fgolder - florida department of environmental protection

Golder Associqles lnc.

9428 Boymeodows Rood, Suite 400Jocksonville, FL USA 3225óTeleþhone (904) 3ó3-3430Fox (904) 3ó3-3445www.golder,com

FGolderAssociates

April T, 2008 993-3902.G

Veolia ES Solid Waste, Inc.5111 South Pine AvenueSuite MOcala,Florida 34480

Attention: Mr. Jeff Inglehart

RE: SEMI-A¡INUAL MONITORING REPORT NUMBER 19

FOR THE PERTOD OF JANUARY 1, 2008 - JUNE 30, 2008

VEOLIA CYPRESS ACRES LAIIDFILL, INC.ocALA, FLORIDA\ryACS NUMBER 2I25I

Dear Mr. lnglehart:

Golder Assôciates Inc. (Golder) is pleased to present this report summarizing the nineteenth

period (January 1, 2008 to June 30, 2008) of operations for the Cypress Acres C&D Landfill.This Semi-Annual Report is submitted in compliance with the monitoring and reporting

requirements of Permit Number 5042-0019903-006. Two additional certified original reports

have been submitted directly to the Florida Department of Environmental Protection and the

Marion County Solid Waste Department. In addition, one certified original report has been

forwarded to Joy Bryant, the site Representative, for inclusion in the operating record. Included

in this report are the results of sampling activities conducted and evaluations of the groundwater

quality and elevation data collected during January 2008, which represent the nineteenth

semi-annual operating period for the facility under the referenced permit.

We trust this report meets with your satisfaction. If you have any questions or comments

regarding this report, please do not hesitate to call.

Sincerely,

GOLDER ASSOCIATES INC.

Project Hydrogeologist

Attachments

OFFICES ACROSS AFRICA, ASIA, AUSTRALIA, EUROPE, NORTH AMERICA AND SOUTH AMERICA

Golder Associoles lnc.

9428 Boymeqdows Rood, Suite 400Jqcksonville. FL USA 3225óTelephone (904) 3ó3-3430Fox (904) 363-3445www.golder,com

GolderAssociates

R.EPORT ON

SEMI-AI\¡IUAL GROU}IDWATER MONITORINGREPORT i\UMBER 19 FOR THE PERIOD OF

JAIIUARY 1,2008 - JrINE 30,2008VEOLIA CYPRESS ACRES LA}IDFILL. INC.

OCALA, FLORIDAWACS NUMBER 2I25I

Submitted to:

VEOLIA ES SOLID WASTE, INC.5111 SOUTH PINEAI/ENUE, SUITE M

OCALA, FLONDA 34480

Submitted bv:

Golder Associates Inc.9428 Brymeqdows Road, Suite 400

Jacksonville, Florida 3 22 5 6

DISTRIBUTION:

2 Copies Veolia ES Solid Waste,Inc.1 Copy Florida Department of Environmental ProtectionI Copy Marion County Solid Waste Department2 Copies Golder Associates Inc.

April2008 993-3902.G


Golder Associqles lnc.

9428 Boymeodows Rood, Suite 400Jocksonville, FL USA 3225óTeleþhone (904) 3ó3-3430Fox (904) 3ó3-3445www.golder,com

FGolderAssociates

April T, 2008 993-3902.G

Veolia ES Solid Waste, Inc.5111 South Pine AvenueSuite MOcala,Florida 34480

Attention: Mr. Jeff Inglehart

RE: SEMI-A¡INUAL MONITORING REPORT NUMBER 19

FOR THE PERTOD OF JANUARY 1, 2008 - JUNE 30, 2008

VEOLIA CYPRESS ACRES LAIIDFILL, INC.ocALA, FLORIDA\ryACS NUMBER 2I25I

Dear Mr. lnglehart:

Golder Assôciates Inc. (Golder) is pleased to present this report summarizing the nineteenth

period (January 1, 2008 to June 30, 2008) of operations for the Cypress Acres C&D Landfill.This Semi-Annual Report is submitted in compliance with the monitoring and reporting

requirements of Permit Number 5042-0019903-006. Two additional certified original reports

have been submitted directly to the Florida Department of Environmental Protection and the

Marion County Solid Waste Department. In addition, one certified original report has been

forwarded to Joy Bryant, the site Representative, for inclusion in the operating record. Included

in this report are the results of sampling activities conducted and evaluations of the groundwater

quality and elevation data collected during January 2008, which represent the nineteenth

semi-annual operating period for the facility under the referenced permit.

We trust this report meets with your satisfaction. If you have any questions or comments

regarding this report, please do not hesitate to call.

