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12.Uni-dir.(NON-OP)-50°C>+200°C Page 1 of 88 TEST VALVE INFORMATION DOC N° SPE 77/300C2 Shell-GSI Contract Number: FE Tightness Cl: ITEM N° Project & P.O. Number: Test valve no: Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0 Drawing: Material - Trim: Valve Nominal Size (DN / NPS): TEC Code: Pressure Class (PN / LBS): Valve Serial No: Heat No. Body: Test Temp. Range (°C): Heat No. Bonnet: PRE TESTING CHECK LIST SPE 77/300 (CMT / MESC ver. 13.0) SPE 77/300A, SPE 77/300B, SPE 77/300D (all CMT / MESC ver. 13.0) Confirm Does the test rig conform to C.2 of SPE 77/300 and figures C.1a, C.1b, C.1c? YES / NO YES / NO Is the tank and valve strong enough to withstand all forces exerted during the handling of the valve ? YES / NO Is the purity of the Helium equal to or higher than 97%? YES / NO Is the test rig suitable for testing the valve in both directions ? YES / NO Are the test rig valve end connectors provided with a pressure vent connection and a suitable thermocouple connection ? YES / NO TEST VALVE Is the test valve in accordance with the general arrangement drawing? YES / NO Is there a bill of material and does it indicate for every material the max. and min. temperature, hardness values and the origin of the industry standards? YES / NO Has a MESC buying description or valve DATA sheet been produced for the test valve? YES / NO Has test valve assembly been witnessed by Shell-GSI or its representative? YES / NO Has a HSE plan been produced for all testing work to be carried out? YES / NO Are test valve internals dry and thoroughly cleaned and degreased,dust and oil free? YES / NO Have pre-condition photographs been taken prior to valve assembly? YES / NO Has the valve passed the normal production tests in accordance with the manufacturers testing procedures? YES / NO Ensure the test pressure to be applied falls between 20% and 80% of the pressure gauges full scale. YES / NO Which device is to be used to measure leakage through the test valve ? SPECIFY YES / NO TAT @ AMBIENT TEMP. (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyy Step Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria Item (barg) Test cycles (min) Test Test Procedure Para. 1 0.0 Run-in Time to cycle Mech. Cycle SPE 77/300 C.4.2.1 2 2 Seat A 5 C.4.2.2 3 a 0.0 Seat A 1 C.4.2.3 b 0.0 Seat A 1 c 0.0 Seat A 1 4 0.0 C.4.2.4 5 17 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below 6 0.0 Seat A 1 12. Uni-directional (on/off) valves from –50 °C to > +200 °C without extended bonnet (non- operable valve): Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated and Low Temperature. NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE MANUFACTURER Design Temp. Range (°C): APPLICABLE DOCUMENTS TEST RIG CONNECTION & SUPPORTS For prototype- and production leak (pneumatic and FE) testing, do the testing operators have the NDT method leak testing levels LT1, LT2 or LT3, qualification/competences in accordance with BS-EN 473 (2008) and/or ISO 9712 (2005) + CORR.1 (2005) and/or ASNT SNT-TC-1A (2006)? TEST EQUIPMENT Do all test/measuring equipment and instruments have a system calibration certificate, traceable to (inter)national standards, to guarantee accuracy and have a valid calibration date not exceeding 3 (per ISO 15848) months for the mass spectrometer and 12 months for other equipment, prior to any test? BTO (Nm) ETC (Nm) Time Start Time Finish Seat leakage (ml/min) Allowable seat leakage (ml/min) SPE 77/300 para C.4.12 Table C.11 seat leakage (N2) + torques (BTO and ETC) at 1st cycle SPE 77/300 para C.4.12 Table C.11 seat leakage (N2) Shell / Body Test SPE 77/300 para C.4.12 Table C.10 body/shell leakage (He), no pressure drop. (+soapy water test on castings) Continious formation of bubbles? (YES/NO) Mech. Cycle + FE SPE 77/300 para C.4.12 Table C.11 seat leakage (N2) + torque (BTO and ETC) C.4.2.5+ C.4.2.2

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Page 1: Mesc Proxy Serv Let

12.Uni-dir.(NON-OP)-50°C>+200°C

Page 1 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

PRE TESTING CHECK LISTSPE 77/300 (CMT / MESC ver. 13.0)SPE 77/300A, SPE 77/300B, SPE 77/300D (all CMT / MESC ver. 13.0)

ConfirmDoes the test rig conform to C.2 of SPE 77/300 and figures C.1a, C.1b, C.1c? YES / NO

YES / NO

Is the tank and valve strong enough to withstand all forces exerted during the handling of the valve ? YES / NOIs the purity of the Helium equal to or higher than 97%? YES / NOIs the test rig suitable for testing the valve in both directions ? YES / NOAre the test rig valve end connectors provided with a pressure vent connection and a suitable thermocouple connection ? YES / NO

TEST VALVE

Is the test valve in accordance with the general arrangement drawing? YES / NOIs there a bill of material and does it indicate for every material the max. and min. temperature, hardness values and the origin of the industry standards? YES / NOHas a MESC buying description or valve DATA sheet been produced for the test valve? YES / NOHas test valve assembly been witnessed by Shell-GSI or its representative? YES / NOHas a HSE plan been produced for all testing work to be carried out? YES / NOAre test valve internals dry and thoroughly cleaned and degreased,dust and oil free? YES / NOHave pre-condition photographs been taken prior to valve assembly? YES / NOHas the valve passed the normal production tests in accordance with the manufacturers testing procedures? YES / NO

Ensure the test pressure to be applied falls between 20% and 80% of the pressure gauges full scale. YES / NOWhich device is to be used to measure leakage through the test valve ? SPECIFY

YES / NO

TAT @ AMBIENT TEMP. (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.1 0.0 Run-in Time to cycle Mech. Cycle

SPE 77/300

C.4.2.1

2 2 Seat A 5 C.4.2.2

3a 0.0 Seat A 1

C.4.2.3b 0.0 Seat A 1

c 0.0 Seat A 1

4 0.0C.4.2.4

5 17 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

6 0.0 Seat A 1

12. Uni-directional (on/off) valves from –50 °C to > +200 °C without extended bonnet (non-

operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

APPLICABLE DOCUMENTS

TEST RIG CONNECTION &

SUPPORTS

For prototype- and production leak (pneumatic and FE) testing, do the testing operators have the NDT method leak testing levels LT1, LT2 or LT3, qualification/competences in accordance with BS-EN 473 (2008) and/or ISO 9712 (2005) + CORR.1 (2005) and/or ASNT SNT-TC-1A (2006)?

TEST EQUIPMENT Do all test/measuring equipment and instruments have a system calibration certificate, traceable to (inter)national standards, to guarantee accuracy and have a valid calibration date not exceeding 3 (per ISO 15848) months

for the mass spectrometer and 12 months for other equipment, prior to any test?

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torques (BTO and ETC) at 1st cycle

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2)

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. (+soapy water test on castings)

Continious formation of bubbles? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.2.5+ C.4.2.2

Page 2: Mesc Proxy Serv Let

12.Uni-dir.(NON-OP)-50°C>+200°C

Page 2 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

12. Uni-directional (on/off) valves from –50 °C to > +200 °C without extended bonnet (non-

operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

FUGITIVE EMISSION TEST RESULTS @ AMBIENT TEMP. (HELIUM) per Shell MESC description:

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Warming up procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

TAT @ ELEVATED TEMP. (+200 °C.) ( HELIUM) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

7 0.0SPE 77/300

8 25 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.4 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Mech. Cycle + FE

Page 3: Mesc Proxy Serv Let

12.Uni-dir.(NON-OP)-50°C>+200°C

Page 3 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

12. Uni-directional (on/off) valves from –50 °C to > +200 °C without extended bonnet (non-

operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

FUGITIVE EMISSION TEST RESULTS @ ELEVATED TEMP. (+200 °C.) (HELIUM) per Shell MESC description:

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Warming up procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

TAT @ MAXIMUM ELEVATED TEMP. (NITROGEN 100%) per Shell MESC description: Test Temp: °C. Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

9 2 Seat A 5

SPE 77/300

10a 0.0 Seat A 1

b 0.0 Seat A 1

c 0.0 Seat A 1

11 0.0

12 17 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

13 0.0 Seat A 1

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torques (BTO and ETC) at 1st cycle

C.4.4 +C.4.2.2

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2)C.4.4 +C.4.2.3

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.4 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.4 +C.4.2.5

Page 4: Mesc Proxy Serv Let

12.Uni-dir.(NON-OP)-50°C>+200°C

Page 4 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

12. Uni-directional (on/off) valves from –50 °C to > +200 °C without extended bonnet (non-

operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

Test Temp: 0 °C.

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Cooling Down procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

FUGITIVE EMISSION TEST RESULTS @ MAXIMUM ELEVATED TEMP. (NITROGEN 100%) per Shell MESC description:

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

Page 5: Mesc Proxy Serv Let

12.Uni-dir.(NON-OP)-50°C>+200°C

Page 5 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

12. Uni-directional (on/off) valves from –50 °C to > +200 °C without extended bonnet (non-

operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

TAT @ -20 °C (NITROGEN 100%) per Shell MESC description: Test Temp: -20 °C. Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

14 2 Seat A 5

SPE 77/300

15a 0.0 Seat A 1b 0.0 Seat A 1c 0.0 Seat A 1

16 0.0

17 0.0 17 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

18 0.0 Seat A 1

FUGITIVE EMISSION TEST RESULTS @ -20 °C. (HELIUM) per Shell MESC description: Test Temp: -20 °C.

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Cooling Down procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C) +torques (BTO and ETC) at 1st cycle

C.4.6.1 +C.4.2.2

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C)C.4.6.2 +C.4.2.3

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.6.3 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C) +torque (BTO and ETC)

C.4.6.4+C.4.2.5

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

Page 6: Mesc Proxy Serv Let

12.Uni-dir.(NON-OP)-50°C>+200°C

Page 6 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

12. Uni-directional (on/off) valves from –50 °C to > +200 °C without extended bonnet (non-

operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

TAT @ LOW TEMP (NITROGEN) per Shell MESC description: Test Temp: °C Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

19 0.0 Seat A seat leakage (N2, He if T<-110 °C)

SPE 77/30020 0.0

21 0.0 FE Time to carry out FE Fugitive Emission (He) See FE results below

FUGITIVE EMISSION TEST RESULTS @ LOW TEMP (HELIUM) per Shell MESC description: Test Temp: 0 °C

Part / Item:

Static Measure NOTES

Highest measured valueStem / ID Packing boxGland / OD Packing boxBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Warming up procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

C.4.6.4+C.4.2.5

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.6.3 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Allowable Leakage FE (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

Page 7: Mesc Proxy Serv Let

12.Uni-dir.(NON-OP)-50°C>+200°C

Page 7 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

12. Uni-directional (on/off) valves from –50 °C to > +200 °C without extended bonnet (non-

operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

TAT; LOW & HIGH PRESSURE SEAT TEST @ AMBIENT TEMP (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

22 2 Seat A seat leakage (N2)

SPE 77/300

C.4.7

23 7 Seat A seat leakage (N2) C.4.7

24 0.0 Seat A 1

STRIPDOWN TEST (MESC SPE 77/300 Section C.4.8)

Part Mat. Ht. No's. & Markings Record Observations Regarding Condition of Parts

BODY BONNET / COVERCLOSURE ACLOSURE BOBTURATORSTEMSEAT RING ASEAT RING BSEAT INSERT ASEAT INSERT BBONNET EXTENSIONSTEM EXTENSIONGLANDGLAND BUSHGLAND FLANGELIP-SEALSPACKING TOP / BOTTOMPACKING INTERMEDIATERTJ GASKETFS GASKETBOLTSNUTSSEALSOthersOthersOthersOthersOthersOthers

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.7.6 +C.4.2.5

Item (GA dwg)

Mat. Conform Certs. (+Heat- and cert. No's.)

Page 8: Mesc Proxy Serv Let

12.Uni-dir.(NON-OP)-50°C>+200°C

Page 8 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

12. Uni-directional (on/off) valves from –50 °C to > +200 °C without extended bonnet (non-

operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

MAXIMUM ALLOWABLE FUGITIVE EMISSION LEAKAGE RATES (MESC SPE 77/300 Section C.4.11, tables C.7 + C.8 + C.9)Stem / ID Packing Enter Dimensions

belowDiam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Diam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Gland / OD Packing

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Body / Bonnet or Cover

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Body Joints / Closures

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

MAXIMUM ALLOWABLE SEAT LEAKAGE RATES (MESC SPE 77/300 Section C.4.10, tables C.5 and C.6)Type Acceptance Test Low, Ambient & Elevated Temp (≥ -20 °C, in ml/min) Low Temp or Cryogenic Temp (< -20 °C, in ml/min)

Soft seated Metal seated

DN (mm) 0 0.00 0.00 1,5 ml/min *DN = 0.00 4,8 ml/min *DN = 0.00

Allowable leak (Pa*m3/s) : Class A = 1.78 E -8 x stem diam (mm), Class B = 1.78 E -7 x stem diam (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

End flange (Ref. only)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Sealant Inj. Ports / Drains / Vents

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Soft seated (ISO 5208, Rate A)

Metal seated (ISO 5208, Rate B: 0,018 ml/min *DN)

Metal seated (ISO 5208, Rate C: 0,18 ml/min *DN)

Page 9: Mesc Proxy Serv Let

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Page 9 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

12. Uni-directional (on/off) valves from –50 °C to > +200 °C without extended bonnet (non-

operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

NOTES

CALCULATION METHODSTorque Values: Calculation @ 2bar Experience @ 2 bar Calculation @ 100% DP Experience @ 100% DP COMMENTSDesign opearting torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Test operating torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Actuator type:Packing bolt torqueOthersOthers

EQUIPMENT USEDHelium Mass SpectrometerPressure console; Digital Pressure Gauge Pressure gauge ManometerFlow-meter: Flow-meter: Torque meter: serial number Torque tool model Thermocouple (Stem Packing)Thermocouple (Ambient)Thermocouple (Internal Body)Thermocouple (External Body)OthersOthersOthers

FOR METAL SEATED BUTTERFLY VALVES IN PRESSURE CLASSES 900# AND ABOVE IT MIGHT BE BENEFICIAL FOR THE VALVE MANUFACTURER TO DETERMINE SEATLEAKAGE RATES IN THE NON-PREFERRED DIRECTION.

