engineering manual hf212 solder paste - farnell element14 · engineering manual ... • measured
TRANSCRIPT
Suitable for use with: Standard SAC Alloys
Engineering Manual LOCTITE GC 10 T3 Solder Paste
GC 10 – The Game Changer
January 26, 2016 Engineering Manual GC 10 Solder Paste 2
1. Performance Summary
2. Introduction: Properties, Features & Benefits
3. Operating Parameters
• Printing: Process Window
• Printing: Continuous and Abandon Time Testing
• Slump Testing
• Tack-Life Force
• Reflow Process Window
• Reflow Performance Testing
• Voiding Data
4. Reliability and Specification Testing
5. Operating Parameters: Storage
• Printing & Reflow Performance
6. Product Summary
Contents
January 26, 2016 Engineering Manual GC 10 Solder Paste 3
1. Performance Summary
2. Introduction: Properties, Features & Benefits
3. Operating Parameters
• Printing: Process Window
• Printing: Continuous and Abandon Time Testing
• Slump Testing
• Tack-Life Force
• Reflow Process Window
• Reflow Performance Testing
• Voiding Data
4. Reliability and Specification Testing
5. Operating Parameters: Storage
• Printing & Reflow Performance
6. Product Summary
Contents
January 26, 2016 Engineering Manual GC 10 Solder Paste 4
GC 10: Performance Summary
Flux
• Halogen-free flux: passes IC with pretreatment IPC-TM-650
2.3.34/EN14582
• Halogen-free flux classification: ANSI/J-STD-004 Rev. B for
a type ROL0 classification
Paste
• Suitable for printing up to 125mm/s (5”/s)
• Optimized for long hot soak reflow profiles
• Excellent coalescence in air & nitrogen atmosphere
• Excellent humidity resistance
• Excellent solderability on challenging surface finishes,
including CuNiZn
• Colourless residues for easy post-reflow inspection
• Long 12 month shelf-life when stored below 25C
January 26, 2016 Engineering Manual GC 10 Solder Paste 5
1. Performance Summary
2. Introduction: Properties, Features & Benefits
3. Operating Parameters
• Printing: Process Window
• Printing: Continuous and Abandon Time Testing
• Slump Testing
• Tack-Life Force
• Reflow Process Window
• Reflow Performance Testing
• Voiding Data
4. Reliability and Specification Testing
5. Operating Parameters: Storage
• Printing & Reflow Performance
6. Product Summary
Contents
Introduction Basic Solder Paste Properties
Flux Description GC 10
Alloy SAC305
Henkel Powder Size Type 3
Powder Size range, m 45-25
Metal Content, % 88.5
Malcom Viscosity, 10rpm Pa.s 207
TI 0.50
IPC slump @182C (0.33mm x 2.03mm)
first space no bridge
0.15
IPC Solder Balling preferred
January 26, 2016 Engineering Manual GC 10 Solder Paste 6
January 26, 2016 Engineering Manual GC 10 Solder Paste 7
Introduction GC 10 Features & Benefits
Product Attribute Process Benefit
Halogen Free • No added halogen
• Measured <900ppm chlorine and bromine and <1,500ppm total by
oxygen (O2) bomb test
Halide Free • Flux classification ROL0 in accordance to J-STD-004B
Application
• Designed for printing and pin-in-paste
• Excellent wetting to a broad range of metallisations, even through
long hot soak profiles in an air atmosphere
• Compatible with existing halogen free solutions
• Suitable for medium to large board assemblies
• Designed for long 12 month shelf-life stability without impact to
printing or reflow
January 26, 2016 Engineering Manual GC 10 Solder Paste 8
Introduction GC 10 Features & Benefits
Product Attribute Process Benefit
Technology Printing
Advantages
• Wide process window for printing and minimal slump
• Abandon time of up to 2 hours; work life > 16 hours
• Excellent print capability and reduction in print related defects
• Suited for high throughput production, where yield consistency on print
deposits is key
• Improved paste transfer efficiency
• Allows on line paste utilisation protocols to be re-written
Technology Reflow
Advantages
• Optimised for long hot soak reflow processes
• Very shiny Pb-free solder joints over wide range of reflow
• Excellent coalescence
• Excellent humidity resistance
• Excellent solderability on challenging surface finishes (ENIG, Copper OSP,
CuNiZn and Imm Ag)
Low Voiding
• Low void levels increases solder joint reliability
• New chemistries allow pursuit of class 3 void levels in accordance to IPC7095B
on industry surface finishes: ENIG, Copper OSP, CuNiZn and Imm Ag
• Low voiding in CSP/BGA
Residues
• Clear, transparent and colourless
• Pin testable after 4x reflows
January 26, 2016 Engineering Manual GC 10 Solder Paste 9
1. Performance Summary
2. Introduction: Properties, Features & Benefits
3. Operating Parameters
• Printing: Process Window
• Printing: Continuous and Abandon Time Testing
