the transmission electron microscope

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The chapter gives insight into the transmission electron microscope technique. From "Electron Microscopy and Analysis" textbook by Peter J. Goodhew, John Humphreys and Richard Beanland. Courtesy of Taylor and Francis Books UK.

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Page 2: The transmission electron microscope

Contents (Note: Page numbers are as in the whole book so that the index remains valid)

Acronyms …………………………………………………….……………………… iii Preface ………………………………………………………………………………. iv

4 The transmission electron microscope 4.1 The instrument ……………………………………..… 66 4.2 Contrast mechanisms .…………………...…………… 76 4.3 High voltage electron microscopy (HVEM) .………… 108 4.4 Scanning transmission electron microscopy (STEM) .. 110 4.5 Preparation of specimens for TEM ……………..……. 110 4.6 Questions …………………………………………….. 121

Further reading ……………………………………………………………..……. 236 Answers ……………………………………………………………………………. 238 Index …………………………………………………………………………..……. 243

Page 3: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 4: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 5: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 6: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 7: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 8: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 9: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 10: The transmission electron microscope
Page 11: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 12: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 13: The transmission electron microscope
Page 14: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 15: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 16: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 17: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 18: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 19: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 20: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 21: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 22: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 23: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 24: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 25: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 26: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 27: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 28: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 29: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 30: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 31: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 32: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 33: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 34: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 35: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 36: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 37: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 38: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 39: The transmission electron microscope
Page 40: The transmission electron microscope
Page 41: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 42: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 43: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 44: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 45: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 46: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 47: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 48: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 49: The transmission electron microscope
Page 50: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 51: The transmission electron microscope
Page 52: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 53: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 54: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 55: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 56: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 57: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 58: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 59: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 60: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 61: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 62: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 63: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 64: The transmission electron microscope
Page 65: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 66: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 67: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 68: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 69: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 70: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 71: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 72: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________

Page 73: The transmission electron microscope

Reproduced by kind permission of Taylor and Francis Books UK under a Creative Commons Licence (BY-SA).Third Edition (electronic copy) by Peter J. Goodhew, John Humphreys, and Richard Beanland.

Electron Microscopy and Analysis,__________________________________________________________