ,.,1'"2".,,5.°,:-r:rlnc;, 2. Page 1 I. Intorma"on in 11>8snadr, are

ot I /'l:w.not require.: by ede'

a. Stal$ G9I1.ralol'110 •

'S~~~ez .

C. Slal~ Trans. to _151 II ri "lI 'I7. TransportBr 2. Company Name - 8, US'E?A 10 Number 0, TllInsporte(s Phone ( -J. ... ,) ill'r..:. , I

E. Stat. Trans: /0 e;·' ,M'·. '(C1' '.' I c'I" I .. ,I I ! I , I f I I I I I9. Oesignate<l Facility Naffie and Sile AdarB$$r.I_~f· ,..,,:"" .•/, ,_~J, •.... ~ ...._.. ...-.,...,..41:"':#-.' .....,.,...-"- .v...., ...f i! ~,.....,..-..J ,}:;.r-,.~."'t'

,...,.... ,:...J._ ."''';;: r;:~' .......; ~I~ll-";;' ."4,,.::;.-0 ..t,"'-.,,,,·._"'" ~J- .tI"I-""..-;...-

10. US "PAlO Number

/</r.-' } 'r;" 'c'" YJ:.r'.0 F. Transporte(a Phone (.... ." _~ ....r_I_...), .

- G. Stete Fecillly's 10I .,~. .-r ., -:i 71.:;0'1 ! f II:"! ;I "fj1 n H. Facility's Phone (

.

J -.' £ -' .....

TT. US OCT Oesc,iption ilnc!uf1i"g Prc:;er Shipping Name. l-1=aro elJ:;!l, ."" 10 'lumber)HM _

'12, Comainers I 13., I Total

No. : Type , Quant'~1! J~i~! . I:IWl/Voil Wasle No.

a. ...-~ ,! .-

".1' . ~'l ... ) I"; I II 'I I i I I J I I I f I~I ..I·j

d,

.-:1.·· ..~.,-.';"

I II , I I I 1 I I I '.' I I ·i.

• rJ

;.":./ ; ',-

i J. Adaltlona' C.ncnpHoo. lor Materials Listed Above,

; '" .... '0'-.-..;.,.1' p.~ , (- ~d1;':"'i ,.rt~.~t:I-/ ~"""'.~ i"A 0"'1,.' ~'4 '•• n ~ .! s.·,· f C.

L,:;::cling Ci~10' jutes :'sted ,\Cove

I~·u-Ylc .. ' I',.

. }; , /;

o.,i 15. Special Hanollng Ir.struc:ians and AcdUionallnlormalion.

J -f. ~:: ::;-;;.I~ ':::Jlv' :: 1Z ~ ,-", :...:.1 .~.:!-. __ ~.-..-- .-~' ..I ".,'"..

I :;...-;;:;-::;-"l< __

,i I.. "" # l"

16. GENERATOR'S CERTlfIC.lTICN: I he,eby ~ec:aro thar ~r.e CCNen\S "t tnis ccnsi"mMnt are tUlly aM acoura,e/y ouc"bed aoove,yproper :;hippmg n3me ana 3'H Classified, pacxed, marKee. at",a :at9i.fJd. ana 3r! in ail respects in pro~er c:::;ndition tor transport 'by t'llghwayacc;:,rctng to a;policsbte ir\:ernationalllild nanonat -government :e~uj.:ltlO"',It lem a large quantity gene,ator, Icertify Ihall have a progr:lm in placalo reduce the volume end :o.icit( of wa.te gei'eraled to lh&aeqr ..... I have aOlermlned to ~economic-ally practicab~e ana thai ~h3\1e setected the praCticable melhod of !ftIa1menl. ,Iorage. or orspo:sal currOl1tfy available to mewn~cn mtnJmizes the pra$~nt anafutur& Ih'Bal to human health and the eovironment; OR, it Iam a small quanti~19Bneralor,1 have made a gooa tallh dlfort to minimize my wasle 98n&rallOn ana ie/BCI

'Ihe best waste'management malhoalhat is avallaDle tome ano thall can atford.

Is;~nalu,e , ,I ,: ..

J "

Mor.t!l Cay YU:·

I -I " ~I ~I i

I ,../I i. Momh Ci'Y Ye.iF

I .-l -" ..I ~I<Gi_ f

- '!t~ '5.' T,ansponet 2"'Acknow/eagemenl 01 Receipt at Maten.l.~ PrlntedlTyp&Ct NametR

ISignatu,e .Month Cay YearItI I J I I ! I:

'- 84534014819. Discrepar:C"/lnoicalion Spaca

FAeI

~ h;lO"..•...".fa-C."il~ll-y~O,..w-n-e-ror......,O::"fH'-'''Cal-o-r.";:C~&r1J~'li,..ca''":lI~on-O-:.-rece---.,...ip-:I-O:-:thaza=-ro=o-u.:-m--::el~e'::ri:-:al:-~.:'cpve==red:-::-::by~U1:-;Ia:-:::ma":'":"nl':'fft=-1:-e~-:c':"e"':PI~a-:a"':no=t.a"':"l"ln--::lle:-:m:-:T::g.-----------"·

£1'... Fa"" 8100-22 {R... 9IlIll) P"",k>UI .dlll ....... ..-~.

3 - TSD MAIL TO. GENERATOR 'SIGHA1"UJ:iE AND INFORMATION MUSTBE LEGIBLE ON ALL COP1ES

TIERRA-B-004570

. - fj""'" '?~'"",'~'::," ..Depar1me;'t~~eEc:;yrr~~~:~~,:rProteellon. ' ,. ':., Division of Hazardous Waste·Management. .. .~.... Manilest Section·

. ..,;:.~<.,".~' .. ". ,._: .. ' . CN028, Trenton, NJ 08625Pl .... typaM'pdnlln block leit ..... (Form de~n.d lor Ill. on .1I1e (1'·pllchl typewrtter.)

...'"g~l:!

i!ie.

!...ii•0et..i!Ill:..'0itt!l;¥& -1Ji

1..0..i!fi.!!=...J:;o

i!iill"l;

i

tIi..i.!:

-

Fonrr ",ppfO~ OMS No. 205o-<XJJ'J.E;tpi," 9-Jo.-r;

3. '1aimeralotl NO)<\lI...,d MaIling Adoresa' -':'!"'~'" .. ":'f .. ~ ~................ . ..

CREMl~ .COMPOUl'IDS lye •29-75 RIVV-RSIDE AVE, BLDG.17,NEWARK,NJ 07104

4. GeneratatsPhane( 201 ) 485-3212 ..$. Transport"r I Company Nam. 6. US EPA 10 Numb.r

"" ....~.~ .. ,....... ~.... 11'",,"hd41It ....j.,d..,~ r I I IB. US Ei'A 10Numbe,

I I I I I I I I I I I I10. US EPA 10 Number

C. Slate Trana.IO c "" .. A'''.I ; 1': ',.D. Tran.porle"'s Phone ( , :;'i' .

E. Stat.Trans.ID·,oio. ';';~'~F~;l~"L("r,;T"'..f I

'". ':.,

0,.,. .,.,.. ·-as-" ±,,-y- F. Tran.porle .... Phone(..' .w.if u'::; ;:. ~ I "- , r::-:-:::-:-'-::-,-.-:-::-..:...---"-..,------..;G: Siale Facility's 10

GeN

..b.

,

j 'L

NO. H~70/.:; ;).1. 3

00

II, 16.

!

i

!

GENERATOR'S CERTIFICA I'IO.N: I hereby 1e~lltfe thallne C<lnlenlS at tillS con.19nment are fully ana accuralely oescribed'abo". byprocer 3h'pPln9 name and are claSSlhir/l. paCKea, mer.ea, and labeled •• nd are on .11 'espocts In proper cond.t.on 'af transport Oy highwayaccarcing to applicable Intern.tona' and r.ellcr.al government regulations.III am a larg. Quantity generator. I cettilylhat I have e prcgram in plac8to reduca the volume and loxicity ot waste generale<l to tha degree I have determined 10boeconomically p.acticabl" and thaI I have selecte<lthe oractlcpole mothO<l01treatm.nt, storage. O1dl.posal currenlly a.ailable to 1M which mini mites the present and1uturethreal 1/,numan heelth and the .""oronmenl; OR, it Iam um.1I quentlty generator,l have made a good la,thaltotl to minimize my waste ganeretJlm ana seldCt"Ih.b8'lt wasta meneg.ment method tnet i. available to me and thaI Ican atlord. .

.wotlrn OilY 'fur

1~1t~d.·.,1 I

19. Discrepancy Indicalion Space

ISignat~re..</1

..

".,

J ~ I"

., .-ISignalure ./ / ~'j I,-"",",,",;,<

,/ ..... '-"ISi9nalure.

." . ... _..

IWon1h C,;y 'foaf'

,.':'l.t.,4;....,491-:- _•

MOlltll DBy Yur C:I I I I I I l

PnnlltOlTypod Name

Yl.F.OLO ". ;':<1T.;".m,.:~! 17. Transporter 1 ACKnOWledgement of MiCalpl ~i Mat.tlals

.. I ,Pr:nl~eLlarr.yp.,g Nall>f "H ......l'!...... • • -s (~L~ "" ~ ~, -, - •:; 18. Transponer 2 Acl<nOwledgem .... 1of Receipt of Material.

~ PnntedlTypa<1 NameER

845340149

.. .=...-:'"41GNATURE AND INFORMAnOH MUSTBE t:EGIBLE ON ALL'COPf£S

3 - TSD MAIL TO • GENERATOR

II

-. <-~ ... '

TIERRA-B-004571

'9" Slale of New JerserDepartment of Envlronmenta Protection

'I~-.w..~~ Division of HMZ:~~~~tS:~~~enManagement

, , . eN 028, Trenton, NJ 08625PI... pe or print In b!QCkItlle ..... 'Form designed lor UI. on eill. (12·pll""1 typewriter.)

,.. UNIFORM HAZAR DOUS I" Generato,.. us EPA 10 No. Manif.stWASTE MANIFEST J 1. I .1 j , I I I I I I ~oc~mert ~o.

i 3. Gener.:nors Name and MB~lin~ Aodruss ....01' W..,. .. v ~ 0 0 J. I J ~ U V r,J J.-

2. Page 1 I lnforms"on in the .nadeo arass01 I:w.not required by Federal

I· I :2. Cant .. n.,. j 'J. .ill".UVA/Oa-lf .LUU• I '. US OCT Cescro;>t;on(1.~cllJ(Jin.;; ProcerSh;pping Name. Hazst<J Cias.s. and /0 No'meet' I I Tetal ' Unil i':' .,,;'-

:-'M _ : ~o. i ,yOO) , Goar-lily !WWOII WasteNo. "

::! a. i.:1 I.. . I i:iON-j'L].Zi\r'WCt:3 "'lvo;:- ~rn.STE ';:ATER

j tlC"!.' !~GL."L''1'::O £IT 49~O'i

j .. 'i ...T-I.l~·k~1"n'.~!-:::---.....j.---------------------------+=f--+..:!J~~hH,L!J-.~.;J-";;'-+-Jl;.L.~UW-lJl.I..

::>~I-:~-+------:------------------'-'--'--'--'~-..l--'----:'--:"-I.._-L-..:J~.J..--!.,--Ic ! i

I , II I f

I II I, I ! I I ; ~~:~~r~:,r:J. Aoaillon.' CIl'!f:r1pf\on3"lClT'l"irtIlr\a~s !:!sl<l<rl>o.~tI ' .. K. Hanoling Codes fer Wast". ~I.ted Above ..

.;~I~~I~4i~J:I~~1e,~!1)~?:;;~~~~~~c;p~~Yl~:IlA~(~.D1a~~t. e.,;,,~i~V~t·;':, ,'> ..... ,,; .

, " :. ".

III

I I

d. '-lI'

.,."'"'. Ib. d.

':5. Special Mandling Instructioo. and AO£litlonat Iniotmat,on

~mRK CRD£it

C.i:CAL 'NO.

:20.- .......~~------

Mon", C...y Y•• t

1t>ft.J I J 'iI 19 '1..'. ---, , .. ........, .. ! ......

1:" ",'3t';'SCCr.'l!f"~ ACliCr.Ow19'Cg-eme"t :)1 F;~e~ct ~f '.1a~-o-nal'"

,::;~:r,t(k::/7 tPIlO ,'l ...~e ........ ; Signac\,;re

I .; ........-...:' ."

ISignatuttl

19. Cisctepancy Indicalion Space-- 845340150

E:PA.".,m &1n(l..~ (R••• QlIl41 P.... ,.ua ad"'",," ""'_

8 - GENERATOR COpySIGNATURE AND INFORMATION MUSTBE L£GI8LEON ALL COPIES

TIERRA-B-004572

0,,,,/3 No. 2050-0039. ~. Ne·;

InfOlmatlon '" tha snaGe<! a,ea.• hy Fedara.

11. US DOT Daser;plio~ (/nctl:cJlng Prope!' SN;;plng Name •. "iaard Ctass. and tD Nu:".,a'/HM ~ '.

c.

CONTAINS UA'rE:R - 65

; .. \'I~l-:--:-_+-:,:::,,::-~:"::"=:';"::"::':::"""';::"='~"::'-~":""" -'-- f-9I~~~j,:...j-y.e.~.JU.,l,j,1,L+-'~i-JI~WJ~.Ll..l-AT~b--,-_-+-- f-:-""-L-..;~~-C.-.I.--l."'-:'-l-_...J...;:....l'---L---l-

BON-aAZARDOtJS Dn' WASH WATERNOT RE:GU!Jl.'l'ZD BY 49CPR

li5iJ'I

II;0

fi'lI

I.s

J.• A~<1I~IOn~~~i~)l'~Ab.~~...•. ~': ::.A!21'It01iXnK .S'l'Jl.oYAD. ,.. '

a, .," . ,,

PROPILB NO. K32~92

CECAL ffO1

1·16. GENERATOR'S CERT1FlCA nON: lnersby de<; are mat me contenu 0 t ISconsignment a'a fully and aecurotaly deSCribed above by

p,oca! shipping nama anO are clasSIfied, packll<l, ma'kee. and labeleo, an" are in all ,espad. in propar oemlillon for transport by hignwayaccording to applicable international and r.atlona! govammant ,egulatlons.If j am a la,ge quantity geM,ato,. Icertily that IMve a ;>'og~m in place to ,educe 1M VOIUmaana .lO~icityof wasta gana,alse 10 lhe degree Ihave dalermined te ~e~onomicaHy prllc!icable and Illa.!Ihave wle<:la<l lh. pract;"".,le method cf trealment, $Io'age. or d'$posal currently avallaDla to ma ",hien mlnirr.'zes lhe present ar.ofulura,nreal to human Mallh ano the environment; OR, If lam a small quantily genarlltor,l have matle a good faith atl0:110 minimize my wastegensr&bOn aM selectlha baSt waste management matho<llhat is availabla to me and t!lat I can af1ord. . /)

I .r.i :"

MO(lIn Day

I

Signature\.

845340151-I~~~;;;a::~~~~:--:-::-:,=:-.:"'r:--.:-~:---rS;;;;;;;;;;;;;-:7t:;""'7:-~-:-;:---.----.r.:::;;;-:t:;:;;--v.;:;;

EPIl. Form B1QO-a~.lIIB8t~~ od_~~ .,,;"::...:'"~.~'•

3.- TSD MAIL TO - GENERATOR". .-...<-~- . --:-~..-.:' ..

TIERRA-B-004573

:llill~iiGo

"!"..e"0EIII

'0..Go..C

~,.-.

;..!l

1Iti!'I•&!J!i'.1II:0..~~Ii'0. i- .s

"

I 3. G8neratq(, Name ana Mailing Address .

I C!:1U1::CAL COMPOUNDS nqC •.I 29-75 RrrnRSIDS >'VS.,.I 4. G""eralo(s Phone I' }.I 5. Tr_nsporlar 1Compa"y Nam.

! W:~~~~~~~~rr....2Y:.-.iJL-!!J!~YI:.:~~J!LJ~~~~~fiI 1.

:~.....,:--_..,.-.."....=-:-:-=--:-~:C:7.:':=------.L;;t-...l-...l--;I;;;-;h;;:.l.;:;:;+'~~...J.....J..-+±~~~~:.;p,:~~9, -o.a.gnaled facility Name and Sit. Addre,a

CSEJaCu. ~AS::Z MA."9.AG.z..~rl'lOaL!ST~ A~~~r;m\?.;"'C, "l,E'N' J1!P.SEf 0711.5

11. US DOT Description (lncJuding Pro;;er Shipp",;; N3me."iuard Class. 4nd 10 Number)H'~ -'

a.

Dn "':\SR \>lA-rE.R~~~ .. ~"'7"" ~ ..,. ...".~

d.

J. .Addi'ional Descriptions lor Material, Wated Allo"..

~, 2':-: tiC 4,~~J~~ri~_~B~HlAM:biiija ... h1.,J.l a ,Jla.1.:t', e. ",.1JC..,.

15. Spacial Herulling Instrucllons and Additional Irdonnation

16. GENERATOR'S CERTIFICATION: I h.,ally dec:'118:hallhe :ont8nllol this consignment are fully and ac:urat8lydo,cribetl above byproper SnippIng name ana .re classi\ied. pac~.ell. marKell' and labeled, and ara in an naapeetSin proper condition 10' trMspot1 by hiQhwayaccoroin .. to applicable internallonal and nat'onal gevemment tegvlatiOtls •It iam a large Qu.ntity gananator. ic"rllfy that Ihavlla program In place to naducethe voIuma and tQlllclty ol .... 't. qenllfatBd to Ille degree I h.v. det.rmlned 10 beeconomically practiceD I. ana that Ihaveulacted tha practicable mlllhod oftrealment I\oraga. 01diaposal currently avail.IlI.1O me whicll minimizaa the pnaaenlandfuture threat 10human heanh and the environment; OR. if Iam a ,mall ~uantlty genenator.l havemade _good taitllatlOft10 minlm;za my weste gene,.tlon and aeI«t!lIe best 'Nasle management method that is avaUable to m" and that can afford. . ..' .

i'nntBO/Typ.O Name

!'iaI':ll:1 4' • ,.., .." ISi..n.tu,. 0'" .J.(.4..,~.J' .~.,J~

Slgn.ture ,; '"":''. i--U.t,...-f ......t..L.LI•. Tr~nsport.,t ACknow.eogornatlt 01 ".caipt of MatanalS

~ ,Pri/'tealTypeo Namo '-';",~ H<k.".' I.')=J p:' !..,.J;) .......,,.;. p :;.),r'-4i".~.:::. - -,\. _.-." 0'1

J,lOf>liJ.cay .'Y.... :~ 1e. Tran,porter 2 Aeknowleog"menl 01!'Iaceipl 01 Mal.ri~sRT F'f1Olell[;ypell NameaA

~9. DIScrepancy lnaicat,on Space. -.- 845340152

"i(" ~:.'~."'", ~

F..ciUty Ownll' or Opere tor. CarlifiUlion of receipt of huardou. !!'.t",ial~ ~ by this m~I.!-tllXC89t· ... noled 1lT.ltllfl\ tV. ...r, +' " _.

pnntedlT~p:.~_a:~ .•• _ .• _. __ ~,_ .._...... ::~:L·::..~~.~~... ,.,.<:;:t~~:~~(t!)~,";?"~,:<,;,,~,,t·~~.f7!:.~:r;-r:"" 'S1GHATURE AND INFORMATION MUST BE LEGIBUi ON Au.. COPlESEPI>.Form87W-21\R..-.91Bajp......,." o<li1loM .... 0_"

8 - GENERATOR COpy

TIERRA-B-004574

,~~' (AfV. i.-a&i

Slate of New JerserDepartment of Envlronmenta Protection

Division of Hazardous Wasle Management;j~.:'::'...' ....~ ...i<:- ';, ..". '··Manlfest SlICtlon .

,'. , ~',. p,.."'f.' •.. . . "'. . . eN 028,.1renton, NJ 0.8625-Ple ... 1typa'';' pnn,.ln bloe!<,lellotS. [f'orm doolgn.d lor uta Oft .Hlo (12·pltch) lypowlllat.)

'f

:~to~~tNo.20504XJ9. 5"'''.8 ~3(;.law. 'Ion ,n thB !Ioaoed Brea5

F .. .,,,._ i .....UNIFORMJiAZARDOUS 1. Generato ...s US EPA 10 No,1: .WAsTE MANIFEST I•

I 5. US EPA10 Numoer

!h,.-~~~~~::='=~=~~~~~~~~!!::::~~~':=:':'-7.~;;7~~~~:l.....:!f...J~~;'=:===:='::'-~:-o~r.l-..,.t-aL':""''::':'-1L2~~~~~~~~~.ll..l~~~~1tl~

9 Oe$tgnat.d·Faeility Name ana Site AddreS$i .! W~~.Eill~mm~~----~l....1L!lL1U~..t.U1~~~~~~~~=

Gene'!!to( .. Namo amI Mailing Address

C1:l'EM:Io.L CCMPOmn)S me.29-75 IUVERSIDEAW. ,BLOO.17 ,.NEWARK,NJ

Generalor'l Phone I )Transporter. 1 co.m,e " .•. ,'!'~.

07104

.........

F, Transporte~" !"hone (G, Slate Faoilit)lT 10

1\7 .. I f' H. i'aeilily'$ Phone {

12. Conto,,'o" I 13.- TOlal

"<0. IType' CuantityI..

Wasle No.11. US DOT Oll$cripUan (Inciud/ng P1'operSl1ipping Nama. HiUtlffJ Class, and ID NumoerjHM

r· .

I,NCh'-HAZ;\RDCr"g~iO'1' RZGULATGD

DY;:: WASH WATERBY 49C1!'R

R..T

o;o,1----J.._-+ -4-...Jl..--l..--J-.:.--!-,.l......l..--..l.-.2--!---L-.l..--l.-..l--e.

CONTAINS WA'l'13R 65d,

I;ifl'3

IItI

IIi'0

I11

J. Aeoition.,al Oe.cn£!fOI1S 10r.Mohlrtals Listed AO. ove, . :.• A.l1MO~Iml· ACETA'lE ::. :~ .l.MiIOU1.U!l.Sl1L!'A'rJt~:a. ":,,-,~ .. ' u.. •.. , . ' - ... "j", ,J,,~ .' '... -'1!

~}:>.;;f~'A!it'Jil'U:::':;;';';t':t,,,},~:::'. ~",' 1O'./~:;.;:;.'" ,;: i" .15. .spe<:lal Handling Inslruellon. and Acditien.1 InformatIon

2RCFILB NO. k-3:6~2WORK ORDER

11>. GENERATOR'S CERTlfl .." .. his con.i9"",onl a1'e fully aM acc~fa1ely describad obo-re oypropar aIlipplng name ar.d are clusilieo, packed. marked, aM 'ao.• led. and aro in all ro.pects in prop.,.. eonailion 'or transport oy hignwayacccroing :0 applic.ble ,"Iemotlonal and national government fegulations.IIlam a largo quantIty goneratOf, I eertlfy that I have a program in place 10 reduee Iho volume and toxicity of waste ;onotatad 10 the degree j hav. C1otormined to eo~nomically pracoosble anq tI1at1havo $oloc~o" the oracl1cabl8 method oll~almonl. 'lorag8. or dispo$al currently avoilableto ma wh.cn minHr.lle. Ihe o",..,nl",,<1rutu", threottP human Meith Indlhe environment; OR,lf lam a small quanlily ~oneralor,1 have made a gooo failll effort to minimjze my wasla generation and &electIhe best ...ula managemont methoo thaI is avo liable 10 me and that Ican aIIenl, ,f.. .:'. ;'" ' ,

rur'..; ,".IIi'ISignatU;& "Li _

i"rinte<lJ; ylXt<lNa",e

~. ~'~. ~. ~17. Transponor 1 AeknOwledgamenl of Re~lIlpt 01 Malenal.

19. Discrepancy Indic~llo.n Space

845340153,...CILj....,_.,....-~_..:.-~---::.-~.....,-~-,.....,..,..,...-~..L..-...,...,.....,-...,.,:--:---..,-:-::"...-:;..- .....---,-.,..-...,.,,.-------------+ 20. r Operator: CertJr.callon ot f&C<liptollllL'tardoua malariala covered by !his mar;lh!'1 a'~.Pt a. nelecl in Ilam 19v'

~",., ._.SiGrtATUR£A'NO INFORMATION MUSTB£ lEGISU! ON ALLCOPU€S

TIERRA-B-004575

;;

. f Slate ot New Jerser- 1 Department of Environmenta Protection

.\~ " DIvision of Hazardous Waste Management. ?W.: Manifest Sec:llon -.' •. .. ,/. "'r eN 028, Trenton, NJ 08625

Pl.... typo'oiprlntln block Iellel'S, (Form desilln.d tr;r us, on .111. (12-pllch) lyp.wrU.r.)

845340154I'crm ,ApprcverJ. OMS No. 2Q51J-0039_ Expires 9-:;C-,

1. Genaralor's uS EPA 10 No.

t~ll J1D I 01 a 191 211161 il 91 C H. Faclllty's Phone -,~ ....

12. eonlame" I 13.11. t..'SDOT Oes-cn~Uon (fr.cfuding Procer Shippir.t; Name. ~lUsrd C!a-ss.and :D .VL"rr.cer) 70tal

HM No. Type' Quenlily

I 14. ii~~~,i

.. ;'.: •. 1;.•.•. ;

Wasta':'!>.

i 'I 015,0 I 01 cl ;:;

'5. Special Hanolill9 Instructions and Acdibonal InlormaUc"

WC~ ORDER NO.; A - .J;7/1-.$DECAL ~ro0 s I).

16, GENERATOR'S CERTIFICATION; I t.areoy declare Ihat !he cONenl. of thiSconsignment ara fully ano accuralely oasc"bed 300"'" ~yproper .hipping Mme and are classitled, packed, marl<e<l.aroa :acaled, and ara in all "!SpeClS in p,o~r condi!:",", lor trar.:>ort ~y hi(lnwayaccording to applicaole Int"malional and naUonal governmenl regula\lOnS_IIIam a large quantity generator. IC8nlfy thaI Ihave a prcgram in place to reduce the volume and toxicity of wasta generated to tha de(,lreal have determlne<lIQ be8Clmomical1ypracticable and that Ihaveselecled the oractlcable method of treatmant. slOr... a. or disposal currunlly available to me wilich mjnirni~es :he p,...sentatldIl:ture threallo human r.eallh and tneenvironment OR"f I am aSmaliQUanlltygenaral0r.1 havemads a good faith effort to mi",mile my waste "enaraticn and selectIhe besl wa"e ",.anssement melhod Ihat is .vallaollilo me aM thaI Ican afford: / ..t· ", ::;,.,"

,. 17. ~;ar:::i;;or:.~r1 ACKr"~w~ee-;f;!me-rrt of f1ec~!pt ,~ Ma~~r~J.:s-~~~L-_......::=::L:~~!:....J.~E:!2.L':'?-~~:",:,,:,--:-=---_.J--:::";'~=~'L_";'~~::!:~L ..J~~~~~~ ...:JI ta '\

19. OiscrepanC'lln,lication Spacej

1,(

fII;

EP", Form 8700-22 ,Rov,9

3 - TSD MAILTO • GENERATOR

TIERRA-B-004576

,~j\o,';.~ "'" ., ••••IN_J .... '.. . Department of Envlronmenla Protection

\ ~}J . 1 .0{70 -;r Divlsionco~:~:~~1:~r:~~~~~;~gement', .... type or "rlnlln bloclll.U ..... (Form dulgne<l for " •• on elite (12-l>llcll)·lyp .... rltu.)

845340155

~ON-~])O!J'S 'DYE WAST!: tilA'tDNO'!' REGUAL'rED ~l ..90'R

1. Generator's US EPA 10 No.UNIFORM HAZARDOUS.WASTE MANIFEST"

3. Genorato(s Name and. !"'ailinll Adorass

rnll

'''-' ...:O.s,gnatea Facility Nam. and Site Aao,e ...9.CHBHIC'\L WAS'rE MJU'lAGEtt1EN'r OF NEW F. Transporl"'S Phone {. '. '. } . i100 I.IS'l"ER AVSNUJ: G. Stal.FacW:ysIO· _

~J( . NEW'J!JRSn 07105 a St !t21 1461713!!) H, Fecll;ty'sf>!1one(12. Contain.", i 13.

US OOT C9icriptio,:.JlncJuding Proper Shipping N..me. Hazard Class,and iD Num~rJ I !~,atHM ~o, i Type' Q:J.ntity WasleNa."

G .. \IltR O.ATaR ~I~I

!? SpilC,el Handling InslNctlons ana Ace;l!onal Informallon

')lASTs:PROFIn NO. K-J2125

:6. GENERATOR'S Cl:R lflCA 1 : hereoyoeelara :1\11the r.ontenlS 01 mlS consl\lnrnent are tully and aCClJnt~jy d!$C(lbed above byorope, ,n,pplng name olea are clasS/IIOO. packed. marK80, anc iaDeIe<l. ana ara in alllflp8C1S in prop~r conaition IQr transport by highway

.ae:;ordlnglo appliC30lo intemal10nal and national government ragullrlloM, •It Iam a large quantity ganerater.! certify that I h.... a prog,am in piece to roduco lhevolume and toxicity of WIl$l& generatad to 111&degree Ihave del~fmined 10beeconomically practicable and that Ihave selected !he o,ac:Jcable methed ollteaunent storage, or dispoul cu,,,,ntly avallablato me whiCh minimizea Ihe pr.581\1 andfulure Ihraat 10numan health ena tha en."onment OR. ill am a small quantily generalof.1 hava me<le a good talll! elfottlo minimize my weste generallon and selectthe !>eot waSle management melnod Ihat is available to me ana thaI I can aHora ••

.\ MOn:h Day 'fellr .Print8<1JTypeo Nama

.' T -

~AIl

= i--'.....'+A-.:;;--L,;~ ~~l-t:.:8::.,";;::'::~:;:"::~::':':':;':':~==':':';:':'::'::':;:::':":~==;:;""---~;-::;:-:::-::-::-----_:""_--Z~:""_-------:":"--:-:--=---l':"",-Jl;-'}.~~. I't-:F_".-__ -:-~-:-_=--...;..---- __ ---.J-.---------~--------.l....l-..L...J-..L.....i..-··

Hl:. Oiscrepancy Indication Spaca

.,~" . Month

!

,....

I1

IManit! DIly Yur I11 ~ ,;

E"PA Form 8700-22 (An, '911131P..... _ edi_ ----. .

3 - TSD MAtLTO - GENERATOR'- ..MUSTSE LEGIBLE ON ALL COPIES

TIERRA-B-004577

"-=j Oep'rlm.:''::·~~::::'';:''~ P"'l<dIonDivision of Hazardous Waste Management

__ ~.~ ; Manliest Seellon-., 3,886 aal- recelveli eN 028, Trenton, NJ 08625

"lei .. type or prtntln block leUe... (Fom> d.slgned 'ot UM on IIlllt (12-pltch)lypotwrilltr)

845340156

Fqtm Approwd. OMS No 205O-OO3Il bpi,,,,, 9-30-9

.: Mani'est 2, Page 1 I Informa\JOn in 1M snadlld lUeasOocum.Jln~N.%"ot "j', I I:w,no~ fequl~ed by federal

7. Transporter 2. Comp,ny Namll 8. US EPA10Number

. ~ I I I I I I I I I r I ID.' Tl1>Nj:i0!llH"aPltone t$bql ""'1~'7x. -9}'.Ii. SlaleTmn$.IIl).' ..• · -: .• j' 'I. 'T•• i:- ..1

10. US EPA 10 Numb<lrF.Transporter'a Phon& C'< )'

b. '. RO UASTB :!LA...".L.V_~.3:::'E: r..:rQ01D N. O. S.FL_~~'~LZ ~r~OZD ~~1J13i"~-':""!A""._,''' ~.""~""~/"'l,-"'''' -,..."-'~~~f'V"

. * . -" ..... -........ .....'b.

. '

c.

t . '.'-' .. ¥.. ,~); ..... ' ~J',J'~c :0", •. 1

I I I " f I:" I.';:j ;

r Id,

I I

1S. Special HanaH"", Instruclions and Additionol Infonnation

PROFILE 'NUMB.!R lil~Bl?Ot-CCI729

(2tn) -4BS-321Z ...·DECAL 44.5243

\

16. GfNERATOR'S CERTIFICATION; I neraby declare lhal the conlent, of thi$con$;gnmant are tUlly and accurately described above byprop$r shipping name and a,e cla.. ified. pack&O. mar1l&d,and labeled, ano ara in all ,aspects in proper condition fo, transport by highwayaccording to applicable inlernational and nalional government regulations.If I am II large Quanllty goneralo"l certily tl1at I have a program In plac810 reduce the volum8 and lo.icity of wasle generatild to lhe "og,ae Ihav""etermi,,od 10 be

I economically praC1icabktand thai I haveselected \he craclicable method 01 trealmen!. storage. o,dlsDOS.1currenlly available 10 me which m'nlm,zea the present and

Ifuture tnreallo human heellh and Ih" ""vironment: OR. if I am aamall quantlly g8neralor, Ihavemade agooa failh etfort 10minimize my wa'ie generation and Jlelectthe beSI wasle manegembnt method thai is available to me and lhall can alford.

PrintedlTyped Name ISign~."Jre . 'i ~~1I"r_,., 'P ~T~ T '!"-r"" 'T . . I' ,,"'''-./~ .. c·

Monrll Oay Ye,;.-

I " k.I, ':.1 !r n. T ... n~orter 1 AcknoWledgement of Receipt 01 Matenals

~ .Prinle<l!Typed Name: 1":"'''0 ....1:10: ,,11'..,,'7.,....,. ::~. C' t., ,..,. ..• <t,·) ),1-~ 1a. Transporter 2 ACknowle.dgemenl or Rec&lllt of Malerlal.

~ PtinledfTyped Name A

I!1\

/ ~

}J ~ Si~t.1' (..- tl --I f/ /

/ .Month Day YearI II I '/ I

Mcnth Oay Year

"'11h.11A"' ...1 I

ISignaiure

19, Oisctepancy Indlcabon Space :...-~_.F" '..eLl : ':-;.:.:,,~ •.L'~-"~ I" ;~ ~.. ~ .... - : -;.~ ...t ,20,' fa.cillty Owner Of Operator. !,::erlificalion of receipt of hliZ&rdoue mlilerials _red by Chismanilest e.eepl .. noted in Item 111.

y .·,;'prlnle<IIT.yp~ rume • IS~ . -/.'. }ofA:t1e C. Christian '1 '. ~~ f tr, / ('!,r" 41-:t'~ .,..-

MQtlth 04y Yell'

4 .\ I. '1<: 1....1"SIGNATURE ANC INFORMATION NUSTBE LEGI8LEON ALLCOPfES

TIERRA-B-004578

,-_ •. L. "'LJ

-- , Slale of New JerSerOepartment of fnvlronmenla Protecllon

\~;~,. Division of Hazal'dous Waste Management~Il,.~ , Manifest Section '

" . ' ~ '41" *Ill >l i-1!~ei'i7""" ' eN 028. Trenton. NJ .08625Pl.... tyPe or print in-b'oel< litte.,. (J'1jnn ",.t1g"l(l!tlTu •• on .m. (12·"lIefl) typ.writer.) .'.: ' .

I'

845340157

"',UNIFORM HAZARDOUS t. G.naralo,., us EPA 10 No. 'Manilaat .":' :WASTE MANIFEST.I 9. rpent~~.

3. ·G"ner.tol" Nama,and'Mailing Address.. - , ~.;. .. ."

.CHBMlCALCOMPQUNDS.I~C.2~:':'7$ RIVERSIDE AVE.,~EWAjUC

4, G..n",at~r', PhOne I -, t ) . _ ,,;' ,5. ',an.poJ1ar I Company Nama

c'-~bLDOV!::t 'CORP ...

9. 'O ... gnau~a Facliily Name and Sit. Addres.

:OJ:,OOVER CORPORATION,:iiT. L r STATB ROAD 651, ARYO~I.l\.,VA 23004

1t. US DOT D.scriphOn (InC/~r1lng'Proper Shipping Name, Hazard Class, and ID Number)HM .".'

.r:I ·d.

I~~===~===~ ":"'---:---;-.l.-4L~~~~~~1

a,

x-.

b.

Co '.

_~."''-'J~_:-::...,.:~;":'.", ~.

•"'6'" ~.•..

J'lJ·:TlL\.NS~RI'l!R DECAL 452'37EM.EnGENCY PHONE (201 )485-1111, GU!DE BOOK 10-'27

I·S. GENERATOR'S CERTIFICATION;! nereoy dec~ara thllt In" contents of thi~ conslgntnentare fully and aecurately Oa.cnl>od above byprop"" shipping name .nd .ra cla .. ified. paclced. marlled. and label8d. and are in all r"pe<:1s in proper condilion for Iran.port by highway.ccQrding to applicable intarnational and. national gov"rnment regula tiona. . .III am a large quantity genarator.1 certify Iflat j have a program in placa 10 reduce lhevolume and toxicily olwaategeneraled to the degree I have determined to bli""onomically practicable and thaI I hue ... laded th" ~ctlcabl" methoo of !'Betman!. 'toraga. or disposal curr~11y .... ilable 10 me which minimlus lhe presenl anafutura Ihreat to numan heallh and the enVIronment; OR, II Iam a small quantIfy genal.lor,1 have made a geod lallh afler! 10mmlm'ze my wasle generation aM Mle<:1

' the be.t waste management metl100 tflat is evailable to me and Iflatl can ellord'.. '.

. PnntedlTypaa Name I Signature

s.~I-l~e:::.,,-T:..:ra~n~~0;rt:e::.r.:::2~A;:C::k:.:n:ow::.:::le::d:;:g.:.,,m:.::::,,:.:nt:.:o::t.:.R:::ee=e'~P.:.t.:.OI:.:M::.;:.at:::a.:.ri.:.ala:':"'T"::::-:== ~::"'_-"' --;~ __ =--.,.,....:..1I .Print8dIT),ped Name .

II .' ...

Mom" C4Y Y~rl1~ ,62 ,9 ~ l;)

T ',7. T ran~port., 1 ACl<ncwl"d\iern"nt 01 A~e,pl 01 Mal"tla'a

: Plint.dlTyped Namo/I/' C"~.;~~ ,~I c;; .;N _ ' --s :: U J , -1'"; .~.~.:'? -

Yeaf

Sionature

19. Di.crepancy In",lcatlo,. Speee. . ~., .. , .........-._.';"'" .._ .... ..-......

..~.....: . .;,- ...... --

'..5a1·',!&1~. discrepancy .... ~._,,-

j'·rl-,.-"'-::';':';;';;:;';;';":;';"-=-"':";:---:::-=~,:":"":-:-:=,=":=~= __""":,:-:-:,:::-==::-::-::-::-;:-==--:-=::-: __ ~,.,....~-:,::--...,..---- "",,T ;ro•. .facd'l)tp",.n.!'f.Of 9p,.....t~r. C~J1illcaJl..Onof reeeiptof flllUrdoua materi.'. co.ered. by tld. m.nilftt~. Rnoted in 1l8m'19. " .._._.•

,,', :;Y,",;,Prin.I,qtf~pWNa""l'J7'~-.;:~.t··:,:. --c.'" '.0·"··· .. -·_· "~. SlgnaWfe' _.~. .-,~' ...... ,""""" _-.~ _.,.. ..•...••. ~·~T·~:,.fc~?:"."T·~~~'!ra.daC~·.Chdst:1.an·· ':' '. i-1/t."o. c/l Y!.ir:.~:':.. ......

." .

• ~PAForm81~2 (Rov'11181~_willa ...... -..... . ',' .:;SIGlilA n,lRE'ANI:1JNFORMA nON MUST BE LEGIBLE ON ALL COP. .. ~ •3':'::TSD.MAIL.T9.:~GE'NERATOR .. \.

TIERRA-B-004579

STATE OF ARKANSASDepartment of Pollution Control and Ecology

_ P.O. Box 8913 Uttle Rock, Arkansas 722.19-8913

d . Telephone 501-562.-7444

Pl .... ae print Di~~e: (Fafm designed fof use ~n elite (12-pllchl type_ltsr.)

/~.I'i-7j

UNIFORM HAZARDOUS ... I

·.wASTEMANIFEST3.~fj_andMallnO"(1l1-

Chemical Compounds2975 Riverside AvetI:Qe Newark•.~~~~~( 201~ ...11175.1...-1 eom--..-Tn-State Motor Transit Co.

......... -. ..,.:'9.~f<>dIlty_-SIte-

Rinec:o1001 Vulcan Rd.-HaskellBentOn AR n015

~ "Waste Chloroform~N 6.1 UNI888 POll:1- ---..:....----------------------I-J-.L-+-..L...J-.J--l--l..:::::J,;::+---+;A b.Non-Regulated Material (Motor Oil)T

o .-R

""Non-ReguIated M4teria1 (Dye)~. . .

.--'

I&.SP<><*d_loItnJClIono and ~ 1""-' .'

New JerSeyT~HazardoQs ID'D~E Soo83New Jersey Tmiler ID # yt.-li= spzt'3,Ie. GENEflATOR'S CERTlFlCA"QH: I ""rwby d"" lhat the conteole of thla conelgnllHlnt arvlully and accul1llely deacrlbed ~ .. by p...,pe,.ehipp;nQ. name ami ....

da ... Ifle'd. pacl<ad. metl<ad. and 18I>ll1ed. and In all rw.,paC1a In prope, con<lltion IOf tmnaport by hlghway according to appUcable Internallonal and nationalgovemment ~u .. tlo'" and Ari<an .... otete fItlIUlatlona. ' '" I am' a letlle quanllty genenltor, I ""tilly thai I heve a preO""" In place to reduce tho velumn and IOJdclty of waste generate<! to the d .. gree I have determinttd to IHIeconomically pnletlcDbI. and lIllIIl hIlve .. lectod the practicable method of __ nl, al-OO. Of dlapoUl currently availDbI. to me which minimizes the pnlaant endIutura thfOat to human h""llh and the onv\r<lrlment OR. III am a amalI quarrtlty Il_ratar. I he-.. made a lIQod faith effort to mlnlml •• my weal .. genatllllon and aelectlhe beat waste management method _10 available to me an<:I tlIat I can affO;'d. , . ' , ." " ' -,

845340158

5tUPMINl'. ONCE DELIVERED, THE TRlAr ..-. !

TIERRA-B-004580

Chemical Compounders29-75 Riverside Ave.Newark, N~J~ 07104

s. 6. us EPA 10 Number

7.

9. o."gn<rted facility Nom. and S'.e ,l,dd,... 10.

Laidlaw $nvironmental services3527 Whiskey Bottom Road

us EP,I, 10 Number

C. Faali!)"'. Phon.

II. Waite Shipping Name and O...mprionTy •No.

a.

l3· DFN

13.TotolauO"'

'11·5 .G b.EN~I------------------------------j---+-+-----t--A c.ToRI- +-_---il--t +_:-I d.