Page 10: Mesc Proxy Serv Let

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Page 10 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

12. Uni-directional (on/off) valves from –50 °C to > +200 °C without extended bonnet (non-

operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

Sequence 12. Typical pressure / temperature / mechanical cycling for uni-directional (on/off) valves from –50 °C to > +200 °C without extended bonnet (non-operable valve).

X = No test S = Seat test B = Body and fugitive emission test T = Torque test Indicated numbers above X, S, B and/or T are the amount of mechanical cycles to be performed.

Page 11: Mesc Proxy Serv Let

13.Uni-dir.(OP.)<-20°C>+200°C

Page 11 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

PRE TESTING CHECK LISTSPE 77/300 (CMT / MESC ver. 13.0)SPE 77/300A, SPE 77/300B, SPE 77/300D (all CMT / MESC ver. 13.0)

ConfirmDoes the test rig conform to C.2 of SPE 77/300 and figures C.1a, C.1b, C.1c? YES / NO

YES / NO

Is the tank and valve strong enough to withstand all forces exerted during the handling of the valve ? YES / NOIs the purity of the Helium equal to or higher than 97%? YES / NOIs the test rig suitable for testing the valve in both directions ? YES / NOAre the test rig valve end connectors provided with a pressure vent connection and a suitable thermocouple connection ? YES / NO

TEST VALVE

Is the test valve in accordance with the general arrangement drawing? YES / NOIs there a bill of material and does it indicate for every material the max. and min. temperature, hardness values and the origin of the industry standards? YES / NOHas a MESC buying description or valve DATA sheet been produced for the test valve? YES / NOHas test valve assembly been witnessed by Shell-GSI or its representative? YES / NOHas a HSE plan been produced for all testing work to be carried out? YES / NOAre test valve internals dry and thoroughly cleaned and degreased,dust and oil free? YES / NOHave pre-condition photographs been taken prior to valve assembly? YES / NOHas the valve passed the normal production tests in accordance with the manufacturers testing procedures? YES / NO

Ensure the test pressure to be applied falls between 20% and 80% of the pressure gauges full scale. YES / NOWhich device is to be used to measure leakage through the test valve ? SPECIFY

YES / NO

TAT @ AMBIENT TEMP. (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.1 0.0 Run-in Time to cycle Mech. Cycle

SPE 77/300

C.4.2.1

2 2 Seat A 5 C.4.2.2

3a 0.0 Seat A 1

C.4.2.3b 0.0 Seat A 1

c 0.0 Seat A 1

4 0.0C.4.2.4

5 17 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

6 0.0 Seat A 1

13. Uni-directional (on/off) valves from < –20 °C to > +200 °C with extended bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low / Cryogenic Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

APPLICABLE DOCUMENTS

TEST RIG CONNECTION &

SUPPORTS

For prototype- and production leak (pneumatic and FE) testing, do the testing operators have the NDT method leak testing levels LT1, LT2 or LT3, qualification/competences in accordance with BS-EN 473 (2008) and/or ISO 9712 (2005) + CORR.1 (2005) and/or ASNT SNT-TC-1A (2006)?

TEST EQUIPMENT Do all test/measuring equipment and instruments have a system calibration certificate, traceable to (inter)national standards, to guarantee accuracy and have a valid calibration date not exceeding 3 (per ISO 15848) months

for the mass spectrometer and 12 months for other equipment, prior to any test?

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torques (BTO and ETC) at 1st cycle

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2)

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. (+soapy water test on castings)

Continious formation of bubbles? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.2.5+ C.4.2.2

Page 12: Mesc Proxy Serv Let

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Page 12 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

13. Uni-directional (on/off) valves from < –20 °C to > +200 °C with extended bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low / Cryogenic Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

FUGITIVE EMISSION TEST RESULTS @ AMBIENT TEMP. (HELIUM) per Shell MESC description:

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Warming up procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

TAT @ ELEVATED TEMP. (+200 °C.) ( HELIUM) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

7 0.0SPE 77/300

8 25 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.4 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Mech. Cycle + FE

Page 13: Mesc Proxy Serv Let

13.Uni-dir.(OP.)<-20°C>+200°C

Page 13 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

13. Uni-directional (on/off) valves from < –20 °C to > +200 °C with extended bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low / Cryogenic Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

FUGITIVE EMISSION TEST RESULTS @ ELEVATED TEMP. (+200 °C.) (HELIUM) per Shell MESC description:

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Warming up procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

TAT @ MAXIMUM ELEVATED TEMP. (NITROGEN 100%) per Shell MESC description: Test Temp: °C. Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

9 2 Seat A 5

SPE 77/300

10a 0.0 Seat A 1

b 0.0 Seat A 1

c 0.0 Seat A 1

11 0.0

12 17 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

13 0.0 Seat A 1

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torques (BTO and ETC) at 1st cycle

C.4.4 +C.4.2.2

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2)C.4.4 +C.4.2.3

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.4 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.4 +C.4.2.5

Page 14: Mesc Proxy Serv Let

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Page 14 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

13. Uni-directional (on/off) valves from < –20 °C to > +200 °C with extended bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low / Cryogenic Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

Test Temp: 0 °C.

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Cooling Down procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

TAT @ LOW TEMP (NITROGEN) per Shell MESC description: Test Temp: °C Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

14 2 Seat A 5

SPE 77/300

15a 0.0 Seat A 1b 0.0 Seat A 1c 0.0 Seat A 1

16 0.0

17 0.0 17 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

18 0.0 Seat A 1

FUGITIVE EMISSION TEST RESULTS @ MAXIMUM ELEVATED TEMP. (NITROGEN 100%) per Shell MESC description:

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C) +torques (BTO and ETC) at 1st cycle

C.4.6.1 +C.4.2.2

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C)C.4.6.2 +C.4.2.3

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.6.3 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C) +torque (BTO and ETC)

C.4.6.4+C.4.2.5

Page 15: Mesc Proxy Serv Let

13.Uni-dir.(OP.)<-20°C>+200°C

Page 15 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

13. Uni-directional (on/off) valves from < –20 °C to > +200 °C with extended bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low / Cryogenic Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

FUGITIVE EMISSION TEST RESULTS @ LOW TEMP (HELIUM) per Shell MESC description: Test Temp: 0 °C

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Warming up procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

TAT; LOW & HIGH PRESSURE SEAT TEST @ AMBIENT TEMP (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

19 2 Seat A seat leakage (N2)

SPE 77/300

C.4.7

20 7 Seat A seat leakage (N2) C.4.7

21 0.0 Seat A 1

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.7.6 +C.4.2.5

Page 16: Mesc Proxy Serv Let

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Page 16 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

13. Uni-directional (on/off) valves from < –20 °C to > +200 °C with extended bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low / Cryogenic Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

STRIPDOWN TEST (MESC SPE 77/300 Section C.4.8)

Part Mat. Ht. No's. & Markings Record Observations Regarding Condition of Parts

BODY BONNET / COVERCLOSURE ACLOSURE BOBTURATORSTEMSEAT RING ASEAT RING BSEAT INSERT ASEAT INSERT BBONNET EXTENSIONSTEM EXTENSIONGLANDGLAND BUSHGLAND FLANGELIP-SEALSPACKING TOP / BOTTOMPACKING INTERMEDIATERTJ GASKETFS GASKETBOLTSNUTSSEALSOthersOthersOthersOthersOthersOthers

MAXIMUM ALLOWABLE FUGITIVE EMISSION LEAKAGE RATES (MESC SPE 77/300 Section C.4.11, tables C.7 + C.8 + C.9)Stem / ID Packing Enter Dimensions

belowDiam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Diam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Gland / OD Packing

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Body / Bonnet or Cover

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Item (GA dwg)

Mat. Conform Certs. (+Heat- and cert. No's.)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -8 x stem diam (mm), Class B = 1.78 E -7 x stem diam (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

End flange (Ref. only)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Page 17: Mesc Proxy Serv Let

13.Uni-dir.(OP.)<-20°C>+200°C

Page 17 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

13. Uni-directional (on/off) valves from < –20 °C to > +200 °C with extended bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low / Cryogenic Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

Body Joints / Closures

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

MAXIMUM ALLOWABLE SEAT LEAKAGE RATES (MESC SPE 77/300 Section C.4.10, tables C.5 and C.6)Type Acceptance Test Low, Ambient & Elevated Temp (≥ -20 °C, in ml/min) Low Temp or Cryogenic Temp (< -20 °C, in ml/min)

Soft seated Metal seated

DN (mm) 0 0.00 0.00 1,5 ml/min *DN = 0.00 4,8 ml/min *DN = 0.00

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Sealant Inj. Ports / Drains / Vents

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Soft seated (ISO 5208, Rate A)

Metal seated (ISO 5208, Rate B: 0,018 ml/min *DN)

Metal seated (ISO 5208, Rate C: 0,18 ml/min *DN)

Page 18: Mesc Proxy Serv Let

13.Uni-dir.(OP.)<-20°C>+200°C

Page 18 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

13. Uni-directional (on/off) valves from < –20 °C to > +200 °C with extended bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low / Cryogenic Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

NOTES

CALCULATION METHODSTorque Values: Calculation @ 2bar Experience @ 2 bar Calculation @ 100% DP Experience @ 100% DP COMMENTSDesign opearting torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Test operating torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Actuator type:Packing bolt torqueOthersOthers

EQUIPMENT USEDHelium Mass SpectrometerPressure console; Digital Pressure Gauge Pressure gauge ManometerFlow-meter: Flow-meter: Torque meter: serial number Torque tool model Thermocouple (Stem Packing)Thermocouple (Ambient)Thermocouple (Internal Body)Thermocouple (External Body)OthersOthersOthers

FOR METAL SEATED BUTTERFLY VALVES IN PRESSURE CLASSES 900# AND ABOVE IT MIGHT BE BENEFICIAL FOR THE VALVE MANUFACTURER TO DETERMINE SEATLEAKAGE RATES IN THE NON-PREFERRED DIRECTION.

Page 19: Mesc Proxy Serv Let

13.Uni-dir.(OP.)<-20°C>+200°C

Page 19 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

13. Uni-directional (on/off) valves from < –20 °C to > +200 °C with extended bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low / Cryogenic Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

Sequence 13. Typical pressure / temperature / mechanical cycling for uni-directional (on/off) valves from < –20 °C to > +200 °C with extended bonnet.

X = No test S = Seat test B = Body and fugitive emission test T = Torque test Indicated numbers above X, S, B and/or T are the amount of mechanical cycles to be performed.

Page 20: Mesc Proxy Serv Let

14.Uni-dir(NON-OP)-50>80≤200°C

Page 20 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

PRE TESTING CHECK LISTSPE 77/300 (CMT / MESC ver. 13.0)SPE 77/300A, SPE 77/300B, SPE 77/300D (all CMT / MESC ver. 13.0)

ConfirmDoes the test rig conform to C.2 of SPE 77/300 and figures C.1a, C.1b, C.1c? YES / NO

YES / NO

Is the tank and valve strong enough to withstand all forces exerted during the handling of the valve ? YES / NOIs the purity of the Helium equal to or higher than 97%? YES / NOIs the test rig suitable for testing the valve in both directions ? YES / NOAre the test rig valve end connectors provided with a pressure vent connection and a suitable thermocouple connection ? YES / NO

TEST VALVE

Is the test valve in accordance with the general arrangement drawing? YES / NOIs there a bill of material and does it indicate for every material the max. and min. temperature, hardness values and the origin of the industry standards? YES / NOHas a MESC buying description or valve DATA sheet been produced for the test valve? YES / NOHas test valve assembly been witnessed by Shell-GSI or its representative? YES / NOHas a HSE plan been produced for all testing work to be carried out? YES / NOAre test valve internals dry and thoroughly cleaned and degreased,dust and oil free? YES / NOHave pre-condition photographs been taken prior to valve assembly? YES / NOHas the valve passed the normal production tests in accordance with the manufacturers testing procedures? YES / NO

Ensure the test pressure to be applied falls between 20% and 80% of the pressure gauges full scale. YES / NOWhich device is to be used to measure leakage through the test valve ? SPECIFY

YES / NO

TAT @ AMBIENT TEMP. (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.1 0.0 Run-in Time to cycle Mech. Cycle

SPE 77/300

C.4.2.1

2 2 Seat A 5 C.4.2.2

3a 0.0 Seat A 1

C.4.2.3b 0.0 Seat A 1

c 0.0 Seat A 1

4 0.0C.4.2.4

5 25 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

6 0.0 Seat A 1

14. Uni-directional (on/off) valve from –50 °C to > +80 °C and ≤ +200 °C without extended

bonnet (non-operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

APPLICABLE DOCUMENTS

TEST RIG CONNECTION &

SUPPORTS

For prototype- and production leak (pneumatic and FE) testing, do the testing operators have the NDT method leak testing levels LT1, LT2 or LT3, qualification/competences in accordance with BS-EN 473 (2008) and/or ISO 9712 (2005) + CORR.1 (2005) and/or ASNT SNT-TC-1A (2006)?

TEST EQUIPMENT Do all test/measuring equipment and instruments have a system calibration certificate, traceable to (inter)national standards, to guarantee accuracy and have a valid calibration date not exceeding 3 (per ISO 15848) months

for the mass spectrometer and 12 months for other equipment, prior to any test?

