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    Turbidity SensorTS100

    Edition 3.0

    User

    Manual

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    Greenspan Customer Service+61 7 4660 1888

    Technical Support When You Need ItThe correct choice of sensor should be supported by professional advice to ensure long termsuccess in the field. Greenspan Technical Services is dedicated to customer support andprovides assistance in the selection, installation, deployment and commissioning of sensors with afull range of consulting services.

    A full technical support and field advice service can be accessed by ringing Customer Service on+61 7 4660 1888 between 8am - 6pm, 5 days a week.

    All requests for information will be serviced within 24 hours.

    All Greenspan products are designed, developed and manufactured in Australia and can besupplied at short notice.

    Warranty Details

    Greenspan warrants all new Greenspan products against defects in materials and workmanshipfor 12 months from the date of invoice. During the warranty period, we will repair or, at ouroption, replace at no charge a product that proves to be defective provided that it is returned,shipping prepaid, to Greenspan Technology Pty Ltd.

    Greenspans liability and obligations in connection with any defects in materials andworkmanship are expressly limited to repair or replacement, and the sole and exclusive remedy inthe event of such defects shall be repair or replacement. Greenspans obligations under thiswarranty are conditional upon it receiving prompt written notice of claimed defects within thewarranty period and its obligations are expressly limited to repair or replacement.

    This warranty does not apply to products or parts thereof which have been altered or repairedoutside of the Greenspan factory or other authorised service centre, or products damaged by

    improper installation or application, or subjected to misuse, abuse neglect or accident. Thiswarranty also excludes items such as reference electrodes and Dissolved Oxygen membranes thatmay degrade during normal use.

    Greenspan Technology Pty Ltd will not be liable for any incidental or consequential damage orexpense incurred by the user due to partial or incomplete inoperability of its products for anyreason whatsoever or due to inaccurate information generated by its products.

    All Warranty service will be completed as soon possible. If delays are unavoidable customers willbe contacted immediately.

    The sensors should not be dismantled unless under instruction from Greenspan. Incorrecthandling will void the warranty.

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    Contents

    1. INTRODUCTION

    Overview 1Theory of Turbidity 1

    Turbidity and Suspended Solids 2

    Stream Water Turbidity 2

    2. TURBIDITY MEASUREMENT

    Formazin Definition 3

    Calibration Considerations 3

    3. THE HARDWARE

    Overview 4

    Sensor Design 5

    4. INSTALLATION

    Connection 6

    General Methods of Installation 7

    Typical Locations 7

    Option 1: Non Turbulent Conditions 8

    Option 2: High Turbulent Conditions 8

    Other Considerations 8

    Turbidity Deployment 9

    5. CLEANING AND MAINTENANCE 11

    6. QUICK CALIBRATION CHECK METHODChecking Calibration Using Calibration CupsTR100 12

    Calibration of Turbidity Cups 13

    7. FORMAZIN CALIBRATION METHOD

    Test Setup 15

    Formazin Standards from Ref Stock Suspension 16

    Preparation of Formazin Standard 16Materials 17

    Procedure 17Checking Standard Against a Hach Turbidimeter (Optional) 17Calibration Method 18

    Preliminary Setup 18

    Zero Checking 18

    Full Scale Checking 18

    8. REFERENCES 20

    9. SPECIFICATION and CERTIFICATE of CONFORMANCE 21

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    10. APPENDIX

    Errors in Measurement 23

    Bench Testing 23

    Noise 23Offsets 23

    Bubbles 23

    Algae 23

    Colour 23

    Turbidity Sensor Cleaning Pump TP100 24Function 24

    Installation 24

    TP100 Specification 26

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    INTRODUCTION 1

    Overview

    The Greenspan TS100 Turbidity Sensor utilises a high gain infrared optical

    system to detect the back-scatter intensity of suspended particles

    by transmitting a beam of 880nm wavelength and measuring the received

    intensity of reflected light.

    Advanced digital filtering techniques are used to eliminate ambient light and

    stray signals from the measurement of data.

    A current loop output of 4 - 20mA is provided on the TS100 Series Sensor.

    The external optical surface is coated with a special polymer which resistsfouling from algae growth. It does not eliminate the problem but increases the

    time between cleaning.

    The sensor is packaged in a 316-grade stainless steel or Acetal co-polymer tube,

    with

    O ring sealed Acetal co-polymer end fittings. The design is rugged and well

    proven and can withstand the harsh conditions found in any field environment

    Theory of Turbidity

    Turbidity is the term used to describe the reduction in water clarity or

    "cloudiness" as perceived by the human eye caused by the scattering of light due

    to particulate matter suspended in solution. The greater the turbidity, the more

    cloudy the water. Increases in turbidity reduce the transmission of light.

    Because most aquatic plant growth and marine organisms depend upon natural

    light radiation for survival, and light penetration in water is dependent on the

    clarity of the water, the measure of turbidity is useful for assessment of water

    quality.