O. Addili<><1olo...cnptiom for Mot.rial. lilt.d ,l,bove

PROCESS WATERe. Hondling Ccd .. for Watte. lined AboY. --

15. Special Handli"lllmtnlctlont and ,l,dd'rtionoll"formarian

PROFILE NO. 6-CEM-OOl

~~~~=====::.;:.:.,;,;=:::.---..,.-----::::;;::::O"~~----------ANJI-_.c;;.,.I::.=J.J::::::::.£L.!:<::!o<:-J._L-=::L.....!::~~~~t.A __ _I_~boIl~'""'~"""_{;.,_7i::'::::;;JI'.e-------...c:;.....I...LI-,..=:.1.L-L ..o 18. T,ontporter 2 M""",ledgement of Recti t of Mot.noaI Prin~/Typ'" Na_

19. 0ita'1tf>01>C)' fndicoTlon Space

845340159F

TIERRA-B-004581

11 I 1 bto k leiters•••• typo or p n n c . ere ..:--... .

IUNIFORM HAZARDOUS /1. Generalor's us EPA 10 No.

IMandu~ 2. Pags 1 I Information In the _haded IreasWASTE MANIFEST " 1,1 1 J I 1 I 1 I I or"f"e,' Nt at Is not r<lQ"lred by Federal :aw.

3. Gener_tor' 8 Name and Mallinq Addre~s '::l~?::"';:. -..'~ ~ '~~-.!"- i..:::: ~ S~JA~!ew! •. •"~n\...::~i , ..' ":".- ";:;;. 150,·.,-; : li:".,:-~,:ic ':-""-'1&

~I"'.I~;'<, Ii"; ; a, State G~lrato"l IO-{Gen, Site- Addr8S$1 -,-.

4. Generator's Phone ( I I .~ .:: .I _~:~:~<t".;:~~-'-:~~~i~>:.~~>:.c"_:~':_~,~~~<c! 5. Transoorter 1 Company Nome S. US EPA 10 N"molr C. 51ole TraM. ID-NJOEPE :·h ;-',t ','i" .,. I

I I.~ t",!.,.....·-:~ ,...,-,:, ~ ....... :o -. 'n r' I' 1 ;), I 'f I if I ";, 'I ,:, . P<Jea1 No.... -"'1·" y Jc.I'i./,

I 7. Ttanapor1er 2 Company Nom/> a. US EPA 10 NumDIIf 0, Tranaport9rI'plloOe( .~;i-~;'!Clil::::*.'1I t ! I I I I I 1 1 I I E. SUue Tran•• 10-NJDEPE . 1 , " r"' Ii 9. Designated Facility Nam/> aM Sita Address 10. US EPA 10 Numoer .: .' Decal No." .. , , , .. iI ~lC..:r.f~!'" i;"ti;~ ,-, - .. ,..,

F. Transporter's Phone r······ )I ~..........

! !i:... 1. :>: .., ::i a,.•.. '. - G. Stal..-FaciJlty'slD~-:""" -)if.! ~ -(. 'r

"I -'., ';1 , I ~I I ·1 , .! ·1 b"-',) -•• ¥.. ~ - , .iJ ~I'l

f :. ,.. ,H. Fadiily's Phone {

I US DOT t::"seTIPlionf;Clw1/ng Proper ShiPp/n8,Name. Haz3rrJ C:ass or Oillis;"". I 12. COl'lla,"ers 1 13. i 14.11.

I TVP"I Telal : I.~ liM NumO., and PacKmg roup) I UM Waste No.No. Cuan"ty ·l.A1/I/Clta.

II" R.:. ; :~ / ~ ......:.:.;;_:., l.,g ... ~ ....; ....a . ".,. . ,f; • ' '. - -~:!-P . .' " .,. .. "t-.:~I:t. ) I I ~-,. ;

, .'-j.,, ';0 ~.i--. ;J~; .. ~( . -;- ;

!i;;~-c&..L.:t.~,. • , .. - f:'"~ l~

,j .j' r(((:'1 I

t; ,I I ~ I , f I

jlo.

II

j I j,

- I I I ! I r I I , I l Ic. :I

1 Ii ,I I I t 1 , ,

IJ1

jJ.5'0

I1Iii.s - ~ j-:-'i-~t------------------------------;--"--~-+--'---'-'--+-_"""_",-_'---l._-1

ifIi51

fill"

JIi'0

I.s

Id.

J.. Additional Oaso1pllons tor Materials Listed ~llov<l;t~~t Al~ ...tl()-lf ..4t~~".l"'i'~'·:·....hft i~;c1"tf..~it;e.:'~_:!ll'lt -r

15. Sp8Cllll Hanalitlg Instructions iIl1dAdditionatlntormallon.il<C' 1-,;

16. GENERATOR'S CERTIFICATION: I horeoy dIKlarQ that I~e .:onl ..nts at \hIS censl~"menl are tUlly 3/ld accuraleiy aesc"e&<l"",ove "1 ilrO~9f sI1,ao,n~"ame ana areclesslfied. packed. marked, IIl\d !.tIled. IIl\d are :n all ,.spe~s In proper ;;Qnc,t!on tor ltQn$port by tli!ihway ac:orcing :0 appllcaDie ;nternatiQnal ana ~al1cr.aigovernment regulations.

H I am a largl quantity ganeratot. Icettlfy Illall have a program In place to reduce Ihe ""Ium. iIl1d toxIcity ot Wll5te S""erated :0 the degree I have ClIlermined 10 beeconomically practlcabl. end ",at I have selected the oractiCable method Of treatment SlOflIg., or disposal currently available to me which mlnimlzas :ha present anoMure threat :0 human health and the erMronment: OR, i1 f am a small Quantity glnerltor, I have maoe I good faIth !lffO" :0 mInim;.;:. my wast. ;;lnerallOn otId ~llC":tne oes' wal'a manaqamant mel!1odIhal ;s avaHallle 10 me .,,11 that I C3I1 arlarc.

T I 17. ,,,nSlloner I ACknowl8<lg8ment01 Reeliol ot MatenaJs: Pnnlae:vryp8d N<lme

~ .......K . ,. t; . ::::'i j, .-p -/. ". '-', "' ...~ 18. TransPOlt8r 2 Acknowledgement 01 Receipl 01 MararilllsT Pl1ntedfTYP8dNameEII

.Signalu,..

19. Discrepancy Indicatlcn Space

1O ...... ~r.,.; ............... _:~ ... _._.-

TIERRA-B-004582

TIForm Approved. OMS No. 2050-0Q:J9. Exei[6S f1.'J().94

UNIFORM HAZARDOUSWASTE MANIFEST

_.3.a....-n Nome and M.alnQ_ .....

Chemieat Cmnpounds1975 Riverside Ave. Newark

1.T~2~Nome

9.Qn.ioljJnat-.d n.¢i-I/t'i N41it'n_ and Sit. Add,..

Rineco1007 Vulcan. Rd.-HaskellBenton. AR 12015

..

"Non-Regulate1i M~al (Dye)Q

E/I:1-:- -/U..u.Lq'+..J..+..J...,...I4a-A:~""'_l'--~~A

To.1- -!--l--lYf-J-l--1-1--l--lL-I-_+

"

'.

18. GENERATOR'S CERTIFICATION: I ~by de<:1Ml thai I'" contents olthl. OOI1signment ar& !ulIy an<! ~uratety descnlled above by proper shipping name BJ1d .m.claealfted. pacl<ed, nwltltd•• nd labeled, and are In all reepecte in proper condition lor Il'llrnlPOI1by highway aoooraing 10 applicable Intematlonel and nel!onalgovernment regulallons an<! J\rI<anlUIlI .tate reguIalIonLIf I am a iatQe quantity gene",tor, I cerUfy IheII h ..... it program In place 10 rsduce the volumn an<! tOldcily of waale gen"",led to the detl"'" I have determined to ~oconomlcaJly pmC\lCel>le end that I have .. ftleted the p_Ia method ollreatment, .. orage, or dlepoaal currently availabie to me which minimize. the present andIuture threat 10 human healfh and lhe environm8<'tt; OR, If I MI • amall quantity generator, I have mede a good Iatth e!fon to minimize my waste generatlon and selectthe best ",aale menaoement melhod thai Is avellablelo me and that I CIIn 8lfoId.

11.~ t ~oI~of_

- .' ,..

TIERRA-B-004583

, ~ ==-.=,~=c====

SlafeofNewJetsey -~~, '~l'Q~J'~:!~iDepartment of Environmental Protection and Energy ~Q, /7-

Hazardous Waste Regulation ProgramManifest Sectron

eN 421, Trenton, NJ 08625·0421'>Ieue type or print In blo"k leiters (Form dU'gne<! for use on elIte (12-01l"hl lYoawrite. I

~

"._" .,." .~ )!

, .~

-

;6. GENERATOR'S CERTIFICATION: I h"soy Oe<::arethai :no cont.nt. of thil; ronstgnm"ntar& ''''&ly and accUrately'c:eSChti<l<l'cev. cy proper sr.,op,ng .,ame ana a,.!Classifieo. pac~eo, manced, end labeled. and are In ail .. spec:. In prope< c::>nditlon lot :ranspon by higtway =raln'l 'a ~j;pl;cao,e :n:smaIlOnai ana nallona'QQVernmanl "'IlulatiOfls.

III am a larg" quanlily genSflJlO(,, cltt1i!y that I haw a pfO\ll'am In place to ..cluce ths volum. and tOxicity pt wute gllllenll8C :0 Ih" d"9roe I have determtned to be Ieconomically praetical:ie and thai I have lalected the praet!caele method of treatmant. sro.age, or dispoell Cll... ndy avail.blela m. wnicn m,nim,zes th. pAsent.mofulur. threat tq human h.allh and the lIIlvironr.>ant: OR, it I am a small quantlly ,.enerator. 11':... made a gOOd faith effort ~o mlnim,~e my wast. ~9ner3l10n ;J(Id .ellle:ttI. l:Ie.t· .••• ,. man.gement method that i8 availat:l. 10 me and !hSlI can affc,~.

T I '7. ',an.ooner I AcknOWledgement of Rec.ipt of Materilll8

ISign.un

1g:. Olser.paney indicalton Space

845340162

EPA """" Il7OO-22 (Rev. 81118)Pro • .,... _iono ... -.8 -=--GENERATORCOpy·---~ SIGNATURE AND INfORMATION MUST BE LEGIBLE ON ALL COPIES

TIERRA-B-004584

State of New Jersey .Oepartment of Environmental Protection and Energy

Hazardous Waste Regulation Program .Manifest Section

eN 421, Trenton. NJ 08625-0421Pie.... typtl o. p.lnt In blccx lett .... (Fonnd.sign.d lor .... on elite 1121'1l"hl Iy .wrlle,.j

..Ei

UNIFORM HAZARDOUS 1. Gen8,alo,'s us EPA 10 No.WASTE MANIFEST Info,matlon in Ihe shaded a,us

<-Mo",.~ OilY Y""f

3. Oen,,"IIO". Name .nd Mailing AddrassO'reo:icaLCa.:lpOUnds. InC.29-75 lliversJ:ae Avetrue&lo'nrk. NJ 071C4"'- .,.

. t....

I.Wasre No.

d. '"!"

19. D,screpancy Indication Space,- 845340163

-'.: --:''':'~'"::o:v''~'~~~" •4. "Oe"enilor's Pllone5. . T,ansporte, 1 Company Name 6. us SPA 10 Nume...

T • 7 Transpo'ta, 1 Ackncwiel1gement of ReceIPt Of Matenal.: P'lntedlTyped Nam.

i1--------...J{JkR:BJ!:J~r:..~lkJA:llll;d;...--J.-_.j~~il;t{AJ....J.L.~~Z~~~:::::---_...l~~llia3jljlSll~ 16" Tran.pone, 2 Acknowteagemenr ot AeceiDI 01 Materlal$r Prinled!Typea NameE1\

t:"~. . tt ..._-r .....1~ -:"".,,'--'_

7. T,ansp<lrte, 2 Company Name

9. Des,gnated Fae'lity Name and Sile Addre.s

nesearcb Oil O.:m~>·:::'655 Transport Read..~, ........1__ -I ,..., ,- ."fl..,,,!':'

11. us DOT Desc,lption (lnCludmg Proper Shiap,':1. Name. Hazsrd Class or Oiv.!!,a"-HM iO Numaer and Packing faup)

ma:.u%X:r:b·lM!»-blle<Ubrprot;qx:t.IX~::sx~tx~~~~~x~~~~x~~=~,x

ClE

N-'- '-i.azar~.~ r,jcst~ 5Clitii:~.::-"S...

(Gilorci.:.enzl~r:a) •..A

• c.T ){0~

o.

(- .

H3zardou~ Waste Solid,n.o.s •9,NAJ077,~GIIr,?Q(~001)

0\, b.

ProntedlTYPed N Manrn Day

16. GENERA TOR'S CERTIFICATION: I he,eby <lecIate. thaI the conu",rs 01 (illS consignment a,a 'ully ano accuraldly <fe,enOed'OO"e 0Y p'cce, sh,pomg name aM areclassolia<J. pacKed, marl<ed, ana faceted. and are .n all respects ,n p'ope, COMmon la, "aosPOrt I>y ll'9hway accor<l'"lJ '0 iDP,icao". ,n.amallonal and nationalgoyernment (egulations.

III am a large quanli~ ge"e(8to<, I Cllf1ify thl!! f haVtt a program-in place 10 reduce the \/Ofumeand 'o.ic,ly IJI was'e gM ....aledlO the degree r haY" deletrnmed to DeoconomlCaKypractk:aI>Ieand 1M. I have selecled lI1ePfaeticabl" methOdof 'realment. S!Ofage.or d~POsarcurrently ayeilable 10"'e wnIC" mInImizes the PfeSMI 1n"Iulu'e Il1,eallo htlman lIealth and .he """i'onmenr. OR, jf I am a smau quanlity generator. I have made a l;OOd ',11'1> efton :0mso,mi:e my waste generat,on ana ;e'ecltile best waSle manage"",nt method Ihat is ayailable 10 mil and 1M' I can alfota.

EPA Form 81t)G,.22 ,RfJV. Mal Ptfttou. ~itliOM 8 ... ClbIo(e ...

3- TSD MAIL TO-.GENERATOR

TIERRA-B-004585

-. State of New Jersey \

Department of Environmental Protection and EnergyHazardous Waste Regulation Program

-A ~.; ... _-." 1'." -- Manifest Section, " eN 028, Trenton, NJ 08625-0028

k Ie« .... : 'IF"':';' deal ned 10' use on "llIe (12·pltchl tv\>e .. rtter.l " "

: ' UNIFORM-HAZARDOUS_:~J':,WASTEMANIFEST

1. Generator's US EPA 10 No.

I!1ieGo

)

.- "' .... ~~t·'!'I":t!. ..... -- •• ~.~:,

4. ' OOn.,n;;Qr's Phon ••

9 ... Des<!l"aled Facility NQlT18 lltld Sila Addrasa. • .... :".-_.J.. - •• -

51's'nCa ~..ROID1L'lTA:r.11391'COOtrrl 'ROAD 176

,11. US DOT Oaset1ptlon (rifcIvaing Proper Shipping Namtr, Hazard Ciass. and /0 .v"mC8r)

HMa.

x

I~b.~I~ i~1-c.~::-_I--"":::"--:"__ ,,,,,,,_':--l;.;;"-'-~oif£~-r~r-----------+...L-!.-l-!-+-...1..-L-!.-l-t---L-'-.L......J_.i-l

i I~it::-l-.d-, -I--1-...:.::..~~:...-_---......- ----jf--.L-=--I-.L-!-L-i.......L.L.J-:--l....:.:...J;":;':L...-:.L.-1

~,% ....t\....>.

11..~.(-f..l'.e~'IIcI~

If6.t~ .."ej "f t

IIli

fIi

J~,;;C.!l1~P~a,:~l!ScrJPliQll.$ for Malert;lls Lm~Above_

:U~~~~ffi~t~~~t~~[~r'~'~~f]~!F'~.-'-

15. Special Handling InSULlCtlOns and A<laltional InformaliOil

EHERGENCYCO~"IACT~ caEM'I'!tEC 1-300-4;';'4-9300CALLa. HUST IDEETIJ'Y VAN WATEilS & ROGDS AS SH!?!'E.lt.t S. GENERA TOA'S CEflTlFICA T10N: I MIOOY aee:are tn.tlM :cnUlnlS ot In,s consignment are 'uUy and acc,-ral~ly aaSCflDeCl aDo .... by proper slnpplng nam. ar.d ere

classtlled, packlKl. marked, lltId ~kId, anll ",e In all ~specis in pr_r condRion lot transpon by h~hway according ,0 appli<;ablll inlernatlonal and natiollal

liovemm..,\ l'$Qula!ions. 'III ~ a IaTg~ quantity gon",alOf, I C8n!fy that I hove a program in place to reduce It", volume and toxicity of weste, g8Ml'8ted 10 Ihe d&gl'lt$ I ha"" determined to be8conomi<:ally pt.cllcaDle and tMlllIavtl seleded lhe pracVcabl8 method of :reatmen1, ~Ioraqe.or dl.oosaJ clllfentty aval1able to me which minimizes the prooenl andfulunJ Ulmar to hUman h"aJlh and the envirorlment; OR, if I am • small Quantity generatOr, I have mada a geed flllih er.on tQ minima .. my wastelienerBlIOll and s.ledmo b".t waste management mell10d thaI is avo~abl .. to me ana thaI I can alford, •i I PtlnteolType<I Name I I' Signacute Month Oay y"",

I,

t t7.R..iL /:.fi,u~/Lr;:J.J!;:p~~~'f_----J.-~iC~""~2~~~~~~::::--------i~~~Jl..1Z~Will!!0, 18,RTl!R

19. {)~~~~J~~ ~~:.-,r.~~;'l::.~..t/~~(~.;',~ "_ '........ :, ... '...._~ .1 .. ..:-~ •. '". "'~.:-=- ."10:, .~r~~C< ~-"""""'.~'

4~ ct~~~:.:...::.;;;,;..::.::.~..:.;;.;..;..~~7-..::-:~~~~=-:.-:::~7.:"":--~:-::-;----.:--.-;..--.---:-:-:-~-:-::------------11-y ~I-~ C

PIES

-. 845340164." , ."'. .... ....... .~"'"

TIERRA-B-004586

845340165..~.----~' -.".,_ ....-~..... --~ ....._-_-.- .~-"

TIERRA-B-004587

-OCCUPATIONAL HEALTH SURVEY REPORT

PREPARED FOR:

Chemical Compounds, Inc.29-75 Riverside Avenue

Newark., NJ 07100

CONDUCTED BY:

Joseph N. CapuzziOccupational Health SpecialistCIGNA Loss Control Services

ACCOMPANIED BY;

Mr. Arturo CelleriSafety Manager

DATE OF SURVEY;

October 3, 1995

845340166

fLEA" RJtA,D CARDULLYThU co.. ""..,. haa __ • NrTO)' .r,..... pnmUoo, ........... t, or ....... tIo.. (~II porUnotat to> lloo!)'pO .r oppllod ror or prot1d4<l)

ror lloo p..rpo r .""",,<1IaI1Ioo tolldlo•.. r rid< ....dcn.~ A1Il)' ncomro .......... or ...r.... lIdott prt>'t'lded II_t IMIJIdod mu(e ror odricol\'.m 0 .. retr port .r Joc-I .. _ ,... _, retain f•• ,.......... ,....,.- II II .. t __ 10 ........ t • ..,.Iocol .....,. ro" mar "" Co .,....olde • .. r.pr_Uoo,. ~.rlq>loo.,., pro<Iu<t .r .~-

TIERRA-B-004588

--Chmnical Compounds, Inc.Newark, NJNovember 9, 1995Page I

INTRODUCfION

On October 3, 1995 an Occupational Health Survey was conducted at the given location to evaluateemployee exposure to various airborne contaminates. An executive SUDlDlmy and results of the surveyfollow.

The data presented in this report reflect conditions as they existed on the day of the survey on whichthe air sampling was performed. Information, as supplied by plant contacts was relied upon to help indeveloping conclusions and in the evaluation of programs discussed in this report.

STANDARDS AND GUIDELINE§-:>.

StandardslExposure Limits for employee exposure to various materials evaluated during this survey arediscussed under the Results heading, and also found in the Data Tables of this report (See AppendixI, Table 1). Information on the sources and types of standards and guidelines are listed in Appendix II.Generally employee exposure results are compared to current Occupatianal Safety and HealthAdministration (OSHA) regulations/standards, called Permissible Exposure Limits (PEL), and can befound at 29 CFR 1910.1000, which are often called the Z tables. Where other accepted State-of-the-Artindustrial hyw,ene practices or guidelines, such as the American Conference of Governmental IndustrialHygienists (ACGIH) Threshold Limit Value (TLV) are lower or differ in their approach the most currentvalues for these guidelines have been used and noted. The use of these standards and guidelines arethought to give reasonable protection to the health and well being of employees exposed to thesematerials. Please see the Appendix section of this report for the results.

The ACGIH TLV's arc included in this report as exposure standards because for many substances theACGIH TLV's are more conservative than OSHA standards. The ACGIH TLV's are more conservativebecause they are based primarily on the prevention of disease. Incontrast, OSHA Permissible ExposureLevels (PEL's) are required to take into account the economic feasibility of reducing exposures inaffected industries, public notice and comment, and judicial review. The TLV's are guidelines that referto the airborne concentration to which it is believed that nearly all workers may be repeatedly exposed.day after day, without adverse effect

EXECUTIVE SUMMARY

Air sampling for ethylene oxide, xylene. nitric acid and methanol reveled that on the day of the survey,none of the employees' exposures exceeded the OSHA Permissible Exposure Levels for the abovecontaminates .

Recommendations for the implementation of your respiratmy protection and confined space programsand for the installation of an emergency eyewash/shower are being resubmitted. New recommendationsfor improved housekeeping and the use of eye protection arc included with this report.

845340167

PLUB llL\O CAltD'ULLyTl>Jo".po", .... • .....,..r~ ...,...................... t, (wlIIdo_ .. ..-Uo lIIaiJpe .tlno .......• pplled r...... ~r... III. pwpoH at .apporUnlUla raa- ar riak lIIIdonntIIllc- All)' '" lnrona._ ..,.,n- b not .........ocI .. a ...-- tor a4YI<e........... rat: .sport ar )'H _,. ........ rar,......_ po It 10 IIItt ~ Ia .......... .." .... <h&ty,.... .... ,. bay.C. pra_ .....~!"' ........ ~ ,.--IIM.

TIERRA-B-004589

" ."':.- ....~.:

-

-

. ,~ .. :..

Chemical Compounds, Inc.Newark, NJNovember 9, 1995Page 2

METHODS

Air Sampling

Unless otherwise stated, samples were taken in the employees breathing zone to obtain samplesindicative of the actual employee exposures. Gillan 513 and 113 air pumps provided the vacuumsource. Pumps were calibrated prior to and after the samples collection and were checked for properoperation and flow were necessary and possible. No changes in flow rate were measured, unless notedin the comments section of the results section.

Air samples collected were analyzed by Environmental Health Laboratory in Macon, Georgia andCromwell, CT which arc: accredited by the American Industrial Hygiene Association.

--RESULTS

Air Contamina.nts '.

Table I pres~nts the results of air sampling and analysis. Exposure concentrations are presented inmilligrams per cubic meter (mgIM1) or parts per million in air (ppm) by employee and location. Alsopresented, are the applicable Threshold Limit Value (TLV) or the OSHA Pennissible Exposure Levels(PELs).

DISCUSSION

Air Sampling

Chemical Compounds, Inc. is a manufacturer of dye intenncdiates for hair dyes. Vmous chemicals arereacted in 6 reactor vessels within the plant Many different reactions take place, however, of majorconcern from an industrial hygiene standpoint is the reaction involving ethylene oxide. It is one of themore frequent reactions. Ethylene oxide (ETO) is a highly reactive gas or liquid that can affect the skin,eyes, lungs, and nerves. Ethylene oxide has been found to cause mutations lllld cancers in animals.Based on these reports lllld human epidemiological studies showing a higher than expected rate ofseveral cancers, ethylene oxide is considered a suspected human carcinogen.

Nitrogen is introduced into the reactor vessel The:pressure in the:vessel is then checked to assure theve:sse! is holding pressure and there are no leaks. ETO is then piped into the vessel from outside of thebuilding. The ethylene oxide is reacted with 4-tluoro-3-nitroanaline (NFA) under pressure withpotassium fluoride added as a catalyst to yield the dye intermediates, NHNF A.

Personal and area sampling for ethylene oxide indicated that employees are exposed to levels belowboth the OSHA Action Level of 0.5 ppm and the OSHA Permissible Exposure Level of I ppm as an8 hourTWA.

845340168PL&A.Q ItL\D CoUIDtlLLY

11>10 "" ...... .,. ... _boo ........,.of,..... ...--.~ or __ (wNcloonr1o porUoNootto"'l:)TO .,--. fttr ... prtn'\lIooI)M ,..."... af _rtioItIlo f\mdIotI.,""" _ Nillli+ Alrt- .....tIH or .......... proriIJM .. Mt .......-,.,. atMoom t..,UI*" ........ ' ...... 17'"' •• ,. rota" ,.,.,...... - __ It..aat IIdIeoIad to -..... • .,. ..... <Io&ty,.... -,. to .............. ,.

prom-,.~..-IqJIaa, pndlKt." .ponaa ..

TIERRA-B-004590

) lical Comp<lUnds, Inc.j-. ..... ark, NJNovember 9, 1995Page 6

TABLE I

Concentration

ethylene oxide

Sample I Location SamplePeriod

AirContaminant

ppm

Standard!Guideline

10:24-2:51QK#l Carlos Molina!Operator

< 0.21

QK#2 Area Samp1c1at reactor

10:26-3:02 ethylene oxide <0.2 1

~ Petro NaranjolI ,.u • assl operator1:59-3:02 xylene

rm-l Petro NaranjolI .-..- assl operator1:59-3:02 xylene

Jl:36.2:~ nitric acid

11:45-12:14 methanol

~ Carlos Molina!I -.-_..- Operator

100

100

nitric acid < 0.05 2~ Carlos Molina!I -.----Operator11:36-2:52

Mill Petro Naranjolasst. operator

200< 48 ppm

PLUSIlUAD CAUn1LLYTIllo"."'11)" _dertok .... "'*"C)' .f , ...........IftI, "",lplD"''' .r do (.. bldlev•• l> portloont to Ill. I)"po of In '1'p!W f'T 'r pr.\'Idfil)far 11M_ f _rUDe tIH _1I.r rl>k -""lIlIla. AJI, do. Of lDf.r U. _ It .. t lDl<DdN botItut. f•• "d.1<o....... rot)" n.ptl'l Of _1, , ••ta. fer , ....... purpo It 10 In.... dod I ppiORI'0' ..... dutr , ... m., h.vo to pro,."" ... r.p............ rk........ pr.dlK1 U ..

)

TIERRA-B-004591

-Chemical Compounds. Inc.Newark. NJNovember 9, 1995Page 7

--.•

APPENDIX II

845340170

I'lJWII; BAD CA.RUtlLLY"TbU-1-117 loa '."'""" .f)".~""'''''''''''-' .P__ tIooo (_ • ....-u- to .... .,.. .,_."""",..,. ..........I.p pIII1lO" .f 1-r1lDt ... 1\oDdlo. of AJI)' ................. ~ ~.tIo.proridod .. aot...- ..•~ ,.,......tn r.er osporl Iopl.....,..;i )'0' _)' main f ,..w ......,.-. It. "'"..-..." .oppIollt""1 .... 1doOl)')'Oo .... " loa". Ie .......... • .. fo

~ltoo,. ~ _ w ....... 1IooI.

TIERRA-B-004592

-

Chemical Compounds, Inc.Ne.wark. N JNovember 9, 1995Page 8

Standards and Guidelines

A listing of the appropriate health standards can be found in the following table. Included in tW.stableare the following:

1. permissible Exposure Limits (Title 29 Code of Federal Regulations (CFR) Part 1910.1000). ThePEL's represent the legal exposure limits set by the Federal (or State) Department ofLabor/OSHA.

2. The 1995 _ 1996 Threshold Limit Values which are guidelines developed by AmericanConference of Governmental Industrial Hygienists (ACGIH) to protect the health and well beingofworkeIS.

For a compTete listing and explanation of the use of the PEL's and TLV's, please consult the abovedocuments/sources.

OSHA Pennissible Exposure. IACGIH Threshold Limit Value

Level (PEL)' (TLV)%

Substance Units 8-Rr.' STEL' Ceiling' g_Hr.' STEL' Ceiling'

ethylene oxide' ppm 1 - - l,A2 - .

mct1umol (skin) ppm 200 - - 200 250 -nitric acid ppm 2 - - 2 4 -ll)'lene ppm 100 - - 100 150 .

flU.Pununwlo I::xpOlUl'C J.iJnm, Ti 029 Coda 0 reoom I<cgula on Pitt 191( .100, uocupauonLi :;atoty-iiiid·

2- n.VJ. g.HourllG-Houc4. STEL5. Ceiling (C)6. ETO

HoaIlh A.dministndloA'I'braoholcl Limit v &1uepublizlhod by lbc Am.ri~ conf_cc of Oovomm.maIlt1dustrial HygienisU (1994.-199.5).Tho Umo-wcigbtod avongo for an & or 10 hour wade shift ill & 40 hour work wHk..Short term ..xpooouo limit (1$ minlJteS).Cellini limil, lb. cQnccn1nltion. that shoulcl not be .JlCCCcled during any p&rtof lb.. worlting .lCpO$IUll.

PEL folll1cl ill tho compRbcnsi" .. OSHA Slandud for Ethylono OXide (29 CFR 1910.1(47).

Action Iev .. l 0..5 ppm.

•••••• Ai•••••• A2........ A3•••••• A"........ A.5........ NIe

Confumod Human CuciDopn;suspeclecl HUIUB Carciaopn;AWmal earciDopa,Not CIuoifilble .. & HuawI CarciaoCon:Not S~ .. & HUIDNI Carciaor;eaIiI>Uu of intended chane",

845340171

P1.&\SB R.IA.D e.utDUlJ"yTItIa "" .. ,."7 .... ull4or1ablla _ .rye_...- .... 0<J"iIt!II-' ar th.. ( ....- w !lN17POaf'-"_ • ......, fa .... praTIdod)ra. u.. ,..."... af wppo !IN fIoItdloo. at'rioI<........... A.Jq .-.n ar ..,. 110. pI"IO'lttIad II ... It>I4tldad .. • oultotittM ..... a<Mco!'ta.. a .afetlt azport ye. _,....ala .....1"...... ~ It "' ""aarlopl4uty".. ... ,. ha,.a W.... - ......

pnm'-. ""rIqlbco, pn- ............

TIERRA-B-004593

Chemical Compounds, Inc.NcwatK, NJNovember 9, 1995Page 9

--

.•

'. APPENDIX III

845340172PLILU& IlltAD CARDULLY

TWo ..... P.. 1 .. va4orta-. _ "'1 ..--. or .,....-<--" tlO ... ."..., ....... - • ..- ........... ¥Ido4)r.r 1M l""'l"'".' _r1IaC'" l\ItM:UM.f """" Wi AIl'f 1'__ 1' - 1'hhcI .. DO. III-.Ncl .. a..- f.r_fnJ ... "'«7 ••perta ............. 1......,..-la flor J"IW' IIllDO to MIpploIlt • .,. .... 1.....,.yo.... ,. "" ... tlO "..mr.... Ia

"'--'.~"""""""d"'''''''''''

TIERRA-B-004594

-

-'

Chemical Compounds, Inc.Newark. NJNovember 9, 1995Page 10

METHODS TABLE

Analyte Flow Rate CoUection Media Analysis Analytical(liten per Methodminute)

ethylene oxide 0.1 Qazi Ketcham tube Solvents by Gas FID;NIOSHChromatography 1501,8286

modified

methanol 0.178 silica gel tube Solvents by Gas FID;NIOSHChromatography 2000

nitric acid 0.2 Orbo 53 tube Anions by Ion Conductivity;:::. Chromatography NIOSH 1903

xylene 0.2 charcoal tube Solvents by Gas FlD;NIOSHChromatography 1501, S286

• modified.FID = Flame.Ionization Detector.

845340173PlJl.AA JlEAD CA.RUULLY'

t...._ ....,..... ••....,..f.,.... pnoa ............... ow 110.. (w1dcIInor 11"'-" lIoo t)"P* of ........ '" oppllod lbr or proYidod)

r.r dM P"'"J'lUO .f .. flPOI'dI>& ClI. I\mcd .. of rid< -...... AiII'/ .-- -. or __ don - .. - IoloDdod .... ....tIodcuto for ..-Iloo .. 0 .. roty""port or I..... co-.l,." marrobin lOr y.w .............- It It _ ..,. .... -,.,.... "or luoo" .......... 0 .. f•

........-. .. ........-. pr1I4uct Of' • .....-

TIERRA-B-004595

845340174

TIERRA-B-004596

".'

~\\..\.-..,

NOY 23

,._,.:~

1981:DONALD LAN

SECRETARY OF STATE

845340175

CERTIFI.CATE OE INCOREORATION

of


THIS IS TO CERTIFY, that I, GEORGE L. GARRISOt

do hereby associate myself into a corpor~tion under and by

~irtue of the provisions of an Act of the Legislature of the

State of "New Jersey entitled "An Act Concerning Corporations"

(Revised Statutes of New Jersey, 1937, Title 14 and Title 14A)

and the several supplements thereto and acts mandatory thereof

and do he~eby agree to take the number of shares of capital

stock set opposite my name.

FIRST: The name of the corporation is:


SECOND: The location of the principal office i~

this State is at 1135 Clifton Avenue, Clifton, New Jersey 07012

THIRD: The nAme of the agent therein and in

charge thereof upon whom process against this corporation may

be served is GEORGE L. GARRISON.FOURTH: The purposes for which this corporatior.

is formed are as fol~owa~ To engage in any activity within the

purpo8e~ for which corporations may b~ organized under New Jers

Statutes Annotated, Title 14A, entit·~ed "Corporations, General"

.......FIFTH: The name and post office addresses of

TIERRA-B-004597

.-

--

-

"

845340176

the incorporators and the number of shar es subscribed for by

them, the aggregate of such subscription being the total amou

of capital stock with which this corporation will commence

business, is as follows:

GEORGE L. GARRISON.1135 Clifton AvenueClifton, New Jersey 07013 .•..•...••.•..•.• 100 shares

The period of existence of this corporat

is unlimited.

SEVENTH: The total authorizedicapital stock of..the corporation is two thousand five hundred (2500) shares of

~ommon stock without nominal or par value. Allor any part of

said shares of common stock, without nominal or par value, may

be issued .by the corporation from time to time and for such

consideration as ma~ be determined and fixed by the unanimous

vote of the Board of Directors as provided by' law.

The number of Directors constituting thE

first Board of Directors shall be two and shall be:

George Moncayo 7 Berard BoulevALdOakdale, Long Island, N.Y. 11769

Anna Maria Moncayo 7 Berard BoulevardOakdale, Long Island, N.Y. 11769

IN WITNESS WHEREOF, I have hereunto set my hand

and seal this 16th day of November, 1981.

~:.~~~~ L.S

TIERRA-B-004598

-

-

i 845340177

'.,' .

.:-;

STATE OF NEW JERSEY. SS. : ..'COUNTY OF PASSAIC

1BE IT REMEMBERED, that On this /C •.:CL day of

November, 1981, before me, a Notary Public of the State of New

Jersey, personally appeared GEORGE L. GARRISON who, I am

satisfied, is the person named in and who executed the fo~egoi~

Certificate, and I, having first made known to him the content~

thereof, he did acknowledge that he signed, sealed and deliver:

the same as his voluntary act and deed.

.WQ2 A. JNNEJ1A' .A NOTARYPUBUC OF HEW:I£R8'EY

MY COMMISS10N EXPIRES oct 9, 1985

. ~·c ···

TIERRA-B-004599


29-75 Riverside Avenue. Newark, New Jersey 07104(201) 485-3211-2 • Fax: (201) 485-4870

Emergency and Remedial Response DivisionU.S. Environmental Protection Agency290 Broadway, 17th FloorOffice of Regional CounselNew York, New York 10007-1866

January 28, 1997

To Ms. Amelia Wagner,

As per request, please find enclosed a re-submittal to the following responsesto the "Request for Information" received on July 10, 1996 at Chemical CompoundsInc.. The reason for the re-submittal was to further verify specific responses whichour company regards confidential information. If you should have any furtherquestions or require additional information, please feel free to contact Jim Giannottiat (201) 485 - 3212.

Sincer$<,ly,.r~ .

Jim Giannotttijg.lJGC.c: AC/SG

866300001

TIERRA-B-004600

__ ATTACHMENT A REOUEST FOR INFORMATION

BackgroundThe United states Environmental Protection Agency ("EPA") isinvestigating the release of hazardous substances into thePassaic River. EPA has information indicating that hazardoussubstances from your facility located at 29-75 Riverside Avenuein Newark, New Jersey may have been discharged into the PassaicRiver.

/

Please provide the information requested below, including copiesof all'available documentation that supports your answers.1) How long has your company operated at the facilitydesignated above? If your company no longer operates at thisfacility, during what years did your company operate at the

"facility?2) a) Does your company have or has it in the past had a permitor permits issued pursuant to the Resource Conservation andRecovery ~ct, 42 U.S.C. §6901 e.t. ~.? If "yes", please providethe years that your company held such a permit and its EPAIdentification Number.

~. b) Does your company have or has it in the past had a permitor permits issued pursuant to the Federal Water Pollution controlAct, 33 U.S.C. § 1251, !It. ~.? If "yes", please provide theyears that your company held such a permit.3) Did your company receive, utilize, manufacture, discharge,release, store or dispose of any materials containing thefollowing substances: Yes No2,3,7,8 tetrachlorodibenzo-p-dioxin

or other dioxin compoundsAcetic acidAdipic acidAmmonia.AnilineBenzeneBenzo(a) anthraceneBenzoic acidBenzyl chlorideButyl benzyl phthalateChlorobenzeneChloroethyleneChloroform1,2-dichloroetheneoi-n-buty1 phthalateEthyl benzene- 1

866300002

TIERRA-B-004601

-

,-

Yes NoFluorantheneMethanol '"Methylene Chloride2-methylnapthaleneNaptha distillateNapthalene2-nitrophenolPetroleum etherPhenanthrenepyreneTetrachlorobenzeneTetrachloroethaneTetrachloroethyleneTrichloroethaneTrichloroethyleneToluene -xyleneArsenicCadmiumChromiumCopperLeadMercuryNickelSilverZinccyanidePCBs

4) a) Provide a description of the manufacturing processesfor which all hazardous SUbstances, including, but not limitedto, the substances listed in response to item (3), were a productor by-product.

b} During what parts of the manufacturing processesidentified in the response to items (4)(a), above, were hazardoussubstances, including, but not limited to, the substances listedin response to item (3), generated?

i) Describe the chemical composition of thesehazardous substances.ii} For each process, what amount of hazardoussubstances was generated per volume of finishedproduct?iii) Were these hazardous substances combined withwastes from other processes? If so, wastes from whatprocesses?

2

866300003

TIERRA-B-004602

"'.,

5) Describe the methods of collection, storage, treatment, anddisposal of all hazardous substances, including, but not limitedto, the substances listed in response to item (3) and (4).Include information on the following:


b) If hazardous substances were taken off-site by a hauleror transporter, provide the names and addresses of ~he wastehaulers and the disposal site locations.

c)' Describe a~l storage practices employed by yourcompany with respect ~o all hazardous substances from the timeoperations commenced until the present. Include allan-site andoff-site ~torage activities.


1i) When drums were stored outside, were empty drumssegregated from full drums?

stored outside, were the drums storedstored on areas that had been pavedPlease provide a comple~e description

d) What processes do you use to treat your waste? What doyou do with the waste after it is treated?6) a) For process waste waters generated at the facilityWhich contained any hazardous substances, including, but notlimited to, the substances listed in response to item (3) and(4) :

i) Was the waste stream discharged into a sanitarysewer and if so, during what years?ii) .Were they treated before being discharged to thesanitary sewer and if so, how? Please be specific.iii) If the waste waters were not discharged to thesanitary sewer, where were they disposed and duringwhat years?iv) Please provide the reSUlts of any analysesperformed on any waste process streams generated at thefacility.


-3 866300004

TIERRA-B-004603

i) Did the drains connect to a sanitary sewer and ifso, during what years?ii) If the floor drains or other disposal drains atthe facility were not discharged to the sanitary sewer,where did they discharge and during what years?

c) i) Did any storm' sewers, catch basins or lagoons existat any time at the facility and if so, during whatyears?ii) If catch basins or lagoons existed, were theylined or un-lined?iii) What was stored in the lagoons?

-iv) Where was the discharge from any of thesestructures released and during what years? Was thisdischarge treated before its release and if so, how andduring what years? What was the chemical compositionof any waste waters released, and during which years?

d) Please supply diagrams of any waste water collection,transport or disposal systems on the property. .

e) Also, EPA has information relating to several instancesof discharge of process waste water 'into the sewer system in 1992and 1995. Please provide a detailed description of theseincidents.7) a) For each hazardous SUbstance, including, but notlimited to, the substances listed in response to item (3) oridentified in the responses to item (4), above, provide the totalamount generated during the operation of the facility on anannual basis.

. -

b) Were any hazardous SUbstances, including, but notlimited to, the substances listed in response to item (3) oridentified in the responses to item (4), above, disposed of inthe Passaic River or discharged to the Passaic River? If yes,identify the hazardous substances, estimate the amount ofmaterial discharged to or disposed of in the Passaic River andthe frequency with which this discharge or disposal occurred.Also please include any sampling of the river which you mighthave done after any discharge or disposal.8) Please identify any leaks, spills, explosions, fires orother incidents of accidental material discharge that occurred atthe facility during which or as a result of which any hazardoussubstances, inclUding, but not limited to, the substances listedin response to item (3) or (4),. were releaseq on the property,into the waste water or storm drainage system at ~he facility or

4

866300005

TIERRA-B-004604

· "~ •.-.. :.'-'-."," . ~"." ..,.. ..,:: -". ._ , .- ...

~ to the Passaic River. Provide any documents or informationrelating to these incidents, including the ultimate disposal ofany contaminated materials.

a) Please provide the results of any sampling of the soil,water, air or other media after any such incident and before andafter clean-up. Please provide in this information all samplingperformed for or by NJDEP.

b) Also, EPA has information that due to an industrial sewerline break in 1992, an unreported quantity of aniline wasdischarged to the Passaic River. Please provide all informationrelating to this and any other discharges and any measures takento mitigate the impac~ of the discharges.9) a) Was your facility ever subject to flooding. If so, wasthe flooding due to:

i) overflow from sanitary or storm sewer back-up,and/or

b)event.

ii) flood overflow from the Passaic River?Please provide the date and duration of each flood

- 10) Please provide a detailed description of any civil,criminal or administrative proceedings against your company forviolations of any local, State or federal laws or regUlationsrelating to water pollution or hazardous waste generation,storage, transport or disposal. Provide copies of all pleadingsand depositions or other testimony given in these proceedings.

a) EPA has information that your facility has received.several notices of violation for discharges of waste water intothe sewer system, inclUding a NJDEPE Field Notice of Violationissued on January 7, 1992 and a PVSC Notice of Violation issuedon February 9,·1995. Please provide information on how theseviolations were resolved.11) Provide a copy of each document which relates to thegeneration, purchase, use, handling, hauling, and/or disposal ofall hazardous substances, including, but not limited to, thesubstances listed in response to item (3) or (4). If you areunable to provide a copy of any document, then identify thedocument by describing the nature of the document (e.g. letter,file memo, invoice, inventory form, billing record, hazardouswaste manifest, etc.). Describe the relevant informationcontained therein. Identify by name and job title the person Whoprepared the document. If the document is not readilyavailable, state where it is stored, maintained, or Why it isunavailable •.--

5

866300006

TIERRA-B-004605

~ 12) a) Did you or anyone else sample the soil, ground water,surface water, ambient air or other environmental media at thefacility for purposes other than those identified in questionsabove?

b) If so, please provide all other documents pertaining tothe results of these analyses.13) a) Has your company owned the facility at the locationdesignated above? If so, f.romwhom did your company purchase theproperty and in what year? If your company sUbsequently sold theproperty, to whom did your company sell it and in what year?Please provide copies of any deeds and documents of sale.

A '


c) To the extent that you know, please provide the names ofall parties who owned or operated the facility during the periodfrom 1940 through the present. Describe the relat1onship, ifany, of each of those parties with your company.14) Answer the following questions regarding your business orcompany. In identifying a company that no longer exists, provideall the information requested, except for the agent for serviceof process. If your company did business under more than onename, list each name.

a) state the legal name of your company.b) state the name and address of the president or the

chairman of the board; or other presiding officers ofyour company.c) Identify the state of incorporation of your company and

your company's agent for service of process in thestate of incorporation and in New Jersey.

d) Provide a copy of your company's "Certificate ofIncorporation" and any amendments thereto.

-

e) If your company is a subsidiary or affiliate of anothercompany, or has SUbsidiaries, or is a successor toanother company, identify these related companies. Foreach related company, describe the relationship to yourcompany; indicate the date and manner in which eachrelationship was established.

f) Identify any predecessor organization and the datesthat such company became part of your company.

6 866300007

TIERRA-B-004606

_ .i......,~.".",_ - .~'.'.~.';, .:.- ..

- rdentify any other companies which were acquired byyour company or merged with your company.

h) Identify the date of incorporation, state ofincorporation, agents for service of process in thestate of incorporation and New Jersey, and nature ofbusiness activity, for each company identified in theresponses to items (14)(e), (f), and (g), above.

g}


15) Provide the name, address, telephone nUmber, title andoccupation of the person(s) answering this "Request forInformation" and state Whether such person(s) has personalknowledge of the responses. In addition, identify each personwho assisted in any way in responding to the "Request forInformationll and specify the question to Which each personassisted in responding. Please include the names and addressesof former employees who were contacted to respond to any of thequestions. •

-7

866300008

TIERRA-B-004607

-- CERTIFICATION OF ANSWERS TO REQUEST FQR INFORMATION

State of New Jersev

County of _E~s~s..a:e~X'l;.... _

I certify under penalty of law that I have personally examinedand am familiar with the information submitted in this document(response to EPA Request for Information) and all documentssubmitted herewith, and that based on my inquiry of thoseindividuals immediately responsible for obtaining theinformation, I believe that the submitted information is true,accurate,-and complete, and that all documents submitted herewithare complete and authentic unless otherwise indicated. I amaware that. there are significant penalties for SUbmitting falseinformation, including the possibility of fine and imprisonment.I am also aware that my company' is under a continu~ng obligationto supplement its response to EPA's Request for Information ifany additional information relevant to the matters addressed inEPA's Request for Information or the company's response theretoshould become known or available to the company.

a1herto CelleriNAME (print or type)

presjdentTITLE (print or txpe),

~ ££tltltttf'SI 'ATURE i·

--.Sworn to b~ me thi~7day of"Z.'i ,JGli'\.., 19.....w.

C-;.-;;d=.->' .....----

-866300009

TIERRA-B-004608

- CONFIDENTIAL

INFORMATION CONTAINED HEREIN RESPONSE TO QUESTION # (48) CONCERNS PRODUCTS,MATERIALS AND PROCESSES IS PROPRIETARY AND CONFIDENTIAL AND MEETS THE

REQUIREMENTS OF 42 U.S.C. §9604(e)(7)(E)

CHEMICAL COMPOUNDS. INC.RESPONSE TOREOUEST FOR INFORMATION DATED JULy 9.1996

The following are the responses of Chemical Compounds, Inc. to the Request forInformation from the United States Environmental Protection Agency, dated July 9, 1996.

.-I. Chemical Compounds, Inc. (CCI) has operated at the facility in Building #17 at 29-75Riverside Avenue since 1990. It acquired the facility in July, 1986 (See Deed -Attachment 1) and installed equipment through 1990. During the 1986-1990 period itcontracted with another entity for the manufacture of its products (See, TerminationNotice to Southwest Photo Chern., Inc. - Attachment 1).

2. (a) Yes, CCI has had a permit pursuant to the Resource Conservation and RecoveryAct since 1990. Chemical Compounds lnc.'s EPA Identification # is NJD 108661737.(See Acknowledgement of Notification of Hazardous Waste Activity - Attachment 2.)

(b) Yes, CCI has a permit pursuant to the Federal Water Pollution Control Act, itsamendments, the Clean Water Act and the Rules and Regulations of the Passaic ValleySewerage Commissioners. The Permit Number is 20407122 and CCI has had the permitsince July 20, 1992. (See copy of the Sewer Connection Permit with Passaic ValleySewerage Commissioners-Attachment 3.)

.-866300010

TIERRA-B-004609

- 3. Yes, the following is ccrs response to question NO.3.

--

::;~i~:i'~·1~iBll~!lq1is·miimm~f:f.t~~t~;\::%8kl::'·'.:·:-:::~~J:~:~j~~%~;~;·:f~i:jw~~~2,3,7,8 Tetrachlorodibenzo-p-dioxin or I X

allier Dioxin CompoWldsAcetic Acid X IAdipic Acid X

Aniline X IBenzene X

BellZo(a)anthracene X

Benzoic Acid X

Benzy Chloride I X

I BUlylBenzyl PhthaJate i X

I Chlorobenzene I X JChloroethylene J X

Chloroform :: X ri

1.2-Dichloroethene i X

Dj-a-butyl phthalate XEtJlyl Benzene X

Fluoranthene I XMethanol X I

Methylene Chloride X

2-Metllylnapthalene I XNaptha distillate X

Naphthalene X

2-Nirrophenol X II Petroleum Ether ! X

PhelUwtluene I XPyrene X

Tetracltlorobenzene XTetrachJoroethane

--XTetrachloroethylene X

Trichloroethane f XTrichloroethylene 'I X

Toluene I X

Xylene X

-866300011

TIERRA-B-004610

CadmiumxXx

I Mercury I 11 X

1Nickd

-I'I X

Silver I X

E ZiDc i X ICyanide X

I PCBs I I X

CoDDeI'

LeadX

..... _--.._--_._~------

REDACfED-INFORMATION CONTAINED HEREIN RESPONSE TO QUESTION # 4a CONCERNS

PRODUCfS, MATERIALS AND PROCESSES IS PROPRIETARY ANDCONFIDENTIAL AND MEETS THE REQUIREMENTS OF 42 U.S.C. §9604(e)(7)(E)

_....1---------- ._--- _._----_._~--~---

866300012

TIERRA-B-004611

._-------~~.--~-~._-

-REDACTED

INFORMATION CONTAINED HEREIN RESPONSE TO QUESTION # 4a CONCERNSPRODUCTS, MATERIALS AND PROCESSES IS PROPRIETARY AND

CONFIDENTIAL AND MEETS THE REQUIREMENTS OF 42 V.S.C. §9604(e)(7)(E)

..._._---_._----

866300013

TIERRA-B-004612

-

-

-

REDACTED

INFORMATION CONTAINED HEREIN RESPONSE TO QUESTION # 4&CONCERNSPRODUCTS, MATERIALS AND PROCESSES IS PROPRIETARY AND

CONFIDENTIAL AND MEETS THE REQUIREMENTS OF 42 U.S.C. §9604(e)(7)(E)

866300014i. .&•.. 4 .«.4

TIERRA-B-004613

---_ .._-- -"-_ ..__ ._-"

--

REDACTED

INFORMATION CONTAINED HEREIN RESPONSE TO QUESTION # 4a CONCERNSPRODUCTS, MATERlALS AND PROCESSES IS PROPRIETARY AND


.'

"

866300015

,J !,~4. .!'" ..... Q . . 4. -*F (..s. _ J ._. i:.W_'_., .,

TIERRA-B-004614

-

,.- ."

REDACI'ED

INFORMATION CONTAINED HEREIN RESPONSE TO QUESTION ## 43 CONCERNSPRODUCTS, MATERIALS AND PROCESSES IS PROPRIETARY AND

CONFIDENTIAL AND MEETS THE REQUIREMENTS OF 42 V.S.C. §9604(e)(7)(E)

-

-"-0' 866300016

4.4-.,._

TIERRA-B-004615

REDACTED

INFORMATION CONTAINED HEREIN RESPONSE TO QUESTION II 4a CONCERNSPRODUCTS MATERIALS AND PROCESSES IS PROPRIETARY AND


-

4(b) Anachmenl 4 contains a list of process waste water streams and their respectivehazardous waste components.

i) The hazardous components generated as by-products in the waste water streamdue to the impurity of the raw materials are detected in ppb concentrations, andare noted in Attachment 4.

ii) The amount of hazardous substances generated per volume of each finishedproduct is not available. The hazardous substances generated in lhe waste waterstream of various products are contained in the range of SOO - ISOO gaUons of99.99 % water. Therefore. an estimated amount of hazardous substancesgenerated per volume of water is < 0.01 %. (See Attachment 4.)

'.

866300017

TIERRA-B-004616

-- iii) The hazardous substances located in the waste water stream are generated onbatch scale operations. The by-products are present in the waste water streamafter the separation of the product by filtratioll. After filtration, the waste waterstream is treated for regulated effluent exceedances. After treatment, the wastewater is stored in a 10,000 gallon tank. A number of process waste water streamswill combine in the 10,000 gallon storage tank.

5 (a) The following table is a list of employees at eel who were or are responsible for themanagement of hazardOUS substances:

j:~:;:~1'~;;~1~'J~~~Jll~'r. ~"""":"" '•..,,.,ii ··'~::t1~£r!Rn~ij.9fiB~i~~!~~!ltti~r~f,:,,~

Alberto Celleri Co-President Overall Operations

Harold Sullivan Co-President Overall Operations

Arturo CcHeri Chcmi callEn \'i ronmemal Waste Water T reatmentlHazardousEngineer Substance Storage

Jim Gianllotti Chemical/En \·ironmental Waste Waler TreaunentlHazardousEngineer Substance Storage

866300018

TIERRA-B-004617

- 5 (b) The following table is a list of transponers who were responsible for off-sitedisposal~including non-hazardous waste water:

,-..

Tn-Slate Motor Transit Co.MODO<J50Jll'N8

f~Htlllt~:~!P?r~~r,~:·~··.·'NFranks Vacuum Tmck Services.

Inc.NYD<J827'.l2&14

4500 Royal Ave,Niagra Falls. NY 1+303

.......]~~l::~g!,~il::'.'.Research Oil Co.

2655 Transport Rd.Cleveland, OH 4415

OHDOO4178612

Freehold Cartage (nc.NJD054 126 164


Systech EnvironmentalIlJ97 COWlty Road 176

Paulding, OH 45879OHDOO5048947

Laidlaw Environmental ServicesMDD<)80554653

3517 Whisky BOHomRoadLaurel. M.D 2()4H

Laidlaw Environmental Services3527 Whisky Bottom Road

Laurel. MD 20424

Maumee ExpressNJD')l166073S0

P.O. Box 278Somerville. NJ 081'(76

Rineco Chemical Ind1007 Vulcan Rd. - Haskell

Benton. AR 72015ARD981057870

Oldover CorporationVAD098443443

P.O. Box 63Rt. 1. State Rd. 652Arvonia. VA 13004

Old over CorporationP.O. Box 68

Rt. L, State Rd. 652Arvonia. VA 23004

Freehold Camlge Inc.NJD054116164

Chemical Waste M;umgernent ofNJ

NJD089216790


Ion Lister AvemleNewark. NJ 07105

P.O. 11:\Joplin. MO (,4802

ECOFLO2750 Patterson Street

Greensboro. Maryland 27407NCD9l!0842132


100 Lister AvenueNewark.. NJ 07105

Rineco Chemical [nd.1007 Vulcan Rd - Haskell

Benton, AR 72015ARD981057870

866300019

TIERRA-B-004618

:iM:N.ameQrBaZllrdllus::i*;·lj;r}1:;i:·~~t)$tilnce; /i::-;f

Raw Materials

or

LaboratOl1'Supplies

Acetic Acid

Adipic Acid

Ammonia

Benzoic Acid 50 lb. Bags I 2000 lb. Palates< I lb. Glass Bottle· Laboratory Scale

Chlorofonn < 4- L. Glass Bailie - Laboratory Scale2 gal. Solvent Lab Disposal Container

55 gallon sls drum - Waste5.000 gallon Tanker Truck - Waste

~.(JOOgallon S/S Storage Tank - Waste