• Slump Testing
• Tack-Life Force
• Reflow Process Window
• Reflow Performance Testing
• Voiding Data
4. Reliability and Specification Testing
5. Operating Parameters: Storage
• Printing & Reflow Performance
6. Product Summary
Contents
January 26, 2016 Engineering Manual GC10 Solder Paste 10
Operating Parameters Print Process Window (LOCTITE GC 10 SAC305 T3 885V)
• Excellent printing in the range 30 –
120mm/s, 0.4mm to 0.27mm round
apertures
0.8mm, 0.5mm & 0.4mm pitch round apertures, (120µm stencil)
Speed mm/s
Pre
ssu
re
kg
/m
m
120100806040
0.04
0.03
0.02
>
–
–
< 1.33
1.33 1.67
1.67 2.00
2.00
0.8BGA Cpk
Speed mm/s
Pre
ssu
re
kg
/m
m
120100806040
0.04
0.03
0.02
>
–
–
< 1.33
1.33 1.67
1.67 2.00
2.00
0.5CSPCpk
Speed mm/s
Pre
ssu
re
kg
/m
m
120100806040
0.04
0.03
0.02
>
–
–
< 1.33
1.33 1.67
1.67 2.00
2.00
diam Cpk0.30mm
Speed mm/s
Pre
ssu
re
kg
/m
m120100806040
0.04
0.03
0.02
>
–
–
< 1.33
1.33 1.67
1.67 2.00
2.00
0.5BGA Cpk
Contour Plot of 0.8mm BGA (0.4mm aperture) Cpk Contour Plot of 0.5mm CSP (0.31mm aperture) Cpk
Contour Plot of 0.30mm diam circles Cpk Contour Plot of 0.5mm BGA (0.27mm aperture) Cpk
January 26, 2016 Engineering Manual GC10 Solder Paste 11
Operating Parameters Print Process Window (LOCTITE GC 10 SAC305 T3 885V)
• Excellent printing in
the range 30 –
120mm/s, 0.28-
0.22mm round
apertures
• Limited process
window with
0.20mm apertures.
GC 10 T4 may be
required
0.28mm – 0.20mm round apertures, (120µm stencil)
Speed mm/s
Pre
ssu
re
kg
/m
m
120100806040
0.04
0.03
0.02
>
–
–
< 1.33
1.33 1.67
1.67 2.00
2.00
diam Cpk
0.28mm
Speed mm/s
Pre
ssu
re
kg
/m
m
120100806040
0.04
0.03
0.02
>
–
–
< 1.33
1.33 1.67
1.67 2.00
2.00
diam Cpk
0.25mm
Speed mm/s
Pre
ssu
re
kg
/m
m
120100806040
0.04
0.03
0.02
>
–
–
< 1.33
1.33 1.67
1.67 2.00
2.00
diam Cpk0.22mm
Speed mm/s
Pre
ssu
re
kg
/m
m
120100806040
0.04
0.03
0.02
>
–
–
< 1.33
1.33 1.67
1.67 2.00
2.00
diam Cpk0.20mm
Contour Plot of 0.28mm diam circles Cpk Contour Plot of 0.25mm diam circles Cpk
Contour Plot of 0.22mm diam circles Cpk Contour Plot of 0.20mm diam circles Cpk
January 26, 2016 Engineering Manual GC 10 Solder Paste 12
Operating Parameters – Separation Speed Print Process Window (LOCTITE GC 10 SAC305 T3 885V) • Excellent printing in the
range down to 0.22mm round apertures.
• Fast separation speed is preferable.
0.8mm BGA – 0.18mm round apertures, 120m stencil thickness, 60mm/s,10kg
0.18
mm
dia circ
les
0.20
mm d
ia cir
cles
0.22
mm
dia circ
les
0.25
mm d
ia cir
cles
0.28
mm
dia circ
les
0.5m
m BGA
(0.2
7mm ap)
0.5m
m CSP
(0.3
1mm a
p)
0.5m
m uBG
A (0
.35m
m ap)
0.8m
m BGA
(0.4
mm a
p)
5
4
3
2
1
0
Cp
k1.33 ref1.67 ref
Fast
Medium
Slow
Variable
Separation speed. Cpk Loctite GC 10 SAC305 T3 885V
Operating Parameters Continuous Print and Abandon Stability Assessment
Paste
added to stencil
Paste
kneaded
Dry under
stencil wipe
1hr pause Print 5 PCBs Print 5 PCBs
• Printing
• DEK Europa
• Stainless steel, laser cut
• 120m thickness
• Vacuum tooling
• 250mm, 60 squeegee
• 60mm/s squeegee speed
• Fast separation speed
• Conditions typical, 22C, 40% RH
• Koh Young KY-8020T volume measurement
Print 15 PCBs,
dry wipe every 5
2hr pause
Volumes
Measured
Blank stencil
1000 or 2000
cycles
Print 15 PCBs,
dry wipe every 5
Volumes
Measured
January 26, 2016 Engineering Manual GC 10 Solder Paste 13
Henkel Board 0.8mm BGA to 0.18mm diameter circles Process flow for Henkel print test as shown below
January 26, 2016 Engineering Manual GC 10 Solder Paste 14
Operating Parameters – Abandon Stability 22C/40%RH Print Process Window (LOCTITE GC 10 SAC305 T3 885V)
• Print Capabilities
• Excellent printing in the
range down to 0.22mm round apertures
• Single knead cycle required after 2hr abandon at 0.20mm round apertures
0.8mm BGA – 0.15mm round apertures
120m stencil thickness, 60mm/s, fast separation, 250mm squeegee, 10kg
0.18
mm dia circ
les
0.20
mm dia circ
les
0.22
mm dia circ
les
0.25
mm dia circ
les
0.28
mm dia circ
les
0.5m
m BGA
(0.27
mm ap)
0.5m
m CSP
(0.31
mm ap)
0.5m
m µBG
A (0
.35m
m ap)
0.8m
m BGA
(0.4m
m ap)
5
4
3
2
1
0
Cp
k
1.33 ref1.67 ref
Initial
1hr
2hr
2hr + knead
Variable
Abandon time 1hr, 2hr, 2hr + 1 knead Loctite GC 10 SAC305 T3 885V
January 26, 2016 Engineering Manual GC 10 Solder Paste 15
Operating Parameters – Abandon Stability 22C/40%RH Print Process Window (LOCTITE GC 10 SAC305 T3 885V)
• Transfer Efficiencies
• Excellent printing in the range 0.40mm down to 0.27mm round apertures
0.8mm BGA – 0.5mm BGA round apertures
120m stencil thickness, 60mm/s, fast separation, 250mm squeegee, 10kg
252321191715131197531
160
120
80
40
0
Print No.