Sincerely,


Project Hydrogeologist

Attachments


April2008 l- 993-3902.G

TABLE OF CONTENTS

Cover Letter

Table of Contents

SECTION

Table ITable2Table 3

Table 4

Figure IFigure 2

AppendixAAppendix BAppendix CAppendixDAppendixEAppendixF

I

PAGE

1.0

2.0

3.0

4.0

5.0

MONITORING PROCEDURES....... ................2

2.1 Semi-Annual Groundwater Monitoring Program "'.'..'...22.2 Monitoring Well Installation ..,........ ......."'.' 42.3 Piezometer Installation .'.'."..'... 5

MONITORING PROGRAM RESULTS............. ........,.......6

3.1 Semi-Annual Groundwater Monitoring Results ..'.'.....'.'.63.2 Quality Control ...'... 8

CONCLUSIONS AND

IN ORDERFOLLOWING

PAGE 12

LIST OF TABLES

Groundwater Monitoring Sites

Summary of Groundwater Elevation Data-January 30, 2008

Summary of Purge Volumes and Field Parameters-January 2001 to January 2008

Summary of Detected Parameters in Groundwater-EventNo. 19

January 28, 29, &. 30, 2008

LIST OF FIGURES

Potentiometric Map of the Upper Floridan Aquifer - January 30, 2008

Local Groundwater Flow Direction (MW-3) - January 30, 2008

LIST OF'APPEI\DICES

Groundwater Collection and Instrument Calibration Field Records

Monitoring Well and Piezometer Installation LogsHydraulic Gradient CalculationsLaboratory Analytical Reports and Chain of Custody FormsFDEP Parameter Monitoring Report Forms (Form 62-522.900(2))DER Form 62-522.900(2)

Golder Associates

April2008 -1- 993-3902.G

1.0 INTRODUCTION

The Veolia Cypress Acres Landfill, Inc. (the Site) is a permitted C&D disposal and

recycling facility located in Ocala, Marion County, Florida at the location shown on Figure l.

The Veolia Cypress Acres Landfill, Inc., formerly known as the Sandman Trucking Corporation

C&D Landf,rll, is presently owned and operated by Veolia ES Solid Waste, Inc. (Veolia)

(formerly Onyx Waste Services Southeast, Inc.) under Florida Department of Environmental

Protection (FDEP) Operation Permit Number SO42-0019903-006, issued on November 72,2003'

The facility consists of approximately 36.77 acres of disposal area within a property boundary of

approximately 48.6 acres. Golder Associates lnc. (Golder) has been retained to perform

groundwater monitorin g at the Site in accordance with Specific Condition 12 of the referenced

permit. Specific Condition 12 includes requirements set forth in the Monitoring Plan

Implementation Schedule (MPIS), which is attached to the permit as Exhibit 1. To facilitate

information tracking, the facility has been issued Water Assurance Compliance System (WACS)

Number 2125I by FDEP, This report presents the findings of the nineteenth semi-annual

groundwater monitoring event, which was performed in January 2008 in accordance with the

referenced permit.

Golder Associates

April2008 -2- 993-3902.G

2.0

2.1

MONITORING PROCEDURES

Semi-Annual Groundwater Monitoring Program

In accordance with the referenced permit, the monitoring system on-site consists of

six groundwater quality monitoring wells (MW-2, \/I\N-4, MW-5, MW-6, MW-7, and MW-8)

and two additional groundwater elevation monitoring points (MW-l and MW-3), as shown on

Figure 1. A list of monitoring points, WACS identification numbers, and monitoring well types

is presented in Table 1. The nineteenth semi-annual groundwater monitoring event was

performed from January 28 to 30,2008, in accordance with the MPIS. A summary of the

groundwater sampling procedures is presented in the following discussion.

Prior to purging and sampling activities, all monitoring wells were opened and groundwater

levels were allowed to equilibrate to atmospheric conditions. Subsequently, the depth to

groundwater was measured to within 0.01-feet relative to the top of well casing. The purpose of

the groundwater level measurements was to obtain data and calculate approximate groundwater

table elevations at each well to evaluate the general direction of groundwater flow in the upper

surficial aquifer (the upper Floridan aquifer) underlying the study site. A summary of

groundwater elevation data collected on January 30, 2008 is presented inTable2.

After measurement of groundwater levels, groundwater samples were collected for

laboratory analysis from monitoring wells MW-2, MW-4, MW-5, MW-6, MW-7, MW-8,

MW-8R, and MW-9D. Note that, in accordance with recommendations presented in the

October 2005 quarterly monitoring report, replacement well MW-8R was installed immediately

south of Mw-8. This replacement well was installed to verif' water quality trends observed in

sample results for MW-8. In addition, monitoring well MW-9D was installed on January 28 and

29, 2008. During the January 2008 event, decontamination and sampling procedures were

performed in accordance with FDEP's Standard Operating Procedures (DEP-SOP-001/01) for

groundwater sampling (FS-2200). Prior to introducing equipment into the wells, purging and

sampling equipment was decontaminated using a Liquinox and tap-water wash, followed by a

tap-water rinse, with a final deionized (DI) water rinse. Prior to sample collection, each well was

purged using a QED Sample Pro Bladder Pump. Given that the well screens were completely

submerged, the equipment volume purging procedure was used, as per FS-2200. Purge water was

containerized within 55-gallon drums, The purge water was sampled for mercury to determine

proper disposal. During the purging of each well, the temperature, pH, specific conductance,

dissolved oxygen, and turbidity were measured from the discharged groundwater and recorded on

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April2008 -3- 993-3902.G

field groundwater collection records. Groundwater samples v/ere collected following

stabilization of temperature, pH, specific conductance, dissolved oxygen, turbidity, and depth to

groundwater, In addition, purging activities were continued until the measured turbidity was less

than l0 Nephelometric Turbidity Units (NTUÐ. Groundwater sample collection records and

daily equipment calibration records are presented in Appendix A. A summary of purge volumes

and freld parameter measurements is provided in Table 3.

