titan g2 60-300 · 2013. 12. 10. · product data titan™ g2 60-300 page 2 application results on...

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Product Data Titan G2 60-300 Deep sub-Ångström performance with the largest high tension range in S/TEM imaging and analysis optimized for a wide range of materials NanoResearch strives to increase our understanding of nanostructures and functional materials by linking the macroscopic material properties to the properties at the smallest level of detail: down to atoms. This continuing drive pushes for the better understanding of local atom organization and for the characterization of atoms, chemical bonding and even the electronic structure. The Titan™ G2 60-300 is the most powerful high resolution scanning transmission electron microscope (S/TEM) with the largest acceleration voltage range of 60 to 300 kV for 2D and 3D material characterization and chemical analysis, down to the atomic level, and delivers the ultimate performance in S/TEM imaging and chemical analysis by allowing the option to combine C s -correction, a monochromator, and a novel available ultra-stable high brightness electron gun (X-FEG) in one instrument. The Titan G2 60-300 with C s -correction enables studies in STEM mode with a focused probe or in TEM mode with a parallel beam with 80 pm guaranteed spatial resolution. The system is based on the Titan platform technology which is unmatched in mechanical, electronic, thermal, and optical stability and is designed to deliver the ultimate performance in all TEM, STEM, energy filtered TEM (EFTEM), diffraction and electron energy loss spectroscopy (EELS) & energy dispersive x-ray spectroscopy (EDS) modes. The flexibility of operating the Titan G2 60-300 in the range of 60 to 300 kV allows the optimization of this important parameter to the requirements of the material examined, from ultra-light carbon compounds to ultra-dense heavy metal materials. Additionally, with the wide pole piece gap of the S-TWIN lens, the Titan G2 60-300 is designed for dynamic experiments, which space to do more around the sample area. An innovative modular and patented design makes a field upgrade with a C s -corrector possible, allowing you a two-step approach to corrected microscopy in your laboratory. The stability, performance and ease of use of Titan enables corrected microscopy to be taken to the next level where new discoveries on the structure-property relationships of materials become possible at ever-decreasing scales. Titan is poised to bring electron microscopy into the new era by expanding the boundaries and achieving new results in NanoResearch. Key benefits • Increase your imaging and analysis capabilities with C S -correctors and/or a monochromator • Maximize the quality of the results by choosing the optimum acceleration voltage (60 to 300 kV) to minimize artifacts and maximize contrast • Increase your lateral resolution to the 80 pm level with a large objective pole piece gap for ‘space to do more’ • Maximize the information obtained of your sample in field free imaging (< 2 Oe) with nanometer resolution on magnetic material • Maximize the flexibility in diffraction (NBD, CBED, LACBED) with the new calibrated condenser system • Maximize your coherence and brightness of the electron source with the unmatched performance of the ultra stable X-FEG electron gun • Minimizing the energy spread of the electron source by adding a monochromator(< 0.2 eV) for HRTEM and with EELS spectroscopy applications

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  • Product Data

    Titan™ G2 60-300Deep sub-Ångström performance with the largest high tension range in S/TEM imaging and analysis optimized for a wide range of materials

    NanoResearch strives to increase our understanding of nanostructures and functional

    materials by linking the macroscopic material properties to the properties at the smallest

    level of detail: down to atoms. This continuing drive pushes for the better understanding

    of local atom organization and for the characterization of atoms, chemical bonding and

    even the electronic structure. The Titan™ G2 60-300 is the most powerful high resolution

    scanning transmission electron microscope (S/TEM) with the largest acceleration voltage

    range of 60 to 300 kV for 2D and 3D material characterization and chemical analysis,

    down to the atomic level, and delivers the ultimate performance in S/TEM imaging and

    chemical analysis by allowing the option to combine Cs-correction, a monochromator, and

    a novel available ultra-stable high brightness electron gun (X-FEG) in one instrument.

    The Titan G2 60-300 with Cs-correction enables studies in STEM mode with a focused

    probe or in TEM mode with a parallel beam with 80 pm guaranteed spatial resolution.

    The system is based on the Titan platform technology which is unmatched in mechanical,

    electronic, thermal, and optical stability and is designed to deliver the ultimate

    performance in all TEM, STEM, energy fi ltered TEM (EFTEM), diff raction and electron

    energy loss spectroscopy (EELS) & energy dispersive x-ray spectroscopy (EDS) modes. The

    fl exibility of operating the Titan G2 60-300 in the range of 60 to 300 kV allows the

    optimization of this important parameter to the requirements of the material examined,

    from ultra-light carbon compounds to ultra-dense heavy metal materials. Additionally,

    with the wide pole piece gap of the S-TWIN lens, the Titan G2 60-300 is designed for

    dynamic experiments, which space to do more around the sample area.