MeulaJlol 55 gallon Stainless Steel Drum250 gallon Plastic Totes

·UlOO gallon S/S Storage Tank - Waste5.000 gallon Tanker Truck· Waste< 4- L. Glass Jars - Laboratory Scale

2 gal. Solvent Lab Disposal Comainer55 gallon sls drum· Waste

Methylene Chloride 55 gallon Stainless Steel Drum~.ooogallon S/S Storage Tank - Waste

5.000 gallon Tanker Truck· Waste< 4- L. Glass Jars - Laboratory Scale

2 gal. Solvelll Lab Disposal Container55 gallon sls drum· Waste

Toluene 55 gallon Stainless Steel Drum·LOOOgallon SIS Storage Tank· Waste

5.000 gallon TmIker Truck· Waste< 4- L. Glass Jars· Laboratory Scale

2 gal. Solvent Lab Disposal Container55 gallon sls drum - Waste

Xylene 55 gallon S/S Drum250 gallon Plastic Totes

~.OOOgallon SIS Storage Tank - Waste5.000 gallon TllIIker Truck· Waste

< -+ L. Glass Bottles· Laboratory Scale2 gal. Solvent Lab Disposal Container

55 gallon sls dnun - Waste

.-Waste Water

Storage(ppb Concentralions)Based on Analytical

Data

By.P,-~ ,,,,,lid OIl th. Wi .....

WAter WC;jln~

AniIi.... &'IZ.ne.Bcnzuic Acid. Cldo,oo",lZCIl ••ChlotoHnn. £U" 1 (lcnz.......

Methanol. Me1hvl~,," Chl<ltideN./,hlhoknc.2~Ni''''I~''''DI.

Tclt:l~hl<'l'o.t11\"I",,~.T"lwIlC.XylOl"'. '.ad. Zi"". Cy:.,id"

55 galloll dmm • Waste

~oo. 4,000 gallon S/S Storage Tank

10,000 gallon SIS Storage Tank

5.000 gallon TalIker Trucks - Waste

866300020

TIERRA·B·004619

- The SS gallon drums or 250 gallon Plastic totes containing hazardous substances listedin items (3) & (4) are stored on wooden palates outside on either a paved area withasphalt or a concrete pad. (See Attachment 5 for a facility layout for the storage areas ofhazardous substances.)

In December 1993, a concrete diked area was constructed outside the building locatedon the southeast part of the building with a capacity of25,OOO gallons. The diked area iswithin an 18 inch thick concrete berm approximately 4 feet high. [nside is the waste waterstorage area with (2) 4,000 gallon Above Ground S/S Storage tanks and (1) 10,000 gallonAbove Ground S/S Storage Tank on top of an 8 inch concrete slab. [n the past, the wastewater and or flammable solvents such as methanol, xylene, & toluene were stored in a5,000 gallon Tanker Truck in that same area. [n addition, waste tlammable liquids werestored in a 4,000 gallon Above Ground S/S Storage Tank in the diked area. SinceSeptember 1995. waste flammable liquids have been recycled. Currently, the 4,000 gallonS/S Storage Tank is being utilized for waste water storage.

Empty drums are segregated from full drums. The empty drums are located at themost southeastern part of the property. adjacent tb or in an enclosed shed.

5 (d) The waste water streams are treated by neutralization, chemical precipitation, orcarbon tlltration. The process waste water streams are transferred to one of (2) 1,500gallon mixing tanks for the introduction of treatment. One treatment involvesneutralization by the addition of Sodium Hydroxide or Sulfuric Acid to meet dischargeregulations. Another treatment involves carbon filtration for the removal of organics. Thedrain water is collected in an Above Ground S/S Storage Tank located in the basementand treated tor heavy metals. The treatment for the drain water involves chemicalprecipitation with the addition of lime tollowed by filtration. After treatment, the wastewater is transferred to a storage tank and analyzed.

If the treatments are effective. the waste water is transferred to a 10,000 gallon AboveGround S!S Storage tank. After the tank is full the waste water is combined with thesanitary waste water from the facility and pumped out of the building into the PVSCsanitary sewer which flows approximately 70 yards to an interceptor of the industrial park.The solid waste generated from treatment is non~hazardous and disposed off-site to aregulated facilitv. Carbon tiltration and chemical precipitation treatment methods haveonly been used since October, 1995. Prior to that time. the waste water was treated byneutralization.

--866300021

TIERRA-B-004620

- 6 (a) i) From July 1992 to the present, the process waste water stream was dischargedinto a sanitary sewer connected with Passaic Valley Sewerage Commissioners.Before July, 1992, the process waste water stream was connected to a 5,000gallon tanker truck for off-site disposal.


Hi) Before CCI obtained a permit for discharge to the sewer, the waste waterstream was collected in a 5,000 gallon tanker truck. When the tanker truckachieved maximum capacity, the water would be sent to a TSD facility fortreatment. eel obtained a permit for discharging process waste water to thesewer on July 20, 1992. (See Attachment 11, for manifests.)


-6 (b) i) & ii) From 1986 - February, 1992, the main manufacturing floor at the facility

was equipped with internal floor drains which were directly connected to thesanitary sewer. From February, 1992 through July, 1992, the drain water wascollected into an above ground storage tank located on the basement floor and sentdirectly to a 5,000 gallon tanker truck. When the tanker truck became fun, it wassent for off-site disposal. From July, 1992 - April, 1993, the drain water was sentto the 5,000 gallon Tanker Truck. then was combined with process waste waterand then transferred to an above ground storage tank in the basement. Aftersampling and analysis for effluent exceedances, the waste water was combined inthe basement with the sanitary waste water from the facility and pumped out of thebuilding into the sanitary sewer.' In April, 1993 CCI replaced the 5.000 gallonTanker Truck with a lO,ODO gallon above ground S/S Storage tank.

From 1995 to the present, the drain water has been transferred to an above groundS/S storage tank for the treatment of heavy metals by chemical precipitation. Aftertreatment, the drain water is transferred to another above ground storage tank foranalysis. If the treatment has been successful, the drain water is sent directly tothe 10,000 gallon Storage Tank, and mixed with the process waste water. Afterthe tank has accumulated to its maximum capacity, the waste water is combinedwith the sanitary waste water from the facility and pumped out of the building intothe sanitary sewer which tlows approximately 70 feet to an interceptor of theindustrial park.

c-866300022

TIERRA-B-004621

- 6 (c) i) There have been no storm sewers, calch basins,or lagoons located at Building #L7,29-75 Riverside Ave., Newark, N.J. since the beginning of operations ofCCl

ii) N/A

iii) N/A

iv) N/A

6 (d) The facility layout for Ihe collection, storage, and disposal of waste water can belocated in Attachment 6.

-

6 (e) On January 7, 1992 the Newark Fire Department and the New Jersey DEPresponded to a complaint of a discharge at the CCI facility. CCl's next door neighbor hadplugged up the sewer line. and when CCI'S personnel excavated the line 10 attempt toclear it, the contents of the line. including water cdlored purple with Red # 3 and Blue # 2dye was disbursed into the excavation. This water was pumped out of the excavation ontothe ground where it was observed by the Fire Department and DEP. eCI was ordered toclean up the discharge, which was analyzed and shown to be non-hazardous. (See analysisof soH and liquid samples - Attachment 8). eel was charged with discharging to thePVSC sewer without a permit (See Attachment 7).

Subsequently, after CCI obtained a PVSC permit, it was cited by PVSC for havingdischarged waste water to the sewer which contained some volatile compounds and metalsin excess of permitted concentrations. These discharges exceedances have been resolved,and current treatment methods appear to be keeping wastewater discharges withinpennitted parameters.

7 (a) The total amount of hazardous substances generated during the operation of thefacility on an annual basis can not be determined. The hazardous substances which arecontained in the waste water stream are determined by the purity of the raw materials. Asa result. contaminant concentrations differ from one manufacturing batch to another.

7 (b) Chemical Compounds Inc. has not discharged any hazardous materials into thePassaic River.

8 (a) There have been no leaks. spills, explosive fires or other incidents that occurred atthe eCI facility that resulted in hazardous substances being released.,-

866300023

TIERRA-B-004622

- 8 (b) eCI did not discharge any hazardolls material into the Passaic River. (See answer to6( e) for deSGription of incident.)

9 (a) Yes. CCl's facility is subject to tlooding due to the close proximity of the PassaicRiver. Flooding does occur due to the overflowing of the Passaic River. As a result. thewater generated due to the tlooding of the Passaic River is analyzed. treated and stored atour facility before discharging to the sewer.

9 (b) Flooding occurs during very bad storms, the dates of each occurrence are notknown.

-

10 (a) In 1992, due to the discharge described in 6(e), CCI paid administrative costs to theNew Jersey Department of Environmental Protection for the discharge response. TheNJDEPE Case # is 92-01-07-1025. [n addition. CCI was charged with violating theWater Pollution Control Act for negligently discharging a pollutant into a municipaltreatment works without possessing a valid industrial pretreatment pennit issued by thePassaic Valley Sewerage Commission. CCI pled guilty to a fourth degree water pollutionviolation with 'a tine of$5,000 for the offense and had to provide a check in the amount of$1,760.85 payable to the Office of the State Environmental Prosecutor to be used topurchase a one page advertisement in the Gloucester Times conveying a positiveenvironmental message.

eCI also paid for administrative costs when the Bureau of Emergency Responseresponded to a chemical fire at the facility on October 5, 1993. The case was closed. TheNJDEPE Case #'s are 93-10-05-0736 & 93-1O-05-l110.

On September 14, 1994. eel had received a Notice of Violation from the Division ofFacility Wide Entorcement - NJDEP. The inspection identified a violation of the SolidWaste Management Act (NJ.S.A. 13: IE-I et seq.) and Regulations (NJ.AC. 7:26-1 etseq.) promulgated thereunder. Remedial actions to correct the violations wereimplemented by eCI within days and 110 further enforcement was required thereafter.

With regard to violations of discharge permit limitations. CCI resolved the matter byentering: into a Consent Order and Final Judgement with the Passaic Valley SewageCommissioner on November 24. 1994. by which it paid $6.000 to PVSC and entered intoa compliance schedule. which was subsequently extended to July I, 1996. (See ConsentOrder and Final Judgemem and other relevant documents - Attachment 9 & 10.)

-866300024

TIERRA-B-004623

..- II) For the purchasing of listed hazardous substances. such as raw materials, in item (3)or (4), the following table indicates eel's suppliers since the beginning of operations.Documents such as invoices. bill of ladings. and a purchase order book for receiving thesehazardous substances are available.

--

Xylene

Acellc Acid

BrowlI Chemical 302 West Oakland Ave.Oakland, N.J. 07436

Duso Chemical 173 Smith SlreetPoughkeepsie. NY. 12602

Brown Chemical 302 West Oakland Ave.Oakland. N.J. 07436

TcxtiJe Chemical 990 Jersey AveNew Brunswick. N.J. 0890 I

Jones Chemical &0Munson SlreetLeRoy. NY 14482

TC,"'lilcChemical 990 Jersey Ave.New Brunswick. N.J. 08901

JLM Industries 8675 Hidden River ParkwayTampa, FL 33637

BrowlI Chemical 302 West Oakland Ave.Oakland. N.J. 07436

Te."'lile Chemical 990 Jersey AveNew Bmnswick. N.J. 08901

Bl'o\\1IChemical 302 West Oakland Ave.Oakland. NJ. 07436

Tc....ule Chenucal 990 Jersey AveNew Brunswick, N.J. 08901

Brown Chemical 302 West Oakland Ave.Oakland. N.J. 07436

Textile Chemical 990 Jersey AveNew Brunswick. N.J. 08901

Texlile Chemic.ll 990 Jersey AveNew Brunswick. N.J. 08901

Adipic Acid

Benzoic Acid

Methanol

Methylene Chlonde

Toluene

866300025

TIERRA-B-004624

-

For laboratory supplies, the tollowing table provides information regarding suppliers:

Acetic AcidAdipic Acid

Benzoic AcidChloroform

Methylene ChlorideMetlUUlolTolueneXylene

JT Baker

Fisher Scientific

89 Newbury StreetSuile 103

Damers. MA 01923

711 Fortes AvenuePittsburgh. PA 152J9-4785

For the hauling and disposal of listed substances, such as waste water, plant andlaboratory solvents, in items (3) or (4), the following table indicates CCl's past and presenttransporters and disposal facilities. Documents. such as manifests. for the disposal of thesehazardous substances are in Attachment I I.

Methanol, XyleneWaste Flammable Liquids

Freehold Cmage lnc ECOFLO270() PanefSQ.IlSt.

Greensboro. NC 27407Dye Waste WaterNon-Hazardous

Chemic:ll Wasle Management Chemical Wasle Management100 Lister Ave.

Newark. NI07105Methanol. Xylene Oldover Corporation

Waste Flammable Liquids

CMorofonn. Methylene Chloride. Tri-SI<ltc MOlOrTransit Co.Xylene

Laboratory SolventSWaste Flammable Liquids

Dye Waste Water Laidlaw Environmental ServicesNou-Hazardous

Dye Waste WaterNon-Hazardous

Waste Dye(HC Yellow # 2)

Methanol, XyleneWaste Flammable Liquids

Franks Vacuum Truck Servicernc.

Freehold Cartage Inc.

Oldo\"er CorporationRoute f. Slate Road 651

Arvonia. V A 23004R.incco

WO? Vulcan Rd. - HaskeUBenton. AR 72015

Laidlaw En\'irolllllem.al Services3527 Whiskey Boltorn Rd

Laurel. !\rID20724

Rcse,lrcl! Oil Company2655 Transpon Rd.Clel·eland. OH 4415

Svstcch Environmental113!}7County Rd. 176Paulding. OH 45879

866300026

TIERRA-B-004625

-

-

-

12 a) & b) There has been no sampling of the soil. ground water, or surface water at thefacility for purposes other than those identified in the responses above. However, anOccupational Health Survey was conducted by ccrs insurance company to evaluateemployee exposure to possible various airborne contaminates. The survey included airsampling for xylene, methanol and orhers As a result. none of the employees' exposuresexceeded the OSHA Permissible Exposure Levels for the above contaminates.Attachment [2 contains the report provided by CCI's insurance company.

13 a) Yes, CCl has owned the facility at 29-75 Riverside Ave. - Building # 17 since July1, 1986. Attachment I contains a copy of the deed of sale. The property was purchasedfrom Industrial Development Associates. Inc ..

13 b) N/A

13 c) In 1888 the Freeholders of Essex County sold the property to Triton Boat Club ofNewark. This transaction is recorded in Essex County Deed Book K-24. Page 133. OnMay 16, 1902, Patton Paint Company acquired the property from the Triton Boat Club ofNewark, as recorded in Deed Book 1-35. Page :70. Patton Paint Company was amanufacturer of paint and varnishes.

Thereafter, Pittsburgh Plate Glass Co. which manufactured paint and varnishes, tookthe subject property. The property was identified as Block 614. Lot I. The currentfacility - Building # 17 - was constructed by the Pittsburgh Plate Glass Co. as a chemicalresin manufacturing facility for its operation. PPG, Inc. which was formerly calledPittsburgh Plate Glass Co. purchased the property on January 31. [941. and held theproperty to August 2, 197 I .

In 1971. the site was sold to a developer, Riverside Ave. Properties. lnc .. Deed Book4382. Page [023. Riverside Ave. Propel1ies. Inc. thereafter leased the site. On October11, 1979, the property was sold to another developer. Industrial DevelopmentCorporation, which sold the property a month later to Industrial Development Associates.The principal ofIndustrial Development Associates is Anthony V. Pugliese. III. IndustrialDevelopment Associates leased the building to S.B.S. Chemicals. Inc. and Desachem Co.,Inc, manufacturers of chemicals and detergents. S.B.S. Chemicals and Desachem Co., Incoccupied Building # 17 pursuant 10 a lease agreement with Industrial DevelopmentAssociates. which argument expired on August 14, 1985. Thereafter. the building wasvacant and the lot and block numbers were changed and subdivided from Block 614, Lot 1(partial) to Block 614, Lot 66. eCI has no relationship with the pasl owners or tenants.

866300027

TIERRA-B-004626

- 14 (a) The legal name of [he company is Chemical Compounds tnc.

14 (b) The president of the company is \1.r. Alberto CeBerl. Mr. Celleri's address is toBaldwin Court, Roseland. NJ 07068.


14 (d) Attachment 13 cOn£ains a copy of the company's "Certificate oflncorporation"and amendments thereto.

14 (e) eel is not a subsidiary or affiliate of another company.

14 (f) Chemical Compounds Inc. has no predecessor organization.

14 (g) Chemical Compounds Inc. has nor acquirfld nor merged wi[h any other company.

14 (h) N/A

14 (i) There are no previous owners of(Cl.

15. The person answering this Request tl.lr Information is Alberto Cdleri. President ofCCI, 10 Baldwin Court, Roseland. New Jersey 07068 (201) 364-0370. Mr. Celleri haspersonal knowledge of the responses. Mr. Jim Giannotti. 72 Califon Drive. Coloma, NJ07067. (908) 382-5591. a Chemical Engineer a[ eCI, assisted with the preparation ofthese responses.

866300028

TIERRA-B-004627

866300029

" .........,a "-" {i.

TIERRA-B-004628

,-

-

...:::....0': ~.:~' ~. -,......

"

'.

\

.-: ..... :..". - ....

..

". DEED I(.·~'II·,I allll n'lIl1'n 10;

J r:;!U.~"'" ~ Ilc:vcJ ()p"",nl'I\:!S £(JC iu cc.:s

(ir-iUliur.Tn

Che,ni.~J Compc....'''lu. Inc._.) (iranlil:C.

__ "r-- ....' ..,.

';"lH'q.., Gc1t'ri son, J::~quirc.f'J5 l:lillull t.v..,nu,,",·linuu. I';.;", ,I..,n ...,y U7015

" , ,\:t~;~t'i~::~~~~i~~:":'............ ", ... ,.,:,",,~~~~ ... ;..

866300030r'....~.......~:~~'.:

TIERRA-B-004629

-

-

. - -

...

:- ....

t04-0Ito· .--CAHI AMOSAlE ~ ...... (~_. An"co. TaING O.~ __ I"llIAl........ :lUIIVl.i

e:-. ......,lIU ..... LU E Il IU.. '... caOI...c..-.-c.u. 0 IfJ 01Gi_

DEED•JIIJ Y I • III uo:. .nUl 1:Iced il RIlId" on

BETWEEN HIUUS'1'RJ.hL IJJ::VJ::I.Ul·NJ::lI'J' /\S~'UCJ.l"L'J::S,l41 LOltiZa AV<:m.l1!G.u:fiald, llal~ Ja.CSI·l¥

... (,Ullluf,jjUon ot 'he ~...lc ur th:w .JarSc.y.l~l 1,.. n:;:.1Avenue. Gat'tio1u. iluw Jarsey

r"lorr"d IQ .... Ihe \.i",nlur,

AND ChUOliC.11 Compounds, Ll\c.

III 'f.1 I 1",Y 1t"."I, S l ,lIlhulJ!:, rJ",.. .J,..: L' s..:y

h,:I&:lInl In iU ihC' lililIIlOS:C'.

. T,."sI., uf O",!'cnbip*. !III: (i.al1ll~t 1''''''5 amJ -':-UII\,\')" IU",mih:U. u"n~hlilp -:') En.: I1CU('lCr')+d""orlbcd belo", II> Ih" ( ..... 0' .... I hI' lrall.fer 1.\ lIIall. [,,, Ihe """.of ClnCl /lull,l, ~c1 th n,,'~Y f'x va

'rhouliO)nu (SI!I!i.OllO.lllJl l)oJl,IJ.'!: .11111 CltJ/lllll--------- .....----- _

----------------- ....-- -_ .. - --- -- --- ---- - 11tt: (; ......... ;J~ ... ull...,4cl.'~i- 1":':':lfll ut ('u:.. munc)'.

Tall M."''III""k N...o No (Ir"p"rl)'

Jhl~t."n, IN.J.:>,,\ .. lIo:l)·!.1I ;"1l",i"'I'~I"l" ..1 New;u:k61 ~ I.ul Nil. Ct6 o'\\.':cuun&Nit.

l:ax i"&:nldiQ.i ....~ lUullbe.r i" a,';.ibhh: CUI Un: lI..~c- ul Ihi .. Ikell. '0 .......... , d • ., ..... ;t... 1

J'ruperlr~ The p"I(II.:II)' .:.....p.p.b ..."j she Iian,J ilU,1 ;.&11dM: hhikJil.lp. ;;11111:lIoU"~U'U:~ UII 11M:bud inCi ty ..r Il~w" L'k

Essux ;ukl .s,.:sIC- " .. New JC(~r. rh" aq..1 dc."M.:UltUUQ Ia..

Ih.Coullty u(

De:in9 knuwl1 ant! d~!:u,:L·jbl..:d i.IH liJ;·upIH •• o,. I..L,L ",;" .Ib 11l",t oilL. "sucJcJescribed on a "':t;lt~ifl ~utJtljvi:;i.(.J" IU.".II .;;:nt~tLi'; "l~&:",p~uh_.1 Sui."'j· ..i~ionLot 1 - Ulock 614 Nuwack '1';.lC Hill'" I'r",,,,rL,,1 hy 1S.•.:L"il.:, H."lcO...ua1J ~Watson. doted JUlie 25. IlI84, ;lIld (il",1 ill III<... ~:~SI:lX Cuullt;y R<::c}lstcl"SOffi.ce on February 4, 19115 o)s ~Iap He.. J5!1<4. 'j'his conveyancl1 is ",uue5ubject to iJnd UJ.OIl<] wlt;1\ the..: riqht "I il1lJrc:ss .ancl l..:<.jr"sti <lIang,over .:11111through Lhu ",,,';"III.,,,l .1 n:.. I,. i.1 .. lit .",,1 ''''UY i,"'II I.U.· in 1.1,,::atorementiuned Iluhuiv i"j Ull 'Aolp.

See Sehedule A aceachad hereto fur aJdieionaL uescripcion,

d31S1lU:I - ,..li ...... '}' -r ......, 1i;J'r ..' . ....'1" .'7

.'

.J

TIERRA-B-004630

-

-

--

S<.:UEUULE 1\

All those certain tr<act "I: p"rcuJ lie l ..nd, a~d allY im-tS now or hereinafter c~nsLruCLud theruon lyLnq and be-

provt;menh c ey of Essex in till::. eic.}· (.f UC\oI..rk. and the Seaeeinq Ln t e Dun ' .• f 1Jof New JeJ::sey, being furchar dCSl;J:1.I..". ;'5 (. II"''' ~

Being knovn and dcsllnated as Lot C 1ft Block 614 a" shovn on Hapene1c.lecl "Kap of Subdivision of Lot 1 - IIl0ck 614" filed FeblN4ry 4, ·1985 1ft

the E.,,_ Counc.y 1l.. ,lscer's OLUce .s Hap Nuad.4.!.r 3594_

... ins {.. teher describ ..o a.. Collowa:

llEClNHINGat: • paine uhere ~ha "orthe4storl" bOl4ndar" Une of Lat I1n Ilock 614, .S sho ..... on the ilbove ..entiuned •• 1', interaeccs chc UnitedState. P1ethead and lulkhead Line alan .. tbe ra.a.ic R.iv... , and running. chence:

(I) AJong "aId Picth ... d and Il4lkhc.;uJ I.ine, llorth ]8 d....ne. 47 ..inure...... 20 seconds Ease 81.94 Ceet to 0\ point; t1,,:nce:

(2) CQncinuillJ: alonG SOlidPierhead ilnd Bulkhead l.ine. lIorth 31 decree.09 ..inutos 20 seconds East 25.41 (ect to a point; thence:

(3) North 51 decrees IS _inUles 40sc:co"ds lIost 100.OO"£eet ta a point;thenee:

'. (4) lIarch 69 decrees 4] .inutes 30 s ..conds Yest 5Z.33 feet to a point;cha.nce:

(5) So~t~ 36 delrees 51 .laut •• 20 sacnnds lIest 79.00 fece to a pointin the lIorthensterly ooondnry Ii" .. (I( \.ot I: thonee:

(6) Alanl said Hortheasteri,. loou"dary line of loOt J, South 52 desr ....37 ..inutes 40 ...conds t-st 141.72 feet to & p01nt in the UnitedStlll ..S Pierhead 411dBulkhead LJllc alld the puint and plaCIl ofBEGIJfHl"C~

Selne 81so kllown ..s I••'t lib in Block 614 on ~hc 'ax Hap of th .. Cit)' of Nrvar

866300032 .:.-.'•..

TIERRA-B-004631

........ ':.. ...::.:

-"

,....

-'

.- .....~

Th6 conveyL&I1":u c.( the r.,), <:<Join<J C<i1SU.IlQl1t fue in~lcess <i1nd O1qrass ismilde I!l(prcslily llllbj~ct to the (; ....lntur··U .... ll".'l:i('n 1:0 mllint ..dn S,lIl1l1Clt i.ts own cuU~ -land .aX(J~IUh: ill cu.".•..,,, w, th il11 uthut:s UKiIU] .. aGlQnnd it. is unol.,clieOU<l "II"'t t:htl (;I',ll1t'~r !'h.1I1 h.I\'r, nn r.~s[l..nsibilityor obi i~ •• tj(>l\ in that, •·•.l<J~ .. rl Wh...l..H",Vr:.""

This conveylJnce is madoa sub j.:ot. tn tho .'n ~luwi nq cuvenant. which shaflbe conscrue,l .;IS a covenant runniuCj wi t:h th", lanu bindinl] the. Grantee.les successor,; ~lnd ass Iynl!.

The Grllnt:ee, ics SI1CC~SS(It'S Lind assigns. 51:.:1J1 100obligated to paytq,e Grantor. i cs SIJCC(!IiSOCS 01'1<'1<lssigns. Cive I St.) percant of eheCOSl: of snnw rCiRov~l, ~lI"'L"d .hH"vicG, ;'11.1 .1lCtcrinr je,nitori011 andma-intenanCQ service .,rtrihut;,hl..: 1'0 tho.: pn:JIIis~s ownoel by tile Graneorof whi ch the prom i 5.:lS """VHy,,') \I..,r"II ..... 1I· r 0 ..".. :<1 .. £1:1 Tl:_ 'rhe. <:Cllntaecoven.,nts to p••y <lily <I, •• 011 .. f tile. ,"I:L.It",u;,d.T riONts within ten (10) dl%.ysuf t:h~ cecci £It uf the l;r<lIltur'!l hiJ I I'm" liillaG. rn the .::vent: that t:he ••__'0

C&:lIl1tee C"ils t:o poy ~... y at' ;,L1 ur ,-h" ~C""cs"l" costs within thirtyDO} days of tit.. r<::ccil't ••f (;r:-lnl.or's hill fcn° 1::"I1e. said casts shall

-become!a liell ;AlJ'ainst lllcSI< p,"clasic.s '-/hich li.::n Ghall IIQ subordinateto any moa:t:g4gl:. l-i~n ilg ••i nst tlh:SU prmai ,ws provi <leel that. the proceedsnf' such mortlJiHIQ hilvQ !>cun inv.-,!>!',':<I illt .. the pr"llIis.::s described above.

Tn'll Grilnte~ .. .tau covenants '.'ll! thl;: (;.",lntu&: to join .lny propertyowner's o1SS0Ci<lei on fonn",r1 lillh:'il~qucnL to thi s conveyance to administerthe tcr.ms of tho C(JvenDnt. Th.~GC.-J1l1:lll·I·cpt·ascllt.s thilt it shallcause any of tho remaining pn'(lerty 'IWnoilc1 hy it .1t 29-75 RiversideAvenue, NI!WlIt'lc, New Jel'sllY, of which thcs6: premises ~Qrmed 01 part,to bl! charged with a simiJ.u- covenant :11'1<1that i I: sho1l1 fairly andevenly ilcminister same ..." to .,11 of 1:1J~ p"omi sas .lffacl:lld.

This conveyance is- 5uhjec~ t" Ci/Ren'en!:s lInd l·cstrjction5 of recordif any. zoning ol:dinances, 5t.:ltO. cnunl:Y i/nll muuicipal 1ilws orordinances affocl:ing tho premises illld such st .. te of facts as an accuratesurvey would reveal.

1')0'- f ')1'5'''~,'', ..II /',1.1, ••

TIERRA-B-004632

l ;··.··!'Ilf, ,.., '..'11;

'.

...

'.

1·,II...~lIIift hI «;r •• ttur. "[b,,· 'in ,"UUU!lo\:'l'I It •.:.i. U...• (i ...mhl, '&on '~lInc W" 04..-1 lu ~1U;uUlh~·r .hc.M"IIpc:rly. 1hi.> ,111:0loi1110.: is .:0&.11: .... ··.·uu· u 01)0.In ptoiot.h .. • ,·i:..·CN.J.s :,. -1(•.-1.(.;. n~u..I""f"'~ 'uc:""'"' ciLo.ltClu' t~I;"""" h;III:l11I14:.II~',,"-.·IIu .. ,un,,· I· · i un , ,. bu.-I. ..Hi·'· , ·lfiU'''· ••• I"U"~'••"-hr U llr:.. milt:E~'''' I" aUu"iUt;"' J''''!~tl''·'l' hI h,· 1·••I·I".~" ,~.IU"·.I It , ~, " •••

-

Si~n.CI"". TI:Uli Ik ....'lJ i, ~i.a:n,·d mNI .*~IL"'''''''III h, .'n: (il04""" \ ,IIUIIoI:I t.':U'IKllalll: .dhi.-'l:U .. ) ",I Lh~•.buc::ltJht' hilI U( Ihe J41~tI''''''OC .. it" ~~lqk";Ur:).·..1 .~ alhM:d

••• : •• r ... -." ..... ~.. I ,IIJIIS1'1ll/\I. lJt,:va;:J.CJ!"·I£::u·r I\SSOClr.TES- .....•: ,~, r.I ..( .'. . II\' : I IIlJWj'I'1I 1/\ I. n.!-:VEJJ(lI'~Jl::If1; CU1U'ORA'I'IOI-l .....~~~..cd h)o:,": ... '0 ';"11,010.11 P ••• L.ttt,.;l .., L-+:' {. "{:.";'; j '. I

{:;t~;:~:v',.,:fJ;1i:' ..c .;. ' Ilr: : "'.

\~ Crlt;ra~:l'ugJ:.ies-,:;"-·~····'''·- ......S'....CI"')· Alii 11I1II'( ·..~.'./~:;;;;i·j'df"~:....l~\';...,1II.....~:~.;.:~:::~:'~..;'~ ._~".' .. r!1! •••

. S1'ATl: (W NI-:W JI:KSI'\·. ('OW'" \' Ill· '·;,H•.,I( ~s..I l'UK'" F'" 111,".HI ,J u1 y I 1'~lC.

Plltri..:i .. l'u'.! I ic!:(:pcncun:dly ..-;aUN: ...... nn: UK· iUkJ Un,. PC''''''''' iu.·lllu"'·k:"~I.·d u... k ....... ,. '411'U)O ~1I~':K:Uu ••• Umc:

1;'1 Illis I""""" i. II,c "',· .. ·••• 1' .. 1 l."huH.· i .11 IlO::VI:lu[lIHcmt:Asaocilltes "ie ""',H.r.""" ua"..... ill II.B 1).:,,&1;....) ehb- p:n..II .... .IIt- ~u,,,,,inl "ll1"~!lI I.. the ...~n.i"t= .t4 .h,~ ............II)' UII:IwullCl "'"'''.H;'''''t: .. '.i-.;t:, ,,-1.41t.

,.n thany V. 1'lIq IlC"C: • r 11 .1,,' , , ", "I 'hc ,....r'''.lio ...;(''OJ II...~ I ~'"d IMI-a.Mr.'''''' h·ln ·....·" It, Ih...• .""'1""'.1."'''' .n ,....,,·.dutn,u \".., 1 )"" h.... ''""11 hJ· a JII"''':'

U:~UIUiIiUti"~I iu~114. "' I ~ ·Iul': •

hU d.-b ''':U~tH' L."'."110 .111: I"t',-.:'. ,.,.,........ UN: ....· ..... " .... 11..,. .. "11 ...·'. "'.1:11 ...1I.Al'"d ..... I"~.....-aI:lei chi. IIC.,..'" s.paI Ih':II III ....... I:n i4IU.-..1 14.I" Ulflh ul JIH'''' t;u:u,~un.. .!.:III 1110:lull ~rkI""I""I"""I ... Ic".. i..u ,,,,..1, .. ,.. I., I..... I... II", ...... 'Dl ...r ..1 li.k i, S 1 !liS ,UIIO. !oISI....... ; ..:.•.. '.~ ...

.. (Slid e."l>ickrla,i,,,, i. ""lined ill I'<.J,S.A~ll:I!·~ I .. ' ....····'/t\. 1.;/'11/;"": .:~"IJC'h." :altd tl.WI.fa I.. Itd"It'"' IIII:'"un t" i 0.":...... . .~, ~..' .lllly J : 1'1Kh ~, i !.;! _...... < q:.:~y ...:.. .-', .·..;,..;:;,-=~;,':'·0;·:::.l:..ttl:i.f;"~~- ;.: ~!'

lIe'I~;;p'';;;'~-:'-:~~-'~~'I;<:j-:~--;;-j'~~"~~i' l';, tL'j eL, PuqU asa:;. \. ....i::.. ,.~ .:....~ :t:,Q St. .. tc uC Naw .lCl:Soy ...- ...~\.~~,,~~~.;.~):~.:, ..'

.....I· uccl ..,.:. '" _ .

".JJ"' ' ........-.

TIERRA-B-004633

• ' •• ' c· ." ; -\-"~,,-

t..'

',.,."..,... .

:~I

, '.~

- ..

-----------. "

~ ..-

..

DIAG~~~ OF THE BUILDING

~ .. '-4 ... .,1_ .. ..:.. ....<..1ItI c:

l--/,Z,"--l---------.

r 1:_ ....... (.~ .._, .."

II-I

f------------,I 4".~__'C .... ~ •II,~-------------.:

I·j

-l

rT

...

,IIII

----=-------:·1.1'

""I

:------ ... _---_ ....

.,11... ... _ .. l- - ..... ~. . . .: 'ff'.- .....• oiM.rt. ..

~.. - .... -

TIERRA-B-004634

-

-

-

. .. ~-.' ,. - .". .",., ..._ .... ';'':';.;;-:.,,;' .- .

i ~.

END /0 I 1'1' 0-September 10, 1990

Southwest Photo Chern, Inc.350 Elect%a StreetPat1Ona, california 91766

Attention: John Jeleniewski

Reference: Contract dated December 20, 19'83

Dear John:

Back in 1983, we entered into a Contract dated Decerrber 20, 1983 wherebyyou agreed to perfODn certain services for us. Paragraph 8 of saidAqreement provided that the Contract would extend for a period of five (5)years and annually thereafter unless either party gave the other ninety (90)days notice of teDni.nation.

'!he purpose of this letter is to give you ninety (90) days notice oftermination of our 1\groeIrent of ncccrrber 20, 1983 ;;u-rl anv subs<:xJuentill'l'lendmentsthereto. You are advised that the .J:"CStrictive covcnrint conb.linEXiin the Agreement and the confidential in.fonration obtained under saidarrangerent with us is protected in accordance with our Aqxeenellt.

C>.1r relationship has been a good relationship, and we o1Wreciatc theassistance you have given US in the past. QJr arrangEment is temil'1ated inaCCOJ:dancewith our Agreement and this .letter •

very truly }'OUrs,

866300036

TIERRA-B-004635

866300037

TIERRA-B-004636

..,.- . )

_.. ....

866300038

TIERRA-B-004637

866300039

TIERRA-B-004638

"_.

1 of 22



PERMIT # ~ ---I20407122

(Please use the Permit Number on any correspondence with PVSC)In compliance with the provisions of the Federal Water Pollution Control Act,its amendments, the Clean Water Act and-the Rules and Regulations of thePassaic Valley Sewerage Commissioners:

(herein. after referred to as the Permittee)is authorized to discharge from a facility located at

~----------~~9-75 Rive~side Avenue - Building #17

~ --iNewark, New Jersey 07104

tu th~ Passaic Vallev Seweral!e Commissioners Treatment Works in accordance. - .with discharge limitations. monitoring requirements and other conditions set forthherein.

EFFECTIVE DATE '-----,07/20/92

EXPIRATION DATE ~----,07/20/97


Rev: 02/96

By"~a'~~ -,EXECUTI. CTOR'

866300040

TIERRA-B-004639

866300041

TIERRA-B-004640

'," ." ..... '"

- CHEMICAL COMPOUNDS me.

WASTE WATER POLLUTANTS

The following is a list of pollutants detected in eacb specific waste water stream. Thepollutants typed in BOLD faA:e are detected regulated compounds in our waste water discharge. TheDumbers indicated in the table (and in parenthesis) are of an average concentration analyzed in-bouse or at an accredited laboratory - throughout the year:i.

PRIORITY POLLUTANTS

HeavyMdol8

VOAC~ BNA Cone.b.

NDAPA 0.& Methylene Chloride Phenol (300)(38) 2-Nitrophenol (450)

COD - 450,000Aoetooe (13,200) Nitrobenzene (2S6)

ppm ChJorofonn (25) Aniline (2680)l,2-Dich1oroethaDe (130) 2-Nitrcaniline (&00)

Toluene (1650) 3-Nitroaniline (870)ChlorobenzeDe (381)

- Ethylbenzene (26)ChlorometbaDe (550)

Benzene (960)o-Xylene (4150)

m.p-Xylene (103)

HCBlue#2 <0.20 1.0 2.0 Tetrac:hloroethyleDe 2-Nitrophenol (650)(220) bis (2-Ch.Loroethyl)Ether

COD - 60,000 ppm Chloroform (19) (440)

NHNFA <0.20 0.3 <0.10 Chloroform (12) Phenol (320)Methylene Chloride (25) l-Nitrophenol (770)

COD - 42,000 ppm l,Z-Ditilloroethane bill (2-ehloroisopropyl)Eth«(1800) (7700)

Tolueae (41) NitrobeD2eDe (73)Chlorobenzene (57) 2-NitroaniJine (820)o-Xylene (32,000) 3-Nitroaniline (860)

NPD <0.20 0.35 0.20 BelowMDL Phenol (26)2-Nitropheool (155)

COD - 82,000 ppmlsophomne (180)

2-Nitroaniline (300)3-Nitroani1in8 (980)

...--866300042

TIERRA-B-004641

-

HC Yellow#2

COD - 110,000• ppm

PRIORITY POLLUTANTS

VO..4 C8ncb

2-Nitroaniline (100)

BNA. Cone..h

<0.20 0.32 <0.02 Chlorobenzeue (2810)Xylenes (49,100)

l,l-Dkblorobenzene. (169)

2-Cblorophenol (496)Nitrobenzene (259)

2-Nitropheaol (3380)2-Nitroaniline (5510)

HC Yellow # 4 <0.20 0.850 <0.01 Methylene Chloride(94)

l~lNcbloroethane(7200)

Acetone (8600)Chloroform (53)

Xylenet (260)

bis (:khloroethyl) Ether(47,600)

bis (2-Ethylbexyl)pbthalate (107)COD - 190,000

ppm

DNHA 1.43 0.9 <0.01 BelowMDL 2,4-Dinitropbenol(12,100)

HCYellow#5 1.43 0.8 <0.01 t ,2,4-Tricblorobellune(44.2)

4-Chloroaniline (442)

BelowMDL

Nom 0.269 0.277 <0.05 BeJowMDL BelowMDL

COD - 225,000ppm

HC Red # 3 <0.20 < 0.01 Metllylene Chloride (31)Chloroform (41)2-BulaDOOe (54)

Bromodich10r0methane(31)

Toluene (11)m.p .Xylene (35)

l~Dicbloroethane (SO)

0.372

•••• MOL - Mean Detection Limit

866300043

TIERRA-B-004642

- .. ' .. - ':- '~.-:.... . ...

CASt~~~

.~ FILE•..100 tw1EFIELD 10

1180

ACCREDITro lJ,B(RATllRIES ne.IXUTll£ (R;ANIC AWLYSIS DATA

tlATRIXOlWTl1lf FACTlR __ ~ --DATE EXT1lICI£DDATE ANALY2EDANAL'tZED BY

toAqueous

- ....

9508916

LARRY

._..--....-...__ .--_..._._ ...._._-- ..........................................................CAS t ClJ'FIlII) lCIl to. CAS t CIJ'AlJI) ~ rn........................................................... ............................ ~.............................1117MB Acrolein U 61 788~ 1,2-Dichlaropropana U U

1071Jl Acrylonitri 11 U 66 101l6101., cia-l,3-Dichloropropene U. 4.87487' Chiorolllllthlflll "8 W 20 79016 Trichloroethene U 4.0

748J9 Bro.a_thana JIlO .. 20 714J2 8lInunll 960 .. 4.11/'S0l4 Uinyl OIloridl U 211 124481 Oibro.achloro .. thanl U 4.0

7500} Chloroethene U 211 7900., 1,1,2-Trichloraethene U 4.0;'l;1I92 Methylenl Chloride U 10 111061026 tr1lR5-1,J-Oichloropropllnll U 4.0

67641 Acetone 24008 .. 18 110758 2-ehloroethylvinylether U 20 .

]';150 Carbon OisulFlte U 4.0 7'252 8rollOloI'II U 4.11

75694 TrichloroFluoroMithane U 4.0 1)91796 2-HexlIRone Uil 9.0]1;).,4 1,1-Dichlorollthene U 4.0 108101 4-Methyl-2-pentlnone 68 ~.O

75J4J 1,1-0ichloroethane U 4 •• 127184 Tetrachloroethenll U 4.0

I1j60115 trans-l,2-0ichloroethene U 4.0 79J45 1.l,2,2-Tetracnlotoethane U 6.G67663 ChloraFar. 31 III 4.8 108883 Toluenll \;OQ lJ ;,0

107062 1.2-0ichlaroath~1 U 4.0 108907 Chlorobenzenll 68 III 4.0

78933 2-Bu tInane 1801 4.0 108414 Ethylbennne 26 10

71556 1,l,1-Trichloroethane U 4.0 100425 Styrene U 4.0

t:im5 Carbon Tetrachloride U 4.8 m028i • IP-Xylene J7 l.I 28--~llO54 Uinyl Acllhtll U B.O 95476 o-Xylenll 2~0 W 21

J4 Bro.adichloroeethenll U 4.0 156m cie-1,2-Dichlorollthllnl U 4.~

SI!ROIiA!E C(]MPllH)5 RECfP..QY L1MUS ....illllL1 ,2-Dichloraethene-d4 -lli. "

J6-114 ~Toluene-d8 --.1i "

89-111 -JILBro.a'luorobenlllne -.2lt .86-11; -..tL

J _ Indicates co~ound concentration 'ound belo- MOL. B - IndiCltea cOlpound found in associated blank.U _ Indicates coapound analyzed for but not detected. W - Result eKceeda s~eci'ic ground weter quality criteria.-

I ~Iaga .ra beeed on Specitic Ground w.tlr Quality Criteria tro. Haw Jersay Aegister dated February L, 199J.,

-.866300044

TIERRA-B-004643

' .....,:;.:....; ..... -;.. :..:..~ ."'-."~.'

ACl:REDI TED LABlJRAT~IES, It«.:.", atll 1lRG;lH I C RHAL. 'isIS DR TA

CASE HlJ'EER 3180 MiRlX AqyeousSAnPLE. tU'ID '1~O1l9'6 OILUT1~ F~ SU

~TA FILE >81194 DATE EXTRAl.'ED 06aB19SIEN"r HArE 0:1 DATE AtaYZED ozrnm

.ELO ID tQ!PA ANAl.. VZED BY P!U.

.......................................................... ..........................................................CAS • ClJII(lJO llOIL ro.. CASf; W1POJO lJ>/L rn............................................................ ..........................................................1089~2 Phenol JGO J SOO ~9SG7 ~Chloro-}-.ethylphenal U 1UOO90;578 2-Chlorophenol U 508 88162 'Z,4,6-Trichlorophenol U 500'il5487 2-l1Ilthylphenol U 500 9~954 'Z,4,S-Trichlorophenol U 500lQB'94 3&4-Methylphenol U SOU m85 '2,4--0initrophenol U 25001i8]'j~ 2-Hi trophenol 450 J 500 1001127 4-Hi tropheno I U 2500105679 2,4-0i .. thylphenol U SOD 5'4S21 4,6-oinltro-2~thylphenol U 2500

120832 'Z,4-0ichlorophenol U m 87965 Pentachlorophenol U 25011111444 bis(-2-ChloroethyIIEther U SOD 111142 2,4-Dinltrotoluena U 50Ut;417J1 1,J-Oichlorobenzene U IJOO 84662 D.ethylphthalate U 51101116467 1.~Oichlorob8nlene U 500 700572; 4-Chlorophllnyl-phenylether U SilO100516 &nzyl Alcohol U 1000 a6737 Fluorene U suo'I'0;5Ul 1,'Z-Dlchlorobenzene U 500 1110016 4-H itroan iIIRII U 25UU1086111 bis(2-Chlorolsopropyllether U 500 86}06 H-Hitrosodlphenylaline U 500621647 ~HittosO-Ol-n·prop~la.lnll U 5011 101m 4-8roDOphenyl-phtnylether U SUU1,7n1 Hexachloroethane U I)UII 118741 HDx4chiorobenzene U SuO9119~3 HitrobenleM 74 JW 500 IIS018 Phenanthrene U SOU79S91 15ophorone U 1)00 1211127 Anthracene U SUIl

6,850 Benz011: Acid U 2500 84742 DI-n-Butylphthalate U SODU1911 bist-2-ChloroetbDxyl"ethane U SOG 2U6440 Fluoranthene U m

-'~0821 1,2,~Trichlor9benZllne U Sill) 1290110 Pyrene U 50U20; Haphthalene U 500 8S687 Butylbenlylphthalate U SOD

tIl64;'8 4-chloroaniUna U 100U 91941 },} '-oichlorobenzidlne U 100U'i768; Hexachlorobutadlene U 500 56553 8enzota}Anthracene U 'dOnIJ76 Z-ftethylnephthelene U 500 117817 Bist2-Ethylhexyl }Phthll.te U "juu

,'7474 HexachlorocyclopB"ttdiene U 5DO 218019 Chrysena U 5DOn~'d7 2-Ol1oronaphthdene U 500 1178411 " Di-npOctyl phth.lete U !HIU

38744 2-Hl troan 11 ina 800 J 2500 2~99'2 BenlotbJfluoranthene U m151m Di.ethyt Phthalate U SOD 207009 8enzDtklFluorenthene U 'Ull

2011969 Acen.phthylellll U 1)00 50m BenzolaJPyrene U 500'19892 }-Mitranl line 871 J 2500 193}9, Indenall,2,J-ed}~rene U ~UOam9 Ace"aphthenll U 50a 5370J Oibenzote,h}Anthr.cene U .,00"2649 oIbenzofuran U ,00 191242 Benzol9,h,i)Perylene U ~OO606202 2,6-0initrotoluene U 500 62759 K-Hltrosodi .. thyle.ine U SUU

;lJ!RQiAfE gkfllJ:t)SHitrabenzene-dSt.Fluorob tphenyITerphenyl-d14fhenoHiS2-f 11IOrophenoI2,4,6- Tribtollllflhenal

J - Indicate' co-pound concentretion found below bDL.U _ lndlcat" I:ollpoundan"lyzed rar but not detected.

REQMRY .JJItm.. ..'JlBI.\§...-..!l. " }I)-114 .-.JL.---!l " 0-116 -!L-.-J! " }}-141 ~~ " 18- 9" .-IlL~ • 21-1110 -lL-.--l1• 1O-12J .JL..

B • Indicete. C~lpound round in a'sociated blank.W - Reault Ilxcae¢l specIfic ground Witer quality criterla.-

_ f1.gs are based on Specific Ground Weter ~alitl' Criteria rtollHell Jeney Register dated FebrVIry 1, 199'._".. '-/1Ittllylphenol"nd 4-nlthylphenoI can not be 5tpltlted by the .tllod apphed

866300045

TIERRA-B-004644

el1-1S-1'39b 04:S3P11 FROM'.'.- .

INTEGRATED At'!H-'r'TlCAL LAB TO

-i.,. ~.: re1:ed", ...

. , :Leba

- II

772'5898 P.05

In~egrated Analytical Labora~ories, Inc., I '

273 Fran~llnRoadI I

Randolph. N.J. 07869

ANALYTICAL DATA IlEPORTfor

Chemical Compt.l1Ulds roc.13-15RiYerAde ..be.Newuk, NJ 01111

Project NIIlIe: PVSC MONITORiNGLab CAse NtllDber : 10950 • 2.904I .

B6t. METHOD QmcnoNuM!J'

201 361-4252Fax: 201 989·5288

1 '~

< - LESS TifAN THE MRt

Lati !D.: ~l-~tm:ooi ,M:drix~aict :.Aqueous - p.J,1LPer~.ead.roimite: 100 ~

;

C~poUad

C2L1bJiledwleV'myl CIi10rideBlOiDomiMhaD..ChI~TricbJorofillOromctbanc

'l.l·bic&loroetllelleM'-yleGe Qloriclatrui·I.2~DichlOroetheD.1.1.bicl1loroedlaaeOalaroform1,I,i·Tnchl~!O~~oridel,:i.iJ~BeD2ZGe~Tric:Illuroecheao;1.2~~~

Cone. Q

< 10.0< 10.0

1< 10.0j

L < 10.0! < 10.0

< 10.0< 20.0< 10.0< 10.0

18.S< 10.0.c: 10.0< 10.0<: 10.0< 10.0·< 10.0

MDL10.010.010.010.010.010.020.010.010.010.010.010.010.0lO.O10.010.0

VOLATn.ESMcthodQ4

Compound

Bromodichloromethane2-OJoroechyi Vin~ Ether~s·I.3·DichloroprciptmeToluenertans-I,3-Dic:hJoropocpalll1,I,2'Tric:JllotOllchWT~oroeaheaeDibromocblorometh:aa.ChlorobenPIMEchyl~'rotal XyleacsBromotona .l.I,2.,1·T~blol'Olicbane1,3-Dic:bloro~1,4-Dic:bJoro~1,2-Dic:bJoro~

Date Sampled: 12126195Time Sampled: 15:00Date Aaalyud: 112196

•Cone. Q MDL

< 10.0 10.0< 10.0 10.0< 10.0 lO.O< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0

.< 10.0 lO.O< 10.0 10.0

. .• I lie:::=::=>AU HIDEP prOtOcol were followii:d dutin& analyses.~.' i: ~-

TOTAL CYANIDEMethod 335.1

MOL0.05

nace Samp*f: 12J2619STillie Sampl«f: 15:00Date Aaalyzed: 1J2J96

These data have beCn reviewed and ace:epted by:

t- q z,.

I ae. ,:UOO~~ko=

Tbe.fiability ot.IDtepW.Dcf Aa.I~ ~.1Dc. is limiWd to !he actual cost ofdwaaaJ)"IW performed.

TIERRA-B-004645

.~~~fi[·...b.

- IIl

.' ....•• "';"...... -''J .......-+I .•i

Integ,.ated Analytical Laboratories, Inc.273 Franklin RoadRandolph,N.J. 07869

201 3610.4252Fax: 201 989-5288

ANAL'YTIe.u,. DATA REPORT(oe

Chemical CompoundS. Inc.Z9-75 RiYnde Aft.NcwarIl:. NJ 01101

Project Name : PVSC • MONITORINGLab Case Number: 10950 • ~

MDL .. METHOp Dmcn9N UMIT < .. LESS THAN THE MOL

SEMIVOLATlLES - BASE NEUTRALSMetbod625

Coac. Q< 100< 100< 100< 100

· < 100:<.100· < 100

<·100<'tOO<100<UIO

: < 100·<100·< 100< 100

'< tOO.< 100,< 100!< 100'< 100;< 100'< 100i< 100i<: 100~JOO<100:< 100<IDOI

Dm3ampJed: 12126195Time Sampled : 15:00

--Date AD:IlyJ.ed : ]/11/96

MOL CompoW1d Cone:. Q MIlL

100 DielhylpblhalalC < 100 100100 Fluonlae < 100 100100 4.Ch.Ioropbeayf-phecylDChec < 100 100100 4·Nitroaailiu < 100 100100 N-Ni~pbcuylamino < 100 100100 l,2-Dipbenylhydrazinel Awbeaz.eae < 100 100100 4-Bromopheayl-pbenylethec < 100 100100 Heuda1ofobenane <100 100100 Pbaunttwca. < 100 100100 AIlthn.ceoe < 100 100100 Catbaz.ole < 100 100100 Di-o-bwylpbtba1a&e ' < 100 100100 FJuotUllhelNi < 100 100100 DeaUdiM < 100 100100 P7ftlOO < 100 100100 3,3 '.DilDlltbylbeGZidiM <100 100100 Buqlbeazyfpbm.lare < 100 100100 3,3' ·DichJorobea2:icf < 100 100100 Bauo{a]aDchncm8 < 100 100100 ChI')'MlMl <100 100100 biI(2-Edaylbexyf)phtfaalata < 100 100100 Di-IHCCylphtbabw : < 100 100100 Beazo{h ]fllIOrIIUbcati < 100 100100 Beuo(k)ftuonatbeGC < 100 100100 B.zam(.)~ < 100 100,100 1Ddcao{1,2.3~)pynrae <100 100100 Dibauf-..b1udaceDo < 100 100100 BeuoCI'.II,i)peryltao < 100 100

i ,

".:....." ... QuNt licit.I !, .

i:'i'

866300047. ::

TIERRA-B-004646

•. -e4.-L~-l996 P-.:I:c:;2Ft1

i~~~, .,' -VCic..

,",Lab.- II

FROI'I INTEGRATED At+L YT ICAt... LAB TO p.e:::

,Integrated Analytical Labora1;ories, Inc.273 Franklin RoadRendoJph.: N.J. 07869

I ; :.

201 361·4252Fax: 201 989-5288


CJaenW:al Compounds, Inc:.29-75 Riftnide A~e.Newvk, NJ 07101

Projec:t N'lImC : PVSC • MONITORINGLab Cue Number: 10950.2903

Li "

Ub m : 29OS-oIC1ieat m !001Mab'ixlUdiC. i!~ -IGIIL~ Mbiatair. 100

iCompoad

!,Lad :;%iDc

, Resutt Q

< 100, < 100'< 100< 100< 100

/<'1~' -)"'-~, ..,_...-

< UIO,< 100< 100'< 100;< '00,< 100'< 100kloo

, ,

Result Q< 0.04fo.zz

~OLAT~-AC~Methodm

0* Sampled: 12126195TUDeSampl«l : 15:00Oat. AaaZyzed: 1/11196

It-

MDL100100100100100100

1000100 :100100100100100100100

METALSEPA Series 200

O*SUDpIed: ' 12/26I9STim. SaazpJed : 15:00Daf6 ADalyzecl : 1111/96

MDL0.04 '

.1

0.01. ' ..:.... :" .

=: Q- Qual-~. ~

- i,

866300048tf_ Yodl: CRtUiocILab I 11<WZ

TIERRA-B-004647

.. -'.

FROM INTEGR,CorED · • YTII'·-~ I "8 rlJ• . Ot "":S- L996 04: S3PM ~ ........ ......

.~;".~ I~~r~ Analytical Laboratories, Inc•. Labs 2n1 FMJ~kJinRoad 201 36'~4252

Ril~dorp~;N.J. 07669 F~x:201 989-528aI I '. 'j:

772S8'38 P.04

'-ANAL \'TICAL DATA REPORT

forChemical ComPounds, lac.

%9.15 R1v4Qide Aye.Newark, NJ 07101

Project Name ; PVSC • MONITORINGLab Case Number: 10950 -19OJ'

MOL .. METHOD DEfECTION LIMIT < ;.,kES§...THA~ THE MOL! i I

!Lab 10 ; 29Ci3~ 1

I .'

O .. ~:OOI iMatrixJVDiIl. : Aqueous - IDIIL ;Perceot ~oi.ture: 100 '

GENERAL ANALYTICALO.Ce SampJed :

Time SIIDIp!ecf :12126i9515:00

I. Compound (Method)I '

MDL Date AnaJ):ud

; . tJiocbeai~ 'Ehy~ Daaaad (.w:s.l) i 18&10",. I i.

- -~ S~ Solids (160.2) I i < 10.0NA10.0

112196113/96

. Q - ~fiotr

: - : I

All NJOEP:ProtDcol were rolJPwed ~uring anaJyses. These data have been reviewed 3I1d accepted by:. i

'.

. .,' ' .. ;~ .~ ..-

II

11

TIERRA-B-004648

SURROGAIE CcpouNOS1,2-0iehloroetnane-d4To luene-d1SBrQlllllfluor~-

J • Incllc.tea cOllPOund concentration found belOll ImL.U • Indicae .. campou1danal~ed for but not .ucted.

RECOYEBT ...IJ.I!l!t. ~--In X 76-114 ~-..ll!1 t; 111-110 ......2L---!n " 86-115 -RL-

a • Inclicaus c~ found in associated blank.V • Result exceeds specific ground W8ter qualIty criteria.*

* Flags are based on Specific Ground vater Quality criteria ffllll New Jersey Register dated Februllry 1, ~993.

-866300050

TIERRA-B-004649

"I..:Cl:,.€C1 TEJ LAC'Cr"AiClHE:i. ltf..:.&fA iJRJ;r.HIC r.NALYSiS DATA

CCI

MATRIXOIWflCN F~TrR __ -!... _

DATE EXTRACTEDl}A l'E ANALYZED~YZED BY

- C~..:E tU'l8ER.'i.;rnu IU1l!l:"R

lATA FILECL ISl.lT tIAI"':EF:aO ID

UGil I'IlL............ _ ~•......•.•• ~~...••.•••....•••••........c~••~~••.c ••••••• a••••••••w •• a=-=•••-=••• &•••••aa•••o•••s .............................c••••••••••••••••&z•••~~•••w.lall9o:.2 Phenol U ,U 9»9';4 2~~~5-'rlchiorophenal U ~~Q

'i~';i'9 2-ll11orophenol U ,0 S1211, 2,4-0lnitrophenol U m'·~48l 2-rollthylphenoi U ~O mlrll 4-lh t I'ophenoJ IJ 25Ui~::J}911 J&4-nethy lphenoI u .;U »J4~11 4,6-Qlnllro-2-~th~lphenol ;J 2~IJ

3~~5 2-"1 ll'o~henoI 6ilG ,q 37867 Pentachlorophenol :J 2!;-~)

tU",6lo 2.,4-iJllIlefhylphenol 1J ~lj 121142 2,4-01nittotoluene :J ~!)

: 'lt1aJ 2 2,~lchlotophenal U t;u !3466~ Olelhylphthalate ~:...;; ~:i.:04 hi~(-2-Chlor~ethyllcther ~ ,u JlJu':i7'D ,1,-J';' i~rQ~hen~:f "~hl!'~~)i.~~~a:~ ., ~I.:,

~-l}~l 1.3-Ulchlor~en.~~e Sij BA :~: Fll.io.~"e '.,j ,..... , :~~~Otcr.~G~~b~n:!n~ " ~i) lU\Wl& 4-111' ro!n! IIr.e ., 'l~ij

... ;~4ooIj/ ,j ./

::;'!~:r; :enl;11 ~lc~/lOi u ~U a~.Hj6 N-.', ~:"'l]5~C:p~.!"!y1e::11"!

"~::j~ 1!2-0ich!cr~ben:ene •,j:\..".: ~::tS':3 ~:::~~~~~~~.~~~~:n;.l~~~~p

0, ..;.~....~~Co·.i: J ~s", ....~~.~r~ (':'~~":,}:J:.:J :.; i ~.~~

~ ~~~'j ~u .. , ~_·~i-O- ~:" ... _L. ... , ·:-~'tt r:;~·;;-·;!-'1";::~,~;:.-~1!!i!-!'

-;. ':':t:~ ;,)~~~~r':t;'!"l!~e " .~JJ

~ . _. ~,!v~(r; ~.~:a~t~h~r-? jj ~'i 1~:;12? ':";:hracene "::'

.I~.~~j HI ~.~l:enzetle :.J O:'J 3"742 Ol-n-aut~i~htha'~t~ " ...':j

.:~~~1. 1.;o~Ml'onll ~tl 2U6~:) Fluilran::;ene " .:..hi':J e~n:~lc :;CI" " 2':0 ~:':91Jl:U P<;rene J "'oj

•• U ",::}'ll ~15(-2-Chioroelhot~Ir,~[hene U ~a a,6i!7 ~tvlbenL~io~t~a.~·~ ; '.J

" ;~J~-C.cn:~~~b~·::~:r~,:,:u2~1 1.2~4-frlch:Ot~Cen:enll ~ "U 91:'':'1 OJ ........... 1)

.. "'01:: f(a~hthalere ~J 7i) :"':'':'J e~n:~(a;~ihr~(er.e ... jJ.~..,#

.,;~ .:.;':l ~':,iQrOcnl: 11'11 ~ ~~ ·~~t"'l '3i 1{1-"t~~:,;1!,,-=:-:~1!.:V~ t ...~;.,: '"~ ., ;'J" •• ' '~J..' ~

.jJ"~cJ ~xacn.ul'o~ul~oiane lJ $0 21SUl'l Chl'y~ene iJ ~!J

':~.'~ ~4tethylna~hthaltne U ~;j llill4U j)1- ...~ctyl phlhalat~ ;j ·,· ,';~':').i ~x~c~;~t~cyc!opentaalene 'J 7lJ 2\1,';~2, BenIolb!ftuoranthene ~'j. ° •

~l,ij) <:.I}ojlor"naohthaiene lJ ~O 2il7OS9 Den1n(~)FiUDr~ntnene :J ,,;!

~1l7U 2-~1 \roanJ11ne !J 2~;} ,ljJ28 eenZll(aiPytene iJ :.. ~."t; IllJ U\!llt:h~l:'.l!lthaiale J ~tl 1m,:" Inceno\ 1.4: .J-·:d;Jo',;rene " ...~1

'J

~'oll;':'6i:1 Clcenailhth,lene J :;u ~77U3 UlbenZo{~,hj~tnr~t!re j ... :;

·..;·...u1J2 '-I'lltrail"\ill'e :j i!~t) "'U,,·I.I.·I Een:oI9,h,ilPerylene !J ~il"".1."-,,~3}19 Pleeneontl1ene IJ ,0 61~9 ,~~ltro30dl.eihylaD,ne oj

~~ _I·.

1.::!~"'J OHle!l'Zoful'iln :J IJO 2JlJ29 2!~Olnltroc~lorODentene ij '!~LjO

I;U6~IJ:l ~,6-0Inltr"toluene .U 50 229715 2,5-0Inltro~henol U Z:"JU'7':'~;lJ "-~niol'O-J-.ethyipl1enol U ~O a~lI1Jl 2!4,o-Trinltrapnenoi [1 '!~r;u..• .J ... -, 2!~.a-;richlor~phenol :J ~U'.·/0.1.

:.tii?&liB;;; '';:':it'',j.~l(!$

~IIt robe..zelle-l,l~,-rIUOI'r.Dlphenyl~erpllllnyl~l.iP!IenoI~S2';: IllOrophetlOl2~.,6-rrlbrolGJlhenol

_ !nclcalea cCIIlpOlunciconcentntlon #ound Ilel~w :1lt..~ ; _ Inalcates COIII!!0una analyzed Fot but not detected •

~;Uj!Jtlf!

-22'--2!l. ,~ll--!!X--l1. ~~" 1a-t2J -l!-B • Indlciltesco.pound found In aS30lclated blank,

W - ~esult exceedS ,paciFIC ground water qualIty crlterll.·

~J!.>-l:~'.'-116))-141lit- 9421-llJO

• flag' Itll based on specIfIC GtO~ Watel' QuaILty Criteria fl'o.Hew Jersey Reglltar dated February 1, 19YJ.u J-,"lell1ylphetlol and 4'"l'1elhylpl1enol can not be separated by the .thod applied

866300051

TIERRA-B-004650

CORROSION MANAGEMENT, Inc.

Certified for: NJ, PAt DE, cr, NY (DOHINJ #14116 NY #11376OS EPA CLP Lab

ANAL'YT:tCM. DATA REPORT PACKAGE

CHEMICAL COMPOUNDS, mc.Waste waterCUStomer

m: MATR:IXLAB

NUMBER

DATE '"TD'IIi:

COLLECTED

ATLABDATE

.Aqueous 220698 ,09/21/95 08:30 ,09/22/95

supervisor/Manager Signature:

QuU~~~Richard S. Le.Ji1le

1995.reserved.

Page # 2

0" 866300052

TIERRA-B-004651

.~.-".' .:.,.'

INDUSTRIAL CORROSION MANAGEMENT,1152 Route 10Randolph, NJ 01869201-584'-0330OCTOBER 4. 1995

INC.

Certified for: OJ, PA, DE, CT. NY'(DOH)NJ #14116 NY #11376US EPA CLP Lab-- PRIORITY POLLUTANT ACm FRACTION ANALYS:IS BY GC/MS

~ .iumtler:Client:Sample soUX'ce:sample ID:Sample date:Sampled by:At lab date:Matrix:

220698CHEM:tCAL COMPOUNDS, INC.Waste waterNPD ML'.09/21/95 Extracted Date:CUstomer Analysis Date:09/22/95WATER

Data File: >I7063

09/26/9509/26/95 Column: 30m SPB-5

Dilution Factor: 10Init Sample vol..,SOm! Final volume- 10m!

Cone. in sample _ «Cone. on Quant Report/Initial Volume)*Final Volume) *1000

ParameterResultug/l

MethodBlankug/l


2-ChlorophenoL2-Nitrophenol?henol2.4-Dimethylphenol2.4-Dichlorophenol2.4,6-Trich!orophencl?entachlcrophenol~.4-Dinitrophenol•.6-0initro-2-methylphenoL.-Nitrophenol'-Chloro~3-methylphenol

UUUUUUUUU[]

U

•

UUUITUUUUUUU