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torques (BTO and ETC) at 1st cycle

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2)

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. (+soapy water test on castings)

Continious formation of bubbles? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.2.5+ C.4.2.2

Page 21: Mesc Proxy Serv Let

14.Uni-dir(NON-OP)-50>80≤200°C

Page 21 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

14. Uni-directional (on/off) valve from –50 °C to > +80 °C and ≤ +200 °C without extended

bonnet (non-operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

FUGITIVE EMISSION TEST RESULTS @ AMBIENT TEMP. (HELIUM) per Shell MESC description:

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Warming up procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

Page 22: Mesc Proxy Serv Let

14.Uni-dir(NON-OP)-50>80≤200°C

Page 22 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

14. Uni-directional (on/off) valve from –50 °C to > +80 °C and ≤ +200 °C without extended

bonnet (non-operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

TAT @ MAXIMUM ELEVATED TEMP. (NITROGEN 100%) per Shell MESC description: Test Temp: °C. Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

7 2 Seat A 5

SPE 77/300

8a 0.0 Seat A 1

b 0.0 Seat A 1

c 0.0 Seat A 1

9 0.0

10 26 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

11 0.0 Seat A 1

Test Temp: 0 °C.

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torques (BTO and ETC) at 1st cycle

C.4.4 +C.4.2.2

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2)C.4.4 +C.4.2.3

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.4 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.4 +C.4.2.5

FUGITIVE EMISSION TEST RESULTS @ MAXIMUM ELEVATED TEMP. (NITROGEN 100%) per Shell MESC description:

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Page 23: Mesc Proxy Serv Let

14.Uni-dir(NON-OP)-50>80≤200°C

Page 23 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

14. Uni-directional (on/off) valve from –50 °C to > +80 °C and ≤ +200 °C without extended

bonnet (non-operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

Cooling Down procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

TAT @ -20 °C (NITROGEN 100%) per Shell MESC description: Test Temp: -20 °C. Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

12 2 Seat A 5

SPE 77/300

13a 0.0 Seat A 1b 0.0 Seat A 1c 0.0 Seat A 1

14 0.0

15 0.0 25 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

16 0.0 Seat A 1

FUGITIVE EMISSION TEST RESULTS @ -20 °C. (HELIUM) per Shell MESC description: Test Temp: -20 °C.

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C) +torques (BTO and ETC) at 1st cycle

C.4.6.1 +C.4.2.2

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C)C.4.6.2 +C.4.2.3

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.6.3 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C) +torque (BTO and ETC)

C.4.6.4+C.4.2.5

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Page 24: Mesc Proxy Serv Let

14.Uni-dir(NON-OP)-50>80≤200°C

Page 24 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

14. Uni-directional (on/off) valve from –50 °C to > +80 °C and ≤ +200 °C without extended

bonnet (non-operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

Cooling Down procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

TAT @ LOW TEMP (NITROGEN) per Shell MESC description: Test Temp: °C Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

17 0.0 Seat A seat leakage (N2, He if T<-110 °C)

SPE 77/30018 0.0

19 0.0 FE Time to carry out FE Fugitive Emission (He) See FE results below

FUGITIVE EMISSION TEST RESULTS @ LOW TEMP (HELIUM) per Shell MESC description: Test Temp: 0 °C

Part / Item:

Static Measure NOTES

Highest measured valueStem / ID Packing boxGland / OD Packing boxBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

C.4.6.4+C.4.2.5

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.6.3 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Allowable Leakage FE (mbar*l/s)

Page 25: Mesc Proxy Serv Let

14.Uni-dir(NON-OP)-50>80≤200°C

Page 25 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

14. Uni-directional (on/off) valve from –50 °C to > +80 °C and ≤ +200 °C without extended

bonnet (non-operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

Warming up procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

TAT; LOW & HIGH PRESSURE SEAT TEST @ AMBIENT TEMP (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

20 2 Seat A seat leakage (N2)

SPE 77/300

C.4.7

21 7 Seat A seat leakage (N2) C.4.7

22 0.0 Seat A 1

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.7.6 +C.4.2.5

Page 26: Mesc Proxy Serv Let

14.Uni-dir(NON-OP)-50>80≤200°C

Page 26 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

14. Uni-directional (on/off) valve from –50 °C to > +80 °C and ≤ +200 °C without extended

bonnet (non-operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

STRIPDOWN TEST (MESC SPE 77/300 Section C.4.8)

Part Mat. Ht. No's. & Markings Record Observations Regarding Condition of Parts

BODY BONNET / COVERCLOSURE ACLOSURE BOBTURATORSTEMSEAT RING ASEAT RING BSEAT INSERT ASEAT INSERT BBONNET EXTENSIONSTEM EXTENSIONGLANDGLAND BUSHGLAND FLANGELIP-SEALSPACKING TOP / BOTTOMPACKING INTERMEDIATERTJ GASKETFS GASKETBOLTSNUTSSEALSOthersOthersOthersOthersOthersOthers

Item (GA dwg)

Mat. Conform Certs. (+Heat- and cert. No's.)

Page 27: Mesc Proxy Serv Let

14.Uni-dir(NON-OP)-50>80≤200°C

Page 27 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

14. Uni-directional (on/off) valve from –50 °C to > +80 °C and ≤ +200 °C without extended

bonnet (non-operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

MAXIMUM ALLOWABLE FUGITIVE EMISSION LEAKAGE RATES (MESC SPE 77/300 Section C.4.11, tables C.7 + C.8 + C.9)Stem / ID Packing Enter Dimensions

belowDiam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Diam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Gland / OD Packing

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Body / Bonnet or Cover

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Body Joints / Closures

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

MAXIMUM ALLOWABLE SEAT LEAKAGE RATES (MESC SPE 77/300 Section C.4.10, tables C.5 and C.6)Type Acceptance Test Low, Ambient & Elevated Temp (≥ -20 °C, in ml/min) Low Temp or Cryogenic Temp (< -20 °C, in ml/min)

Soft seated Metal seated

DN (mm) 0 0.00 0.00 1,5 ml/min *DN = 0.00 4,8 ml/min *DN = 0.00

Allowable leak (Pa*m3/s) : Class A = 1.78 E -8 x stem diam (mm), Class B = 1.78 E -7 x stem diam (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

End flange (Ref. only)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Sealant Inj. Ports / Drains / Vents

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Soft seated (ISO 5208, Rate A)

Metal seated (ISO 5208, Rate B: 0,018 ml/min *DN)

Metal seated (ISO 5208, Rate C: 0,18 ml/min *DN)

Page 28: Mesc Proxy Serv Let

14.Uni-dir(NON-OP)-50>80≤200°C

Page 28 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

14. Uni-directional (on/off) valve from –50 °C to > +80 °C and ≤ +200 °C without extended

bonnet (non-operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

NOTES

CALCULATION METHODSTorque Values: Calculation @ 2bar Experience @ 2 bar Calculation @ 100% DP Experience @ 100% DP COMMENTSDesign opearting torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Test operating torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Actuator type:Packing bolt torqueOthersOthers

EQUIPMENT USEDHelium Mass SpectrometerPressure console; Digital Pressure Gauge Pressure gauge ManometerFlow-meter: Flow-meter: Torque meter: serial number Torque tool model Thermocouple (Stem Packing)Thermocouple (Ambient)Thermocouple (Internal Body)Thermocouple (External Body)OthersOthersOthers

FOR METAL SEATED BUTTERFLY VALVES IN PRESSURE CLASSES 900# AND ABOVE IT MIGHT BE BENEFICIAL FOR THE VALVE MANUFACTURER TO DETERMINE SEATLEAKAGE RATES IN THE NON-PREFERRED DIRECTION.

Page 29: Mesc Proxy Serv Let

14.Uni-dir(NON-OP)-50>80≤200°C

Page 29 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

14. Uni-directional (on/off) valve from –50 °C to > +80 °C and ≤ +200 °C without extended

bonnet (non-operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

Sequence 14. Typical pressure / temperature / mechanical cycling for uni-directional (on/off) valves from –50 °C to > +80 °C and ≤ +200 °C without extended bonnet (non-operable valve).

X = No test S = Seat test B = Body and fugitive emission test T = Torque test Indicated numbers above X, S, B and/or T are the amount of mechanical cycles to be performed.

Page 30: Mesc Proxy Serv Let

15.Uni-dir.(NON-OP)-50°C≤80°C

Page 30 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

PRE TESTING CHECK LISTSPE 77/300 (CMT / MESC ver. 13.0)SPE 77/300A, SPE 77/300B, SPE 77/300D (all CMT / MESC ver. 13.0)

ConfirmDoes the test rig conform to C.2 of SPE 77/300 and figures C.1a, C.1b, C.1c? YES / NO

YES / NO

Is the tank and valve strong enough to withstand all forces exerted during the handling of the valve ? YES / NOIs the purity of the Helium equal to or higher than 97%? YES / NOIs the test rig suitable for testing the valve in both directions ? YES / NOAre the test rig valve end connectors provided with a pressure vent connection and a suitable thermocouple connection ? YES / NO

TEST VALVE

Is the test valve in accordance with the general arrangement drawing? YES / NOIs there a bill of material and does it indicate for every material the max. and min. temperature, hardness values and the origin of the industry standards? YES / NOHas a MESC buying description or valve DATA sheet been produced for the test valve? YES / NOHas test valve assembly been witnessed by Shell-GSI or its representative? YES / NOHas a HSE plan been produced for all testing work to be carried out? YES / NOAre test valve internals dry and thoroughly cleaned and degreased,dust and oil free? YES / NOHave pre-condition photographs been taken prior to valve assembly? YES / NOHas the valve passed the normal production tests in accordance with the manufacturers testing procedures? YES / NO

Ensure the test pressure to be applied falls between 20% and 80% of the pressure gauges full scale. YES / NOWhich device is to be used to measure leakage through the test valve ? SPECIFY

YES / NO

TAT @ AMBIENT TEMP. (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.1 0.0 Run-in Time to cycle Mech. Cycle

SPE 77/300

C.4.2.1

2 2 Seat A 5 C.4.2.2

3a 0.0 Seat A 1

C.4.2.3b 0.0 Seat A 1

c 0.0 Seat A 1

4 0.0C.4.2.4

5 42 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

6 0.0 Seat A 1

15. Uni-directional (on/off) valve from –50 °C to ≤ +80 °C without extended bonnet (non-

operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and Low

Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

APPLICABLE DOCUMENTS

TEST RIG CONNECTION &

SUPPORTS

For prototype- and production leak (pneumatic and FE) testing, do the testing operators have the NDT method leak testing levels LT1, LT2 or LT3, qualification/competences in accordance with BS-EN 473 (2008) and/or ISO 9712 (2005) + CORR.1 (2005) and/or ASNT SNT-TC-1A (2006)?

TEST EQUIPMENT Do all test/measuring equipment and instruments have a system calibration certificate, traceable to (inter)national standards, to guarantee accuracy and have a valid calibration date not exceeding 3 (per ISO 15848) months

for the mass spectrometer and 12 months for other equipment, prior to any test?

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torques (BTO and ETC) at 1st cycle

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2)

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. (+soapy water test on castings)

Continious formation of bubbles? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.2.5+ C.4.2.2

Page 31: Mesc Proxy Serv Let

15.Uni-dir.(NON-OP)-50°C≤80°C

Page 31 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

15. Uni-directional (on/off) valve from –50 °C to ≤ +80 °C without extended bonnet (non-

operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and Low

Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

FUGITIVE EMISSION TEST RESULTS @ AMBIENT TEMP. (HELIUM) per Shell MESC description:

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Warming up procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

Page 32: Mesc Proxy Serv Let

15.Uni-dir.(NON-OP)-50°C≤80°C

Page 32 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

15. Uni-directional (on/off) valve from –50 °C to ≤ +80 °C without extended bonnet (non-

operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and Low

Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

TAT @ -20 °C (NITROGEN 100%) per Shell MESC description: Test Temp: -20 °C. Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

7 2 Seat A 5

SPE 77/300

8a 0.0 Seat A 1b 0.0 Seat A 1c 0.0 Seat A 1

9 0.0

10 0.0 42 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

11 0.0 Seat A 1

FUGITIVE EMISSION TEST RESULTS @ -20 °C. (HELIUM) per Shell MESC description: Test Temp: -20 °C.

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Cooling Down procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C) +torques (BTO and ETC) at 1st cycle

C.4.6.1 +C.4.2.2

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C)C.4.6.2 +C.4.2.3

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.6.3 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C) +torque (BTO and ETC)

C.4.6.4+C.4.2.5

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

Page 33: Mesc Proxy Serv Let

15.Uni-dir.(NON-OP)-50°C≤80°C

Page 33 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

15. Uni-directional (on/off) valve from –50 °C to ≤ +80 °C without extended bonnet (non-

operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and Low

Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

TAT @ LOW TEMP (NITROGEN) per Shell MESC description: Test Temp: °C Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

12 0.0 Seat A seat leakage (N2, He if T<-110 °C)

SPE 77/30013 0.0

14 0.0 FE Time to carry out FE Fugitive Emission (He) See FE results below

FUGITIVE EMISSION TEST RESULTS @ LOW TEMP (HELIUM) per Shell MESC description: Test Temp: 0 °C

Part / Item:

Static Measure NOTES

Highest measured valueStem / ID Packing boxGland / OD Packing boxBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Warming up procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

C.4.6.4+C.4.2.5

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.6.3 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Allowable Leakage FE (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

Page 34: Mesc Proxy Serv Let

15.Uni-dir.(NON-OP)-50°C≤80°C

Page 34 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

15. Uni-directional (on/off) valve from –50 °C to ≤ +80 °C without extended bonnet (non-

operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and Low

Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

TAT; LOW & HIGH PRESSURE SEAT TEST @ AMBIENT TEMP (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

15 2 Seat A seat leakage (N2)

SPE 77/300

C.4.7

16 7 Seat A seat leakage (N2) C.4.7

17 0.0 Seat A 1

STRIPDOWN TEST (MESC SPE 77/300 Section C.4.8)

Part Mat. Ht. No's. & Markings Record Observations Regarding Condition of Parts

BODY BONNET / COVERCLOSURE ACLOSURE BOBTURATORSTEMSEAT RING ASEAT RING BSEAT INSERT ASEAT INSERT BBONNET EXTENSIONSTEM EXTENSIONGLANDGLAND BUSHGLAND FLANGELIP-SEALSPACKING TOP / BOTTOMPACKING INTERMEDIATERTJ GASKETFS GASKETBOLTSNUTSSEALSOthersOthersOthersOthersOthersOthers

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.7.6 +C.4.2.5

Item (GA dwg)

Mat. Conform Certs. (+Heat- and cert. No's.)