    An innovative modular and patented design makes a fi eld upgrade with a Cs-corrector

    possible, allowing you a two-step approach to corrected microscopy in your laboratory.

    The stability, performance and ease of use of Titan enables corrected microscopy to be

    taken to the next level where new discoveries on the structure-property relationships of

    materials become possible at ever-decreasing scales. Titan is poised to bring electron

    microscopy into the new era by expanding the boundaries and achieving new results in

    NanoResearch.

    Key benefi ts•Increaseyourimagingandanalysiscapabilities

    with CS-correctors and/or a monochromator •Maximizethequalityoftheresultsbychoosing

    the optimum acceleration voltage (60 to 300 kV) to minimize artifacts and maximize contrast

    •Increaseyourlateralresolutiontothe80pmlevelwith a large objective pole piece gap for ‘space to do more’

    •Maximizetheinformationobtainedofyoursample in fi eld free imaging (< 2 Oe) with nanometer resolution on magnetic material

    •Maximizetheflexibilityindiffraction(NBD,CBED,LACBED)withthenewcalibratedcondensersystem

    •Maximizeyourcoherenceandbrightnessoftheelectron source with the unmatched performance of the ultra stable X-FEG electron gun

    •Minimizingtheenergyspreadoftheelectronsource by adding a monochromator(< 0.2 eV) for HRTEM and with EELS spectroscopy applications

    C09FI75_1 DS TiG2 60-300_E.indd 1 16-7-09 16:44

  • Product Data Titan™ G2 60-300

    Page 2

    Application results on Titan G2 60-300

    Cs-corrected HR-STEM image on Ge112 at 300 kV with Fourier transformed showing 63 pm information transfer.

    Cs-corrected HR-TEM image at 300 kV in Ge .0.7 eV energy resolution (upper image).0.2 eV energy resolution (lower image).

    Atomic resolution holography image (upper left) on gold grain boundary using an image Cs-corrector and an X-FEG. The Fourier transformed (upper right) shows sub-Ångström information transfer (arrows).

    The reconstructed amplitude (left) and phase image (right) is shown below.Courtesy of Prof. M. Lehmann, M. Linck, Dr T. Niermann of TU Berlin, Germany, Prof. Hannes Lichte of TU Dresden, Germany, and Dr B. Freitag of FEI Company, The Netherlands.

    Monochromized EELS spectrum on Si ,SiO2 , SiOxNy revealing the diff erent bonding states in the compounds.

    Young’s fringe experiment on gold on carbon at 80/200 and 300 kV showing sub-Ångström information transfer.

    AtomicresolutionEELSmappingonBaTiO3/SrTiO3interfaceacquiredusinga Probe Cs-corrector at 200 kV. Sample courtesy of C.L. Jia, Ernst Ruska Centre, Research Centre Juelich, Germany. Image data courtesy of Prof. Gianluigi Botton and Sorin Lazar, McMasters University, Canada.

    Cs-corrected HR-TEM image on a fi lled SWCNT with fullerene structures on the surface of the SWCNT acquired at 60 kV acceleration voltage to minimize the beam damage. Sample courtesy of Prof. N. Kiselev, Institute of Crystallography, Moscow, Russia.

    For detailed description see separate application note.

    C09FI75_1 DS TiG2 60-300_E.indd 2 16-7-09 16:44

  • Product Data Titan™ G2 60-300

    Page 3

    Technical highlights•Optionalultra-stable,highbrightnessSchottkyfieldemittergun

    (X-FEG, for more details see separate product data sheet)

    •Newthreelenscondensersystemwithquantitativeindicationof

    convergence angle and size of illuminated area for quantitative

    measure of the electron dose and illumination conditions

    •Flexiblehightensionfrom60to300kV(60,80,120,200,300kV)

    •Onspecialrequest60kVCs-corrector alignments available

    •ElectrongunmonochromatorforhighenergyresolutioninEELS

    with symmetric energy distribution in zero-loss peak and improved

    spatial resolution, especially at low kV HR-S/TEM

    •CS-correction (probe and image CS-correction)

