machinability assessment of titanium alloy ti-6al-4v for biomedical applications

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Machinability Assessment of Titanium Alloy Ti-6Al-4V for Biomedical Applications Ashwin Polishetty 1 , Guy Littlefair 2 and Praveen Kumar K 3 1 Deakin University, Geelong, Australia 2 Head, School of Engineering, Deakin University, Geelong, Australia 3 Department of Mechanical Engineering, VIT University, Vellore, India [email protected], [email protected], [email protected]. Keywords:Titanium alloy, Ti-6Al-4V, Machining, Casting, Femoral implant Abstract: Titanium alloy (Ti-6Al-4V) has a wide range of application in various fields of engineering. Titanium is mainly used to manufacture aerospace components like landing gear, fuselage, wings, engines etc. and biomedical components like hip joint, knee joint, dental implants etc. Titanium has outstanding material properties such as corrosion resistance, fatigue strength, tensile strength and a very good biocompatibility which makes this material very alluring for biomedical applications. Contrary, the machinability of the material is problematic because of the phase transformations and thus, titanium alloy is a challenge for machining operation. This research is a comparative analysis between the implants manufactured by traditional method of casting and machining. The femoral stem of the hip joint replacement is designed and the component is machined using a five-axis CNC machine.The machined component was subjected to surface roughness testing, tensile testing and bulk hardness testing. The values were compared with the values of titanium implants manufactured by casting. Introduction Pure titanium and titanium alloys are a commonly used material for design applications in aerospace and biomedical industries. They are used for knee joint, hip joint, dental, spinal cord replacement etc. They play a vital role in biomedical application because they have excellent specific strength, corrosion resistance, light weight, no allergic problems and have the best biocompatibility among the metallic biomaterials [1]. Biomaterials are artificial or natural materials, used in the making of structures or implants, to replace the lost or diseased biological structure to restore its form and function. Titanium has all the properties that a biomaterial should have such as excellent mechanical properties, biocompatible, high corrosion and wear resistance and osseointegration [2]. Pure titanium and titanium alloys are used in a wide range of applications which demands high level of reliable performance. Mechanical biocompatibility is an important factor since the research and development of beta type titanium alloys are increasing. There is a development of new titanium alloy with super elasticity. The young’s modulus of biomaterial is said to be always equal to that of bone. If the young’s modulus of biomaterial is greater than that of bone, bone resorption occurs. Titanium alloy Ti-6Al-4V the most widely used titanium alloy for biomedical application has low young’s modulus than that of stainless steel and Cobalt based alloys [3]. However, its young’s modulus is slightly greater than that of bone. Titanium alloys are classified as commercially pure titanium alloy, alpha beta titanium alloy and metastable beta titanium alloy [5]. Of these Ti-6Al-4V Advanced Materials Research Vols. 941-944 (2014) pp 1985-1990 Online available since 2014/Jun/06 at www.scientific.net © (2014) Trans Tech Publications, Switzerland doi:10.4028/www.scientific.net/AMR.941-944.1985 All rights reserved. No part of contents of this paper may be reproduced or transmitted in any form or by any means without the written permission of TTP, www.ttp.net. (ID: 128.184.132.53-13/06/14,04:33:41)

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Machinability Assessment of Titanium Alloy Ti-6Al-4V for Biomedical Applications

Ashwin Polishetty1, Guy Littlefair2 and Praveen Kumar K3 1Deakin University, Geelong, Australia

2Head, School of Engineering, Deakin University, Geelong, Australia

3Department of Mechanical Engineering, VIT University, Vellore, India

[email protected], [email protected], [email protected].

Keywords:Titanium alloy, Ti-6Al-4V, Machining, Casting, Femoral implant

Abstract: Titanium alloy (Ti-6Al-4V) has a wide range of application in various fields of

engineering. Titanium is mainly used to manufacture aerospace components like landing gear,

fuselage, wings, engines etc. and biomedical components like hip joint, knee joint, dental implants

etc. Titanium has outstanding material properties such as corrosion resistance, fatigue strength,

tensile strength and a very good biocompatibility which makes this material very alluring for

biomedical applications.

Contrary, the machinability of the material is problematic because of the phase transformations and

thus, titanium alloy is a challenge for machining operation. This research is a comparative analysis

between the implants manufactured by traditional method of casting and machining. The femoral

stem of the hip joint replacement is designed and the component is machined using a five-axis CNC

machine.The machined component was subjected to surface roughness testing, tensile testing and

bulk hardness testing. The values were compared with the values of titanium implants manufactured

by casting.