200200360200200200200no200200200

ug/l • micrograms/liter or ppbJ: Indicates a compound was analyzed for but not detected at the MOL.J: Indicates an estimated value. It is utilized when a reported value

meets the identification criteria but the result is less than thespecified detection limit but greater than zero.

B: Indicates that the analyte was found in the blank as well as thesample. :It indicates possible/probable blank contamination.

NO: Not Determined.IND: Indeterminable

Copyright IeM, Inc., 1995.~ r~r •••rved.

-"10

.~~ (... _ .. S.4 ..,......i ,.. £ ... ~ .• ,s64C ~....S.t$5j t ..iis ..J5S$$w ..;":G ...JH. . _.,::' .. A_

866300053

TIERRA-B-004652

" II INDUSTRIAL CORROSION MANAGEMENT, me.

I ~~S2 Route 1.0Ranc;lolph,NJ 07869 certified for: NJ, PA, DE, CT, NY (DOH)

I20~-S84-0330 NJ #1.4116 NY #~1.376OC'IOBER 4, 1.995 US SPA CLP Lab

I - PRIORITY POLLUTANT BASE/NEUTRAL ANALYSIS BY GC/MS

I Lab NUmber: 220698Client: CHEMICAL COMPOUNDS, me.

'

Sample source: Waste waterSamp~e ID: NPD Mt..' s"I Sample date: 09/2.J./95" Sampled by: CustomerAt lab date: 09/22/95I ~atrix: WATER

II'.ar_to<IN-NitrosodimethYlaminebis(2-Chloroethyl)e~erI ~.3-Dichlorobenzene

1.,4-Dichlorobenzene

11,2-Dichlorobenzene..bis(2-ChloroisopropylletherN_Nitroso-di~n-propylamine

•

HexaChlOrOethan8NitrobenzeneIsophorone .- --bis(2-chloroetboxy)methane

t' 1,2,4-TriehlorobenzeneNaphtba~enerexaChlorobutadiene~ch1orocyelopentad1ene

_ .u:oronaphthaleneI lJJ.metbylphthalate

Acenal?htbylene12,6-D~itrotoluene• Acenapbthene

, l-2,4-Dinitrotoluenet Diethyl phthalate

'

4 -Chlorophenyl phenyl etherFluorene.N-NitroBodiphenylamine1,2-Diphenylhydraz1ne (Azobenzenel

.4-Bromophenyl phenyl ether -Hexaehlorobenzene .phenanthrene

I AnthraceneDi-n~butylphthalate

'

F1UOrantheneBenzidine_PyreneButyl benzylphthalate3,3'-Dichlorobenzidine

'

BenZO(&)anthraceneChrysene.-bis (2-Ethrlhexyllpb.t:balateDi-n-oety phthalate

_Benzo (blfluoranthene

.~I ug/l - micrograalS/liter or ppb111ft U: Indicates a compound was analyzed for but not detected at the MOL •

._~ J: Indicates an e8ti~ted value. It is utilized when a reported value

Imeets the identification criteria but the result.is le8s thlm the

_ speci£ied detee:tion limit but ~eater than zero.

:

. ... B: Indicates that the analyte wall found in the blank .s well as thesample. It indicates possible/probable blank contamination.

. NJ): Not Determined.

,: - COpyr:~ ::t::-:::5• • ~1All rigb.tsreserved •.

i- ~

Extracted Date:Analysis Date:

09/26/9509/26/95

mit Sample vol- SOm!

Data File, ;>17063

Column: 30m SPB-5Dilution Factor: 1.0

Cone. in Sample .. ((Cone. on Quant Report/Initial Volume) ·Final Volume) *1000Final volume- 10ml

Result:.ug/lMethodBlankug/l

uUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU

uuuuuuUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU


LL

200200480460480240360580200200200460400200300400920300200380200460400340200200380380180160500120200100240200100100600200140

866300054

TIERRA-B-004653

INDUSTRIAL CORROSION MANAGEMENT,~~52 Route 10Randolph, NJ 0786920~-584~0330OCTOBER 4, l.9 95

INC.

Icertified for: NJ, PA, DE, CT, NY (DOB)NJ #14116 NY #11376US EPA CLP Lab

.-IIPRIORITY POLLUTANT BASE/NEUTRAL ANALYSIS BY GC/MS

(Continued)Additional Base/Neutral Targeted Compounds

ILab Nuraber;Client:Sample source;Sample m:Sample date:Sampled by:At lal:ldate:Matrix:

220698CHEMICAL COMPOUNDS, me.Waste waterNPD. MU's09/21/95 Extracted Date:Customer Analysis Date;09/22/95WATER

. Data File: >I7063

09/26/9509/26/95 Column: 30m SPB-5Dilution Factor: 10

I Init Sample vols 50ml Final volume- LOmlCone. in sample. ((Cone. on Quant Report/Initial Volume) '"'FinalVolume) "'1000

I Resultug/l

MethodBlankug/l

MinimumDetectionLimitug/lIparameter

Benzo(klfluoranthene-. : Benzo{alpyrene

IIndenO(1,2,3~Cd)pyreneoibenz (a,hlanthraceneBenzo(g,h,i)perylene

UUUUU

uuUUU

140~oo220100100.'

--ug/l • microg~ams/liter or pphU; Indicates a compound was analyzed for but not detected at the MOL.J: Indicates an estimated value. It is utilized when a reported value

meets the identification criteria hut the result is less than thespecified detection limit hut greater than zero.

~ B; Indicates that the analyte was found in the blank as well as thesample. It indicates possible/prohable blank contamination.

ND: Not Determined.!NO: Indeterminable

~opyright ICM. Inc., L995.All rights reserved.

I. -.-fI'

~I

11-n···:.......

86630005512

TIERRA-B-004654

. -. .- ," .. ~ ... -.'." ...... '.~

12/13/1995 22:24 2617725898

tnt_gretH Ana'ycice' Laboretorie8. Inc.273 Frwnklin RoadRandolph. N.J. 07869

ANALTIlCAL DATA REPORTlor

a-dcaI~r-.19-1SRl ...... A....~NJ 17111

~ N.-r. INTEllNAL MONtl'OmNGLU Cue NUIUbw: 10H0· Z6'O

201 361-42:52FaIL:201 989-5288

Pa.GE \')1

..

MOL - METHOD PETECTION UM'T

IA ID: 2640-01-cu-&ID: 001"'''rialUnill: ~ - ",IL~ Moitturo: 100

CoaapauH

~Via,l ddaridlIB...........~Tri~lDIlCII-.e1.I-D~MedlJI .. dIIoricII1nU-1~·Dic:JlIoroIdIeM1.1-D~QIorofonDJ,I. J.TticIlJoroIdIIMe.m..~1.1·Dk:bJ~~T~I.Z-DidLluropcos-

COlI(.

<50<50<50<50<50<50< 100<50<50<50<~<50<SO<50<50<50

MOLe ........50 Bromodidllorolillld...50 1-ChlorooMbJlYiaJI ....50 cla-I,3·0iCbJoropras-e'0 TollItIIC50 1nM-1.3.Diddcllupa .......50 l.l.1·T~IOOT~50 DlbrolDOCblol'OlDll"b'M:SO Odorot.a- iC50 EIl)'I'--so X71a1a. Cotal50 Bt'llGIOb1:a50 l,l.2,2-T~50 1.3-D~50 1.~DicbIorobaaMIe50 l.2-DidlIoi ....

< - 1d!SSTHAN WE MOL

DUe SaapW: 11/17/95"n_s.mpw: 11:30Ow AaaJ7J*l: 11121195

c.e.<50< 50<50<50<,.,<50<50<502110<so

-49100<50<50<so<50161

MDL

50so,.,5050so5050'050

ZOOO50505050

"so

YELLow--

., ".#::~.. ?tJI;E-

866300056

TIERRA-B-004655

12/13/1995 22:24 2017725898 ENVlRO CC1'" INC PAGE Ul

Incegrllted Analytica' Laboratoria, Inc.273 Fntnldin RoedR.~Dlph. N.J. 07869

201 3B1-~2Fax; 201 989·5288

ANAL YTlCAL D"TA REI'OaT-~eo-""IM. •Do1! JU..... ,,"-Hewn. NJ mi.

rr.;eea N..-: INTERNAL MONITOlUNGLIIhc...N"'-': 10J5l·Z64I

MOL- MHT < - 5S A

SDUVOLATILES (aN")

lab JD: 2640-01- D*SaIapW: 11117195Ci_ID: 001 r_s.mpw: 11:JO

MMtWUaita: ~-IIIIL 0_ ADal)'DII : 11/21'"

PwcaMoi ..... : 100

C_peuIIli e-. MDLCClID~ eo.c. MDLI

]-N~ < 100 100 CariJuoW < 100 100

A_pbdMot < 100 100 Di-a-htylphlbalallt < 100 100

2.4-Diai~ < 100 100 Pluorudleae <100 100

4-Nib'Cpllllol < 100 100 Beuid .... < 100 100

2.4-DwUOlolucae < 100 tOO Pt- < 100 IW

DibauofunD < 100 100 ].]' -DillllCbylbluidi ... <100 100

DicthyJpblbllale < 100 100 ButyI"-'zylphlbaliM <100 100

FlllGRllO < 100 100 3,3'·Dic:blorobczidia. < 100 100

~,1""',,,,, < 100 100 Beazo(IJutbr- < 100 100

4-N~ < 100 l00~ < 100 100

...6.Dioiho-Z--ebyIJlb-li < 100 100 bit(2-EtbyUluyl)pbtIaWIc <100 100

N-Niwmdlp.,,-a. < 100 100 Di-ao«C)'lphlllll* < tOO tOO

1.2-DiP-y.ydnziD.r"IlOb-- < 100 100 s.m(b)ft- p' <100 tOO

4-BIO&IIOPbca,l-pbaa)'Jc6or < 100 100 Beuolk)nllOl1allbeae < 100 100

H~ < 100 100 BeuoI'IP~ < 100 100

~ < 100 100 bid-(1.2,3<d)prr- <100 100

~ < 100 100 D1"baaz(I.b]lllldu- <100 100

~ < 100 100 Bcuo{J.Il.iJpwy- < 100 100

yellow #.~ " f'U~E 'I

-

-866300057

TIERRA-B-004656

12/13/1~~5 22:24 2617725899 ENVIRO CCJttP IHe

Incegr8ted Analytical Lsbaretar' •• Inc.273 Franklin Roed~.ndolph. N.J. 07989

MOb- MffilOP 0W£P911 LIMIT

lAb m: 2640-01-eu.tID: 001MMtWUaiaa: A... - "IlL"""t MoilCUlr. 100Ca.pouRoIIN-NitIoeodilOCdly~~AIliJiae\li1(2~>ed-2..Q1oropbeDa11,3·Dida.lorobea-1,4-~JMazyt alcoholl,2-Dtd&IorobaI-2-Mdb)'lJlbeaa'bM(1-chJoroUopcopyI)eCblr4-MedlylpiMeo&N-N~1"P'GP)''''2-AmiDoCoI- +...~-HaecIalo~N~~2-N~2,4-0u..byl~

ANALYTlCAL D.TA REPORT..CII8DiaI~'"

D-75.h ........N.wvIt. Nl mlt

ProjKt NuDe; INTEIlNAL MONlTOJUNGlAbc..N-w: I,", -:z.-

201 361-4252Fu:: 201 989·!528B

PAGE 69

c...< 100< 100< 100< 100

496< 100< 100< 100< 100< 100< 100< 100< 100< 100< 100m

< 1003310<100

MDL ClXIIpouN100 bil(2.Qforoccholy)DICIbaDe100 IIcaziIriG aid100 2,4-Dimecby1aaiUM100 1.4-D~100 1.2.4- TricbJorobcGliello100 N.cIlaIe..-lOO~100 HcudIlorubu~lDO 4-OIarv-3.-d1y",,-1100 2.M.. yID.......100 Hellchlofocydopenculieac100 2.4,6-Tricbb,-,100 2... '-TridlluiupMDol100 2-c:b101oD'~'''''''100 2-Nicn:.ai1....100 DiJacdaylpbtb,J"r100 2.6-D~-100 A-rblJay'-100

< - [ESS DlAN $ji fdD[Due SeaIpW: 11117195TUDESuaPaI: 11:30o.a ADaIr": l1/211W

c...<100<500< 100< 100< 100< 100< 100<100<1110<100< 100< LOO<100<1005$10<100< 100< 100

MDL

100!GOSDO1001001001001001001001001001001001001001001110

CGotiD'''' 0II..u .....

-

If "-pole

coIt)ooo~CDco

...-

TIERRA-B-004657

.. ',', .-.. "

2iU 772'58'3812/13/1'395 22:24El'NlRO CO'oF INC PAGE 62

Integrsced Analytical I.8borlltori_, Inc.201 361-4252

Fax: 201 989-5288273 Ff'8nklin RaedRandolph, N.J. 07869

LM JD : 1639-001_0-.10:001MmU/U": A...-- -".tL,...~100

Csql III

Qaloca "V'.. )'I~Bwuo ~O.&uo m-T~I.l~

" ~QIariden.-1.2~1.1~CIIotDIana1.1.1-TridllunlldUDc.-T~

1\ :f1.2~-tV a--

TlicYoaCIIl.1.1-Did11uoupr i

~ALYT1CAL DATA REPORT-OF I '<=- -*...,,' u." A-~NJ071.1

P'nJG H-= rvsc MONITOIUNGI..M c..N ...... : 1_-%6Jf

< • WS WAN i'iiiPm:VOLATILESMetboclG'

0 ... s-pIed: 11117'"TiIllD SuapI4ld: 11:30D.. ADUl'_: 11121195

ea-. Q MOL Qn~ ~ Coac. Q MDL

<50 50 Bron1Qdlchloromemanc < 50 .so<50 50 2~yl V'lAyt EdMr <so 50

<50 50 cie-l.3·Dicbloiapupa» <50 SO

<50 50 To1_ <so SO

<so SO cnu.-1,,)-DicJI1ocoptopeae <SO SO

<~ 50 l.l,2·T~''''- <50 50

< ICIO 100 T~ <SO 50<so SO Oilll'omadalOCOiiiCCllme <so 50

<so SO Cal~ <50 50

53.1 ...~ SO Ethyla-- <50 50<50 \\\ SO r.. x,.a- 160 50

<50 50 B,_b. <SO 50

7'ZOO- 200 l.l.2.Z-T~ <SO 50

<SO SO l.J-Did!IoiubcaZcDO <50 50<SO 50 1....D~ <SO 50

<50 50 1,1·~ <so SO

• Results from dUuled ample andylb.

~ II' ;2639-001a-m:GOlMIIriVU- :A....-. ,..a....... W ....... IOO

0- SuapW: 11/17'"TIme SuupW: 11:30DMa A.l)"J*l: 11111.195

MOL

< o.G$ Q.O:S

- LabonIoryD

n.1iIbillt)' of~ AIIIIydI:II ~. JD;. la I1alfttd to IIIIId1III COIlof .... ,.. PA~-'

----.~:...,,-- ....

TIERRA-B-004658

12/13/1~95 22:24..

26177258S8 PAGE a5

l~egr8ted Analyticall.8barlltori •• Inc.

- 273 Frwnldin RomRendolph. N.J. O'18S9

ANAL l'TICAL DATA aEI'ORTIbr

o-ical <:anvow ...1f..7! Aft.~NJI71.1

PraJst H_ :rvsc. MONIrOJUNCLaII Cue N..... :1_·XJI

MBL - ""wo'6 DaCftaS uMITSfMlVOL4tlli -xam: < - lEU WAN WE DL

MedIodm1.IIb m : 11531-001 o...s.npw: 11/17/95cu.am: 001 T_SempW: 11:30w.arixlUllica : A.- .J&aJL 0... Aa.I)'1IId : 111111?S,.... McMaaw: 100-

C-. .... ... Q MOL.... < 100 1001-0" ,, ej < 100 100 .•2-w.rby ..... < 100 1004-Medaylpb .; <100 1002,Ni.... .,. ej < 100 1001.4-nu.cla)'~ < 100 100~ ... <.tOO 5DOz.~ < 100 1004-Qbv.3....a.yIJ'I-aC < 100 u».- l,4.6-T~ < 100 100..4-'. Tril:IIlon ,t 01 < 100 100:z,~ < Joo 1004-H1 ... :,.~ < 100 1004,6-Di8ifIo.~"'" < 100 Joo~ < 100 100

METALSEPAs.n.211

Ub JI) : 2611:001 o-s-pw: 1l/1719SCimlm:OOI T',-~: 11:30.....wu.... : ""P- -maIL Dele MIl": 1l1Z2J9!r..:-t ..~ 100

C_.a... ... Q MOLI...ld 0.1$ O.eMZi-= 0.9 OralQ - Qaalifier

All _ ........ __ .. ,....... durin&_ .... These d... b... ~~

Midaalt II, lcftill. 0,. l.Iboraory D

oCDooo

i-

".

TIERRA-B-004659

12/13/1~95 22:24 2017125898 ENVIRO CO"IP INC PAGE 04

Integrated AnalyticalLebarstariu. Inc.273 Fr'entJjn Roeds:l."daiph. N.J. 07869

ANALYTICAL DATA Jl.EPO)n'"fDr

o-ka' Compowck, -.D-1JIU.........Ncwutt. NJ mi.

PraJ-:t H... : pvsc. MOHD'OIUHG.....c..N ..... :ll1t51·2OI

Ub m : 2631-001c::u-a m : 001M.uWUaira : ~- ,..Jt.PvclIIIt MoMIln: 100

eo-pauDlIN-NiUO"'di"""4byluDiDtADiliDebiI(%~yl)aCbor~.1~J.~8eaJ:)1 U:oIIolI,%~lMGl-dlJoroiloproprl)cdlcrN-NitrellllMti~"'"~N1I&afJ 11M""

.........-1Ia(%~)''''''''1.z. T~N ....~~2-M_r'-apb'MJe-H~

... 2.Q1on1D11p1a .........2-N~Dia.Ctly1~1.6-DlAiUotol-M-pbdl'"3-NiaGMiIiMAclMIIi' .....z.~on-.orur-

201 361-4252Fex~201 989-S2BS

SDUVOUTlLE$ - BASE NEDTlLUSM.modQ!

DIIiI SuIIpIed : 11I1719ST.-...... : 11:30.o...MIoIy..t: 11121195

CQIIC" Q MDL CllIDfIOU'HI CON:. Q MOL

< 100 100 D..... yI~LL

< 100 tOO

< 100 100 PllIOtMI < 100 100

*47SlO .(GO 4-CaJ0r0pbMyl""rlMbw < 100 100

<100 . 100 4-Nill'aallillM < 100 100

< 100 100 N-NiUwodiph-,.Waiao < 100 100

< 100 100 1.2-Dil'h-rlll.ydru:iDelAzioben1cM " 100 100

<100 100 ~1-pblarldbV < 100 100

< 100 100 H~ < 100 100

< 100 100 ~ < 100 100

<100 100 ~ < 100 100

<100 100 c..-.. < 100 100

< 100 100 Dk4lllt)ipildlal* < 100 100

< 109 100 FhlClflDCla_ < 100 100

< 100 100 Bcu;jdi •. < 100 100

< 100 100 ~ < 100 100

< 100 100 3.3'-DimdIa)'ilJallidiar < 100 100

< 100 100 Butylbeal)'lplltUWa " 100 100

< 100 100 3.3·-DicIaI~d- < 100 tOO< 100 100 a-m(aJutbr- < 100 100

< 100 JOO Qry.- < 100 100

< 100 100 bi.I(%·Edl)'IJMIIIrl),.. ........ 107 100

< 100 100 Di+GCtylp'+·'- < 100 100

< 100 100 Ieuo(b lnllCll'lllGMae < 100 100

< 100 100 BeuD(tl~ < 100 100

< 100 100 a-m(a]pynM < 100 100

< 100 100 lad-(1.2.3~ < 100 100

< 100 100 DibMz( .... ~ .< 100 100

< 100 100 Beozo(a,h.1l1*>'1- < 100 100

Q-q.li-.. ~ a..uk r.-diJuN4 ~7"ia.

Coer! ..... - .....

--

TIERRA-B-004660

;. .-:-.:; -;':. --.:::~-"" -. -' . '-'-.

866300062Integra1:ed Analytical Laborat:ories, Inc.273 Frankl"lIl RoadRandolph. N.J. 07868

"ANALYflCAL DATA. REPORT"for

ClHmica1 Cumpouads IDe.29-75 Rivenide AYe..Newark.NI mOl

Project Name: SELF-MONITORINGLab Case Number: l09SO-1719

201 361-4252-Fax: 201 989-5288

MpL _ METIIOD pETECTION LIMIT< .. LESS WAN TIlE MOL

Date Sampled: 819195rUDe Sampled: 11:00Date AnalyZllld: kJ15195

* Cone. MOL< 100 100< 100 100< 100 100<100 100< 100 100< 100 100< 100 100< 100 100<100 100< 100 100< 100 100< 100 100< 100 100.c: 100 100< 100 100< 100 100

-

Lab m: 1719-06i.Clieo1 ID: 002MalrixIUaits: Aqueous - "gIL

CGmpouad

CllorometbaDeVinyl chlorideBromomedwleChloroethaaaTridJlorofluorometbaao

- 1,l-DichloroetbeDoMethyleoe chloride1raDS-I,:Z-Dic:hJoroetheoel,l-DichloroetbmoClloroform1,I,I-TrichloroetbmeCaIboa. tetneh10ridel,2-DichloroethaaeBcmJ:DoTrich1oroetheae1,2-DicbloropropIBe

< 100< 100<100< 100< 100< 100<200< 100< 100< 100< 100<100< 100<100< 100< 100

Cone:.

VOLATILES

MOL Compound

100 Bromodichloromctbaae100 2-eb1oroetbylviuyl ether100 cis-l,3-Dichloropropeae100 Tolueao100 traDs-I,3-DiclJloropropqB100 1.1,2- TrichJoroetbaDe200 TetrachJoroetheoo100 DibromochJorometbaae100 CIJorobeazaao100 Ethylbeomao100 Xyleaes, lata!100 Bromoform100 1,1,2,2- Tetraehloroetbaao100 1,3-Dichlorobeuzeue100 1,4-DichlorobeuzaHl100 1,2-DichlorobeazeGe

TENTATIVELY IDENTIFIED COMPOUNDS

lAb m: 1719..()(J2.Clieat ID: oo:zMatrix/Uaits: Aqueous - "'&fL

COMPOUNDESTIMATED

CONCENTRATION

146000_ ..=,; .~-=-- _._ ....- -...

Datil Sampled: 119195Tune Sampled: 11:00Datil Analyzed: 8/15195

RETENTIONTIME

5.82.

.-New York Cordfied Lab , 1140Z.

TIERRA-B-004661

866300063Int:egrat:ed Analyt:ical Laboratories. Inc.273 Franklin RoadRandQlph, N.J. 07868

201 361-4252Fax: 201 888-5288

""DNHA- .::#-/3"ANAL YI1CAL DATA REPORT"for

Cbemica1 Compounds IDe.2!I-1S Riverside Ave..Newark, NJ 01101

Project NIUIle: SELF-MONITORINGLab Case Nwnber: 10'SO - 1m

MDL - MEWOD DETECTION LIMIT

Lab ID: 1719-002Clieat ID: 002MatrixlUnits: Aqueous - PIlL

COIDpouod

N-NitrosodimethylamiDePheaolAniliDebis(2-Chloroethyl)etber2<blorophenol

•• 1,!-Dichlorobc:azlDo1.4-DichlorobeazmeBem.yl alcoholl,2-Dichlorobeazeue2-Metbylpbeoolbis(2~oroisopropyl)otbec4-MethytpheDolN-Nitroso-di-a-propylamiDo2-AminotollJellO +4-AmiDotolueuHeuchJoroethaDoNitrobeozeDeIsopborona2-Nitropheool2.4-Dimcthylpbaaol

Cone.

< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0

BASE NEUTRALS ACIDS

MDL Compound

160.0 bis(2.Chtoroethoxy}meUllUlll160.0 Benzoic acid160.0 2.4-Dimelhylaoilioe160.02,4-DichJol'Opbeaol160.0 l,2,4-Tricblorolxmzeae160.0 Naphtbaleae160.04-Cbloroanilinc160.0 HexachJOl'Obutadieall160.0 4-ChIoro-3-methylpheaol160.0 2-Metbyluapblba1eall160.0 HexachiorocycJopeawlieae160.02.4,6-Trichloropheaol160.0 2.4.S-TrichloropheDol160.0 2-ch1ol'Ollaphtbaleao160.0 2-NitroaniliAe160.0 Dimethylpbtbalato160.0 2.6..JJiniuocoluene160.0 Aceoapbthyteae160.0

< - LESS THAN THE MOL

Date Sampled: 8/9195

.,

lllDC Sampled :Dale Analyzed :

Cone.

< 160.0< 800.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0~ 160.0< 160.0< 160.0< 160.0< 160.0

11:00"siISI9S

MDL

160.0800.0160.0160.0160.0160.0160.0160.0160.0160.0

'-160.0160.0160.0ltiO.O160.0160.0160.0160.0'

CoaciDued on next pap.

-

TIERRA-B-004662

:".. , .,.:.~.:' .'. .:..:.:. .~ .. ;. . ,';'.::'-.

866300064Integrated Analytical Laboramries, Inc.

~

.n~

_ P Labs 273 Franklin RoadRandolph. N.J. 07869

. .,.

201 361..4252Fax: 201 888·5288

'ANALYl'ICAL DATA REPORT'foe

Cbemic:al Compounds IDe.2,g..7S RiTerside .be.Newuk, NJ 117101

Project Name: SELF-MONITORINGLab Case Number. 10950· 1719

MDL - METHOD RETECTION LIMITBASE NEUTRALS ACIDS

< - LESS THAN WE MpL

-

Lab ID: 1719-002Clicm ID: 002MatrixlUaits: Aqueous - ~

Compound3-NitroaDiliaoACCDaphthoao2.4-DiDitrophcnol4-Nitropbeool2,4-DiDitrotolueae

•• Dibcn7.0fiuulDiethylphtbalateFluolalO4-Cblorophaayl~henyletber4-NitrolDi1iDe4,6-Dinitro-2-methylpbe:aolN-Nitrosodiphcnylamine1,2-DipbeDylhydtaziDe/ A%ObeuDlDO4-Bromophenyl-phalyletberHeuchlorobe:Dz.cnePmtaehloropheaolPbcnaDd1reDeAnthrxeaa

Cone.

< 160.0< 160.012100

< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0<: 160.0< 160.0< 160.0

MDL CompoWid

160.0 Carba'mlc160.0 Di-a·butylpnthalatc160.0 Fluonntheae160.0 Benzidine160.0 Pyreac160.0 3,3':Dimethylbenzidine160.0 ButylbeazylphthaJate160.03,3'-Dichlorobcnzidino160.0 BeI17.o[aJIIllhrace=160.0 Chtyseae160.0 b~-Ethylhexyl)pbthaJa&e160.0 Di-a-octylphthalate160.0 Benzo[b)lJuoraatheae160.0 Benzo(k)f1uorantheno160.0 BeazD(a]pyreae160.0 lndeao[I.2,J-cd]pyreao160.0 Dibeaz[a,h]antbraccuo160.0 Benzo£r,b,i)peryleno

Date SalJlpled :Timo Sampled :Date Analyzed :

Cone.

< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0< 160.0<2 160.0< 160.0< 160.0< 160.0

81919511:00f17t519S

MDL

160.0160.0160.0160.0160.0160.0160.0160.0160.0160.0

"160.0160.0160.0160.0160.0160.0160.0160.0'

.,

All NJDEP protocol were followed during anaJyses. These data have been reviewed and accepted by:

- ."Tba liability of IDferrated Aulytica1 Labontorics. IDe. is ~iod to tbo actuaJ COlt of the 1III&!r- perf01mod.

New J~ O:!atifial LaW·I47Sl New York Cc:rtiJIec1 Lab I 11402

TIERRA-B-004663

866300065Integrated Analytical Laboracories. Inc.!i,.nt:es- _c:ed

" 8Iy1:IC:&l"..: Labs- 273 FnmkJinRoad

Randalph. N.J. 07869

..~...

:ANALYl'ICAL DATA REPORT'for

Cbemiaa1 Compounds lac.2.9-75 Ri'fersicle ATe.Newark. N1 O71Dl

Project Name: SELF-MONITORINGLab Case Number: 10950 - 1m

201 381-4252Fax: 201 989-5288

MDL - METHOD DETECTION LIMIT

Lab 10: 1719-oolClieat 10: 001MlICrixIUaits: AqueowI -14s'L

Compouad

ChlorometbaaeViDyl chlorideBromomedwsoCbloroethaaoTrichlorotluorometbaae1.1-Dichloroetblll2eMetbyleae chloridetraas-l.2-Dich1oroetbeae1.I-Dich1oroet.lwaoCblorofOrm1.1.1- TrichloroedwJoCarboa tetncl1Ioride1.2-DicbloroetbaDoBcazeaeTrich10r0etheao1.2-Dichloropl'OpUlO

Cone.

< 100< 100< 100< 100< 100< 100<100< 100<100<100< 100<100< 100< 100< 100< 100

VOLATILES

MDL Compound

100 BromodichlorometlwJe100 2-Ch1oroethylvinyl other100 cu-1.3-DicbJoropropeae100 TolW!DO100 b'aI1lI-l.J-Dichloropropeae100 1.1.1-TricbJoroethaae200 Tetrachloroctheae100 DibrollJOChJorometbaDe100 Chlorobeazeae100 Elhylbenzene100 Xylene&, ~taI100 Bromoform100 l.l.2.2-TetncbJoroetbaoe100 1.3-Dichlorobcozeae100 t,4-Dichlorobelmme100 1.2-Dichlorobeazeae


Date Sampled: 8/9/95Time Sampled: 11:00Date Analyzed: 8/15/95

Cone.

< 100< 100<100<100< 100<100< 100<100< 100<100<100<100< 100~ 100< 100< 100

MDL

100100100100100100100100100100

" 100100100100100100

TENTATIVELY IDENTIFIED COMPOUNDSLab ID: 1719-001CJjIlll! 10: 001MItrixlUDits: Aqueous - ".eIL

COMPOUND

U.abawaL

ESTIMATEDCONCENTRATION

. i:.· ...-IS100D ;.

_.--.. ~.--".

Date Sampled:TUlle Sampled:Date Aaalyzed:

RETEN'l10N'J'IMB

5".76

8/9/9511:008/15/95

TIERRA-B-004664

·.; .' :,.".

866300066Integrated Analytical Labaramries, Inc.273 Franklin RoadRandolph. N.J. 07869

".. ..

201 361-4252Fax: 201 989-52B8

"ANALYTICAL DATA REPORT'for

CbemiCIl Compounds IDe.29-75 Rinmde Aye.Newark, HJ 07101 -

Project Name: SELF-MONITORINGLab Case Number: 10950 -17D

MPL _ MEWOD DETE£PON LIMIT < - LESS WAN WE MOL

-

LabID: 171~Clieat ID: 001MatrixlUDics: Aqueous - Po,1LCompound

N-NittosodimcthylaminoPhenolAnilinebi&(2~oroetbyl)echer2-cb1oropheDoi1.3-Dichlorobeuzcae1.~DichlorobeuzcaeBeaz:yl alcohol1,2-Dichlorobauzea,o2-Mcthylpheaolbis(2-ehloroisopropyl)ether4-MetbylphaaolN-Ni~-o-pIOPYIamioo2-AmiDolol- +.....AminotolueneHeudlJorocthaDeNitrobcn%ea.eIsopboroDe2·NitropheDol2.~DimcthylphCQOI

Cone.

< 40.0<40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0

BASE NEUTRALS ACIDS

MDL CompoWld .-40.0 bis(2-CbJorocthoxy)methaDe40.0 Benzoic acid40.0 2,4-DimethyllUliline40.0 2,~DichloropheDol40.0 1,2,4-TrichJorobeazmo40.0 Naphthalene40.0 4-Chloroaailiao40.0 Hexachlorobutadjeoe40.0 4-Chloro-3-mcthylpheool40.0 2·Methylaaphthal-40.0 Hexachlorocyclopeoradiene4{).0 2,4,6-TriChloropheool40.0 2,4.5-Trichloropbeaol40.0 2-Cb.10r0uapbthaleoe40.0 2-NitroaDiline40.0 Dimethylphtbabte40.0 2.6-DiDitrotolueao40.0 Acenapbthyleoe40.0

Pate Sampled :Timll 5.1mpled :Pate ADalymd :

Cone.< 40.0< 200.0< 40.0< 40.044.2-

< 40.0442-

< 40.0< 4{).0< 40.0< 40.0< 40.0< 40.0< 40.0<: 40,0< 40.0< 40.0< 40.0

8/919511:009115/95

MDL

40.0200.040.040.040.040.040.040.040.040.0

'·40.040.040.040.040.040.040.040.0"

CootiJlued 011 DCltt pap.

--'

NBI!' Jcnoy Oertificd Labl 14151

.•.• ._ t..,;.","=- _

New York CcIUfiod Lab , 114Ol.

TIERRA-B-004665

,'-. - .:.-..... ,..:;'-

866300067Integrated Analytical Laboramries. Inc.273 Franldin RoadRandolph. N.J. 07869


Chemical Compounds Inc.'2.9-75 Rinrside .be..Newark, Nl 07101

Project Name: SELF-MONITORINGLab Case Number: 10'50 - 171'

201 361-4252Fax: 201 9S9-5288

MOL - METHOD DETEcnON LIMIT

Lab ID: 1719-001Clieat m: 001MabixlUnits: Aqueous - nIL

Compound

3-NitrouiJineAcenaphtheDe2,4-Dinitropheaol4-Nitropheaol2.4-Dinitrotoluea.o

• DibeuzofurmDiethylphtbaWeFluoreae4-ClIorophaayl-pbeuylcth«4-NitrouWiaa ...

4,6-Dinitfo.2--methylpheaolN-NitrosodipbenylamiDa1.2-DipheDylhydrazinei Ambeu.zeae4-Bromopbel1yl-pbel1ylotherHeuchlorobeazeDo .PeDw:hJoropbaIoJPhcDaDduaaeADthRceae

Cone.

< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0<.40.0< 40.0< 40.0< 40.0< 40.0< 40.0

BASE NEUTRALS ACIDS

MDL CompoWld

40.0 Carbaiole40.0 Di-o-butylpbtha1ate40.0 Fluorantheoe40.0 Benzidine40.0 Py~a40.0 3,3' -Dimetbylbemidino40.0 Butylbenzylphtbalata40.0 3.3'-DichJorobeuzidino40.0 Beozo(a]aothraceno40.0 QuyIeIla40.0 bis(2-Ethylhexyl)phtbalato40.0 Di-n-octyipbtbalate40.0 Benzo(b]f1l1Oranlbene40.0 Bem:o(k]fJuoranthene40.0 Beazo[a]pyreao40.0 Iadeoo(l,2,3~]pyreae40.0 Dibem{a,h]aot1u1lceae40.0 Bem:oli,b.i]peryleae

< <II LESS THAN WE MDL

..Date Sampled :Time Sampled :Date Analyad :

Cone:.< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0< 40.0

8J919SU:oo8IiS195

MDL

40.040.040.040.040.040.040.040.040.040.0

"40.040.040.040.040.040.040.040.0"


-.

1llIliiability ofJntepted ADalytica1 Uboratori",lac. is limited 10tho actuaJ c:qst of tile aaaJy_ peafo:tmacL

.. '·New·Yom ~ l.-b 111402

TIERRA-B-004666

866300068Integrated Analytical Laboratories, Inc.273 Franklin RoadRandolph. N.J. 07869

201 361-4252Fax: 201 989-5288


ChemiCll1 Compounds Ine.29-75 Riverside Ave.

Newark, NJ 07101

Project Nome: Internal MonitoringLab Case Nwnber : 10950 - 1439

MOL _ METHOD OillCTJON LIMIT < ...LESS THAN THE MOL

LabID: 1439-001-CUeot ID : 00 1MatrixlUnit:s: Aqueous - jJ.cfLCompound Cone.

ChloromethaneVinyl chloride ..Bromometha.aeChIoroethaneTrichlorotluoromethaae

, l,l-0ichloroemcneMethylene chloridetrans-l,2-0ichlo~theftel,l-DichloroethaocChloroform1,1. I-Trichloroct1wleCarbon tetrachloride1,2-Dichloroct1wleBeazeocTrichloroemeul,2-Dichloropropane

< 50.0< 50.0< SO.O< SO.O-< 50.0< 50.0< 100.0< 50.0< SO.O< SO.O< SO.O< 50.0< 50.0< 50.0< 50.0< 50.0

VOLATILES - (6011602)

MDL Compound

50.050.050.050.050.050.0100.050.050.050.050.050.050.050.050.050.0

Bromodichlorometbane2.chloroethylvinyl etbercis· I,3-DichloropropeneTolul!tttlIrans-l,3-DicbJoropropene1,1,2· TrichloroethaneTetnachloroethc;nco ibromochloromethaneChJorobenzeneElhylbeozoacXylcnes. lolaIBromoforml,l,2,2-T etrachloroechane1,3-DichlorobeoU:tlc1,4-Dichlorobel1U:tlo1,2-Dichlorobcnz.ene

Date Sampled: 7n195Time Sampled: 14:00Date Analyzed: 7112195

" Cone. MDL

< 50.0 50.0< 50.0 50.0< 50.0 50.0< SO.O 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0< 50.0 50.0

Lab m : 14394'1Client ID : 001 ~r:)MatrixlUn.i1s : Aqueo 6

Result

< 0.05

TOTAL CYANlDE

~Opp Date Sampled :Time Sampled :Date Analyzed ;

MDL

0.05 •

7n19S14:00711'1J9S

-. All NJDEP protocol were followed during analyses. These data have been reviewed and accepted by:

-lbo liability of Inteptcd Allalyrical Labomories. 1Jlc. is limited to !be actual case oft!ut lIIA1yses performed.

New Jcncy Certified Labl147S1 New York Co:tWcd lAb , 11402

TIERRA-B-004667

866300069Int:egrated Analytical Laboratories, Inc.273 Franklin RoadRandolph, N.J. 07869

201 :361-4252Fax: 201 989-5288

ANAL YrlCAI:. DATA-REPORTfor

Chemical Compouads ~29-75 Rh'erside A"eo.Newark, NI 07101

Project Name: SelC-MonitoriD;Lab Case Number: 10950 -1438

'. D~

BOL = METHOD PETEcrJON LIMITBASE NEUTRALS


Lab ID : 1438- 001Client ID : 001Muri~m~:Aq~~-~g~CompoundN-NittosodimethyllUJlineADillnebis(2-011oroethyl)ether1,3-Dich1orobeDZenel,4-Dichlorobeo:l=leBenzyl alcohol1,2-Dich1orobeuzenebis(2-cl11oroisopropyl)ethcrN-Nitroso-di-n-propylamiDD

HexachloroethaaeNitrobeDzeaDIsopboronebis(2-011oroethoxy)metbaDe1,2,4- TricblorobenaAoNaphthalene4-CbloroanillDoHexaehlorobutadieuo2-MethylDapbthaleneHexaehIorocye1opentadieno2-C1Joronaphthaleuo2-NitroaniliDoDimethylpbthalate2,6-DinitrotolueacAccoaphthyleuo3-NitroauilinoAcenaphtheao2,4-DinitrotoJueaoDibeDzofUrm

Cone. MDL Compound .'

< 50.0 50.0 Diethylpbthalate< 50.0 50.0 Fluorene< 50.0 50.0 4-ChloropheDyl-phenylether< 50.0 50.0 4-NitroaDilino< SO.O 50.0 N-Nitrosodipbeoylamino< SO.O 50.0 l,2-DipheoylbydrazineiAzobeDzeDD< 50.0 50.0 4-Bromopbellyl-pbenylether< 50.0 50.0 HexacbJorobenz.eae< SO.O 50.0 PbelWlthreGo< 50.0 50.0 AIlthnceao< 50.0 50.0 Caroazole< SO.O 50.0 Di-a-butylpbthalale< 50.0 50.0 FJuoraathelle< SO.O 50.0 Benzidine< 50.0 50.0 P>'t-< 50.0 50.0 3,3'-Dimetbylbeazidille< SO.O 50.0 Butylbeu.zylpbtbaJaae< SO.O 50.0 J,3'-DicblorobellzidinD< SO.O 50.0 Beuw[a]aothrKeDe< SO.O 50.0 Cbryseae< SO.O 50.0 bis(2-Ethylhcxyl)phtbaJate< 50.0 50.0 Di-a-octylpbthalate< SO.O 50.0 Benzo(b]ftuoranthene< SO.O 50.0 Benzo{lt]ftUDrllllthelle< SO.O 50.0 BeI1ZO(a)pymac< SO.O 50.0 IndeIlo(l,2.3-cd]pyreae< 50.0 50.0 Dibeaz(a.h]8Ilthrxeao< SO.O 50.0 B=li.b,i]peryleoe

Date SampIDd: 7n195Time Sampled: 14:00Date Analyzed: 7ltS195

Cone.

< 50.0< 50.0< 50.0< 50.0< 50.0< SO.O< 50.0<50.0< 50.0< SO.O< SO.O< 50.0<50.0< SO.O< 50.0< 50.0< 50.0<50.0< SO.O< SO.O< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< 50.0< SO.O

MDL50.050.050.050.050.050.050.0SO.O50.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.050.0SO.O50.0

All NJOEP protocol were followed during analyses. These data have bee.n reviewed and accepted by:

--lchael _I:.aboratory O'

The liability ofIatepted ADalytical Laboralories, r.m.. illimitlld to the actual cost or-the ualysos pedoImod.

New Jeney certified Labl147S1 New York Cortifiod Lab , 1l.t02.

TIERRA-B-004668

'..866300070

Integra1:ed Analytical Laboratories, Inc•.273 Franklin RoadRandolph. N•..!. 07869

201 361-4252Fax: 201 989-5288

ANALYrlCAL DATA REPORTfor"

Chemical Compounds Inc:.29-75 Riverside AYe.Newurk~ NI 07101

Project Name: Self-Monitoring:Lab Case Nwnber : 10950 -1438

MOL .. METHOD DETEcrJON LIMITACIDS /

UtI ID : 1438- <1>1CUeat ID : 001MatrixlUnits : Aqueous - lAglL

Compound

.-Phenol2-Chloropheaol .'2-Mcehylphenol4-MethylphCDol2-Nitrophcaol

.. 2.4-0imeChylpheoolBea%Oic .cid2,4-DiehIorophCDol4-Q10r0-3-methylpbeool2,4.6- TriehIoropheaol2.4.5-Trichloropheaol2,4-DioitrophCDOl4-Nitropbeaol.4.6-0initro-2-methylphCDolPentachlorophenol

Lab m : 1438- 001Clieat m : 001MatrixlUnits: Aqueous - p.f/L

Compound

pH

< - LESS THAN THE MDL

Date Sampled: 7n195TUDe Sampled; 14:00Data Analyzed: 7/~/9S

Result Q MDL< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 50.0 50.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0< 10.0 10.0

pHlCorrosivit)'

.'

Date Sampled; 7n19STUDe Sampled: 14:00Date Analymd: 7/13/95

Result

12.51

MDL±.02

AU NJDEP protocol were followed during analyses. These data have been reviewed and accepted by:

-,The liability ofIatcpUcd Aaalytical Laboratories. IDe. is limited to tho actual cosC of tho aaaI)'ICI perfurmcd.

New Jency eatifiad UbI 14"1S1 New Yorlc Ccrtif1Cd Lab, 11402

TIERRA-B-004669

·.J ° ACCREDITED LASORATlJUES III:.

VIl..ATILE ORGANIC ·~YSI$ DATA

""4£ IU'IlER.-. PI.£ ItJ&R

fA FILEU.IEHT IW£fiELD fD

271'?i02011>AJIl4g;t

°BEW........................................................................................................... _-.~.....101018 Acrolein U101131 Acrylonitrile U74871 lJllaroMthue U748J? Bro-a.thane Um14 Vinyl lJllaride U]SOO; lJllara.thlne 0m92 "-thyl.ne Chloride J267641 Acetone U7Sl5O Carbon Disulfra. Um94 Trichlorofluoro .. thane U7';3'!i4 1,1-Dichloroeth.ne U7';34; 1,1-Dichlorolthane U1'!i66 OS trans-l,2-Dichloroethenl U6766; O1lorofo,.. 41107062 1,2-Dichloraeth~e '!iO789JJ 2-&tanane 5421m 1,1,1-Trichloroethane U

~J'!i Carbon Tetrachloride U- '0'4 Vinyl Acelat. U.14 Bra-adichlaro .. thane J1

SUBftIliAI'£ Cllml.HlS1,2-DichJoroethlne-d4Toluene-d8Bro-afluorabenzen.

J - Indicates coepaund concentration found below noL.U - Indicates caepound anel}lzed for but not detected.

II

61662020202011118

4.D4.114.04.04.04.114.114.04.04.0B.1l4.0

866300071

"'TilleDlLUTJ~ FACTlR _DATE EXTIKTEDDATE AHALVZEDANPL'iZED BY

Agucpy.10

IlL........................................ , .................................................. ~ ...788;'100n01S7901671432124481mos100610261107587'!i25259178610810112718479J4'!i10888;1089071004141011425m0207n47615mZ

1 ,2-Dichloroprap.nlei.-l,J-DichloraprapeneTrichlarcetheneBenzeneDibrolOchlaralllhane1,1,Z-Trichloroethanetren&-l,J-Dichloraprapene2-chlaroethylvinyleth.r8ralOlo,..2-Hexanane4-Methyl-Z-pentenoneTetrlchlaraethene~1,1,2,2-TetrachloroethaneTolueneCh lorobenzeneElhy lbenzen.Styrene',p-Xylen.a-Xyleneci$-l,Z-Dichlaroethene

LIMITS76-11488-llD

. 86-115

SIADJS-IL.-JL......lIL

uuuuuuuuuuuuU

17UUU

JSUU

4.a4.04.lI4.04.04.04.0

204.09.07.04.06.0'!i.D4.0

104.0

2821

4.0

B - Indiclte$ eoepound Found in .aaaeilted blank.II - Result exceeds specific ground water quality criteria.-

- F'lalJ$ are blsed on Specific Ground Water Qudit,. Criteria fro. Hew Jersey Register dated f'ebl'tllry1, 1993.

IIiii

11

TIERRA-B-004670

ACCREDITED lAIlIRUlIUES, lit:.866300072

IlIA IRGAHIC ~YSIS DATA

-' "ASE IU1IO 1m IfRTRIX AoueqvsSMI\£ tmlER Y'iU7m DlLUTlltl FACT~ ,OAT" FILE >F1B?Ii DATE EJ<TRACl8) Q5124/9lja.(EHT IlAI'E. CCI DATE IlNrt.VZED Q61vmFIELD 10 REOO AI«.YZED BY PetL

.......................................................... ..........................................................CAS • CIJ1PW«) \.GIL 10.. CAS • COIPaJI) lJOtL to........................................................... .._ ......--.._----- ..----_._._----11189S2 Phenal U 50 mOl 4-Ch lora--'", thy Ipheno I U '"'1511]8 2-0tloropheno I U 50 88062 2,4,6-Trichlorophenol U 509'i~7 2-Met"!llpheno I U 50 91)954 2,4,5-Trichlorophenol U 250Itl1UY4 }&4-neth~1 pheno 1 U 50 51m 2,4-Dinitrophenol U 2501I11i"i5 1-N1 troDl1enDI U 50 1001127 4-Hitrophenol U 2110lu5679 2,4-01~thylphonol U 50 mm 4,6-Dinitro-2 ... thylphenol U 25O1~O8}1 'l,4-0Ichloropheno I U 50 87865 PentlchlorophenoI U 25O111444 blsl-'l-ChlorDolh!lIIEthtr U '10 121142 2,4-0initrotoluene U 50'lAin 1 1,l-DichLorobenzene U 50 84662 DllIthylphthallle U 50lU6467 1,4-Dichlorobenzeno U 50 7OU5nJ 4-Chlorophenyl~phenyl.thlr U 50100516 Benzyl Alcohol U 50 86737 Fluorene .. U 50"'5,U1 l,2-tlichlorobenzene U '1U 1011016 4-Hitrolnil in U 25111011601 bis(2-Chlorol~o9ropyllether U 50 B6J06 H-Hilrcsodiphenyla.ine U 50621647 H-Hitro~o-oi-n~propyla.lne U 50 10155' 4-8roMOphenyl-phenylelher U IillIIm1 HeJac~loroethane lJ 50 118741 Hexachlorobenzeno U 50'111~'iJ Hilroblnnne U 50 8ma Phenanthrene U 50- 78591 IsophOrone U 50 120127 AnthreceAtl , U SO,5'!lil Benzoic Acid U 150 84742 Oi-nwButylphthalale U 50111911 bis(-Z-Chloro.thox~)Mlthane U 50 206440 Fluoranthltlle U SO12Ull21 1,2,4-Trlchlorobenzene U 511 129000 Pyrone U SO,,1211} Ha!Jhlhtlene U 50 85687 Sutylbenzyiphthilite U 1)6

10647!1 4-OIJoroaniline U SO 91941 },}'-Dichlorobenzidine U 100

Bi'68J Hexechlorobutadil"1 U 50 56S5} SenzD(a)Anthracen. U SO'11576 2~Mlth!1lntphthalene U 50 11m] 8is(2-EthylhexyllPhthalete U 50}7474 Hexlchlorocyclopentadlene U 511 218019 01.,.._ U 50'1lli87 2-L1hloronlphthalene U 1i0 117840 Di~ctyl phthll.te U 511ll1l744 2-HI Irolni line 1UOJ 250 205992 Benzo(blfluorlnthene U 58Ul113 Dl.I~1 Phthalate U 1i0 211718'1 Benzo(k)Fluoranthene U 50

"C 298'1118 Ac~nllohthylene U liO 50328 8enzo(llPyrene U SO..,9m l-Ni Iroant Iilll U 251 mm Indent(I,2,J-cdlPyrene U 50m29 Acenl9hthene U " m13 Dibenzo(l,h)Anthrlcene U 50))2649 Dibenzofuran U liD 191242 Benzo(g,h,ilPerylene U 586U6202 2,6-0Initrololuene U 50 62m H-Hilroaodi .. thylaaine U 51

SlJ{lQiAl E !JIII!JH)S REW.Q! ...L.lllJl1. ..mIlLIfltrobenzene-dS -11' '5-114 ....mL1-Fluorablphenyl --!ll 41-116 .JL.Terphenyl-dl4 -l1.!I: lJ-141 .-JIlLPhenoI-dS --2!' 11- 94- -lL-2-Fluo~henol --l2Z , 21-110 .JaIL2,4,6-Tribl'OlOphenol .......... NOT DETEtTED ••••••••••

J - ImJ icates cOlllpoundconcentration 'ound bel ....1Il.. B • Indicates cllllpound'ound in IIIOCi"ted blink.- !_lnchcales coilpound an.lyzed ror but not dettICted. U - Ae5ult"exclld6 speciFic ground Miter quality criteri".·- ,• fl.,s are b••ed on SpecifiC Ground Wiler QUality Cr,teril '1'08 Hew Jersey Regiltlr dated February 1, 1"'.•• Hlettlylphenol and 4-l'Iettlylphenolcan not be seplI'lted by 1"- .Ihod applied

TIERRA-B-004671

-case ~Salllple '1CUInt N_II'1_ld ~r:

ACCREDITal LAIOIIATauES. UIC.GEHERAL CHElUSTRY AIlALYSrS DATA

2n3 NIItrix:Date leeeiveell ....l!lU-Lu..zZ- _05119/952507'011

REDO

USULTSDJWTrt1l

FACTlIIIl£THOD BLANK

RESULTS IIlL

866300073

AlW.ysr$llJ.Te

Cyeni de , Total 0.01

IIlL UlUTS

NO 0.01 1. lID

..

TIERRA-B-004672

866300074

....... - .. ~.~~

TIERRA-B-004673

LAB 0 Rot~, VacuumFiller

DryerPress

o 15()lIgal.1500gaO 010,000 gal. Treatment

W.Water Tank TreatmentTank Diked Tank

Area GJ GJDSbctl-

O~ooligal.OSturage

Locatiun ufal

Emllt~' Drums

i··co·NcuTi················j PAD

STORAGEAREA

SafetySupplies OFFICESLocker

IlATIIROmr

FillerPress

1::1~

(

CHEMICAL COMPOUNDS INC.29·75 Riverside Ave.Newar N.J. 07104

Elevator

EmployeeBathroom &

Shower

(

TOSECONDFLOOR

TIERRA-B-004674

866300076

_ ....._~.,~~.......... _.""'- -_.~'-_.._........,..,

TIERRA-B-004675

OFFICES

BATHROOM

RAMP to Basement LAB

CHEMICAL COMPOUNDS INC.29-75 Rivcrsidc Ave.

WASTE WATER PLAN

Si

~

rainWaterTreatment InTank for

Heavy Metals "" ~

Drain Water Ollt - '--- DStorage Tanl;.Sent to III,nOn - fOI" Aftergallon Storage Treatment

Tank

PRODUCfION AREA

ALL PROCESS & DRAIN WASTEWATERTRANSFER TO A HOLDING/STORAGE

TANK NEXT TO SAMPLE POl NT INBASEMENT AND THEN IS PUMPED om

OF BU1LDlNG TO SEWER

Wastewater Out -to Sampling Pointfor Discharge 10

Sewer

Wastewater In -from Production to

Storage TankAfter Necessary

Treatment

.a .

0,concrct~

, ;~~gO~l... .:'.~'J D...............r---...:==~....,--l..-----_--.:.-_...:....-_--- ---::t:I

Datc: 'J7

Water ~Meters :Sanitary 1

Wastewater 0Collection :

. User Charg~ 1Prelrealmenl, m;t.s& Local Limil IM$

Sampling

To Manhole Tic-InApprox. 70 ft.

PASSAICRWE~

AdjacenlBldg. /I 7

TIERRA-B-004676

866300078

TIERRA-B-004677

-.'.' .. • .. '.1 :~':._.'._>.'.::: :~~ >... '....~ .. .......•... :.; .. :, .• : :1.... ' . . ',' :..:

_ ...' -:. . .. -.' .... . ~,'...

•~. ,.~. .Je~ney Papartmant ¢f Environ~ental Proteotion.and

Oivision or neBpons1~~8 Party sit. Re~edia~iQnuureau o~ ~merg~nay ~esponge

neqiol'l I

J.1!Y..~~T_+G;a.'l'TOJf

866300079..

r· ..'.' '':'.. '.

.~..' ..-..... -. .... - .... : .

File ;:. 0,714P1\C CODE: 'rEF ;: ••::I,:~ • '.

'.~.:'. ...

::j'gst.i.gator: 1-Iatthew Garamone~. Christopher Gibbons Tillie Arrived: 1115

.~L(H:af;.C!n: . Chemical Colt1~oundst J:nc."\11dre·~.:i(. 29-75 Rivel:'Slde i\venue

.:-;..:... Newax:k, NJ

.;.':"'!;'.':c')'nsible l'arty::.· CheIllical CotnRounds, Inc.'~~:~h7 Address: 29-75 Riverslde Avenue

Net.;ark, NJ

Time Dep~rted:.l~OO•. '.','-. I~ •.

....;:: .

. .. ;...

',-,

, ,;'c·;>.t.ion phon4 II: 201-4:.15-3211

,~ '(' .. , .;.1;. ..

Bob swales - Newark OEK ~hQne t .

Phone "" :":'-,Ln of Complaint: Oper. piccitto • NJSPH,Il: Lna Bll r:eau

... - .. :.....

TIERRA-B-004678

~ .. " .. -'--'~-.··:t~i;;i:::31 Compou"nds I Inc. manU.factures hair tjye~. In partfcul:<1lr ( th~.;.;.,.. ,.. i.r l.~y has b.aan £JJ:·odl.lctng reel ''J and He-blue #2 hair dyes, '1'he d.ark":.;...T!.~' liquid observed on the grQund aJ:ound the ou1;slde.,of the ,,;"~:::~~>":'~':":'~~~lLit:( is attriol.1ted to these two dyes. 'rhe .f"clC.lllty sto~es its .\.'t~~T'~.";':~i! :ll'J'.lid f.rem theil':" proceSSS$ in a. ~ ,500 9allon cap«c.i,ty t:ank.l:',:\:;~'~;t.

. ';:':~ In t~Q r'ear (.If. ~hn facility. Olsposal of this matet"ial i. ,',;:;';':.•::.

..I;'·j:; ChemlC<ll 1';,H.lt'l h:-lnngarnent. which manifests the waste as a .. ::,.,.::~,.',;:;;.:;,·;.:-:l~!.::'i\t:dou-s prO(;':'::;f;; liqu.id ".o.s, prior to recycling' r.tsth.:lnQl rn',:~!,:~:::<~'.'.;:: ~ Fr·)ce~.:SGS I thi~ E,1C 11ity also disposed of waste methanol, tht'QUcih .-:' ."."; :~:":.~1 h'.::w tEl t'I:1n~I{J':O;-:1("rll\~ ':.H1d had an EPA 'Jenera tOl': n.umbar ass~qn.d to .",~ ;':". ~I,tty c...t!UD 1:;8 -\i!~-:L"J3?>. ThG faCllity maintains " tanker ..;"','1':1-.: :J!:' metnanul-?n"",lte W'l.th a ca~acity of 4,000 gallons fortnair.. ::.~.'.'::'i. Floor d.l'.'nillS at the facil~ty dischargo! into the sanitary; ......

" ,·...:t· ,·;·\'stem c1CCol:'dill9' to Mr, Celliri. The facility I powever, has no":.r-;,.~t!r.it from PVSC tc d;u$charge any material trom their~rocesse.s into~~esar:tarv line.

""0 ·;c[ndo:tf ~nd Kirschner went to Clara Maa" Kospital in Bellev Hie. .c.:.le to chemical 'exposure at: the incidant. location. In addition, 8 ";-~.'i ::'.a:'p . ':":':;,l at he NaD -:-Greco Co. ad aCQnt to the incIdent IocatLon . ;.:~~:'" '.s_~~;:i--:t:::e'~ical attentl.o!1 for chern at! exposure at flrst tare dica18,~.::' .. _:. ;

"'::7:;'..:,;) l.n Kearny. fnvestigators fl:'oJ:l the Essex Co~ntY' Prosecutor's ..;~~t~t...;;;:.,.:.::;r.i'::'; and thoe Div.lSion of Criminal JUstice also performed an :~~;}~;):.{'.":'.r~sl:igat:iol"l ot thi~ incid-ant.Invest1 at 5 ..";"(;".~"::

-,--:...:s~;ada' NOV to Chemlca 1 Co Q "':_ t! .. 1"1' -looW:U;92 all ,.;.")'.,.~'i ,.n;:;:i-:~ol:.l lcatl.on of a dlscharge ot a bazaroous: SUbStance pursuant to"\~~ .. ,:!' "

• --'4:-l'-'lo.;-:clll act, _.rhe ~a';i Ii ~Y co~tracted ENSIr rnc. of Newark to . · ...W_~~~:k.:

:~'':"":'':;,\1 tl..clean-up Ot all.f.l:ee-standing liqu d on the property and to.. :;'.,;~:::;~':.' '~. '.11 ,~,".nules for anal~·s.ls of the stained areas of 9round and '.:<, .:;.. :; .....

:.. ,.:·~"..\hdl.nq liquid. Tne a'ffectEld areaa were Covered with pla$t:ic·.-:" ..;~.\:,Gi,::•... ;.:...:,,~:! tlHI Reed t~') remove any contant1nated soil bilsed on these.. ...,_/'.: :". ." ',:" ,;, : . . , .. :.:;'

~.. .);//:~',.:; '.'

\:-;: •.\·ai~n:.1: HER Region r t'CiBponded to Newark to investiqat:Q the ' ...:·\:f\·~;:.:.; .. 1; ;."l t:hCJ NJSP ~rarine Bureau ot the illegal dumping ot an unknowrL~~: ..! ".:'.".~=·i·~~:1 .i :ltc,'l the. P'l ssaic. Rivet" from the Chemical Compounds t facility .;';1!t~:rt ..";: • .': .-i 5.idHlr9e. of an llnknown, dark. purple liquid containinq acetic.c!d~'r~:",l:~":>':: ::Icetl.C= anhydride oC9urred onto the ground at the facility. ...-~.!._.:.~.... , !Ol·.~. of. Ne\ol'ari<was h.lred by the facili~y to parfon a Clean-up~ ..:~,.:~. ;;:.

:. ',,'.;!!., issued fot" thh. discha.rqa and thfl J.ncident' is under a'~:':.;' ..;:·.-.::li:'l<ll investigation by both t:he Stat. and the County;. .";~~~::

.; ."L¥~\~.. ;~.:J:. '.' f~,~~;..]~. ~~T

___ ._~ .'.~"'",;,,~ .o....-_--,;, __ .

TIERRA-B-004679

' .. ". ..".. :~"........ . 0.:." •.,. ... ~ I:. '-:'" '. . '!!";9-'

.," '".. ''; ";"'~''al,,''V-e.'~~;'. "~~;'.·1~~'·;':

.: ::..~.~~;' ~--.._ "_..-._ - .

... '. :' .• ":':: .=.. : .... ._ ...-.- ....... _ ..... ~._~......... _-_ ..... -... D·~Ci----_

LL ;":...

..---- ....- ..- -.- .... __ .. ..,., ....

. --- _.-

-.:. ":;-:•..

:'."'1 ."

..........~..v.~

-

.'

TIERRA-B-004680

-

-.

.-'-:",:-"'.-.: ..- 1- "1" •

.- ....

. \ -!"••

NEWARK FIRE DEPARTMENTOFFICE OF HA2:ARDous MATERIALS188 MuIbeny StreetNewark. New Jeraq 07102

(201) 733-ns08

STAl'ILEY J. XOSSUP_"..CIIW

Fu: (201) 733-7488

Chemical Compounds29-75 Riverside AvenueNewark, NJ 07104 January 10. 1992

attn: Mr. Harold Sullivan

On January 7, 1992. the Newark Fire Depamnent's Hazardous Marenals Unit respondedto your facility, Chemical Compounds at. 29 Riverside Avenue. The complaint regardedunidentified liquid flowing from a hose line on the second floor of your building, down a set ofexterior stairs, onto the ground and into the Passaic River.

This action is a violation of the City of Newark's Hazardous Materials Regulations. Youarc in violation of the following:

Section 8.4 Drainage from production facilities. including buildings. and other processareas shall be SO engineered as to provide a means of secondarycontainment for spilled hazardous materials.

Process wastewater and cooling water pipes. plant drains and similarinstallations which drain into sewers. storm drains. public wastewatertreaUUent plants. watercourses or other routes which drain to waters of thestate shall be engineered so that spills of hazardous materials will notescape through them to waters of the State. If hazardous materials capturedin secondary containment systems drain into process wastewater lines,provisions must be made to treat or remove the hazardous materials beforethe water is discharged.

On January 1,1992, you or one of your employees disconnected a hose line leading intoa waste recovery truck. The hose line was rerouted, enabling liquid to flow onto unprotectedearth. and into the Passaic River.

866300082

TIERRA-B-004681

. .~..' . .-.' .

.... ~.' .; o •• ~ .~ ~ 0° .: .' .. ' . ~.

• 0- '.

.~..~- , Section 10.1b It shall be unlawful to use or operate any bulk: storage area or part thereof

without:

(b) providing for the se~gation of potentially reactive chemicals which x...materials or which may react 80 as to fann hazardous materials. and whichpresent or cause a hazardous or dangerous condition.

(t was noted that oxidizers. (M & T Chromic Acid) are stacked on top of corrosives.(Ethylene Cholorhydrin)

Section 12.2 All loading. unloading or transfer of hazardous materials shall take placeby a qualified person.

All vehicles and rail cars carrying hazardous materials shall stand or beparked only in a secure area where they are under the care, custody, andcontrol of a Permit holder. \

A person who loads or unloads hazardous materials shall comply with theapplicable Federal laws and regulations, in addition to any local and Staterequirements.

An unqualified person disconnected the hose leading to the waste container. If the person 'I-was qualified he would have been required to know that the product he was discharging onto theground was hazardous.

Section 15.1 In the event of fuel explosion. structural failure, leakage or other dischargerelating to hazardous materials requiring notifications under Federal or Statelaw, the permit holder shall also notify the Director.

The penniuee shall submit to the Director within ten days a copy of thewritten report pursuant to the Hazardous Substance Discharges: - Reportsand Notices Act. NJ.S.A. 13:IK·lS. and regulations promulgatedthereunder.

The pennittee shall also provide infonnation to the Director relating to they.bility of the pennittee to contain and dispose of the hazardous material. tthe estimated time it will take to complete storage and disposal. the degreeof hazan:l Cl'Cated and the quantity and type of material released. TheDirector may verify that the hazardous material is being contained andappropriately disposed.

..- The appropriate agencies were not notified wben the spill. leak or discharge occumd.A private citizen reported this incident to the State Police •

866300083.. ,..,.

TIERRA-B-004682

-

-

. ."

Section 17.1c Failure to abate, correct or rectify any noncompliance with the provisionsof these Regulations any pennit conditions or any provisions of theHazardous Materials Management Plan with the time specified in the Noticeof Noncompliance;

Section 17.3 If the cause of the noncompliance is not abated, cOlTCeted, or rectifiedwithin the time specified in the Notice of Noncompliance, a Notice ofViolation shall be issued.

The Notice of Violation shall be in writing and shall include a referenceto the original Notice of Noncompliance, the unconditional right to ahearing and the remedial action to be undertaken.

Under conditions of imminent hazard the Director.may issue a Notice ofViolation without issuing a Nop.ce of Noncomplian~e.

Section 17.4 A request for a hearing by the pennittec shall be given to the Director inwriting, setting forth in particular any defense the pennittee might have inregard to the alleged violations, and a brief statement of the factual mattersin support thereof. The notice of the bearing date shall be given by theDirector at least ten (10) days prior to the hearing date •

.Section 18.4 Every Permit holder shall insure that a qualified person shall be in charge

at all times and at each and every place where hazanious materialsoperations are carried out. The. qualified person shall remain on thepremises as long as the manufacture, use processing, or handling ofhazardous materials is being camed out and shall return to' the premiseswhen required under emergency circumstances. To be a qualified person,the individual shall be knowledgeable in the chemical and physicalprocesses utilized by the Permit bolder.

The Permit holder shall furnish to the Director a list of qualified persons Xwith their addresses and telephone numbers to be contaCted in the event ..' .of any emergency circumstance, to be updated annually. The director shallprovide said personnel with passes to be shown to City emergencypersonnel to allow the bolder to pass through any manned emergencybarricades and enter the permince facility in the event of an emergency.

The person who placed the hose leading from the building to the ground and into the riverdid not remain on the premises.

866300084

TIERRA-B-004683

: :' ".- ...~...-.:: .~-

........./..-:..

-

-

_.

Section 20.2 Whenever in these Regulations any act is prohibited or is made or declaredto be unlawful, or whenever in these Regulations the perfonnance of anyact is required or the failure to perform any act is made or declared to beunlawful, the commission of any such prohibited act or the failure toperfonn any such ac4 shall be punished by a fine or not more than$1,000.00 per day per violation or by imprisonmeot for a term of not morethan 90 days, or by any combination of such fme and imprisonment. E~day any violation of these Regulations continues shall be considcn:d aseparate offense. .

You have been found" to be in violation of five sections of the City of Newark'sHaUroous Materials Regulations.

Battalion Ch~f A. Apostolico

1(Ob1:r:r/ 1'tCj ~

f!) .12

t~\ ~I7JJ.:~Ei--- )

.J itJc,

AA:lm

866300085

TIERRA-B-004684

866300088

•..~ ...~.~

TIERRA-B-004685

·, . ..866300087

.'Ja.nuary 31, 1992

Ensi Inc.194 Avenue LNew!JXk, NeT 07105

Attn: -:.Fred Virrazzi

Nytest is pleased to submit our Project No. _'~9~21~861~~4~~~~Log. in No. 10097 on your sample (s) re~eived: 1/09/92

I

Test s&mple (5) associated with this project will be retainedfor a period of thirt~ (30) days, unless otherwise instruct-ed.'My staff is available to answer any questions concernin~ ourreport and we look forward to serving your future analyticalneeds.Very trul~ yours,~5tr;:z41Ramo GiganteExec. VP

Inc.

II

i,I

-

RG:+,Ene.

SHIPPED VIA: UPS RED

box 15180 60 seaview blvd.. port washington. ny n050 0 (516) 625-5500:: . fax (516) 625-1274

TIERRA-B-004686

·, "- .. ' ••••• cc'·, .f: .--:_.-. ,.

f .. nytest environmentolnc .

1-

