thermal response and reusability testing of advanced

50
' t. ~ .' AEDC-TR-79-62 = APR 2 4 1981 Thermal Response and Reusability Testing of Advanced Flexible Reusable Surface Insulation and Ceramic RSI Samples at Surface Temperatures to 1,200°F E. C. Knox ARO, Inc. April 1981 Final Report for Period April 4 - 5, 1979 Approved for public release; distribution unlimited. F,gl;~,'l.. .~ 3[ u. c.,. t;ir .'-o,cg P..i..rlc ' ",',,', " , t o~ .~ itrt iIq U,.,uG-¢,I -C.... ,,04 ARNOLD ENGINEERINGDEVELOPMENT CENTER ARNOLD AIR FORCESTATION, TENNESSEE AIR FORCESYSTEMS COMMAND UNITED STATES AIR FORCE

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Page 1: Thermal Response and Reusability Testing of Advanced

• ' t. ~ . '

AEDC-TR-79-62 • = APR 2 4 1981

Thermal Response and Reusability Testing of Advanced Flexible Reusable Surface

Insulation and Ceramic RSI Samples at Surface Temperatures to 1,200°F

E. C. Knox ARO, Inc.

April 1981

Final Report for Period April 4 - 5, 1979

Approved for public release; distribution unlimited.

F,gl;~,'l.. .~ 3[ u. c.,. t ; i r .'-o,cg P..i..rlc ' " , ' , , ' ,

" , t o~ . ~ i t r t iIq U,.,uG-¢, I -C.... ,,04

ARNOLD ENGINEERING DEVELOPMENT CENTER ARNOLD AIR FORCE STATION, TENNESSEE

AIR FORCE SYSTEMS COMMAND UNITED STATES AIR FORCE

Page 2: Thermal Response and Reusability Testing of Advanced

NOTICES

When U. S. Government drawings, specifications, or other data are used for any purpose other than a definitely related Government procurement operation, the Government thereby incurs no responsibility nor any obligation whatsoever, and the fact that the Government may have formulated, furnished, or in any way supplied the said drawings, specifications, or other data, is not to be regarded by implication or otherwise, or in any manner licensing the holder or any other person or corporation, or conveying any rights or permission to manufacture, use, or sell any patented invention that may in any way be related thereto.

Qualified users may obtain copies of this report from the Defense Technical Information Center.

References to named commercial products in this report are not to be considered in any sense as an indorsement of the product by the United States Air Force or the Government.

This report has been reviewed by the Office of Public Affairs (PA) and is releasable to the National Technical Information Service (NTIS). At NTIS, it will be available to the general public, including foreign nations.

APPROVAL STATEMENT

This report has been reviewed and approved.

JOSEPH F. PAWLICK, JR., Lt Colonel, USAF Director of Test Operations Deputy for Operations

Approved for publication:

FOR THE COMMANDER

Cf JAMES D. SANDERS, Colonel, USAF Deputy for Operations

Page 3: Thermal Response and Reusability Testing of Advanced

UNCLASSIFIED REPORT DOCUMENTATION PAGE

! REPORT NUMBER ~2 GOVT ACCESSION NO

L AEDC-TR-79-62

4 T ITLE ( ~ d Subttlte) THERMAL RESPONSE AND REUSABILITY TESTING OF ADVANCED FLEXIBLE REUSABLE SURFACE INSULATION AND CERAMIC RSI SAMPLES AT SURFACE TEMPERATURES TO 1,200°F

7. AUTHOR(.)

E. C. Knox, ARO, Inc., a Sverdrup Corporation Company

S PERFORMING ORGANIZATION N ~ E AND ADDRESS

A r n o l d E n g i n e e r i n g D e v e l o p m e n t C e n t e r / D O A i r F o r c e S y s t e m s Command A r n o l d A i r F o r c e S t a t i o n , T e n n e s s e e 37389

I|1. CONTROLLING OFFICE NAME ANO ADDRESS

NASA/JSC/ES3 H o u s t o n , T e x a s 77058

14 MONITORING AGENCY NAME & ADDRESS(JLdlIIerenf Irom Conlrolt |n80fl ico)

READ INSTRUCTIONS BEFORE COMPLETING FORM

3 RECIPIENT'S CATALOG NUMBER

S TYPE OF REPORT & PERIOD COVERED F i n a l R e p o r t , A p r i l 4 - 5 , 1979 B PERFORMING ORG. REPORT NUMBER

S. CONTRACT OR GRANT NUMBER(s)

10. PROGRAM ELEMENT, PROJECT, TASK AREA& WORK UNIT NUMBERS

P r o g r a m E l e m e n t 921E01

12. REPORT DATE April 1981 13. NUMBER OF PAGES

47 IS. SECURITY CLASS. (0! fhic raporfJ

UNCLAS S I F I ED

ISa. DECLASSI FICATION / DOWNGRADING SCHEDULE

N/A 16. DISTRIBUTION STATEMENT (ol thlc Rapowl)

A p p r o v e d f o r p u b l i c r e l e a s e ; d i s t r i b u t i o n u n l i m i t e d .

17. DISTRIBUTION STATEMENT (ol Ihe abstract entered In Block 20. I I dllfarm~t born Raporf)

IS. SUPPLEMENTARY NOTES

A v a i l a b l e i n D e f e n s e T e c h n i c a l I n f o r m a t i o n C e n t e r (DTIC) .

I9. KEY WORDS (CMfJnue on reverae aide II neceaaary ~ d I ~ n t l ~ ~ block numbe~

m a t e r i a l t e s t i n s u l a t i o n f l e x i b l e f a b r i c c e r a m i c t e m p e r a t u r e e x p o s u r e

ZO ABSTRACT (C~ l l nae m rav~aa aide I I n c c o a e ~ ~ d I d M f i ~ ~ block n m ~ r )

T e n - m i n u t e e x p o s u r e t e s t s w e r e p e r f o r m e d on s a m p l e s o f an a d v a n c e d f l e x i b l e r e u s a b l e s u r f a c e i n s u l a t i o n (AFRSI) made o f a q u a r t z g l a s s f a b r i c a n d s a m p l e s o f a c e r a m i c t i l e r e u s a b l e s u r f a c e i n s u l a t i o n ( R S I ) . The s a m p l e s w e r e t e s t e d i n a w i n d t u n n e l a e r o t h e r m a l e n v i r o n m e n t t h a t c a u s e d t h e s a m p l e s u r f a c e t o h e a t t o 1 , 2 0 0 ° F d u r i n g e a c h e x p o s u r e . No s e r i o u s d e f e c t s i n t h e s a m p l e s w e r e d e t e c t e d a s a r e s u l t o f t h e e x p o s u r e . The t e s t

FOR. 1473 ED,T, ON OF 1 NOV SS IS OBSOLETE DD , j AN ~3

UNCLASSIFIED

Page 4: Thermal Response and Reusability Testing of Advanced

UNCLASSIFIED

20. ABSTRACT. C o n c l u d e d

t e c h n i q u e u s e d p r o v i d e d a s u i t a b l e a e r o d y n a m i c h e a t i n g e n v i r o n m e n t f o r c a n d i d a t e m a t e r i a l s e v a l u a t i o n .