    Due to the effects of erosion within catchment areas, tiny particles of clays, silts

    or small organic particles are washed into water bodies. Industrial wastes and

    sewerage can also contribute particles.

    Oceanographers, Engineers and Geomorphologists who are studying the

    movement of suspended sediments find turbidity a useful factor in defining

    relative changes in sedimentation between sites.

    The rate at which the water is moving limits the amount of suspended solids it

    can carry.

    The inherent simplicity of turbidity measurement allows for the continuous in-

    situ gathering of data. This is very useful when monitoring rapidly varying

    turbidity conditions, and it is the main advantage compared with the laboratory

    sample method.

    UM-010-0006-TS GREENSPAN TECHNOLOGY 1

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    Turbidity and Suspended Solids

    Suspended particles in the water are the principle source of turbidity.

    Assuming that the turbidimeter has been calibrated to give a linear response to

    standards (such as Formazin) varying only in concentration, the relationship

    between suspended solids concentration and turbidity depends mostly onparticle size, composition and particle concentration. Even in streams that

    transport sand during storm event runoff, strong relationships between

    suspended solids and turbidity have been observed. In such cases, the

    turbidimeter is responding less to the coarse fraction, but because the

    concentration of the fine fraction (the main source of turbidity) increases

    proportionately with the concentration of the coarse fraction, the turbidity is an

    adequate index of the total suspended load. The relationship between turbidity

    and total suspended solids in this case is non-linear. A linear relationship

    should only be expected in cases where the particle size, shape and composition

    do not vary through time. (Ref: Gippel, AJSWC, 1994)

    Stream Water TurbidityIf turbidity is established as an index of suspended solids, then considerable

    savings will result from reduced labour costs for field sample collection and

    laboratory analysis. Stream water turbidity is likely to reflect catchment

    condition, so a catchment-wide network of continuously recording instruments

    could be used in a surveillance role to identify areas of landslips, stream bank

    disturbance, or inappropriate land use practices. (Ref: Gippel, AJSWC, 1994)

    UM-010-0006-TS GREENSPAN TECHNOLOGY 2

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    TURBIDITY MEASUREMENT 2

    Greenspan turbidity sensors are of the back scattering type and respond to theaverage volume scattering of particulate matter over a defined angular range.

    Both particle size and concentration affect readings.

    Output is calibrated in terms of NTU (Nephelometric Turbidity Units).

    The instrument does not measure in absolute terms but relative to a Formazin

    standard, (see below). A comparison is made of the intensity of scattered light by

    a sample and the intensity of scattered light by a standard reference.

    Formazin Definition

    Formazin is a white insoluble polymer formed by the condensation reaction

    between hydrazine sulphate and hexamethylenetetramine, (Ref: Gippel,

    AJSWC, Nov 1994). It forms a mono disperse dispersion of approximately 2.5

    m geometric mean volume particles (Gippel, 1988a ).

    Formazin reference solution is supplied as 4000 NTU primary standard and is

    diluted with high quality distilled water to lesser concentrations for calibration.

    Secondary standards of Formazin are available from various manufacturer's,

    often as a gel suspension or sealed latex suspension, and are stable for up to 1

    year when properly stored.

    Secondary standards provided with reference test equipment are usually used tostandardise the instrument before each reading. (Ref: Standard Methods, 1995)

    Calibration ConsiderationsVarious Turbidity units have been used to reference turbidity measurement.

    (JTU, NTU, FTU, EBC, CNU, FAU, FNU) they are not all equivalent and they

    should not be confused with mass concentration.

    ISO 7027 recommends the adoption of FNU (Formazin Nephelometric Units)

    and FAU (Formazin Attenuation Units), (Ref: Gippel, AJSWC, Nov 1994)

    The most recognised and widely adopted reference standard is Formazin,

    one FNU is equivalent to one NTU, (Nephelometric Turbidity Units) so NTU

    has been adopted by Greenspan for turbidity calibration.

    Derived standards are only stable for a few days and therefore have to be

    prepared each time the instrument is checked.

    Proper laboratory handling is essential as Formazin is a suspected

    carcinogen. A simplified method not requiring Formazin is provided

    in this manual using Greenspan Turbidity Reference Cups TR100.

    UM-010-0006-TS GREENSPAN TECHNOLOGY 3

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    THE HARDWARE 3Overview

    The TS100 turbidity sensors utilise an infra-red optical system to measure

    scattered reflected radiation across an angle of 30. Infra-red transmission is

    used because light of this frequency is heavily attenuated in water, therefore the

    beam penetration is reduced to practical limits and infra-red interference from

    sunlight is also reduced with depth.

