![Page 1: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/1.jpg)
Sedimentation & filtration
Present by : Ngoc Tran Shamia salih
Hong Nguyen
![Page 2: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/2.jpg)
Sedimentation
Sedimentation is the natural process in which particles is carried to the bottom of a body of water and forms a solid layer
![Page 3: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/3.jpg)
Sedimentation
![Page 4: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/4.jpg)
Purpose
To measure the diameter of the particles
At fixed time intervals samples were taken from the suspension at different depth
![Page 5: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/5.jpg)
Industrial use
Water treatment
Food industry
In geology
Blood test
![Page 6: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/6.jpg)
Hydrometer Hydrometer is used to determine the
specific gravity or relative density of liquids
It is normally made of glass and it is usually weighted with mercury or lead shot to make it flow upright.
![Page 7: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/7.jpg)
Hydrometer
The operation of hydrometer is based on Archimedes’ principle
The lower the density of the substances, the further the hydrometer will sink
![Page 8: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/8.jpg)
Hydrometer
There are different types of hydrometer used based on the density of the liquid
variety of scales of hydrometer used depending on what you want to measure
![Page 9: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/9.jpg)
A Type of Hydrometer
![Page 10: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/10.jpg)
Procedure Measure a white solid powered (20g)
![Page 11: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/11.jpg)
Procedure Fill a 1000ml cylinder with 900ml of
water
![Page 12: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/12.jpg)
Procedure
Pour the white powder into the cylinder and shake it until the water and the powder are evenly distributed
![Page 13: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/13.jpg)
Procedure Then place the hydrometer into the
cylinder
![Page 14: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/14.jpg)
Procedure Measure the temperature
Then set the timer
Measure the height of the hydrometer at 0 seconds
And then start recording the height in time intervals until the height is constant
![Page 15: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/15.jpg)
![Page 16: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/16.jpg)
p
eB
amFforcebuoyantThe
:.1
2:.2
2pOD
D
AuCFforcedragThe
mgFforcegravityThe G :.3
Motion of sphere particle
DBG FFFdt
dumforceofSum :.4
m
uACg
m
uACgg
dt
du pD
p
ppD
p 2
)(
2.5
22
0.6 dt
dutakingbysettlingnalgravitatioFor
pfpD
ppt AC
mguvelocitySettlingTherfore
)(2
:
![Page 17: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/17.jpg)
If the particles are sphere of diameter Dp
At low Reynolds numbers the drag coefficient varies inversely with Re of particle
MOTION OF SPHERE PARTICLE
6:.1
3ppgDmparticleofMass
4:.2
2p
p
DAparticleofArea
fD
pfpt C
DguvelocitySettling
3
)(4:
18
)(3&
Re
242gD
uDuFC fptptDD
Re=G*D/µ)
![Page 18: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/18.jpg)
To calculate values of effective depth from the equation: L = L1 + 0.5(L2 -VB /A) or table 2
L1 : distance along the stem of the hydrometer from the top of the bulb to the mark for a hydrometer reading.
L2 : overall length of the hydrometer bulb (L2 = 14.0 cm)
V B :volume of hydrometer bulb (V B = 67.0 cm3)
A = cross-sectional area of sedimentation cylinder (A = 27.8 cm2)
To find the value correction factor α from table 1
To find K value from table 3
CALCULATION DIAMETER OF THE PARTICLE
![Page 19: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/19.jpg)
SG=2.53 α=1.024
%100)(
% 1
pM
bLP
![Page 20: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/20.jpg)
Reading L1=10 L=14.7
![Page 21: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/21.jpg)
At 220C & SG=2.53 K=0.01307
![Page 22: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/22.jpg)
CALCULATION & ANALYSIS
t
LKDp %100
)(% 1
pM
bLP
Temperature : 22 0C
Volume (ml) 900ml
Dry mass (gram) 20g
Concentration: 22%
SG : 2.53g/cm3
K (Table 3) 0.01307
a (Correction Factor Gs) 1.024
b (Correction Factor Temp)
4.4
T (min)Actual
reading Effective L D (mm) % P
0 20 13.04
1 18 13.37 0.05 69.63
2 17 13.53 0.04 64.51
3 15 13.86 0.03 54.27
4 14 14.02 0.03 49.15
5 12 14.34 0.02 38.91
6 11 14.51 0.02 33.79
7 10 14.67 0.02 28.67
8 9 14.83 0.02 23.55
9 8 15.00 0.02 18.43
10 7 15.16 0.02 13.31
11 6 15.32 0.02 8.19
12 6 15.32 0.02 8.19
![Page 23: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/23.jpg)
0 2 4 6 8 10 12 1411.50
12.00
12.50
13.00
13.50
14.00
14.50
15.00
15.50
16.00
f(x) = 0.897557613913866 ln(x) + 13.0126256633382R² = 0.9471580873965f(x) = 13.0591584665652 x^0.0624606743875519R² = 0.954148973226955
f(x) = 0.187002197802198 x + 13.2449142857143R² = 0.975805758487322
Height Vs. Time
Time (min)
L (
mm
)
![Page 24: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/24.jpg)
THEORY OF FILTRATION
Filtration is a very important step in the entire process of solid-liquid separation which can be sub-divided into four major stages
(1) Pretreatment
(2) Solids concentration
(3) Solids separation
(4) Post-treatment
![Page 25: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/25.jpg)
Types of filtration
Basically, there are two types of filtration (1) Depth filters - used for deep bed
filtration where particle deposition takes place inside the medium and cake deposition on the surface is undesirable.