AFgC Amald AFS Telm

UNCLASSIFIED

Page 5: Thermal Response and Reusability Testing of Advanced

AEDC-TR-79-62

PREFACE

The work reported herein was conducted by the Arnold Engineering Development Center (AEDC), Air Force Systems Command (AFSC), at the request of the National Aeronautics and Space Administration (NASA), Johnson Space Center (JSC), Houston, Texas, for the NASA/Ames Research Center (ARC), Mountain View, California. The results of the test were obtained by ARO, Inc., AEDC Group (a Sverdrup Corporation Company), operating contractor for the AEDC, AFSC,. Arnold Air Force Station, Tennessee, under ARO Project Number V41C-56. The NASA-JSC program manager was Mr. Bill Moseley (E53), and the NASA-ARC program managers were Messrs. Howard Goldstein and Roy Wakefield. The data analysis was completed on June 28, 1979, and the manuscript was submitted for publication on August 2, 1979.

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AEDC-TR-79-62

C O N T E N T S

1.0 I N T R O D U C T I O N ........................................................ 5

2.0 A P P A R A T U S ........................................................... 6

2. I Test Facility .......................................................... 6

2.2 Test Article ........................................................... 6

2.3 Test Ins t rumenta t ion . . . . . . . . . . . . . . . . . . . . . . ' . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

2.3.1 Tunnel Condi t ions ............................................... 7

2.3.2 Test Data ....................................................... 7

3.0 T E S T D E S C R I P T I O N .................................................... 8

3.1 Test Cond i t ions and P rocedure .......................................... 8 3.1.1 Test Cond i t ions .................................................. 8

3.1.2 Test P rocedure .................................................. 8

3.2 Data Reduct ion ....................................................... 10

3.2.1 IR System P h o t o g r a p h s o f Sample Surface Tempera tu re . . . . . . . . . . . . . . . 10

3.2.2 Sample Tempera tu res ............................................ 10

3.2.3 Hea t -Trans fe r Measurements ...................................... 12

3.3 Uncer ta in ty o f Measurements ........................................... 12

3.3. ! General ........................................................ 12

3.3.2 Tunne l Condi t ions ............................................... 13

3.3.3 Test Data . . '. .................................................... 13

4.0 R E S U L T S A N D D I S C U S S I O N ............................................. 13

4.1 Sample Test Env i ronmen t .............................................. 14

4.2 Test Results .......................................................... 14

5.0 C O N C L U D I N G R E M A R K S ............................................... 15

R E F E R E N C E S .......................................................... 16

I L L U S T R A T I O N S

Figure

1. Tunne l C ................................................................ 17

2. Instal lat ion P h o t o g r a p h and Sketch .......................................... 18

3. P h o t o g r a p h s o f Test Samples ............................................... 20

4. Details o f Test Samples .................................................... 24

5. T h e r m o c o u p l e Loca t ions in Test Samples ..................................... 29

6. P h o t o g r a p h s o f Damaged Samples .......................................... 31

3

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A E DC-TR-79-62

Figure Page

7. AFRSI Spectral Emissivity ................................................. 33

8. Blackbody and AFRSI Total Emissivity ...................................... 34

9. Flow-Field Shadowgraph of Sample 2, Run 23 ................................ 36

10. Heat-Transfer and Shear Stress Distributions on Wedge Surface . . . . . . . . . . . . . . . . . 37

11. IR Camera Photograph Indicating Surface Temperature of Sample 2, Run 23 . . . . . 38

12. Influence o f Sample Emissivity on IR Camera Temperature Calibration . . . . . . . . . . . 39

13. Temperature Response of Sample 2 to Test Environment, Run 23 . . . . . . . . . . . . . . . . 40

TABLES

1. Test Summary ............................................................ 43

2. IR System Color /Tempera ture Calibration ................................... 44

APPENDIX

A. SURFACE E Q U I L I B R I U M T E M P E R A T U R E C O M P U T A T I O N . . . . . . . . . . . . . . . 45

N O M E N C L A T U R E ....................................................... 46

4

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AEDC-TR-79-62

1.0 INTRODUCTION

The structure of the space shuttle orbiter will be protected from the reentry thermal

environment by a system of ceramic Reusable Surface Insulation (RSI) tiles that can be i'eplaced quickly, as necessary, after one or several missions. This thermal protection system

design allows quick turn around of an orbiter subsequent to a mission and thereby makes the

shuttle concept cost effective; however, the cost of this system is significant. In an effort to recluce the total insulation costs, the National Aeronautics and Space Administration/Ames Research Center (NASA/ARC) has developed a less,:expensive Advanced Flexible Reusable

Surface Insulation (AFRSI) for possible use on th~ leeward surfaces of the orbiter as a replacement for the ceramic tiles. The AFRSI wdl experience relatively low heating rates and

is expected to reach an equilibrium surface temperature of about 1,200°F.

The suitability of the AFRSI requires testing in a simulated environment prior to

commitment for use on the orbiter. Radiant heating facilities provide the required temperature but not the other necessary conditions, most notably the surface shear. Plasma

jet facilities provide the desired temperature and shear, but the shear and heating rates are often too high. Moreover, particles in the flow for these facilities can produce serious material erosion, distorting the performance evaluation. The AFRSI needs to be tested in a

clean, convective heating environment that provides realistic surface shear. The AEDC yon K~rm~n Gas Dynamics Facility (VKF) Hypersonic Wind Tunnel (C) satisfies these requirements and was selected for testing the AFRSI samples largely because several

materials evaluation tests'have been conducted in this facility over the years. A summary

description of the testing techniques developed from these tests is presented in Ref. !.

t

In the present application the desired test environment was obtained by utilizing a wedge to support the materials samples and inclining it at a 25-deg angle to the Tunnel C Mach number 10 flow. The desired surface temperature and shear values, which were the primary

test conditions, were provided.

The principal objectives of the subject test were to determine the thermal response and reusability of the AFRSI thermal protection materials. A second objective was to obtain performance comparisons between AFRS! materials and the ceramic RSI tiles which the AFRSI are intended to replace. This report presents a description of the test technique

utilized and some typical test results•

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A E O C-T R -79-62 t

2.0 APPARATUS

2.1 TEST FACILITY

Tunnel C (Fig. l) is a closed-circuit, hypersonic wind tunnel with a Mach number l0

axisymmetric contoured nozzle and a 50-in.-diam test section. The tunnel can be operated continuously over a range of pressure levels from 200 to 2,000 psia with air supplied by the

VKF main compressor plant. Stagnation temperatures sufficient to avoid air liquefaction in the test section (up to 1,800°F) are obtained through the use of a natural gas-fired

combustion heater in series with an electric resistance heater. The entire tunnel (throat, nozzle, test section, and diffuser) is cooled by integral, external water jackets. The tunnel is

equipped with a model injection system, which allows removal of the model from the test section while the tunnel remains in operation. A description of the tunnel may be found in the Test Facilities Handbook (Ref. 2).