    The sensor is constructed of environmentally inert materials, 316 stainless steel

    and Delrin plastic. The form is cylindrical with the following dimensions:

    Transmission LEDs

    B. Reception Photodiode30

    C. Infra-red Lens

    Optical Head

    A.A

    B

    C

    C

    Side ViewFront View

    275

    *44.4

    25

    TS100 Turbidity Sensor

    All dimensions in mm

    *47mm max for Delrin

    Alignment Mark

    A

    Alignment Mark

    Figure 1. Overview

    The standard package includes:

    1 316 stainless steel body- Delrin optional

    2 Delrin sensor head

    3 Delrin cable gland.

    4 Optical filter lens

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    Sensor Design

    A digital synchronous detector system is used to eliminate common mode carrier

    signals and effectively provide a narrow band limited signal path. This method

    ensures minimal interference from stray light frequencies (ambient light) and

    maximum reception of signal strength.

    The optical system is embedded in epoxy compound for stability and

    waterproofing and ensures an ambient light proof, mechanically robust

    mounting.

    Quality electronic components are used throughout for reliable long term

    operation and boards can be easily accessed and serviced.

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    INSTALLATION 4ConnectionThe TS100 is designed as a three wire 4-20mA current system and is nominally

    powered by 12V DC. The sensor is normally supplied with open ended bare

    wires for connection to power and external data logger.

    The following diagram illustrates the wiring arrangement for the TS100.

    50 ohm

    o

    o

    9 27VDC,

    typically +12V

    Ground

    Blue

    Red

    Green

    Load or m A meter

    Output

    Power

    TS

    Figure 2. Connection

    The input voltage range is 9-27V and it should be noted that as the quiescent

    current is 80mA and at full scale the output current is 20mA the total is

    1000mA. The resistance of the cable is 9 ohms per 100 metres, therefore a 25m

    length of cable will give a voltage drop of :

    100mA x 9 x 25 = 0.225V for the active red wire

    100

    This is duplicated for the return green wire:

    0.225 + 0.225 = 0.450V

    Therefore, approximately 0.45 volts less is developed across the sensor. That is, a

    12V supply with 25m of cable will effectively provide 11.55V at the sensor.

    The sensors are protected against reverse voltage occurrences and against

    voltages of 2KV such as may occur during lightning storms. However, if using in

    areas prone to lightning activity it is recommended that lightning arresters be

    fitted to all input cables.

    UM-010-0006-TS GREENSPAN TECHNOLOGY 6

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    General Methods of InstallationThe Greenspan Range of Water Quality Sensors can be installed into a variety

    of applications including:

    Rivers, Lakes and streams Bore Hole and groundwater wells

    Tanks and Reservoirs

    Wet Wells for Water and Sewer Systems

    In all field applications, mechanical, electrical and physical protection of the

    Sensor, cabling and associated fittings must be provided.

    Consideration needs to be given for the protection against vandalism, animal

    damage, theft and extreme weather conditions.

    There are a many ways of positioning sensors in the field in order to ensure the

    continuous collection of data and the safety of the device.

    Some methods commonly in use are:

    1. Floating Buoy for use at sea, can be installed with telemetry/cell phone

    communications.

    2. Suspended Sensor attached to a guide wire and winch board, which is

    useful for profiling applications.

    3. Fly wire across stream/river, sensor tethered to fly wire and fully

    immersed.

    4. Installed in PVC conduit with sensor emerging from the immersed end.

    5. Sealed waterproof, self contained vessel including batteries and

    continuous logging equipment. Excellent for concealment.

    6. Strapped to pylon or post in areas that become submersed, cabled to

    bank. Ensuring 100mm clearance from post.

    7. Hand operation for spot readings.

    Typical Locations

    1. Edge of river/stream/lake embankment.

    2. Side of boat/vessel.

    3. Mounted within a stilling well off stream from main flow.

    4. Mounted within drainage channels/pipes.

    5. Suspended from dam walls.

    6. Sensor anchored to bed of lake/stream.

    UM-010-0006-TS GREENSPAN TECHNOLOGY 7

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    Field Installation must ensure:

    The sensor is anchored or held in position or located so it is not subject to

    any movement during normal operations.

    Sensor is protected from direct sunlight to avoid high temperature

    fluctuations Sensor is protected against high turbulence and possible debris loading

    during flow events

    Option 1: Non Turbulent Conditions

    Where there is no possibility of the sensor being affected by turbulence it can be

    suspended into the water body using a stainless steel hanger cable. For

    example where the sensor is installed into a large water storage tank. The

    sensor will hang vertically into the tank and not be subject to movement from

    water movements. The stainless steel wire prevents loading of the sensor cable.In Sewer Wet Well and Water Tank applications where high turbulence and

    debris loading may affect the sensor, the following minimum installation

    standards must be followed:

    Option 2: High Turbulent Conditions

    Where turbulence and water movement will act on the sensor it is recommended

    to mount the sensor in a stilling well or mounting cradle attached to the side of

    the well. This could simply be a length of PVC pipe bolted to the well wall in

    which the sensor is located or could be an extension pole with a sensor cradle at

    the lower end. Potential ragging and debris build up on the sensor & cableshould be overcome by extending the stilling well to above the high water level

    or by cable tying the sensor cable up the cradle mounting arm. The movement

    of the sensor must be eliminated such that the sensor is not subject to twisting

    motion from swirling water during pumping, or from sideways movement due to

    ragging of the sensor.