(2) Surface filters – Used for cake filtration where the solids are deposited in the form of a cake on the up-stream side of a relatively thin filter medium.
![Page 26: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/26.jpg)
Rotary Filtration
Purpose: To separate water and solid
![Page 27: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/27.jpg)
A pre-coat is a layer of fine particular material added on to the filter septum before filtration to form a coating cake
![Page 28: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/28.jpg)
Rotary vacuum filter drum
+ consist of a drum rotating in a tub of liquid to be filtered.
+ pre –coat
+vacuum sucks liquid and solids onto the drum pre- coat surface .
+ the solids adhere to the outside of the drum
+ knife cut the solid out of drum .
The knife advances automatically as the surface is removed.
https://www.youtube.com/watch?v=4MFI-JFhBAU&feature=youtu.be
![Page 29: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/29.jpg)
The pump • Vacuum filtration usually
involves the use of a vacuum filter flask, a filter trap, a water pump
• the liquid is sucked down into the filter flask by the action of the water pump, and any excess liquid that overflows out of the filter flask is caught in the filter trap
![Page 30: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/30.jpg)
Procedure
Fill the tank with the mixture Turn on the valve for water go to the
pump Turn off all the valves which are drain
out the water from the tank, pump, and drum.
Turn on the main switch and all the buttons.
![Page 31: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/31.jpg)
Continue
Vacuum pump Agitator drive Filter drive Pre-coat drive Filtrate pump
![Page 32: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/32.jpg)
Valve for water come to the pump
(blue)valve for water drain out the tank after finish
(green )valve control the water go to the pump
Drain valve
Valves drain out all water after finish
![Page 33: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/33.jpg)
The filter-cake resistance
specific resistance the local porosity and permeability (or specific resistance), as well as the constitutive relations for the drag force between the phases and the solid matrix stress are required to obtain the numerical solution of the equations.
The medium resistance is a function of the medium itself and the material being filtered.
Resistance arises from the filter cloth, mesh, or bed, and to this is added the resistance of the filter cake as it accumulates.
The filter-cake resistance is obtained by multiplying the specific resistance of the filter cake, that is its resistance per unit thickness, by the thickness of the cake. R = µr(Lc + L)
![Page 34: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/34.jpg)
THE PROPERTIES OF A FILTER CAKE
The key properties of a filter cake are the cake porosity and permeability
The cake porosity (ε ) is a measure of the fluid capacity of the formed cake or the fraction of a porous medium available for fluid flow.
The cake permeability ( k ) is an indication of how easily the fluid can pass through its voids under an applied pressure gradient.
The extent of permeability is determined by the porosity of the medium and also the sizes of pores in its internal structure.
![Page 35: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/35.jpg)
θ: Angle comprising the sector immersed in the suspension
Dry cake
Wet cake
Batch filtration
Rotary filtration
![Page 36: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/36.jpg)
MASS BALANCE FOR THE SOLID IN THE CAKE
Solids accumulate in cake = Solids removed from suspension. LAԐ the volume of water in the cake
The volume of water contained in the LAԐ is much smaller than VF1 the volume of filtrate.
![Page 37: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/37.jpg)
PRESSURE DROP DURING CAKE FILTRATION
![Page 38: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/38.jpg)
![Page 39: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/39.jpg)
)2
(1 2
msck
mcsc
FF RPXtf
RtXAt
V
A
Q
PXtf
tXAt
V
A
Q sck
csc
FF
21
PXtf
tAt
XVX
A
QG SCk
CC
SFS
FF
21
Fraction Submergence of drum surface θ/2π : fk
Time cycle 2π/ω : tc
The time immersion period in each cycle : t= tc * fk
Rotation velocity ω (rad/s)
If the Rm is very small
Amount of solid
Rotary Vacuum Filtration
Filtration Flux
θ: Angle comprising the sector immersed in the suspension
![Page 40: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/40.jpg)
CONCLUSION
The diameter of the particle The concentration of the particles The cake permeability ( k ) is an indication of how easily the fluid can pass
through its voids under an applied pressure gradient
The cake porosity (ε ) is a measure of the fluid capacity of the formed cake or the fraction of a porous medium available for fluid flow Pressure drop
Total pressure drop: P drop cross filter & P drop due to filter medium
Specific cake resident: the local porosity and permeability
The speed of the drum rotation ω The filtrate flow rate
The amount of solid
PXtf
tXAt
V
A
Q sck
csc
FF
21
PXtf
tAt
XVX
A
QG SCk
CC
SFS
FF
21
![Page 41: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/41.jpg)
References
Unit Operations textbook Dr. Lo Dr. JangMr. Minh TranFriend: Codyhttp://www.engineering-resource.comhttp://www.filtration-andseparation.comhttp://www.engr.uky.edu
![Page 42: Sedimentation & filtration Present by : Ngoc Tran Shamia salih Hong Nguyen](https://reader030.vdocuments.mx/reader030/viewer/2022032612/56649efb5503460f94c0ea24/html5/thumbnails/42.jpg)
QUESTIONS