The local flow conditions needed to meet the test requirements were produced by using a

large wedge to process the tunnel free-stream Mach number l0 flow through an oblique

shock wave. Varying the wedge angle and the tunnel free-stream conditions tailored the flow conditions on the surface of the wedge (where the material samples were placed) to provide the needed local flow conditions. The wedge (Fig. 2) is a 15-in.-wide by 41.5-in.-Iong flat

plate mounted on a 13-deg wedge block. The flat plate has a i.5-in, backstep occurring 17.5 in. aft of the sharp leading edge, which permits mounting material samples flush with the plate surface. It was desired that a turbulent boundary layer exist on the material samples.

This was accomplished by welding three rows of 0.078-in.-diam spheres across the wedge, 3 in. from the leading edge. These spheres caused the normally laminar boundary layer to

transition to turbulent flow. An installation sketch of the spheres is also shown in Fig. 2. i

2.2 TEST ARTICLE

Four test articles were furnished by NASA/ARC, photographs of which are presented in Fig. 3. These articles, or samples, were fabricated at NASA/ARC and consisted of various combinations of Advanced Flexible Reusable Surface Insulation (AFRCI) and ceramic Reusable Surface Insulation (RSI). Shown in Fig. 4 are planform sketches of the test articles denoting the different combinations of insulation used on each sample. Using several materials on the same test sample enabled direct comparisons of the thermal response of these materials. In addition, the total wind tunnel test time required to test the various materials was reduced. Variations among the AFRS! samples were the weight of the fabric, the weave of the quilting, the felt thickness, and the edge formation. The RSI samples were

of different thicknesses and had various silicon coatings applied to their surfaces. Typical

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AE DC-TR-79-62

construction characteristics for the AFRSI and RSI tiles are also shown in Fig. 4e. All

samples were bonded to l/8-in.-thick aluminum plates which in turn were attached to

Bakelite ® plates of various thicknesses to maintain a total thickness of 1.50 in.

2.3 TEST INSTRUMENTATION

2.3.1 Tunnel Conditions

Tunnel C stilling chamber pressure is measured with a 500- or 2,500-psid transducer

referenced to a near vacuum. Based on periodic comparisons with secondary standards, the

accuracy (a bandwidth which includes 95 percent of the residuals, i.e., 2~ deviation) of the

transducers is estimated to be within +_0.16 percent of pressure or +_0.5 psi, whichever is

greater, for the 500-psid range and within + 0.16 percent of pressure or + 2.0 psi, whichever

is greater, for the 2,500-psid range. Stilling chamber temperature measurements are made

with Chromel ® -Alumel ® thermocouples which have an uncertainty o f +_(I.5°F + 0.375

percent of reading in °F).

2.3.2 Test D~ita

The instrumentation in each sample consisted of thermocouples (22 in samples 1, 3, and

4; 23 in sample 2) placed at positions of interest to evaluate the thermal response. The

thermocouples were o f AWG No. 36 (0.005-in. diam) plat inum/plat inum-rhodium (13

percent) material. The locations of these thermocouples in the samples are shown in Fig. 5.

The precision of these thermocouple measurements is _+ 4 deg for temperatures between 70

and 1,200°F.

A radiometer supplied by NASA/ARC was utilized to view a 0.5-in.-diam area of the sample surface about 2.8 in. aft of the sample leading edge and on the wedge centerline. This

instrument recorded the total radiant heat flux emitted from the sample area, and its output

was recorded in millivolts. The precision of the recorded signal is estimated to be +0.015

m Y .

The VKF infrared system was used to map the sample surface temperature. The system

utilizes an AGA Thermovision ® 680 camera which scans at a rate of 16 frames per second. The camera detector is sensitive to infrared radiation in the 3- to 6-tz wavelength band.

Camera calibrations are performed with a standard blackbody reference source, have consistently been within + 1 percent of the camera manufacturer 's calibration, and are repeatable within + i percent in absolute temperature. A description of the VKF system is

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A E D C-TR -79-62

given in Ref. 3. The output of the IR camera was displayed on a color TV monitor in real

time, and at selected times the monitor was photographed with a 70-mm color still camera.

Color movies (16mm) were taken of the samples intermittently during the run.

Shadowgraphs were taken after the samples reached the tunnel centerline and at selected wedge angles to record the flow-field characteristics.

Five Gardon-type heat flux gages were installed in the steel wedge ahead of the samples

(see Fig. 2b for locations). These gages had CR-AL thermocouples installed as part of the

gage, and the output of the gages provided confirmation of the boundary-layer state on the

wedge. The output of the gages was recorded at the same time the output of the sample

thermocouples was recorded. A general description of these gages is given in Ref. 2.

3.0 TEST DESCRIPTION

3.1 TEST CONDITIONS AND PROCEDURE

3.1.1 Test Conditions

The desired test conditions on the material samples were obtained by pitching the wedge

about 25 deg to the Tunnel C Mach number l0 flow and adjusting the stagnation pressure

and temperature. Pretest estimates showed that it would be necessary to set the tunnel

stagnation pressure as high as possible at the maximum tunnel stagnation temperature in

order to achieve the material temperature of 1,200°F within the 10-min exposure time. Following is a list of the tunnel stagnation conditions and the wedge local flow conditions

that existed during the test. A verification of the wedge flow conditions is presented in

Pt' Tt' P, T w, V w, Re x 10 -6 , w

M psia OR t l psia OR ft/sec ft -I W

10.14 1,200 2,150 3.3 0.083 676 4,207 0.95

Section 4.1.

A test summary showing all configurations tested and the variables for each is presented in Table 1.

3.1.2 Test Procedure

In the VKF continuous flow wind tunnels [Hypersonic Wind Tunnel (A), Supersonic

Wind Tunnel (B), and Tunnel C] the test article is mounted on a sting support mechanism in

8

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A EDC-TR-79-62

an installation tank directly underneath the tunnel test section. The tank is separated from

the tunnel by a pair of fairing doors and a safety door. When closed, the fairing doors,

except for a slot for the pitch sector, cover the opening to the tank, and the safety door seals

the tunnel from the tank area. After the test article is prepared for a data run, the personnel

access door to the installation tank is closed, the tank is vented to the tunnel flow, the safety

and fairing doors are opened, the model is injected into the airstream, and the fairing doors

are closed. After the data are obtained, the test article is retracted into the tank, and the

sequence is reversed with the tank being vented to atmosphere to allow access to the test

article in preparation for the next run. The sequence is repeated for each configuration

change.