    In all sewer wet well applications regardless of the mounting system used it is

    recommended to also utilise a stainless steel hanger cable* to prevent loading

    the sensor cable during installation, removal and maintenance. The stainless

    steel wire must be securely connected to the sensor using the hanger hook and

    the sensor cable should be cable tied at regular intervals up the stainless wire.

    An outer sheath of hose or tubing can be fitted over both cables to reduce

    ragging and debris build up on the cables. At the top of the well the stainlesswire can be attached to a bolt or mounting point.

    *Note, the stainless steel suspension, hanger cable can be provided by

    Greenspan. (Part No 7SK-100)

    Warning:Under no circumstances must the sensor be installed such that it can

    collide with the sides of the well, or other solid objects within the well.

    Sensor installation under these circumstances will lead to sensor

    damage that will not be covered under our normal warranty

    conditions. In these cases the sensor must be mounted into a cradle or

    stilling well as per Option 2.

    UM-010-0006-TS GREENSPAN TECHNOLOGY 8

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    Other Considerations

    Environmental compatibility should be checked before using the sensors and

    advice sought from Greenspan if any doubt exists. The 316 stainless body can be

    used in a majority of situations but care should be taken against possible

    corrosion in high Chloride, Sulphate or Ferric solutions.The body should always be totally immersed under the water to ensure that the

    sensor is at water temperature and to also avoid any possible anodic/cathodic

    action taking place on the stainless body at the water-air interface. At some

    sites it has also been noticed that clamps used to support the sensor made of a

    dissimilar metal to the 316 stainless body can cause spot corrosion due to

    electrolysis.

    Turbidity DeploymentWhen mounting turbidity sensors in water ensure a minimum clearance around

    the optical head of 50 mm and approximately 250 mm forward to reducereflection from non-data surfaces. Note that reflection errors increase the closer

    the transmit LED is to a reflective surface. Therefore in tight installations it is

    preferable to rotate the sensor so that the Alignment Mark is furthest from the

    reflective surface. The Alignment Mark on the head is positioned adjacent to the

    transmit LEDs, see Diagram 1, page 4.

    When installing in very shallow water immerse to at least 250-300 mm

    minimum to prevent infra-red radiation from natural sunlight affecting

    readings. It is preferable to point the sensor face down or at an angle.

    Alternatively, process the resultant data file so that only data recorded in non

    daylight periods is accepted.

    When installing directly into a flowing medium, angle the sensor head such that

    it is inclined at an angle of at least 45 to the horizontal and such that the

    sensor lens is facing downstream. This will minimise the damage to the lens as

    a result of impact from travelling particulate matter.

    If using the model TP100 lens cleaning pump it is important to ensure pump is

    primed prior to positioning sensor at depth. This can be achieved at just below

    surface level by manually triggering the pulse line or driving it from a logger,

    and checking for correct pump operation and then lowering sensor to the desired

    depth.

    To manually check the pump operation, press the test button located inside theTimer Controller unit or briefly connect the trigger wire from the pump to

    ground, (negative pulse) or to +ve supply (positive pulse).

    When the cleaning pump is activated the force of the water creates artificial

    turbulence and if left untethered, can cause slight displacement of sensor

    position. It is preferable that the logged readings do not coincide with the pump

    activation cycle, which may lead to errors. To minimise this, do not start the

    recording logger at the same time as the pump timer and tether the sensor.

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    Most sediment transport occurs during storm events and flood conditions.

    Protection from floating debris damage is an important consideration along with

    adequate tethering of sensors.

    UM-010-0006-TS GREENSPAN TECHNOLOGY 10

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    CLEANING AND MAINTENANCE 5

    Protection of the lens surface is vital to maintain the accuracy of the calibration.

    The prevention of algal growth and marine encrustations on the lens (and body

    in general) is desirable. Both the polymer and Turbidity Cleaning Pump assist

    in this process. Please refer to Appendix for further information on the Lens

    Cleaning Pump.

    The lens may be cleaned using warm soapy water, a soft cloth and a gentle

    rubbing action.

    WARNING

    DO NOT USE METHYLATED SPIRITS or ALCOHOL on LENSSURFACE

    If scratches are evident on the lens which cannot be removed through polishing

    please contact Greenspan. It may be possible to recalibrate the offset to

    eliminate the effects of the damage. Alternatively, the lens/head can be replaced

    and the unit re-calibrated.

    Note that regular cleaning of the lens will, in time, remove the polymer coating

    applied during manufacture. Please contact Greenspan if you wish new coatings

    to be applied.

