status of pid detectors at bigrips

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Status of PID detectors at BigRIPS H. Sato, Detector team, RNC 2016/8/31 Expert Meeting @Gland Rapids 1

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Page 1: Status of PID detectors at BigRIPS

Status of PID detectors at BigRIPS

H. Sato, Detector team, RNC

2016/8/31 Expert Meeting @Gland Rapids 1

Page 2: Status of PID detectors at BigRIPS

PID detectors at BigRIPSParticle identification TOF-Br-DE method with track reconstruction

TOF: b

Plastic scintillator

PPAC x2

PPAC x2

Br with track reconstruction

PPAC x2

DE: MUSIC, Si

Isomer tagging: Ge1st stage

2nd stage

Br35, b35 Br57, b57

TOF, Br, DE Z, A/Q TOF: Time of flightBr: Magnetic rigidityDE: Energy loss

Target

Beam dump

Trajectories at focuses are measured for track reconstruction by using two double PPACs to improve A/Q resolution.

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Page 3: Status of PID detectors at BigRIPS

PPAC

●isobutane (C4H10), 10 Torr

●~150V/mm electric field

●Electron avalanche

Delay-Line read-out+

Parallel Plate Avalanche Counter : PPAC 2D position sensitive detector

240x150 double PPAC

Delay

line (X)

Delay

line (Y)

Particle

Cathode (X)

Cathode (Y)

Anode

Bias

voltage

X1

4.3 mm

X2

Y2

Y1

4.3 mm

high efficiency

anode

AX AY BY BX

A-side B-side

Particle

Double PPAC

H. Kumagai et al., NIMB 317(2013)717-727.

3

Page 4: Status of PID detectors at BigRIPS

Today’s items

1. Discharge problem Change of the material of the electrode Development of the anti-discharge unit

2. Endurance test with high-rate beams Efficiency Position resolution

3. Fabrication of the electrodes Clear strip gap Damage problem

Recent topics on the PPAC

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Page 5: Status of PID detectors at BigRIPS

1. Discharge problem

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Page 6: Status of PID detectors at BigRIPS

1. Damage due to discharge

Damaged spot

Electrical discharge sometimes occur with several tens of kHz of beams.

240 mm×150 mm Cu cathode ~5mm

ions

+

anodecathode

H.V.

Trip of H.V. modules frequently happens.

The occurrence of the damage must be avoided.

Damage on the cathode electrodes can be seen.

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Page 7: Status of PID detectors at BigRIPS

Change the electrode materials

Au, Al, Cu Ag Ag-cathode(~50 nm-thickness)

Empirically, silver electrode is more tolerant to the discharge than the others.

The occurrence of the discharge depends on the material of electrodes.

●Small electrical resistivity : Al > Au > Cu > Ag●Large thermal conductivity : Al < Au < Cu < Ag

Resistivity [mW cm] Thermal conductivity [W m-1 K-1]

0℃ 100℃ 0℃ 100℃

Al 2.5 3.55 236 240

Au 2.05 2.88 319 313

Cu 1.55 2.23 403 395

Ag 1.47 2.08 428 422 7

Page 8: Status of PID detectors at BigRIPS

Anti-discharge unit

H.V. is forced to become 0V to stop the discharge before ions hit the cathode electrode.

with anti-discharge unit +

cathode anode

H.V. 0V

cathode

+

anode

no damage

without anti-discharge unit

ions

+

anodecathode

H.V.

Anti-discharge unit (ADU) is being developed by Kumagai-san.

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Page 9: Status of PID detectors at BigRIPS

Function of the ADU

H.V. Power supply

Signalseparator

Preamp.

+12 V

20 ms Uni-vibrator

PPAC

Anti-discharge unit

Gas: C4H10 10 torr

10 MW

10 kW

220 pF

Power MOSFET

Anode sig.

Anode

Cathode

No discharge

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Page 10: Status of PID detectors at BigRIPS

Function of the ADU

H.V. Power supply

Signalseparator

Preamp.

+12 V

20 ms Uni-vibrator

PPAC

Anti-discharge unit

Gas: C4H10 10 torr

10 MW

10 kW

220 pF

Power MOSFET

Anode sig.

Discharge sig.

Anode

Cathode

Large anode signal due to a discharge drives the power MOSFET.

discharge!

Discharge occurs

shunt

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Page 11: Status of PID detectors at BigRIPS

Function of the ADU

H.V. Power supply

Signalseparator

Preamp.

+12 V

20 ms Uni-vibrator

PPAC

Anti-discharge unit

Gas: C4H10 10 torr

10 MW

10 kW

220 pF

Power MOSFET

Anode sig.

Discharge sig.

Reduce the damage on the cathode electrodes.

Anode

Cathode

H.V. becomes 0V within ~30 ns after the discharge.

This prevents ions from hitting the cathode.