The procedure for obtaining the test measurements evolved during the progress o f the

test. Initially there was concern for the survivability of the cloth samples at wedge angles as

large as 25 deg; hence, the wedge was injected at 6 = 0 and rotated to 25 deg, while the

sample (No. 3 was used) was observed for any indication of failure; the procedure was

reversed for retraction. No indications of failure were observed. Next the sample was

injected and retracted at c$ = 25 deg and again observed for indications of failure. No

problems were encountered during injection, but on retraction the top layer of the cloth

sample was blown away (see Fig. 6a). It appears the turbulence encountered during

retraction through the tunnel wall boundary layer at such a large angle was too severe. A

possible explanation of the absence of failure during injection through the same turbulence

is that the increased fabric temperature decreased its strength prior to retraction.

Consequently, the initial procedure described above was adopted for the remainder of the

test.

The samples were exposed to the flow for 10 rain each time they were injected. The output of all the instrumentation was recorded every 0.5 sec until the wedge reached the

25-deg pitch angle; then data were recorded every 5 sec for the remainder of the run. The IR

system TV monitor~ was observed, and when the sample surface temperature reached

approximately 1,200°F a 70-ram photograph was taken. Another photograph was taken just

prior to retraction.

The samples were observed directly during exposure, and whenever any unusual

circumstances developed (fabric tears or loose tiles) the 16-mm movie camera was used to

record the events. In addition, the injection cycle of each run was recorded on 16-mm film.

After retraction, the sample was cooled by high-pressure air through the tank door nozzle and adjustable manifolds on each side. Also, the steel wedge has internal water-

cooling passages which aided in cooling the sample. Whenever the sample's aluminum

support plate cooled to 150°F, the sample was injected for another run or was replaced by

9

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A EDC-TR-79-62

another sample. The nominal temperatures of the tiles at injection ranged from 70 to 140°F. Any damage to the samples was photographed using a 70-mm camera prior to continued

testing (see Fig. 6b).

Each exposure is termed a run, and all the data obtained are identified in the data tabulations by run number. The samples tested during each run are listed in Table I.

3.2 DATA REDUCTION

3.2.1 IR System Photographs of Sample Surface Temperature

The calibration of the IR system itself is detailed in Ref., 3, and the only other information required to obtain the sample surface temperature is the surface emissivity.

A representative sample of the fabric insulation was examined to determine its emissivity over the range from 3 to 6 #. The results are presented in Fig. 7. The sample total emissivity

was computed by the equation

6 (1)

t" = 6

3

where

~ =

ebZ =

X~.=

sample spectral emissivity from Fig. 7 at 530°R

blackbody spectral emissivity at 530 ° R

IR camera spectral response factor obtained from the manufacturer

Both ebX and (ebX Xx) variations with wavelength over the range of interest are presented in

Fig. 8a, and (e~) (ebX XX) variations are shown in Fig. 8b. The values of the integrals are

shown in the figures; from these the sample total emissivity was computed to be 0.62. For

this emissivity, the color calibration with temperature for the photographs of the IR system

TV monitor is listed in Table 2.

3.2.2 Sample Temperatures

Because of the expense of platinum wire, the thermocouple leads were only about 12 in.

long and terminated at a 50-pin connector inside the wedge support. Copper leads were used

10

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AEDC-TR-79-62

from the other side of the connector to the instrumentation. The output of the sample thermocouples was dependent upon the connector temperature with this type of hookup;

hence, the temperature at two locations (TRI and TR2) on the connector were measured using

CR-AL thermocouple wire. The connector temperatures were measured with direct readout

instruments in °F.

The total output of each thermocouple was computed by first calculating the equivalent

platinum millivolt output of the connector thermocouple using the following equation:

EI~ = 0.42282 4 (2.66830 x 10-3) TR1

where

E R = equivalent millivolt output of a platinum thermocouple at temperature TRI

TR I = measured connector temperature in °F

The second connector temperature (TR2) was used as a redundant measurement. The equivalent millivolt output (ER) was added to the output of each platinum thermocouple to

obtain the total millivolt output of each thermocouple (ETc). The temperature for each platinum thermocouple was then computed from the equation

TC i ffi Ao+ AI(ETCi)+ A 2 ( E T C I ) 2 + . . . + AN (ETci~

where the coefficients A0 ..., AN are defined below and " i " denotes the TC number.

(3)

Range o f

ETCi, mv A0 A1 A2 A3 A4

-0.422 ~ ETC ~ 1.175 591.727 270.981 -11.8644 53.7323 -37.7430

1.175 ~ ETC ~ 5.604 605.398 234.610 -17.7323 2.18924 -0.122826

5.604 ~ ETC ~ 11.024 657.117 192.452 -3.8197 0.0687992 - - -

A 5

11.9930

11

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A E D C-T R-79-62

3.2.3 Heat-Transfer Measurements

The output of the Garden-type heat gages was converted to heat flux by the equation

= (SF) (,~g) (4)

where AE is the measured gage output in millivolts and SF is the gage scale factor

determined from direct measurements of the gage output for a known radiant heat flux

input. The heat-transfer coefficient was then computed by the equation

h = ;J (5) o T t - - T

g

where T t is the tunnel total temperature and Tg is the gage temperature.

3.3 UNCERTAINTY OF MEASUREMENTS

3.3.1 General

The accuracy of the basic measurements (Pt and T0 was discussed in Section 2.3. On the basis of repeat calibrations, these errors were found to be

A P t - - = 0 . 0 0 1 6 = 0 . 1 6 p e r c e n t

P t

A T t

T t - 0 . 0 0 4 = 0 . 4 p e r c e n t

Uncertaint'ies in the tunnel free-stream parameters and the model temperatures were estimated using the Taylor series method of error propagation, Eq. (6),

(a 2 = ax,)2 ax2)= axa) 2 " " " °r ax, ) = (6)

where AF is the absolute uncertainty in the dependent parameter F = f(Xi, X2, X3...Xn) and

Xn represents the independent parameters (or basic measurements). The term AX, represents the uncertainties (errors) in the independent measurements (or variables).

12

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A EDC-TR-79-62

3.3.2 Tunnel Conditions

The accuracy (based on 20 deviation) of the basic tunnel parameters, Pt and T~ (see Section 2.3) and the 2a deviation in Mach number determined from test section flow

• calibrations were used to estimate uncertainties in the other flow parameters using Eq. (6). The computed uncertainties in the tunnel free-stream and wedge flow parameters are summarized below.

Uncertalnty~ (+-) Percent of Computed Value

M M P T V Re __ wE_ wE_ w_E - w

0.8 2.5 6.3 3.5 6.3 2.9

3.3.3 Test Data

The uncertainties of the test data parameters are summarized below.

Data Type

IR Color Boundary* Temperature

Ames Radiometer Output

Sample Temperature at 1,660°R

Connector Temperature at 575°R

Gardon Gage Heat Flux, ~, Btu/ft2-sec

Gardon Gage Temperature, Tg, OR

Gardon Gage Heat Transfer Coefficient, ho, Btu/ft2-sec°R

Uncertainty,

(±) percent of actual value

1.00

0.14

0.35

0.67

5.00

0.50

6.00

* See Fig. 11 for color/temperature calibration

4.0 RESULTS AND DISCUSSION

The purpose of this report is to present a description of the test technique used to achieve the test objectives and to present some typical test results. The test technique used is described in Section 3.0; the wedge surface flow conditions (corresponding to the material sample local flow conditions) are verified and typical results are presented in this section.