    UM-010-0006-TS GREENSPAN TECHNOLOGY 11

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    QUICK CALIBRATION METHOD 6

    There are two methods in this manual for checking the calibration. The firstuses TR100 calibration cups and the second uses Formazin reference solution.

    CHECKING CALIBRATION USING CALIBRATION CUPS TR100

    To enable quick and easy checking of sensor calibration Greenspan can supply

    calibration cups (TR100) matched to the particular sensor. There are two cups,

    one for zero and one for full scale. These are simply slid over the sensor head

    and the reading obtained should match the recorded reading taken when the

    sensor was newly calibrated. Any difference will indicate that calibration has

    changed.

    NOTE: An individual cup will not measure the same turbidity value on

    different sensors. The cup must be calibrated and matched to an

    individual sensor prior to use. See Calibration of Turbidity Cups.

    Method

    1. Gently remove any debris which may have accumulated on the sensorhead with a moist soft cloth, avoid scratching the turbidity lens. Dry the

    lens.

    2. Remove the protective cap on the high and low turbidity calibration cupsand pour 2.5ml or 1/2 teaspoon of silicone oil into each and allow them to

    form a level, bubble free layer over the calibration suspension in the base

    of the cups.

    3. Slide the low value turbidity calibration cup over the sensor head until itreaches the bottom, (some silicone oil may overflow). Rotate the cup,

    while keeping firm contact on the bottom, to line up the alignment mark

    on the cup with the mark on the sensor head.

    4. Once the cup and sensor are in place and aligned, remove your handsfrom the sensor and allow the assembly to stand in a vertical position

    (with the cup on the bottom) while taking the reading.

    NOTE: Air bubbles trapped between the sensor lens and the

    calibration suspension will cause high and erratic readings. Be

    sure to use an adequate amount of silicone oil to prevent this

    from occurring and ensure no air bubbles are present prior to

    installing the cup. It is also important not to break contact with

    the interface prior to reading the calibration point.

    5. Connect the sensor output to a milliammeter. Check that the reading is

    equivalent to the recorded value assigned to that sensor for that

    calibrator cup.

    6. Repeat steps 3-5 for the high calibration cup.

    7. If the output reading is not within 3% of expected reading (value markedon Reference Table for that sensor) the sensor is out of calibration.

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    8. Remove the cup and wipe the sensor head clean of oil with a soft cloth.

    9. If re-calibration is necessary, contact a Greenspan authorised agent for

    re-calibration.

    CALIBRATION OF TURBIDITY CUPS

    Function

    Each cup and sensor must be matched prior to use in checking. If this was not

    done at the factory, then the matching can be performed by the customer on the

    bench using the following procedure. Note that this assumes that the sensor has

    been accurately calibrated recently. Once matched the pair should remain

    stable indefinitely.

    Method

    1. Gently remove any debris which may have accumulated on the sensor

    head with a moist soft cloth, avoid scratching the turbidity lens. Dry the

    lens.

    2. Ensure that the sensor has been accurately calibrated, if not, return the

    unit to a Greenspan authorised agent for re-calibration.

    3. Engrave a permanent alignment mark laterally, anywhere along the

    sensor head. Be careful not to scratch the sensor lens.

    Alignment Mark

    4. Clean and dry the sensor head with a soft cloth.

    5. Remove the protective cap on the high and low turbidity calibration cups

    and pour 2.5mL or teaspoon of silicone oil into each and allow them to

    form a level, bubble free layer over the calibration suspension in the base

    of the cups.

    6. Slide the low value turbidity calibration cup over the sensor head until it

    reaches the bottom, (some silicone oil may overflow). Rotate the cup while

    keeping firm contact on the bottom, to line up the alignment mark on the

    cup with the mark on the sensor head.7. Once the cup and sensor are in place and aligned, remove your hands from

    the sensor and allow the assembly to stand in a vertical position (with the

    cup on the bottom) while taking the reading.

    NOTE: Air bubbles trapped between the sensor lens and the

    calibration suspension will cause high and erratic readings. Be

    sure to use an adequate amount of silicone oil to prevent this

    from occurring and ensure no air bubbles are present prior to

    installing the cup. is also important not to break contact with the

    interface prior to reading the calibration point.

    8. With the sensor output connected to a milliammeter. Record the reading ofthe sensor onto the Turbidity Reference Table in the calibrator kit, using a

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    waterproof pen. Also, record the serial numbers of the turbidity sensor and

    turbidity cup. These may be changed or removed later with methylated

    spirits if the calibration is redone.

    9. Repeat steps 6-8 for the full scale calibrator cup.

    10. Remove the cup and wipe the sensor head clean of oil with a soft cloth.

    Note that the same cup may be used on different sensors of the same range with

    correspondingly different readings being obtained. Each reading is valid for that

    particular sensor and all are recorded on the Turbidity Reference Table provided

    in the TR100 kit.