~~~,lr. Id~ntiflcnr;on and ~oKulrs.. ---..._ ~.~~.~ - L09 In No.: 10997

Sample No: 1"... "Lab Sample 10 No.: 1099701

..R"sulaHe••

Allowable Levels

pll OJ 20 C

Ignitab;~1.ty_ F PHCorros;vity. inches/year'r.nctivity to cyenid,,_ PPMR~activitY to Sulfido, PPMTotnl Sol Ids _ XPetroleum Hydrocarbons, PPH (Dry Ut.)PCll's ,PPH (Pry wr.)

2 • 12.5140

0.250

..

4.35> 212

< 0.01< 1.0< 1.049.35350.. 2.0

.'

-

NO • None Oetected.. .. Less tll~

._.-------_ ..~......-.

00010---:-: .. 866300088

TIERRA-B-004687

.., .

.,"

- "._--'---

-_._-------, ... -...

\.,~TECHNION INC ..

2S0 Delawanna AvenueC1i~ton,. New Jersey 01014

201.-173-501.3FAX .~ 201-773-4788

LAB DEP t: 01190

'.'

"

--

C~IE~~ Chemica~ Compounds Inc..CLIEN'r REF:. 22592

MATERIAL: One (1) composite fromeleven (11) drums

DA'rE~TECHN:ION REP~

DATE RECEIVED;:LAB 1D:

2-27-92.160312-25-920122'r

I.,:,..'- i:

·f,:;.','

L.~.-~-:',:i:' ..::~.:.I"•.. :-

ANALYSIS REQ: RCRA waste characteristics " .-, .

The above samples were as received on 2-25-92 and analyzedas requested. .

. .ANALYST: Sam Yart, Mara Fishman •.

CERTIFICATE OF ANALYSIS

TEST RESULTS: ..','~ 6",'

.- '~ "'.~.~';,.'-.J." .:.

- All test results are as attached.

-':.. I·..•

.:'.': .~ .• ~ ".a ..

- ..J'. 866300089

Respectful1y submitted,

"~~" / /.;,,,"':.j'/C-?";' /- ..,;trlit:.<.-<:. /<:-,( t:-

v Susan Baturay, D.Sc.Laboratory Director

SB/sn16031

._----- ._--- .

~---- ..._. _ ..

...., ,. .... .-

..-...:~.t~.__ -..... ., :...... - •.

.<~;,:y~;;~~{~!~i1.2. . . ~..,

... ,.'0,

TIERRA-B-004688

-

--.. __.

-

-- ._._--_ ........ -... -, ..~ ... _.~_.

---...--..

"-~~HN:rON me.,

250 DB1aw~na.AvBnu.c~ifton, N.w J.rsey 070~4

Lab Dap i~ 07190

CL:rENT: Chemica~ Compounds :rnc_

RUN DATE/TIME: 2-27-92/~0:OO

SAMPLE r.D.= Cqmposite

I.£ETALS

ArsenicBariumCadmiumChromiumLead:·iercuryse~eniumsilver

TES~ RESULTS FOR TCLP METALS

RESULTS BLANX

SAMPLE T.YPEr Liqui.d

SAMPLE DATED: 2-25-92

O.O~O.O~O.O~O.O~O.O~0.002O.O~o .O~

Test results are in mg/I, unless specified.

N.D.N.D.N. D.N. D.N.D.

;N.D.N.D.N.D.

<0.01<0.01<0.01<0.01<0.01<0.002<0 •.01<0.01

N.D_~ Not DetectedM:o. L. : Minimum Detection Limit

----._.- ..........

~'-"

• -....... .or ....... .-. '--."'''- .....: ........ -

MAX. ALLOWABLELIMITS

5.0100.0

~.. ~. 05.05.00.21.05.0

866300090

i:

. f.~"'. {.

0, '~.. .~.

~.~:.

~.".;.; .

TIERRA-B-004689

...•..::..

TE~ION INC ..,250 Delawanpa Avenue

c~ifton,New Jersey 07014Lab cap It 07~90

..._.--CL"I:ENT:.·-Chemica~ compounds Inc_

-

RUN DATE:: 2,-27-92.

Liquid .-

SAMELE 'r'l'PB:

DA'rE SAMPLED: 2-25-92

SAMPLE LD. : composite-,. ~-... ..- .. -.,

. -HAZARDOQS WASTE CHARACTERIST~CS .,'

W~STE CHA~CTERISTICS RESULTS BLANKMAX. ALLOWABU

MRM LIMITS (ppm)~.

(mq/kq) 5.-5"0':"250500

30000>140

2<pH < l2~5

PCB (mg/l)Reactivity for CN-(rng HCN/)l)Reactivity for S-(mg H2S/l)Total Pet.Hydc.(TPHC) (mg/l)Ignitability (oF). NotCorrosivity as pH

N.D.N.D.N.D.3.0

Ignitable4.5

N.D.N. O.N.D.N.D.N/AN/A

0.365.Q.

10.0·0.10N/AN/A

". T~st re~ults are in rng/l, unless specified.

M/A: Not.ApplicableN.D.: Not DetectedMDL~ Minimum Detection Limit

...~-~-.----.

--.....

866300091 L:__..'~,.'

....~,..:":.:.... _.

,"

'. :.. - ' ...:~... '." .::....

- "-TEC~J:OH IHC.,2$0 De1awanna Avenue

'Clifton, New Jersey 07014Lab Dep f:. 07190

CLIENT: Chemical compounds rnc. SAMPLE TYPE: LiquidDATE SAMPLED~ 2-25-92_,._.,__RUNDATE: 2-26-92

...- - .. ,..,

SAMPLE ID~2J4567a91011,-

RESULTS FOR pH MEASUREMENTSRESULTS (unit) . : ~;.. _ ........

5.25.14.95.14.25.84.35.74.14.24.2

•.

.;'.,

" .~.

'.,~'.

f'{-I,.il.I

...",{t..:'::.

--,';' -.~_.- .---... . ......

f .i".;.}.::..

.·0-:::::-',.--:- ~:--' .. 866300092'-'" ': 0"

'.

TIERRA-B-004691

I)',

~. :. ,j ,

Ij

, i

S i le IU

.

(lilLe" S/Ild

TillieSp/d I\nillysis

PP.VM#/,jl;.,,-t!) NoDiJtt..v", 1 ;-~lf.qJ

~Yf.\ tfJ ,..;..'11,Pit-v'" II~ ;, -~t/-t

DiuM.fl.s J.J,'!-'!£~"'n #,b ~ oJ 'l.l/J.

.... ..... r F. C III" j;") II, )Tn:ih;. , +.I:"r:d rh:!ll'~ll"'h ...1,11" o,hn'/

~;..,,, iJelLlWol1f1U i\~'U1IULl

(;li::,IO, NoVi J.;, ~i~Y O!(ll'l

,)---:-- ..'

"

LPn 10 d ;'.

(llJ/) 7'!~\"5{)13, ,'. Fl\X nr (201177J,...4700",:,

. e.ofll\POv~ D.5 ,. "'i:nOJECT 110.

....i;i'O",'U" 1-lL~'!h.. ~-----:----."":'"'.. .. ..• :I'~.i:~.

.......,,:, .

!'/'lIUIJUCT 1If111E CH ~1\1' tAL

~Ull[mU Ul .I~'.'I~ 9~lo.c'==--·---. ~:. ell" III Of CUSTODY

Ii./'.; ....

Silnlllli n9 Poi nt "iri;.d S'ilmp1109 l1l!thod Silmp 1eDescription Hateria'

DI!.~fV&J 1/ 1- J / . ' G-1Z.f-1(JJ'I' II I ~

II " II:

/t II I • ... .:,.

II II It i i

,

" '.' I .~ ."

II t , ,

II • I' II

'nECEJ~E\): or

~

OnGI\HI ZII T lorl .01\ TEIT ItlE

fi:PC/(AJIOtJJjJC *,~.t./~10

.\

·_-··-------1---------1------1--------1,------·- ---.:.---1-----"". ;.

.. I'" .

,.,, .

'\.

"

~. .....

TIERRA-B-004692

\ '·8 III If~ .........--·"U~i'd:~; i.,ou "t.,;;t~"'l •. 11 ~

,:.11 OelaW;UII' '"','IjI\UU"

;"";,,I\,I'I(:':.'!' ) ,',"nl". \ ),!

,,;I, I (::"i,i TO,,:.·;:' '.1

',' 1 •• };',,,:{ n \'~ (2011'n~l,.,nO!J" I '

" ,I ," ",' '1'110IlUC.I, IIhlI£ chUl'lI<-1I1 C"~(.J.<. l'Il"J(CT II" -----:..." --+--------

;; , . Ie Ull ECH U U1 \ IlaPle l'~...LIfJ.~:---'-;;" r-,'A-u..c.=-- ..c •••. ' .l::~gn"u"1,...:3:-:=!-'~M.."",o:......l4--,;'...J~J..l-f~,1-• ."..'::--' ~-------

:~' ~ Of CUS100Y II'

)

, "

" '. .', "

Sile II)Sill! TYlle

-~-_\~=-,_=--_,---~,,--_--:-:,"__ --r-:---i-----I------"-IICAlilrl:sSillnp) e

H<lteriilJ 7tf -

~.

ol\l E IT I tiE

.Ffi{jql! l/'3tJ •

S anll)' iI1g Po i11t "all,1I- S'ilUlPling I-IllthollOescril)tion

!\nillys isT i111l!Spld. =

...Dt,»t"I#'1 ;·;,/-12. ,"flu'{x'f"M "ltl.,..::.:j...:::..·).:-t(Jf~2.1_>-' _.I-------r--~_--I-:..-.---I--.:..----,I-------

pf:vf'l ~JI ::J.-j~-V" p~('I\ r I" Ml\o$ I"\l. ,

"",I

-:. ",

1.'

_--'I----I-----'I------.:.._--~---~·---:..---_-I,-..:-------I----------""'

: ;

onG"" Ill'. nOliIlECE1VEU 01

"&2.fl/i = "_ftlll

_#J"'_N1'frJ_C _1-.--.---1--I

TIERRA-B-004693

SAMPLE LOG~J:N SHEET -"",

'- "\or.: ( of.....L-Tec!lnion Tnc. I

. p~

[Jei) ,: 01190 I

. ".~..... ::y (Print Same): i,Jd.I'I,c1-~ L.og-in Date: 2 -:l~- 9 7.-...... 1",; ....

-. ~AA.

...~!';cC'2:; ;:Signature):

-

O"! c''''"",...,.." r ..... _! •CORRESPONDINO

' ,

.:.t" _~C .9#. --- .l.~"

,".V. '0 C k-e.. lc,wl SAMPLE ASSIGNED ANALYSIS REMARKS:..... "_:T:<;. \.v\ I

5 ':iU:£:::'V'fA. f 0 lI\ If\~

TAG LAB REQUESTED , CONDITION OF".' ..;.:-:':

-:~7~·_·.'::-,"

i 1# SAMPLE SHIPMENT I E'l!C:~':--

~.ovSt'Jd "'- -rc.. L P Ii ~1_.1~_M\)~Sc-!",'\ rrC"Mnt IA'ndC -- ~I '\ p,,- R,/'

:M:IevOrat.B

:u~.!,~......~~..~' 1/ ."/ -rp14c ,

;..--':- .~..:.,;"," l'":'t'tIl"I"':\~ IJ <..., 011 1''''' .l, 'vfll~'1 tS )

~,;.:al, C/ -( f? 1J fl(!./ /... \ v' I IJlJ'f (Gt) ).'~:~~:t:f''''''' at ?:-tHntlAbIcnI

I

. "'\ I "'.A /J TJ rr .• ~'

•.:_:~; L. f b• I II' "/

.::oii: ."il"billi'Slickct } 77A(I(\O ~j\ 1~tm«td" ....criC

"'/VI

-~ (j-:.- .....-..

,·.:.;;;~i~:.. " !".a ..-tKI',..,~.-c

- - ..

~~••'t':','t;.... rfOC Lt.....

.:..~2 "" Q>oiIo-ot•. .C:.l.If~

~~t:':~1 Ii ,.....' _ •.• :::~"nt""cn.·"1

L..·~iI'Il

~ ::.ni...: -"-:,".3I~ ...~.)ft·.

:.b,.~..~r.:.-."C':IJ. ~1":M1'k'

.:;:.~",.::,:J .....r.sei.

'-~_,,";ru! Y..nIc>·

::.n~~cn: ...ciS .'tI La:

""~.':WNt:c .....J:

~

Sample Tr:msrer,!

r,.accioft:A.I'C ,~

. .. :

Ir.

~,

C''''

.;

;t

..

:."

.'.:=:"

..;",,- ..:..',.

"~ !~JO ;Ll~ 1IM::t .rK~ 01rnaIvdoft

"::.,":,_-_ )2...Q..<;;; ••tI I--~ ("if 2-Z 7 I/- tJJ..n~"'?YI ~ C"",£05/k :r (;I. ..... fJ /-(. .

olol.-d{;'ne J. f'otr-'. II D/'LlM'l s;;,,,,h'

...'~

CIo:!': '-866300095 .".: :....

TIERRA-B-004694

866300096

TIERRA-B-004695

c-

-

'. _ •• 01

....; .;:- :114,. C U

GABRXEL M. AMBROSIO, ESQ.464 val~ey Brook AvenueP.O. Box.911Lyndhurst, New Jersey 07071(201) 933-8844Attorneys for Plaintiff

Icnni1j A. MARGOUSt'.J. t:11

SUPERIOR COURT OF NEW JERSEYCHANCERY DIVISION - ESSEX COUNTY

PASSAIC VALLEY SEWERAGECOMMISSIONERS, a body politicand corporate .of the state ofNew Jersey,

DOCKET NO: C-338-93Civil Action

plaintiff, CONSENT ORDER ANDFINAL JUDGMENT

".CHEMICAL COMPOUNDS, INC.,

Def.endant.

This matter having been opened to the Court by Gabriel M.Ambrosio, Esq. (John T. Ambrosio, Esq., appearing) on behalf of theplaintiff, the PASSAIC VALLEY SEWERAGE COMMISSIONERS ("PVSC" ),alleging that the defendant, Chemical Compounds, Inc. ("ChemicalCompounds"), violated the provisions of N.J.5.A. 58:14-1 et seg. bydischarging pollutants in excess of Sewer Connection Per.mit No.20407122 ("Permit"), the rules and regulations of the PVSC and theCategorical Pretreatment Regulations promulgated by the UnitedStates Environmental Protection Agency ('"USEPA")at 40 C.F.R. Ii

414, and the defendant, without admitting any fact, liability orfault as to any or all of the allegations of the complaint, havingconsented to the entry of the within Consent Order and FinalJudqment, and for good cause thus shown;

866300097

TIERRA-B-004696

IT IS on this day of December 1994;- ORDERED that:civil Penalties

1. Within 10 days of the date hereof, the defendant,Chemical Compounds, shall pay to the PVSC the sum of 5ix~thousanddollars ($6,000.00) (the "Settlement Amount") in settlement of allcivil penalties that could have been assessed against the defendantfor allegedly having violated the provisions of N.J.S.A. 58:14-1 etseg. -by discharging pollutants in excess of the Categoricalpretreatment effluent limitations promulgated at 40 C.F.R. @i 414and incorporated by reference in the Permit between July 1, 1991

,and th!! present, including, but not limited to, those allegedviolations set forth in the complaint filed by the plaintiff inthis action. All settlement payments shall be made payable to the

"passaic valley Sewerage commissioners."compliance Schedule

.' 2. Chemical Compounds shall comply with the followingschedule for the purpose of controlling and eliminating dischargesin excess of the Lead~ Zinc and cyanide limitations of the Ii 414

Categorical Pretreatment Regulation and the Permit:(a) Chemical Compounds shall immediately. conunence

and implement a study program for the purpose ofidentifying possible raw materials and in-plant processeswhich may be the source of Lead and Zinc entering its

wastewater system.

- 2 -

866300098

TIERRA-B-004697

_" ~.' • t • '- .••• ; '••-" .-.

(b) On or before December l, 1994, ChemicalCompounds shall.submit a First Interim Report to the PVSCdetailing its compliance with the discharge limitationsfor Lead, Zinc and Cyanide. If the results of the FirstInterim Compliance Report indicate that no additionalpretreatment control equipment is required, ChemicalCompounds shall.be in compliance with the limitations forthe discharge of Lead and Zinc on or before December 1,~994. If the results of the First Interim ComplianceReport indicate that additional pretreatment controlequipment is required to achieve compliance with thedischarge limitations for Lead, Zinc and Cyanide,Chemical Compounds shall retain the services of aqualified environmental consultant who shall evaluate itsexisting wastewater pre~reatment system and makenecessary recommendations for the purposes of controllingand eliminating discharges in_excess of the Lead, zincand cyanide discharge limitations of the Permit.

(c) In no event shall final compliance with thedischarge limitations for Lead, Zinc and Cyanide beextended past April 1, 1995.

Progress Reports3. Chemical Compounds shall submit to the PVSC monthly

progress reports concerning its compliance with the requirementsand obligations of this Order.

- 3 -

866300099

TIERRA-B-004698

-

-

.-

Final Report4. within ninety (90) days of completing the corrective

action described in paragraph 12, the defendant shall submit to thePVSC a final report concerning its compliance with all applicablepretreatment standards.

Force MajeureS. The completion date for the corrective action described.in paragraph '2 or for the submission of any report required by

this -Order, shall be extended for the period of time that thedefendant or its agent is prevented by a Force Majeure event fromproceeding with the corrective action or subm±tting the requiredreport. As used in this Order, a Force Majeure event shall mean anevent which is beyond the reasonable control of the defendantincluding, but not lindted to, such events as fire, explosion,inclement weather conditions (that create unforeseen delays), labordisputes, inability to obtain or unavoidable delay in the deliveryof materials, inability to obtain or unavoidable delay in securingmunicipal approvals and/or work permits, inability to obtain orunavoidable delay in securing State approvals and/or TreatmentWorks Approval and unforeseen subsurface conditions. If the'occurrence of a Force Majeure event causes or may cause delay inmeeting any completion or submission date set forth above,defendant shall notify the PVSC in writing within ten (10) days ofthe occurrence of such event, the precise cause of the delay, themeasures taken or to be taken by the defendant to prevent orminimize the delay, an estimate of the date by which such measures

- 4 -

866300100

TIERRA-B-004699

-

.-

('....-will be completed or such report will be submitted, and an estimateof the duration of the delay. The defendant shall promptlyimplement all reasonable measures to prevent or minimize any suchdelays, prevent or minimize any adverse impact on the PVSC systemas a result of such delays; and to comply with all requirements ofthis Order as soon as possible;

6. If the PVSC finds that: (a) the defendant has compliedwitn the notice requirements of the preceding paragraph and: (b)the d~lay or anticipated delay has been or will be caused by aForce Majeure event, the PVSC shall extend the time for performanceunder this Order no longer than the delay resulting from the ForceMajeure event. If the PVSC determines that: (a) the defendant didnot comply with the notice requirements of the preceding paragraphor; (b) the event causing the delay does not constitute a ForceMajeure event, failure to complete the corrective action underparagraph '2 or to submit any report required hereunder shall be aviolation of the requirements of this Order and subject thedefendant to sanctions under the applicable statutes andregulations. The burden of establishing that any delay is causedby a Force Majeure event rests with the defendant;

General Provisions7. The corrective action undertaken by the defendant

pursuant to this Order shall constitute the penalty for anyviolations of the Categorical pretreatment effluent limitations

-promulgated at 40 C.F.R. It 414 during the period covered by thecompliance schedule. In the event that the defendant completes all

- S' -

866300101

TIERRA-B-004700

· ::'~".,.- . '--'~- .~ ~. -. '

-corrective action on or before the completion dates set forth inthe comJ;lliance schedule, and as modified by any Force Majeureevent, any such exceedances experienced during this period sha11not be subject to additional penalty~

8. The defendant further understands that any exceedance ofthe effluent limitation for discharges of Lead, Zinc and/orcyanide experienced after the final completion date set forth inthe'compliance schedule, shall be subject to further enforcementproce~dings and civi1 penalties.

9. Nothing in this Order shall preclude the PVSC from takingenforcement action against the defendant for matters not set forthherein or in the complaint.

10. All provisions of the Permit shall remain in full forceand effect and are not modified by this Order. The defendantexpressly understands that the compliance requirements contained inthis Order do not modify any provisions of the Permit or any dutiesor liabilities of the defendant thereunder.

11. This Order shall be binding on the defendant, itsassignees and any trustee in bankruptcy or receiver appointedpursuant to a proceeding in law or equity.

12. Defendant shall perform all work conducted pursuant tothis Order in accordance with prevailing professional standards.

13 • This Order shall not relieve the defendant from obtainingand complying with all applicable federal, state and local permits,as well as all applicable statutes and regulations while ~arryingout the obligations imposed by this Order.

'- - 6 -

866300102

TIERRA-B-004701

-

14. The obligations and civil penalties of this Order areimposed pursuant to the police powers of the State for theenforcement of law and the protection of public health, safety,welfare and are not intended to constitute a debt or debts whichmay be limited or discharged in a bankruptcy proceeding.

15. In addition to the PVSC'S statutory and regulatory rightsto enter and inspect, the defendant shall allow the PVSC and itsauthorized repres~ntatives access to its facility at all times forthe p~rpose of monitoring defendant's compliance with this order;

16. The defendant shall make available to the PVSC alltechnical records and contractual documents maintained or createdby the defendant or its contractors in connection with this Order.

17. The PVSC reserves the right to require the defendant totake additional. actions as authorized by law shoul.d the PVSCdetermine that such actions are.necessary to protect human health,the environment or the PVSC system. Nothing in this Order shall.constitute a waiver of any'statutory right of the PVSC to requirethe defendant to undertake such additional.measures should the PVSCdetermine that such measures are necessary, subject to thedefendant's rights under this Order, applicable statutes andregulations.

18. The defendant shall not construe any informal advice,guidance, suggestions or conunents by the PVSC or by person(s)acting on behalf of the PVSC, as relieving the defendant of itsobligation to obtain written approvals as may be required herein,unless such advice, guidance, suggestions or comments by the PVSC

- - 7 -

866300103

TIERRA-B-004702

shall be submitted in writing to the defendant.- 19. The defendant shall give written notice of this Order toI

any successor in interest. prior to transfer of ownership of thefacility which is the sUbject of this Order and shallsLmultaneously verify to the PVSC that such notice has been given.

20. No modification or waiver of this Order shall be validexcept by written amendment duly executed by the defendant and theI?vst.

21. The court shall retain jurisdiction uver the parties tothis action solely for the purpose of enforcing the provisions ofthis Order.

22. The PVSC reserves the right to reopen this case in theevent the Commissioners of the PVSC, at their next available publicmeeting, do not accept the recommendations of the chief counsel toenter into this Consent Order and Final Judgment.

23. This Order does not constitute, nor shall it be used asevidence of the findings of any fact or the admission of any facts,fault or liability on the part of Ehe defendant, nor shall any ofthe alleged violations settled herein be utilized in any way as

-prior violations for the purposes of characterizing any otherviolations, alleged or actual, existing or hereinafter committed.

// ~

~

./. /"'- ,' ..{,.. ., "" ."' ..~'"/ .... . --,' '

Hon. Harry A. Margolis, P.J.Ch.

--. - 8 -

866300104

TIERRA-B-004703

The undersigned hereby consent to the entry of the foregoinqorder, both as to substance and form.

GABRIEL M. AMBROSIO, ESQ.

Dated: ';/)/9Y ohn T. Ambrosio, Esq.Attorneys for the'PVSC

,,\. (


Dated:

Print Name

- print Title , Position

JTA:jaChemical Compounds.con

-.- 9 -

866300105

TIERRA-B-004704

866300106

..

TIERRA-B-004705

"-~' .~,..:.

VIOLATION NOTICEHAZARDOUS MATERIALS REGULATIPNS

ClTY C '':' NEWARK.FIRE DEPARTMENT

1010 lath At . ." Newark. N.J. 07106(2(11) 733·74&5

[2 NOTICE OF VIOLAnON AND ORDERTO TERMINATE

o NON COMPUANCa o COURT ACTION REQUIf,lEO

.~.- ~.81ock: LOI: ~~ _

OW/-;{;FI:.. AGENT:

NlIma H£!(Qld 5ulJ iyl.lOAddrua :-!9-75 Riverside AvenueTo"'''tSlaII/Zlp Na\~arkt NJ 0710~

N,UT',O C1\t'!ni.<.:a.l c:onpouncts/Id.;i,ou ---lJ.-7 5 ~e:rsid'Z Avenue

Towt1/SlataiZp N~·,".'lrJs, NJ 07104·H'-/."pClmll~: _---------~-----

LL, 'r-r'~ ~ ___"

rt~~~~!'= COMPU,"C<DUECAT~ ..':':~;:~,NsPECTION' ':~

.-- .TAKE NOTICE tl1at you have been tour:d to be in viola lion of the City ot Newark OrdInance (6S&FE amended March21.1990) governing hazardous malenals: .

.. .See !:.i.on (3.'1

3CC'.:ion 10.1 5

Soection 12.2

Se::r.iQIl 15 ..L

section 18.4

" you have any ques,lons concernln9 this mattor. please call: ..l,(.r.l20iLJ1L1-).J.z~3a~~ J.:.B:u9t;;S'-- _

H82mal Off.leer OotoCale-L-:. . i Inspoct9r /. /-J. ~I ,,' " I

- .:, "\ .J ' I..'-.;'4~mtt)0 'X· ")' c..._Cffic rill CharQa Fire Prevention &'Safety Date.

866300107

TIERRA-B-004706

...

-NEWARK FIRE DEPARTMENTOFFICE OF KAZAROOUS MATERIAl.s188 Mulberry StreetN(\'\Vl\rlc. New JCnlcy 011.02

STAN1.EY J. KOSSt/P

(20t) 733-7300 Fax (201)733-7~88... •....- ..•....-- ..-..-.- •__ .. ~~._7a _

(:hemkal CompoundslIJ~':5 RivCfSid..: Avellue;-'!n...;~rk,NJ 01104

JIU1UIU)' 10, 1992

;llll:: ;'.11".H:.u·old Sl\lHv;\I~,.'

, --On J<\II\H\ry 7. 19<;l2, rhe Newilrk Fire Depurrment's Hazardous Marerials Unit responded

t(, yel~" facility. Chemical Compounds nt, 29 Rive~id¢ Avenue. The cOlllphlinl regardedill\id\'~n;..~'d!illUid llmving ('mill II hose Iilie (In Ihl: second noor of YOIIl' bl.tHding. down a set of\.:x:l~l'ior.•t.li ..s, 01110 lhe ground and inlO the Passaic River.

Titis actin'n is il violation of the City of Newllrk 's Hl1Zllr<.!ousMllh:finl~ Regulations. You'H·C in violation of the following:

- .'Section 8.4 Drainage fmm produclion (aciliric,;, including buildings, and other proce.n

areas shall be so engincered as to provide a means of secondaryconlaimnent for spilled hazardolls marerials.

~ .Of' •

Process wastewater anq cooling water pipes. plnnr drains nod similarillStclllations which drain inro sewers, s(or.n drains, public wllstewalertreatment plants, wiuercOtirses or other roUles which dmin to waters of thelltate shall be ~Ilgineered so lhul spilJs of hazardous materials wilJ notescape through them to waters of the State, If hazardous materials capturedin secondary cont<linmcnt systemll Qrnin into p~ess wastewater Jines,provisions must be mnde to treat or remove the hazurdou!I materials beforerhe w:ucr is discharged.

011 j anu:u-y 7, 1992, you or (JIIO of your employees diseonnecred a hose line leading imc.1 ". :Ie rccov.~ry truck. The hose line was rerouted. enabling liquid to flow Onto tlnprotcctcd~I\: 'd into Ihe Passaic R.iver .

.-..

866300108.. ' : ..'~---

TIERRA-B-004707

~t.{.ti\ln HUh Ir ~I\i\\lbe untnwful to use or opemlc any bulk :lrornge aL'ell or part thereofwilhll\ll: "

1\ wttS !\oLed thnr oxidi1.ers. (M & T Chromic Acid) 1\r~ sfRcked 011 lOp of corrosives.

(l!.lh)'l4ma ChoIOl"hydrin)

(h) pruviding fm lhe seGregation of potcnti;llly loellctivc chetnicnls

whichlll;\tcri"ls or which !\lity relIct so I\S La fonn ha1.:lrCloulI matcriulll, nnd whichPl'~:;Cl\l or C:lUSC it h;t7.nrc.lo\ll' or dallg~l'UU:l condition.

-

~;cctiOI\ l2.2 All louding.. IIl\lotluing 01' transfer of hi\Zllrdolls Il'Iluerinls shall Lako phlceby u qualified pClllUIl •

.' AU vehicles ilnu mil cnrs clUT)'ing hllzard()L\s 111i\lerii\ls llhall !ltl\l\d or bepn

rkedollly in " secure area where they :U'C~lOdc("the care, custody, Rnd

control uf n Permit holder.

/\ person' who ImtdS or \lI1lo:lds hnznrtlous :naterhtls shall comply with theapplic:\blt; pCOCl'i\1 I:IWS t\Illll-.:glll:lliol\S, in IIddition to any loc:ll and state ,/. .'reqll\remenls.

I\n 1I1\l1\lalificd pl;}l'son disconnected the. hose leading to the waste conlainer, [f the personw", qualWed he would have been required to ~now that rtIC preduet he was discharging onto the

" sroul\l.1 Wl'l~h:l7:\rOolls. .

"

- Section 15,1 111the event of fire. explosion, stntctuml fl\llure, lenkage or olher discharget'e13ting [0 haz.ardous materials requiring notifiCalions under FedCl'lll or Statelaw, the pennit 1'f1lder shull also notify (he l)irector.

The pernlittee shall submit to the Director within ren days a copy of thewritten 1'CP<>l't pursul\nt to the HazardOUS SubsllInce Discharges: • Reportsa.nd Notices Act. NJ.S.A. 13:1K-lS, and regulations promulgated

thereunder. ." I

The ,\pproprintc ;tgcllcies were not notified when the spill, leuk or discharge occurred.'r\\'~\tl:: citizen l'epolted this Incident to dlC State Police.

The pcrmiucc JlhaU also provide inFormlLtiotl to the Director re\l\ting to the:Ihilhy of the pemtince 10cootnin and diSpOse or the hazl\n!ous material,Ihe cslimalcll time it will lUKe 10 complete slOmge itnd dil;pt)Slll, lhe degreeof haz.ard created and the quantity and tYpe of material released. TheOit'ector mny verify that the hazardatls material is being contained andapprnpriurcly disposed.

-866300109

TIERRA-B-004708

-

.-_ ....

:';\'l'lilltl 11.1c Failure ~u almt~. correct or rectify ltny lloncnlllplilll1<,:C' with the provi:lionllo[ chese Regulations uny permil conditions 01' any provi$iollS of lheHa;{':Irdlllls MntCI·it,ls Maungcmcnl Phll1with rho time specified in the Noticeof NOl1cnmplillllcc;

Section 17.3 If the c,tuse of the noncompliance ill not abated. corrected, or rectifiedwithin the time specified in the Notice of Noncompliance, It NOlit.-c ofVil,I:Iriun :-h:\11 h~ ilil;t\CU,

.'

The N"otice of Violanon shall be in writing and shall in'eludea referenceto Ihe originnl Notice ot- NOllccillpHnl1ce, the unconditionnl right to It

hc;\ring anti Ih~ remedial i\CILOllto be ~ndc:rl"ken,

Under t;om.litions of imminent hazard rhe Directoi' may issue a Notice ofVio};uion without issuing n Notice of NOllcumpli.ulce.

St'diOI\ 1'7.J A request (01' n hCilring by lhe pcrmillcl:: shull be giv~1I to che Director illwriting, setting forth in pnnicular any defense the pellTlluce might have inregard to Ihe alleged violations, and j\ brief statement of the factual matters

." in support lhereof. 'nle nOlic~ of dIe hcmring dare shall be given by lheDirector at least ten (0) days prior to the hearing date.

- Section 18.4 Every Pel'l'llil holder shall insure that'a qualified person shall be in chargeat all times and at each and every plKce where hazardous materialsoperations lire catTled om, The 'lualified person shall remain on theprcmi:>es as long a\ ',the mllnufucrurc, lIse processinG. or handling ofhazardous IllRteriuls is being carried our and shall return to the premiseswhen requll'ed LInder emergency CirtllJnlital\CClI. To be il qualified' person,lhe individual shall be knowledgeable in the chemical and physicaltJ(occsses utilized by the rcrmit holder,

.'

The Pennit holdc.r shall furnish to tJle·DifC'.ctor a list of quulified personswith their addresses and telephone numbers to be contacted in the event\)f :\11)1 emcrgency circlimsllInce. to be updated annually. The director shallpreville said pCl'llonncl w'ith p;\Sses 10 be llhown 10 CiLy emergencypersonnel to allow the holder to pass through My manned emergencybarricades Rod enler the perminee facility in the event of I\n emergency.

The person who plnced the hose I~:\ding f..om the building LOIhe ground ltnu into Lhe rivet

<iLL nN r:m:,iJl 00 the premise$, .

-'866300110

...... " •• ' -r •• " ..

TIERRA-B-004709

- S\'c,',ilm 10.2 Whcm:wr ill lIn;:.-e I~l;guhlljonll any aCI Is I'nlhlbitcd 01' 1$1\111duor declaredLo be UII!tlWt\t1, or whenever in these Reglliarlon~ the pcrfOinlance of anyoct. is required or the fnilure to perfoml l\I1y act is made or declured [0 beunlawful, Ihe cCll1llni:;,~ion of IIny lIuch prnhibiled net or the f"HuI'C' 10I'crfunn :\IIY lluch IICI, l'hnll be I)tllli:ihcu by II lint:. OI'Jl(lt more thunSI,()()O.{)() per d;\y per vioilltion or by imprisonmc'l~ for a term of 1101morethml90 dayll, or by :lOy combination of such fine nnd imprisonment. Eachdny allY viulalion of thcNU I~cgul:uiolls CUJltil1ll1.:,slIhall be considered nsepamtc ortensc.

\\1lI have' been fotilld ro b~ ill violation of five secrie)n:; of the City of Newark's

!'"·,,,01"'0; ~""",iul' Regul.,;"",: .....---?Z1ft' h?f1: .!}~!~,,11~.' :J. (;/t';..I [(t-.,. '", ....... i J

l "a; . ,,"(--.~ Oallaliol1 Chief A. Ap(lSlOlico

.'

,":.'\:(11\

..~ '

...

-.866300111

TIERRA-B-004710

-..... _ .... -.

','

:j

,"

'J'i

-

. ,..:,. --':.,;.

NEWARK FIRE DEPARTMENT

OfBce oCHSI23rdous MateriaJs188 Mulbeny- StreetNewark. NJ 07102

StaJueyJ. KossupDirectOr/Fire Chief

}~~~~.

(201) 733-7506 Fax (201) 733-7468

Chemical Compounds. me.29 Riverside AvenueNewark. NJ 07104

Jamuuy 31, 1992

.....;;,..

- ,aM: Mr; tIarold Sullivan

....On January 31, 1992. a reinspection was conducted at your facility on 29 Riverside

Avenue. The purpose of this was to check on the violations issued on January 10. 1992, The'conclusions".of this reinspection are as follows:

" . - -, .

Section 8.4 Drainage from production facilities. including buildings, ' and other process areasshall be so engineered as to provide a means of secondary conrainment for spiikdhazardous materials. Process wastewater and cooling water pipes, plam Jr:.linsand similar installations which drain intO sewers, stonn drains, public wlU;tewateftreattncnt plants. watercourses or c-J!erroutes which drain to waterS of the stateshall be engineered so that spills of h~zardous materials will not esc.1pe tJ1roughthcm to watcrs of the State. If hazardous materials captured in secondarycontainment systems drain into process wastewater lines. provisions must be madeto treat or remove the hazardous matcrials before the water is discharged.

nus VIOLATION HAS BEEN ABATED.

AU internal drains in the building from the first floor have ret:n re-piped, enabling [hemto drain into a 1,000 galJon tank located on the ground floor. Aftcr'the material hill>been PHrested, it is pumped into a hazardous waste trailer.

Section lO.lb providing for the segregation of potentially reactive chemicals which llrehazardous materials or which may react so as to fonn haz.'U'dous materia Is. .tndwhich reaction may present or cause a hazardous or mmgerous condition.

THIS VIOLATION HAS BEEN ABATED..-

The oxidizers, M' & ,..chromic acid., have been relocntcd to a different loc<ltion .11111 are

~o Ion~r "o<~on ~p of==':~7'Y~~~~_866300112

~~., ,~:i..-

TIERRA-B-004711

., ..j

Section 12.2 All loading, unloading or transfer of hazardous materials shaH mke place by aqualified person:

All vehicles and mil cars carrying hazardous materials shall stand or be parkedonty in a. secure nreu where they IU'C under the care, custody, and control of aPermit holder.

A person who loads or unloads hazardous materials shall comply with the.. applicable Federal laws and regulations, in addition to any local and state

requirements.--- THIS VIOLATION HAS BEEN ABATED.

Mr. Sullivan explained that his employees have been trdined. on the unloading and transferof hazardous materials. Mr. Sullivan also stated that in the event of a leak: spill or accident hisemployees will know what to do. I instructed Mr. Sullivan to send me a lener documenting this,to which he agreed: ...

Mr. Sullivan was also infonned that flammable liquids with a flammable rating of threeor more should be stacked no more than two drums high, as we found three drums stacked on

lOp ofeacho~ m me frontnfme bUi;;;a; arI~

Battalion Chief Anthony Apostolico

AA:lm

-._ .

.-- 866300113

TIERRA-B-004712

.\~.' .." ._-- _.----

a- • "_.. ,... '.-

866300114 -,.

TIERRA-B-004713

"' .. It-

Scott A. WeinerComm./sStOner

St3ie of New JerseyDep8'tment af EDYInmmeDtall'Joteetloa. aad Enerv

Division of Rle::spanSb1e Party SJte RemedladonMetro ~ Oftk;e

2 BabcDdt Place .west Orange. NJ 0705%

Tel •• 609-669-3955Fax..20t-669-3993

Karl J. DelaneyDlredDr

Chemical Compounds Inc.29-75 Rivers~de AvenueNewark, NJ 07~04Attn: A.lberto Celleri

February 26, 1992

Dear Mr _ Celleri, ".The New Jersey Department of Environmental Protection and Energyis authorized, pursuant to the New Jersey Spill Compensation andControl Act,··N.J.S.A. 58:l0-23.1~ et seq. to collect all costsassociated with a discharge and incurred by the State in the removalof hazardous substances or mitigation of damages. Accordingly,oversight costs (salary, materials and indirect costs), in the amountof $708.60 were ~neurred by the Department when the Bureau of..Emergency Response responded to an illegal dumping of aceticacid/anhydride which resulted in contamLnation of the ground and thePassaic River on 1/7/92 in Newark, Essex County. CEPE case number

92-0~-07-].025 -Pa~ent of this amount will not relieve the company from potentialliabil~ty for civil or administrative penalties, adait~onal costsincurred by the Department, nor any other responsibility or obligationunder the law, including responsib~lity fer damages which may havebeen caused by the discnarge. Your payment of tftisamount merely.satisfies the Bureau's interest in recovering its actual costs o~ the

above referenced response action.You must submit a check to the cepartment payable to the"Treasurer

istate of New Jersey" with~n 30 days after receipt of thisnotice. P ease send your check and the vhita copy of attached for.:

DEP-062A.to:.New Jersey Department of Environmentalprotection & EnergyBureau of RevenueCN 41.7Trenton~ NJ 08625-0417

yOU may contact Walter Janicek of the Bureau of EmergencyResponse at 20~-669-3955 it you have any questions or require furtherinformation~ ~

866300115

TIERRA-B-004714

. ,

.'.

:.

- ..'

coenenwoQ-a.-a.en

, .

) )

.....---... '. 'J'·~'(;-ii.:-;.;j.~;".:l';;...·)'j:;·:·~vrr'·....·-· ..,....-;-·'0' -" • ~"- ,-.' --, ............. ,t'-~1' ,,· • .,.._.... :-r,;,f~h{;I".·,",•• -I"" . ': ..~

i· .;. ~~. NowJ.... , """'Om" 01.......... '. P.m."", ... Eno.gy """._ • ~

• .:.1$1191

' 'DCheckher.lfR.vtsedBlIllng (ENFORqEMENT INVOICE ) ~::::,e'd _",.' ---------. • 1

I,

IFACILITY 10 NO•

TYPE: 0 FlnllP.nlllly mOos'1 Recovery PROGRAM 10 Nd'. ill qiL!6f.!'07-1 025 .