In accordance with the MPIS, groundwater samples were collected from MW-2, MW-4, MW-5,

MW-6, MW-7, and MW-8 for the nineteenth monitoring event (Event No. 19). The samples

were analyzed for: volatile organic compounds (VOCs) listed on Environmental Protection

Agency (EPA) Methods 601 and 602 (using EPA Method 8260B); total aluminum, total arsenic,

total cadmium, total chromium, total iron, total lead, and total sodium by EPA Method 6010; total

mercury by EPA Method 7470; ammonia by EPA Method 350.1; chlorides by EPA

Method 325.2;nitrate by EPA Method 353.2; total phenols by EPA Method 420.1; sulfate by

EPA Method 375.4, and total dissolved solids (TDS) by EPA Method 160.1. As per the

recommendations of the October 2005 monitoring event, one additional sample was collected

from replacement well MW-8R and analyzed for mercury. One additional sample was collected

from each of MW-8 and MW-8R for filtered mercury analysis. In addition, as per the

recommendations of the Second Response to Comments (January 7, 2008), a deep monitoring

well (MW-9D) was installed and sampled for total and filtered mercury. The samples were

collected directly from the bladder pump effluent.

The sample containers were identified with a unique sample number, preserved as required, and

placed in a cooler to be chilled to approximately 4oC. At the completion of groundwater

sampling, the cooler(s) containing samples were shipped via overnight courier to

TestAmerica,Inc. (formerly Severn Trent Laboratories, Inc. [STL]) in Tallahassee, Florida, a

NElAC-accredited laboratory, for the required analyses.

In addition to the groundwater samples referenced above, QA/QC samples were collected and

submitted to the laboratory to provide assurance that the collection and handling procedures did

not conhibute to potential detections of targeted parameters. A trip blank (labeled Trip Blank),

provided by TestAmerica Inc,, accompanied the VOC samples from the time of sample

collection until arrival at the laboratory and was analyzed for parameters included in EPA

Methods 601 and 602. One equipment blank was collected (labeled EB-01) and submitted to the

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April2008 4 993-3902.G

laboratory to be analyzed for all of the targeted parameters. As indicated above, a mercury

sample was also collected from the containerized purge water to determine proper disposal.

2.2 Monitoring \ilell Installation

In addition to the scope of work presented above, as per the recommendations in the

January7,2008 Second Response to Comments, a deep monitoring well was installed

in the vicinity of MW8À4W-8R. With the exception of wells MW-8 and MW-8R

(installedtoapproximately 66 feet below ground surface [bgs] each), the remaining site

wells were generally installed in a highly weathered to semi-competent limestone, It was

therefore assumed that limestone would be encountered at this location at a depth of between

70 feet and 85 feet bgs. Standard penetrations tests (SPTs) were performed beginning at a depth

of 70 feet bgs to locate the limestone interface and document the lithology. SPTs indicated a

gradual increase in limestone content and competency from a silty weathered limestone

(at approximafely 70 to 74 feet bgs) to more a competent limestone and sandy limestone

(at approximately 80 to 91 feet bgs). Acid testing confirmed a matrix dominant limestone. As a

result, a 6-inch diameter surface casing was installed from ground surface to within the partially

weathered limestone (approximately 85 feet bgs) and grouted in place. The following day,

drilling continued with the collection of SPTs from 87 feet to 93 feet bgs. Drill mud circulation

was lost several times between 89 and 93 feet bgs. In addition, blow counts were recorded at

greater than 85 blows per foot, SPT recovery was poor, but indicated an increase in limestone

competency with depth, Slow advancement from 9l to 93 feet bgs (approximately 2 hours)

coupled with very high blow counts resulted in the determination to set the well to 93 feet bgs.

The monitoring well was set using a 2-inch diameter, 5-foot, 0,010-inch slotted PVC screen. A

filter pack consisting of 20130-grade silica sand was installed via gravity from 93 feet to 86 feet

bgs, and a2-foot thick bentonite seal was placed from 86 feet to 84 feet bgs. The remaining

annular space was filled with Type VII Portland cement, installed via tremie pipe from the surface

to the specified interval. The monitoring well was completed with a2-footby 2-foot concrete

pad, protective aluminum outer casing, and two steel bollards to protect the outer casing from

vehicular damage.

The monitoring well was developed using a submersible pump operating for approximately

50 minutes at a rate of approximately 1 gallon per minute (gpm). Development ceased when

the purge water contained a nominal content of silVclay based on visual observations. Purge

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April2008 -5- 993-3902.G

water was contained on-site in a 55-gallon drum pending the laboratory results. The locations,

tops-of-casing and ground elevations of MW-9D and MW-8R \ iere surveyed by Central Florida

Surveying and Mapping (CFSM), In addition, to confirm previous survey data by CFSM, top of

casing elevations for wells MW-3, MW-4, and MW-8 were resurveyed. The well installation log

for MW-9D is included in Appendix B, and the location is shown on Figure 1.