Page 35: Mesc Proxy Serv Let

15.Uni-dir.(NON-OP)-50°C≤80°C

Page 35 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

15. Uni-directional (on/off) valve from –50 °C to ≤ +80 °C without extended bonnet (non-

operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and Low

Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

MAXIMUM ALLOWABLE FUGITIVE EMISSION LEAKAGE RATES (MESC SPE 77/300 Section C.4.11, tables C.7 + C.8 + C.9)Stem / ID Packing Enter Dimensions

belowDiam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Diam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Gland / OD Packing

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Body / Bonnet or Cover

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Body Joints / Closures

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

MAXIMUM ALLOWABLE SEAT LEAKAGE RATES (MESC SPE 77/300 Section C.4.10, tables C.5 and C.6)Type Acceptance Test Low, Ambient & Elevated Temp (≥ -20 °C, in ml/min) Low Temp or Cryogenic Temp (< -20 °C, in ml/min)

Soft seated Metal seated

DN (mm) 0 0.00 0.00 1,5 ml/min *DN = 0.00 4,8 ml/min *DN = 0.00

Allowable leak (Pa*m3/s) : Class A = 1.78 E -8 x stem diam (mm), Class B = 1.78 E -7 x stem diam (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

End flange (Ref. only)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Sealant Inj. Ports / Drains / Vents

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Soft seated (ISO 5208, Rate A)

Metal seated (ISO 5208, Rate B: 0,018 ml/min *DN)

Metal seated (ISO 5208, Rate C: 0,18 ml/min *DN)

Page 36: Mesc Proxy Serv Let

15.Uni-dir.(NON-OP)-50°C≤80°C

Page 36 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

15. Uni-directional (on/off) valve from –50 °C to ≤ +80 °C without extended bonnet (non-

operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and Low

Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

NOTES

CALCULATION METHODSTorque Values: Calculation @ 2bar Experience @ 2 bar Calculation @ 100% DP Experience @ 100% DP COMMENTSDesign opearting torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Test operating torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Actuator type:Packing bolt torqueOthersOthers

EQUIPMENT USEDHelium Mass SpectrometerPressure console; Digital Pressure Gauge Pressure gauge ManometerFlow-meter: Flow-meter: Torque meter: serial number Torque tool model Thermocouple (Stem Packing)Thermocouple (Ambient)Thermocouple (Internal Body)Thermocouple (External Body)OthersOthersOthers

FOR METAL SEATED BUTTERFLY VALVES IN PRESSURE CLASSES 900# AND ABOVE IT MIGHT BE BENEFICIAL FOR THE VALVE MANUFACTURER TO DETERMINE SEATLEAKAGE RATES IN THE NON-PREFERRED DIRECTION.

Page 37: Mesc Proxy Serv Let

15.Uni-dir.(NON-OP)-50°C≤80°C

Page 37 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

15. Uni-directional (on/off) valve from –50 °C to ≤ +80 °C without extended bonnet (non-

operable valve):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and Low

Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

Sequence 15. Typical pressure / temperature / mechanical cycling for uni-directional (on/off) valves from –50 °C to ≤ +80 °C without extended bonnet (non-operable valve).

X = No test S = Seat test B = Body and fugitive emission test T = Torque test Indicated numbers above X, S, B and/or T are the amount of mechanical cycles to be performed.

Page 38: Mesc Proxy Serv Let

16.Uni-dir.(OP)<-20>80°C≤200°C

Page 38 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

PRE TESTING CHECK LISTSPE 77/300 (CMT / MESC ver. 13.0)SPE 77/300A, SPE 77/300B, SPE 77/300D (all CMT / MESC ver. 13.0)

ConfirmDoes the test rig conform to C.2 of SPE 77/300 and figures C.1a, C.1b, C.1c? YES / NO

YES / NO

Is the tank and valve strong enough to withstand all forces exerted during the handling of the valve ? YES / NOIs the purity of the Helium equal to or higher than 97%? YES / NOIs the test rig suitable for testing the valve in both directions ? YES / NOAre the test rig valve end connectors provided with a pressure vent connection and a suitable thermocouple connection ? YES / NO

TEST VALVE

Is the test valve in accordance with the general arrangement drawing? YES / NOIs there a bill of material and does it indicate for every material the max. and min. temperature, hardness values and the origin of the industry standards? YES / NOHas a MESC buying description or valve DATA sheet been produced for the test valve? YES / NOHas test valve assembly been witnessed by Shell-GSI or its representative? YES / NOHas a HSE plan been produced for all testing work to be carried out? YES / NOAre test valve internals dry and thoroughly cleaned and degreased,dust and oil free? YES / NOHave pre-condition photographs been taken prior to valve assembly? YES / NOHas the valve passed the normal production tests in accordance with the manufacturers testing procedures? YES / NO

Ensure the test pressure to be applied falls between 20% and 80% of the pressure gauges full scale. YES / NOWhich device is to be used to measure leakage through the test valve ? SPECIFY

YES / NO

TAT @ AMBIENT TEMP. (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.1 10.0 Run-in Time to cycle Mech. Cycle

SPE 77/300

C.4.2.1

2 2 Seat A 5 C.4.2.2

3a 3.5 Seat A 1

C.4.2.3b 7.0 Seat A 1

c 11.0 Seat A 1

4 11.0C.4.2.4

5 10.0 25 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

6 10.0 Seat A 1

16. Uni-directional (on/off) valves from < –20 °C to > +80 °C and ≤ +200 °C with extended

bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low / Cryogenic Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

APPLICABLE DOCUMENTS

TEST RIG CONNECTION &

SUPPORTS

For prototype- and production leak (pneumatic and FE) testing, do the testing operators have the NDT method leak testing levels LT1, LT2 or LT3, qualification/competences in accordance with BS-EN 473 (2008) and/or ISO 9712 (2005) + CORR.1 (2005) and/or ASNT SNT-TC-1A (2006)?

TEST EQUIPMENT Do all test/measuring equipment and instruments have a system calibration certificate, traceable to (inter)national standards, to guarantee accuracy and have a valid calibration date not exceeding 3 (per ISO 15848) months

for the mass spectrometer and 12 months for other equipment, prior to any test?

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torques (BTO and ETC) at 1st cycle

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2)

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. (+soapy water test on castings)

Continious formation of bubbles? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.2.5+ C.4.2.2

Page 39: Mesc Proxy Serv Let

16.Uni-dir.(OP)<-20>80°C≤200°C

Page 39 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

16. Uni-directional (on/off) valves from < –20 °C to > +80 °C and ≤ +200 °C with extended

bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low / Cryogenic Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

FUGITIVE EMISSION TEST RESULTS @ AMBIENT TEMP. (HELIUM) per Shell MESC description:

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Warming up procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

Page 40: Mesc Proxy Serv Let

16.Uni-dir.(OP)<-20>80°C≤200°C

Page 40 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

16. Uni-directional (on/off) valves from < –20 °C to > +80 °C and ≤ +200 °C with extended

bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low / Cryogenic Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

TAT @ MAXIMUM ELEVATED TEMP. (NITROGEN 100%) per Shell MESC description: Test Temp: °C. Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

7 2 Seat A 5

SPE 77/300

8a 0.0 Seat A 1

b 0.0 Seat A 1

c 0.0 Seat A 1

9 0.0

10 26 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

11 0.0 Seat A 1

Test Temp: 0 °C.

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Cooling Down procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torques (BTO and ETC) at 1st cycle

C.4.4 +C.4.2.2

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2)C.4.4 +C.4.2.3

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.4 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.4 +C.4.2.5

FUGITIVE EMISSION TEST RESULTS @ MAXIMUM ELEVATED TEMP. (NITROGEN 100%) per Shell MESC description:

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

Page 41: Mesc Proxy Serv Let

16.Uni-dir.(OP)<-20>80°C≤200°C

Page 41 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

16. Uni-directional (on/off) valves from < –20 °C to > +80 °C and ≤ +200 °C with extended

bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low / Cryogenic Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

TAT @ LOW TEMP (NITROGEN) per Shell MESC description: Test Temp: °C Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

12 2 Seat A 5

SPE 77/300

13a 3.5 Seat A 1b 7.0 Seat A 1c 11.0 Seat A 1

14 11.0

15 10.0 25 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

16 10.0 Seat A 1

FUGITIVE EMISSION TEST RESULTS @ LOW TEMP (HELIUM) per Shell MESC description: Test Temp: 0 °C

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Warming up procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C) +torques (BTO and ETC) at 1st cycle

C.4.6.1 +C.4.2.2

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C)C.4.6.2 +C.4.2.3

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.6.3 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C) +torque (BTO and ETC)

C.4.6.4+C.4.2.5

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

Page 42: Mesc Proxy Serv Let

16.Uni-dir.(OP)<-20>80°C≤200°C

Page 42 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

16. Uni-directional (on/off) valves from < –20 °C to > +80 °C and ≤ +200 °C with extended

bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low / Cryogenic Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

TAT; LOW & HIGH PRESSURE SEAT TEST @ AMBIENT TEMP (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

17 2 Seat A seat leakage (N2)

SPE 77/300

C.4.7

18 2 Seat A seat leakage (N2) C.4.7

19 10.0 Seat A 1

STRIPDOWN TEST (MESC SPE 77/300 Section C.4.8)

Part Mat. Ht. No's. & Markings Record Observations Regarding Condition of Parts

BODY BONNET / COVERCLOSURE ACLOSURE BOBTURATORSTEMSEAT RING ASEAT RING BSEAT INSERT ASEAT INSERT BBONNET EXTENSIONSTEM EXTENSIONGLANDGLAND BUSHGLAND FLANGELIP-SEALSPACKING TOP / BOTTOMPACKING INTERMEDIATERTJ GASKETFS GASKETBOLTSNUTSSEALSOthersOthersOthersOthersOthersOthers

MAXIMUM ALLOWABLE FUGITIVE EMISSION LEAKAGE RATES (MESC SPE 77/300 Section C.4.11, tables C.7 + C.8 + C.9)Stem / ID Packing Enter Dimensions

belowDiam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Diam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.7.6 +C.4.2.5

Item (GA dwg)

Mat. Conform Certs. (+Heat- and cert. No's.)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -8 x stem diam (mm), Class B = 1.78 E -7 x stem diam (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

End flange (Ref. only)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Page 43: Mesc Proxy Serv Let

16.Uni-dir.(OP)<-20>80°C≤200°C

Page 43 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

16. Uni-directional (on/off) valves from < –20 °C to > +80 °C and ≤ +200 °C with extended

bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low / Cryogenic Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

Gland / OD Packing

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Body / Bonnet or Cover

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Body Joints / Closures

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

MAXIMUM ALLOWABLE SEAT LEAKAGE RATES (MESC SPE 77/300 Section C.4.10, tables C.5 and C.6)Type Acceptance Test Low, Ambient & Elevated Temp (≥ -20 °C, in ml/min) Low Temp or Cryogenic Temp (< -20 °C, in ml/min)

Soft seated Metal seated

DN (mm) 0 0.00 0.00 1,5 ml/min *DN = 0.00 4,8 ml/min *DN = 0.00

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Sealant Inj. Ports / Drains / Vents

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Soft seated (ISO 5208, Rate A)

Metal seated (ISO 5208, Rate B: 0,018 ml/min *DN)

Metal seated (ISO 5208, Rate C: 0,18 ml/min *DN)

Page 44: Mesc Proxy Serv Let

16.Uni-dir.(OP)<-20>80°C≤200°C

Page 44 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

16. Uni-directional (on/off) valves from < –20 °C to > +80 °C and ≤ +200 °C with extended

bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low / Cryogenic Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

NOTES

CALCULATION METHODSTorque Values: Calculation @ 2bar Experience @ 2 bar Calculation @ 100% DP Experience @ 100% DP COMMENTSDesign opearting torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Test operating torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Actuator type:Packing bolt torqueOthersOthers

EQUIPMENT USEDHelium Mass SpectrometerPressure console; Digital Pressure Gauge Pressure gauge ManometerFlow-meter: Flow-meter: Torque meter: serial number Torque tool model Thermocouple (Stem Packing)Thermocouple (Ambient)Thermocouple (Internal Body)Thermocouple (External Body)OthersOthersOthers

FOR METAL SEATED BUTTERFLY VALVES IN PRESSURE CLASSES 900# AND ABOVE IT MIGHT BE BENEFICIAL FOR THE VALVE MANUFACTURER TO DETERMINE SEATLEAKAGE RATES IN THE NON-PREFERRED DIRECTION.

Page 45: Mesc Proxy Serv Let

16.Uni-dir.(OP)<-20>80°C≤200°C

Page 45 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

16. Uni-directional (on/off) valves from < –20 °C to > +80 °C and ≤ +200 °C with extended

bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low / Cryogenic Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

Sequence 16. Typical pressure / temperature / mechanical cycling for uni-directional (on/off) valves from < –20 °C to > +80 °C and ≤ +200 °C with extended bonnet.

X = No test S = Seat test B = Body and fugitive emission test T = Torque test Indicated numbers above X, S, B and/or T are the amount of mechanical cycles to be performed.