PI.... ild.nUly, epproprllt.,cllegor':'.l \,Iii)o Cd~nl~ '.,\ IAUlhodl~:'h .il:.. : 0 lriduilrllp~o Local· ',. I 0 RegkJI\a111 oCotnm8rdllloPrtvlle 0Locel . 0Other· ---:-:--;;:=..-~•• I' •• t.~'. I U;'" 'or'.r:r .. IIH,~'-Il !;:;.I)Ul ..... -f:(.,j~!~~==~

~~~~gft!~»~M~\~4;if:::;i::~*$t!f~jh:\;:S1·;i;:::U';j{;;,;;~h~t¥..·e~t!t¥jtj:.··

QlVtslON i·P•S•R•

. . ~' EMERGFlCY RF:SPQN.SE

,I': e.. : - _".,"fl.'tJ!e'tr'MnHi'1'1;~~;niP'o~lli:l8'~I..rl' t~':'~:II'llll','.' ~'~V"·I·"lvl.."".'I. t···' •.• "J·l'1 .•• I ...;•.....

.' " AItdt".1·'f291t,75:'RlvQt'llIida,·Aventle'·" ~'"" I· Nevar:k,N.J 07104

. .p:...1 f·, I: ," I,"f. I :,j':, ,'.(··1 ~

,: I

,"

: ..217/92 ADMINISTRA'l'IVE 005'1' RECOVERY$708.60

• DATE DUE: L (., $70fL 60AMOUNT DUE:'.':. Mak' check plyable 10: T ... ur.... Sletl 01 New J.r .. , MaY 10: NJOEPE. Bur .. u or n.VII'IUI

eN 411. Tr.nton, N.J. 08625-4)417.;1 , ..::,. c(JrY DISTRIsunON: W"f1~ ..R_j"dllC~CIIfIY Yellow· C"""'Oll'1 PUr!. BUrt'Ollo/Rtverlut' Gottklllod- Dltisioll

•."'~.~~a~·:",~J.4·_~~~.i.":":'·':_.4'_"""''''' __ ;''~:''''';'':'''; ..... 'a..••·... -.~_I.:..l..; ......I~._~I •.•_ .••..•• _ ..... "0. • • .... , •. '~ ...... ~.- .....'.:_ ... _h •.. ~

i, . I .

....:.· ..·..:.- ...... .;. • .J.. .... -:...1 ••

: ..

.. "

,'" ;.~. ':, f

: 1: '." ,".~- ...

'. ,

i,.

,".'

)

, '. ~

I~

I'

f ;

:j-r

': ;

, . 1'j ,

i·

TIERRA-B-004715

--... '

,. _~ ••• 'WI

-NEW JERSEY DEPARTMENT OF ENVIRONMENTAL E?ROTECTION AND ENERGY

BUREAU OF EMERGENCY RESPONSEADMINISTRATIVE COST RECOVERY WORK SHEET

PROJECT ACTIVITY I TI:f:

'.'. CASE

I.D.NO. 92-01-07-1025-33Case Name: Chemical Compounds


REGULAR OVE~IMERESPONDER PATE RATE HOURS AMOUNT RATE HOURS AMOUNTM. Garamone 10/92 52.20 4.0 208.80

C. Gibbons 1/7/92 52.20 3,5 182.70

- M. Garamone 1/9/92 52.20 2.0 104.40 (Report)

M. Garamone 1/8/92 52.20 1.0 52.20

M. Garamone 1/9/92 52.20 2.5 130.50Total .- 678.60

Equipment:-4 Draqer Air samplinq tubes - (Acetic Acid) - 4 x 7. 50 sa/ = $30 •00

866300117'"

TIERRA-B-004716

" ° .:" • • " •• _"0.·' +.":~. " :", c'" •.••.

-~ubpaet1a luttS- {Detum

~uptrtnr (ttuurf Df New Jersey10K'

Stab of N,nt JlrsfU ))8.a.toutdlJ Df iBtrnr )

Custodian of RecordsChemicaL Compound, Inc.29-75 Riverside AvenueNewark, NJ

R.J. Hughes Justiee ComplexYouuehcrtbycomtmndedtoappeVl1 25 Market 5tH 4th floor-. Friday"

In 1M-CIty of Trenton on January 24th at 11: 30 AM

to &fve eviden:; ~rorc the Slate Grand JurY ~d you are Oldcred 10 ~pe~ wrthou! prepayment

or witness rec 10d br~, wilh you the followin.c records: -------------:See Attached Schedule "A" '"

".

- If you fal 10 appe3l' iIld produce the said rC(Mds, I warnnt may be Issued tor your arrest

and you may be cNrFd 'With contempt.

~TNESS. the Jb'x:;Inhle $aaUI!l D.·tenae, Jr., ~ of th! ~ CbJrt.

~ 13th ~ ~ January ; 1!~.

I

~~ . assen,L-i,.609) 984-4470

.u~~L,--~ ,(11{9:I. and Oft cll'!hJ-I ICrved It on the withIn named r(4d/ Ll~at ·7r

• 11 •by denver "I' COl'Y to h~

~- ....; ..... -. .~. "

TIERRA-B-004717

-

-

...-..... :

..... "'"

.-

custodiu of RecordsChemical Compound~ rnc~29-75 Riverside AvenueNewark, NJ

--------------------------------SCHEDULE A

1. In answer to this subpoena, the records shall:.a. Be delivered in the same condition and order as they are kept

in the ordinary course of business:a complete inventory shall accompany the records as toexactly what records are contained in each carton or

--envelope; andthe records shall be delivered in a secured carton orenvelope as to protect the records and k~ep them in proper~order.

b.

c.

d. The term "document" shall mean any ORIGINAL WRITING .(handwritten, typed or otherwise reproduced) formal orinformal, in your possession, custody, or control, regardlessof where located and includes, but is not limited to,contracts, agreements, communications, letters, telegrams,regulations, memoranda, surveys, studies, summaries, reports,manifests, brokerage agreements, bills of lading, testanalysis results, notices, announcements, transcripts, fieldnotes, weigh tickets, telephone memoranda, purchase orders,instructions, charges, manuals, brochures, photographs,schedules, price lists, messages, records, invoices, taperecordings, notes of interviews or communications, calendarentries, records of meetings, applications, newspaper andadvertisements, video tapes, information retrieval systems,and any other method of electronic ~torage, and materialprepared for circulation to any past or present division,affiliate, officer, director, employee or agent~ In allcases where originals are not available "documents" also meancopies of original writings and non-identical copies thereof.Without limitation of the term ·control" as used in thepreceding sentence, a document is deemed to be in yourcontrol if you have the right to secure the document or acopy thereof from another source or public or private entityhaving actual possession thereof.

2. All documents reflecting the procedures or instructions foroperating the centrifuge located on the second floor of ChemicalCompound, Inc •., 29-75 Riverside Avenue,. Building 117..

866300119

TIERRA-B-004718

.\

-- .\.' "\

'I.j

. ..~ ~--.----=-.:. "'-...• -. ~-~. '"' ' .. ;" .'" : .

. ,.

3. All documents reflecting the procedures or instructions for thecleaning and draining of the centrifuqe located on the secondfloor of Chemical Compound, Inc., 29-75 Riverside Avenue, Building'17 ..

4. All documents or records reflecting the Chemicals or other :substances which were either mixed in, processed by,.or used l.Ilthe centrifuge (located OD the second floor of Chemical Compound,Inc., 29-75 Riverside Avenue, Bui1di.ng 117) between December 1,1991 and OD or before January 7, 1992. Also included in thisdemand are documents reflecting the schedule that this unit iscl~aned, including the date immediately prior to January 7, 1992.

5. All documents reflecting the disposal of wast~ for the periodDec~er 1, 1991 to January 8, 1992.

6. All documents pertaininq to discharges fram Chemic~l Compound,Inc. or any of.it's facilities, into the Passaic Valley SewerageAuthority, including but not limited to analyqis, correspondenceand operating procedures. •

"

.-

.'~.866300120

TIERRA-B-004719

~ .... c ... ·_. _,.:

.. :: ..

-ROBERT J. OIL TUFO

• nORNEY GENERAl.

~taft of ~££U aJ ers£\!DEPARTMENT OF LAW ANDPUBLJC SAFETY

DIVISION OF CRIMINAL JUSTICECHoelt

RICHARD J. HUGHES JUlIT1CE CDMPI.EXTRENTON. NEW JERSEY 0811250(1011&

TELlPWONe -"lI4·lIlIOQ

ROBERTT. WIHTl!RDIRECTOR

August 18, 1992

'.•

Jonathan H. Roth, Esq.129 Wash!"ngton StreetP.O ..Box 1779Boboken, NJ 087030Dear Mr. Roth:

..Enclased please find copies of the draft Waiver of Indictment

and Trial by Jury and Accusation prepared in accordance with yourJuly 13, 1992 letter. Advise me if you have any changes and I willthen file them and obtain a date with the Court for the plea.

The terms of the plea, pursuant to our recent discussions, arethat Chemical Compounds, Inc. plead guilty to a fourth degree waterpollution violation, N.J.S.A. 58:10A-IOf(3), as contained in theenclosed. The state will. accept a fine of $5,000 for the offenseand Chemical Compounds, Inc.·will provide a check in the amount of$1,760.85 payable to the.Office of the State EnvironmentalProsecutor to be used to purchase a one page advertisement in theGloucester 'raes conveying a positive environmental message.. Thedefendant will not be identified in the advertisement •. '

As soon as r determine from you that this is satisfactory, Iwill schedule a date V!th the Court •.

- ~.~.,~ W. Gl'••~

JWG/dk.Enclosure_.

.... ..,. ----~ .-•. It-i •., ~ ...... ~.•. "" ~ "' ...... __ :.:.._ :,"... -••• '.:--' ...... ~.... -,_ 0. •• "'-:- • • • -' ......... - ...... : -~.... :.:;. --

. >:i.',".:.' ": .,* .: .. ~•.. ..::-..... :- :I.i, ...:.-;.... .' .'::'

·-N."" Jws • ., I. An eQu,1OpportunityEmplo~r 866300121

TIERRA-B-004720

.-"

866300122

.-. SUPERIOR COURT OF NEW JERSEYCOUNn OF ESSEXLAW DIVISION - CRIMINAL

STATE OF NEW JERSEY

v. WAIVER OF INDICTMENT ANDTRIAL BY JURy

CBE,MlCAL COMPOUNDS, INC.

CBEMICALCOMPOUNDS, INC., the above named defendant,charged with unlawful discharge of a pollutant, contrary toN.J.S.A. 58:10A-IOf(3) and N.J.S.A. 58:10A-6a; being advisedthrou~h its agents of the nature of the charges against themand of their right to indictment and trial by jury, herebywaives prosecution by indictment and trial by jury and requests,-to be tried by the Court.

Dated in Newark" New Jersey, this day of, 1992.

Signed and deliveredin the presence o£.. CHEMICAL COMPOUNDS, INC •

By:

Reported By: Approved and accepted on thisday of , 1992,in the presence of the

defendants and in open court.James W. GlassenDeputy AttorneyGenera~

- The Honorable.Tudgeo~ the S"uE.er£orCow:::t.

TIERRA-B-004721

-

- -.

··~C""""" ... ·••.


STATE OF NEW JERSEYACCUSATION

v.CHEMICAL COMPOUNDS, me.

CHEMICAL COMPOUNDS, INC. having been charged underoath with violating the Water_Pollution Control Act and havingin writing waived indictment and trial by jUrt and havingrequested that the Defendant be tried by Accusation by theCourt, and the request having been granted;

DEPUTY ATTORNEY GENERAL JAMES W. GLASSEN, for theState of New Jersey, alleges that

COUNT ONE(Unlawful Discharge of a Pollutant - Fourth Degree)


on or about January :7" 1992, at the City of Newark, in theCounty of Essex, else~here, and within the jurisdiction of thisCourt, did negligently discharge a pollutant into a municipaltreatment works, namely the Passaic Valley Sewerage Commissionsewer syste= in the area of 29-75 Riverside Avenue, Newark,without possessing a valid industrial pretreatment per.mitissued by the Passaic Valley Sewerage commission, that is,CHEMICAL COMPOUNDS, INC. did negligently release, spill, leak,pump, pour, emit, empty or dum2 into the Passaic ValleySewerage Commission. sewer system, wliic:li..l.eadsto'the. Passaic-

,'" '. " .. "." " .~ '. . • 0".'.. ·.:··~:(I-~Z.?")/". .866300123

---~-"~- --- -- ..-.- - ~ .

TIERRA-B-004722

,- .

-

- .

Valley Sewerage Co~ssion sewage treatment worksr which thenflows into waters of the State, a pollutant, namely industrialwastes, without possessing an industrial pretreatment programpermit issued to CHEMICAL COMPOUNDS, INC. by the Passaic vall~ySewerage Commission, contrary to the provisions of N.J.S.A ..58:10A-10f, N.J.S.A. 58:10A-6a, and N.J.S.A. 2C:2-7, andagainst the peace of this State, the government and dignity ofthe same.

ROBERT J. DEL TUFOATTORNEY GENERAL OF NEW JERSEY "..By:-:;J~am-:::-:e-:s~W;-.~G;-:;l-a-s--s--e-n------

Deputy Attorney General

-2- 866300124

TIERRA-B-004723

JONAnfAN H. RO'IKAdmitted in N/. NY, .vA

LAW OFFICESJONATIIAN H. ROTII

U9 WashingtOD SueecP.O. Box 1779

Hoboken, New Jersey 07030

(201) 792-0870Fax: (201) 659-1088

O/CormsttlMARISA Y: PAll.ADlSQ

Itdmi#ed in !iJ. NY, CO

-

August 28, 1992

Mr. Harold E. Sallivan, PresidentChemical Compounds, Inc.29-75 RLverside AvenueNewark, New Jersey 07104Mr. Alberto CelleriChemical Compounds, Inc.29-75 Riverside AvenueNewark, New Jersey 07102Damon R. Sedita, Esq.Schwartz, Tobia & Stanziale22 Crestmont Road

~ Montclair, New Jersey 07042RE: State of Hew Jersey v. Chemical Compounds, IDC. /Draft

Waiver of IndictJDent and Trial by Jury andAccusation

.,

Gentlemen:I enclose herewith correspondence from James W. Glassen,

D.A.G. in addition to Draft.Waiver of Indictment and Trial by Juryand Accusation. Kindly review the $~e and provide me with thebenefit of your comments and/or questions as soon as possible. Theterms of the plea are set forth in Mr. Glassen's letter and are asfollows:

1. Chemical Compounds, Inc. will plead guilty to a 4thDeqree water pollution violation under N.J.S.A. 58:10A-1~f(3) as contained in the enclosed;

2. Chemical Compounds, rnc. will pay a $5,000 fine and$1,760.85 for an environmental. advertisement in theGloucester Times.

866300125---_ ...•-, _ .. ~.. _~ ~. .... t:-':"'_:".~.' __ •••• _, .•• _ .... "•••• 0" .-

TIERRA-B-004724

-

--

THE LAW OFFICES OF JONATHAN H. ROTH

Mr. Baro~d Ew 5u~livan, PresidentMr.. Alberto Celler:iDamon R. Sed.i.ta, Esq.August 28r 1992Page 2

I look forward to hearing from you •.'

--

JHR:slkEncs.

,"

.......

yours,

Roth•.

-~.'.. .

866300126

TIERRA-B-004725

".

CHEMICAL COMPOUNDSt INC.21175 RIVERSIDE AVENUENEWARK. NJ 07104

6235

.septembe,r 9 ;9~

t~~OF~~ ~ ~ N([ I $"SfOOO.OO

Five thousand and 00/00 '•• ,•. ~ .. , •••••••• ~ wi DOLLARS

I

iI8

iI'---_ ....--~---------~-~.-~----_......

CHEMICAL COMPOUNDSt INC.2111&fUVERBlOE AVENUENEWARK, NJ 07104

6236

I $ 1,7~O.B5One thousand seven hundred sixty and 85/00 ........... jIo ....... " •

comCDwoo-N...,

fOR _ ---....

lil-umua

)

TIERRA-B-004726

--

_.

rf! MP 71647

1n1ho~d •4'C County at -Doc..1Iog.. ex...ou.,.,. .......- CIty SIo<Pan ~~ "'" CcIar

NOTICI< • 'ICU MIIG 10 I'\£IlI HOT GUU'Y _ 1'0 CllNTUI' _ ctWlOlE ~ .. -...-,lIllVolf ) DIll'S ~ TO '!HIE IWlIOlCEDFOIl "lOUI -.vwa ..COIOII'. 'i'OUOUSTI«m'V'!HIEQSI(. WHOSEAOlRESS__ ...-IS_ON'" -......orc.t:#'ltlllRNIOIlIlIl", 'ICU ....... lll;;o __ ~rr_1I! 1oEaSSAIlVO'OA 'i'OU;::J,- ~CQlPII"

- You WIt:£. .b~ .e..:.t'--AoQP..-!J / )) 077f /c6~~ _vi 18____ M.

_atQlutl_·· _

CGurt'lolollla-'-....,;.. ~:__----------

1/'/- 7"??SUMMONS .•

866300128

TIERRA-B-004727

·__ .-'- •State of New JerseyDepartment of EnvIroumeatai rrotedfoD and IDergy

Division of Responsible party Site RemediationCNOZ8

Trenton. NJ08625-0028 ,

-Jeanne M. FoxAaing Commissioner

Karl J. DelaneyDIrector

November 30, 19.93

Chemical Compounds Inc.29-75 Rivers~de AvenueNewark, NJ ..0.7102Attn: Alberto celleriDear Mr. Celleri,

The New Jersey Department of Environmental prote~tion and Energyis authorized, pursuant to the New Jers~y Spill Compensation andcontrol Act, N ..1.S.A. 58:10-23.11 et seq. to collect all costsassociated wi~h a discharge and incurred by the state in the removalof hazardous substances or mitigation of damages. Accordingly,oversight costs (salary, materials and indirect costs), in the amountof $866.47 were ~ncurred by the Department when the Bureau of~ Emergency Response responded to a chemical fire at Chemical Compounds'Inc. on 10/5/93 in Newark, Essex county. DEPE case # 93-10-05-0736 &93-10-05-1110. -

pa~ent of this amount will not relieve the company from potentialliabil~ty for civil or administrative penalties, adait~onal costsincurred by the Department, nor any other responsibility, or obligationunder the law, including responsib~lity for damages which may havebeen caus~d by the discharge. Your payment of tnis amount merelysatisfies the Bureau's interest in recovering its actual costs o~ theabove referenced response action.

You must submit a check to the Department payable to theIITreasureri state of New Jersey" with~n 30 days after receipt of thisnotice.- P ease send your check and the white copy of attached formDEP-062A to:.

,..

New Jersey Department of Environmentalprotection & Energy CBureau of Revenue -~~CN 417Trenton, NJ 08625-0417

You may contact Walter Janicek of the Bureau of EmergencyResponse at 201-669-3955 if you have any questions or require furtherinformation.

.",........'

Sincerely,

~~~~ureau of Emergency Response,

~"- "

... ""-".' 866300129

_ _ . .- :--;;,. -.:. "r '-:._ _.•. ::.- •• ~.' .~. ~ •••• ; ~~.~ ~ ~ ; ~ ~ --I.- - _ ~_:"" .'."

TIERRA-B-004728

DEPE.()6!A NllW Jersey Department of Environmental Protection and Energy

~. oChec:khllfe If Revissd Billing ( ENFORCEMENT INVOiCe)

l)oatmcftt/J, __ --

DataRec'dAmOllftl

DIVISIONR~P•S .R•

. 'TYPe:., FACIUTY 10 NO.

FROGRAM EMERGENCY RESPONSE 0 Fin8fPenalty ID Cost Rscoys'Y PROGRAM 10 NO. 93-10-05-1110

Chemical Compounds rnc. PI.... identIty .pproprl.te categOfY:

CaselCompany Name(]County Authority: [] Industrial

Address 29-75 Riverside AvenUe 0Local ' 0Regional e~~Newark, NJ 07102 rEI Private C1Local

. . = Specify

',,'" .DA"T.E:'·(';·; "S,: \rw';;i*;;{mtffm~~i'f,:lj~l~m!!'?!g~l~I~~P~!~~i:®t?~l~tf\W#Jt,%]~~~:1H~~tt*f1fr4~~,!jl~.~!~2~~J,0;;%"1;f.1A 5'5 E·SS:ED~;;,;

-- COST RECOVERY11/12/93 ADMINIS~RATIVE

$866.47

- p

DATE DUE:DECEMBER 30, 1993 .. AMOUNT DUE: 5866 47.

Mallecheck payable to: Treesurllf, State of New Jersey~ Mail to: NJDEPE. Bur.. U of R.venue

eN 417, Trenton, M.J. 08625.0417

copy DISTRlBUTION: Whill!' • Rl!'miltQnCI!' Copy YI!'U- • Comp.",y Pi"k • BUTI!'OU ," RI!'"l!'tflk Goldl!'lIrod· D;";6;0,"

.'

- ."

c

-'. ' 866300130

,.. "., .... .. .". -..- -.

TIERRA-B-004729

.: .

/01-3-73 - /1.:;-0-----NEW JERSEY DEPARTMEN'r OJ!" ENVIRONHE!lTAL PROTECTION AND ENERGY

BUREAC' OF EMERGENCY RESPOHSBADMINISTRATIVE COST RECOVERY WORK SREET

CASE NAME: Chemical CompoundsPAC t V3SR

CASE # 93-10-05-073693-10-05-1110

COS'l CALCULA'l!:rON: $866_4-7

" REG~ O.T.RESPO RATE HOURS OUNT RAT HOURS AMOUNT

B. Doyle N/5/93 64.43 3. o· r 193.29 104.03 0.5 52.01J. Hoyle .10/5/93 60.66 3.0 ,'181.98 97.95 0.5 48.97

~..-.

- ...Req. Total = 375.27 O.T. Total = 100.98

REPORT:B. Doyle "a. 10/5/93 64.43 4.0 257.72

:Report Total = 257.72

EQUXPMENT:.

Item:HazCatOVADraqer Tubes

Amount ...75.0050.00

7.50

Equipment Total ~ 132.50

TOTAI:& AHOmrJ! DUB = Se 66 .47

866300131

TIERRA-B-004730

. '.1

••• : .... "': •• ;.,.. -. ~ _:".~",:"'~:,,-. of' •• ~."'~ •

. ..". :-:..... '~.'

~,"·;f~iwE.009'~-;:;5;,\:~rynt~.:."':~.~:~:"'~-./~1 .

.' : .r;: .~

- ~,:.~~t·:;'j,l~':. \'. . .;:.~. -r"·,. "9~r- . : .

':"-;'~~.~~'~~IDi'i;;~7,·~·O"CE9F\10LA~~~i}~ llt: <J If. __ .._ ..10 NO •.~~.:.;._.:;::..L,;_ :...11._~;"';"'~--- --- --, :~.'..:~~~;~~e:aU FACIUTY' CJ./.:F-.fl1/ CA-~ ,Co fJ1 P (} IAN t)"S-i:jg--~· ... '-G~CP.~ON'~F FACILITY),- 7,--e.;J.;R.~,9 ~ A-I. (II ~Zr~K) I"t .V7 I ,N·

,NAME OF OPERATOR.....8--L-i;1i:~To C;:"L-I-U; - Pfl€.5:I~~-rJ-;-- ','

'1"~

New JeraVY Oepanmem of Environmental Protecdcm and EnelgyDivision of Facility Wide EtIl0lCMlent:

Mew Sureau of Water & Hazardous Wute 61foJalment2. Babcock Placa. West Orange, N.J: .07052-

'. (201)669-3900. ':.' '......

.---- ..-.' . :. You are hereby NOllAEO that during my Inspection of your facility on the above date, the following

alleged violatlon(s) of the Solid Waste Management /ttd, (N.J.SA 13:1E·1 et seq.) and Regulations

(N.J.A.C. 7:26-1 et seq.) promulgated thereunder were observed: These viol8\,iQn(s) have been recorded

as part of the permanent enforcement history of your facililY.

." .~..- ...- ..

Remed1a1 action to correct these violations rn.Ist be initiated immediately and be colJl)leted by. '

o Gr. I4-. 1tJ, . Within fifteen (15) days of receipt of this Notice of VIolation, you

shafl submit Inwriting, to the invest!gatof issuingthis notice at the above address, the correctivemeasuresyou haVe taken to attain compBance. The issuance of this doaJment serves as notice to you that a violatfon

has occurred and does not preclude the Slate of New Jersey, or any of its agencies from initfatlng further

administrative or legal action, or from assessing penalties, with respect to this or other violations. Vio~ns

...~ of these.~Iat~ns.are ~~ by~~ of up to $SO'~.~:~~~~~' .

ill /. ' '~:/J. " , _. . 1.(£ ," '. U;~fv"" ~~

. '. Facility ReceiplJ ~- ... '. ' ~.0MsJ0n d F8ci1ty Wk»EnforclImflllt

.}I~~i~~~'~;~~E:~~£:~:~~:·:__~;:;;. _" ·,_.····.-··_4·.:· .•. _ .~..:- ..; ..... '. .,.' .. ~.. '. '~..... ' ..

-

TIERRA-B-004731

;.'

New Janey Capartmant of Environmental protection and En8fgyDivision 01 Facility Wide Enforcement

Metra Bureau 01 Water & Hazardous Waa1e E"nfarcementZ Babcock Plac». W9lIt Orange, N.J. 01052,

:~.(20~) 669-3900~

"'-'." -

~...NOTICEOF VlOUnON

-

You are herllby NOTIFIED that during my inspection of your facility on the above date. the following

alleged violation(s) of the Solid wast? Management Act, (N.J.S.A. 13:1E·1 et seq.) and Regulations

(N.J.A.C. 7:26-1 et seq.) promulgated thereunder were observed. These violat~n(s) have been recorded•as part of the permanent enforcement history of your facirrty. ,

I '

OE"';~.I~ON. OF VIOe:..':"N r.l;fe.. 7: .2-6 - "1. t;:l) I-i-L;)~'"". ,f.,L-,01¢\'t.~...,Jd I.. 0' . 1. ~"",.u........, ~, ~;I ~IOf. C ( \ '2-. -: Iv" ,l. tJ~ , ?=efl.~ C~/-;",?'...y

j. r.,;) l.J-.:~ t\ """;.I..a P (J k ..)...-A....( J,.. I..

Remedial action to correct these violations truSt be initiated immediately and be completed by

Q c:; I'+ . ., lI- : Within fifteen (15) days of receIpt of this Notice of Violation, you

shall submit in writing, to the investigator issuing this notice at the abo~ address, the corrective measures

you have taken to attain compliance. The issuance of this doalment serves as notice to you that a violation

has occurred and does not precJude the State of New Jersey, or ~ of lis agencies from initiating further --

administrative or legaJ action, or from assessing penalties. with rasped to this or other vlolatlo~s. VIolations

of these regulations are punishable by penalles of up to $50,000 pervioJadon~" .. :..

Facility R

, .'...... 866300133:._. 4.~~~--...·-·...,-- --;"--.-- ~ ...:--- .

TIERRA-B-004732

866300134

..~,.- .. _ i Pi.

TIERRA-B-004733

. ". ,'" .- ..~. "..,,--" .:.~ .... ,;_ ..__ :._--~· ''5" ...... )':lo=== •••:}-

·•'.:.-"

t' ,•..

\

.'

State 0' Ne. JerseyDepartment of Envlronment8J Procectlon

DMslon o"Hazardoul Wate ManagementM8nlfll' S~on

/ : eN 028, Trenton; NJ 08825All block "11_ IFonn d...... lor _ on "II. (12-flncllllypewrftK·1

866300135

1

1 1. T'aIl.pone, 2 ~mpany Nlme .. US a'A 10 Number

, I I I I I , I I I r Io...rRmllOr1e(~p~ (.~'~~~.

e. SraleTI'&IlI./O .'.,< ";!:';r~"'-"-"-k~r';a~~;;t-

JI

iiIit.II!

Il-I

fI'5

i.ll

,., .., J I F." " '::.J".....v....·_';d 12:'0'"

I ;:,_",",,_._",j{~-~:"~~I~ ~:i9J6:i4hl§i

,·1·

I I

1

I

1~~=-=-::=====~~-::::-:=-:::::-:::-:~~::=.:-=:::::-:::::::::-::::7.::::-:-:::~~~~--:------------=A- /2 C:-GCO?, :6. GENERA"'OR'~ C:;ilTlF1CAnON: I hlrlllY ClltCja~ !hll :n. ecnllnlS o/Ihl' con.ig"m"'I'~ /Ully1110Jcc:Jra:'IV ;:uet:""<J leave 'rf

proper ""oping na",. ane .re o;.'lII.ifted. pack.a. mlrlel(!, Ina lll)eled, an., III ill "" "'P_ 1ft prop.r =moiticn ;O':rI/lIflOn cy h,gll'.Qyaccording :0 lIIlpliC30lo i":.mall~" Ill" nlltDNII 9011.m",_ reg\lllllOnL"I am Illrg. Quantity ;."aretor.1 c.ttlfylll.11 have. pro';jram Inpilei 10noducemevolum. 'fId 100000tyofwut.gen_ed to lhl dl9t1e Inl', dllllmined to ce1C0nomicaily praC::caOII ano Ihlt Ihi.. ",IKteCllh'llraC:lC:al)11 metnod ollreeunem. slOraq .. ordllDOMi cutnlnUy ~YailIOIIIOm~ WhICllmlnim,reall'll ,ruenl JnllfulUrelh .. 11to human nealth andlheenYltollm.,,~ OR, it Iam. amlllquemtty g...... to'.1 hi.. madlIgOOG tal'" lIfonto m""mlumy wHII ... n.... tlon lI/'lO:l1t8Cl:Ihe bat Willi rn:anaqlmlnl mlmco :hll ia 'YIIIIDI. 10me ilia thlll can IKon!.

;>.nlltllll-:"1~1C N.m~.':" ..: -r ---- ~ ....

WCII!fI Oly ru,I I I I I

.:.

~ la. iran.ponlr 2 AcKnow'I09I11len' 01R"::llpl ot ue .... &lI

~ P'intldlT"pea Nam.I..

JISiVne

-•

Month tHy Y•.,. CI I I I 1'1 ,

.-- • ~ ri \...J -,..

"..; : .-..".:....;..,.,. ...

VA Fotm~(A ... _IP ... _~ .. _

't _ Ten MAtt Tn _",CNJrDATftIaSIGNATURE AND INFORMATION MUSTSE LEGIBLE ON AU. COMS

TIERRA-B-004734

·1·,. . ...:.'SiI··-;:

iId:2 "j ::..J,..Il:lii=•1a~<-• ••

1~

iitiIJ1fl..·.tI

iII•iI.

1" Ce!NtiIA TOR'S C£IITIFICA liON; I MrwOy I:l~ thai "'t c:on .... " q' ll'Ii. cOO$"lnmenl .... ""Uy aMI ~(ety ~ocri lrY .pn::_ s/lippi"ll n ...... and ..... das,r..cl. pecked. "'tIi<ed. ilia Ial>eIt4. .."a art in «ll .. ~ in P"<lPI" COtHlilion f .... ~011 by IligllW.aylCGO"diog \0 '9Pl~ inlemaliono.l &n4 MtioNlIlO"WlU1lont '~U1"_ ,'. . . , '. .Ifl ...... "'~.ll...rmly~, re.r1ity_1 h.... PfOll .... in plel»IO rHucemc .oIumetndlQkleilY ~ln'~~';;"'''''Jolh.~,,,,,, Ii d" •• mh\H 1Oll$ .

'. KO<><>m....... ~ ~_r IaClH__ ctlC_mflIlo<l Oltl'l.tm-. .,o,...,..Ot'is_~.¥aila~lOm.""'ch ......nlrnlz _t_: !uIuT. lllrul 10!tuman h_enc:l1ha m 1'Oft<I*1t 011,111..... ""oil ~uMllily g"'*!&Icr,1 ~ .. m_ .gooN 1aIlI'1~1o ..... imiq",y_' ~onll1!l-"'«

~.~~".'-~I, __ thal~ ••• tlabJ:'IO""~1II11 Qo\.t1DN. ~.'"., _ " :, , .. :-..-::. .. :: ::. .,;,., .. c __ .

866300136

TIERRA-B-004735

-,CI

IIE.~1:tfie.I•if~~.!

II aI.. II

I ..Ito', II...

I' T0

"i II

f..;:ti1....-

;,tI.•1f,•..II!•I'5

iJ

"

--

'11. US OoT Owcription (~,.,.". S/Iipping N_. HUWau.. .-.d 10 N~~M- - --

...

11.-

-0- ~.'.'

.....:

~._lalR& AND INFOR ..... TION 1lU8T8£

866300137

TIERRA-B-004736

-I-t!;,:;:..i'l::IirB~L·JI:..i..1:',Q '.-i \z .-~J~.

"

~f-It~t-:-'~-+::-~~~~~~..e..--f,.'o7--+-~=-..L.:::>o.--t~t...+':-~~.u.w~~Cl!~...To,,~+....;.+-:-,-...,...._-,- "";~ "";"";~L-wf--J~-!.-'--.l.-.L-+~-+;~~~~

----------

866300138

TIERRA-B-004737

FRO'1 CHEM WRSTE tU

_.

866300139

TIERRA-B-004738

P.03

-i{I:!

*i~!!.!..iI

I Q

r:J "• ri ~

! ..T

01; ~'t! '."'!.-.;zi•I' "w ..··~

11, US DOT o.:.,,~ (Inctud~ Ptw-$hJppI1Ig 1Wrr .. H.unf eu... ~""10 NumM!r/: IiN', - ,',..' . ....

b.-

866300140

TIERRA-B-004739

-.eo, IMV,IIIII

-:f; Slale of New Jerse,Department of Envlronmenta Protection

\ Dlvl.lon of Huardous W.. te Management. ~ Manlf •• t Section ..• - ~~~~~m~

P1o_type 0. flllnlln blocll .. lt.oft. (Form d.. IQnlld 10. UN on .111. (12-pltchllyJMwrllorl

866300141

..§~[I:II!!

f.!iiit1I·i!~·I';•is ~

- I

il!:~ I= ,I I-;e. I! I

~ !Ii: .-

~ :!g I

I a.. !! ~~ !I ~"0 ......S ;

0~ ~......~ ,,~ :! i_ .

b.

If!!~..,-/fA> ZA R. ",,'-' 5 rE.j2- LIS noli I:I Dfle JU",-r; £7 i·, ,1' '-1-1

~It !

15. Specw H.neling In~ltUctlon&!nd....<l<lltionallnronn.lion.. V' .., I~.' ·:,:{;,.li ~. -:2' LJ'-' ;;.., - .. ~......,..n- - ~........- r ........

D IE 1!..Ii 'i."ti 1"2 g Sb

i S~n.tu ••

I.'.Ionrn C~y '1'•• ,

I~/ ,;.11911'-. ~. r;a.r::spor.er 1 ACl{nowledgement of Receipt of Maten ...~A-M

~1-:-:~~:==::l~-f::~-7:'::~,:::!:::;;;=:::::~=::;:---_":---:;;-""''''';;;:;=----:,-'-:;'-''-:'''-;~-----_.J:::::~..u)..L~!.LI1a ,a.~TI~

ISlgnat\;.~ I'l~

J'"ISignaNA

.tJonrn a.'1 Y..,

101II < II II)r1 •• # •

!.Iontll Day '1'_«I I I I I I ~

P"ntl<llTy"e<l Name·' " ..•

ITa. ck ;;-tY'/tTrVT"nopon.r 2 "'c~no_o.moim of R.coilll at Mllfi1&1oPrlnll<llTyplld Name

Ci.c:repancy Inc2ic.atlon Spece .. ~.. r

".(

- ....- .

I.IontIl O.y YHi'

I I I I I ,

1

+ h:20::-.~f::':O:-::C::':'h~'Iy':"o;:;::",::n.::r:-:o::,-::o:;-:Il:-::.::ra::to::r:::.';:ce::=rtJ1:::· icI=u7::cn:':"::O:;,,"::,..,.=,:::·p:;"t:o,iil\:::uatdou:;;;:::::';:o:-:ma:::t::on::o:-;:lo~C::r:IV=_=;:by:-::t/I:::io:-:m="':::if;:Hl::-:.::l<U:::P:;"1u:::-:n::o:::le<1=-:In::-::llam==~l:::8.-----------~

, PMlfldlTypecl Nome • ISl4na1Ul'e" . 0" -

El'A Fcnn 1700-ZlIII .. , W~I p_ .,done ON_B-GENERATORCOPY

SIGNATURE AND INFORMAl10N MUST BE L£GIBLE ON ALL COPIES

TIERRA-B-004740

i!....E·,:,.......;;..ei'Q

i 0";WIWI J.. ..:;~=-e..1 Q£ IE:; "I I

~0 Ai T"... ()'S "..II.,;;z,5...

5. r,.nsporterl Company Name,'. ", ;•. ,

(;:f :J":'''''';~olC. .j;;:'~~~~;;:~::_I.;.j;;7. 1,... aporte,2 Company Ne,... .... :;-<:,.::. ',.,

;..,. '". ,~, .. (",,:.~~:_:~,,~--.:::-.; .

11. US DOT O.. criotloa.fI"CI~d;"Q Prop.~ Shipping NMTll. Huard Clm ."d 10 Numbflrj '.•nM . " . '

..b.

">.,

d.

.': .........

.. ... ~.- -:.....; _.,/

~e. Gl:NERATOR'S CERTIFiCATION: IlIe,el>'( declare II'I&llI\e conlenla 01 this con'iIlnmenlar Ily and accurately descrioed aoove byoro:>tr ,hipping nam. and aro cJaaallied. pac~ed, mart<ed. and labeled. and aro in all .... pecta in pr~e, condilion lor uan.pon by h,ghwayaccorcllng to apPlIcable Internatione. and n~t1onal gQllemmenc r.gulallona. 'If I am 51arge quantity qaneratbr.1 certify that (havee prOll"mIn placa to roducelheYDluma e"d toxicity of wllte generated to tho degree' have dalermined to oaoconomically procticaOI. and Ihlll have ,elected the p"etlcable mothod oft,.al11'lant slO"ge, 0' dispo .. l currently avallaOle to mo which minlmi .. a Ihe p,e,.,.t andlulu,. Ih,eat to human health and the envlronme~t: OR, ill am a 'mall quanllty g..,eralor,1 h&va made e good faith affort to minimize my waata gene"lio" and .. IeelIho il.ol WOIlo monogamont molllod thollo a.allablo 10 me and thai I can alford. .. , . .

T 17.~.toIIap0 18.."TI ~>.r.~

18•

.. , EPA F.n1I t~.a; (~".1I8!I1~ odl\l4M .... ~ ..:_."..... I'!'.""U 1~ rnDV

TIERRA-B-004741

-

Slale of New JaBerDepartment 01 Environment. Protection

Division of Haurdou.Waata Management, . Manlf .. t Section

866300143

.' ,., .r:I ' '\-1~ i d.

~ I!

..-,a....":! ocanomlully PfllCll

cab1, Ind ttl'll hi'" ... llCIed tho pra cabl, m,ttlod 0 tl1l'lmon~ ,IOflg6. ordl,pOoa currently a.liloblolo me whictl mlnlmll" Ihl plMOfl

l

fUlurolhrut 10 human hulth and the In.lronm""~ OR, II I am I.mall qUlnll1y gonlrator,l hav.made I good 'Illtletfort 10.minimize myw .. le gen,rallon UI.d II

Ih. bo.1 waet. management method that I, availabl.IO m. and thlt I can afford ... ' ':. . . - . " .- ". ··f.::~·,;~.,/:'.Il:i!~J~~'

TSlg~ IJ 17 ~ -, ';'jJ~:-:: c".;·r.!~~-~th:1~

(Y/l f7 J.J' C~ A J J l'P"I~'~';';' -'\· ....:'1~:z.1-:'-i101~.-•..~~:..,.-,i'"\ .._-~.~:;i-: ~~~:.,\,;

:-_ MMIh;.-'o.y1-:: 'i'-j -:(.1"rt~Mp<>rte, \ Acknowledgemenl 01 Aeceipt of "'allf1a. ISIgMaIU",

HI. ,,,n'oonor 2 Acknowl,dgement Of Rocolpl olldl"""W

.,Print.edfT'yp~ !'I_I.. ~,,', ~.

III. Oiocrep"ncy Indlcetlon SpecI

I.- F~CI~I-"':"";"---";"';;~-";"'--"""--"'----';'~';""'--"""'--"""'-"""'-----------~";'~";:::';':~;';';';;;';;'~~ ,20 •. Focility 0..,,"- or Opel.lor. CartlUcallon 01 ,..,.Ipl 01 hUlrdouo mOI./loll cove/ad by lilts man II... I.C.pl II nOlad In It.m 111. ~~1-?'-:{~~~y ~nl8<l/T.J.pecj N-.n.....,;.;,;..,~~;<:li." ':.'" • \S1grnltllfl .-. ';:.' .. ,1''-'' ~~"W-:~AlMtflt.!Da"

:", :.~~_~~mM,;:;~;:a';'~'.::;-.:"L.c.:, - ~:.\:",.~":I.~a~:,:i'~~·~·~·.. ' :.~

TIERRA-B-004742

is;;;l!l

.~

>:..e.!WI.:.lI:I;;;-[,; 1i.Q

'"III 0 ..£ E

~ ..E

i A ~,

J.-e r..... a*"-0 R

t e.-

o I-iz:

J.

d.

I·

wS.OO7 Oescription ilrrCJu,ji~gPr.;;p.rStll~pl';9.Nllm", Hsza~dClass,snd;O "'"mOtlr)rj,M - ,. ..~~ -",:-": :: '_r_o

':"""

...~§r~I.J..i!'!..i1Ii~i·eoI..i'0

, I:'}.: .I~.'"

j .-

b.

i :i ",I,

'!..

ii I ~.I ~s.IIII ',6,iIIIIIrRANSPaIIT•R

:...; .'

SpOCIa.1Hanolinq. [rl.Jltuctlon, and Addjlion:;llnJao~IIUon

,. ;',_i- :'i:. .•j:_ 71- ti-J '7>.j 7 '.~

.::'GENERATOR'S CERTIFICATION' I herelly declare thet tM contenl' of this conSIgnment arofully and accurately r1~crt~od abov. byprops:- :it1:;}plr",gni!r':'\-=and aro clawilil1d. pack&d. markea. and laolled. &ll\J .iltl ill sll respects in proper condj~Ofl iOl transport bY. nighwlYaccordin. to appllcaole international and nationalllOvernment rB\lulation.. "IIlam e la,ge quantilY9anorator;1 cenily'hall hevea programln place to reducethevolume and 10xICIty01wule gene,aledto the deg'H Ihavedelermined 10b.economIcally practicable and that Ihave ,elec1ed t.... practicable method ollr.otment, storage. or dispooalCtJr",ntly available to me which minimize. tn. present""clutul. throat to human heall~ and Ihe .nvironme~r, OR, ill om a 'mall quen'i~eneralor. Iheve mad. I good faitllelfon \0 minimize my ",esle g.nerluon lItId seiee:Ihe be'l wa.te managomenl m~lhod thaI Is .ve,lable to me a"d that I can ord. . _. -.".. ~ .. .:. :, .

TIERRA-B-004743

.,

=.....!......;.,:;:.-..ie..·e-o..'"'"~~'P(;.

!r!.0

'"..· ::'§... f

! N

j fR4

.5 ";"

0OS R~·Q-;

-""-

- ,.

11. US DOT D~,cripllon (Inc/udlflg Proper Shi,;;'lng Nomo, Ha:ar,iCla$$. or.d ID NlJir.tNt;HM

a. I

II

/r "

:. ii,

"J""] I ... /.;;

..,..:<.., :! .:.:.,'C

:6, CENEJ'lATOR'S CERTlFICA nON; j .h.ereby declare thaI tn. conte"t. ollhi. Co~,i9"mo"t ar .. I'Jlly a"o accur.le'y o.scrib.d abovo 0,",cpcr :~ipr.-Ir.g".ma alK! aro c~sSlf,ltd. packlld. ma",ed •• "0 loooleo. ano .ra In &1,1relpect$ ,n proper condlUon lor Iransport by highWayaccording 10 appllcabla inl.rnalional and natlon.lllovernm ..nl regula_.III am a la~9 quantity generalor. Icertlly Ihal I heve • pr"'lram in place 10roduce Ihe volume and lo.icity oj wIOta gentnlleo 10the degr" Ih... oeterminlld 10b~economically praclicable and Thall have .. I.cled the o~etlC3bJe meThod oftrealmenl, .lorage. ordosp05l1 currently availabl~l~ mewh,cn minimizeslhe preaentandiUlure U".al 10human neallh andlhe envtronment, OA,.' Iam asmaUquanl,lyganerator,I havamadeallooola,Ihellontom'mmlze myw •• legeneraUon lI1dselectthe best 'NIlSle management method thaI i. avaUable 10 me and that I can allord. . .

.,": .;...:.-:~T'~.'·

,_ ~..:: ,:, ....

TIERRA-B-004744

.,

.:;-'~·'/I·~U.todtUoni ao.oallCo •.

.• • .• ,..I·~I .... - _: ••• : •

.. ,; ; - TSD'S.STATE-'0·.

-'-'

TIERRA-B-004745

....-

866300147

i.5..Ii&..5~~5'liu

iiIIgo

f.i'0,IIS

III

~ I I : i : ! i i :' :

I,

i.!l! b.

...("':,4..;.. 'r&"~l .

:;; ,:_ ..... J ....:."

G~Nt.:I;,.~r~R'S C'S,RTJFICAT10N: i~·tr~bY d8Cla(~~r]~ !."!! t:on:31~~'c~~hi, t;O~~9~m'!nt iire !uily andaCCIJl·at.eIYcos:ricf'd aco'fl!' b~'"1"C;;d! 'l~;::;.;;.-:;;.l,ano'if' um,: .f'\: ':"~:.!:~~'h:r1.;,c~~,",,- ;;~lr1t~. ar~:J I=.:..-!;-O: .;.&.,d .,.r;a Ih 1],: ;-31~""~f:'"l'1""::-""~r'!.ii:IO,:'\ for :ra."l.1~c.r:.:t': ~i~:-:·""..t;*Iccor:!in9 fOap~ticabl~ interna-Lion.1and n.tlQn.~ ~?""Qrn.JTI.ntNtgu,attOf'l'.III sm .'.'0" 111anlity generator,l certify that I have a program In place!O roduC8lhe,oiume and lox",ityolwaalagen.rated IOlhe deg"", I hive determined to ".tConcmic311'" practicable and.".' 1have S;illected t.~or~c:iC.:Jblerr.~lhot:l of ~realment. storage. ordfsposaJCUn~ntlY ~IHable: I~ ~lJwhicn minimtlOS the pr~tar ..:::rctureUue!t t~ human hea:tn and 1heetWlrC?nml-:'t. OR,I1. am a 'Small -etu.;l.ntltygene,ator.1 have mad •• ejOOCl:faith .ff0r'!to mlnlmlr& my wQ,tec;eneratiot't .anc1SQlill!"C:"th. tesl wasle mar.a~lmenl melnoc lhlt" l,alleell!O me and thle I can IHoro. .' , : ;

• .5

Name ~JII .'.''f "J; /-/~,;'I'IZ+

Transpon.r 2'Acknowledgam8f1t 01 Re<:tIlllt'Pl Materials

PrintedlTyp<lO Name ,:~f,,::.' ' ,:.-'~;""'",~. .... ISl9nl\l.lre

-- ;g. DiscnIllltlC'J Indiullon Sptlc.. ··f~i:. '.~'-; ...,-:',',"-

...... ' ..

TIERRA-B-004746

:.. ..-'~ -~---- ..

866300148

I'....~..ii

'0:'s-31

H....!~..i.t'3

I.~.Ii'0..ta'i~

.Ii

--1..l!i :&•·=I-aa'!fI-!-•ir•:Ii'lI

!.!I_.

15, GENERATOR'S CERTIFI~TlON; I ll.. et:y dllCl.~ ..~!..,.,.."nl.,,13 ¢f this ccn .. ~nmonl 3ro ~lIy and iCC"r3tely c:esc"il"d aMv. eyproper $~.lpPlng n.a"'. and are claulfled, ple~ed. minced. lnd !abeied, Imi Ir. inaJl respects in ore"er condition tor trans~(t by n<gh"'"y3ecorCnlllo applicable mtemattor.aJ Ind nilianal ~o,.,"m.nt regujatlo~.. '..' . . • ' _ •.

. .If.!~ a Ilrgo qulntily-g.e<1enl1or.1 comly Ihl1l na,. I program in placo to roduca thnalum. and toxic:tyol wuta lIaneraled 10 the dogr ... l hav,; delermlnlHtlO be.. 8<:onomlcaJly practleacle and that I have seritc1ed the cr.ct,cable melhod 01lr6Ilmonl. slorag., or dispoul cu~nlly I,ailablela ma·whic:>minimizes the pruantancl. future tnreat 10nurr.an hal.ltf'lar:c.tne ~ironmem: OAI ~fI am 8 smllU quantity ;-Dn.ralor.1 have made. ~cod faith effort to minim:i.z:emy waSil genel'1ltion end •• "ct

:he bBsI'",asr.e mar13~er.1.r:t ~.tnod ttiJt i,J\lallaoie to me .ana t"at I C:ln afford... .

iII!,;I---..,=--~-=--:-~--------~------;-:;-===--_-::'--"':":"'"-----------~-""--':"'--""""-P<lnl8Q/T~pll<l ~amo •

'Q !\~<'lTn,. ~Mcnlh o.y y~.-

to!)I ... 1,2~-'_'---~." .T 17. i'rll'lScorter 1 ACknOwtea-;ementot tlec:trOl 01 M4'1:enloj,

~ Prf·Jd'TIPed Name"" L11~; ~,,,,~ ~ .1<':"

Monlh O.y Ye.'

I J'L ~ il ;'l9~';; 18, Transpana,2 ACkno.,.M._er.r 01 RllCeiol at Mltoriala~~::-:~::::~..:.;.;=.:.:..:...;.;,::.:-~----.:..:...;-------~---.,-;::------------------------i prJnI,;fy~ ~am. . , ..' _ _ . __

Mandl O.y._ YUt

I I I : I I

19, Oiscrepancy Indic311cn Space .,-......... ._ •••• - -~----~-_ ... ,~- .... _.- -- .' - .. ~ .... ~_ ••• -j "-- •• _.~-.---"'~- "'-

r - .. .' _.. ,. ;'. ,. ,.'"- ,-• - '. - .- , .- ".-.,.

~ :'<. ..J -..., :;".-...-,~;~-:~~ "::'J';'r-; -_. - - .-_.-. - -,,---,_., ::L --_.,;]J ~ ../-< T:(~?/""'CiJC:-"';":'- u· - - ~~ -... - • • . .. -.

-_..~-_.~ ..

.-...;

Month . D4y ~ Y.. "-·,I;I?lh;.. ..~l·--. ,

SIGNA'TI1RE-AND INFORMATION AtUSTBE L£GIBL! ON AUrCOPIESV...Fonn 47OG-<2l~.'W8I1 P........UlIOd'_ .... 0_\8.

3'- TSD'MAiLTO ~G'aiERATOR'

TIERRA-B-004747

-

.:,,>-.

+ - .I.... ~..~~ .// ..... ~.to: :

866300149,:;- ....,.

7. ..-9.

C!m..'UO.L .nASTZ ~1ANAGEHENT OF110 LISTER Ave.; -~~ 11" ~ 'r.l'~ r!T."·r 1'1 ~, ,., c:

.... Jr .....•·WateN;"1t. US DOT CescMptie~ ('ncl"ci"g Proper Sf1lcr:in;; Name. l-Iaz3rd C:ass. 311<110 .Wm:>."

HM -

j...,.i-.\ !

qfsA 01 a~7Cl-i-lli~.s.DOUS O"IE ~~110..5'3.NO':" F.2CD1\LT~~· SY ..9CYR

-~ l,C'"

-·(~·~;r-:

~Id.

16. C:"NEllATOR'S C:::RTlFIC,\TlON; I hereOy eellre Il:allh • .:01".1'1' 01 tn,s cor,s;Qn"'ent sre lully anc acc .. rtll~' o~ribe<l aco.e OV.rcper &h'!lpin~ .,ama ana .r. cta • .,lled. packed. marMed. and I.celed, ana a in III re.peeu 'I' proper cendll'on for transc:ort tly hl9n ....aYaccoroinll to ~plicac,e inlematicnal ana national llo•• rrmenl r~U'aliOns. .• .If Iam a large quantity gan.ralor,1 certify Ihlt I ha •• a crtlllnm in ;>I.c.lo redllClI tIl•• olum. ar.d lexiclty ar....Ut. ,.n.ralea :0 the oagr.e' hi •• O.l.rmlned to tleeconomically prac:icaole ana :/1.III'I ... e &elec:.e<llh. Pnlcticable method of lreatment, .Ionllle, '>r ai>posal ClJrTenllyIVIi/ae .. to ma whIch minimlZH the pnlum ar.dhllurelhr •• UO human health;l1lo Iheenvironment OR.,11 am a small quar,:llylle".ralor,I haw mADIIllC'Od failh Itlortto minimizl my wasl,,~anlratlon and HlectIhl oesl westa managemenl melhOCllhall. a.lflaof. to me Ind Ihat I can INo..." ,

MOr.ttr =.y (of .... ;

1-:11 • II ;I: i

I SiC~·~h.:te •, ;/ r( I

.~

Ei'A F...-rno..Z (A... .llIBlI P ......... odi_ --

3 - TSD MAIL TO· GENERATOR

TIERRA-B-004748

ie:::2:

iie.!....~.

•866300150

~UCAL- w~STE ~lANAGEHEm OF110 LISTER Ave.; - .:-R"'n v .~~c;~"'t'V 0'7' "'C:.

I

I No.11. US OCT ;:;&$crj~llc~ ;lncl"C!:rg Pro;:sr Sh;Ol'inr;;Name •. "IiU3rd C:aS$. ~n<110 Num()sn

HI.l -

~7C-1-i-U.,i\V..5.DOli S OY 3 Vi7&...S{ai'A'!:'""'.:3.nOT ~.2C'UM..T:::D ;S~ 49~

. -~r, ,.' ~••• _~. •

a~al aN!~~rI)Af--.:+_+- -;----:-----------------~L..J.--'-___+-l..-L+....!..-..l-..:....-+_---i~...l..-...:.r:4r:..:..

b. I

I~I I

::"\0 ....

I .- .;;~~.;;t;.~I

I IQ.

15. Special HM1<1linll,ns\llJclJon, ,na Acallional InlormallOl'l

lS. GENERATOR'S C.ERTifIC.\,TION: I hereby -etelare :t:.ac ~hfJ .:;onttmts ot tnis Gonsor;nrr.en.t are (I"I;U'1and 3cc:...raUtW oe.scribttd 800"e bYp(~iPer,r.lopin .. ;'lame .1r.;J Ire tlas:sifi.d. packed, milt1f.ed, and Iiteled ..ana u't In a,l respects in prc?"t c::naition tor transport C-vhj9~wayIccoro,ng'IO applic:aol. inllfn2ticn'I anc ~ationaJ lla.errmeot regullticnl. - -.... .II I am a laroe qUlll1t1lygene",tor. r e.ortl1ylnall ha.e.cro ...ram in al'c, 10 ",duco.h •• olum.,r.d toxidlyolwlSle'lntrlt,a:o the"lI9reel ha •• ollermlnI<lIO ~economically prac:LCaole and :hat llulva .... ec:e<l tna prsc:.cable metnod 01 'rllunan .. 'lcrs ..e. "dbpo.el cu"antly ,vallatle to me which mir.imr:a. the present 'I'dfulurell1rOll to human he,lIh ana th' environment OR .. ' I an: a ,m~1 quar.:Jty. ..onarator.1 have mace, goad lalth eHOrl to minimize my waste ..e"eralion InO_lthe O<I.twaste manag.merll m'tIlOll tnall. av,ileolel0 me ,nd l1Iat I can ellord. .

I Si .. "a!~r.;/ r(

Mer.t.? =.y le."j'~I • ~~ j

.;1~...;;:.:::.~~~-:.:..::.:........:...----------;'7'::=::::-::~------;~--------:-:---=--..."..--K

::--:::-::-~~4!?¥.:7:~t:f:.B~~:;:;-;:;:;:::::::---.:....--...:r-~:O::"'''l''''"!''~~~~-==----..L;;~LJ.l.~~~r-::::....::-=~=_=:=~;.:.:.:~~~.:...;"";;....:--~....:---..,..-;:-:==::::-;;---------------:-:--~.:...:..,,.......JTaa

0.... Ye.r'4'1...1

..... I'Oe ... Y"'I:I .::1-

/

EPAF...-700-U (~"'.,ilDIII P........ odJUono -_ ....