Tra
nsfe
r Eff
icie
ncy %
0.5 Vnom
1.5 Vnom
_X=98.5
_X=97.7
_X=94.4
Initial 1 hr ab 2 hr ab
252321191715131197531
160
120
80
40
0
Print No.
Tra
nsfe
r E
ffic
ien
cy %
1.5 Vnom
0.5Vnom
_X=88.8
_X=85.6
Initial 1 hr ab 2 hr ab
_X=86.9
252321191715131197531
160
120
80
40
0
Print No.
Tra
nsfe
r Eff
icie
ncy %
0.5V nom
1.5 Vnom
_X=84.7 _
X=84.9_X=83.2
Initial 1 hr ab 2 hr ab
252321191715131197531
160
120
80
40
0
Print no.
Tra
nsfe
r Eff
icie
ncy %
0.5 Vnom
1.5 Vnom
_X=84.7
_X=83.5
_X=82.4
Initial 1 hr ab 2 hr ab
0.8mm BGA (0 .4mm ap) 0 .5mm BGA (0 .34mm ap)
0 .5mm CSP (0 .31mm ap) 0 .5mm BGA (0 .27mm dia ap)
January 26, 2016 Engineering Manual GC 10 Solder Paste 16
Operating Parameters – Abandon Stability 22C/40%RH Print Process Window (LOCTITE GC 10 SAC305 T3 885V)
• Transfer Efficiencies
• Excellent printing in the
range down to 0.22mm round apertures
• Single knead cycle for best results after 2hr abandon at 0.20mm round apertures and below
0.28mm – 0.20mm round apertures
120m stencil thickness, 60mm/s, fast separation, 250mm squeegee, 10kg
252321191715131197531
160
120
80
40
0
Print No.
Tra
nsfe
r Eff
icie
ncy %
1.5 Vnom
0.5 Vnom
_X=92.0
_X=92.1
_X=90.6
Initial 1 hr ab 2 hr ab
252321191715131197531
160
120
80
40
0
Print No.
Tra
nsfe
r Eff
icie
ncy %
0.5 Vnom
1.5 Vnom
_X=96.3
_X=96.1
Initial 1 hr ab 2 hr ab
_X=95.0
252321191715131197531
160
120
80
40
0
Print No.
Tra
nsfe
r Eff
icie
ncy %
0.5 Vnom
1.5 Vnom
_X=99.6
_X=99.4
_X=95.7
Initial 1 hr ab 2 hr ab
252321191715131197531
160
120
80
40
0
Print No.
Tra
nsfe
r Eff
icie
ncy %
0.5 Vnom
1.5 Vnom
_X=95.1
_X=94.6 _
X=88.3
Initial 1 hr ab 2 hr ab
0.25mm dia round apertures 0 .22mm dia round apertures
0 .20mm dia round apertures 0 .18mm dia round apertures
January 26, 2016 Engineering Manual GC 10 Solder Paste 17
Operating Parameters – Continuous Print Stability Print Process Window (LOCTITE GC 10 SAC305 T3 885V) • Print Capabilities
• No impact on print
performance after 8 hours (1000 cycles) and 16 hours (2000 cycles) printing
0.8mm BGA – 0.18mm round apertures, 120m stencil thickness,
60mm/s, Fast separation, 250mm squeegee, 10kg
0.18
mm dia circ
les
0.20
mm dia circ
les
0.22
mm dia circ
les
0.25
mm dia circ
les
0.28
mm dia circ
les
0.5m
m BGA
(0.27
mm ap)
0.5m
m C
SP (0.31
mm ap)
0.5m
m µBG
A (0.35m
m ap)
0.8m
m BGA
(0.4m
m ap)
5
4
3
2
1
0
Cp
k
1.33 ref1.67 ref
Initial
1,000 cycles
2,000 cycles
Variable
Continuous Print Stability 1000 cycles, 2000 cycles
Loctite GC 10 SAC305 T3 885V
January 26, 2016 Engineering Manual GC 10 Solder Paste 18
Operating Parameters – Continuous Print Stability Print Process Window (LOCTITE GC 10 SAC305 T3 885V) • Transfer Efficiencies
• No impact on print
performance after 8 hours (1000 cycles) and 16 hours (2000 cycles) printing
0.8mm BGA – 0.5mm BGA round apertures, 120m stencil thickness,
60mm/s, Fast separation, 250mm squeegee, 10kg
454137332925211713951
160
120
80
40
0
Print No.