Page 46: Mesc Proxy Serv Let

17.Uni-dir.(OP)<-20°C≤80°C

Page 46 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

PRE TESTING CHECK LISTSPE 77/300 (CMT / MESC ver. 13.0)SPE 77/300A, SPE 77/300B, SPE 77/300D (all CMT / MESC ver. 13.0)

ConfirmDoes the test rig conform to C.2 of SPE 77/300 and figures C.1a, C.1b, C.1c? YES / NO

YES / NO

Is the tank and valve strong enough to withstand all forces exerted during the handling of the valve ? YES / NOIs the purity of the Helium equal to or higher than 97%? YES / NOIs the test rig suitable for testing the valve in both directions ? YES / NOAre the test rig valve end connectors provided with a pressure vent connection and a suitable thermocouple connection ? YES / NO

TEST VALVE

Is the test valve in accordance with the general arrangement drawing? YES / NOIs there a bill of material and does it indicate for every material the max. and min. temperature, hardness values and the origin of the industry standards? YES / NOHas a MESC buying description or valve DATA sheet been produced for the test valve? YES / NOHas test valve assembly been witnessed by Shell-GSI or its representative? YES / NOHas a HSE plan been produced for all testing work to be carried out? YES / NOAre test valve internals dry and thoroughly cleaned and degreased,dust and oil free? YES / NOHave pre-condition photographs been taken prior to valve assembly? YES / NOHas the valve passed the normal production tests in accordance with the manufacturers testing procedures? YES / NO

Ensure the test pressure to be applied falls between 20% and 80% of the pressure gauges full scale. YES / NOWhich device is to be used to measure leakage through the test valve ? SPECIFY

YES / NO

TAT @ AMBIENT TEMP. (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.1 0.0 Run-in Time to cycle Mech. Cycle

SPE 77/300

C.4.2.1

2 2 Seat A 5 C.4.2.2

3a 0.0 Seat A 1

C.4.2.3b 0.0 Seat A 1

c 0.0 Seat A 1

4 0.0C.4.2.4

5 42 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

6 0.0 Seat A 1

17. Uni-directional (on/off) valves from < –20 °C to ≤ +80 °C with extended bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Low / Cryogenic Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

APPLICABLE DOCUMENTS

TEST RIG CONNECTION &

SUPPORTS

For prototype- and production leak (pneumatic and FE) testing, do the testing operators have the NDT method leak testing levels LT1, LT2 or LT3, qualification/competences in accordance with BS-EN 473 (2008) and/or ISO 9712 (2005) + CORR.1 (2005) and/or ASNT SNT-TC-1A (2006)?

TEST EQUIPMENT Do all test/measuring equipment and instruments have a system calibration certificate, traceable to (inter)national standards, to guarantee accuracy and have a valid calibration date not exceeding 3 (per ISO 15848) months

for the mass spectrometer and 12 months for other equipment, prior to any test?

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torques (BTO and ETC) at 1st cycle

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2)

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. (+soapy water test on castings)

Continious formation of bubbles? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.2.5+ C.4.2.2

Page 47: Mesc Proxy Serv Let

17.Uni-dir.(OP)<-20°C≤80°C

Page 47 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

17. Uni-directional (on/off) valves from < –20 °C to ≤ +80 °C with extended bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Low / Cryogenic Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

FUGITIVE EMISSION TEST RESULTS @ AMBIENT TEMP. (HELIUM) per Shell MESC description:

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Cooling Down procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

Page 48: Mesc Proxy Serv Let

17.Uni-dir.(OP)<-20°C≤80°C

Page 48 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

17. Uni-directional (on/off) valves from < –20 °C to ≤ +80 °C with extended bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Low / Cryogenic Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

TAT @ LOW TEMP (NITROGEN) per Shell MESC description: Test Temp: °C Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

7 2 Seat A 5

SPE 77/300

8a 0.0 Seat A 1b 0.0 Seat A 1c 0.0 Seat A 1

9 0.0

10 0.0 42 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

11 0.0 Seat A 1

FUGITIVE EMISSION TEST RESULTS @ LOW TEMP (HELIUM) per Shell MESC description: Test Temp: 0 °C

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Warming up procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C) +torques (BTO and ETC) at 1st cycle

C.4.6.1 +C.4.2.2

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C)C.4.6.2 +C.4.2.3

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.6.3 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C) +torque (BTO and ETC)

C.4.6.4+C.4.2.5

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

Page 49: Mesc Proxy Serv Let

17.Uni-dir.(OP)<-20°C≤80°C

Page 49 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

17. Uni-directional (on/off) valves from < –20 °C to ≤ +80 °C with extended bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Low / Cryogenic Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

TAT; LOW & HIGH PRESSURE SEAT TEST @ AMBIENT TEMP (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

12 2 Seat A seat leakage (N2)

SPE 77/300

C.4.7

13 7 Seat A seat leakage (N2) C.4.7

14 0.0 Seat A 1

STRIPDOWN TEST (MESC SPE 77/300 Section C.4.8)

Part Mat. Ht. No's. & Markings Record Observations Regarding Condition of Parts

BODY BONNET / COVERCLOSURE ACLOSURE BOBTURATORSTEMSEAT RING ASEAT RING BSEAT INSERT ASEAT INSERT BBONNET EXTENSIONSTEM EXTENSIONGLANDGLAND BUSHGLAND FLANGELIP-SEALSPACKING TOP / BOTTOMPACKING INTERMEDIATERTJ GASKETFS GASKETBOLTSNUTSSEALSOthersOthersOthersOthersOthersOthers

MAXIMUM ALLOWABLE FUGITIVE EMISSION LEAKAGE RATES (MESC SPE 77/300 Section C.4.11, tables C.7 + C.8 + C.9)Stem / ID Packing Enter Dimensions

belowDiam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Diam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.7.6 +C.4.2.5

Item (GA dwg)

Mat. Conform Certs. (+Heat- and cert. No's.)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -8 x stem diam (mm), Class B = 1.78 E -7 x stem diam (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

End flange (Ref. only)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Page 50: Mesc Proxy Serv Let

17.Uni-dir.(OP)<-20°C≤80°C

Page 50 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

17. Uni-directional (on/off) valves from < –20 °C to ≤ +80 °C with extended bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Low / Cryogenic Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

Gland / OD Packing

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Body / Bonnet or Cover

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Body Joints / Closures

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

MAXIMUM ALLOWABLE SEAT LEAKAGE RATES (MESC SPE 77/300 Section C.4.10, tables C.5 and C.6)Type Acceptance Test Low, Ambient & Elevated Temp (≥ -20 °C, in ml/min) Low Temp or Cryogenic Temp (< -20 °C, in ml/min)

Soft seated Metal seated

DN (mm) 0 0.00 0.00 1,5 ml/min *DN = 0.00 4,8 ml/min *DN = 0.00

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Sealant Inj. Ports / Drains / Vents

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Soft seated (ISO 5208, Rate A)

Metal seated (ISO 5208, Rate B: 0,018 ml/min *DN)

Metal seated (ISO 5208, Rate C: 0,18 ml/min *DN)

Page 51: Mesc Proxy Serv Let

17.Uni-dir.(OP)<-20°C≤80°C

Page 51 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

17. Uni-directional (on/off) valves from < –20 °C to ≤ +80 °C with extended bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Low / Cryogenic Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

NOTES

CALCULATION METHODSTorque Values: Calculation @ 2bar Experience @ 2 bar Calculation @ 100% DP Experience @ 100% DP COMMENTSDesign opearting torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Test operating torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Actuator type:Packing bolt torqueOthersOthers

EQUIPMENT USEDHelium Mass SpectrometerPressure console; Digital Pressure Gauge Pressure gauge ManometerFlow-meter: Flow-meter: Torque meter: serial number Torque tool model Thermocouple (Stem Packing)Thermocouple (Ambient)Thermocouple (Internal Body)Thermocouple (External Body)OthersOthersOthers

FOR METAL SEATED BUTTERFLY VALVES IN PRESSURE CLASSES 900# AND ABOVE IT MIGHT BE BENEFICIAL FOR THE VALVE MANUFACTURER TO DETERMINE SEATLEAKAGE RATES IN THE NON-PREFERRED DIRECTION.

Page 52: Mesc Proxy Serv Let

17.Uni-dir.(OP)<-20°C≤80°C

Page 52 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

17. Uni-directional (on/off) valves from < –20 °C to ≤ +80 °C with extended bonnet:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Low / Cryogenic Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

Sequence 17. Typical pressure / temperature / mechanical cycling for uni-directional (on/off) valves from < –20 °C to ≤ +80 °C with extended bonnet.

X = No test S = Seat test B = Body and fugitive emission test T = Torque test Indicated numbers above X, S, B and/or T are the amount of mechanical cycles to be performed.

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18.Uni-dir.≥-20°C>+200°C

Page 53 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

PRE TESTING CHECK LISTSPE 77/300 (CMT / MESC ver. 13.0)SPE 77/300A, SPE 77/300B, SPE 77/300D (all CMT / MESC ver. 13.0)

ConfirmDoes the test rig conform to C.2 of SPE 77/300 and figures C.1a, C.1b, C.1c? YES / NO

YES / NO

Is the tank and valve strong enough to withstand all forces exerted during the handling of the valve ? YES / NOIs the purity of the Helium equal to or higher than 97%? YES / NOIs the test rig suitable for testing the valve in both directions ? YES / NOAre the test rig valve end connectors provided with a pressure vent connection and a suitable thermocouple connection ? YES / NO

TEST VALVE

Is the test valve in accordance with the general arrangement drawing? YES / NOIs there a bill of material and does it indicate for every material the max. and min. temperature, hardness values and the origin of the industry standards? YES / NOHas a MESC buying description or valve DATA sheet been produced for the test valve? YES / NOHas test valve assembly been witnessed by Shell-GSI or its representative? YES / NOHas a HSE plan been produced for all testing work to be carried out? YES / NOAre test valve internals dry and thoroughly cleaned and degreased,dust and oil free? YES / NOHave pre-condition photographs been taken prior to valve assembly? YES / NOHas the valve passed the normal production tests in accordance with the manufacturers testing procedures? YES / NO

Ensure the test pressure to be applied falls between 20% and 80% of the pressure gauges full scale. YES / NOWhich device is to be used to measure leakage through the test valve ? SPECIFY

YES / NO

TAT @ AMBIENT TEMP. (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.1 0.0 Run-in Time to cycle Mech. Cycle

SPE 77/300

C.4.2.1

2 2 Seat A 5 C.4.2.2

3a 0.0 Seat A 1

C.4.2.3b 0.0 Seat A 1

c 0.0 Seat A 1

4 0.0C.4.2.4

5 17 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

6 0.0 Seat A 1

18. Uni-directional (on/off) valves from ≥ –20 °C to > +200 °C:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Elevated Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

APPLICABLE DOCUMENTS

TEST RIG CONNECTION &

SUPPORTS

For prototype- and production leak (pneumatic and FE) testing, do the testing operators have the NDT method leak testing levels LT1, LT2 or LT3, qualification/competences in accordance with BS-EN 473 (2008) and/or ISO 9712 (2005) + CORR.1 (2005) and/or ASNT SNT-TC-1A (2006)?

TEST EQUIPMENT Do all test/measuring equipment and instruments have a system calibration certificate, traceable to (inter)national standards, to guarantee accuracy and have a valid calibration date not exceeding 3 (per ISO 15848) months

for the mass spectrometer and 12 months for other equipment, prior to any test?

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torques (BTO and ETC) at 1st cycle

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2)

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. (+soapy water test on castings)

Continious formation of bubbles? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.2.5+ C.4.2.2

Page 54: Mesc Proxy Serv Let

18.Uni-dir.≥-20°C>+200°C

Page 54 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

18. Uni-directional (on/off) valves from ≥ –20 °C to > +200 °C:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Elevated Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

FUGITIVE EMISSION TEST RESULTS @ AMBIENT TEMP. (HELIUM) per Shell MESC description:

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Warming up procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

TAT @ ELEVATED TEMP. (+200 °C.) ( HELIUM) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

7 0.0SPE 77/300

8 25 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.4 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Mech. Cycle + FE

Page 55: Mesc Proxy Serv Let

18.Uni-dir.≥-20°C>+200°C

Page 55 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

18. Uni-directional (on/off) valves from ≥ –20 °C to > +200 °C:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Elevated Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

FUGITIVE EMISSION TEST RESULTS @ ELEVATED TEMP. (+200 °C.) (HELIUM) per Shell MESC description:

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Warming up procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

TAT @ MAXIMUM ELEVATED TEMP. (NITROGEN 100%) per Shell MESC description: Test Temp: °C. Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

9 2 Seat A 5

SPE 77/300

10a 0.0 Seat A 1

b 0.0 Seat A 1

c 0.0 Seat A 1

11 0.0

12 17 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

13 0.0 Seat A 1

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torques (BTO and ETC) at 1st cycle

C.4.4 +C.4.2.2

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2)C.4.4 +C.4.2.3

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.4 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.4 +C.4.2.5

Page 56: Mesc Proxy Serv Let

18.Uni-dir.≥-20°C>+200°C

Page 56 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

18. Uni-directional (on/off) valves from ≥ –20 °C to > +200 °C:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Elevated Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

Test Temp: 0 °C.