3 - TSD MAIL TO. GENERATOR

TIERRA-B-004749

...".. " ''''',01 N_ J,n'r. .. ~ . .it Depar1ment of Environmenta ProtecUan

) : ~ Division of Haxardous Waite Management~ . Manlfest Section

, .. '. ..i."'.. • eN 028, Trenton, NJ 08625Pl.... type orp~nlln bloct t.I1.... (Formd•• llln.d '0. us. on .nt. (12·pllc:h)Iyp.wrtl., 1

-Is0:-..l!:

i,~

e.Ii:II.....IiI G

!

:! II

I !II.A

i T0

'0 II..J.... Ia.; IZ I! i..-~~'

i. II Ii l...I I

I

! I!Ii j

~ \.....

I III

~ \II

ii ,• ~i A

H'1 sS p.. 0u ~S

!II.

.-

866300151

Form Appro~. OMe No. ~o-oo:J9 E,APJl8390:.

. UNIFORM HAZARDOUS 11:. ~~IO~S U,S EPA IO.~t1., ~', ·Doc"'u"m",.·I~.tINtI.2. Pagel '. II,nlorm11'.0. n in. lhd• s.!'aae<lFaf.,.WASTE MANIFEST n i1 1\\ /1", A'lll-i.:1 J 1..,171''71:t:';'j"~r' .1.... 01'/ '" ':w.no

, r.qu~ •• ,... y Ide'

9. O.'"\lnalelrFacllity Name and Site Aaar_ 10. US cPA 10 Numter _ .. -', " ,. ,<. - •. " . - .'.-

C,,,r:;fljC~-'" ;v'A~r" /'!4.J~E..;"'.~.,jf ._.;-:·V~~ ::J.;;I!~C/lt"lt' F,Transporter'.Phone( 'I .:. i':J,. '. ~. v ~ -- G. Stal. Facility's 10

/_';;' ......~ ,.:: ," .....",.~. , I ... .,'. ~ t-:-:--;=:=::-;:~~-7---:---:~--':----" _ ., •..,:" _ j_ .., ""'? ,...,_ :'J/'1''1-''171-4'111 11.'1"71 T,j" H.Facilil·/sPhone( ~"'f) t..',~r::"'"..:.:!1,.;. _, . .. ," - 112. C~n",,"ef':ll ,. 13. I u'n41:t i . . I

11. US OCT Oe,cnplion (Including Prepe' Shipping N.m.:. H:uarrJ C:.ss. ana 10 N~mbl') I To.al r I WaSle No,HM _ No. Type, Quanllt'l WI/Voi

...1

~~ I - _ I ! ,," I I I

I ! I j I i I I I i I I" r~ \ \

I I I...~·I I I I I .'1." (·~·I··

f !..-: .-'..f-_"" ;,i.l~ w A!.:!:!. ;:.;- -, -:":::J;>~ _'" " ,... ... ,... I..... ~1.......,-:..~- .:- ":"

cl.

is. Spec:al Hano~ingInsUu~lons and AcaitlonallrltOrmation• I -i:-' ~ ::;::; qr.LO.,l"..l c,:. j..:.. '~f~~: ~e.... w- ~ - .-, .

...,---- .'

n.-:=: .~ '7""7- =t. I t'1",i16. GENERA iDR'S CERTlFIC,\ TleN: I h.,ety ::ocia", :hal ~~. centen\! ,)j :nls consl~nm.nt arl tUlly ano acc~ralelY cescrlb<!d aoove ~y

. prc~er 3hl"plng 1"l3me ana JfI!l c~assltl'Q. p3ckeCI. marKed. ar.o 1aceted; ana ar. in aU (espe(:ts in proper c=nd~tion tor ttan:s;oort bV nl,':'wayacco:.rcing to applicable lr:ternallona~ and national gC'/l!Imm.nl :-89uI3UOns.III am ala,,.. quanlity ~enlralc,.1 clrtify lhall have a pro.'r:Jm in piece to re<luce ml volume end laxi<:ityolwule ~ene.ate<lto the degreel hev.detennined to~.eco.nomicallypractic.1Dl6 IIInd that I ha ....e selected the e-f1I.(:tJe::tbl.mettlod o1;reet."Tlent, !ilora-ql. orditP091 cu.,.-entfy ava~la~e 10me wnicn mlnirn'zelll the- prese-nt 30atuture th.eallO humen nealth end the anvironment. OR, ,11am a small Quantlty,?ceneralor.1 hev. meet e gOOdfaIth .IIort to minimize my WIU1I generaDOn ana .. lOCIIhe beat wasla·manegem.nl melned \het is avo,laol. 10.m. eno lnat I can e ord.

~7. 7rlnl~oner' Acxnow1tteg.,-rn",nl of t=I'&¢~ipt J); Mater.:::us - -----:- '. .c. ... -Month CI1y 'fa;;

1~~I'91.ld-Lpnnl.dI~YF'elI Name \--l -"J . t:' ,... ~_ ,'-_ .... ~- -... .

It8. ' Tran.pone. 2"Acl<nOw,eaglm.nt 01 Receipt 01 'VIal.nab ISignalureMonrtl O.y rUf

I I I I I !PrintedITyped Name

,~. CiS¢lepar.C"/lnC:icatltln Spaca

,.ACILl--......,._----.,...--.....".---=-~ :--: :-:':'"==-----=~=~"7.'"7---:c--~~-~~~:-:::----------+ 20. faCility Owner or Operetor: C.ltilicatoon of roc.opt 01 h8Zllnlou. m... rilil. cpwrea by \h.. ",am'eot except u noM<!1n 110m1'iI.,

V ~nledlTYPed Neme~ .. t r":i ~~.,..r';l.1/ . ; WI r~/.jV

Alonrn Oq YMl'

i '~l-: I 41 .:--;:1r~El'''' fatm 11CO-i2 (R... l1l8I1 p,....,.,. odlllonl __

3 - TSD MAIL. TO - GENERATOR '

. '-SIGNATlJAE MD INFORMATION AlUST8E LE:GIBLE ON ALL COPIES

TIERRA-B-004750

'HW .... ,t~E'<· .... 1-a~;'~.~, .Slale 01 New Jerser,.. ': . "~ - Department of Environmltnla Protection

' .. ' .:' Division of Hazardous WallIe Management. ; _,:-'::':' .-:. . . Manifest Section .

:.. ~_~"'" ...;.~::"' :.:,;~".:, .. ' . .' eN 028, Trenton, NJ 08625Pl,Ai, typ. o;'prtnlln blOck 1.11.... (F'onn dlllgnod lor us, on .Ill, (12-pllch) tyl"'wrll") .

866300152

MCN-HA=Ai~OOS ~Y3 W~~~~~ERHO'l' ~$GULrl.'!'3D 3"! 49Cn.

"

I·~,:lu' 1\, :"'I~'

O. ,TI1Ift$po~(' Phon. ( ... ';'~:;" .. tt '';;~ i.'.ESta1e TI1Ina.'D~.:;"~·_;t~r ..;"I.Tl..,,-::;.r·

I 11. US OOTo •• cn"tion ('nc:ujing PracsrShipPlrlg Name, Haz.;JtdCla$.!, aIId 10 NumIJsr) 11

2. C,mtaln.rs I T~~ - . ~il I·U

~,~ ~'f:"'UI rlM "_ . Nc. ITY~I I Cuanhty. WWolI .vaste No.

1,,/\ 11 ....1J~<tl\hN I

I ! 11 "II I I I

1 I IIII

Co

r I I

..:'\j:':!i r·· ..

15. Special Hanclling In$U'\JClionsar.e Aoclitlonat Inforrr.atlon

I I j IK.Hanclin'il cae .. lor Wasta Li:S'ed Abc.e ~

:~~~~;;;~:~.:.;I~:~~~·:~,~··i.-~t,Iin-"'p'''l' 0.:: .< ~ ~'"" <l q "'Co I I

: J'lACd~bonal o~cnplICns10r Matanals WIIBO. AbOllI."- . -;.' ,. . . .

I ~~i~~~=:r..~~~:;r~~;o:iN~~OPh~71_~,~~.b.

PRCBZLZ NO. &-32525

IIII----,~=---"""~------~=-----------.-.~,.....---",.,.,....l

Pnnt.KliType<l Name

~.O'LD ~. ~0~.1..~'1

ISignal,~~_ ,".,"

Montn O.y Yur

1.III".u:d..,1 rl;t'

ti'i:ISs

~I 1i. T,ar.$poner 1 ....ckno .. '.OQ.m.nl of Fe<:e,pt Ji Mllerlll~

~ I pnn~~T~eCl N&'l'\ oJ\. • ; _s _ l ~Ll:.~ 'V_~,..,_.~ 18. Transpon .. 2 ,6,Gkno.. leoliemoH>l "I Recllpl 01 Malln","

~ PrI/1tlKlfTYl*i Hamee '.II

.0' -

111,DI.ctl~CV Inclicatlon SPIce - . - . - , ..- --.--

;9, r~lii"p,,!Jjfo 4bcrL --

ISignalUre ,/ / .'.J I,-,""",,-., - -.;1 -./ . ..",. -ISignature

. :.......... '-, :"

'A<Jn:.'1 C.y '(u.t ,.

10141n~94-:'I

MOrIt/r o.y YUt 14I i I I i I :

.. r'".' ..- ~

aiP~~kEPA Fonn.lnQ.l:2 u~04,8/1IlI1Pr9YiCNll M!'IlOM_ QbIOloi... - . .••• .. - ··..::....:'"4IGNATlJAE AND INFORMATION MUSTBE I:iGlBLE ON ALL -coPtES ..

3 - TSD MAIL 10 - GEHERATOR

TIERRA-B-004751

Q.. Slate of New Jerse,Department of Envlronmenta Protection

)\"'\11 Division of Hazardous Waste Management. -1!~~ Manifest Seetlon. .;.-..... CN 028, Trenton, NJ 08625

p. elf prf~IIn block 1.«..... {Form d.tlgned for u .. on till. (12-jlllchl typ.writer.)

866300153

~,


1. Generator'S US E?A 10 No.Pteo8.1

cm:::."'UQL CO~S INC.2~-75Rr~~SICE aVE., BLDG.17r

~_ G.n"rator'. Phone ( I

J.. Generator'. Name a"~ Mailing Aaareu

5. Transpcn.r 1 CcmpanjOXl <l.

D•• ,gnalld FleHily Name ana Site AaarUI.~.,n

~n,.

-1--:-'--+------------------+-7-~~~:;wJ~~;....L3;L::ll.JiLl..llJ

~iC!'i-aUl\..r;pct;s ::I'~Z~J1~ r'1ATEatiC'! ~GUIATZD BY 4gcn

o.

o,1-__ -L -'--''---'----'--.:....-:--.:......:-.:......:.......l-_...L.....:J~:.:.l;...:..:..;,..!...,;:~Co

':5. Sp&Clal Hllnaljng Instruc:ioMI and AcclltJonilA tnlormatton

d.~~~.:::;:~:?~1~~.t_~!-•.• ;:~.:.. ~. ~~~'~J";.~~"~

. -." ." .. '.-:,-, . -,;. .......

-;'10RX CRDG :10 ._ .....,;;.;).~..... _

DZCAL 5"0. ,.i. Ci~NERATOR'S C,RTlFIC;'TlON: I ~,,~cy oee:ar. :nol :to•• C~~lenlS of Ihis con"9nmenl." fully and "c~Lnlt.ly ~"c(jbea 1e0'. ~v

::::--:ar s-tupplnq name and aJtI ctauafifod. ~3Ci(eo. :ftarxec. ana .aoeled. and .are In 311,-usPec:s in prep., ;:ondltion !or trar.sccn !:y "tg:'lWIYa,:~rdlno to apPliC3,ble IntemaUDnallnd nalton&l ;ovemment rll!~l,J.l.tion....ill am 0 lor9. Quantity gon.ratcr.1 certIfy that Ihive a prO<l~m in pllclla toduceth •• olurneand toxicIty a"Mast.~.n.ralod to the C:e<;r.... I ha.ea.terrnined to ~ocono,,"Co1Uvpracticallil ano tna,l ha .. M,eC1e<lll'l. oraC-Jcabl. method of tre.oun",,~ .10(391, crC:lscoeal curr&nlly "I~.cl. to me whlcn mlnunlZaa the presenl uCS!uture threat to numan ne.,th and ~!':•• nVln:mrn"n't OR,lf 1Im.a small cuantity generator. I have rr.atj ... ;coc tallh etfontQmlnlml4e myw.aua glneration .and _led~re ~e.st "'Nasre rt:anagemenl me.hoa :..'":at is ,lvallao ... to me and that 'can attord.

';- • __ , , ..... ., • J .. """'_

I SignalU

1- .....an':::=cnllr· ":-CI<r:owl,c~-err.e~t:lt ~~elOt :;r ~.Aatl!naIS

?·:ntBd/7 ipeQ ,\jarr..

~a, -r3~'Oorter 2 Acknowla~tnont <:If Reea'PI of Materiels

?rinjed/T~ped Nam. Slgnllur.

19. ~jscrepancy Indic~uon Space

......

7~:-;:'~:_:::::_:_::-:-:~~~:_:::::;;::::::"':';'7.====;_;:::===:::::_::=::;::::7.:::_=:~:::_:~~:-=~~=-:"::------------I~I---:;~...:.-:;:---:-:'=:...-_-----------,.-;:-==:--;,..-----.;.....----~---...,..,......,.--=,.---:-:----I20. Facllily Ow".r or Op.ralor: Canllieallcn of '1eIIPt at haUn!oua malenlb coverOll bV \II .. m.nll.ot exc.pl b notOll in 111m111.

P"ntt<llTYlled Nam. Signatura IrIcnrll· lAy YHi''-·r.

, 'r IePA FOhn a7CG-22lR.". QIS.d:~ P~I(lUI_"iOf\l .,.. ~ ...

8 - GENERATOR COpySIGNATURE ANO INFORMATION MUSTBE lEG18tEON AU. COPIES

TIERRA-B-004752

- ri'fEiiie.~lQ

It•1'lioJ....Q

-lz5

_1

iiIJ~-=I'!

I,•iI!'I..I...,i_s-

-'

.~., ....--

866300154

UNIFORM HAZARDOUS L'.,Ge,.n ....ral'o~l.uls~,A.II~ _~.-?:.::,<~,...•' qO~u·~~I~~Q.,'- l.PogIF'l' lnf~mlljon ,n In, .nallea .rus,'WASTE MAN.JFEST 1_' ., .. '8IW '. I I -' L .. -';1 ., .. T:o't,,:';t::~1J:,;..a~~lI'luHla by F~der.,

,.":.. 1"

, 16. GENER.a.TOR'S CERTIFICA nOH: I,heracy ~ec are met Ino con,ont. olih .. co~.,gnmlnt .rl ,:,lIy and accurat.iy dellCnblCllOC'lI Cy, p,ol'.' .hlpping name enD are cl'IS,fild. paduld, marud, aJ1d laoeled .• ncl are ,n ait respects III proper ccncliUon lor I1lnl;)O" by highway

accerding to IPplicable intemeuooaland nltlonal gOVOff'mont :1IgUIIIIOI''''' .If:am •• arg~quanl;ly generaw"l oo"lly thaI Ihave. pro~",m in cllce to leducotho,olum, and ~o.ielty OlWIS10generated 10 Ihed.."eel ha'e determined to::.economically practlcaCi.andthat, have ,.11C11Il the orac~("Ilole m.lhocl cltre.rmonl. s,o(ag •• or disposal GUn.ntly Iv.,I.ol.IO mewhlen min",.."Il.lhl present""-future thrlllt 10human hea'th and the .rwironm.nt: OR. ,I I IlJl\ a .mall qu.ntity g.neretor,1 have mad. a good laith ItlOlt 10 min.mize my .,.,ute gonerelion and $11K":the be" 'Kute managament m~t~lld,th.t " available to me and that I can afford. 1 ':. -- n . 'PnnlO41Tvped N,ome ., I Si..n,~.. ff t~.L:='_ tI. I·r. . Manrn D.ay Y.a,

'O.,n1',l"I -::: c:Tn',T ~~ /t".. -~-/../ /,'" "r" ;-;/" .......- I ·1';1 ~r ".:"\~~li, T(an.po~.r t ACl<r.owledQemont 01 Rece1pt 01 Mate"IJS -, I...", MOnln Oay Y... .-

j()I41.:l1 II 'f.;,

Monrtl Day Yol.'

:I , II 1 I

r._· .-"- : •...-.:""':.- . .~--::-.- ~'...__ .----.~-

TIERRA-B-004753

-- "

- A-. S..t.ol"-J·~·rDepartment ot Envlronmenta Protectlon

.

;)JI,'\ Dlylslon ot Hazardoul WIISte Management'" . : Manlf.lt Section'. . 'eN 028. Trenton. NJ 08625

PI .... typo or prtnlln block I.tt .... (Fonn d•• lgn.d lor use on .1110 (12-pllc!lJ typowrHet.)

866300155


t. Generato(s us EP'" 10 No.

.13. G.neral~rs Name and Malling Address,

~CAL CCMFOONDS nc•.23-75B-~SIDE~VS.,~~-G.

4. Gen.ralOrs Phono ( 'J' ~ ~ ..•5. Transporter 1Company Name

1.

9. .Ou,gnated FacLlily Name and Slle Addre ••CSfJUc..~ ~i~':;Z MAN1\Gz.:.~r:loa L.£.;;';,'!:..~A'l:lCZ.~~?-'C, !:Z!'f J1!!tS::::'Y 0'71~S

11. US DOT Descripllon Ilnelu;Ji"~ Preps, Ship;;:r., .'VJn:s •. '-!az.:Jfd C1~ • .Ifld /0 NumOer)HIA -'

e.GE

"'5Cm-~,\z.,~OU$ Dn 'il\5:=t ''1,-,-1\"'\-1-.'" ~~~"""Q''''' ~ ..,. A1.r1,"""='tl

~...Ta~I-~~_~_---"--,,,,--,"-----~---------------!-~,.-l.~"""-!-J--.L-~~-!---+";:

50...I..:!&.;!J.!~1•....-t'I'!!!:;....c:....;i "Ii

..."'i s

: p

- :I 0R

Jl r!R

,AC•LITy

IS, ~~ '!X lL"tCrn..E 110 •. l(- 32525

1&. GENERATOR'S CERnfIC,l,T10N: I horsCy doc~3re :r,at :1:0 contenlt of this con.i9n",ent are lullY and accuretely de.criCed aeave byoroo.r sn'oping name and ate clauilioO. cacKed, ma"oO. and labeled, and are in ~I respectll in proo..- condition lor lran.port by highwayaccordi"g !o applicable inlomolional ana nallonal govomment regulltlonL"i om a iarge quanlltY genorator.1 certify thaI IMvo a program In place te reduce the volume and toxicity olwuto genarale<l to 111.aogrn I hove ao'ermlnod 10 beeconomically praclicaCle and IlIatl have .slectod Iho prlctlcaCIa method oflreltrnent, 'lorago. 0< dlspooll currently oVIHlblo to me whicn mlnimlZH 1110p.... nl..,aluluro Inre.l to numan hellih and tno environment. OR." Iam a .mell ~uanllty genenltor,l ha .. mode. good 1.1111'"01'110 minimize my ...ute Ilenerldon ..,a Hoctthe oost 'Naste manelle",ent metnod that is .vallaC.e to me and that I can afloret. . ' . •

i'nnleCJ7ypl<l Nlme

!'i:,aro:- 1~" . 1 1 ~·1.

'8. Tran.porter 2 Acknow1edgem ....1 01 Recelpl 01 MalllnoJl~nllu",

19. Ci.crepancy Inoicatlon Space

. ~ :~~ ".~'-'.":"7--: ....~, ',~:.,

"':. ., ~>-,- .... <II:!' .!". ••

. . ~.," ....... ', ..,.... / .

20. Facility Owner Dr Op.rolor. ~nllicabOn 01 recelol 01 hlWlretOU*!,!,llOrtala ~red by IIIls ",!!,i~!"I.";"Cept .. noted 1n,IIom 11. ..' .: .. ..-: t·.;; ..r.. Pnnletil'Typod Nam. . . ..~,:: •..t:.:::.. ~ature. ..~:~~e"'~ ..~'!:::~.: ...:l:-,.:"",Mont!? Dq.~'I'HJ

........__ .__..._ .. ..~_.--..-.::.:::..~ ':-.:::..._~~ .:".·it.·,"':~ ...;;.;;~;'~,"'.,::::~":";"r'" r;!!:' ....:t~~~;~.stGfoIAT\JREAND INFORMAnON MUST BE LEGIBLE ON AU-COPIES

EP", Fwm a7'CJ00022 tR~ If.' ~". ~!~ ....co.o4 ....

".,e- ... enJi.-rna r'!.npy

TIERRA·B·004754

...;'... State of New Jersey'~ t I Department 01 Environmenta( Protection,.. .. ~i'''~,• ~ . . Dlvlrlion ofHazardolllJ Waste Management

.4'f",:r~A~ ":~":': ,.)".. , \'.( •..;.:...... -: ..:r.· .. '·.Manlfe,tSectlon ". ' .. . ,_ ... ,. --:-t".. _"-. . ..' • >, .... " . ,. ,eN 028, .Trenton, NJ 08625-~ 'Pi::;ol'!y~:'o.-rp;;-niln b'O~ 10tto;S: (F';"" 40.19ned lor u's. an ;'111.(12"i'hch~ ty ........ , .... ). . -: ",

_ 1'J~"""'UNlf.bRM::HAZARDOUS 1. Geo?raI0(3USE?AIONO. • Mani'''1• WASTE MANIf'EST . -l I.. oocumartrr·_

___ ~_.,_. __ -..-:. __ . _ ~~----:4

,\tHW-e<I, (RE¥ ...... '

---:::" 866300156. Fcmr,v;ptT1'MIi a",

2. Pag. 1

01

G- Siale Htcill\y'3fD.'c ;

, 1. US OOT Oe$cription (IrrcJurtlngPfOpiJrShippin, Name, Hazard CI.,:r, ~nd ID NlJmoerJ

HM

.,1 ~ H. F.cillty'. Phooa ( ., 'Q ~

12. Coota.,o.rs I 13. I :~,l".' ',' ,- '.•.. Tetll lJniL ,,1_. , , ,No. ITypo' Quantity .Wtl'Iod ." Wat8 Ner."-,

I !-

b.

NCli-fiAZ;\RDct.:S DY;: WASa WA'!'Z~~~O'rnzGULATSD BY "9Ci'R ~I

"ATa~l--I-_...... -----------------------+-'-""':"~--~--l""-;~!--:"-+-_.L--L_"':----''--

~Id.

15. .spacial Handli~g Ins\l'UctiOn~ and Additional Informalion .._

\5 QENERIoTOR'S CERTIfI5, 10Pl•. ,Idlgci 6uc,d dial 5'6 ,_lit .. itS """"is CC"si9ome"llre fully and accl:ratoty :lucnbed 10oY. bY;"'I',cc

ltf..~ipciog nlma end are clUlllied, packed. man<od, enclso.olad, !I1Q a" in .11 ratptClS in proper conclItion lor lTanl\Xlrt l))I hi<;ln.....v

aCCOrding :0 applicacta :nlernallor:al and utlon&l governmenl fI\lulallOns.!II am alar;s Q\Janllly gan.ralor, Icartlfylhall have a program in plac.to reduCllh •• olumaand tOll.,c1tyolwUla<;;anaratadlo Ih.d""rM Ihe.a oatorminod to o.economically prSt;l,caol. and \hIll ha.e .. tacto<! tha oraC-:'C3clamotl\od 01trastman~ storage. cr dl,posa, currently Ivailaols to m. wh.cn mir.lrniz., the Dresenl ar:dtutu .. threalto hum811h••dth and tha .. wlfonmen~ OR, it lam a ,mill qUlolityt/lsneratDr, Iha.s mada • 'Ocod 'aith effcrtlC minimize my WUIS 'Oon.raIlO

nand .. Ieel

Ih. beSt ....a.l. mlna'Oemant melhod lltall3 a.llilbl. 10 me .~d Ihat I Call a ani. ,f. i ' .f '.~. ; "Pr.:llOOlTyPac Nama . ISignalura .' ,': i .'-:;: .~..... .wonth Day Y!i,i:

-q~ 'Ie''' c:,.,' '.,._ Lf'r' ';-',:'..l 1."1", 4,;:' I,

_.

17, Tfln.oorte, I ACKnOw,"ogomenl 01 Aec8lcl oll<latonals -r.1-1

'-'. ~'-:-:w:r--"_." ..' •

____ . __ ...... __ .r-.

TIERRA-B-004755

,-

-0,f S'laleof New Jener1; Oepartment of Envlronmenta Protection

.' ~'rl' > Division of Hazardous Waste Management" . w~ ,. Manilest Section '", . _<" . , ,'" eN 028, Trenton, NJ 08625

P1.... !vpi o>rp;{nt In block Ia"ers. (Fo>rmd.slaned lo>rus. on .me (U-pltch) !vp .... 'U.,.}

866300157

1. Ganerator's US E?A 10 No,

t ,.,1, I,,' UNIFORM HAZARDOUS.;_' ,WASTE MANIFEST .

3. Genorator'S Nam. arRilMall,na Accrus. ,Cxrd:r¢Ari ,C~DS-INC. .' , "

" ::Z9-7~~mRS!Da AW;i BLDG~11 ,NEWAlUC,"~.. Gon.r'I~}:$ Phone { :- l' - _.-5. Transponer .1. Company ~am.·

1~~~~~~~~~ILJ,i..I.(.1.!..u....!-IJh~~~~~I1~~~~-lillili2~:..:-4~~~~~~

-.,,-0. ,' •• _ ..._..~•.,.';" ".'

DeslQnated Facll,ity Namo and Sila AcdreSs .

'~CAL WASTE ~AGm-mtlT100 LISUlt AVS1iI03'~rz;'1A..'Ut. ~fi!"fl .rm-..s~ :}7105

F. Tr3I1sporte~$.Phon. ,.-":';"'}:,~::i:'~~~"t;_.G_ $lala Facility'$.IC:;;:· ..

, ',' 12. C<>ntalne~ I' 13. 1'. ,','<,-. ·1"'...-.. ,-1'_ L:S OOT Oescnt:tion (Including Pr::Jcsr ShiCptt:g Naor:tI. :..tllzIJrd C.'ass. ¥ld .'0 Numc,') • T~tBl Una ~'". : - -;> •..'rh" .

!'i1A No, Typ. ; Quantity IWl.'Voll.:',,,~asll!,~,.,'

NON-Q'AZA.R!X)OS DYE hASH .N'ATERMOT REGULATED 3Y (9c.."?1t

".".:

15. SP&ClaJ Hanolin-g Iflstr'Jction! ana A«;d:iuo:,\81InfcrT':':ltiCn

~mt cRDEP. NO.: tf - 3 '7/I~DECAL ~tO. J /)..

~_. >l ,;,. '1'"...- .,.;:.%:7::' 1..(

- ... -_ .." -~.-'-16. GEHEIlIlTCR'S CE!ITIFICATlOH,! t••,ecy cecla,a ,hat ma comen" ~ :,.... cpns;Qrmentlfe Mly and accurately ce.c,~"o>d oaova by

prOye' ,hipping n~m.e ina are classil:ed. packed. marked, .nd lall<iled, and are In all :UCBCU in proper con~lti"n /~r Iran. par! ~y hlgnwayacco~,n\J to appllc~ole ,nl~m3tionaJ and national ..ovemmenl f09ulauonl,If I am ala, .._ quantity g.ne'alor, I unify ch..tl h..va aprc.~rarn in placero rld~celha volume-and toxicity 01 wuto ~on''"tld 10 Ille dagre.1 have c'eterrnlned co-bee<:onomically practicable anc ll1all hlveaalOCled lI1aaf8Cl,cable method 0>1tr.atman~ s(orlgl, or dl1pcsal CUmlntly available (0 me .. hicll m,nimi~.s:he present II1dI~luro threat 10human ~eallh and the an.ironmont OR. III am a sIr ...1Iauarrtlty Qenaralar. I have mada .. QOO<llailt'el1art:o mlnimize:ny wasl ... e~er31lon andslIieC.Ihe beSt wuta rr.anagam,nt method thlt is available 10 me and Ih3t I an afforo: I ."" ..- .- ..,;:';",.

':' Ii,,~...it-_-::-=L:t~5.=-'L:~~~~~~~-::;7:':=~:----"";~--::,;;,,~:::~:::i~--:;:!~~~~L-_.!!.:2:!l~~~~.2~~~;,;::,;~;,::,;~=:::;~:,:,:::,~~~::,:,:,;;=::":",_---'--r;;-:==---~-_-r._------,,""",,:,:~~~,,:,,,,---!T~,

it

I

YHr:

I

3 - TSD MAIL to -GENERATOR

TIERRA-B-004756

::...-- ---~-"-'-"--:_~- _.::- :.....-.._._.---_ ..--=----- -- ---- -~ --'--'--- ---- '-- -- -- -'-..', ',"

866300158

..1iI1iI'I

1I~

II,.

••s

..,

t 1 j I 1 I10. ·us ErA 10Numoer

JSRSEY.i ::,~,.9. .De:stgn3\e<] Faclllly Namtl and Si18 AaClreu

CHBMIC.~ WASTE ~tAGEI-umT100 LlS'l'Bll A~tJE·'l'tZ',",-0j( . NEWJ!?S3Y 07105

I No.11. US DOT Ce"cripli~ (Including P!uper Shipping ~me .. '1uarrf CIBs.s.and /0 NUmNrj

HMG 1.\ ~CN-f!A~-o~S DYE WASTE r~~~l'I ~CT REGUAL~ B~ 4902E~

b ~ I·...

...T 'l'

cA ~I I,.II

II.

. "..,. ....

15. ~ecial Handling InstNc:J01'\S and Aooi\lOnaJ Injormation

~6. GENERATOR'S CERT FIC.\ 10 :. /'l8"'Oy aeclar. tnll 11'1" OOnlent3 at 11'1.. ca".", .. "",,,nt are fully and ac<:Ut~leIVaescnbe<l above bypropet ,mpplng nlme and are claulfied. ~ked. mar'e<!. ana lao.led. aM are In au respects In propet COtlo,uon lot tnInapoftby /'Iignweyaccordlno to applicabl. ,n\emaUoneland national OO'i.mment ,...ulatiOl1t. . • .III am a 18'g

eouantity generelO_.ll;ottlfy thllt I have I ptogrem In place 10reduce me volume ind toxicity ol ..... leg.neraled 10the degr-I have determined 10be

econom,cally preetlcaOle Ind tholl hl't8 .. 1ec1edtha oroc:iao",me\llod olltallm,,"\' storoga. ordii~o .. 1currently lvaillbl. 10m. which min,m'laoma p"""I"'''luture tI'ltlltle numan hea,lh &nOIl'Ie."vitonment OR.illam urn all qUlntltv,Pclneralar.1 ha •• mede ageod laltl1lifort to minimize my wuta ;enlratlOll and"*'tt/'Ie but wuta manlgem"", metnod Ihat io avallabla 10 me ano tl'lall can I cmI..

.-;_ .... "

't;:r' •••...

.... ;,. ....

1~ OloarlllatlCV IndlClUO<1Spacl -. " .... ~:, ..'~}IJ,. f_.~:•. j,

-. "':' "': .P~-"'.,r.......

:~:t;,1~~~.·t.;:;'"~: Monrlr OIlY Y.., I

11 Gl"

EP" form e7tlO-22(A..;."" .. l- .... --- •3 - TSD MAIL TO - GENERATOR'-- .. -

AlUSTBE LEGIBLE ON ALL COPIES

TIERRA-B-004757

- ',' -~... _,,",,-, ellEV._.~fi';'" ' . Siale of New Jersey_ .;. Department of Environmental Protection

. ,,,f ' ' .., Division 01 Hazardous Wast. Management.' ",,;:. Manlfelt Section

_ _..:. .,.. 3.S86. aal- rece..1ved eN 028, Trenton. NJ 086251..... Iyp.or print In block .. t1..... IF.. nn 0I"'9ned I.. ' .... on aliI. (1:l-pllchl typewI1"r I

866300159Form Appro-rL OMS No. 2C5O-<I03S. Ex"i,. 9-:Ji)..'

UNIFORM HAZARDOUS . 11.,~ne'IIO(S US EPAiO)l0i...-. ',' ,- M.':;~~sI 2..!'.gl t." I InlOrm,"tiO,n in. m. snaded .... s. ,WASTEMANIFEST ~1/1,jIDr 'I"'IRI~I(.,' ITJ.I3r-' f)OCU~r~N~ or-' :"1 I:w.n~~.r.q~~~ed b:: Fede ..",

7. Transporto,ZComp."Y Nlme 8. . US EPAIO Numller ~.,'T'B"'P~!1--sPl1o""~1 r1'~"1'!: ~,l__ ,'I I 1 I If' I j I l' ~ Sta.e Tram.. Io.v--·'-~." '"".;i·"'':'~ <:t·' "",' I

10, US EPA ID Numoer,F, T-rIlnsport;'( •. Phon. e\o/, '} -- --9. fmOl, ;gnal Flcili" Name, and Sile Add""'-:--" . ,'._,·0 •....1.:...1" t .... '-L,'~'r'-"'. "...........~r ..~_~ -t'.~ •

". • . K7 tr /':.s-~ ,,' . I:.... , ....r:·fC'· ,/1 "''-:<I1",f:rr/;.J'I'I ~]!;1f .....r; ";,,-,,,..,1'

~I'. it 4~'/J' _" I .,..'I 12. Containe~ I 13. I 14. 'I - ~. 'I' '.. ;n. US DOT Description (Inr:iudin9 PlOpsr Shipping Name. Huard Class. and 10 Numosr) To'al Unil . '. ,i HM No. IType Quantity IWWol .W .. leNo. '

.......

,,1\0 WAS'rS ?:...uU!.~:.E LJ:QC::J 11:'. a. s.~~~~LZ ~!QG!D ~:J13

1'::,I..-;-"'!7 ..... --.,.,. _.'!',.,-~.-,-..,.. -"'I. ........ - ... ~ ..... .,. "n I roh

- - :

~.'

.'. '.. .-

:::' 9'· @S5~1 -I ',t ··1.

:,-; '-,:, "

:i~~hF~~¥:;r I I I I I ,:'Cr.: < t . j' - '

(2Cl) 485-J21:"-'-eCAL US~49

i\~-=-,..,--=----:-:=-----------...-;:;:=::::---------------:-:......,..--=--=-!

,-.- -

:<b.

\<:.

\d-

O' '.

I f

1I

1 I I ,l.~ 1"':1.

z."'..EliGnlC'!~S?C~5Et(;U:DE:' 27,' ~_'IUlR.')nl""'l' ·t 0;., t:: ~

16. GENERATOR'S CfRnFICATION: l.h,erebY decla,ell1at the conlents or tnlS CO~lillnm.ntare '.ully and accuralely dosCflbed above ~yproper .hipping n.ma lInO .rl c:taSSllled. procklHl, manted. and la~eled, ana Ire ,n all , .. pecu In proper comllllon lor lransport by h,gnway

.. Ic:<:arlilng to applicable inlemational .nd na,lonal govomm ... t rOllulations.{f I am allrge Quenlily generalor. Icertify Ihlt I hive I pro.grvn in pllCIIO reouce the YOlumeand toxicitf 01 wlsle generated 10 the ~e9fea,1 have de'ermir.ed ta b4economiCally practicable and tnall hlve .. lected lIlecract,cablemllnod oltrellment. slorago, or lilscolI' currenlCy a,"ilab,ota mo wnicn mln,m,rOllhe prtsenllt'o'utu .. tn ... t to humen heolln end tho envlfonment: OIt.,llam a .mall ~uanlily qlneralor. 1 h.,o mede a good tllin etlon ta m,n,m'ze my waste goneration ano .elect1M best weste men.gemon1 method thel'S a,alleble 10 me and thaI I e:-n afford.

PrinledlTyped Name ISign,:"',.

n~ !l....T.:"l "! "'~""'T.""""T :. # " I

Montn Cdy Yu'

I • I.. ~I•.' .~I I

T 17. Tt8I1.pan0l1 Acknawiedgement al Receipt of Mat.ne"

: ,PrintedlTyped Name .' .' .: r:,;,.... ... I'!<!I! '!'t'Q'u9'uo'C 'P; &: . I,' ...., .,,',1. '/ J .~~ lB, Trenlponer2 Acknowledgemontof Receipt a! Materiala

~ PrintedlTY!*1 NIIItI.--!R

'J"!

ISig¥ldje £.I.P7I /.11.'.(..-"

- I (/ ./\SI\lna1l:''' /

- ~_ ..... -

.Monm ~y Y..,rI I ., I '1 I

'-.

'. ......

Montll Day YHr

~ .{ I,', ~I~I

19•• Oioc:MPll'OV Indication Space

, .",-,t :·':~6:t'~·::~,·'~"·~,,,,-·,,· "~' - ,.'." ~,,;<".: - ... ,';

} ,20.' Fecilty Owner at Operator. ,cartlllcalion 01 _siPl at l>azrtrdourt meleriala ~ by III;. m.ni!"" except u notacIln I,.... la.

v >:.prinllldlT:Y~Na~ !'fAr!.C. Chr:btuc" ···..I~.....::...... ;,""I ,;" /: ·~...,.,o~ . .-";,r I r._, .;F' • ..-,{.. # ,r, ...., ....

--SIGNATURE' AND lNFORMAnON-.USTB£LEGrSLE'ON ALL"COPIES

TIERRA-B-004758

'-',

" (~.~f~.~" ~.;:? ."0, -::.: .. r:I<-. --0:' State of New Jltl'38r.. . '.' ,i Department of Envlronmenta ProteellolT

" ; \.1 .' • DivisIon of HazardOlls Watte Mlnaiement. .' -,,~ . . . .' Manilest Section -',. :.. .

; '~~! .• - ~ "4·1~·~.h·to ~-1'7 -.. . CN028.Tr.ntDn.N~~~~25. ..:.::~·,;.Plou. type or print In btQcl<Tillers. (l'Orm ~M'I~ol1/l 'itl'UI. on .111. ('2-pltch) typ.write,.) '. .. .

866300160

..'~'"·UNIFORM HAZARDOUS 1. GeneraIC'" US cPA 10 No. '. M""::"~~~.~:.-:WASTE MANIFEST· ..J_ '!\ ,';

3. ·GenenlCo!'. Nam. Ino' MaWng Adaraaa

:CHBMibi' CCMPOmmS ;.INC ~','2~:';:;7S' RI VERSU)'t·AV~., ,;NEWARK.

.... Gen~rat~r" Phon" , • "', ~" '.,5. ·Tran.poner 1 CcmpanyName=J~ribVE~·C~P.~:-·5t -00$19na(&O FaG~h~ Name and. Stte Aadres,

~~~'oLOOV::R CORPORATION·':::HT.l, 'STATZ ROAD 651.,' A3VO~J:.l\., VA "13004 .

0::"'.:.....;;ig;0

j2

Go..i&c""":III'8~&...~•:5

.-.i.!i~r"r.;.!!~-5'3......

.~... &

..cI~....l!.lr!i';•!.s- o'

"

'"

11,'11~~US COT Oes<:r;ptic" (In';,~drng 'Prop;" Shipping Nam". Hazard Class. and ID N<JmNr)

HM -=-a.

,:0., .

RQ WASTS F~~~~ELS LIQUr~,PL&~LE ~IQUln UN!993

":'t' 1 1 ~ ~ .~

.X

b.

c.

',,"~... ,

._.,-~:~~ -.

~~::;\~...,......_.;;..-.~

._" .... - ""-..-. ,,'-~'., -!'-, .... -

.nJ~'l'WSPOR-r2R DECAL 45237EMEnGE..~CY :?l-!f)NE(201 14.-S 5-1117 ,- ' '\'

16. GENERATOR'S CERTIFICATIOH: t ~er.DV docianJ I~al tM conlonts 01 thIS 00n5lO""'""la .. fully Ma aCCurately de,cnt>o<l abo.a oy ..proper,hipP"'!l nl..,. ano a.. cta .. ;Iied. pacnd, mari<ed. and lice led: ~nd an ;" ell r.. peets .in·proper condilion 'or '",n, pan by .~jghwayaccordmotC appUc&l>l, "':ernaUDnaJ ana nlllcnt] government regulat,,,,,.. • , '. ". .

•• '111 am'a la'll' qUlntlty g~nerator.1 cartily t~"'ll ha.e ,oro gram i" plac, to raaucelhe volum" a"d toxicity ofwute generated ICthe deg ... I hl.e determlnoa to be'c .'-economically preclicabl. and thaI Iha•• 'elected the eracticable method 01~Iun,nt, 'torag ... ord/.posa' cur"!ntly l .. it.CI. to,m. whicn mmimiz,. the Dresen! anCl.

'uture threltto human ~.allh ."d the ,n'","Onmen~ OR, ,'1 em a small qUa"I,!y generator. Ihi.'" m-.:l. a \load '81th .!tonlo m,mm'lOmywaste generalian and HIact' '.lI1•. bes' wllta. menegemenl method tha' i••• ,Hable 101M and thai I can atford; . . •. ' .

PnmldlTyPld Name

.. "'::.... fOf1'T T

ISigllat\lre MOIll/l C"y1IJ 10 ,. .<]

I"....rl.s,T 1i. Tran",o"or 1 Ac.nO ..... d •• m.nt 01 Roe.'ot Of Mar.n ...AA :.!'irt)earrYPed Nam,..rj c:....~ ~ I~ I 0,# -;~ :: U ..x .,' --t :;-. /.·.,. ...1- -~ 1-':.:S::,_T;.ran:..::::",:.:ort;,=,,:.,r:.2;.A:.=e;.k:.,n.:.ow..:..;letI;.:.,:9:.:"_m..;e..;n.;,t.;,0_'R..;.;.oc;.e_'::-l't_"_'_M-:-"l_._n_als .,.-;;:--:-:=-:::- -.:;...,_-,-:- -:-_..,.. .....__ -'-~T ' Printed!Typed ,,!ame" .• '-''-~ :~7~;'_~: :;:..::.' ..

:: ..I"ur

'9. D;~~~cy~~~~c:a,b~~.~rce ,_

;.··~·.~.\:~i~Sit5f~,'-:~:~4~;~e:rap·Uq'.L

,- .., ,{. 2O."Fa~U~-o~~ or·9P1.rato;>r:cel1lficali.on ohllCaiptol tl&tattIoua m.lotiall CO\'Orwd.lrf lhiaJ!'8"iI<eat aocaptU·notld Ift'''""lD •.~-· _. "._. __~'~ ~T .. ;-0' ~')J..vrrpad-·Nam"""::::;-'-"-:';"·i~·, ' -,,' .... , .."_ ..........-_ •. '-' ·SIQRlrute-.,. . .- ..,.;.'_.-.., ........... _~,_ ,~,, __ . .... • Mantll Dq YH/',: .. ':;~ .........,..~·,-\"""';:.~u...... - 'C "Ot~'-~ -;..;.'~.. ~.¥ ,., :.- .. ' '-"";';;'Il..' . 0.':.- ,.A'''n·J! _.",~. '!, . ..' w·~. "":r! :';.."'!::-"' .... -~.: •. ";".", -~.............. • - ~"'::U,;,...-a ~.. -... "J ,.,. Ii .,-.".,.{~.;t.:Li..~---..,., . ,.. r

~:~, EJ:~,o"" I1Ol)-22 (A_.,!8".~~OO_-- ,¥', •. :7'":'-;::~ ;~~ ':;SIGNATUREM4l:!JNF9RMATlON MUSTBE LEGIBLE ON AU COp~-3 - TSo...~~IL. T!l..: GENERATOR ._\ .....

.-,-.-... _. ~. ," -- , -" .

;:' ';"'" .M, .. , .• ~. ~~'• ..... ;.:... ;".- .;, "':' ..:~.. ......

------.-" ... ::""",,,,'.. . ..~."-'- '.

TIERRA-B-004759

STATE OF ARKANSASDepartment of pollution Control and Ecology

• P.'0.Box 8913 UttJe Rock. Arkansas 72219-8913;: c' . " Tttlephone- 501-562.-7444

. . ..,...,.. .•.. . . .' '

PI;;a. prlnt ~rtYp;;~(FOrm deslgnf>d for use on elite (12,pitchl typewrjt~f.1

866300161 /~.I'i-j' j

TIForm Appro""'. OMS No..2050-0039. ~~.9;30:1?:4

UNIFORM HAZARDOUS.. ' .WASTE'MANIFEST- 3,-.,n----Chemical Compounds

2975lUveiSide Aveuoe ' .. Newark..~~( '101~-17175.T_ t eon-n-r-Tri-&ate Mocor Transit Co.T._2.~-

9. ~ __ ..-.and 51'- Addt9M

RinecO1007 Vulcan Rd.-Ha.skell

.Benron. AR 72015

..Waste Ql10r0form N!ix:ture6.1 UNl888 PGll

b. Nan-ReguJ.a1ed Materis.1 (Motor Oil)

<I..

Ie, GENERATOR'S CSlTIACJinON, I herei>Y deel Ihallhe eontem 01 thla consignment are ruIJy and accurately described ~ by proper Shtpp;ng name and arecIaaaifI.-d, packed, m8tl<ad. and labeled, and In all r88lMCU1 in proper conclitlon for InInapa<t by hlQhway 1ICC0tdinp to applicable International and national

OCMImment negulatione and Atl<ena8lIIItaI. negulelIoM. .,tli am'a I...... quantity generator, I certIfY 111811haye a progmrn in pf_ to reduce the ""Iumn and to>deftY of wasta generated to lI1e degree I have determined to b*economically pntClIcable andll1et I have eele<:te<l the practicable method of treatment, .lOr8Q., or dlsppl&i cum>nlly a"';labhl 10 "'. whicl'l ",;nlmlz.s the preeent endfuture threat to human heaJtlt and II1e environment; OR, H I am a amaJj quamtty 0"'-01', I have mad. a.good faJtl1ettort to mlnlml,e my waala g.ner&llon and selectII1e beat _e rnatW\lemantmetl>Dd tha1la aveiIebI& to .... andll1et 1CllII a1totd. - . .. , • ..... .'"'.:- ..

~ 17.~'~_o/~crl-

A:L':::'~~~~-1~!...J.;~~~~~ .J...::;;~~~!::~~~f=.~~~f:::~::::=----...L;uf:I:i.Jwt1~~j..::..::;;::::,:;..;...;:;~::::::.:::.::.:.:::;;:::..::.;::;:;.;:=;..-------,--r.~---------------.,.,......,,,,.-=-~-ITe-II

-~- SiQtloonAl-lJi:n:rt> t:.cl-L.15tl.J I

18.T"'- 2"-.-_crlReoololal-

- ~"- ..

.-to." -~ .'~ .. - .", ~ ~"-. - .......---...

.~ ......... _, .. :",r=-~': "'';'',_''';-'~''' .',_ .. ,,"; .•.•.•

:-, ~-~...~.:~:---.?'T·--~--~..

,.,:";'~~.' _ " __ . .-.r ":'-.'~ ".-;:

AST1 SHIPMENT. ONCE DEUVIRED. I'llE TaUJ-. I

TIERRA-B-004760

866300162

G b.EN~I___-----_---------- -----------f---+--+--""":""""":""-+---"'"A CoTaR~___-------------------------------If----+--+----+--I d.

.. 13· DF ~1-5 . Ga

t

II

Chemica~ Compounders29-75 Riverside Ave_Newark, N_J_ 07~04

6- 5·

A. Tronspert,r1 Phon

6. US EPA 10 Homl>.r

9. Oesi9nat.,j Faciuty Nam. and Site Add,... 10.

Laidlaw ~nvironmental Services3527 Whiskey Bottom Road

us EPA10 N~mb ..

B. Trantport.,'1 Phone

C. facility'. Phane

301-953-958311. Wa,'e Shipping Nam.. and Oewiptian

12. Cantoj.en

No. Typ ..

13.Tatal

Qvort"

1-4.Unit

WI/Vol

a.

WASTE

O. Addmonal Detcriptian. fa' Matoriol. LQ• .,j Aboot.

PROCESS WATERE~ H~ndnno Cod'" for Wcntr$ listed Abo ..... - .~

1'. Special Handli"ll l.otnJclion. and Additionallnlo""atian

PROFILE NO. 6-CEM-OOb.

~~~~::::.::=::....:..~c::::::.:=l=::.::..::::...:.:=:::.:..:::...::.:==----,...-----:-:~~:::=:=-----------------~~1---_&;..e~::::.J,~~I-/.-=~~~..<.-:::=.. ........o----l---V.L#''4e:.t~f7'I~=",t:-----_--.J~..L.J.,~::u'-...L~~~~~~~c::::::.:=!~::::..::.:...::=!::.:..:~==-----r:::---------''-~---------------~

PtinMd/Typed Na_

19. DIocrepancy Indicction Spaa

F,

j

!J~.

TIERRA-B-004761

10 '10 ---------~---- -- --------------- - -;;-----,---,-

866300163 .~/';}; / ~ /' ~ -r:>1 7- jState 01 New Jersey -~ ~ g" , (J7(Jl

lJepartment 01 Environmental Protection and ener9Y(j 'r /911 •Hazardous Waste Regulation Program /. .,

Manifest SectIon " •eN 421, Trenton. NJ 08G2S-<J421 '

_ 'I .... tv~. or ~r!nl In block letters (Fo"'" designed lor u .. on eill. 112·p;Icl'l1 ~ewrtl.r I F""" ADom.-.r1 OMS No 205<J.C039 Exc,,..9-:::

UNIFORM HAZARDOUSWASTE MANIFEST II, Generalor', us E?A 10 NO.

., 1",1 I I 1 I I 1 IMamte.n-

OOCU;nenl No.I I - r I I! f-::----=~~~:_7:::=:;---'----'---'-"....:-...:-...;---:..-:...-'---'-.:.......:.....~...:..-..:.-.r~~=~~-

I~~~~=-:-::--~~~II~~~"""'------~~~~~~~~

US E?A 10 Numo.r

I D1 I "11" 1 --;1 'Ius EPA, 10 Numc.,

3. GeneratOr's Name WioCS M3J~n; Addr~B .;:,..e,r;:;.;·,t _.·~~-·qti."'::;'t

_", .-!t~ "'''!''i t:!.c A··"~ ..~;""'"~:"~f' :;4'; ~ I r ..

If:;:..=..1!~·.51f2...!c·~0:0>-.5't;......·Qi>I:

51s",~'·~~..."c:

f•oS

i•.-5,.if~~~~!•~l;r;c:•2'·e•:j'l;

I.Ii

,\\,

\

~

i

.:~

4. GonenHor'. P"'on. r 15. Transponer 1 CompBIlY Name 6.r ,.

a., I

7. TraIl.pa"o< 2 Company Name

jO. us E?A ID NumberC-&Slgnared Facility Na/TIe ana Site Addr9M

JttL;"~oIl!'" ".;"t;::"~,::.",,,;~:.. ... ~!l.~. l? ;';;.,:: -l i/.-I •• ~~-=-",,'r::.(1- or"~ __ ~

9, ",',' Decal NO:-i"', f- , ",

F. Tr""sponer', PMn" ( ..L'"~_) ,,' ..

I ~r I ., .j .j" H, Facfity'. P"'one ( .-.;a•.) ,-,,"i h ~l~o11. US DOT Ce5cnptlon-f/"c;udfng Pror;s,. Shiacmg N.m •• Haz:Jf'Q Cass or elvis/Ott •

HI.! TO NumO.r and Pac,~ing Group) /

'2. Conl3m .... I 1:J. I 14, ,

I I Total Unrt ~ ~No. 7"vCEII CU8Intitv ,\;\'r.l\la!~ . Wa.r..a No,

a'jIG ;i..:.;._~ /l ...• ~·,iOlt~~4 __ "':",1_":. , ...... ...- .... ~~- .. '":I.·ri .1.,

., "':n j .::...... , ,'(.; l- .. £"1 -'-." );: ; ,i." t: :;. .

ii.&:ci d"''f II

~ 0'1R

~ ~ IRJ--.,.....:-_+ +.....l...-'--!--.:..-+-"--L....:....-L-!-_.J....c::...L:,:.:L-,:...L-....jI I

15. Speeoat Hanallng Insuuctlons and AOdltional InlarmallC"

Ii!C' # ~,

16. GENERATOR'S C,-"TlF1C.ATIOH: 1n.8ra-by ctteuU"y'laI tn. c:Onttffit3 at mlS ccnsignmam ate ~uH"'!lnd ac.::.Ifale~y :::e5c:-:.:::1!d3.CO'lB -::J"I pro~sr snipPing "ame ana ar.clauorJed. p""ked. :natked, atId IlIbe~ • ."d are ,n 011ro.pecl3 in pro~.r cona,Uon :0' :ran_port ':1V hl;;hway ac:::~:"; :0 acl'lic;.llli. ,"'omaben" ana nall"""governmant r09ul8llons,II I am a largo auantlty goneralOr. I cer1lty 'I'IatlMvo a pll:11ram in placolo rodues tit. velum. and lexiCty al waste g.n .... lod '0 '1'1. d .... "'" I I'Iav. dotermined la t.oecnomically practlcwle ond that I hova solOC1odlh. of3,~lcaole m.thod 01 :reatm.nt. Slara~o. or :!j.pcsal ::;mnll;' avallante 10m. which minimlzo, lha prH41nl Voafuturolhrea' :0 human health and Iho environment; OR. If rom. smal. duanllty qene'lUor, j nav. maca I gcod flllih amn:~mmlm". my .. uta .in.tallen and sa'e",~n. cast waate mana.gement method tnat is a'lailable 10 me a.nd :nat I can .affcro.

TI 17. 7ranscorter 1 Ackn-owlo8dqement ot Receiol of Mate"LtsR

ISigna,tur.A _ Pnn,ledlTypltO Nam.

.J. (",

N -/, K, .:_: 'j l; ,..:,'- ,- or. ., .s .... . . ..p

la. Tranopor1.t 2 Ackn"",'odgom.nt 01Receipt 01 Material.QR

Ptln'adlTypltO Name ISign~TIR

HI. Ois<;r.paney l<l(llC&Uon Sp~

Montll O.y Y..

1-:"-= h" /i Ii:';

MonriJ D.ey Yur ir

r , I I I' •

--- ....

TIERRA-B-004762

866300164 TIForm ApprovN. OMS No. 205().()1J39. &ll:i~!f:30-94

. UNIFORM HAZARDOUSWASTE MANIFEST

3.<J--.n ......."""MoilIn<l-

Chemicil OJmpounds2975 Rivenide ,Ave.'-O' ...mcr'lI~( .,

Newark.

!..T,.,....,.,...,c-..-Maumee1.Trv>o<><>rt- 2 CO"'lMl"Y- !'

Q.o_",, __ """$lO·~R.inec:o1007 Vulcan Rd.-HaWill •Benton. AR not5

..