Tra
nsfe
r Eff
iency %
1.5 V nom
0.5 Vnom
_X=98.5
_X=96.5
_X=94.1
Initial 1000 prints 2000 prints
454137332925211713951
160
120
80
40
0
Print No.
Tra
nsfe
r Eff
icie
ny %
0.5 Vnom
1.5 Vnom
_X=88.8
_X=87.2
_X=83.8
Initial 1000 prints 2000 prints
454137332925211713951
160
120
80
40
0
Print No.
Tra
nsfe
r Eff
icie
ncy %
0.5 Vnom
1.5 Vnom
_X=84.7
_X=84.0
_X=80.8
Initial 1000 prints 2000 prints
454137332925211713951
160
120
80
40
0
Print no.
Tra
nsfe
r Eff
icie
ncy % _
X=84.7 _X=80.9
Initial 1000 prints 2000 prints
0.5 Vnom
1.5 Vnom
_X=83.5
0.8mm BGA (0 .4mm ap) 0 .5mm BGA (0 .34mm ap)
0 .5mm CSP (0 .31mm ap) 0 .5mm BGA (0 .27mm ap)
January 26, 2016 Engineering Manual GC 10 Solder Paste 19
Operating Parameters – Continuous Print Stability Print Process Window (LOCTITE GC 10 SAC305 T3 885V) • Transfer Efficiencies
• No impact on print performance after 8 hours (1000 cycles) and 16 hours (2000 cycles) printing
0.28mm– 0.20mm round apertures, 120m stencil thickness,
60mm/s, Fast separation, 250mm squeegee, 10kg
454137332925211713951
160
120
80
40
0
Print No.
Tra
nsfe
r Eff
icie
ncy %
1.5 Vnom
0.5 Vnom
_X=92.0
_X=89.0
_X=85.5
Initial 1000 prints 2000 prints
454137332925211713951
160
120
80
40
0
Print No.
Tra
nsfe
r Eff
icie
ncy %
0.5 Vnom
1.5 Vnom
_X=96.3
_X=93.9
_X=89.6
Initial 1000 prints 2000 prints
454137332925211713951
160
120
80
40
0
Print No.
Tra
nsfe
r Eff
icie
ncy %
0.5 Vnom
1.5 Vnom
_X=99.6
_X=96.9
Initial 1000 prints 2000 prints
_X=91.9
454137332925211713951
160
120
80
40
0
Print no.
Tra
nsfe
r E
ffic
ien
cy %
0.5 Vnom
1.5 Vnom
_X=95.1
_X=92.7
_X=87.2
Initial 1000 prints 2000 prints
0.25mm dia round apertures 0 .22mm dia round apertures
0 .20mm dia round apertures 0 .18mm dia round apertures
6543210
300
250
200
150
100
50
0
Time (min)
Te
mp
era
ture
(°C
) 217°C
Profile 2
• No change to reflow performance after 16hours
printing (2000 print cycles)
January 26, 2016 Engineering Manual GC 10 Solder Paste 20
Operating Parameters (Reflow) Paste Properties After Continuous Printing
Initial
1,000 cycles
(8 hours)
22°C, 40%RH
2,000 cycles
(16 hours)
22°C, 40%RH
0.5
mm
CS
P
6.5
mm
Overp
rint
January 26, 2016 Engineering Manual GC 10 Solder Paste 21
Operating Parameters Slump
• Slump evaluation was performed in accordance with J-STD-005A, IPC-TM-650 2.4.35
• First spacing with no bridge recorded after 10 minutes at 182C (35C below melting point 217C)
Stencil
Design/
thickness
A 21
200m
A 20
100m
Aperture
0.63 x
2.03mm
0.33 x
2.03mm
0.33 x
2.03mm
0.20 x
2.03mm
Pass
mark 0.63mm 0.30mm 0.30mm 0.25mm
GC 10
25C 0.33mm 0.10mm 0.08mm 0.075mm
GC 10
182C 0.33mm 0.15mm 0.15mm 0.125mm
A21
200m
A20
100m
Operating Parameters Tack Force
Preload 300g
Preload time 5 secs
Retraction Speed 2.5mm/sec
Deposit diameter 5.1mm
Deposit height 0.25mm
Malcom TK1 Tackiness Tester
January 26, 2016 Engineering Manual GC10 Solder Paste 22
• Tackiness evaluation was performed in accordance with J-STD-005A,
IPC-TM-650 2.4.44
• GC10 tack-life >48hours
0
10
20
30
40
50
60
70
80
90
100
0 6 16 24 48
Tack
Fo
rce
gF
Time hours
IPC Tack force gF
Tack force gF 80% Peak Tack Force
January 26, 2016 Engineering Manual GC 10 Solder Paste 23
Operating Parameters Solder Balling
Initial
Preferred Pass
• Solder balling performance as been assessed in accordance with
an extended version of IPC-TM-650 2.4.4.3
• Clear and colourless residues observed post-reflow