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    FORMAZIN CALIBRATION METHOD 7

    Test Setup

    A test setup such as the one described below is recommended for both zero and

    full scale calibration checking. It is recommended the solution is kept moving

    with a magnetic stirrer mounted underneath the full scale vessel to minimise

    contact with solution.

    The full scale calibration suspension using Formazin is prepared according to

    Table 1. Allow a few minutes settling time for the Formazin to be evenly

    distributed through the test vessel. See figure 3.

    Magnetic stirrer mounted

    underneath F/S vessel.

    Clear Filtered WaterCalibration Suspension

    5L Test Vessel F/S Set 20L Test Vessel Zero Set

    oo- +

    mA

    Sensor Power Supply

    Sensor

    +12V, RED

    Output, BLUE

    Ground, GREEN

    Can use magnetic stirrer for

    minmum solution contact

    Figure 3. Calibration Checking Setup TS100 Turbidity sensors

    It must be considered that the validity of diluted Formazin Solution is time

    dependant. For example, both "Standard Methods for Examination of Water and

    Waste Water" and the US E.P.A recommend that 400 NTU suspension not be

    used for longer than 30 days, and a 40 NTU value suspension no longer than 7

    days if affected by light and temperature.

    A sealable container of 5 litre capacity may be used for storage of Formazin and

    calibration. The sensor should be held in the centre by means of a clamping

    arrangement to eliminate side wall reflections. Ensure that the container used

    for Formazin Calibration is a minimum size of 5 litres and has a diameter at

    least 8 inches.

    The zero solution should preferably be in a 20 litre container painted matt blackinside and well filtered water must be used.

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    Materials

    Hydrazine Sulphate (reagent grade) 5.000g

    Hexamethylenetetramine (reagent grade) 50.00g

    Procedure1. Set oven to 25C.

    2. Transfer hydrazine sulphate to a 5000ml volumetric flask and add de-

    ionised water to almost the mark. Stir to dissolve, then fill to the mark

    with de-ionised water.

    3. Transfer hexamethylenetetramine to a 5000ml volumetric flask and add

    de-ionised water to almost the mark. Stir to dissolve, then fill to the mark

    with deionised water.

    4. Place both flasks in the 25C oven and allow to reach temperature.

    5. Transfer all the contents of the hydrazine sulphate flask to a 10 litre

    container equipped for magnetic stirring.

    6. Slowly transfer all the contents of the hexamethylenetetramine flask to the

    10 litre flask while stirring continuously.

    7. Stop stirring when both solutions are mixed. Seal the 10 litre container

    and allow to stand at 25C for 24 hours.

    Checking Standard Against a Hach Turbidimeter (Optional)Mix the Formazin standard to be checked by making sure the lid is on tight and

    then tumbling the canister several times (10 sec). Fill a clean Hach turbidity cell

    with the standard, wipe the walls with silicone oil, and place it in a Hach 43900

    Ratio/XR Turbidimeter. Record the readings when it is stable, (15 sec). Write

    the value and date on the canister label. If the value has changed by more than

    10% from its value at preparation, then prepare a new standard. Use the

    standard within three days of checking.

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    CALIBRATION METHOD

    Preliminary Setup

    Connect the sensor to +12V (red wire) and ground (green wire) and connect

    current meter, (+), between blue and power supply common (-) green. See fig. 3.

    Zero Checking

    1. With power applied to the unit, place the sensor in the zero NTU bath at a

    sufficient depth to cover the optical head and let the temperature

    equilibrate for approximately 1/2 hour.

    NOTE: Air bubbles trapped between the sensor lens and solution

    will cause high and erratic readings. To reduce this, immerse the

    sensor at an angle and if necessary gently rotate the sensor until

    all bubbles surface.

    2. If output reading is not within 3% of 4.00mA, contact a Greenspan

    authorised agent for re-calibration.

    3. After checking the zero value, rinse the sensor in clean water, wiping with

    a tissue to remove excess water.

    4. If zero reading is correct go to next section.

    Full Scale Checking

    1. Apply power to the magnetic stirrer and allow at least 15 min to give

    circulation of the suspension.

    Great care is necessary handling Formazin as it is a suspected

    carcinogen.

    2. Place the sensor into the test vessel prepared with a full scale NTU

    Formazin solution. If there is any doubt about the accuracy of the solution

    it is recommended it is checked on a Hach Turbidimeter. Ensure sensor is

    in bath at a sufficient depth to cover the optical head. Ensure there areno trapped air bubbles by tilting the sensor slightly whenimmersing.

    3. The expected reading can be calculated as follows:

    Output (mA) = ( ( b x 16 ) + 4 )mA

    a

    where:

    a = Full scale range of instrument (NTU)

    b = Full Scale reading of Formazin Standard as measured by

    laboratory instrument such as Hach Turbidimeter

    for example:

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    If sensor is a 500 NTU range and the Standard is 490 NTU

    output (mA) = ( ( 490 x 16 ) + 4 ) mA = 19.68mA

    500

    4. If the output reading is not within 3% of the calculated value then re-

    calibration is required. Contact a Greenspan authorised agent for re-

    calibration.