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Cooling Down procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

TAT; LOW & HIGH PRESSURE SEAT TEST @ AMBIENT TEMP (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

14 2 Seat A seat leakage (N2)

SPE 77/300

C.4.7

15 7 Seat A seat leakage (N2) C.4.7

16 0.0C.4.2.4

17 0.0 25 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

18 0.0 Seat A 1

FUGITIVE EMISSION TEST RESULTS @ MAXIMUM ELEVATED TEMP. (NITROGEN 100%) per Shell MESC description:

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. (+soapy water test on castings)

Continious formation of bubbles? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.7.6 +C.4.2.5

Page 57: Mesc Proxy Serv Let

18.Uni-dir.≥-20°C>+200°C

Page 57 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

18. Uni-directional (on/off) valves from ≥ –20 °C to > +200 °C:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Elevated Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

FUGITIVE EMISSION TEST RESULTS @ AMBIENT TEMP. (HELIUM) per Shell MESC description:

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

STRIPDOWN TEST (MESC SPE 77/300 Section C.4.8)

Part Mat. Ht. No's. & Markings Record Observations Regarding Condition of Parts

BODY BONNET / COVERCLOSURE ACLOSURE BOBTURATORSTEMSEAT RING ASEAT RING BSEAT INSERT ASEAT INSERT BBONNET EXTENSIONSTEM EXTENSIONGLANDGLAND BUSHGLAND FLANGELIP-SEALSPACKING TOP / BOTTOMPACKING INTERMEDIATERTJ GASKETFS GASKETBOLTSNUTSSEALSOthersOthersOthersOthersOthersOthers

MAXIMUM ALLOWABLE FUGITIVE EMISSION LEAKAGE RATES (MESC SPE 77/300 Section C.4.11, tables C.7 + C.8 + C.9)Stem / ID Packing Enter Dimensions

belowDiam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Diam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Item (GA dwg)

Mat. Conform Certs. (+Heat- and cert. No's.)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -8 x stem diam (mm), Class B = 1.78 E -7 x stem diam (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Page 58: Mesc Proxy Serv Let

18.Uni-dir.≥-20°C>+200°C

Page 58 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

18. Uni-directional (on/off) valves from ≥ –20 °C to > +200 °C:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Elevated Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Gland / OD Packing

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Body / Bonnet or Cover

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Body Joints / Closures

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

MAXIMUM ALLOWABLE SEAT LEAKAGE RATES (MESC SPE 77/300 Section C.4.10, tables C.5 and C.6)Type Acceptance Test Low, Ambient & Elevated Temp (≥ -20 °C, in ml/min) Low Temp or Cryogenic Temp (< -20 °C, in ml/min)

Soft seated Metal seated

DN (mm) 0 0.00 0.00 1,5 ml/min *DN = 0.00 4,8 ml/min *DN = 0.00

End flange (Ref. only)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Sealant Inj. Ports / Drains / Vents

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Soft seated (ISO 5208, Rate A)

Metal seated (ISO 5208, Rate B: 0,018 ml/min *DN)

Metal seated (ISO 5208, Rate C: 0,18 ml/min *DN)

Page 59: Mesc Proxy Serv Let

18.Uni-dir.≥-20°C>+200°C

Page 59 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

18. Uni-directional (on/off) valves from ≥ –20 °C to > +200 °C:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Elevated Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

NOTES

CALCULATION METHODSTorque Values: Calculation @ 2bar Experience @ 2 bar Calculation @ 100% DP Experience @ 100% DP COMMENTSDesign opearting torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Test operating torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Actuator type:Packing bolt torqueOthersOthers

EQUIPMENT USEDHelium Mass SpectrometerPressure console; Digital Pressure Gauge Pressure gauge ManometerFlow-meter: Flow-meter: Torque meter: serial number Torque tool model Thermocouple (Stem Packing)Thermocouple (Ambient)Thermocouple (Internal Body)Thermocouple (External Body)OthersOthersOthers

FOR METAL SEATED BUTTERFLY VALVES IN PRESSURE CLASSES 900# AND ABOVE IT MIGHT BE BENEFICIAL FOR THE VALVE MANUFACTURER TO DETERMINE SEATLEAKAGE RATES IN THE NON-PREFERRED DIRECTION.

Page 60: Mesc Proxy Serv Let

18.Uni-dir.≥-20°C>+200°C

Page 60 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

18. Uni-directional (on/off) valves from ≥ –20 °C to > +200 °C:

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Elevated Temperature.NOTE: ALL WHITE CELLS TO BE

COMPLETED BY THE VALVE MANUFACTURERDesign Temp. Range (°C):

Sequence 18. Typical pressure / temperature / mechanical cycling for uni-directional (on/off) valves from ≥ –20 °C to > +200 °C.

X = No test S = Seat test B = Body and fugitive emission test T = Torque test Indicated numbers above X, S, B and/or T are the amount of mechanical cycles to be performed.

Page 61: Mesc Proxy Serv Let

19.Uni-dir.≥-20<0°C>80°C≤200°C

Page 61 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

PRE TESTING CHECK LISTSPE 77/300 (CMT / MESC ver. 13.0)SPE 77/300A, SPE 77/300B, SPE 77/300D (all CMT / MESC ver. 13.0)

ConfirmDoes the test rig conform to C.2 of SPE 77/300 and figures C.1a, C.1b, C.1c? YES / NO

YES / NO

Is the tank and valve strong enough to withstand all forces exerted during the handling of the valve ? YES / NOIs the purity of the Helium equal to or higher than 97%? YES / NOIs the test rig suitable for testing the valve in both directions ? YES / NOAre the test rig valve end connectors provided with a pressure vent connection and a suitable thermocouple connection ? YES / NO

TEST VALVE

Is the test valve in accordance with the general arrangement drawing? YES / NOIs there a bill of material and does it indicate for every material the max. and min. temperature, hardness values and the origin of the industry standards? YES / NOHas a MESC buying description or valve DATA sheet been produced for the test valve? YES / NOHas test valve assembly been witnessed by Shell-GSI or its representative? YES / NOHas a HSE plan been produced for all testing work to be carried out? YES / NOAre test valve internals dry and thoroughly cleaned and degreased,dust and oil free? YES / NOHave pre-condition photographs been taken prior to valve assembly? YES / NOHas the valve passed the normal production tests in accordance with the manufacturers testing procedures? YES / NO

Ensure the test pressure to be applied falls between 20% and 80% of the pressure gauges full scale. YES / NOWhich device is to be used to measure leakage through the test valve ? SPECIFY

YES / NO

TAT @ AMBIENT TEMP. (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.1 0.0 Run-in Time to cycle Mech. Cycle

SPE 77/300

C.4.2.1

2 2 Seat A 5 C.4.2.2

3a 0.0 Seat A 1

C.4.2.3b 0.0 Seat A 1

c 0.0 Seat A 1

4 0.0C.4.2.4

5 25 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

6 0.0 Seat A 1

19. Uni-directional (on/off) valves from ≥ –20 °C and < 0 °C to > +80 °C and ≤ +200 °C (including elastomeric / rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

APPLICABLE DOCUMENTS

TEST RIG CONNECTION &

SUPPORTS

For prototype- and production leak (pneumatic and FE) testing, do the testing operators have the NDT method leak testing levels LT1, LT2 or LT3, qualification/competences in accordance with BS-EN 473 (2008) and/or ISO 9712 (2005) + CORR.1 (2005) and/or ASNT SNT-TC-1A (2006)?

TEST EQUIPMENT Do all test/measuring equipment and instruments have a system calibration certificate, traceable to (inter)national standards, to guarantee accuracy and have a valid calibration date not exceeding 3 (per ISO 15848) months

for the mass spectrometer and 12 months for other equipment, prior to any test?

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torques (BTO and ETC) at 1st cycle

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2)

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. (+soapy water test on castings)

Continious formation of bubbles? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.2.5+ C.4.2.2

Page 62: Mesc Proxy Serv Let

19.Uni-dir.≥-20<0°C>80°C≤200°C

Page 62 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

19. Uni-directional (on/off) valves from ≥ –20 °C and < 0 °C to > +80 °C and ≤ +200 °C (including elastomeric / rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

FUGITIVE EMISSION TEST RESULTS @ AMBIENT TEMP. (HELIUM) per Shell MESC description:

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Warming up procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

TAT @ MAXIMUM ELEVATED TEMP. (NITROGEN 100%) per Shell MESC description: Test Temp: °C. Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

7 2 Seat A 5

SPE 77/300

8a 0.0 Seat A 1

b 0.0 Seat A 1

c 0.0 Seat A 1

9 0.0

10 26 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

11 0.0 Seat A 1

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torques (BTO and ETC) at 1st cycle

C.4.4 +C.4.2.2

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2)C.4.4 +C.4.2.3

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.4 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.4 +C.4.2.5

Page 63: Mesc Proxy Serv Let

19.Uni-dir.≥-20<0°C>80°C≤200°C

Page 63 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

19. Uni-directional (on/off) valves from ≥ –20 °C and < 0 °C to > +80 °C and ≤ +200 °C (including elastomeric / rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

Test Temp: 0 °C.

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Cooling Down procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

TAT @ LOW TEMP (NITROGEN) per Shell MESC description: Test Temp: °C Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

12 2 Seat A 5

SPE 77/300

13a 0.0 Seat A 1b 0.0 Seat A 1c 0.0 Seat A 1

14 0.0

15 0.0 25 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

16 0.0 Seat A 1

FUGITIVE EMISSION TEST RESULTS @ MAXIMUM ELEVATED TEMP. (NITROGEN 100%) per Shell MESC description:

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C) +torques (BTO and ETC) at 1st cycle

C.4.6.1 +C.4.2.2

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C)C.4.6.2 +C.4.2.3

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.6.3 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C) +torque (BTO and ETC)

C.4.6.4+C.4.2.5

Page 64: Mesc Proxy Serv Let

19.Uni-dir.≥-20<0°C>80°C≤200°C

Page 64 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

19. Uni-directional (on/off) valves from ≥ –20 °C and < 0 °C to > +80 °C and ≤ +200 °C (including elastomeric / rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

FUGITIVE EMISSION TEST RESULTS @ LOW TEMP (HELIUM) per Shell MESC description: Test Temp: 0 °C

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Warming up procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

TAT; LOW & HIGH PRESSURE SEAT TEST @ AMBIENT TEMP (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

17 2 Seat A seat leakage (N2)

SPE 77/300

C.4.7

18 7 Seat A seat leakage (N2) C.4.7

19 0.0 Seat A 1

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.7.6 +C.4.2.5

Page 65: Mesc Proxy Serv Let

19.Uni-dir.≥-20<0°C>80°C≤200°C

Page 65 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

19. Uni-directional (on/off) valves from ≥ –20 °C and < 0 °C to > +80 °C and ≤ +200 °C (including elastomeric / rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

STRIPDOWN TEST (MESC SPE 77/300 Section C.4.8)

Part Mat. Ht. No's. & Markings Record Observations Regarding Condition of Parts

BODY BONNET / COVERCLOSURE ACLOSURE BOBTURATORSTEMSEAT RING ASEAT RING BSEAT INSERT ASEAT INSERT BBONNET EXTENSIONSTEM EXTENSIONGLANDGLAND BUSHGLAND FLANGELIP-SEALSPACKING TOP / BOTTOMPACKING INTERMEDIATERTJ GASKETFS GASKETBOLTSNUTSSEALSOthersOthersOthersOthersOthersOthers

MAXIMUM ALLOWABLE FUGITIVE EMISSION LEAKAGE RATES (MESC SPE 77/300 Section C.4.11, tables C.7 + C.8 + C.9)Stem / ID Packing Enter Dimensions

belowDiam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Diam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Gland / OD Packing

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Body / Bonnet or Cover

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Item (GA dwg)

Mat. Conform Certs. (+Heat- and cert. No's.)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -8 x stem diam (mm), Class B = 1.78 E -7 x stem diam (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

End flange (Ref. only)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Page 66: Mesc Proxy Serv Let

19.Uni-dir.≥-20<0°C>80°C≤200°C

Page 66 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

19. Uni-directional (on/off) valves from ≥ –20 °C and < 0 °C to > +80 °C and ≤ +200 °C (including elastomeric / rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

Body Joints / Closures

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

MAXIMUM ALLOWABLE SEAT LEAKAGE RATES (MESC SPE 77/300 Section C.4.10, tables C.5 and C.6)Type Acceptance Test Low, Ambient & Elevated Temp (≥ -20 °C, in ml/min) Low Temp or Cryogenic Temp (< -20 °C, in ml/min)

Soft seated Metal seated

DN (mm) 0 0.00 0.00 1,5 ml/min *DN = 0.00 4,8 ml/min *DN = 0.00

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Sealant Inj. Ports / Drains / Vents

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Soft seated (ISO 5208, Rate A)

Metal seated (ISO 5208, Rate B: 0,018 ml/min *DN)

Metal seated (ISO 5208, Rate C: 0,18 ml/min *DN)

Page 67: Mesc Proxy Serv Let

19.Uni-dir.≥-20<0°C>80°C≤200°C

Page 67 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

19. Uni-directional (on/off) valves from ≥ –20 °C and < 0 °C to > +80 °C and ≤ +200 °C (including elastomeric / rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

NOTES

CALCULATION METHODSTorque Values: Calculation @ 2bar Experience @ 2 bar Calculation @ 100% DP Experience @ 100% DP COMMENTSDesign opearting torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Test operating torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Actuator type:Packing bolt torqueOthersOthers

EQUIPMENT USEDHelium Mass SpectrometerPressure console; Digital Pressure Gauge Pressure gauge ManometerFlow-meter: Flow-meter: Torque meter: serial number Torque tool model Thermocouple (Stem Packing)Thermocouple (Ambient)Thermocouple (Internal Body)Thermocouple (External Body)OthersOthersOthers

FOR METAL SEATED BUTTERFLY VALVES IN PRESSURE CLASSES 900# AND ABOVE IT MIGHT BE BENEFICIAL FOR THE VALVE MANUFACTURER TO DETERMINE SEATLEAKAGE RATES IN THE NON-PREFERRED DIRECTION.

Page 68: Mesc Proxy Serv Let

19.Uni-dir.≥-20<0°C>80°C≤200°C

Page 68 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

19. Uni-directional (on/off) valves from ≥ –20 °C and < 0 °C to > +80 °C and ≤ +200 °C (including elastomeric / rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient, Elevated

and Low Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

Sequence 19. Typical pressure / temperature / mechanical cycling for uni-directional (on/off) valves from ≥ –20 °C and < 0 °C to > +80 °C and ≤ +200 °C (incl. soft/elastomeric seals/seats/components).

X = No test S = Seat test B = Body and fugitive emission test T = Torque test Indicated numbers above X, S, B and/or T are the amount of mechanical cycles to be performed.