2.3 Piezometer Installation

To determine the local groundwater flow direction in the vicinity of MW-3, three piezometers

were installed using a direct push technology (DPT) rig. Piezometers were installed east and

south of MW-3, along the edge of waste, and north of MW-3, at the northwest corner propeúy

boundary. Figure 2 shows the locations of the piezometers relative to MW-3 and the edge of

waste. The 1-inch diameter piezometers were installed to a depth of approximately 50 feet bgs

each (approximate depth of MW-3). The piezometers were capped and a small hole was drilled

on the side of each, to allow for equilibration. Two days following installation, the depth to the

water table \¡/as measured for each piezometer by Golder and the top-of-casing and ground

elevations were surveyed by CFSM. The piezometer installation logs in included in Appendix B

and the locations are indicated in Fieure 2.

The January 7, 2008 Second Response to Comments also recommended the installation of

additional piezometers north of the landfill between MW-2 and MW-3, intended to represent an

appropriate background groundwater sampling point more representative of the MW-8/ì4W-8R

lithology. DPT borings were to be advanced on the adjoining property to the north. Properfy

access was not granted, and therefore this portion of the off-site investigation could not

be completed.

Golder Associates

April2008 6 993-3902.G

3.0

3.1

MONITORING PROGRAM RESULTS

Semi-Annual Groundwater Monitoring Results

Groundwater elevations were calculated by subtracting groundwater level measurements

collected on January 30, 2008 from the top-of-casing elevations (as determined by a survey

performed by CFSM in May 1999), which are referenced to the National Geodetic Vertical

Datum of 1929 (NGVD). The top of casing for monitoring well MW-8R was measured in

January 2006 by Golder personnel, using the surveyed elevations of MW-8 and MW4 as

reference. As part of Event No. 17, Golder measured the top of casing of MW-8 and MW-8R,

using MW-3 and MW-4 as references. During the January 2008 event, CFSM surveyed wells

MW-8R and MW-9D, Minor differences in groundwater elevations for MW-8 and MW-8R have

consistently been recorded since MW-8R was installed, As a result, MW-8, MW-3, and MW-4

were also resurveyed to confirm the 7999 data. A comparison of the previous top-of-casing

elevation data to the current data indicated no change for MW-4, a minor increase for

MW-8 (0.01 feet), and a reduction of 0.21 feet for MW-3. The concrete pad and

well construction materials for MW-3 were in good condition. One potential explanation for the

change in top-of-casing elevations is the wet conditions the vicinity of MW-3 coupled with the

proximity to railroad tracks. Specifically, the upper portion of the well materials may have

settled over the years after installation due to periodic ground saturation and ground

vibration resulting from routine train traffic.

As shown on Figure l, the shallow groundwater underlying the site flows toward the southwest

on the western portion of site, changing to the southerly direction on the central portion of the

site, and the south-southeasterly direction on the eastern portion of the site. The groundwater

elevation decreases approximately 0.41 feet over a distance of approximately 1,330 feet, which

indicates a horizontal hydraulic gradient of approximately 3.1 x 10-a feelfoot, consistent with

historic data for the site. The vertical gradient measured between MW-9D and the adjacent well

(MW-SR) was approximately 6.0 x 10-3 feelfoot downward. The hydraulic gradient calculations

are included in Appendix C. A summary of groundwater elevation data is presented in Table 2.

In an electronic mail message dated November 13, 2007, FDEP indicated that, due to the

potential for radial flow from the landfill mound influencing the local flow direction of MW-3,

FDEP did not consider MW-3 as representative of background conditions at that time. It is noted

that Golder had previously indicated and still maintains that the MW-3 location is representative

of background groundwater quality conditions, To funher evaluate the MW-3 location, three

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April2008 -7 - 993-3902.G

piezometers were installed around MW-3 at locations shown on Figure 2, including two at the

edge of the landfill mound. Water levels were measured two days following installation and

subtracted from the top-of-casing elevation data provided by CFSM. The results indicate a

relatively flat gradient (consistent with the upper Floridan aquifer at the site) in the immediate

vicinþ of MW-3 with a gentle downward flow toward the southeast, directly toward the landfill.

The data demonstrate that MW-3 is hydraulically upgradient of the landfill. The groundwater

flow direction is shown in Fieure 2.

In January 2008, groundwater samples were collected from the eight groundwater monitoring

wells (MW-z, MW-4, MW-5, MW-6, MW-7, MW-8, MW-8R, and MW-9D). Pursuant to

recommendations in the October 2005 and previous semi-annual reports, a groundwater sample

was collected from replacement monitoring well MW-8R for mercury analysis. Pursuant to

recommendations in the January 2008 Second Response to Comments, a groundwater sample was

collected from deep monitoring well MW-9D for mercury analysis. The locations of monitoring

wells are shown on Figure 1 and a summary of laboratory detected parameters for groundwater

samples and QA/QC samples collected in January 2008 is presented in Table 4. Copies of the

laboratory analytical reports are provided in Appendix D. In addition, Parameter Monitoring

Reports (FDEP Form Number 62-522.900(2)) are included as Appendix E, as required by the

MPIS, Electronic copies of the Parameter Monitoring Reports are provided in Microsoft Excel

format on the diskette enclosed.