    5. After checking the full-scale value, rinse the sensor in clean water, wiping

    with a tissue to remove any suspension material.

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    REFERENCES 8

    GIPPEL, C.J., 1989. The Use of Turbidity Instruments to Measure StreamWater Suspended Sediment Concentration. pp 12, Ch 2.

    GIPPEL, C.J., 1988. Comparison of fine particle size determination by Coulter

    Counter Model TA11 and Horiba CAPA-300. pp 11, Ch2.

    GIPPEL, C.J., 1994. Monitoring Turbidity Of Stream Water, Australian Journal

    of Soil and Water Conservation Vol. 7, No 4, pp 41.

    Waterwatch Queensland Technical Manual., State of Qld, Department of

    Primary Industries 1994. pp. 16.

    STANDARD Methods for the Examination of Water and Wastewater, 19th

    Edition 1995, 2130 Turbidity, 2-8 to 2-11

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    SPECIFICATION and CERTIFICATE of CONFORMANCE 9

    Specification Model TS100

    Standard Ranges available 0-100NTU

    0-250NTU

    0-500NTU

    0-1000NTU

    Other ranges available on request.

    -------------------------------------------------------------------------------------------------------------

    Linearity 0-50NTU 3.0%

    0-100NTU 3.5% or 3.0%*

    0-250NTU 4.0% or 3.0%*

    0-500NTU 9.0% or 3.0%*0-1000NTU 11.0% or 3.0%*

    0-2000NTU 12.0% or 3.0%*

    *NOTE: A linearity performance oftypically 3% for all ranges may be achieved by the use of

    algorithmic data correction. Contact Greenspan Technology for further information .

    -------------------------------------------------------------------------------------------------------------

    Accuracy 3% FS (with algorithm)

    --------------------------------------------------------------------------------------------------------------

    Supply Voltage 9-27VDC

    Reverse polarity protected

    Surge protected to 2kV

    --------------------------------------------------------------------------------------------------------------Quiescent Current 80mA

    --------------------------------------------------------------------------------------------------------------

    Warm up time to stable reading 2 Seconds

    --------------------------------------------------------------------------------------------------------------

    Output 4-20mA, 0-1V, 0-2.5V

    --------------------------------------------------------------------------------------------------------------

    Dimensions length 275mm,

    44.5mm OD Stainless Steel

    47mm OD Acetal co-polymer

    --------------------------------------------------------------------------------------------------------------

    Wetted Materials 316 Stainless Steel,Acetal co-polymer

    --------------------------------------------------------------------------------------------------------------

    Weight (potted) 735g, 316 Stainless Steel

    605g, Acetal co-polymer

    --------------------------------------------------------------------------------------------------------------

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    TURBIDITY

    SENSOR

    22 Palmerin Street, Warwick 4370 Qld Australia.

    Tel: 0746 601888 Fax: 0746 601800

    CERTIFICATE of CONFORMANCE

    Model No TS100

    Customer:

    Ref:

    ProductDetail Serial No. 010410

    Range 0 - 500 NTU

    Output FS 20.00mA

    Zero 4.00mA

    Accuracy +/- 3 % of FS(with algorithm)

    Linearity See User Manual

    Cable Length 60 metres

    Supply Voltage 9 - 27 VDC

    Supply Current 80 mA

    Connection: +ve Red

    gnd Green

    o/p Blue

    Connection Code BW3

    For further connection detail please refer toConnector Chart supplied.

    User

    Notes 1. The sensor is protected against reverse polarity.

    2. Do not attempt to dismantle the sensor as it will void the warranty. Contact your agentfor technical advice.

    2. The lens cover has been coated with an anti-fouling polymer to prevent marine growthaffecting accuracy.

    3. The calibration instrument utilises a flow-through cell within a Hach Ratio Turbidimeterreferenced against Formazin solutions.

    Inspected By ............ / /

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    APPENDIX 10

    ERRORS IN MEASUREMENT

    Error variations can occur in data due to a number of factors:

    1. Bench Testing The sensor is designed for intermittent sampling while fully

    immersed. Therefore any readings taken in air are not valid.

    They may only be used to indicate functional operation.

    2. Noise Environmental transients greater than the mean signal

    contribute to the background noise level. Also signal drift not

    associated with the actual flow conditions is considered to be

    noise. These can be caused by large floating debris, aquaticlife (fish) and installation lines obscuring the optical path

    briefly.

    3. Offsets Reflections from nearby surfaces of conduit, sea floor and

    river bed can offset readings, allow a clearance of at least

    250mm forward and 50mm to each side of the optical system.

    4. Bubbles Trapped air bubbles on the filter lens. Can be removed by

    tilting or stirring the sensor, positioning away from turbid

    water inlets and using lens cleaning pumps.