Introduction

Pure titanium and titanium alloys are a commonly used material for design applications in

aerospace and biomedical industries. They are used for knee joint, hip joint, dental, spinal cord

replacement etc. They play a vital role in biomedical application because they have excellent

specific strength, corrosion resistance, light weight, no allergic problems and have the best

biocompatibility among the metallic biomaterials [1]. Biomaterials are artificial or natural

materials, used in the making of structures or implants, to replace the lost or diseased biological

structure to restore its form and function.

Titanium has all the properties that a biomaterial should have such as excellent mechanical

properties, biocompatible, high corrosion and wear resistance and osseointegration [2]. Pure

titanium and titanium alloys are used in a wide range of applications which demands high level of

reliable performance.

Mechanical biocompatibility is an important factor since the research and development of beta type

titanium alloys are increasing. There is a development of new titanium alloy with super elasticity.

The young’s modulus of biomaterial is said to be always equal to that of bone. If the young’s

modulus of biomaterial is greater than that of bone, bone resorption occurs.

Titanium alloy Ti-6Al-4V the most widely used titanium alloy for biomedical application has low

young’s modulus than that of stainless steel and Cobalt based alloys [3]. However, its young’s

modulus is slightly greater than that of bone. Titanium alloys are classified as commercially pure

titanium alloy, alpha beta titanium alloy and metastable beta titanium alloy [5]. Of these Ti-6Al-4V

Advanced Materials Research Vols. 941-944 (2014) pp 1985-1990Online available since 2014/Jun/06 at www.scientific.net© (2014) Trans Tech Publications, Switzerlanddoi:10.4028/www.scientific.net/AMR.941-944.1985

All rights reserved. No part of contents of this paper may be reproduced or transmitted in any form or by any means without the written permission of TTP,www.ttp.net. (ID: 128.184.132.53-13/06/14,04:33:41)

is the commonly used biomaterial for medical implants and is known as the “work horse” of

titanium industry. They have an enhanced biocompatibility, reduced elastic modulus, superior strain

controlled and notch fatigue resistance. The poor shear strength and wear resistance have

nevertheless limited their biomedical use [3]. Titanium alloy Ti-6Al-4V are not only used in

biomedical application, they are used in direct manufacturing of parts and prototype for racing and

aerospace industry, in marine application, gas turbines etc. The main limitation of pure titanium is

its high cost, rarely found metal and has phase transformation problem due to which its production

cost is increased.

Machinability is defined as the ease or the difficulty with which a material can be machined under a

given set of cutting conditions including cutting speed, feed and depth of cut. Machinability of a

work material is accessed in terms of four factors: tool life, cutting forces, power requirements and

surface finish [6]. Titanium machining has hindered a more wide application due to its relatively

high cost. To minimize the inherent cost problems, successful application must take advantage of

the special features and characteristics of titanium. The machinability of titanium and titanium

alloys is limited by some characteristics and is considered difficult, due to its relatively high tensile

strength, low ductile yield, 50% lower modulus of elasticity and approximately 80% lower thermal

conductivity than that of steel [7]. In the tool contact zones high pressures and temperatures occur.

At higher temperatures caused by friction the titanium becomes more chemically reactive and there

is a tendency for titanium to “weld” to tool bits during machining operation. During machining of

titanium alloys the cutting depth should be large, cutting speed should be from 12 to 80 m/min and

approximately 50% lower when high speed steel tools are used. The heat generated should be

removed by a large volume of cooling lubricants. Chlorinated cutting fluids should not be used

because titanium can be susceptible to stress corrosion failures in the presence of chlorine.

CBN/PCBN and Poly Crystalline Diamond (PCD) tools are employed at high speed machining of

titanium alloy [8].

Experimental Design

The objective of the study is to investigate the surface roughness, tensile strength and material

removal rate for the femoral stem machined in 5-axis machine using titanium alloy Ti-6Al-

4V.Machining of titanium alloy Ti-6Al-4V for femoral stem of a hip joint replacement was done

using a five axis machine (Spinner U-620) as shown in fig.1 and fig.2.

Fig. 1 Face milling operation Fig. 2 End milling operation

The implant profile was designed using solidworks software. The required G-code was given tothe

five axis machine for the necessary operation to be performed. Once the coding is done the design

was stimulated on the screen of the five axis machine. After placing the workpiece in the 5-axis

machine the probe was used to set the origin for the cutting tool before the machining operation.