24hrs 25C 50% RH
Preferred Pass
January 26, 2016 Engineering Manual GC 10 Solder Paste 24
Operating Parameters Reflow Process Window (Air)
• LOCTITE GC 10 solder paste offers halogen containing reflow performance in a
truly halogen free formulation
• GC 10 shows excellent coalescence onto a range of PCB and component finishes
especially during long-hot profiles
• There is no single profile that works for all applications and each process should be
assessed individually, under laboratory conditions the following profiles have been
found to give good results
• These process window guidelines are suitable for Type 3 SAC powder
Profile 1 2 3 4
Peak Temp (°C) 244 254 260 255
Time to Peak (min) 3.3 4.5 5.1 6.0
Soak Time (150-200°C) (min)
(No
Soak)
1.0
2.35 2.80 3.44
Time above Liquidus (min) 0.62 1.46 1.75 1.45
Time above Liquidus (sec) 37.2 87.6 105.0 87.0 7 6 5 4 3 2 1 0
300
250
200
150
100
50
0
Time (minutes)
T e m
p e
r a t u
r e (
° C
) 217°C
Profile 1
Profile 2
Profile 3
Profile 4
Reflow Profiles
Operating Parameters (Reflow)
January 26, 2016 Engineering Manual GC 10 Solder Paste 25
1 2 3 4
1206 c
hip
s
0603 c
hip
s
0402 c
hip
s
Reflow Profile
7 6 5 4 3 2 1 0
300
250
200
150
100
50
0
Time (minutes)
T e
m p
e r
a t u
r e
( °
C ) 217°C
Profile 1
Profile 2
Profile 3
Profile 4
Reflow Profiles
Operating Parameters (Reflow)
January 26, 2016 Engineering Manual GC 10 Solder Paste 26
1 2 3 4
Ove
rprin
ted
So
lde
r b
all
0.5
mm
CS
P5
6
0.4
mm
TQ
FP
12
0
Reflow Profile
7 6 5 4 3 2 1 0
300
250
200
150
100
50
0
Time (minutes)
T e
m p
e r
a t u
r e
( °
C ) 217°C
Profile 1
Profile 2
Profile 3
Profile 4
Reflow Profiles
Reflow Profile
January 26, 2016 Engineering Manual GC 10 Solder Paste 27
Operating Parameters (Reflow – GC10)
2 4
0201 c
hip
s
0402 c
hip
s
1206 c
hip
s
6543210
250
200
150
100
50
Time (minutes)
Te
mp
era
ture
(°C
)
217°C
Profile 1
Profile 2
Reflow Profiles
January 26, 2016 Engineering Manual GC 10 Solder Paste 28
Operating Parameters (Reflow – GC10)
Reflow Profile
1 2
0.4
mm
TQ
FP
0.5
mm
CS
P56
6543210
250
200
150
100
50
Time (minutes)
Te
mp
era
ture
(°C
)
217°C
Profile 1
Profile 2
Reflow Profiles
Operating Parameters Voiding
GC 10 meets IPC7095B class 3
January 26, 2016 Engineering Manual GC 10 Solder Paste 29
• Void performance assessed using 4 different reflow profiles.
• 0.5mm CSP, 120µm stencil
• With component, 0.5mm CSP, SAC305 balls
• GC 10 shows low levels of voiding over a range of profiles
• Void Percentage analysed in accordance with IPC7095B
Profile 4Profile 3Profile 2Profile 1
20
15
10
5
0
IPC
vo
idin
g %
Class 3
Class 2
Class 1
Boxplot of IPC Voiding Percentage
Profile 4Profile 3Profile 2Profile 1
10
8
6
4
2
0
% V
oid
ing
Line Plot of No. of Voids
7 6 5 4 3 2 1 0
300
250
200
150
100
50
0
Time (minutes)
T e
m p
e r
a t u
r e
( °
C ) 217°C
Profile 1
Profile 2
Profile 3
Profile 4
Reflow Profiles
January 26, 2016 Engineering Manual GC 10 Solder Paste 30
Operating Parameters 2nd side reflow
0.5
mm
CS
P 5
6
02
01
0402
1 2 3 4
2nd second side reflow profile
7 6 5 4 3 2 1 0
300
250
200
150
100
50
0
Time (minutes)
T e
m p
e r
a t u
r e
( °
C ) 217°C
Profile 1
Profile 2
Profile 3
Profile 4
Reflow Profiles
Operating Parameters Voiding after 2nd side reflow
GC 10 meets IPC7095B class 3
January 26, 2016 Engineering Manual GC 10 Solder Paste 31
• Void performance assessed using 4 different reflow profiles.