There were no detections of VOCs, ammonia, nitrate, chloride, sulfate, TDS, total phenols,

aluminum, arsenic, cadmium, chromium, iron, or sodium concentrations exceeding applicable

drinking water standards for Event No. 19.

Mercury has been detected above the Florida Primary Drinking Water Maximum Contaminant

Level (PMCL) in the samples collected from MW-8 since January 2004 (the first date this well

was sampled). The laboratory analytical results for January 2008 indicated mercury detections at

concentrations of 0.0033 milligrams per liter (mgll) for MW-8 and 0.0055 mg/l for MW-8R.

The results exceeded the PMCL of 0.002 mgll. The samples were associated with pH values of

4.83 Standard Units (S.U.) for MW-8 and 4.94 S.U, for MW-8R. Although these pH results

are below the Florida Secondary Drinking Water Maximum Contaminant Level (SMCL) range of

6.5 to 8.5 for pH, they are consistent with previous results. Since detected in January 2004,

mercury concentrations versus pH have shown a general inverse correlation. Low pH

is consistently associated with slightly elevated mercury concentrations, and vice-versa.

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April2008 8 993-3902.G

This general correlation continued for the latest event. The mercury concentrations detected in

samples collected from MW-8 and MW-8R decreased from the previous monitoring

event (from 0.0049 mglL and 0.0077 mgll- in October 2007 to 0.0033 mgfl and

0.0055 mg/I, respectively in January 2008). During the same time period, pH values for MW-8

and MW-8R increased slightly (from 4.5 S.U. and 4.7 S,U. in October 2007,to 4.83 S,U. and

4.94 S.U., respectively in January 2008). There were no other parameters or conditions

present in the water samples collected that would indicate that the water quality has been

affected by landfill operations.

The analytical results for the samples collected from MW-9D indicated no detections for total or

dissolved mercury. This indicates that the shallow aquifer mercury concentrations have not

migrated vertically. Groundwater from MW-9D had a pH of 10.9 S.U., which is relatively high

for the site. The pH probe was immediately checked with the calibration standards and found to

be recording accurately. Similar pH values have been observed in the Floridan Aquifer in the

Ocala region (Harris & Earnest, City of Ocala Engineering Department Steal Reuse - Ocala's

Airport Solution, 2000); however, given that the other Site wells screened within the limestone

have never exceeded 8.40 (MW-4 in January 200I), it is unlikely that this pH is representative of

the groundwater conditions at this location and depth. As indicated in the well installation log for

MW-9D (Appendix B), a possible void was encountered at 74 to 80 feet bgs. It is possible that

this void was impacted by groundwater hydraulically connected to the vertical interval where

Portland cement grout was placed, potentially causing temporary artificial inflation of the pH

value. If this is an accurate assumption, a gradual reduction in pH over time would be expected

(and potentially observed in the next quarterly monitoring event).

3.2 Quality Control

Anal¡ical results for the equipment blank and trip blank indicated no detections of targeted

parameters at concentrations exceeding the laboratory practical quantitation limits (PQLs). A

review of the laboratory QA/QC data indicated that all parameters analyzed in the method blanks

were below PQLs, The laboratory data were also reviewed to ensure that the Laboratory Control

Sample (LCS) and Matrix Spike (MS)lMatrix Spike Duplicate (MSD) were within accuracy and

precision, and to determine if hold times were met, the correct methods were used, and the

appropriate reporting limits were achieved. The review indicated that all these criteria were met,

with the exception that the LCS/LCSD for bromomethane was above the percent recovery limit.

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April2008 -9 - 993-3902.G

This compound was not detected above the Method Detection Limit (MDL) for the samples

analyzed, and, therefore, does not invalidate the results.

A review of the equipment blank results indicated the detection of one metal above the

associated PQLs. Sodium was detected above the PQL (L2 mgn-). Nitrate (0.055 mgll-) and

chloride (2.1 mgl) were also detected above their respective PQLs. However, given that

sodium, nitrate, and chloride did not exceed or even approach their respective MCLs for any

samples analyzed, these detections do not invalidate the data. Equipment blank de-ionized (DI)

water was supplied by Sweetbay grocery store located near the site, The results of the IDW

mercury analysis were below the FPDWS. As a result, the containerized purged water will not

require ofÊsite disposal.

Golder Associates

April2008 l0 993-3902.G

4.0 CONCLUSIONSANDRECOMMENDATIONS

In accordance with the MPIS, Specific Condition Number 12 of Permit Number

SO42-0019903-006, Golder conducted the nineteenth semi-annual groundwater monitoring event

on January 28 to 30, 2008. During Event No. 19, groundwater |evels were measured and

groundwater elevations were calculated for each of the monitoring locations on site. The

groundwater elevation data collected indicated that the general direction of groundwater flow in

the upper surficial aquifer was to the southwest on the west portion of the site, to the south on the

south-central portion of the site and to the southeast on the eastern portion of the site. The

groundwater flow direction was consistent with historical measurements. The results also

indicate that the groundwater flow direction in the immediate vicinity of MW-3 is to the

southeast. This data confirms that the MW-3 location is not influenced by the landfill, is

upgradient ofthe landfill, and should be considered as representative ofbackground groundwater

quality conditions for the surficial aquifer in that area.

