vacuum science and technology in accelerators · for vacuum use, the most common getter pump is the...

38
Lecture 3 Vacuum Science and Technology in Accelerators Cockcroft Institute Lectures - 2010 R J Reid Vacuum Science and Technology in Accelerators Ron Reid Consultant ASTeC Vacuum Science Group ([email protected])

Upload: others

Post on 05-Nov-2019

8 views

Category:

Documents


0 download

TRANSCRIPT

Page 1: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 3Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010R J Reid

Vacuum Science and Technology in

Accelerators

Ron Reid

Consultant

ASTeC Vacuum Science Group

([email protected])

Page 2: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 3Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010R J Reid

Session 4

The Production of Vacuum

Page 3: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

3 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Aims

• To demonstrate the main types of vacuum

pump used in accelerators

• To understand the pumping mechanisms

involved

• To understand the advantages and

limitations of each type of pump

Page 4: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

4 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Pumping for accelerators

Mechanical Pumps

• Turbomolecular Pumps

Ion Pumps

Getter Pumps

• Evaporable

• Non evaporable

Cryopumps

Page 5: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

5 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Mechanical pumps

Mechanical pumps (displacement pumps) remove gas

atoms from the vacuum system and expel them to

atmosphere, either directly or indirectly

In effect, they are compressors and one can define a

compression ratio, K, given by

K is a fixed value for any given pump for a particular gas

species when measured under conditions of zero gas

flow.

out

in

PK

P

Page 6: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

6 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Mechanical pumps

Here, we will only look at the turbomolecular pump.

Turbo pumps cannot pump from atmosphere and cannot eject to atmosphere, so they require roughing (forevacuum) pumps to reduce the pressure in the vacuum system before they can be started and backing pumps to handle the exhaust.

There are many types of roughing and backing pumps. Most accelerators now use clean (dry) pumps to avoid oil contamination in the system.

Page 7: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

7 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Turbomolecular pump principle

Page 8: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

8 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Turbomolecular pump principle

Page 9: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

9 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Turbomolecular pump principle

To maximise the compression ratio, blade tip velocities

need to be comparable to molecular thermal velocities.

For a single blade, at zero flow

where α12 is the forward transmission probability

and α21 is the reverse transmission probability

It can be shown that

where Vb is the blade velocity

12

21

out

in

PK

P

0

exp2

bV MK

TkN

Page 10: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

10 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Turbomolecular pumps

Page 11: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

11 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Turbomolecular pumps

Turbo pumps come

in a wide range of

speeds – from a few

l sec-1 to many

thousands of l sec-1

and operate from

10-3 mbar to lower

than 10-9 mbar

Page 12: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

12 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Turbomolecular pumps

Operation can be extended to higher pressure by adding

a drag stage

Page 13: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

13 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Turbomolecular Pumps

Page 14: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

14 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

The choice of bearing type is important

• Oil sealed

• Greased

• Greased ceramic ball

• Magnetic

Turbomolecular Pumps

Page 15: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

15 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Ion Pumps

Based on Penning Cell

Page 16: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

16 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Ion Pumps

Based on Penning Cell

Page 17: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

17 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Ion Pumps

Pumping in the basic diode Penning cell

Page 18: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

18 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Ion Pumps

The Diode pump has poor pumping speed for

noble gases

Remedies

• Differential Ion; Noble Diode

• “Heavy” cathode

• Triode

• Special Anode shape e.g. Starcell

Page 19: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

19 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Ion PumpsUsing a heavier cathode e.g. Tantalum increases

reflected neutrals

Page 20: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

20 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Ion Pumps

Triode Pumps use a different design

Page 21: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

21 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Ion Pumps

Starcell configuration

Page 22: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

22 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Ion Pumps

Page 23: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

23 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Ion PumpsCurrent (per cell) – and hence pumping speed –

depends on voltage, magnetic field, pressure and

history.

nI kP 1.05 < n < 1.2

Pump life depends on quantity of gas pumped

> 20 years at 10-9 mbar

Prone to generate particulates

Leakage current unpredictable, so pressure

indication below 10-8 mbar unreliable

Page 24: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

24 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Ion Pumps

Page 25: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

25 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Ion Pumps

Diode Differential

Diode

Starcell Triode

Voltage +7kV +7kV +2-5kV -5kV

Pumping Speed

(Active gases)

Highest Good Good Lowest

Pumping Speed

(Noble gases)

Lowest Good Higher Highest

Starting Pressure Lowest Lowest Good Highest

UHV Low Low Good Highest

Cost Lowest Higher Low Highest

Page 26: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

26 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Ion Pumps

Page 27: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

27 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Getter Pumps

When a gas molecule impinges on a clean metal film, the sticking probability can be quite high.

For an active gas with the film at room temperature, values can be between 0.1 and 0.8. These fall with coverage.

For noble gases and hydrocarbons sticking coefficients are very low (essentially zero)

Evaporated films, most commonly of titanium or barium, are efficient getters and act as vacuum pumps for active gases.

Page 28: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

28 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Getter Pumps

For vacuum use, the most common getter pump

is the titanium sublimation pump

Page 29: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

29 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Getter Pumps

An important class of getter pumps are the Non

Evaporable Getters (NEGs)

These are alloys of elements like Ti, Zr, V, Fe,

Al which after heating in vacuo present an

active surface where active gases may be

gettered

Traditionally, the getters take the form of a

sintered powder either pressed into the surface

of a metal ribbon or formed into a pellet

Page 30: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

30 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Getter Pumps

Page 31: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

31 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Getter Pumps

Page 32: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

32 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Getter pumps

In recent times, thin films of getter material have

been formed on the inside of vacuum vessels

by magnetron sputtering

These have the advantage of

• pumping gas from the vacuum chamber by

gettering

• and of stopping gases from diffusing out of

the walls of the vessels

Page 33: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

33 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Getter Pumps

Page 34: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

34 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Getter Pumps

Page 35: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

35 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Cryogenic Pumps

Page 36: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

36 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Cryogenic Pumps

There are two major classes of such pumps

• Liquid Pool

• Liquid helium temperature (~4K)

• Closed cycle

• Refrigerator (~12K)

• Supplemented by cryosorption

Page 37: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

37 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Cryogenic Pumps

Page 38: Vacuum Science and Technology in Accelerators · For vacuum use, the most common getter pump is the titanium sublimation pump . Lecture 4 29 of 38 The Production of Vacuum R J Reid

Lecture 4

38 of 38

The Production of Vacuum

R J Reid Vacuum Science and Technology in Accelerators

Cockcroft Institute Lectures - 2010

Cryogenic Pumps