• 0.5mm CSP, 120µm stencil
• With component, 0.5mm CSP, SAC305 balls
• GC 10 shows no deterioration in voiding with pre reflowed boards
Pre reflow
Profile
pre-reflowedNo pre-reflow
Profile 4Profile 3Profile 2Profile 1Profile 4Profile 3Profile 2Profile 1
20
15
10
5
0
Pe
rce
nta
ge
Class 3
Class 2
Class 1
Boxplot of % voidingGC 10 T3
Profile 4Profile 3Profile 2Profile 1
10
8
6
4
2
0N
o.
of
Vo
ids
No pre-reflow
pre-reflowed
Pre reflow
Line Plot of No. of voids
7 6 5 4 3 2 1 0
300
250
200
150
100
50
0
Time (minutes)
T e
m p
e r
a t u
r e
( °
C ) 217°C
Profile 1
Profile 2
Profile 3
Profile 4
Reflow Profiles
Board
Stencil 100m
Pads 500 pads per board, 2 boards tested
Probe 0.9mm 4 point plain crown light spring probe 100g spring force
Profiles 4 reflow profiles
No. of reflow 1, 2, 3 & 4 passes through oven
Atmosphere Air & 1000ppm O2
Time after reflow 1 day, 1 week
January 26, 2016 Engineering Manual GC 10 Solder Paste 32
Before
Test
Operating Parameters Pin Testing
After
Test
7 6 5 4 3 2 1 0
300
250
200
150
100
50
0
Time (minutes)
T e
m p
e r
a t u
r e
( °
C )
217°C
Profile 1
Profile 2
Profile 3
Profile 4
Reflow Profiles
January 26, 2016 Engineering Manual GC 10 Solder Paste 33
1 2 3 4
1 r
eflo
w
2 r
eflow
s
3 r
eflow
s
Reflow Profile (% after 1000 tests)
Operating Parameters Pin Testing
4 r
eflow
s
100% 100% 100% 99.5%
100%
99.9%
99.9%
100%
100%
100% 100%
100%
99.6% 99.9%
98.9%
98.5%
7 6 5 4 3 2 1 0
300
250
200
150
100
50
0
Time (minutes)
T e
m p
e r
a t u
r e
( °
C ) 217°C
Profile 1
Profile 2
Profile 3
Profile 4
Reflow Profiles
Operating Parameters Pin Testing
January 26, 2016 Engineering Manual GC 10 Solder Paste 34
Reflow
ed in N
2
1 d
ay a
fter
reflow
1 w
eek a
fter
reflow
1 2 3 4
Reflow Profile (% after 1000 tests)
100%
99.6% 99.3% 99.8%
99.6% 99.8% 99.9%
100% 100% 100%
100%
100%
7 6 5 4 3 2 1 0
300
250
200
150
100
50
0
Time (minutes)
T e
m p
e r
a t u
r e
( °
C ) 217°C
Profile 1
Profile 2
Profile 3
Profile 4
Reflow Profiles
Operating Parameters Surface Finish
January 26, 2016 Engineering Manual GC 10 Solder Paste 35
OS
P F
inis
h
Silv
er
Fin
ish
T
in F
inis
h
1 2 3 4
Reflow Profile (0.5mm CSP56)
7 6 5 4 3 2 1 0
300
250
200
150
100
50
0
Time (minutes)
T e
m p
e r
a t u
r e
( °
C ) 217°C
Profile 1
Profile 2
Profile 3
Profile 4
Reflow Profiles
January 26, 2016 Engineering Manual GC 10 Solder Paste 36
Operating Parameters Surface Finish
OS
P F
inis
h
Silv
er
Fin
ish
T
in F
inis
h
1 2 3 4
Reflow Profile (0201)
7 6 5 4 3 2 1 0
300
250
200
150
100
50
0
Time (minutes)
T e
m p
e r
a t u
r e
( °
C ) 217°C
Profile 1
Profile 2
Profile 3
Profile 4
Reflow Profiles
January 26, 2016 Engineering Manual GC 10 Solder Paste 37
Operating Parameters Surface Finish
OS
P F
inis
h
Silv
er
Fin
ish
T
in F
inis
h
1 2 3 4
Reflow Profile (0402)
7 6 5 4 3 2 1 0
300
250
200
150
100
50
0
Time (minutes)
T e
m p
e r
a t u
r e
( °
C ) 217°C
Profile 1
Profile 2
Profile 3
Profile 4
Reflow Profiles
January 26, 2016 Engineering Manual GC 10 Solder Paste 38
Operating Parameters Surface Finish
OS
P F
inis
h
Silv
er
Fin
ish
T
in F
inis
h
1 2 3 4
Reflow Profile (6.5mm overprinted solder ball)
7 6 5 4 3 2 1 0
300
250
200
150
100
50
0
Time (minutes)
T e
m p
e r
a t u
r e
( °
C ) 217°C
Profile 1
Profile 2
Profile 3
Profile 4
Reflow Profiles
Reliability and Specification Testing Head in Pillow Test
Copper plate
Solder paste
Solder sphere
250+/-5˚C
Place a solder
sphere onto
printed paste
January 26, 2016 Engineering Manual GC 10 Solder Paste 39
First
250+/-5˚C
….. Initial 3sec 6 sec ….. 1st sphere 2nd sphere 3rd sphere Defect
• Print solder paste on a Cu plate, 0402 pad, stencil thickness
125µm.