During the nineteenth semi-annual monitoring event, groundwater samples were collected from

eight monitoring wells (MW-2, MW-4, MW-5, MW-6, MW-7, MV/-8, MW-8R, and MW-9D)

and submitted to a NElAC-accredited laboratory for analysis.

Mercury was detected in the samples collected from MW-8 and MW-8R at concentrations

slightly exceeding the Florida PMCL, Mercury detections have historically been accompanied by

low pH in the samples collected from MW-8 and MW-8R. This general correlation continued for

the latest monitoring event. The pH for both the MW-8 and MW-8R samples were below the

Florida SMCL. Mercury was not detected in the sample collected form MW-9D. Given that

mercury was not detected in the deeper interval sample from MW-9D and there is a downward

vertical gradient from MW-8/8R to MW-9D, mercury therefore is restricted to the groundwater in

the surficial, non-limestone portion of the aquifer in that general area.

As per the January 7 ,2008 Second Response to Comments, DPT borings were to be advanced on

the adjoining property to the north for background well location determination. Properly access

was not granted; and, therefore, this portion of the investigation could not be completed.

There have been no data to date that indicates that the landfill is the source of the slightly elevated

mercury concentrations detected, The following data support the conclusion of a natural mercury

source in the surficial. non-limestone shallow saturated zone in the vicinity of MW-8:

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993-3902.G

The horizontal groundwater flow direction in the area of MW-3 is toward the

landfill, indicating that MW-3 is upgradient of the landfill;

Historical groundwater results indicate detections of mercury in MW-3;

Relatively consistent detections of mercury at low concentrations have been

reported for samples from MW-8 and MW-8R;

Groundwater exhibits relatively low pH values in the surficial, non-limestone

(siliciclastic) sediments, likely due to low pH of rainwater coupled with

natural tannic acids in the near surface detritus zone and lack of buffering

capacity in the siliciclastic sediments;

Mercury has been detected in soil samples collected from the siliciclastic

sediments in the unsaturated zone in the vicinþ of MW-8 and MW-8R,

where pH values in shallow groundwater are low (July 2007 report); and

The July 2007 groundwater analytical results for the upgradient temporary

monitoring well (TOW-l) installed at the edge of waste (immediately

upgradieni of MW-8) indicated a mercury concentration of approximately

ottã-trulf the standard (0.001 rr'glL) accompanied by very high turbidity(> 1,000 NTU); while the filtered mercury result was slightly above the

merhod detection limit (MDL) (0.00012 me/L). This suggests that the

slightly elevated mercury concentrations observed at MW-8 are not

emanating from the landfill.

Consequently, the data collected to date suggest that the slightly elevated concentrations of

mercury observed in MW-8 and MW-8R groundwater samples are likely related to naturally

occurring mercury in native siliciclastic soils, which is dissolved in shallow groundwater due to

naturally low pH of the shallow groundwater. Mercury has not been detected above standard in

the same vertical interval at a location closer to the landfill, nor has mercury been detected in the

upper Floridan aquifer immediately below MW-8. With the exception of MW-3 (not included in

permit monitoring), MW-8, and MW-8R, the Site wells monitor the uppermost limestone

Floridan aquifer. Therefore, Golder recommends:

one year of quarterly monitoring for MW-9D (three additional quarters) to

veri$' vertical delineation of MW-8/]MW-8R mercury detections and provide

monitoring for the uppermost limestone aquifer in this area;

Each quarterly monitoring event will include sample collection from MW-8,

MW-8R and MW-9D for total and dissolved mercury analysis. In addition,

groundwater measurements will be taken from all Site wells, and piezometers

ÞZl,PZ-z, andPZ-3, to veri$' that groundwater in the vicinity of MW-3 is

not influenced by the landfill; and

In the interim, Veolia requests a conference call to discuss the future

monitoring status of MW-8 and lvIW-8R.

Golder Associates

April2008 t2- 993-3902.G

5.0 PROFESSIONAL CERTIFICATION

I hereby certiff that I have supervised the current field work and preparation of this report, in

accordance with Florida Rules and Regulations. As a registered professional geologist, as

authorized by Chapter 492, Florida Statutes, I certiSz that I am a qualified groundwater

professional, with knowledge and experience in groundwater contamination assessment and

cleanup. To the best of my knowledge, the information and laboratory data summarized in this

report (including the applicable attachments) are true, accurate, complete, and in accordance with

applicable State Rules and Regulations.


Associate and Southeast Resional Leader

RSK/RWP/Iar

FN: G:\Projects\g93\993-39\993-39O2\REPORTSUanuary2008\Report\Final -CypressreportNo19_4408rsk.docx

Florirja Professional Geolosist No. 2505

Golder Associates

April2008 993-3902-G

TABLE I

GROTINDWATER MONITORING S ITESWACS Number 21251

VEOLIA CYPRESS ACRES LANDFILL, INC.OCALA. FLORIDA

SAMPLING POINT

WACS

I.D.