LNon-Regulated M~aJ. (Dye)Q

p;H:1...,... ~w.l:J+-L.+...L..Q...Q.I~-=----4~~~~~AT

oRI-----------------------------+-l..-l..-+-l..+~~--L-L-+---I~::::.:;;;::.~~=-Ic, '.

'.

III. GENERATOR'S cERTlFlCAnON: I M .. by d""""'" ~ th<o Cont"nta of tIlia cona!gnman1 .... fully and occurataly doacnblld above by P<OPM ahlPllIOll name and ;",ciuoifled. pa_. marked. and labeled. and &I'll '" all .. ll\l4lClS 111 prop ... condition for ~ by highway 1ICC0rdloll to "llpllcable Intemanona! and nallonal

government re<.l"Ie~ona and Atl<an.- awe ~"IaIIon ..If I am • larg. Quantity \I"noralor, I certify that I hawl .. prognlm in p"",," 10 ..m.e.. the 'olumn ""d tQlCicrty of weata \I ..nerated 10 the dl>\l ..... I haw dat"rmined 10 beeconomically practicabl .. and tnall hlr; ... Iectlld tIl .. pr.ctlcabl .. rnetllod 01 t...~.n1 •• tOfall", or dlapoul currantly IlVIllobl .. to mo wtliel1 minlmi ..... the pre",,", andlutunllhraal 10 human h ..aI1tl and the """"""",01; OR, K I am • ameli Quantity gon_or. I haw mlOde • good faith otlor1la minlmlzo my wuto gonoratlon and oelectthe boot wul. managomom m"lhod tnalls s'o'Sliable to me andlhall can alfonl. .

T:~.::;::~~=~:;:.:.;.:;;:..;;;.;..;.::.;.:.:.:..:-..-----------r;;;;;;::.;;~---:--:----------~=""'"""':--dH~ /,~~l!l.:.;~;;:::::;:~2:.;~~~::::=-;::;,:.:cl~R;:-=::.:o/:..:--=:.::;::...--------r.;;;;::;::::::--------- """"'=.,--=-_.."..-1T ~-I!

"- o.y -

.'Il .......

. .- ...! ",

EPA Fonn 8Z0o-22.(Re",,9-88) PrwIow.edtlOl'llaabsoletLNonCE, TlfE ORtGINAI. ANO NOT US$ Tlf .... TWO (21 COPIES MUST MOVI WITH ALUlDOUSMINT/STO .... GI/OISPOSAl. f....ClLITY MUST IIETURN TlfIS ORIGINAl COPY to TlfE OINI .... TO .. ----:-r,--;------------ -... .._

TIERRA-B-004763

.r, 866300165Slate of New Jersey

Oepartment ot Environmental Protection and EnergyHazardous Waste Regulatfon Program

Manifest SectioneN 421, Trenton, NJ 08625-0421

(F rm deelgned !a, lUe on eille (1:Z-oltohl typewriter Itv rI t I bl k I t1 Farm AoDf'tJVWd OlA8 No 2C5C-1Xr.J9 &: ru 11-30.'8.5. p. or p n n oe e e",. a Of

UNIFORM HAZARDOUS W~iISqS~,;°i;1,7~,71~r;~eg2.. Page 1 I Inlo,ml!len In Ihe shedltd aro"

I WASTE MANIFEST o! I Ie not 'lKlu1,od ~y Flde,ll law.3. t::itra1ot'. Noml and ~ling Alld'..... S 'ZjI. A:S~.M8M.1l D~r§trnl33 '., ,~/C.AL. Qrfpa~H:> ~. ;~NJA~ t ." •• .~~~

:23-7S A;VOt:.$,'DC ,4v~ '£NA~I<I tI.~ 07/0"/ ik;$l~~i1~~T~~.\>4. Gen8(at"r', Phon!! ( .;LeI 1 .of .8~-..3:U1O. "(J.sP'Jno' I cympan<::!ame a. us £FA ID Numa.,r C. Sllr. Trail ... IO-U.IOEPE ."- I , J ,.:::i, Z, "",

I LDoV EJ: J a,A(P; IV~J;r:7d,OII ~7I'iI31" •.-:,:,;~, ..... 'Cecal No.~·-'.;·, I ) ..:J,1;7,7 '~'r

I 7. Trat1spon", 2 C<lmpany Noml 8. US CPA iDNumOlH o:.l.Tnu'spOrtor'sPhQiiio' elf Dc' ,7111-:7rPr I I I I I I , I I I I E SIale Thln'.IO-NJOEPE ;"'1'" ,:"~,; ";:,~~ .• ,

I9. ~gnll'" Foclhty Nama and S;le Address 10. US EPA 10 Numo .... ~/,~;~.,-, Oooal No.- "'I:,' ','-"i 'U:>OV~ f..:.O;<.p, F; Transporter'. Phon .. t c·";> .~).~ .'••• " .. {.-. \" ;. ~..-; .x.T: / Si71~ Kb. {,:5":J.. .

I\lrAiI1~ 71Zr'1I¥I3Il.fI'l,,3o. Slat .. FaCility's 10J' .,"" .....7<077'~'77'-::',

A'<VCI'/JA, 'h. ;J..;$OO¥ H. Facility', Phone (6'-J<T~6"-

US DOT Do.criplion ~c!udlng Prop., SllloPing N.vn ... Haz:ua C:ass 01" O!vi$Jon. I 12. Comam .... I 'J. r 14.I.I'.

I ivceTCiaJ i Uoit ;, HM ilT.'iumo8' and P3ckmg roup) N,~. CL;a~tltv IINWcIJ W&s:s No.

a. I I;(t.t W~;;;r!: r:"''ilt8·-1£t.£ ~Q,~' (;;/ N.O'~" 4/

1010i1 iJ~/,8'~dG:~ CJ. "''- jX {1f£THAi""4.} ~~£N'£) 4"'1"113 f Pt;. tz:. lao~i Ira 0;'I I . .a, o.

I I 1

I I Ic I ." I

,= I I I I I I I i :f': .~ I~

I/ ..... c.

I" .'

'o •

rc

I I I I I I I I ',f ·t 'I:" ,<1.

I l I f ~,~;;;.' : :J' '.

f I I , i "I I I I"" I II J. AddjjJonaID •• ~orMalonaJs~~&. d. .... ,,' JJ~Atlb.i.:.{~ K., Haoaling Cooos:or Wastas (.,o,od Atcw .. t1,"f:t1I!:t.NQ "'~S'iJJf:~; - ~ '.J<:'~Nc~~ . ........ .... '~4#~< .,;"·t...,~;'..;....:':::'.i . ~~., . fiifJJJ.' ,.' , ~·~~~""i!:~::;~··!~'tI.~ ..~, ....-:~:~.~~~~ tiii .;. ·c.....·,·~;·-i~~ -."'l<"~':'",:~.,-~JM; ..~:·lt;t·.. 'I;AA~ . .;;r..;:;., ~:-~, .....•. :.~;~:~:.;.:; ~~"'.:·."·'·,1~".;~ptr,·;........" .. ....-!--i-:~'.~;' I '.- ..~.'.,.. ·;I:".:·'I·~-;

·:;,:;;fif¥;~-~:;~~~:;~':~~;:;::~l?·[~>(.;<-T' _.,~».:~:~i~:?~':~i-J :f}:~':-.':~.!'~(:::; 'j ;:'., .... ,.'. --.' .... -i r;. d. ," t f 'I: IS. SpeciaJ Handling Insl!""uonl and Aaditk>n81 In/armlIlQn

Ii ".., /". .~--.. I.· /Ii~~£(:<01) 'l-gS-3~1 GUI"P~ IUE"1<..c."EHc.y gaol< .r.l> -;]7

~Ii. GENERATOR'S CERT1FI~T10N; I tlBi&ey C8c:arl 1!1a.t:na CQntef'ltS of Ihis co~s.ig:1ment are fUlly aile accurately d8!1crlCec: Jice'/t.oy Oicper .sn,op •.Mir;l"ams ara us

I c:.... ified. plckeo. marked. and IWeled. and .,.. in III '.'P"ct$ in proper COndillon tor tran.oaM ~y highway acco'ding ~Q -'l:l:;;CIC," .nlomalienal ana nallo."aJ

Igovemm.nt reQullllons.

If I am a l8NJs quantity g.no""Dr. I cortIfYIhaJl hav. a program In plac. to noduce the volume and loxlolty cf waS'" gon.rated 10 ,,,. d89'H I have dOl8rminod 10 ~IaconomlC3J., praC:lcal:l. and lhat I ha," seleotld t~.. p,ao,ical:l. motl1ad of "utm.nt. slo/age. ot di.spooll O1lmlmty ..... Iaol.'o ml wnich mln,m,ZO. Ihe P.... .m an<!future threll t-q hllrnan hea.llh arid th. MMrcnment, OAt :f I am a small quanUty r;8nerator. I !"!~..... mad. a -geod faith ttl'eft ~o r,-:lnlt':'::.:" my WB.-'tGt;S(19r:llion 1nC s.tee:, ~e besf ·ifs.ste mat'lagement :TI8th~ tt'r"t is avaJlaDl" (0 me ar.o ~tuu I Ca1'1aNC.f::l.,Fnn,.afT ypeo Nun.

r j ~1. iransoonM 1 Act<nowle<:lqlmef'lt of R1'C8iC1ct Mllt&nal'$AA Fnnl"!!iTyprtd Name~ .,...;;.. ~ _ .:,'7p

~~~'::':':~::';';'";~::::!:::::'::':':"::'':'::::':':::''':::'''::'=~----;-;;;:::;=:--------------_-;-;-~-=-_-;-;---l.TEA

18. Tten'llOnor 2 AcknowMdQlmlffit at IltcetPl at MltorlaJsPnntealTypld N.,."e

(.

T ~L I---------c-~-c--:---:'''':'"'"'':_:____:_--~--:._:____:____::__:_-__:_....:.....~_:_:____:_:::__--------_l c..~ 20. Fac;11ty Owner or Opel'BlOt: Centflcmlon IX rece<P( af hn.doul mitenllll ooveted by tltIs menl!elt .. cap! U nolod In 110m 18. l-V PrintedlTypod Name ... Signature y.., C.

&~.;:.:- ..~~~'"" •Monm

EPA Form 8"71»-22 (A ..... lilM) Pi'evloI.iI: ~ .. ~8 -::-GENERATOR COpy, .-

TIERRA-B-004764

PI .... type or prlnt I" blocK I. It.,..

State of New JerseyDepartment of Environmental Protection and Energy

Hazardous Waste RegUlation Program .Manifest Section

eN 421, Trenton, NJ 08625-0421(Fo"" dn'!tned lor use on 1111. (12-llllchl lyPIWl1l11r I .. " '0

866300166

d.

'I UNIFORM HAZARDOUSWASTE MANIFEST /

1. G"ne,acor's us EPA ID No. Man,t ... t. . ,I POCU'l'lnt ~o...ulll n 11101.,1.:./;;,/ T 171 ~I or/ 'if' ,(r,( ';.;q; 2.. PI!te t /In'Olltlai1on ilt the shaded ar~u

at r '. .:" nOI ,equil'ed by FlOderal I....J. Generato,'s Name lnd MaJjjng A<ldrl" Olea:ical_~ J' Inc.29-75 :iiv-erside .A,,~

. . New<lr'''7 NJ anOt/,pr:, ~'n'T

~.,.",~~-,\.;",,- '. r ..~..

4. '!'Geri:;';;";; Pl>oIie( "m ,~.. T'aNponer 1 Company Nam.

"-;." :":'t, •• '._ 6. us EPA 10 NumoerC.);i.~"r,.a;,i;; I[}.NJDEft.~"§f' - :-::,"J,:- r', I, 4

~. k;. h h P I:> IT h h J> i ~, '.;".~;,;r-..";.EJ.ce!.Na~/,'/a. us EPA /0 Numoer ,C•.T""~~~"oOi\! _ 't":

J I "J / , I I , I ! , :e.·StotitTn.m fOoNJOEPS-:;:i ':, :s,:'~.;+:US EPA 10Number ::::'~~>::::-~Ooiao(NQ.':~::";I ..••.; '.~)' .....,:.

F: .Tranoporrer's Phone r--r~:,'j' .. ,.'

~~t.;'; TT" r". 'r_. ~:,7, Tr.nspoft., 2 ComplJIY Naml

. r,"<,

./ :1, I " HJacijllys.Phorie (""I.£:li.;": l'\"1n ..

I 12. Coma,n",. I _':1. - I 14 I -, rI Icfal L UnttI No. ! lJpe Cuan"ly !WWol Wu!e No.

II

J I .. J.l, I I I

.-. ;...~'": ,.a o. ....~ .\.

"=" jx• C•

70R

..,z~

! I ~-~.- .".-!, YO 0' 2'f IJ.1),I'I' ... r ,\'1 .. I ,

I. " "~ - -'5'I.;'i& i~'.i... ',I;' 4f'

O.

/-. ~"'~.I I I • r I I

K. Handling Coces 'or W/I5[8I ~"<l Above

• ':c:t:;.··~: \:r'S:;i01~·\·;+tF¥-~J,~,:1,~~~,i1.~"I'·

") ~ • ".Jo;';'_

• b:" "Z. 101\ 'I!;. Spac'aI H':IntJlin'l In.HUCtIOM and Aod~,onaJ Inlormano"

~gElIXry' l1es:xmse it 1-&X:--969-9252

l~. GENERATOR'S CEATIFlCA'nON: I h"'&tJy - •. 'Ila"h. comonr. o"hlS conSignmont are fuliV ana accu,ately oescrloeo '00',. oy prooe' snip",ng name Snd ",eClaSSllled, pacKed. marKed, and labOll9d. and are ,n all r.speets ,n proper COMllton to, IranS-pOrtoy h'gnwIY accordong '0 'PPlieaOle Inramariona! and na'ionllI1cv&rnmenr req~latiorls.

It I am o large Quantity genlllllor. I c~ thal I have I program-tn place 10 reduci the volume IndlO.lclfy of WM'" gl""f3!!'d 10 rhe deg, .. I havi dele"",nl<j 10 Oeeconomically prac1Jeatlle aM till' i hllVlt sEtlec1edIh. p,actlCabJe mllhod ot fr.almenl. slorlge. or d .. oout eurlllnrly IVlnaola to ,'nl Wmell m'ntml:" Ill_ pres'f!l 3Mlulurl IhrOallO human hea/lh and 'h' envlronm_n!: OR, If I am a sm.il quan,iry gen .... rOf. I have mad •• ;000 'allh e11on!o m'nlml" my 'Na,te glnera"on and ""eCl1"e bt15~ Wllste management me1hod that is av ..r1able to me and that I can afford. ..-

p~a~YPe<lN~ /fl?lcJR~ C~Lc~l,gn:~ /~.~, ~ransoort ..;:j Acknowoaaqem.nl 0/ Rec.ipl 01 lAalenals L.-

P"nU'dITYPed Name, /. ,_ I. t f"'\, 1"\, ~ ISigna""e, I A ..1... I) ~.nE ~..w. , .nU~ I::J..J. f~ A r II J1. JY.JJ''..l

18. Tran.poner 2 ACknOWledy<>.".", 01 A8C8tpi ct M.,enlllS • CI

MOnth Day v(l4r

101"0!~ 111~r-,

19. Di4crep~ InoleatlC/1 Space

~-" ~rt;"_~ lI-"' "'"'.. 0<: •

.~ .• "I- .. .'~ ; ....1-·.,;.'·~:" . "••. 1-· ... -~- ~-;-. ,.....• .... ~.- •• ',~" --=:- - ......

EPA Form a.1QO.22.lA .... ~~ ~ ed'.Uon •• ,...~.

3-TSD MAILTO"G'ENERATOR

TIERRA-B-004765

.I.....~A·...-...".;",;~~ . , _ - .

•. J ' ~-~~~Mitalc.'·c, ' : " Slate of New Jersey \'.~ , •.;: ,7' Cepartment of Environmental Protection and Energy. " .....: _~ .:. Hazardous Waste Regulation Program

'~f- ~ " ,. .'S.'""~""",,:. ,.,-"" -- Manifest Section - -.~ '.;0 c., .... 'i'.:..,U - '.:: t- .' eN 028, Trenton, NJ 08625.~028,:,'·· .• < ,<., <... tyP.OI'tiint r';1iI:ick lonors. (F"nn d.. i9nad ,,,, us. on out. 112-pllc111ty;Iawrll... ) .- ~. Fomr AOD~, OMBNa. 2050-0039, &Oi~. ~-e-~~,";J--UN1F.ORM'HAZAADOUS I 1. GO~O''''Or'' US EPA ,0 No. . I Oo~::~o' :z. Pa>;o \ 'l,morrnallon in lh.onadod oroas.q:''':I}'.:',WASTE MANIFEST I....I r In I, r t\ I" I, r .. I, r .. ' .. I.. , I' I T' at ,- Is nol ,equi'ed" by Fod.raI law,

866300167

"'Ii. ~ll( f-.~,- - .....,~:. ' -. -"-,., .l'-.~~ \k(~

~;':'f~ (~;""t.J.

I I

~I RQ~WASTZ,FLAMMASLE LIQUIDS.M.O.S.X . t"!mPT3NE '~.F::'n::) , '1"JrQQ~ l'r. ...-

'I . I'l 1(\ 11 "l" '" I n ,5'Q "fO ,..

i..aI ~~:.',~~~~~:;..:'~;~

~, '~1~::~~~:\i;}::f,~.·~:~~T.~~f::~l(-

-, r r I I I , :'~"i,~~v{r-:;,'4.

l ..J;'_~~~~~O~p~~I:l?r).1~~~~Ust.~~:~·,.;-0"_ -'.. - 0' J~'-:---~ - -':"_,. -: ':(':,_0" K..ti8nclin;C.xi&Sfor.W~.S,UI.!~~·-:~·.::it.-

~~~c¥~,~:.~;t;,~:~:~;·~~~4h~,;:~~,;/"~~:~~-i2:~~~·;~~~~~if~.~~~~~~~,~\t~;,;~t~~::c~2;t+';;h::.j"J~.. ,.·~~{~;+;,~:~~~~r~c~~s.S:~f:'~f·3:}~~'::~\~f:I~~i~i.15. Speciai H,anaUng In$l!uetJM4 3<10 ~noj InlorrnabOn

EHER!i.ENCYCON"tACT: CB:EM1'!U:C1-300-4:'4-9300CAr r E:g 1roSl: IDESTIn V.lN· 'IL"'Di.S & ROGERS AS SRI!'!'!.lt.

16. CiENERATOR'S CESTIFICATLON. I ~",.oy o.<.:ar.,'n .... ,no ccnt.O.'. 01 L~1Scrm"<;nmem are :Ully ana acc:muely ~"'Cl101Kl anO'/. oy ~roper SI1IPl'ing nam. ar:a atOclusiflad. pocked. marked, and Iai:l<llad, .~ are '" all ~SpOC1S In P~"' conolllon rer lran.oport by hl~nway a<:con:llng :0 o,pplicabl" Il1tamation!IJ and nauooal~lJV8mmant~la1icn.s.. .__ -=- .... : ..... ,_ .,. •.• ,. '. ,. '· ... ··1 - . .

" I ..;,:, a ~~ c;uantity g.no .. tor.l certify tI1all have a proqram in plac.lo lBduc. tho volume and to:rlcity '" waolellonolllled 10the d"9f1'" , hllW dolormittW ta beoroncmlCally PfOctlcalllo and tnSlI_ ~actod the practicable m"tnod 01 tr.atment, storage. or dl,oow c:unontly available 10m. which minim in, th. pllIaenl andtutu,," threat 10humen noalth and ilia .nvil'Otl"'anr. OR. jj I am a .mall quantity genermor, I na"" made a geOd taJlh e1lort:o minim.. e my w.... to gan"'abOn ond ."actIne aeS! wa,ta man,""m.nt meth<:d thal i. aVilllaala :0 "'. and thaI I c:ln aNord. •

i I"""

ISi9nalutK: ~-~/;~d',,,~,~:..- ,.."" ."..... .',

I~~~_,c;;~;;;r;~~_

6Momn Dq YoUt ::

" I I I I I ..

,,-','.' .... :"

'.20_ Fo.clJlIyOwnIKDr Op~Ca<tIflcatlon 01rocalpl or hazardool ma~ ~ by thlo "'~ except u _ In lion'll"

:'::'.~nt:!1~fN~r<}}at:1J~/1?'1i7;.;:a1~~~~~~~~~~@'h6~;-,;; .11;~ : 'A;'"EI'''Form811X>-22(_,WUl~-----', ,':., ::',':'.-:.,,~,~G~ry.~E,.~~PI,NfORMATI?NMUST Be'll!G1BL£ON AU COPIES:l-TI;O MAILTO GENERA-TOR~". .._',.'~ "__ ,~_~$l*-'_ .--.' ••. l/

TIERRA-B-004766

866300168!C

TIERRA-B-004767

-

-

OCCUPATIONAL HEALTH SURVEY REPORT . i

PREPARED FOR:

Chemical Compounds, Inc.29-75 Riverside Avenue

Newark, NJ 07100

CONDUCfED BY:

Joseph N. CapuzziOccupational Health SpecialistCIGNA Loss Control Services

ACCOMPANIED BY:

Mr. Arturo CelleriSafety Manager

DATE OF SURVEY:

October 3, 1995

866300169

l"LUJIl JlIAD CARUOLLYT.... ca ..,.'-I -...... I ..... .,. .r,. .. sw-~ .....,.,1IIt, 11' _ ( ...-18 1Iotq,..r ..... _.ppIW .,or,....w.t)Ie, tIL r .. .,.rtlnllIot __ .r "'111-. ,., "-UO' lIN "IlOl""""""". - tor..,..haI ..,. -,.r 1tpI ,... ... , flw ,_._ pupo_ It .._ Ie "* ...,.1Ipl....,.,.. _, ..... to ........... ar•............~.....- - .

TIERRA-B-004768

~'-." --:. ' ..

-

........'::;:.' ~. :....,; -'

Clu;mical Compounds, Inc.N~ark. NJNovember 9, 1995Page 1

. INTRODUcrroN

On October 3, 1995 an Occupational Health Survey was conducted at the given location to evaluateemployee exposure to various airbomc contaminates. An executive SlUDmm:y and ~ts of the surveyfollow.

The data presented in this report reflect conditions as they existed on the day of the swyey on whichthe air sampling was pcrfoImed. InfOtmation, as supplied by plant contacts was relied upon to help indeveloping conclusions and in the evaluation of programs discussed in this report.

STANDARDS AND GUIDELINES

....StandardslExpOSUIC Limits for employee exposure to various materials evaluated during this survey arediscussc:d under the Rc:sults heading, and also found in the Data Tables of this report (See AppendixI, Table I). Infonnation on the sources and types of standards and guidelines arc listed in Appendix II.Generally employee exposure results are compared to cum:nt Occupati&nal Safety and HealthAdministration (OSHA) regulations/standards, called P~ssiblc Exposure Limits (PEL), and can befound at 29 CFR 1910.1000, which are often called the Z tables. Where other accc:ptc:d State-of-the-Artindustrial hyiienc practicc:s or guidelines, such as the American Conference of Govc:mmental IndustrialHygienists (ACGIH) Threshold Limit Value (TLV) arc lower or ditIerin their approach the most currentvalues for these guidelinc:s have been used and Dotc:d. The use of these standards and guidelirics arethought to give reasonable protection to the health and well being of employees exposc:d to thesematc:rials. Please see the Appendix section of this report for the results.

The ACGIH TL V's arc inc1udc:d in this report as exposure standards because for many substances theACGIH TLV's arc: more: conservative than OSHA standards. The ACGIH TLV's arc more conservativebecause they are based primarily on the prevention of disease. In contrast. OSHA Pc:nnissible ExposureLc:vels (pEL's) are rc:quircd to take into account the ecoD.omic feasibility of rc:ducing exposures inaffeetc:d industric:s. public notice and comment. and judicial review. The nV's IIlC guidelines that referto the airbome concentration to which it is believed that nearly all workers may be repeatc:d1y exposed,day after day. without adverse effect

EXECUTIVE SUMMARYAir sampling for ethylc:ne oxide, xylc:ne, nitric acid and methanol reveled that on the day of the survey,none of the employees' exposurc:s cxceedc:d the OSHA Pc:rmissible Exposure Levels for the abovecontaminates .

Rc:commendations for the implcmc:atation of your rc:spiratory protection and confined space programsand for the installation of an emcrgc:nc:y eyewash/shower IIlC being resubmitted. New recommendationsfor improved housekeeping and the use of eye protection are included with this report.

866300170n.un Jt&.U) CAIlD'OLLr .

TWo_,..,bu --t.,,.......-. - -<--II....- ~.' - rw.~lIor"'l"'"1MM .,..". .,rIIk - ~.- • ..",.. II- ,.,.--h .... '..,. ..-iI7M _, ,..-...,... 1111_ .." ...,7M •• , ..,.............~......-.......... .

---- - --~~...:........~---~ ~,-,~._. '_-_A .._.-~ '.,--

TIERRA-B-004769

C1}~cal Compow:u:ls, Inc.Newark, NJNovember 9, 1995Page 2-METHODS

Air Sampling

Unless otherwise stated, samples were taken in the employees breathing zone to obtain samplesindicative of the actual employee expOsutCS. Gillan 513 and 113 air pumps provided the vacnumsource. Pumps were calibrated prior to and after the samples collection and were checked for properoperation and flow were necessary and possible. No changes in flow rate were measured, unless notedin the comments section of the results section. .

Air samples collected were analyzed by Environmental Health Laboratory in Macon, Georgia andCromwell, CT which are accredited by the American Industrial Hygiene Association.

--RESULTSAir Contaminants l.

Table I pres.;nts the results of air sampling and analysis. Exposure concentrations are presented inmilligrams per cubic meter (mgIM~ or parts per million in air (ppm) by employee and location. Alsopresented, arc the applicable Threshold Limit VaIue (TLV) or the OS HA Permissible Exposure Levels(PELs).

'.

DISCUSSION

Air Sampling

Chemical Compounds, Inc. is a mllllufacturer of dye intermediates for hair dyes. Various chemicals arcreacted in 6 reactor vesscls within the plant Many different reactions take place, however, of majorconcern from an industrial hygiene standpoint is the reaction involving ethylenc oxide. It is one of themore frequent reactions. Ethylene oxide (ETO) is a highly reactive gas or liquid that can affect the skin,eyes, lungs, and nerves. Ethylene oxide has been found to cause mutations and cancers in animals.Based on these reports and human epidemiological studies showing a higher than expected rate ofseveral cancers, ethylenc oxide is considered a suspected human can:inogcn.

Nitrogen is introduced into the reactor vessel The prcsswc in the vessel is then checked to assure thevessel is holding pressure and there arc no leaks. ETO is then piped into the vessel from outside of thebuilding. The ethylene oxide is reacted with 4-fluoro·3-oitro8l1a1iuc (NF A) under pressure withpotassium. fluoride added as a catalyst to yield the dye intermediates, NHNF A.

Personal and area sampling for ethylene oxide indicated that employees are exposed to levels belowboth the OSHA Actiou. Level of O.S ppm and thc OSHA Permissible Exposure Level of 1 ppm. lIS an8 hourTWA.

866300171ft.&.Ua JI&AD CAIIDOU.T

TIllo _ _ • ..-, ,.. _-(wIIIdooowto 91"' ...-.- ,.. .. ~,.,. ,..,... rw. ,.,.- "...- .. _ ,.. ......_. -1oC1 apaot 1opI ,....,,....,..,... .-- Jtlo __ ea .,. .... ..,,....,, ea __ •••--..~ .,...-.

TIERRA-B-004770

),ical Compounds, Inc.N.... ark, NJNovember 9, 1995Page 6

TABLE I

)

.- ..' .i..

:1 Sample 1 Location

~ Carlos Molinll!~ Operator

I QKJ#2 IArea Samplc1It reactor

ethylene oxide

SamplePeriod

AirContaminant

10:24-2:51

I ethylene oxide10:26-3:02

< 0.21

• Standard!Guideline

2

<0.2

xyleneXIII Petro Naranjo!un operator

< 0.34

1:59-3:02 xylene

I ppm

F~ Petro NaranjolI- asst. operator

I NANI Carlos Molinll!L- Operator11:36-2:52 nitric acid

<0.34

< 0.053 ppm

100

100

11:36-2:52 I.I.... _ ... ,I.. _ll_:4..5.-1_2:_14_1

.... -...""""'l!.......=*=== __

I NAII2 Carlos Molina!I- Operator

I M"lJ Petro Naranjoll.-.- usL operator

nitric acid

methanol

< 0.05

< 48

PLUSI RUD CARllruLLYTIIlo ..... IIJ U. __ lWIo IWY., .,)'Hr or .- (... IctI.n .. " por\IIMat I. Ulo """ .f Inooro oppa.ol r.t or pr •• ide4)ro.. IM.-- .f'!'l'P" 1M f All, 110.or .. ,.....11.. pr.,._ II M.ill f.r.oIYko... • 00'" ...., or 1_ ,.. , rote.. 10.ro" .- plA"po_ II" MIIMooolooIIoo."lo.l •• , Iopl01"" ,.. "'J " I. proY"" • oar.pmo......... ,.. ... ..,...... 'r .p....IIoL

200

2

TIERRA-B-004771

-

'-:.;. ".'., -~--.. - . .~.:~.~. .-",~. ~....

Chemical Compounds. Inc.Newadc, NJNovember 9, 1995Page 1

'.

"

'. APPENDIX II

866300173rL&AR IIUD e:.utDOLLT

T... _ .. .., ............. _ .. :r-..............-. ....,.. (wI*Mow .. ,.- .... ~ lW.............,..... ~ ..-.-. .. .friok_.il ... AItf- ~ --lW_h••• lot7wqoort.IopI ..... 7"-,. ........ ,...-......- Il _ 7"..,. - .......... "---..~ .......-._ ....

TIERRA-B-004772

Chemical Compounds. Inc.Newark, NlNovember 9. 1995Page 8-

Standards and Guidelines

A listing oC the: appropriate he:alth standards can be f01Dldin the following table. Included in tbi.s tableare the following:

1. Pcmrissible Exposun: Limits (fitle 29 Code ofFedcral Regulations (CFR) Part 1910.1000). The:PEL's represent the legal exposure limits set by the Federal (or State) Dc:partmcnt ofLabor/OSHA.

2. The 1995 - 1996 Threshold Limit Values which arc: guidcJine:s developed by AmericanConferc:nce: of Govc:mmental Industrial Hygienists (ACGIH) to protect the health and well beingofwolbrs.

For a compTete listing and explanation of the use of the PEL's and TLV's, please consult the abovedocuments/sources.

OSHA Pennillible Exposure.

Acorn Threshold Umit ValueLevel (PEL)l (TLV)'

Substance Units 8-Hr.' STEL4 ceiling' 8-Hr.' STEL4 ceiling'

ethylene oxide' ppm 1 · . l,A2 - -mctlw10l (skin) pplll 200 · - 200 250 .nitric: acid ppm 2 · - 2 4 -xylene ppm 100 · . 100 150 .. flil. '~1mKe ~ 1. II Itt !:l1L.1UU, ety-

HMIIh~'1'brabold L.iIllit V&buo publilhcd by 1be Ameri ... Cottferolu:e of Oovemmeatal Judullrial HyPnJsa (199<4-1!l9$).Tho tJ-~ a--e- for .. II OC' 10 bu... wode MiA ia & 010hour .... --.Short t.m .JPImUII limit (15 1Ilillul.o.).Ceiliotclimil, 1be com:onInlion IbaI ohouId tmI: be o~ oIurinc IQ)' part ofb wodWlc oxp_PEL fOWlll ia lite ~iWl OSHA Staodud for E1hyIcno <mole (29 CFR. 1910.1041).A£:cioa tn.l 0., ppn.

.- 2- TLV

3. I-Hour/IO-Bow4- SlU.,. Ceiliq (C),. ETO

•••••• A.l•••••• A2•••••• A3•••••• A4-•••••• AJ•••••• me

CaItfiIm8d m- c.eiaoa:aa;s.-pocUd II1Jmm e-iaoe-;Aaimal Can:iDopa.Not Caaif1abt. •• HaauIa Carcitto~Not saopoc:tod •• Httmaa e-iaopa.aoDce ol iataDded cItaap.

..- 866300174PI.&U& DAD e.utDOLLr

TIlIo ..... ., ... -..... • .....".f,... w ..... _~ ."..r_..,... ....._~flH'dM,..,...., ,....frloll-.Wi A.,_ •• 1_ ...__ Io_ ~ ..........'"- •• fol7..,.n 1IpI-,... -1 ......... ,...- _ RIo__ """ oloiIT,.....,. _ •••...--.:-.......... ...-.,~-

TIERRA-B-004773

.' - .-"",: ... ;':' '.. ." '...::: ~:.,:... :.:,..

Chemical CompoWlds, Inc., New-lIIk, NJ

November 9. 1995Page 9-

.,

- "

-

••

APPENDIX ill

866300175

PJ..&IoG JlLt.D CAaD1lLLYT....... po.,. --""J.,,.....-. er.,.....(~ .. ,.....,. .. I;J'JIO.,_ er~fw .. .--.,~ ....-., i Aaf- _- .--. .......... • fat1....-- ........-.17"-" - ,... .....,....nlo IMJ' ...,.,....,. ,..- .....-....;~ ...... ....-- .........

----_._~~

TIERRA-B-004774

-

--

-'

Chemical Compounds, Inc.Newark, NJNovember 9, 1995Page 10

METHODS TABLE

Analyte Flow Ibte CoUectioD Media Analysis Analytical(liters per Methodminute)

ethylene oxide 0.1 Qazi Ketcham tube Solvents by Gas FID;NIOSHChromarography 1501, S286

-, modified

, methanol 0.178 silica gel tube Solvents by Gas FID;NIOSHI

. Chromatography 2000

nitric acid 0.2 arbo S3 tube Anions by Ion Conductivity;::. Chromatography NIOSH 7903

xylene I 0.2 charcoal tube Solvents by Gas FID;NIOSH

i

Chromatography 1501,5286 .• modified•

FID ""Flame.Ionization Detector.

866300176

PUA.Q DAD CARDtlUoYTIda ....,. .... ....,.... • ..,..".et,.....--. __ do_(wMdooow .. ...- .. llIelJpoet-..-.,.-'er ..............,,... .--.r-a..Go __ .rrtok_MI A., ......... _--IlM ............_....._.~ .....II'.- •• feI7..,.n lotM..--,... -r - ..r- --.-,- It II _t~ .. ..,,- ..,.Iopl ....,,......, .._ ..... wertqoIaa,~ ... .,...-

TIERRA-B-004775

866300177

TIERRA-B-004776

.,-

866300178,,~"'"- 0'""<'2>

NOV 23 1981;

DONALD LANSSCRerARY OF STAn;

CERT'U'rCA'l'E: 02' :I.NCOREORIl'l'IOlf

of


THIS IS TO CERTIFY, that I, GEORGE L. GARRISO~

do hereby associate myse~f into a corpot~tion under and by

y.irtue of the provisions of an Act of the Legislature of the

State of "New Jersey entitled "An Act. Concerninq Corporal:ion~"

(Revised statutes of New Jersey, L937, Title 14 and Title 14A)

and the severa~ supplements thereto and acts mandatory thereof

and do he~.bY agree to take the number of shares of capita~

stock set opposite my name.·FIRST: The name of the corporation is:

CHEMICAL COMPOUNDS, INC.SECOND: The location of the principa~ office i:

this state is at 1135 Clifton Avenue, Clifton, New Jersey 0701::.,: ~~ THIRD: The name of the agent therein and in

charge thereof upon whom process against this corporation may

be served is GEORGE L. GARRISON.FOORTH: The purposes foe which this corporatior

is for~ed are as fol~ow.; '1'0 engaga 1n any activity within the

purpo.e~ for which corporations may be organized under New Jers

.:.statutes Annotated, 't'it~.~4A •.entitled -Corporations. Genera~"

, . FrF'l'H~ The. name and post office addresses of..':.

TIERRA-B-004777

- "

the incorporators and the number of shar es subscribed for by:--,

them, the aggregate of such subscription being the total amou~

of capitaL stock with which this corporation will commence

businesS, is as follows:

GEORGE L. GARRISON1135 Clifton AvenueClifton, New Jersey 01013 .••••.••• •••••••• 100 shares

SIXTH: The period of existence of this corporat

is unlimited.SEVENTH: The total authorized1capital stock of

the corporation is two thousand five hundred (2500) shares ofI~ommon stock without nominal or par value. Allor any part of

said shares of common stock, without nominal' or par value, may

be issued ,by the corporation from time to time and for such

consideration as may be determined and fixed by the unanimouS

vote of the Board of Directors as provided by"law.EIGHTH: The number of Direccors constituting tn,

first Board of Directors shall be two and shall be:

George Moncayo 7 Berard Boulevar.dOakdale, Lonq Island, N.Y. H769

Anna Maria Moncayo 7 Berard BoulevardOakdale, Long Island, N.Y. 11769

IN WITNESS WHEREOF, I have hereunto set my hand

and seal this 16th day of November, 1981.

L •~

.~.866300179

': ."..:~..~. -- .. , ".' ,.....:'._ ....-.:~ .........

TIERRA-B-004778

..

_.

....-

- ,\

..~.. _ ....""f: '_:.... ; ••~.

STATE OF NEW JERSEY . s s • : ..-COUNTY OF PASSAIC

1BE IT REMEMBERED, that on this / r....;CL day of

November, 1991, before me, a Notary publico! the state of New

Jersey, personallY appeared GEORGE L. GARRISON who, I am

sa~isfied, is the person named in and who executed the foreqo~

certificate, and I, having first made known to him the content

thereof, he did acknowledge that he signed, sealed and deliver

the same as his voluntary act and deed~

JMIC[ A.INHEI!A ..lNOTARY PUBUC OF NEW' JERSEY

MY COMMISSION EXPIRES OCT. 9". 1985

866300180

.0;,-

TIERRA-B-004779

UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION2

290 BROADWAYNEWYORK, NY 10007-1866

',.: ,'~ 1 5 2GC3

GENERAL NOTICE LETTERCERTIFIED MAIL-RETURN RECEIPT REQUESTED

Alberto Celleri, PresidentChemical Compounds Inc.10 Baldwin CourtRoseland, New Jersey 07086

RE: _ Dianlon~t Alkali S\lP~4 SiteNotice of Potential Liability forResponse Actions in the Lower Passaic River, New Jersey

Dear Mr. Celleri:

The United States Environmental Protection Agency (UEPAn) is charged with responding to therelease and/or threatened release of hazardous substances, pollutants, and contaminants into theenvironment and with enforcement responsibilities under the Comprehensive EnvironmentalResponse, Compensation, and Liability Act of 1980, as amended ("CERCLA"), 42 U.S.C. §9601~~. Accordihgly, EPA is seeking your cooperation in an innovative approach toenvironmental remediation and restoration activities for the Lower Passaic River.

EPA has documented the release or threatened release of hazardous substances, pollutants andcontaminants into the six-mile stretch of the river, known as the Passaic River Study Area, whichis part of the Diamond Alkali Superfund Site ("Site') located in Newark, New Jersey. Based onthe results of previous CERCLA remedial investigation activities and other environmentalstudies, including a reconnaissance study of the Passaic River conducted by the United StatesArmy Corps of Engineers ('-US ACE"), EP A has further determined that contaminated sedimentsand other potential sources of hazardous substances exist along the entire 17-mile tidal reach ofthe Lower Passaic River. Thus, EPA has decided to expand the Study to include the areal extentof contamination to which hazardous substances from the six-mile stretch were transported; andthose sources from which hazardous substances outside the six-mile stretch have come to belocated within the expanded Study Area.

By'this letter, EPA is notifying Chemical Compounds Inc. ("Chemical Compounds'') of itspotential liability relating to the Site pursuant to Section 107(a) ofCERCLA, 42 U.S.C.§9607(a). Under CERCLA, potentially responsible parties ("PRPs') include current and pastowners of a facility, as well as persons who arranged for the disposal or treatment of hazardoussubstances at the Site, or the transport of hazardous substances to the Site.

Internet Address (URL). http://www.epa.govRqC .. dIR..,yelabie • Printed with Ve{lNb" 011Bned ....... on ~ P.... (Minimum 50% PoRcclnHnMr cordenCI

851640001

TIERRA-B-004780

t •.

In recognition of our complementary roles, EPA has formed a partnership with USACE and theNew Jersey Department of Transportation-Office of Maritime Resources ("OMR") ["thegovernmental partnership"] to identify and to address water quality improvement, remediation,and restoration opportunities in the 17-mile Lower Passaic River. This governmental partnershipis consistent with a national Memorandum of Understanding ("MOU") executed on July 2, 2002between EPA and USACE. This MOU calls for the two agencies to cooperate, whereappropriate, on environmental remediation and restoration of degraded urban rivers and relatedresources. In agreeing to implement the MOU, the EPA and USACE will use their existingstatutory and regulatory authorities in a coordinated manner. These authorities for EPA includeCERCLA, the Clean Water Act, and the Resource Conservation and Recovery Act. TheUSACE's authority stems from the Water Resources Development Act ("WRDA"). WRDAallows for the use of some federal funds to pay for a portion of the USACE's approved projectsrelated to ecosystem restoration. .

For the..frrst.phas~ofthe Lower P-assaicRiver.Project, the governmental partners-are proceeding.---with an integrated five- to seven-year study to determine an appropriate remediation andrestoration plan for the river. The study will involve investigation of environmental impacts andpollution sources, as well as evaluation of alternative actions, leading to recommendations ofenvirorunental remediation and restoration activities. This study is being conducted by EPAunder the authority of CERCLA and by USACE and OMR, as local sponsor, under WRDA.EPA, USACE, and OMR are coordinating with the New Jersey Department of EnvironmentalProtection and the Federal and State Natural Resource Trustee agencies. EPA, USACE, andOMR estimate tha~the study will cost approximately $20 million, with the WRDA and CERCLAshares being about $10 million each. EPA will be seeking its share of the costs of the study fromPRPs.

Based on information that EPA evaluated during the course of its investigation of the Site, EPAbelieves that hazardous substances were being released from Chemical Compounds' facilitylocated at 29-75 Riverside Avenue in Newark. New Jersey, into the Lower Passaic River.Hazardous substances, pollutants and contaminants released from the facility into the riverpresent a risk to the environment and the humans who may ingest contaminated fish andshellfish. Therefore, Chemical CompoWlds may be potentially liable for response costs whichthe govenunent may incur relating to the study of the Lower Passaic River. In addition,responsible parties may be required to pay damages for injury to, destruction of, or loss of naturalresources, including the cost of assessing such damages ..

Enclosed is a list of the other PRPs who have received Notice letters. This list represents EPA'sfindings on the identities ofPRPs to date. We are continuing efforts to locate additional PRPswho have released hazardous substances, directly-or indirectly, into the Passaic River. Inclusionon, or exclusion from, the list does not constitute a final determination by EPA concerning theliability of any party for the release or threat of release of hazardous substances at the Site. Beadvised that notice of your potential liability at the Site is being forwarded. to all parties on thislist.

851640002

TIERRA-B-004781

We request that you consider becoming a "cooperating party" for the Lower Passaic RiverProject. As a cooperating party, you, along with many other such parties, will be expected tofund EPA' s share of the study costs. Upon completion of the study, it is expected that CERCLAand WRDA proce~ses will be used to identify the required remediation and restoration programs,as well as the assigrunent of remediation and restoration costs. At this time, the commitments ofthe cooperating parties will apply only to the study. For those who choose not to cooperate, EPAmay apply the CERCLA enforcement process, pursuant to Sections 106 (a) and 107(a) ofCERCLA, 42 U.S.c. §9606(a) and §9607(a) and other laws.

Pursuant to CERCLA Section 113(k), EPA must establish an administrative record that containsdocuments that fonn the basis of EPA's decision on the selection ofa response action for a site.The administrative record files, which contain the documents related to the response actionselected for this Site are located at EPA's Region 2 office (290 Broadway, New York) on the 18th

floor. You may call the Records Center at (212) 637-4308 to make an appointment to view theadmin~~_~r.~ti.v.er~~or~JQr.the Jp~er rlL5~~~ver. ~r.oject.. .._ _. _~_._ .._._____ _ _

EPA will be holding a meeting with all PRPs on October 29,2003 at 10:00 AM in ConferenceRoom 27A at the Region 2 office. At that meeting, EPA will provide information about theactions taken to date in the Lower Passaic River, as well as plans for future activities. After thepresentation, PRPs will be given the opportunity to caucus, and EPA will return to answer anyquestions that might be generated during the private session. Please be advised that due toincreased security measures, all visitors need to be registered with the security desk in the lobbyin order to gain entry to the office. In order to ensure a smooth arrival, you will need to provideEPA with a list of attendees no later than October 15, 2003.

EPA recommends that the cooperating parties select a steering committee to represent thegroup's interest as soon as possible, since EPA expects a funding commitment for the financingof the CERCLA share of the $20 million study by mid-:-November2003. If you wish to discussthis further, please contact Ms. Alice Yeh, Remedial Project Manager, at (212) 637-4427 or Ms.Kedari Reddy, Assistant Regional Counsel, at (212) 637~3106. Please note that allcommunications from attorneys should be directed to Ms. Reddy.

Sincerely yOUTS,

George Pavlou, DirectorEmergency and Remedial Response Division

Enclosure

cc: Jim GiannottiChemical Compounds Inc

851640003

TIERRA-B-004782

PRPs in Receipt of Notice Letters:

PRP Legal Counsel

J. Roger Hirl Paul W. Herring, Esq.President and Chairman of the Board Andrews & Kurth L.L.P.Occidental Chemical Co. 1717 Main Street, Suite 3700Occidental Tower Dallas, Texas 752015005 LBJ FreewayDallas, Texas 75244 -- - --

Joseph Gabriel Philip Sellinger, Esq.Vice President of Operations Sills Cummis Zuckerman360 North Pastoria Environmental Corp. One Riverfront Plaza1100 Ridgeway Avenue Newark, NJ 07102Rochester, New York 14652-6280 -_. -

Robert Ball, President Lawrence Salibra, Esq.Alcan Aluminum Corporation Alcan Alwninum Corporation100 Erieview Plaza, 29th Floor 6060 Parkland Blvd.Cleveland, Ohio 44114 Mayfield Hts., OH 44124

Mark Epstein, President Eric Aronson. Esq.

1

Alden Leeds Inc. Whitman Breed Abbott & Morgan55 Jacobus Ave. One Gateway CenterKearny. New Jersey 07032 Newark, NJ 07102

Alan Bendelius, President Fredi L. Pearlmutter. Esq.Alliance Chemical. Inc. Cooper. Rose & English, LLPLinden Avenue 480 Morris AvenueRidgefield, New Jersey 07657 Summit, New Jersey 07901-1527

-

William Gentner, President A. Christian Worrell III, Esq.The Andrew Jergens Co. Head & Ritchey, LLP2535 Spring Grove Ave. 1900 Fifth Third CenterCincinnati, Ohio 45214 511 Walnut Street

Cincinnati, OH 45202

Gary Cappeline, President Stephen Leermakers, Esq.Ashland Specialty Chemical Co. Ashland Specialty Chemical Co.5200 Blazer Parkway 5200 Blazer ParkwayDublin, Ohio 43017 Dublin, OH 43017

-_. -_ .. --

Klaus Peter Loebbe, President Nan Bernardo, Esq. and Nancy Lake Martin, Esq.BASF Corporation BASF Corporation3000 Continental Drive North 3000 Continental Drive NorthMount Olive, New Jersey 07828 Mount Olive, NJ 07828

851640004

TIERRA-B-004783

Joseph Akers, Vice PresidentI. •I Gerard HIckel, Esq.

Bayer Corporation Bayer Corporation100 Bayer Road 100 Bayer RoadPittsburgh. Pennsylvania 15205-9741 Pittsburgh, PA 15205-9741

Yvan Dupay, President Arthur Schulz, Esq.Benjamin Moore & Co. Environmental Counsel51 Chestnut Ridge Road 4910 Massachusetts Ave., N.W. Suite 221Montvale, New Jersey 07645 Washington, DC 20016

Alberto Celleri, President Jim GiannottiChemical Compounds Inc. Chemical CompoWlds Inc.10 Baldwin Court 29-75 Riverside AvenueRoseland, New Jersey 07086 Newark, NJ 07104

President Brian Kelly, Esq.Chris-Craft Industries, Inc. Chris-Craft Industries, Inc.767 Fifth Avenue, 46th Floor 767 Fifth Avenue, 46th FloorNew York, New York 10153 New York, NY 10153

John Guffey, President John R. Mayo, Esq.Coltec Industries, Inc. Cohee Industries, Inc.3 Coliseum Centre 430 Park Avenue2550 West Tyvola Road New York, NY 10022Charlotte, North Carolina 28217

Roger Marcus, President Russell Hewit, Esq.Congolewn Corporation Dughi & Hewit3705 Quakerbridge Road 340 North AvenueMercerville, New Jersey 08619 Cranford, NJ 07016

Martin Benante, Chairman James Maher, Esq.Curtiss- Wright Corp. Curtiss-Wright Corp.4 Becker Farm Road 4 Becker Farm RoadRoseland, New Jersey 07068 Roseland, NJ 07068

Antonio Perez, President Elliot Stem. Esq.Eastman Kodak Company Eastman Kodak: Company343 State Street 343 State StreetRochester, New York 14650 Rochester, NY 14650

Edgar Woolard, Chairman Bernard J. Reilly, Esq.E.I. du Pont de Nemours & Co. Corporate Counsel1007 Market Street E.I. du Pont de Nemours & Co.Wilmington, Delaware 19898 1007 Market Street

Wilmington, DE 19898

851640005

TIERRA-B-004784

David Weisman, CEO Jeffrey Schwartz, Esq.Elan Chemical Company Sarber Schlesinger Satz & Goldstein268 Doremus Ave. One Gateway CenterNewark. New Jersey 07105 Newark, NJ 07102

Al Reisch, President NoneEM Sergeant Pulp & Chemical Co. Inc.6 Chelsea RoadCHfton, New Jersey 07102 .-

Mark Tucker. Esq. Kenneth Mack, Esq.Essex Chemical Corp. Fox. Rothschild. O'Brien & Frankel2030WMDC Princeton Pike Corp.CenterMidland, Michigan 48674 997 Lenox Drive. Building 3

LaWrenceville, NJ 08648

Todd Walker, President John Ix, Esq.Fairmount Chemical Co. Inc. Porzio Bromberg & Newman117 Blanchard St. 163 Madison Ave.Newark, New Jersey 07105 Morristown, NJ 07962

Bradley BuecWer. President Robert M. Becker, Esq.Franklin-Burlington Plastics Inc. Kraemer. Burns, Mytelka & Lovell. P .A.113 Passaic Ave. 675 Morris Ave.Kearny. New Jersey 07032 Springfield. NJ 07081

He1U'YBenz, President Anne Conley-Pitchel1, Esq.Hoescht Celanese Chemicals, Inc. Hoescht Celanese Corp.Route 202-206 Route 202-206P.O.Box 2500 P.O.Box 2500Somerville, New Jersey 08876 Somerville, NJ 08876

Francine Rothschild, President NoneKearny Smelting & Refining936 Harrison Ave #5Kearny. New Jersey 07032

He1U'YSchact, CEO Ralph McMurry, Esq.Lucent Technologies, Inc. Hill, Betts & Nash LLP600 Mountain Avenue I Riverfront Plaza, Suite 327Murray Hill, New Jersey 07974 Newark, NJ 07102-5401

Richard Meelia, President Patricia Dut\, Esq.Mallinckrodt. Inc. Mallinckrodt, Inc.675 McDonnell Blvd. 675 McDonnell Blvd.Hazelwood, Missouri 63042 Hazelwood, MO 63042

851640006

TIERRA-B-004785

Richard Mahoney, CEO L. William Higley, Esq.Monsanto Company Monsanto Company800 N. Lindbergh Blvd. 800 N. Lindbergh Blvd.St. Louis, Missouri 63167 St. Louis,MO 63167

Joseph Galli, President Peter Schultz, DirectorNewell Rubberrnaid, Inc. I Envirorunental Affairs29 E. Stephenson St. Newell Co.Freeport, Illinois 61032 4000 Auburn St.

Rockford, IL 61101

Jean-Pierre van Rooy, President Sarah Hurley, Esq.Otis Elevator Company Robinson & Cole LLPNorth American Operations 695 East Main Street10 Farm Springs Road Stamford, CT 06904-2305Farmington, Connecticut 06032

Richard Ablon, President J.L. Effinger, Esq.,

Ogden Corporation Ogden CorporationTwo Pennsylvania Plaza, 25lh Floor Two Pennsylvania Plaza. 25th FloorNew York, New York 10121 New York, NY 10121

Henry McKinnell, Chairman Michael McThomas, Esq.Pfizer Inc. Pfizer Inc.235 E. 42nd St. 235 E. 42Dd St.New York, New York 10017 New York; NY 10017

Raymond LeBoeuf, President Joseph Karas, Esq.PPG Industries, Inc. PPG Industries, Inc.One PPG Place One PPG PlacePittsburgh, Pennsylvania 15272 Pittsburgh, PA 15272

Lawrence Codey, President Hugh Mahoney, Esq.PSE&GCo. PSE&GCo.P.O. Box 570 P.O. Box 570Newark, New Jersey 0710l~0570 Newark, NJ 07101

Phillip D. Ashkettle, President Adam S. Walters, Esq.Reichhold Chemicals, Inc. Phillips, Lytle, Hitchcock; Blaine & HuberP.O. Box 13582 3400 Marine Midland CenterResearch Triangle Park, North Carolina Buffalo, NY 1420327709

Robert McNeeley, President Paul Rivers, DirectorReilly Industries, Inc. Corporate Environmental Affairs1510 Market Square Center Reilly Industries, Inc.151 North Delaware Street 1500 S. Tibbs AvenueIndianapolis, Indiana 46204 Indianapolis, IN 46242

851640007

TIERRA-B-004786

Robert Finn, President . Howard Myers, Esq.RSR Corporation RSR Corporation2777 Stemmons Freeway, Suite 1800 2777 Stemmons Freeway, Suite 1800Dallas, Texas 75207 Dallas, TX 75207

Christopher Connor, CEO Donald McConnell, Esq.The Sherwin-Williams Company The Sherwin-Williams Co.101 Prospect Avenue, N.W. 101 Prospect Ave., N.W.Cleveland, Ohio 44115~1075 Cleveland, OH 44115

George Barrett, President Kirsten E. Bauer, Esq.Teva Pharmaceuticals USA Inc. Teva North America1090 Horsham Road 1090 Horsham RoadNorth Wales. Pennsylvania 19454 North Wales, PA 19454

Robert Senior, President Robert DiLascio, Esq.Three County Volkswagen 30 Park Avenue, Suite 101 I

701 Riverside Ave. Lyndhurst, NJ 07071Lyndhurst, New Jersey 07071

Michael Jordan, President Roger Willis, Esq.Westinghouse Electric Corp. Westinghouse Electric Corp.11 Stanwix Street 11 Stanwix StreetPittsburgh, Pennsylvania 15222 Pittsburgh, PA 15222

Isaac Weinberger, President r~Wiggins plastics Inc.547 Maitland Ave.Teaneck, New Jersey 07666

851640008

TIERRA-B-004787