Page 69: Mesc Proxy Serv Let

20.Uni-dir≥-20>80≤+200°C nosoft

Page 69 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

PRE TESTING CHECK LISTSPE 77/300 (CMT / MESC ver. 13.0)SPE 77/300A, SPE 77/300B, SPE 77/300D (all CMT / MESC ver. 13.0)

ConfirmDoes the test rig conform to C.2 of SPE 77/300 and figures C.1a, C.1b, C.1c? YES / NO

YES / NO

Is the tank and valve strong enough to withstand all forces exerted during the handling of the valve ? YES / NOIs the purity of the Helium equal to or higher than 97%? YES / NOIs the test rig suitable for testing the valve in both directions ? YES / NOAre the test rig valve end connectors provided with a pressure vent connection and a suitable thermocouple connection ? YES / NO

TEST VALVE

Is the test valve in accordance with the general arrangement drawing? YES / NOIs there a bill of material and does it indicate for every material the max. and min. temperature, hardness values and the origin of the industry standards? YES / NOHas a MESC buying description or valve DATA sheet been produced for the test valve? YES / NOHas test valve assembly been witnessed by Shell-GSI or its representative? YES / NOHas a HSE plan been produced for all testing work to be carried out? YES / NOAre test valve internals dry and thoroughly cleaned and degreased,dust and oil free? YES / NOHave pre-condition photographs been taken prior to valve assembly? YES / NOHas the valve passed the normal production tests in accordance with the manufacturers testing procedures? YES / NO

Ensure the test pressure to be applied falls between 20% and 80% of the pressure gauges full scale. YES / NOWhich device is to be used to measure leakage through the test valve ? SPECIFY

YES / NO

TAT @ AMBIENT TEMP. (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.1 0.0 Run-in Time to cycle Mech. Cycle

SPE 77/300

C.4.2.1

2 2 Seat A 5 C.4.2.2

3a 0.0 Seat A 1

C.4.2.3b 0.0 Seat A 1

c 0.0 Seat A 1

4 0.0C.4.2.4

5 25 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

6 0.0 Seat A 1

20. Uni-directional (on/off) valves from ≥ –20 °C to > +80 °C and ≤ +200 °C (without

elastomeric / rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Elevated Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

APPLICABLE DOCUMENTS

TEST RIG CONNECTION &

SUPPORTS

For prototype- and production leak (pneumatic and FE) testing, do the testing operators have the NDT method leak testing levels LT1, LT2 or LT3, qualification/competences in accordance with BS-EN 473 (2008) and/or ISO 9712 (2005) + CORR.1 (2005) and/or ASNT SNT-TC-1A (2006)?

TEST EQUIPMENT Do all test/measuring equipment and instruments have a system calibration certificate, traceable to (inter)national standards, to guarantee accuracy and have a valid calibration date not exceeding 3 (per ISO 15848) months

for the mass spectrometer and 12 months for other equipment, prior to any test?

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torques (BTO and ETC) at 1st cycle

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2)

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. (+soapy water test on castings)

Continious formation of bubbles? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.2.5+ C.4.2.2

Page 70: Mesc Proxy Serv Let

20.Uni-dir≥-20>80≤+200°C nosoft

Page 70 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

20. Uni-directional (on/off) valves from ≥ –20 °C to > +80 °C and ≤ +200 °C (without

elastomeric / rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Elevated Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

FUGITIVE EMISSION TEST RESULTS @ AMBIENT TEMP. (HELIUM) per Shell MESC description:

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Warming up procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

TAT @ MAXIMUM ELEVATED TEMP. (NITROGEN 100%) per Shell MESC description: Test Temp: °C. Date: dd/mm/yyyy

Step Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

7 2 Seat A 5

SPE 77/300

8a 0.0 Seat A 1

b 0.0 Seat A 1

c 0.0 Seat A 1

9 0.0

10 26 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

11 0.0 Seat A 1

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.5.12 Table C.11

seat leakage (N2) +torques (BTO and ETC) at 1st cycle

C.5.4 +C.5.2.2

SPE 77/300 para C.5.12 Table C.11

seat leakage (N2)C.5.4 +C.5.2.3

Shell / Body Test

SPE 77/300 para C.5.12 Table C.10

body/shell leakage (He), no pressure drop. C.5.4 +

C.5.2.4

Visible leakage / pressure drop? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.5.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.5.4 +C.5.2.5

Page 71: Mesc Proxy Serv Let

20.Uni-dir≥-20>80≤+200°C nosoft

Page 71 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

20. Uni-directional (on/off) valves from ≥ –20 °C to > +80 °C and ≤ +200 °C (without

elastomeric / rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Elevated Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

Test Temp: 0 °C.

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Cooling Down procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

TAT; LOW & HIGH PRESSURE SEAT TEST @ AMBIENT TEMP (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyy

Step Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

12 2 Seat A seat leakage (N2)

SPE 77/300

C.4.7

13 7 Seat A seat leakage (N2) C.4.7

14 0.0C.4.2.4

15 0.0 33 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

16 0.0 Seat A 1

FUGITIVE EMISSION TEST RESULTS @ MAXIMUM ELEVATED TEMP. (NITROGEN 100%) per Shell MESC description:

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. (+soapy water test on castings)

Continious formation of bubbles? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.7.6 +C.4.2.5

Page 72: Mesc Proxy Serv Let

20.Uni-dir≥-20>80≤+200°C nosoft

Page 72 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

20. Uni-directional (on/off) valves from ≥ –20 °C to > +80 °C and ≤ +200 °C (without

elastomeric / rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Elevated Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

FUGITIVE EMISSION TEST RESULTS @ AMBIENT TEMP. (HELIUM) per Shell MESC description:

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

STRIPDOWN TEST (MESC SPE 77/300 Section C.4.8)

Part Mat. Ht. No's. & Markings Record Observations Regarding Condition of Parts

BODY BONNET / COVERCLOSURE ACLOSURE BOBTURATORSTEMSEAT RING ASEAT RING BSEAT INSERT ASEAT INSERT BBONNET EXTENSIONSTEM EXTENSIONGLANDGLAND BUSHGLAND FLANGELIP-SEALSPACKING TOP / BOTTOMPACKING INTERMEDIATERTJ GASKETFS GASKETBOLTSNUTSSEALSOthersOthersOthersOthersOthersOthers

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Item (GA dwg)

Mat. Conform Certs. (+Heat- and cert. No's.)

Page 73: Mesc Proxy Serv Let

20.Uni-dir≥-20>80≤+200°C nosoft

Page 73 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

20. Uni-directional (on/off) valves from ≥ –20 °C to > +80 °C and ≤ +200 °C (without

elastomeric / rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Elevated Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

MAXIMUM ALLOWABLE FUGITIVE EMISSION LEAKAGE RATES (MESC SPE 77/300 Section C.4.11, tables C.7 + C.8 + C.9)Stem / ID Packing Enter Dimensions

belowDiam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Diam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Gland / OD Packing

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Body / Bonnet or Cover

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Body Joints / Closures

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

MAXIMUM ALLOWABLE SEAT LEAKAGE RATES (MESC SPE 77/300 Section C.4.10, tables C.5 and C.6)Type Acceptance Test Low, Ambient & Elevated Temp (≥ -20 °C, in ml/min) Low Temp or Cryogenic Temp (< -20 °C, in ml/min)

Soft seated Metal seated

DN (mm) 0 0.00 0.00 1,5 ml/min *DN = 0.00 4,8 ml/min *DN = 0.00

Allowable leak (Pa*m3/s) : Class A = 1.78 E -8 x stem diam (mm), Class B = 1.78 E -7 x stem diam (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

End flange (Ref. only)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Sealant Inj. Ports / Drains / Vents

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Soft seated (ISO 5208, Rate A)

Metal seated (ISO 5208, Rate B: 0,018 ml/min *DN)

Metal seated (ISO 5208, Rate C: 0,18 ml/min *DN)

Page 74: Mesc Proxy Serv Let

20.Uni-dir≥-20>80≤+200°C nosoft

Page 74 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

20. Uni-directional (on/off) valves from ≥ –20 °C to > +80 °C and ≤ +200 °C (without

elastomeric / rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Elevated Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

NOTES

CALCULATION METHODSTorque Values: Calculation @ 2bar Experience @ 2 bar Calculation @ 100% DP Experience @ 100% DP COMMENTSDesign opearting torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Test operating torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Actuator type:Packing bolt torqueOthersOthers

EQUIPMENT USEDHelium Mass SpectrometerPressure console; Digital Pressure Gauge Pressure gauge ManometerFlow-meter: Flow-meter: Torque meter: serial number Torque tool model Thermocouple (Stem Packing)Thermocouple (Ambient)Thermocouple (Internal Body)Thermocouple (External Body)OthersOthersOthers

FOR METAL SEATED BUTTERFLY VALVES IN PRESSURE CLASSES 900# AND ABOVE IT MIGHT BE BENEFICIAL FOR THE VALVE MANUFACTURER TO DETERMINE SEATLEAKAGE RATES IN THE NON-PREFERRED DIRECTION.

Page 75: Mesc Proxy Serv Let

20.Uni-dir≥-20>80≤+200°C nosoft

Page 75 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

20. Uni-directional (on/off) valves from ≥ –20 °C to > +80 °C and ≤ +200 °C (without

elastomeric / rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and

Elevated Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

Sequence 20. Typical pressure / temperature / mechanical cycling for uni-directional (on/off) valves from ≥ –20 °C to > +80 °C and ≤ +200 °C (without soft/elastomeric seals/seats/components)

X = No test S = Seat test B = Body and fugitive emission test T = Torque test Indicated numbers above X, S, B and/or T are the amount of mechanical cycles to be performed.

Page 76: Mesc Proxy Serv Let

21.Uni-dir.≥-20≤80°C nosoft

Page 76 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

PRE TESTING CHECK LISTSPE 77/300 (CMT / MESC ver. 13.0)SPE 77/300A, SPE 77/300B, SPE 77/300D (all CMT / MESC ver. 13.0)

ConfirmDoes the test rig conform to C.2 of SPE 77/300 and figures C.1a, C.1b, C.1c? YES / NO

YES / NO

Is the tank and valve strong enough to withstand all forces exerted during the handling of the valve ? YES / NOIs the purity of the Helium equal to or higher than 97%? YES / NOIs the test rig suitable for testing the valve in both directions ? YES / NOAre the test rig valve end connectors provided with a pressure vent connection and a suitable thermocouple connection ? YES / NO

TEST VALVE

Is the test valve in accordance with the general arrangement drawing? YES / NOIs there a bill of material and does it indicate for every material the max. and min. temperature, hardness values and the origin of the industry standards? YES / NOHas a MESC buying description or valve DATA sheet been produced for the test valve? YES / NOHas test valve assembly been witnessed by Shell-GSI or its representative? YES / NOHas a HSE plan been produced for all testing work to be carried out? YES / NOAre test valve internals dry and thoroughly cleaned and degreased,dust and oil free? YES / NOHave pre-condition photographs been taken prior to valve assembly? YES / NOHas the valve passed the normal production tests in accordance with the manufacturers testing procedures? YES / NO

Ensure the test pressure to be applied falls between 20% and 80% of the pressure gauges full scale. YES / NOWhich device is to be used to measure leakage through the test valve ? SPECIFY

YES / NO

TAT @ AMBIENT TEMP. (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.1 0.0 Run-in Time to cycle Mech. Cycle

SPE 77/300

C.4.2.1

2 2 Seat A 5 C.4.2.2

3a 0.0 Seat A 1

C.4.2.3b 0.0 Seat A 1

c 0.0 Seat A 1

4 0.0C.4.2.4

5 92 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

6 0.0 Seat A 1

21. Uni-directional (on/off) valves from ≥ –20 °C to ≤ +80 °C (without elastomeric / rubber

seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient

Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

APPLICABLE DOCUMENTS

TEST RIG CONNECTION &

SUPPORTS

For prototype- and production leak (pneumatic and FE) testing, do the testing operators have the NDT method leak testing levels LT1, LT2 or LT3, qualification/competences in accordance with BS-EN 473 (2008) and/or ISO 9712 (2005) + CORR.1 (2005) and/or ASNT SNT-TC-1A (2006)?

TEST EQUIPMENT Do all test/measuring equipment and instruments have a system calibration certificate, traceable to (inter)national standards, to guarantee accuracy and have a valid calibration date not exceeding 3 (per ISO 15848) months

for the mass spectrometer and 12 months for other equipment, prior to any test?

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torques (BTO and ETC) at 1st cycle

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2)

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. (+soapy water test on castings)

Continious formation of bubbles? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.2.5+ C.4.2.2

Page 77: Mesc Proxy Serv Let

21.Uni-dir.≥-20≤80°C nosoft

Page 77 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

21. Uni-directional (on/off) valves from ≥ –20 °C to ≤ +80 °C (without elastomeric / rubber

seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient

Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

FUGITIVE EMISSION TEST RESULTS @ AMBIENT TEMP. (HELIUM) per Shell MESC description:

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

TAT; LOW & HIGH PRESSURE SEAT TEST @ AMBIENT TEMP (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

12 2 Seat A seat leakage (N2)

SPE 77/300

C.4.7

13 7 Seat A seat leakage (N2) C.4.7

14 0.0 Seat A 1

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.7.6 +C.4.2.5

Page 78: Mesc Proxy Serv Let

21.Uni-dir.≥-20≤80°C nosoft

Page 78 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

21. Uni-directional (on/off) valves from ≥ –20 °C to ≤ +80 °C (without elastomeric / rubber

seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient

Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

STRIPDOWN TEST (MESC SPE 77/300 Section C.4.8)

Part Mat. Ht. No's. & Markings Record Observations Regarding Condition of Parts

BODY BONNET / COVERCLOSURE ACLOSURE BOBTURATORSTEMSEAT RING ASEAT RING BSEAT INSERT ASEAT INSERT BBONNET EXTENSIONSTEM EXTENSIONGLANDGLAND BUSHGLAND FLANGELIP-SEALSPACKING TOP / BOTTOMPACKING INTERMEDIATERTJ GASKETFS GASKETBOLTSNUTSSEALSOthersOthersOthersOthersOthersOthers

MAXIMUM ALLOWABLE FUGITIVE EMISSION LEAKAGE RATES (MESC SPE 77/300 Section C.4.11, tables C.7 + C.8 + C.9)Stem / ID Packing Enter Dimensions

belowDiam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Diam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Gland / OD Packing

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Body / Bonnet or Cover

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Item (GA dwg)

Mat. Conform Certs. (+Heat- and cert. No's.)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -8 x stem diam (mm), Class B = 1.78 E -7 x stem diam (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

End flange (Ref. only)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Page 79: Mesc Proxy Serv Let

21.Uni-dir.≥-20≤80°C nosoft

Page 79 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

21. Uni-directional (on/off) valves from ≥ –20 °C to ≤ +80 °C (without elastomeric / rubber

seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient

Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

Body Joints / Closures

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

MAXIMUM ALLOWABLE SEAT LEAKAGE RATES (MESC SPE 77/300 Section C.4.10, tables C.5 and C.6)Type Acceptance Test Low, Ambient & Elevated Temp (≥ -20 °C, in ml/min) Low Temp or Cryogenic Temp (< -20 °C, in ml/min)

Soft seated Metal seated

DN (mm) 0 0.00 0.00 1,5 ml/min *DN = 0.00 4,8 ml/min *DN = 0.00

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Sealant Inj. Ports / Drains / Vents

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Soft seated (ISO 5208, Rate A)

Metal seated (ISO 5208, Rate B: 0,018 ml/min *DN)

Metal seated (ISO 5208, Rate C: 0,18 ml/min *DN)

Page 80: Mesc Proxy Serv Let

21.Uni-dir.≥-20≤80°C nosoft

Page 80 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

21. Uni-directional (on/off) valves from ≥ –20 °C to ≤ +80 °C (without elastomeric / rubber

seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient

Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

NOTES

CALCULATION METHODSTorque Values: Calculation @ 2bar Experience @ 2 bar Calculation @ 100% DP Experience @ 100% DP COMMENTSDesign opearting torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Test operating torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Actuator type:Packing bolt torqueOthersOthers

EQUIPMENT USEDHelium Mass SpectrometerPressure console; Digital Pressure Gauge Pressure gauge ManometerFlow-meter: Flow-meter: Torque meter: serial number Torque tool model Thermocouple (Stem Packing)Thermocouple (Ambient)Thermocouple (Internal Body)Thermocouple (External Body)OthersOthersOthers

FOR METAL SEATED BUTTERFLY VALVES IN PRESSURE CLASSES 900# AND ABOVE IT MIGHT BE BENEFICIAL FOR THE VALVE MANUFACTURER TO DETERMINE SEATLEAKAGE RATES IN THE NON-PREFERRED DIRECTION.