NTJMBER

TYPE OF WELLAQUIFERINTERVAL

MONITORED

MW-1

MW-2

MW-3

MW-4

MV/-5

MW-6

MW-7

MW-8

MW-8R

MW-9D

Not Assigned

t2976

Not Assigned

12977

12978

19018

19019

19020

Not Assigned

Not Assigned

Piezometer

Background

Piezometer

Compliance

Compliance

Compliance

Compliance

Compliance

Other

Other

Surficial

Surficial

Surficial

Surficial

Surficial

Surficial

Surficial

Surficial

Surficial

Surficial

FN: c:\Proieds\993\993-39\993-3902\REPORTS\Jæury 2008\R@o¡t\Tabl*\Table I sites rev I GOldef ASSOCiatgS

Checked by: _RSK_

Page I of I

April2008

TABLE 2

SUMMARY OF GROUNDWATER ELEVATION DATAV/ACS NUMBER21251

JANUARY 3O,2OO8

VEOLIA CYPRESS ACRES LANDFILL. INC.OCALA. FLORIDA

993-3902-c

WELLNUMBER

TOTAL DEPTH(fr BTOC)

GROUNDELEVATION

(ft NGVD)

TOCELEVATION

(ftNGVD)

APPROXIMATESCREENED INTERVAL

lfr RTocì

DATE: JANUARY30.2008

DTW IBTOC) GW ELEV. (NGVD)

MW-l

MW-2

MW-3

MW-4

MW-5

MW-6

MW-7

MW-8

MW-8R

MV/-9D

PZ-l

PZ-2

PZ-3

62.4

52.4

52.8

6431

62.6

67.5

69.4

69.9',

66.0',

97.6

52.7

51.7

52.9

82.0

13.4

79.6

78.3

77.6

80.8

86.9

83.0

80.8

80.5

NM

NM

NM

84.85

76.64

82.39

80.90

80.41

83.49

89.37

85.62

83.91

83. l4

82.35

8s.35

85.09

57 - 6't

33-52

42-52

53-63

s3-63

s6-66

56-66

s6-66

s6-66

91-96

42.7-52.7

41 .7 -51 .7

42.9-52.9

44.r9

35.51

41.72

40.29

39.72

42.91

48.73

44.86

43.tt

42.53

41.69

44.70

44.4s

40.66

41.13

40.67

40.61

40.69

40.58

40.64

40.76

40.80

40.61

40.66

40.65

40.64

Notes:

ft - feetI = Total depth measured January 2008, except MW-4, MW-8, and MW-8R measured in January 2007.

NGVD - Elevation referenced to National Geodetic Vertical Datum of 1929

TOC Elev. : Top of casing elevation. Based on survey data reported in May 1999 Survey by Central Florida Surveying & Mapping.MW-3,MW-4,andMW-8resurveyedforverificationinJanuary2003. MW-8R,MW-9D,PZ-l,PZ-2,andPZ-3surveyedinJanuary2008.All surveying by Centraì Florida Surveying & Mapping.

BTOC: Below top of casing

DTW = Depth to water

GW ELEV. = Groundwater elevation

FN: CtProjccts\991\993-39\993-3902\REPoRTsuanuary2o08\Repod\Tables\Tablc2-clvrw,l Golder Associates

Checked by: _RSK_

Page I of I

April 2008 993-3902-G

TABLE 3

SUMMARY OF PURGE VOLUMES AND FIELD PARAMETERS

JANUARY 2OOI TO JANUARY 2OO8r'¡/ACS NUMBER 21251

VEOLIA CYPRESS ACRES LANDFILL, INC.

OCALA, FLORIDA

DATEIVELL

NTJMBER

PURGEVOLT'ME

lq¿Ii DH

ùPt!ut!lLCOND.

frmhm/emìTEMPERATT'Rf,,

loclTTJNBIDITY

ÑTTN

lrtùùt Lv¿r,OXYGEN

(moll )

1/3r/20017/27/20011t28/2002'1/30/2002

t/27/20037/29/2003r/26t20047/t3/2004t/24/20057 /27 /2005r/2s/2006'7t26/2006

v24/200'77/24/2007

t/29/2008

MW-2MVv-2

MW-2M\ry-2

MW-2MW-2MW-2MW-2MV/-2MW-2MV/-2MW-2MW-2MW-2MV/-2

l0l0l0'77

J,t5.4

2.7

3.0

3.8

5.3

9.0

J.4

5.8

4.6

J.t

8.18

7.46

t.J)6.97'7.2r

7. l8'1.23

'Ì.06

7.58

6.91

7.02

7.t97.22

7.00

7.1r

130

300

20

283187

222

223

201 J

206222

218239228224

203

23.5

30.0

26.9

23.7

22.1

24.1

22.7

24.5

2r.823.7

2t.823.8))t23.t21.3

8.5

IO

9

J.J

I.)