13

Page 17: Thermal Response and Reusability Testing of Advanced

A E DC-TR-79-62

4.1 SAMPLE TEST ENVIRONMENT

Shown in Fig. 9 is a shadowgraph of the flow over the sample surface. Several shocks

evidently are emanating from the quilted pattern in the fabric. The inclination of these

shocks is taken to be the Mach angle of the surface Mach number. From measurements of

the angles of the first and last shock that are visible in Fig. 9, the surface Mach number was

computed to be approximately 3.3. This Mach number corresponds to a wedge angle of 25.5

deg for the free-stream Mach number of 10.14. The indicated wedge angle was set to 24.5 deg; an additional degree of deflection apparently was produced by the aerodynamic loads.

From the wedge surface Mach number and tunnel stagnation conditions all the remaining surface conditions may be computed.

The computed surface flow conditions together with a finite difference procedure

outlined in Ref. 4 were used to calculate the surface heat-transfer coefficient and shear

distributions. It was assumed that transition occurred at the roughness location for the

turbulent case. The results are presented in Figs. 10a and b along with measurements from

the heat gages installed in the wedge ahead of the samples. It is seen from Fig. 10a that the

measured heat-transfer results agree well with computed values. The inferred shear values

from the heat gage measurements were computed from the equation below for a Prandtl number of one.

r = 0.117 h a V w (7)

4.2 TEST RESULTS

The sample surface temperature was monitored using the IR camera - - a picture was

taken whenever a region of the sample reached 1,200°F, and another was taken at the end of

the 10-min test period just prior to retraction. A typical picture of this type is presented in

Fig. 11. The temperatures associated with each color boundary are indicated on the picture. This temperature calibration was determined using an emissivity o f 0.62 for the fabric

samples and should be used to infer temperature for only the fabric portion of the sample surface.

To obtain the surface temperatures of the ceramic RSI tiles it would be necessary to

know the emissivity of those surfaces and adjust the IR camera temperature calibration for

the change. Shown in Fig. 12 are plots depicting the variation with emissivity of the

temperatures associated with each color number. The ceramic RSI tiles were not available

for pretest measurements of their emissivity values.

14

Page 18: Thermal Response and Reusability Testing of Advanced

AEDC-TR-79-62

Typical measured sample thermocouple temperatures are presented as a function of time

in Fig. 13 for Run 23. Also presented in Fig. 13a are (I) the IR camera indicated fabric

surface temperature at approximately the center of the fabric sample (see Fig. I l) and (2) the

computed fabric surface equilibrium temperature (1,630°R). The computed value was

obtained by a one-dimensional conduction code (Ref. 5), a brief description of which is

presented in Appendix A. The IR camera results show that the fabric surface reached the

desired temperature and agrees quite well with the predicted equilibrium value. The

temperature just under the top layer o f fabric (TCI4) is about 200°F less than the surface

temperature indicated by the IR camera. This difference illustrates the necessity of having an

external measurement of the surface temperature in materials evaluation tests o f this type. It

would be difficult to install a surface thermocouple in a 0.010-in. layer of glass cloth and

obtain a true surface temperature.

The heat from the surface did not penetrate through the fabric sample until about 200 sec

after exposure. This is indicated by TCI ~, which shows the rise was only about 100°F at the end of the exposure cycle. Even then a difference of about 1,000°F was maintained between

, the exposed and interior surfaces o f the insulation over its 1-in. thickness. The temperatures

at the thermocouple locations in the ceramic RSI tiles are presented in Fig. 13b. The

thickness of these tiles was not available to allow evaluations similar to those of the fabric

sample. However, it is of interest to note that thermocouples located on the edges of the tiles

rose to higher equilibrium values than the thermocouples near the center o f the tiles. The

temperature-time data shown'in Fig. 13 are typical for Sample 2.

The performance of the samples in terms of reusability did not indicate any serious

defects. Sample 2 underwent 15 different exposures with only moderately visible "wear and

tear ." Sample 3 was damaged (see Fig. 6a and Section 3. !.2) for unrelated reasons, Sample l

showed a little fraying of one of the edges and was withdrawn from use to allow posttest

examination, and Sample 4 experienced a tear down the center of both fabric samples (see

Fig. 6b) which may have been related to handling. The preliminary analysis indicates that the

reusability of the materials is good for the test environment to which the samples were

subjected during these tests. However, a detailed analysis will be done by NASA/ARC.

$.0 CONCLUDING REMARKS

Wind tunnel tests were conducted to determine the thermal response and reusability of

AFRSI and ceramic RSI thermal protection materials. The materials were subjected to a convective heating environment which heated their surface to 1,200°F. The materials were exposed for a total of 10 min on each injection with one sample being injected 15 times. The

15

Page 19: Thermal Response and Reusability Testing of Advanced

A E DC-TR-79-62

test environment was produced by a wedge at a 25-deg angle in the AEDC/VKF Mach 10

Hypersonic Wind Tunnel (C). The results of the tests may be summarized as follows:

. The materials testing technique developed at AEDC provided a clean convective

heating environment which subjected the materials samples to the required test conditions without any undesirable side effects (i. e., particle contamination) to distort the results.

. The temperature measured with a thermocouple under the top layer of fabric (0.010 in. thick) of the AFRSi material sample was 200°F less than the surface

temperature measured by the VKF IR system. This difference emphasizes the value of having an external measurement of the material surface temperature in evaluation tests of this type.

3. The temperature measurements on an AFRSI sample, which was about 1 in.

thick, indicated a 1,000°F difference between exposed and interior surfaces.

REFERENCES

1. Stallings, D. W. and Matthews, R. K. "Materials Testing in the VKF Continuous Flow Wind Tunnels." Proceedings, AIAA 9th Aerodynamics Testing Conference, Arlington, Texas, June 1976, pp. 233-237.

2. Test Facilities Handbook (Tenth Edition). "von K~rm~{n Gas Dynamics Facility, Vol. 3." Arnold Engineering Development Center, May 1974.

3. Boylan, D. E., et al. "Measurements and Mapping of Aerodynamic Heating Using a Remote Infrared Scanning Camera in Continuous Flow Wind Tunnels." AIAA Paper No. 78-799, April 1978.

4. Adams, J. C., Jr. "Implicit Finite-Difference Analysis of Compressible Laminar, Transitional, and Turbulent Boundary Layers Along the Windward Streamline of a Sharp Cone at Incidence." AEDC-TR-71-235 (AD734535), December 1971.

5. Marchand, E. O. "One Dimensional, Transient Heat Conduction in Composite Solids." M.S. Thesis, University of Tennessee, August 1974.