    5. Algae Algal growth will cause significant errors in as little as 35

    hours in extreme conditions, if allowed to accumulate on the

    lens. Regular cleaning and maintenance is essential, how

    often this is required is dependent on the severity of the

    micro-organism activity in the particular environment. A trial

    period should be allowed initially to determine the cleaning

    regime.

    6. Colour Stream water in forested Australian catchments is often

    coloured with Gilven. This component is leached from the

    leaves of trees, particularly in areas dominated by barked

    Eucalyptus. Gilven reduces Nephelometric turbidity by up to10%. Light sources with a wavelength of greater than 600 nm

    are insensitive to Gilven such as the Greenspan

    turbidimeters. (Ref Gippel 1989a).

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    TURBIDITY SENSOR CLEANING PUMP TP100

    FunctionTo maintain the optical cleanliness of the Turbidity Sensor by preventing

    fouling due to algal growth. A high pressure jet of filtered water is periodically

    forced across the lens dislodging any buildup of algae. When used in conjunction

    with the non stick polymer an efficient method of cleaning is produced. This

    system is particularly suitable for long term unattended data collection

    situations.

    InstallationThe unit conveniently clamps onto the TS100 sensor for easy installation and

    removal. The power cable is strapped to the sensor cable and brought to the

    surface for connection to the Timer Controller and battery.

    The Controller unit can be programmed for various Intervals and turn-on

    Durations by settings within the box. Please refer to the table below for settings

    available.

    Table 2.

    Switch Setting Interval (Hours) Duration (Seconds)

    0 1 2

    1 2 5

    2 3 10

    3 6 154 12 30

    5 24 60

    6 48 120

    7 72 240

    The duration chosen can easily be tested by momentarily pressing the TEST

    button located internally, this will activate the pump motor.

    A positive or negative going 5-12V input trigger from an external logger or

    Smart Sensor can also be fed to the Controller where a relay switched and timed

    pulse of power is generated. Smartcom software can be programmed to pulse thepump at regular intervals. Background Sampling can be selected in Sampler

    mode and is independant of the normal logged record interval. If the Smart

    Sensor is used as the trigger source, a negative going pulse is output from the

    sensor - please refer to the Smart Sensor user manual for connections.

    Greenspan recommends the customer establishes a cleaning regime dependant

    on environmental site conditions bearing in mind that the more often the pump

    is turned on the shorter the lifetime of the battery. An initial interval of 3 hours

    and a duration of 10 seconds is suggested as a starting point.

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    If possible, it is preferable to test the assembled pump mounted on the sensor by

    immersing near the surface prior to deployment at depth to verify operation and

    pump priming.

    The clamp can be removed from the sensor by undoing the two Allen key bolts

    and sliding the assembly off the turbidity head. When repositioning, ensure thatthe dispersal nozzle vent hole is forward of the optical head lens to maintain the

    water jet across the lens face.

    The pump filter cap is a push fit onto the motor body and is easily removed for

    cleaning.

    Pump Motor

    FilterInlet

    Powe r Cable toCont rol Box

    Optical Head

    Disp ersal

    Nozzle

    Turbid ity Sensor

    TP100Pump Clam p

    Figure 4. Pump Installation

    Note that the pump clamp has been designed to fit the optical head to allow for

    the differences in outside diameter of the sensor tube depending on whether

    Delrin body or stainless steel is used. When assembling the pump to the optical

    head, push the sensor all the way to the end stop and tighten the locating

    screws with a 2mm Allen key.

    The power supplied to the Timer Control unit is internally regulated to

    maintain timing consistency. The pump can be submerged to depths of up to

    50m, with cable lengths up to 70m maximum. It is suggested cable ties are usedto attach the pump cable to the sensor cable.

    It is recommended that a separate battery be used for the pump due to the

    greater power required and the switching transients that may be present. It is

    necessary however, to ensure a common ground between the pump power supply

    and the sensor supply.

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    SPECIFICATION TP100

    Specification Model TP100

    Connections Power +ve Red wire

    Power Ground Black wire

    Trigger Input User option, connections

    internal

    Supply line is protected internally with an

    automatically reset polyfuse.

    --------------------------------------------------------------------------------------------------------------

    Dimensions 115 x 90 x 55 (mm)--------------------------------------------------------------------------------------------------------------

    Power requirements 12 - 15VDC, typically 3 Amps. Supplies power to

    both Timer Control unit and pump motor

    --------------------------------------------------------------------------------------------------------------

    Cable Maximum length 70 metres, with 12VDC supply

    --------------------------------------------------------------------------------------------------------------

    Supplied with 1 x Pump cable

    1 x Pump filter cap

    1 x Timer Control unit, providing a variable timed

    pulse to the pump motor as well as an external

    trigger pulse capability.

    --------------------------------------------------------------------------------------------------------------