The parameters that were used for machining operation are listed below in the table 1.

1986 Materials and Processes Technologies V

Table 1 Face milling and end milling operation parameters

Cutting

Tool

Spindle

Speed(rpm)

Cutting

SpeedVc(m/min)

Overall

FeedF

Feed per

ToothFz(mm/rev)

Table

Feed(mm/min)

Depth of

Cut

(Axial)mm

Depth of cut

(Radial)mm

50mm

diameter

face milling

cutter

2000 314 0.4

0.04

800 0.5 20

16mm

diameter solid

carbide

end

2000 100 0.2 0.05 400 3 6.4

8mm

diameter

solid carbide

end

3000 75.3 0.05 0.01 150 0.2 0.7

The surface roughness, tensile strength and material removal rate of the machined titanium alloy Ti-

6Al-4V sample (as shown in fig.3) are determined. The surface roughness test is carried out in

Taylor Hobson machine and the surface roughness of the femoral stem is determined using ultra

software. The tensile test is carried out in Instron machine of maximum capacity 30KN and the

UTS, yield strength and elongation (%) are determined.

Fig. 3 Machined femoral stem in a 5-axis machine

Results and discussion

The results obtained from the experiments are discussed in this section using graphs and tables.

Surface Roughness Test

The surface roughness of face milling operation and end milling operation is shown in fig.4.

Advanced Materials Research Vols. 941-944 1987

Fig. 4Surface roughness comparisons for face and end milling operations

Surface roughness of the machined surface depends upon the feed rate, cutting speed and depth of

cut. The surface finish is directly proportional to the feed rate and inversely proportional to cutting

speed and depth of cut. In casting process there are residual stress layers that are formed due to

heating of the metal during casting. Due to the presence of air gaps in casting the surface of the

casted femoral stem is rough. Therefore the surface roughness of the casted femoral is very high.

The machining operation of titanium alloy Ti-6Al-4V obtained an average surface roughness of

0.3420µm which is lower than that obtained in casting process. As the cutting speed used for the

machining operation increases from 75m/min to 314m/min, the surface roughness of the machined

titanium alloy decreases. As the surface roughness decreases the texture of the machined surface is

fine which is suitable for the implant.

Tensile test

The tensile test was performed on the titanium alloy Ti-6Al-4V. The UTS, yield strength and

elongation (%) are determined and shown in table 4.

Table 4 Tensile test values for titanium alloy Ti-6Al-4V

Properties Ti-6Al-4V

Ultimate tensile strength (MPa) 872

Yield strength (MPa) 968

Elongation (%) 5

The titanium alloy Ti-6Al-4V has higher elastic limit as it is visible from the yield strength value.

This necessarily means that it can handle higher loads before it deforms plastically. The load

bearing capacity of the alloy is higher hence there is no shape change in stress-strain curve of the

material for higher applied loads. Hence, this material is used for applications where high tensile

forces are applied. There is very little work hardening in the material. The curve droops down once

yielding starts which indicates the softening of material once plastic deformation begins. It can be

considered that the material is safe only till its elastic limit is reached. The applicability is not clear

for loads between yield strength and the UTS. Hence, it is beneficial to verify the properties after

machining or necessary heat treatments. As the loads in the human body are lesser than the elastic

limit of titanium alloy Ti-6Al-4V, it can be used effectively for making hip joint implants. Till the

elastic limit is reached there can be volume changes in the material but no shape changes since the

0

0.05

0.1

0.15

0.2

0.25

0.3

0.35

0.4

0.45

Face Milling End Milling

Surf

ace

Ro

ugh

ne

ss µ

m

Trail 1

Trail 2

Trail 3

1988 Materials and Processes Technologies V

deviatoric component is zero till that limit. The loads on the material should be clearly analysed

before its application.

Material Removal Rate

The material removal rate for face milling operation was 8cm3/min and for end milling operation

was 7.7cm3/min. These material removal rates are low to machine a titanium alloy but it is effective

because the thickness of the femoral stem was 3mm. These material removal rates are good for a

component with small thickness. With the material removal rate of 8cm3/min and 7.7cm3/min, the

femoral stem was machined in 10min. In casting process to cast a femoral stem it takes 2 to 3 hrs.