H.V. becomes 0V

( H.V. recovers in ~5 ms. ) 11

Page 12: Status of PID detectors at BigRIPS

Test of the ADUDischarge was induced using 241Am-alpha by applying the too large bias voltage, intentionally.

The anode voltage (H.V.) was forcibly 0V by the anti-discharge unit.

Anode voltage

Cathode current

8

6

4

2 Cat

ho

de

curr

ent

(A)

An

od

e H

.V. (

V)

Dischargegrowth

600 800 1000 1200 1400

0

Time (ns)

600

200

400

0

800

Without anti-discharge unit

700 ns

Anode voltage

Cathode current

Cat

ho

de

curr

ent

(A)

An

od

e H

.V. (

V)

550 600 650 700 750

Time (ns)

1000

600

200

0

-200

400

-400

800

With anti-discharge unit10

6

2

0

-2

4

-4

8

35 ns

Prevent damages on the cathode electrodes 12

Page 13: Status of PID detectors at BigRIPS

2. endurance test with high-rate beams

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Page 14: Status of PID detectors at BigRIPS

2. Test with high-rate beams

● ~50 kHz of Cs (Z=55) ions for 2.5 days.

● ~70 kHz of Z~60-70 ions for ~5 hours.

● ~400 kHz of Sn (Z=50) ions for ~40 min.

No damage2014

First test with RI-beams for Ag electrode

● ~160 kHz of Ni (Z=28) ions for 1 hour

Apr. 2015

Ag electrodes

Anti-discharge unit

An endurance test of the PPAC against high-rate beams (Z~50) was carried out in Nov. 2015.

2012

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Page 15: Status of PID detectors at BigRIPS

Beam stopper

Plastic

Location of the PPACsTwo double-PPACs having anti-discharge units were located at F3.

F3-1 F3-2

15x15D#04 24x15D#08

150x150mm2 240x150mm2

A-sideB-side A-side

B-side

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Page 16: Status of PID detectors at BigRIPS

RI beams

132Sn (Z=50) purity: 6%133Sb (Z=51) purity: 20%134Te (Z=52) purity: 31%135I (Z=53) purity: 12%

E~220 MeV/u @F3

Beam spot(σ)

@F3-1

@F3-2

AX AY BX BY

AX AY BX BY

2.1mm 3.0mm 2.1mm 3.1mm

6.6mm 8.9mm 8.4mm 9.0mm

Z~50 beams were used.

16

AX AY BY BX

anode

A-side B-side

beam

Page 17: Status of PID detectors at BigRIPS

Bias voltage adjustment

65

70

75

80

85

90

95

100

690 700 710 720 730 740 750 760

effi

cien

cy [

%]

HV [V]

F3-1

F3-1A X [%]

F3-1A Y [%]

F3-1B X [%]

F3-1B Y [%]

A-side

B-side

30

35

40

45

50

55

60

65

70

75

80

85

90

95

100

690 700 710 720 730 740 750 760

effi

cien

cy [

%]

HV [V]

F3-2

F3-2A X [%]

F3-2A Y [%]

F3-2B X [%]

F3-2B Y [%]

B-side

A-side

F3-1 A-side:700V B-side:720V

F3-2 A-side:720V B-side:730V

AX AY BY BX

anode

A-side B-side

beam

Before irradiating the PPACs with intense beams, the HV dependence of detection efficiency for each cathode was measured with a 1kHz beam.

The bias voltage was adjusted for all cathodes so as to realize the efficiency of ~95% in order to reduce unnecessary voltage.

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Page 18: Status of PID detectors at BigRIPS

Beam rate

Rate of the beams @F3 was increased step by step as follows:

1.3 kcps (5min)↓

49 kcps (10min)↓

100 kcps (10min)↓

200 kcps (10min)↓

400 kcps (10min)↓

600 kcps (70min)↓

1 kcps (5min)↓

1000 kcps (60min)↓

1 kcps (5min)

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Page 19: Status of PID detectors at BigRIPS

Results: Endurance

600kcps 70min → No trip of HV modules for both PPACs

1Mcps 60min → No trip of the HV modules for both PPACs

anodeF3-1A

y2

anodeF3-1A

y2

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Page 20: Status of PID detectors at BigRIPS

90

92

94

96

98

100

0 200 400 600 800 1000

effi

cien

cy [

%]

F3 rate [kcps]

total efficiency: Y-direction

Y Total [%]

1k (*)

1k (**)

Calc.

Results: Efficiency

Ord

er o

f th

e m

easu

rem

ents

The efficiency obtained with 1k(*) and 1k(**) just after high-rate beams reproduce the values obtained with the 1.3k (first run). Electrodes were not damaged with

1Mcps beams for 60 minutes.

Tendency of the total efficiency was measured.

rate [kcps] X Total [%] Y Total [%]

1.3 99.86 99.92

49 99.70 99.83

100 99.74 99.80

200 99.57 99.72

400 98.89 99.30

600 97.70 98.51

1 (*) 99.95 99.96

1000 91.92 93.93

1 (**) 99.94 99.95

The tendency of the efficiency change can be explained by the dead time of the PPAC: delay time is 192 ns for X and 118 ns for Y.