16

Page 20: Thermal Response and Reusability Testing of Advanced

TEST SECTION-

~ INSTRUMENTATION QUARTZ WlNDOif S - - RING

SCREEN \ Tlfl~OAT SECT,ON-~ SECTI~- 7 ~S~ETY DOOR

TRANSITION 7 ~ _ F A I R ~ SECT \ WATER /

• n- : _ , _ .. !1_ I , ~ , ~ : - , , N

OPERATION Im I I n n ' i & l

u. lt F E ?

a. Tunnel assembly

A E D C - T R - 7 9 - 6 2

MODEL SUPPO~ INJECT I ON/R.ETHACTIOR SYSTEM

DIFFUSER SECTION

~-'I II I--IZlll ~_~OD~ coo[iNG~ - U ;~B-- ,,R '.INK ll"--II

H ~ : °z'''Es ~L /I TEST SECTION TANK

WINDOWS FOR MODEL INS OR PHOTOGRAPHY

WINDOWS FOR SI-LADOWGRA: SCNLIEREN PHOTOGRAPHY

NOZZLE

AIR DUCTS TO COOL MODEL FOR HEAT- TRANSFER TESTS OR QUICK MODEL CHANGE

PRESSURE TRANSDUCERS AND VALVES

TANK EIq'I'HANCE DOOR FOR MODEL INSTALLATION OR INSPECTION ~ODEL INJECTION AND

PITCH MECHANISM

b. Tunnel test section Figure 1. Tunnel C.

17

Page 21: Thermal Response and Reusability Testing of Advanced

O0

m

~D &

a. Installation photograph Figure 2. Installation photograph and sketch.

Page 22: Thermal Response and Reusability Testing of Advanced

~O

~ ~ \ / ~ Gage Inoperative \ ~ \ • :.- _ ~ \ / During Test \ ~. ~ , ~ \

~ / ~ ! ~ - ~ ~ Is \ Surface-- 7 1.5-~

All Dimensions in nces

b. Installation sketch Figure 2. Concluded. m

J~ -n

Page 23: Thermal Response and Reusability Testing of Advanced

A EDC-TR-79-62

\

\ \ \

J

\

2~

A E D C 3 1 5 2 - 7 9

a. Sample No. 1 Figure 3. Photographs of test samples.

20

Page 24: Thermal Response and Reusability Testing of Advanced

A E DC-T R -79-62

P

_4

J

b

A,E D C 3153-79

b. Sample No. 2 Figure 3. Continued.

21

Page 25: Thermal Response and Reusability Testing of Advanced

A EDC-TR-79-62

A E D C 3 1 5 4 - 7 9

c. Sample No. 3 Figure 3. Continued.

22

Page 26: Thermal Response and Reusability Testing of Advanced

A EDC-TR-79-62

A E D C 3155-79

d. Sample No. 4 Figure 3. Concluded.

23

Page 27: Thermal Response and Reusability Testing of Advanced

A EDC-TR-79-62

AFRSI = Advanced Flexible Reusable Surface Insulation

RCG = Reaction-Cured Glass

12

12

12

AFRSI 593 Fabric Top I/2-in. Felt Taped Edges

(All Dimensions in Inches and Typical for Sample Nos. i, 3, and 4)

AFRSI 503 Fabric Top 1/2-in. Felt Taped Edges

N-18

RCG

N-17

RCG

N-12

White

RCG

N - I I

W h i t e

RCG

6

6

a. Sample No. 1 Figure 4. Details of test samples.

24

Page 28: Thermal Response and Reusability Testing of Advanced

A EDC-TR-79-62

AFRSI = A d v a n c e d F l e x i b l e R e u s a b l e S u r f a c e I n s u l a t i o n RCG = Reaction-CUred Glass

VHT = Very High Temperature Paint

~-- 3 - - D - g l - - - - - 6 ---- 6

6

6

12

I I

N - 2

RCG

L-2

RCG

L-4

RCG/VHT

L-I

RCG

L-3

RCG/VHT

AFRSI 593 Fabric Top

1-in. Felt Two Taped Edges

Panels Tufted Together

1 9

N - 4

RCG/

VHT

6

6

m

N-I

RCG 6

RCG/

VHT 6

All Dimensions in Inches

b. Sample No. 2 Figure 4. Continued.

25

Page 29: Thermal Response and Reusability Testing of Advanced

A EDC-TR-79-62

AFRSI = A d v a n c e d F l e x i b l e R e u s a b l e S u r f a c e I n s u l a t i o n RCG = R e a c t i o n - C u r e d G l a s s

VHT = V e r y H i g h T e m p e r a t u r e P a i n t

AFRSI 593 F a b r i c Top

1 / 2 - i n . F e l t R o l l e d E d g e s

AFRSI 503 F a b r i c Top

1 / 2 - i n . F e l t R o l l e d E d g e s

N-20

RCG/

VHT

N-19

RCG/

VHT

N-14

White

RCG

N-IS

White

RCG

See Fig. 3a 1'or Dimensions

c. Sample No. 3 Figure 4. Continued.

26

Page 30: Thermal Response and Reusability Testing of Advanced

AEDC-TR-79~2

AFRSI = A d v a n c e d F l e x i b l e R e u s a b l e S u r f a c e I n s u l a t i o n RCG = R e a c t i o n - C u r e d G l a s s

VHT = V e r y H i g h T e m p e r a t u r e P a i n t

AFRSI 5 9 3 F a b r i c

1 / 2 - i n . F e l t R o l l e d E d g e s

N - 2 2

RCG/

VHT

N-21

RC6/

VHT

AFRSI N - 1 6 503 F a b r i c

White i/2-in. Felt R o l l e d Edges RCG

N-15

White

RCG

See Fig. 3a for Dimensions

d. Sample No. 4 Figure 4. Continued.

27

Page 31: Thermal Response and Reusability Testing of Advanced

A EDC-TR-79-62

M a t e r i a l

, ~ ~ - ~ 0 ~ ~ n ~ " ~

~ ~ ~ , ~ ~ ~ ~ A - - F e l t

1.50 • ~ ~ ~ ~ ~ % ~_ _ ' j r n u a b r i c

"- ........................... ~ R T V - 6 0 ® Bond

~ ~ ~ ~ ~ - - Ap1 l ~ t i num Support

1 . AFRSI M a t e r i a l

Thickness I in.

0.010

V a r i a b l e

O.010 0 .010

0.125 V a r i a b l e

Typical Thermocouple Locations)

All Dimensions in Inches

II°

/Various Silicon Q --Coatings

Ceramic Material

-------q----RTV-60 ® Bond ...................................

w

,,~ ,~ ~ ,.~ ~ ,.~ ,.j --Felt Strain ,,~ ,,j ,,j ~ ~.~ ,.J ~ Isolation Pad (SIP)

. . . . . . . . . . . . . . . . . . . ~RTV-60 ® Bond ~ ~ ~ ~ ~ ~ - - ~ n u m Support

2 . C e r a m i c R S I T i l e s

e. Typical construction of AFRSI and RSI samples Figure 4, Concluded.