Page 81: Mesc Proxy Serv Let

21.Uni-dir.≥-20≤80°C nosoft

Page 81 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

21. Uni-directional (on/off) valves from ≥ –20 °C to ≤ +80 °C (without elastomeric / rubber

seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient

Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

Sequence 21. Typical pressure / temperature / mechanical cycling for uni-directional (on/off) valves from ≥ –20 °C to ≤ +80 °C (without soft/elastomeric seals/seats/components).

X = No test S = Seat test B = Body and fugitive emission test T = Torque test Indicated numbers above X, S, B and/or T are the amount of mechanical cycles to be performed.

Page 82: Mesc Proxy Serv Let

22.Uni-dir.≥-20°C<0°C≤80°C

Page 82 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

PRE TESTING CHECK LISTSPE 77/300 (CMT / MESC ver. 13.0)SPE 77/300A, SPE 77/300B, SPE 77/300D (all CMT / MESC ver. 13.0)

ConfirmDoes the test rig conform to C.2 of SPE 77/300 and figures C.1a, C.1b, C.1c? YES / NO

YES / NO

Is the tank and valve strong enough to withstand all forces exerted during the handling of the valve ? YES / NOIs the purity of the Helium equal to or higher than 97%? YES / NOIs the test rig suitable for testing the valve in both directions ? YES / NOAre the test rig valve end connectors provided with a pressure vent connection and a suitable thermocouple connection ? YES / NO

TEST VALVE

Is the test valve in accordance with the general arrangement drawing? YES / NOIs there a bill of material and does it indicate for every material the max. and min. temperature, hardness values and the origin of the industry standards? YES / NOHas a MESC buying description or valve DATA sheet been produced for the test valve? YES / NOHas test valve assembly been witnessed by Shell-GSI or its representative? YES / NOHas a HSE plan been produced for all testing work to be carried out? YES / NOAre test valve internals dry and thoroughly cleaned and degreased,dust and oil free? YES / NOHave pre-condition photographs been taken prior to valve assembly? YES / NOHas the valve passed the normal production tests in accordance with the manufacturers testing procedures? YES / NO

Ensure the test pressure to be applied falls between 20% and 80% of the pressure gauges full scale. YES / NOWhich device is to be used to measure leakage through the test valve ? SPECIFY

YES / NO

TAT @ AMBIENT TEMP. (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.1 0.0 Run-in Time to cycle Mech. Cycle

SPE 77/300

C.4.2.1

2 2 Seat A 5 C.4.2.2

3a 0.0 Seat A 1

C.4.2.3b 0.0 Seat A 1

c 0.0 Seat A 1

4 0.0C.4.2.4

5 42 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

6 0.0 Seat A 1

22. Uni-directional (on/off) valves from ≥ –20 °C and < 0 °C to ≤ +80 °C (including elastomeric /

rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and Low

Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

APPLICABLE DOCUMENTS

TEST RIG CONNECTION &

SUPPORTS

For prototype- and production leak (pneumatic and FE) testing, do the testing operators have the NDT method leak testing levels LT1, LT2 or LT3, qualification/competences in accordance with BS-EN 473 (2008) and/or ISO 9712 (2005) + CORR.1 (2005) and/or ASNT SNT-TC-1A (2006)?

TEST EQUIPMENT Do all test/measuring equipment and instruments have a system calibration certificate, traceable to (inter)national standards, to guarantee accuracy and have a valid calibration date not exceeding 3 (per ISO 15848) months

for the mass spectrometer and 12 months for other equipment, prior to any test?

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torques (BTO and ETC) at 1st cycle

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2)

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. (+soapy water test on castings)

Continious formation of bubbles? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.2.5+ C.4.2.2

Page 83: Mesc Proxy Serv Let

22.Uni-dir.≥-20°C<0°C≤80°C

Page 83 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

22. Uni-directional (on/off) valves from ≥ –20 °C and < 0 °C to ≤ +80 °C (including elastomeric /

rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and Low

Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

FUGITIVE EMISSION TEST RESULTS @ AMBIENT TEMP. (HELIUM) per Shell MESC description:

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Cooling Down procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

TAT @ LOW TEMP (NITROGEN) per Shell MESC description: Test Temp: °C Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

7 2 Seat A 5

SPE 77/300

8a 0.0 Seat A 1b 0.0 Seat A 1c 0.0 Seat A 1

9 0.0

10 0.0 42 Time to cycle and carry out FE Mech. cycle + Fugitive Emission (He) See FE results below

11 0.0 Seat A 1

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C) +torques (BTO and ETC) at 1st cycle

C.4.6.1 +C.4.2.2

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C)C.4.6.2 +C.4.2.3

Shell / Body Test

SPE 77/300 para C.4.12 Table C.10

body/shell leakage (He), no pressure drop. C.4.6.3 +

C.4.2.4

Visible leakage / pressure drop? (YES/NO)

Mech. Cycle + FE

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2, He if T<-110 °C) +torque (BTO and ETC)

C.4.6.4+C.4.2.5

Page 84: Mesc Proxy Serv Let

22.Uni-dir.≥-20°C<0°C≤80°C

Page 84 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

22. Uni-directional (on/off) valves from ≥ –20 °C and < 0 °C to ≤ +80 °C (including elastomeric /

rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and Low

Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

FUGITIVE EMISSION TEST RESULTS @ LOW TEMP (HELIUM) per Shell MESC description: Test Temp: 0 °C

Part / Item:

Static Measure Dynamic Measure NOTES

Highest measured value (mbar*l/s)Stem / ID PackingGland / OD PackingBody / BonnetBody / Closure ABody / Closure BEnd Flange A (ref.)End Flange B (ref.)Sealant Inj. SEATSealant Inj. STEMDrainVentOthersOthers

Warming up procedure - Measure temperature: DN150 < every 30 mins, DN 200 to DN 350 every 45 mins DN 400 > every 60 mins

Time Notes

TAT; LOW & HIGH PRESSURE SEAT TEST @ AMBIENT TEMP (NITROGEN 100%) per Shell MESC description: Date: dd/mm/yyyyStep Activity Press Description Number Hold Time Measurement Reference Document Measured Values Accept. Criteria

Item (barg) Test cycles (min) Test Test Procedure Para.

12 2 Seat A seat leakage (N2)

SPE 77/300

C.4.7

13 2 Seat A seat leakage (N2) C.4.7

14 0.0 Seat A 1

Allowable Leakage FE (mbar*l/s)

Highest measured value (mbar*l/s)

Valve body Temperature (outside)

(TV1) °C

Closure member Temperature (internal)

(TV 2) °C

Stem packing area Temperature (outside)(TV3) °C

Room Temperature(Amb) °C (TV4)

BTO (Nm)

ETC (Nm)

TimeStart

TimeFinish

Seat leakage (ml/min) Allowable seat leakage

(ml/min)

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

SPE 77/300 para C.4.12 Table C.11

seat leakage (N2) +torque (BTO and ETC)

C.4.7.6 +C.4.2.5

Page 85: Mesc Proxy Serv Let

22.Uni-dir.≥-20°C<0°C≤80°C

Page 85 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

22. Uni-directional (on/off) valves from ≥ –20 °C and < 0 °C to ≤ +80 °C (including elastomeric /

rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and Low

Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

STRIPDOWN TEST (MESC SPE 77/300 Section C.4.8)

Part Mat. Ht. No's. & Markings Record Observations Regarding Condition of Parts

BODY BONNET / COVERCLOSURE ACLOSURE BOBTURATORSTEMSEAT RING ASEAT RING BSEAT INSERT ASEAT INSERT BBONNET EXTENSIONSTEM EXTENSIONGLANDGLAND BUSHGLAND FLANGELIP-SEALSPACKING TOP / BOTTOMPACKING INTERMEDIATERTJ GASKETFS GASKETBOLTSNUTSSEALSOthersOthersOthersOthersOthersOthers

MAXIMUM ALLOWABLE FUGITIVE EMISSION LEAKAGE RATES (MESC SPE 77/300 Section C.4.11, tables C.7 + C.8 + C.9)Stem / ID Packing Enter Dimensions

belowDiam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Diam (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Gland / OD Packing

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Body / Bonnet or Cover

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

Item (GA dwg)

Mat. Conform Certs. (+Heat- and cert. No's.)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -8 x stem diam (mm), Class B = 1.78 E -7 x stem diam (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

End flange (Ref. only)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Page 86: Mesc Proxy Serv Let

22.Uni-dir.≥-20°C<0°C≤80°C

Page 86 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

22. Uni-directional (on/off) valves from ≥ –20 °C and < 0 °C to ≤ +80 °C (including elastomeric /

rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and Low

Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

Body Joints / Closures

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

OD (mm) 0.00E+00 0.00E+00 0.00E+00 (mbar*l/s)

MAXIMUM ALLOWABLE SEAT LEAKAGE RATES (MESC SPE 77/300 Section C.4.10, tables C.5 and C.6)Type Acceptance Test Low, Ambient & Elevated Temp (≥ -20 °C, in ml/min) Low Temp or Cryogenic Temp (< -20 °C, in ml/min)

Soft seated Metal seated

DN (mm) 0 0.00 0.00 1,5 ml/min *DN = 0.00 4,8 ml/min *DN = 0.00

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Sealant Inj. Ports / Drains / Vents

Allowable leak (Pa*m3/s) : Class A = 1.78 E -9 x gasket outer diameter (mm), Class B = 1.78 E -8 x gasket outer diameter (mm).

FE TIGHTNESS "CLASS A" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

FE TIGHTNESS "CLASS B" = (Pa*m3/s), equals: (atm*cm3/s = atm*ml/s)

Soft seated (ISO 5208, Rate A)

Metal seated (ISO 5208, Rate B: 0,018 ml/min *DN)

Metal seated (ISO 5208, Rate C: 0,18 ml/min *DN)

Page 87: Mesc Proxy Serv Let

22.Uni-dir.≥-20°C<0°C≤80°C

Page 87 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

22. Uni-directional (on/off) valves from ≥ –20 °C and < 0 °C to ≤ +80 °C (including elastomeric /

rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and Low

Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

NOTES

CALCULATION METHODSTorque Values: Calculation @ 2bar Experience @ 2 bar Calculation @ 100% DP Experience @ 100% DP COMMENTSDesign opearting torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Test operating torques Nm Nm Nm Nmambient temperaturemax. elevated temperaturelow temperature

Actuator type:Packing bolt torqueOthersOthers

EQUIPMENT USEDHelium Mass SpectrometerPressure console; Digital Pressure Gauge Pressure gauge ManometerFlow-meter: Flow-meter: Torque meter: serial number Torque tool model Thermocouple (Stem Packing)Thermocouple (Ambient)Thermocouple (Internal Body)Thermocouple (External Body)OthersOthersOthers

FOR METAL SEATED BUTTERFLY VALVES IN PRESSURE CLASSES 900# AND ABOVE IT MIGHT BE BENEFICIAL FOR THE VALVE MANUFACTURER TO DETERMINE SEATLEAKAGE RATES IN THE NON-PREFERRED DIRECTION.

Page 88: Mesc Proxy Serv Let

22.Uni-dir.≥-20°C<0°C≤80°C

Page 88 of 88

TEST VALVE INFORMATION DOC N° SPE 77/300C2

Shell-GSI Contract Number: FE Tightness Cl:ITEM N°

Project & P.O. Number: Test valve no:Valve MESC / TAG / Item No: Material - Body: REV DATE Mar.2010 / MESC 13.0Drawing: Material - Trim:Valve Nominal Size (DN / NPS): TEC Code:Pressure Class (PN / LBS): Valve Serial No:

Heat No. Body:Test Temp. Range (°C): Heat No. Bonnet:

22. Uni-directional (on/off) valves from ≥ –20 °C and < 0 °C to ≤ +80 °C (including elastomeric /

rubber seals/seats/components):

Combined Synoptic Table for Seat Leakage & Fugitive Emission testing @ Ambient and Low

Temperature.

NOTE: ALL WHITE CELLS TO BE COMPLETED BY THE VALVE

MANUFACTURERDesign Temp. Range (°C):

Sequence 22. Typical pressure / temperature / mechanical cycling for uni-directional (on/off) valves from ≥ –20 °C and < 0 °C to ≤ +80 °C (including soft/elastomeric seals/seats/components).

X = No test S = Seat test B = Body and fugitive emission test T = Torque test Indicated numbers above X, S, B and/or T are the amount of mechanical cycles to be performed.