90

92

94

96

98

100

0 200 400 600 800 1000

effi

cien

cy [

%]

F3 rate [kcps]

total efficiency: X-direction

X Total [%]

1k (*)

1k (**)

Calc.

Total efficiency Efficiency of each cathode

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Page 21: Status of PID detectors at BigRIPS

Results: Position resolution

Fitted trajectory using the lest of layers

Measured position

Layer of interest

F3-1

F3-2

AX BX

AX BX

The position resolution is deduced for the layer of interest with respect to the trajectory that was obtained by fitting the measured positions using the rest of layers.

Beam rate [kHz] Beam rate [kHz]

Po

siti

on

re

solu

tio

n (

r.m

.s.)

[m

m]

X-direction Y-direction

150mm

240mm

150mm

0.6

0.65

0.7

0.75

0.8

0 200 400 600 800 1000 1200

F3-1 AX

F3-1 BX

F3-2 AX

F3-2 BX

0.6

0.65

0.7

0.75

0.8

0 200 400 600 800 1000 1200

F3-1 AY

F3-1 BY

F3-2 AY

F3-2 BY

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Page 22: Status of PID detectors at BigRIPS

Results: action of the ADU

F3-1A

F3-1B

F3-2A

F3-2B

50ms/div

F3-2A

F3-2B

discharge

16ms

Signal from X cathodes

enlarged view

10ms/div

We increased the bias voltage of F3-2A up to 750V @1MHz beam, and a discharge happened on F3-2A.

The anti-discharge unit was operated.

Bias voltage was shutdown and recover.

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Page 23: Status of PID detectors at BigRIPS

Unresolved discharge problems

Damage on the anode appears because the lifetime of the cathode becomes longer by using the anti-discharge unit.

Discharge happens with high-rate light beams because higher bias voltage should be applied for enough efficiency.

The ADU cannot stop the electrons which are running to the anode. We prepared the anodes which have thicker Ag layer (50nm 100nm). We will test them on the beamline.

damage

Anode electrode (Al)

Same kind of damages are seen in the case of Ag.

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From the data of the efficiency, we found that the electrodes were not damaged. So, we think that the combination of the Ag electrode and the ADU is effective.

Page 24: Status of PID detectors at BigRIPS

3. Fabrication of the electrodes

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Page 25: Status of PID detectors at BigRIPS

3. Fabrication of the electrodesAg electrodes are fabricated by using vacuum evaporation.

after Ag deposition

mask for cathode electrode(240mm x 150mm)

Ag

mask

mylar filmframe of the mylar film

W boat

Side view

maskmylar film with the frame 25

Page 26: Status of PID detectors at BigRIPS

Non-clear strip gapsSometimes, non-clear strip gaps are seen after depositing Ag.

Ag strip(2.4mm)

Clear gap(0.15mm)

Non-clear gap thin Ag layer

Each strips are connected !

Such electrode cannot be used !

Microscopic view

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Page 27: Status of PID detectors at BigRIPS

Non-clear strip gapsNon-clear strip gaps comes from the imperfect contact between the mylar film and the mask wire.

Silicon rubber is put on the mylar film.

Production yield: ~50% 100%!

Add the spring to apply more tension to the mask wire.

View from downside

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Page 28: Status of PID detectors at BigRIPS

Damage on the Ag filmsAfter depositing Ag on the mylar film, sometimes damages (colored arer of the Ag) has been seen.

Sometimes, they appear immediately after finishing the deposition. Sometimes, they appear several days after.

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Ag Ag

Damage (~mm)Damage (~200mm)

anode electrode cathode electrode

Examples

Page 29: Status of PID detectors at BigRIPS

Component analysis with EPMA

There are no contaminants in the damaged area.We consider that the reason of the damage is due to the wet on the film.

The component analysis of the damaged area was done by using Electron Probe Micro Analyzer.

Electron-microscopic view

Normal region

Wt.(%)C 49.520O 24.740Ag 25.740------------Total 100.0

Ag

O

C

C & O from mylar film

Damaged region

Wt.(%)C 69.288O 13.653Ag 17.059------------Total 100.0

Ag

C

OC & O from mylar film

pock

?

film

wetAg

Spectrum of character X-rays

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Page 30: Status of PID detectors at BigRIPS

Summary

1. Material of the electrodes was changed (Au, Cu, Al Ag).

2. Anti-discharge unit is being developed by Kumagai-san.

3. PPAC worked with 1MHz beams (Z~50) for 60min.

4. There are unresolved problems: one is the damage on the anode and another is the discharge with high-rate light beams.

5. Fabrication technique for Ag electrodes has been modified. Investigation of the damage on the Ag films is continued. (We got a new air conditioner in this summer !!)

Development of the PPAC is reported.

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