• When the solder paste starts to melt, place a solder sphere
(SAC305, 0.76mm diameter) on the printed solder paste
• Place another sphere after 3sec, 6 sec, 9sec… until the
solder sphere no-longer coalesces
• Flux activity at elevated temperatures – up to 20% longer
than industry standard – helping to reduce HiP Co
mpe
titor
G
Compe
titor F
Compe
titor
E
Compe
titor D
Compe
titor C
Compe
titor B
Compe
titor
A
GC 10
14
12
10
8
6
4
2
0
Paste
Av
era
ge
Tim
e (
s)
Head in PillowTime to first defect
Standard Test Result
ANSI/
J-STD-004B
Cu Corrosion Pass
Cu Mirror Pass
Halogen Pass (no added halogen)
Surface Insulation Resistance Pass 6.0x1011 Ohms after 7days
Electromigration Pass 5.0x1010 Ohms after 21days
GC 10 Control
January 26, 2016 Engineering Manual GC 10 Solder Paste 40
GC 10 J-STD-004B classification ROL0
Reliability and Specification Testing J-STD- 004B
January 26, 2016 Engineering Manual GC 10 Solder Paste 41
Reliability and Specification Testing 3rd Party Testing
• SGS report for GC 10
• Sample reflowed flux residue
• Reference EN14582/IC Analysis
• To meet halogen free requirements
• Br<900ppm, Cl <900ppm, and combined <1500ppm
• Halogen – Fluorine - ND
• Halogen – Chorine - ND
• Halogen – Bromine – ND
• Halogen – Iodine – ND
GC 10 has no detectable halogen and is designated as halogen free
Reliability and Specification Testing IPC J-STD 004B
January 26, 2016 Engineering Manual GC 10 Solder Paste 42
6543210
250
200
150
100
50
Time (minutes)
Te
mp
era
ture
(°C
)
217°C
Profile 1
Profile 2
Reflow Profiles
6 5 4 3 2 1 0
250
200
150
100
50
Time (minutes)
T e m
p e r a
t u r e
( ° C
)
217°C
Profile 1
Profile 2
Reflow Profiles
January 26, 2016 Engineering Manual GC 10 Solder Paste 43
1. Performance Summary
2. Introduction: Properties, Features & Benefits
3. Operating Parameters
• Printing: Process Window
• Printing: Continuous and Abandon Time Testing
• Slump Testing
• Tack-Life Force
• Reflow Process Window
• Reflow Performance Testing
• Voiding Data
4. Reliability and Specification Testing
5. Operating Parameters: Storage
• Printing & Reflow Performance
6. Product Summary
Contents
January 26, 2016 Engineering Manual GC 10 Solder Paste 44
Operating Parameters: Storage Printing After Storage 12 months 25C • Print Capabilities
• Excellent print capability
after storage for 12 months @ 25C
• No knead cycle required after 2hrs abandon down to 0.22mm round apertures
0.8mm BGA – 0.18mm round apertures, 120m stencil thickness, 60mm/s,
Fast separation, 250mm squeegee, 10kg
0.18
mm dia circ
les
0.20
mm dia circ
les
0.22
mm dia circ
les
0.25
mm dia circ
les
0.28
mm dia circ
les
0.5m
m BGA
(0.27m
m ap)
0.5m
m CSP
(0.31m
m ap)
0.5m
m µBG
A (0
.35m
m ap)
0.8m
m BGA
(0.4mm ap)
6
5
4
3
2
1
0
Cp
k1.67 ref1.33 ref
Initial
1hr
2hr
2hr + knead
Variable
Abandon time after storage 1hr, 2hr, 2hr + 1 knead
Loctite GC 10 SAC305 T3 885V 12 months 25°C
January 26, 2016 Engineering Manual GC 10 Solder Paste 45
Operating Parameters: Storage Printing After Storage 12 months 25C • Print Capabilities
• Excellent print capability
after storage for 12 months @ 25C
• Excellent print performance after 1000 cycles down to 0.22mm round apertures
0.8mm BGA – 0.18mm round apertures, 120m stencil thickness, 60mm/s,
Fast separation, 250mm squeegee, 10kg
0.18
mm dia circ
les
0.20
mm dia circ
les
0.22
mm dia circ
les
0.25
mm dia circ
les
0.28
mm dia circ
les
0.5m
m BGA
(0.27m
m ap)
0.5m
m C
SP (0
.31m
m ap)
0.5m
m µBG
A (0.35m
m ap)
0.8m
m BGA
(0.4mm ap)
6
5
4
3
2
1
0
Cp
k1.33 ref1.67 ref
Initial
1,000 cycles
Variable
Continuous Print Stability after storage 1,000 cycles
Loctite GC 10 SAC305 T3 885V 12 months 25°C
January 26, 2016 Engineering Manual GC 10 Solder Paste 46
Operating Parameters: Storage Printing After Storage 12 months 25C • Transfer Efficiencies
• Excellent print capability
after storage for 12 months @ 25C
• No knead cycle required after 2hrs abandon
• Excellent print performance after 1000 cycles
0.8mm BGA – 0.5mm BGA, 120m stencil thickness, 60mm/s,
Fast separation, 250mm squeegee, 10kg
37332925211713951
160
120
80
40
0
Print No.