After casting is done the casted femoral stem has to be machined to get a fine surface finish. The

time consumed to manufacture a femoral stem in casting is more as compared to machining process.

With the same parameters, more than 18 femoral stems can be machined in a five axis machine in 3

hrs.

Conclusion

As discussed in the above chapters the following conclusions are made,

1. The ultimate tensile strength and yield strength of the machined femoral stem are higher so that

they can withstand high tensile forces acting on them. Titanium alloy Ti-6Al-4V has high UTS

and yield strength as compared to other biomaterials like stainless steel, Co-Cr etc. Hence,

titanium alloy Ti-6Al-4V is the best choice of biomaterial for medical implants.

2. The surface roughness of the femoral stem decreases as the cutting speed is increased. The

surface roughness of the machined titanium alloy is low as compared to the casted titanium

alloy. The surface texture of the machined femoral stem is fine as that of a bone. It can

withstand high stresses from the adjacent bones.

3. The machined titanium alloy is harder than the normal titanium alloy. The hardness of the

titanium alloy Ti-6Al-4V is 29 HRC which is harder than the bone. It has the capacity to

withstand high stresses from the adjacent bones.

4. The obtained material removal rate is low for a machining process but it is effective to machine

a component with a thickness of 3mm.

5. The time taken to manufacture a femoral stem is short in machining process as compared to

casting process.

Future work

Due to the limited scope of this project and best use of the available resources, tests such as wear

resistance and corrosion resistance are planned under future work.

The values of the test will be taken and compared with the values of the femoral stem manufactured

by casting process. The other components of hip joint such as acetabular cup, the head of femoral

stem can be machined using five axis machines and the articular interface made out of plastic can

be assembled to make a hip joint.

References

[1] Mitsuo Niinomi, “Recent research and development in titanium alloys for biomedical

application and health care goods”, Science and technology of advanced materials, 2008.

[2] 2.M. Geetha, A. K. Singh, R. Asokamani, A. K. Gogia, “Ti based biomaterials, the ultimate

choice for orthopaedic implants”, Progress in material science, 2009.

[3] Marc Long, H. J. Rack, “Titanium alloys in total joint replacement- a material science

perspective”, Biomaterials, 1998.

Advanced Materials Research Vols. 941-944 1989

[4] Carlos Oldani, Alejandro Dominguez, “Ti as biomaterial for implants”, Biomaterials, 2007.

[5] H.J.Rack, J.I.Qazi, “Titanium alloys for biomedical application”, Material science and

engineering, 2005.

[6] Ahmet Hascalik, Farnaz Nourbakhsh, K. P. Rajurkar, A.P Malshe, “Wire electro discharge

machining of titanium alloy”, Biomanufacturing, 2013.

[7] Tengvall P, Lundstrom I (1992), “Physico chemical consideration of titanium as a biomaterial,

Clin materials”, vol-9: 115-134.

[8] Burhanuddin Y, Che Haron C.H, Ghani J A, Ariffin A K, Ibrahim G A, Yasir A, El-Maghribi N

H (2008), “The effects of CBN cutting tool grades on the tool life and wear mechanism when

dry cutting of titanium alloy”, Asian Int. Jour of science and technology, pg:105-110.

[9] Matej Balazic, Janez Kopac, “Machining of titanium alloy for biomedical application”, Journal

of mechanical engineering, 2010.

[10] Mrudula. S, Kulkarni, S. R. Sathe, “Experimental determination of material properties of

cortical cadaveric femur bone”, Journal of biomechanics, 2008.

[11] Luc a Cristofolini, Marco Viceconti, Angelo Cappello, “Mechanical validation of whole bone

composite femur models”, Journal of biomechanics, 1996.

[12] A. Rohlmann, U. Mossner, G. Bergmann, “Finite element analysis and experimental

investigation of stress in a femur bone”, Journal of biomedical engineering, 1982.

[13] B. R. Rawal, Rahul Ribeiro, Rajesh Malhotra, Naresh Bhatnagar, “Design and manufacturing

of femoral stem for Indian population”, Journal of manufacturing process, 2012.

[14] J. A. Simoes, A.T. Marques, “Design of a composite hip femoral prosthesis”, Material and

design, 2005.

1990 Materials and Processes Technologies V

Materials and Processes Technologies V 10.4028/www.scientific.net/AMR.941-944 Machinability Assessment of Titanium Alloy Ti-6Al-4V for Biomedical Applications 10.4028/www.scientific.net/AMR.941-944.1985