0 . 0 0 9

V a r i a b l e

0 . 0 1 0

Vat iable

0.010

0 . 1 2 5

V a r i a b l e

28

Page 32: Thermal Response and Reusability Testing of Advanced

A EDC-TR-79-62

0

In Top Coating of RSI Tile

Top of Strain Isolation Pad

Top of Aluminum Support Plate

AFRSI Panel (Location Noted)

1/4 in. Below Top of Fabric in Felt (Typ, TC Nos. 1 5 ~

210 ~ &- - l l 0 20

Upper Radius Under Top 22

18 0

17

Lower Side of Top Fabric (Typ, TC Nos. 16, 17, 20, 22) 16

&-- 10

14

D • 7 8

9

D I 5 6

13

D • 3 4

12 At Edge of Tile (Typ,.~, D @ TC NOS. 1, 3, 5, 7) ~ 1 2

See Fig. 3a for Dimensions

Note: Thermocouple locations shown are approximate.

a. Sample Nos. 1, 3, and 4 Figure 5. Thermocouple locations in t u t samples.

29

Page 33: Thermal Response and Reusability Testing of Advanced

A E DC-TR-79-62

0

21

In Top Coating of RSI Tile

Top of Strain Isolation Pad

Top of Aluminum Support Plate

AFRSI Panel (Locat ion Noted)

19 18 | • m20 08

•17 7

22

23

1% 4 9

@16

Lower Side of Top Fabr i 7

1 4 0 ~-- ii 0 I0

~---i.'4 in Below Top of Fabric in Felt

At Edge of Tile (Typ, TC Nos, 1, 3, 5, 7, 16, 17, 19, 23)

13

% ""

4 • • 3

12

See Fig. 3a for Dimensions

Note: Thormocouple locations shown are approximate.

b. Sample No. 2 Figure 5. Concluded.

30

Page 34: Thermal Response and Reusability Testing of Advanced

A E D C - T R - 7 9 - 6 2

Damage C o n s i s t e d o f :

( 1 ) R i p p i n g O f f Top F a b r i c L a y e r ( 2 ) T e a r i n g Away F e l t I n s u l a t i o n ,

E x p o s i n g B o t t o m F a b r i c L a y e r

( 2 ) : :~ ~ "~*~ " -~ - ~ll~.

• . ," ~ ~'~:

" ! i i, i --: i-i~"i , .F~°*.-"-:-°": '

" : : '" : : " ~ - I ~ : i-' " : . ' - - ' , "

a. Sample 3 after Run 1 Figure 6. Photographs of damaged samples.

31

Page 35: Thermal Response and Reusability Testing of Advanced

A E D C - T R - 7 9 - 6 2

Damage Consisted of:

(I) Fraying Edge (2) Ripping Off Top Fabric Layer

across Both Panels

• ~

: ~.~:;~'~"~ ~ ~.

..... ~.... . :~--.o~ .'-

b. Sample 4 after Run 18 Figure 6. Concluded.

32

Page 36: Thermal Response and Reusability Testing of Advanced

A E DC-TR-79-62

1 . I I I I I I I I I I

-- Note___ss

I n c i d e n c e r a d i a t i o n s o u r c e w a s a t 5 d e g f r o m n o r m a l t o s u r f a c e .

- - T e x t u r e o f f a b r i c s u r f a c e w a s a s s u m e d t o p r e c l u d e s i g n i f i c a n t v a r i a t i o n o f e~ w i t h i n c i d e n c e a n g l e

i i I "

y_-.

I I I I I I I I I 4 5

W a v e l e n g t h ( k ) ,

Figure 7. AFRSI spectral emissivity.

I I I , 6

33

Page 37: Thermal Response and Reusability Testing of Advanced

A E D C-T R-79-62

3

A

2

1

0

|

_ X~ -- IR Camera R e s p o n s e F a c t o r

/~ (e b X~) d~ = 2 . 0 9 4 X

- - ~. eb~ a t 530 O R

_ i

(ebX X x)

.- A¢~ _ V

_ ; '

-

- / \

3 4 5

W a v e l e n g t h (X), ~.

a. Blackbody emissivity Figure 8, Blackbody and AFRSI total emissivity.

34

Page 38: Thermal Response and Reusability Testing of Advanced

2

,c X x X) eb X

V

_ f ~ (¢X ebX X k) dX = 1 . 2 9 0 3

¢ = 1 . 2 9 0 3 ~ 0 . 6 2 - - 2 . 0 9 4

AEDC-TR-79~2

3 4 5

W a v e l e n g t h ( k ) ,

b. AFRSI sample total emissivity Figure 8. Concluded.

35

Page 39: Thermal Response and Reusability Testing of Advanced

A E D C - T R - 7 9 - 6 2

# -

, / /

, . o M w = 3.3 "

, / * sin-i i_~

. %

/

= 2 5 . 5 d e ~

= 1 0 . 1 , 1

i ¸ :~ ~ ~

?

Figure 9. Flow-field shadowgraph of Sample 2, Run 23.

36

Page 40: Thermal Response and Reusability Testing of Advanced

A E DC-T R-79-62

i0.0

Sym

I Average of Measurements

Max/Min of Measurements

Theory (Ref . 4)

5 = 2 5 . 5 deg

P t ffi l j 2 0 0 p s i a

T t = 2 ,150 OR

Tw ~ 900 °R

D: 0

I O

m I

C~

m

+J

6.0

4.0

2.0

1.0 m

m

0.6--

0.4 0

6.0

4,0 --

2.0 -

T u r b u l e n t ,

I I I I I I I I i0 20 30 40

X, in.

a. He~-transfer distribution along centerline

50

t i

~ o n t

Laminar

0 I I I I I I I I 0 10 20 30 40 50

X, in.

b. Shear stress distribution along centerline Figure 10. Heat-transfer and shear stress distributions on wedge surface.

37

Page 41: Thermal Response and Reusability Testing of Advanced

A E D C-T R - 7 9 - 6 2

AFRSI Sampi~

PoP'inter Which Temperature Was Selected for Fig. 13a

i 1,503 i 1,459 1 1,544

C o l o r

i i i i

1,584 I 1,6581 1,728 1,794 L 1,622 I ~ i, 762 _ _ _ _ I I

Bar Temperature Calibration (From Table 2), OR

Figure 11. I R camera photograph indicating surface temperature of Sample 2, Run 23.

38

Page 42: Thermal Response and Reusability Testing of Advanced

A E D C - T R - 7 9 ~ 2

+a

u

O) o~

20

4J

®

0

.,4

e~

O

;< :3 4~

k

10

0

-I0 m

a ,

2,200

2,000

1,800

1,600

1,400

Figure 12.

-20 I I I I 0 . 4 0 0 . 4 8 O. 56 0 . 6 4 0 . 7 2 0 . 8 0

Sample Emissivity, ¢

Percent change of I R camera temperature calibration wilh sample emissivity

1,200 0.40 O. 48 O. 56 0 . 6 4 0 . 7 2 0 . 8 0

Sample E m i s s i v i t y , e

b. IR camera temperature calibration (Runs 2 through 29) with emissivity

Influence of sample emissivity on I R camera temperature calibration.