Tra
nsfe
r Eff
icie
ncy %
1.5 Vnom
0.5 Vnom
_X=98.9
_X=98.6
_X=97.5
_X=95.5
Initial 1 hr ab 2 hr ab 1000 prints
37332925211713951
160
120
80
40
0
Print No.
Tra
nsfe
r Eff
icie
ncy %
1.5 Vnom
0.5 Vnom
_X=90.9
_X=88.7
_X=88.3 _
X=86.0
Initial 1 hr ab 2 hr ab 1000 prints
37332925211713951
160
120
80
40
0
Print No.
Tra
nsfe
r Eff
icie
ncy %
1.5 Vnom
0.5 Vnom
_X=88.1
_X=87.3
_X=85.8
_X=84.8
Initial 1 hr ab 2 hr ab 1000 prints
37332925211713951
160
120
80
40
0
Print No.
Tra
nsfe
r Eff
icie
ncy %
1.5 Vnom
0.5 Vnom
_X=88.1
_X=85.6
_X=84.3
_X=85.7
Initial 1 hr ab 2 hr ab 1000 prints
1
0.8mm BGA (0.4mm apertures) 0.5mm BGA (0.34mm apertures)
0.5mm CSP (0.31mm apertures) 0.5mm BGA (0.27mm apertures)
January 26, 2016 Engineering Manual GC 10 Solder Paste 47
Operating Parameters: Storage Printing After Storage 12 months 25C • Transfer Efficiencies
• Excellent print capability
after storage for 12 months @ 25C
• No knead cycle required after 2hrs abandon
• Excellent print performance after 1000 cycles
0.25mm – 0.18mm round apertures, 120m stencil thickness, 60mm/s,
Fast separation, 250mm squeegee, 10kg
37332925211713951
160
120
80
40
0
Print no.
Tra
nsfe
r Eff
icie
ncy %
0.5 Vnom
1.5 Vnom
_X=96.5
_X=96.0
_X=94.5
_X=91.8
Initial 1 hr ab 2 hr ab 1000 prints
37332925211713951
160
120
80
40
0
Print No.
Tra
nsfe
r Eff
icie
ncy %
0.5 Vnom
1.5 Vnom
_X=101.8
_X=101.6
_X=100.6
_X=97.1
Initial 1 hr ab 2 hr ab 1000 prints
37332925211713951
160
120
80
40
0
Print no.
Tra
nsfe
r Eff
icie
ncy %
0.5 Vnom
1.5V nom
_X=108.4
_X=103.5
_X=101.9
_X=100.0
Initial 1 hr ab 2 hr ab 1000 prints
37332925211713951
160
120
80
40
0
Print No.
Tra
nsfe
r Eff
icie
ncy %
0.5 Vnom
1.5 Vnom
_X=102.0
_X=99.2
_X=98.5
_X=92.7
Initial 1 hr ab 2 hr ab 1000 prints
0.25mm dia round apertures 0.22mm dia round apertures
0.2mm dia round apertures 0.18mm dia round apertures
Operating Parameters: Storage Reflow After Storage to 12months 25C
6543210
300
250
200
150
100
50
0
Time (min)
Te
mp
era
ture
(°C
) 217°C
Profile 2
January 26, 2016 Engineering Manual GC 10 Solder Paste 48
Initial 1m 40°C 6m 25°C
0.5
mm
CS
P
02
01
04
02
After Paste storage
12m 25°C
January 26, 2016 Engineering Manual GC 10 Solder Paste 49
1. Performance Summary
2. Introduction: Properties, Features & Benefits
3. Operating Parameters
• Printing: Process Window
• Printing: Continuous and Abandon Time Testing
• Slump Testing
• Tack-Life Force
• Reflow Process Window
• Reflow Performance Testing
• Voiding Data
4. Reliability and Specification Testing
5. Operating Parameters: Storage
• Printing & Reflow Performance
6. Product Summary
Contents
January 26, 2016 Engineering Manual GC 10 Solder Paste 50
GC 10: Performance Summary
Flux
• Halogen-free flux: passes IC with pretreatment IPC-TM-650
2.3.34/EN14582
• Halogen-free flux classification: ANSI/J-STD-004 Rev. B for
a type ROL0 classification
Paste
• Suitable for printing up to 125mm/s (5”/s)
• Optimized for long hot soak reflow profiles
• Excellent coalescence in air & nitrogen atmosphere
• Excellent humidity resistance
• Excellent solderability on challenging surface finishes,
including CuNiZn
• Colourless residues for easy post-reflow inspection
• Long 12 month shelf-life when stored below 25C
Thank you!