    •80pmperformance

    •Patentedmodularcolumndesignallowsaccuratemechanical

    stacking system for low excitation of the deflector units in the

    column to minimize instabilities due to electronic noise

    •ConstantPower™lensdesignforultimatethermalstabilityinmode

    and technique switches

    •Lowhysteresisdesigntominimizecross-talkbetweenoptical

    components

    •SymmetricS-TWINobjectivelenswithwidepolepiecegapdesign

    of 5.4 mm and ‘space to do more’ allowing the use of special

    holders such as heating, cooling, dual-axis tomography and

    STM/AFM holders

    •Objectiveapertureinthebackfocalplaneoftheobjectivelensfor

    optimum TEM dark field application work

    •Readyforon-siteretrofitofaprobeorimageCS-corrector

    •Automaticaperturesforremotecontroloperationandreproducible

    recall of aperture positions during aperture change

    •Rotation-freeimagingforeasyoperationandclearorientation

    relationship between the image and diffraction plane

    •Computerized5-axesspecimenstageforaccuratere-callofstored

    positions, tracking of the areas visited during search for the right

    area and ultra stable, deep sub-Ångström resolution with low

    specimen drift

    •Tiltrange±40degreesforanalyticaldoubletiltholdertoorientate

    the maximum amount of zone axis of one crystal in polycrystalline

    material.Withtomographyholdereven±80degreestominimize

    the missing wedge in 3D reconstructions

    •Field-freeimaging(<2Oe)inLorentzmodewith2nmresolution

    for magnetic property studies

    •OnspecialrequestCs-corrected field free imaging in Lorentz mode

    with < 1 nm resolution for magnetic property studies

    •TrueImage™focusseriessoftwareforquantitativeHR-TEM

    applications (for more details see separate product data sheet)

    •OnspecialrequesttheMultiLoaderisavailabletominimizethe

    initial drift after sample loading and maximize your throughput

    •Xplore3D™ software for automated tomography S/TEM

    experiments and Xplore3D Xpress for ultra-fast 3D reconstructions

    (for more details see separate product data sheet)

    Detectors•HAADFdetector

    •OnaxistripleDF1/DF2/BFdetectors

    •GatanUS1000/US4000&Oriuscameras

    •Eagleseriescameras

    •Gatanenergyfilterseries

    •Platecamera

    •Si(Li)EDSdetectorwithsolidangleof0.13srad

    and Fiori number > 4000

    Titan G2 60-300 Energy spread Point resolution Information limit STEM resolution

    Image corrector 0.7 to 0.8 eV** 80 pm 80 pm 136 pm

    Probe corrector 0.7 to 0.8 eV** 200 pm < 100 pm 80 pm

    Monochromator + X-FEG 0.2 to 0.3 eV* 200 pm 80 pm 136 pm

    * Depending on energy filter option

    ** S-FEG 0.7 eV, X-FEG 0.8 eV

    Note: All specifications are at 300 kV

    For a list of specifications of other acceleration voltage please

    contact your sales representative

    C09FI75_1 DS TiG2 60-300_E.indd 3 16-7-09 16:44

  • World HeadquartersPhone: +1.503.726.7500

    FEI EuropePhone: +31.40.23.56000

    FEI JapanPhone: +81.3.3740.0970

    FEI AsiaPhone: +65.6272.0050

    See beyond at FEI.com

    Product Data Titan™ G2 60-300

    DS0056 07-2009© 2009. We are constantly improving the performance of our products, so all specifi cations are subject to change without notice. The FEI logo, Titan, ConstantPower, TrueImage and Xplore3D are trademarks of FEI Company, and FEI is a registered trademark of FEI Company. All other trademarks belong to their respective owners.

    Floorplan Holders•Singletiltholder

    •Doubletiltholder

    •Tomographyholder

    •Pleaseaskforalistoffunctionalholders

    Installation requirements•Environmenttemperature18to23°C

    •Temperaturestability0.2°C/h

    •Heatdissipationintoairnominal4500W

    •Doorheight:2275mm(dependsonconfig)

    •Doorwidth:1050mm

    •Ceilingheight:3500mm(dependsonconfig)

    •Floorspaceneededformicroscope4500x5500mm

    •Weightdistributionmax465kg/m2

    •Powervoltage:3phaseincl.neutralandearth398V(+6%,-10%)

    •Frequency50or60Hz(+/-3%)

    •Powerconsumptionwithallmicroscopeoptionsmax.10kV

    •Electricalconnectionsinglephaseforwatercooler230V,4kVA

    •Coolingwaterrequired,dependingonwatercoolingunitordered

    •Doubleearthconnectionrequired

    •Compressedairsupply,pressuremin.5bar,max.7bar

    •NitrogenN2, pressure min. 1 bar, max. 3 bar

    •SF6gas,properventilationrequired

    •Pre-vacuumpumpoutlet

    •LiquidnitrogenLN2•LANconnectionforremotediagnostics

    Please contact your sales representative for more detailed information

    and for a complete pre-installation requirement document.

    TÜV Certification for design, manufacture, installation and support of focused ion- and electron-beam microscopes for the NanoElectronics, NanoBiology, NanoResearch and Industry markets.

    C09FI75_1 DS TiG2 60-300_E.indd 4 16-7-09 16:44