39

Page 43: Thermal Response and Reusability Testing of Advanced

4~ 0

1,700

1,600

1,500

1,400

1,300

o 1,200

" 1 , 1 0 0

e 1,000

900

800

700

600

500 0

, / - -5 Changing i

~ 6 ~ 25 d e g

/ 9D--5 = 0

, ~d~ ~-Indicated ~~~------ ~ Surface

0 . . , . . . - , - " Computed S u r f a c e T e m p e r a t u r e E q u i l i b r u m T e m p e r a t u r e From IR Camera f ro m 1-D C o n d u c t i o n Code P h o t o g r a p h

( F i g . l l )

Lower S ide o f Top F a b r i c , TC14

0 . 2 5 i n . below Top of F a b r i c , TCIo

Top o f Aluminum S u p p o r t P l a t e , T C l l

I I I I I I I I00 200 300 400 500 600 700

Sample E x p o s u r c Time, t e x p , s e c

a. Temperature rise in AFRSI material Figure 13. Temperature response of Sample 2 to test environment, Run 23.

8 0 0

i l l O

J4 -n

¢0 & bJ

Page 44: Thermal Response and Reusability Testing of Advanced

q~

1,700

I,600

1,500

1,400

1,300

o 1,200 g

~ 12100

1,000

9 0 0

800

700

600

500 0

~---Edge~ TCI6

I ~--TC 5

~ C e n t e r , TC 6

~-TC15

I , , .

I I I I I 100 200 300 400 500

Sample Exposure Time, texp, sec

• b. Temperature rise in RSI tiles Figure 13. Continued.

0.125 in. Below Top of Time

Pad, TC13

I I 600 700 800 m

O o

~0 tO &

Page 45: Thermal Response and Reusability Testing of Advanced

4~

O

1,700

1,600

1,500

1,400

1,300

1,200 g

I,I00 k

1,000 O

900

800

700

600

500 " 0 I00 2 0 0

Edge, TCI7

C e n t e r ,

TCI8

Top o f Strain Isolation Pad, TC20

3 0 0 4 0 0 5 0 0

Sample Exposure Time, texp, sec

b. Concluded Figure 13. Concluded.

6 0 0

0.125 in. Below Top of Tile

7 0 0 8 0 0

> m o o

&

Page 46: Thermal Response and Reusability Testing of Advanced

Table 1. Test Summary

J~ L o

Sample Number

Sample Position,* deg

0

0

180

0

Run

2, 3, 4

9, 10, 11, 12, 19, 20, 21, 22, 23, 24, 25, 26, 27, 28, 29

I

5, 6, 7, 8, 13, 14, 15, 16, 17, 18

*Sample position locates the sample on the wedge. Looking downstream from the wedge f r o n t , the zero p o s i t i o n p laces the AFRSI sample on the l e f t s~de of the wedge, and the 180-de8 sample p o s i t i o n puts the AFRSI sample on the r i g h t s i de of the wedge.

m

o

"!I

W

b~

Page 47: Thermal Response and Reusability Testing of Advanced

A EDC-TR-79-62

Table 2. I R System Color/Temperature Calibration.

Temperature at Color Lower Boundary, OR Color Number Runs

Run 1 2 through 29

1

2

3

4

5

6

7

8

9

10

m

754

1,119

1,289

1,418

1,527

1,623

1,712

1,794

1,459

1,503

1,544

1,584

1,622

1,658

1,694

1,728

1,762

1,794

See Fig. 11 for color temperature callbration

44

Page 48: Thermal Response and Reusability Testing of Advanced

A EDC-TR-79-62

APPENDIX A

SURFACE EQUILIBRIUM TEMPERATURE COMPUTATION

A one-dimensional conduction computer code (Ref. 5) was used to compute the fabric

sample surface equilibrium temperature considering heat input to the fabric by aerodynamic convective heating and heat losses from the fabric surface to the tunnel walls by radiation.

The sum of these heat-transfer mechanisms represents the amount of heat available to be conducted into the fabric sample. The equation for the heat available for input into the

conduction code is as follows:

~I = h o ( T t - r ~ , ) - o ~ ~ 1"4 -TI~) (A-I)

The measured heat-transfer coefficient, ho, from Fig. 10a and the computed emissivity from Fig. 8 (~ = 0.62) were used in the above equation; a is the Stefan-Boltzmann constant, Tw is

the sample surface temperature, and TR is the reference (tunnel wall) temperature (530 to 70°F) for the radiation term.

The conduction code was begun by computing the heat input for the sample initial temperature of 540°R. The conduction code then computed the temperature rise in the

fabric with this heat input for a specified time (6 sec in this case). At that time a new surface temperature was computed and used in Eq. (A-l) to compute a subsequent heat input. The

process was continued for 600 sec, which was sufficient for the equilibrium condition (q = 0) to be reached. Only the top layer of fabric was considered in this computation because

the thermal contact between all subsequent layers was not defined. The backside of the fabric was assumed to be insulated. The physical properties of the top layer used in these

calculations were as follows:

Density = 75 lbm/ft 3

Specific heat = 0.25 Btu/lbm-°R

Thermal conductivity = 8.75 x 10-~ Btu/ft-sec-°R

Thickness = 0.010 in.

The calculated equilibruim surface temperature ~'as 1,630 °R.

45

Page 49: Thermal Response and Reusability Testing of Advanced

A E DC-TR-79-62

ER

ETC

AE

ebX

ho

M

P

Pt

Re

SF

T

Taw

T~

TRI, TR2

Tt

TCi

'~tex p

NOMENCLATURE

Equivalent millivolt output of a platinum thermocouple at connector temperature (TRt or TaD, my

Total millivolt output of the platinum thermocouple, mv

Millivolt output of gardon-type heat gages, mv

Blackbody spectral emissivity at 530°R

Heat-transfer coefficient [see Eq. (5)], Btu/ft2-sec-°R

Mach number

Static pressure, psia

Total pressure measured in tunnel stilling chamber, psia

Measured heat flux or computed heat input to sample surface, Btu/ft2-sec

Unit Reynolds number, ft- l

Gardon-type heat gage scale factor, Btu/ft2-sec/mv

Static temperature, °R

Adiabatic wall temperature, °R

Heat gage measured temperature, °R

Measured reference temperature at connector, °R

Total temperature measured in tunnel stilling chamber, °R

Output of thermocouple i, °R

Exposure time, sec

2

46

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V

X

Xk

6

E~

O"

Velocity, ft/sec

Distance from wedge leading edge (see Fig. 4b), in.

IR camera spectral response factor

Wedge angle with respect to free stream, deg

Fabric sample total emissivity

Fabric sample spectral emissivity

Wavelength, #

Mach angle, sin-1 (l/M), deg

Stefan-Boltzmann constant, 4.761 x 10 -13, Btu/ft2-sec-(°R) 4

Computed shear stress [Eq. (7)], lbf/ft 2

SUBSCRIPTS

W

Note:

Wedge flow conditions

Unsubscripted parameters denote tunnel free-stream conditions.

A E DC -T R -79-62

47