4.7

6.6

8.8 J

5.4

10

I4.1

6.6

6.4

5.4

'Ì.50

4.674.65

6.23

4.99

J.v)3.30

4.81 J

6.02

5.29 J

5.31

4.40

3.5 8

4.69

4.10

r0/24/2007 MW-3 2'7 )J 69 22.0 l0 l 4.'79

U3r/20017 /27 /2001t/28/2002'7/30/2002

|27/20037129/2003

U26/20047/t3/20041/24/2005

7 t27 /2005t/25/2006'7/26/2006

t/25/200'l7/25/200'lU30/2008

M\ry-4

MVv-4

Mrù/-4

MW-4MW-4MW-4MW-4MW-4MW-4MW-4MW-4MW-4MW-4MW-4MW-4

10.5

10.5

8

a')

4.2

J.L

z.z2.5

6.3

4.5

7.5

6.4

7.8

6.5

6.5

8.40

7.54

7.49

7.54

7.43

7.45'7.32

'7.2t

'1.60

?. l87.21

7. l87.20

7.34'l.12

243

310

224

309

222

269298

278 J

28932t375

376

358

418

4lo

23428226rz)+2t2240226229196z+t220236205234222

).216

6

6.2

4-)

6.8'7.5

13 J

l48.6

6.5

9.4

I ).44.811

'1.50

6.56

4.85

4.62

4.69

2.53

3.19

2.50

3.50

2.76 t1.75

1.78

1.55

1.76

1.50

t/31/20017/27/200rt/28/20027/30/2002r/27/20037/29/20031/26/20047/t4/2004t/24/20057/27/20051/25/20067/26/2006t/24/2007't/24/200'7

l/29/2008

MW-5M\ry-5

M\ry-5

MW-5MW-5MW-5MW-5MVú-5

MW-5MW-5MW-5MW-5MW-5MW-5MW-5

15

I 1.5

10.5oô

8.1

4.9

4.0A'

4.7

5.6

2.8

3.8

6.0

4.'l1.5

7.81

7.65

7.63

7.75

7.50

7.49't.32

7.31

7.5r7.28

7.28'7.21

7.26'1.20

'7.30

2t'7260196

260198

253297

279 I269335

314388

340

391

366

23.6

25.2

z+.)23.0

20.9

23.5

21.4

24.6

19.9

22.5

2t.2aaÁ

20.5

23.6

21.2

o

9.8

o

8.2

8.8

10.9

6.0

IJ

l8 J

9.0n1

l9t4.7t2.5l.t

7.50

5.02

3.66

4.2'l4.51

3.25

3.15

2.92

4.90

3.57 I5.20

).) I

z-vq

3.63

3.92

FN Gi\Proj€cts\993\993-39\993-3902\REPoRTsUanGry 2oo8\R€Pod\Tãblås$able 3 FP rev I GOldgf ASSOCiateS 1 ol2

April 2008 993-3902-G

rABLE 3

SUMMARY OF PURGE VOLUMES AND FIELD PARAMETERS

JANUARY 2OOI TO JANUARY 2OO8

WACS NUMBER 2125I

VEOLIA CYPRESS ACRES LANDFILL, INC.

OCALA. FLORIDA

DATEWELL

NT'MBER

PT'RGÊVOLTJME

ls¡lì oH

srl,LlttuCOND.

lrnhm/cnlTEMPERATIJRE

loclTT'RBIDTTY

INTTN

lrt¡tst Lvür,OXYGEN

lnoll ,\

t/26/20047/t3/20041/24/200s7/27/20051/25/20067/26/2006U2s/20077/24/200'7

t/29/2008

MW-6MW-6MVv-6

MW-6MW-6MW-6MW-6MV/-6MW-6

J.I

5.7

10.4

I 1.8

3.0

6.2

7.4

8.8

5.6

't.45

't.43

7.78

7.43

7.52

/.Jbt.+J

'7 -63

7.38

241

217 I218

275

24'7

292

275

306

298

2t.823.0

20.8

23.'l2t.323.7

t9.922.4

20.9

16.0

14Jl8 J

l06.4

IJ

19.9

9.6

o.J

2.963.96

5.37

4.25 I5.10

4.61

3.794.21

3.83

t/26/20047/t4/2004|24t20057/27/20051/2s/20067/26/20061/24/2007

7/24/2007

1/29/2008

MW-7MW-7MW-7MV/-7MW-7MW-7M\¡/-7MW-7MW-7

2.7

4.9

0.'7

6.6

)_)

5.3

5.6

r3.5

1.8

t.5)7.25

7.20'1.14

7.20

7.28

LJ)

7.22

315

297 J

27'7

JOJ

395

350

345

383

)tt

2t.723.1

20.9

22.8

2t.322.7

21.3

23.3

2t.6

r0.47.2 J

1.4 J

9.0

|.'l5.1

13.6

8.9

9.8

3.35

2.83

4.18

2.t81.49

2.28

t.7 |I Ot

2.t4

t/26/20044/9/2004+'t/1312004

r/24/20057/2'7t2005

t0/2't/2005t/25/20064/2612006

7/26/2006t0/23/2006t/251200'l4/19/200'7

7/25/2007

t0t24/2007t/30/2008

MW-8MW-8MW-8MW-8MW-8MW-8MW-8MW-8MìV.8MV/-8MV/-8MV/-8MW-8MW-8MW-8

6.7

5.2

1.3

J.l

t.25.3

3.5

1.8

2.2

2-9

3.6

2.7

4.6

1.9

z-)

4 ',t5

4.81

4.50

5.08 J

4.7 |

4.96

4.7 5

4.68

4.53À41

5.2'7

4.83

5.05

4.5

4.83

69'72

70J84

r02l0l93

96

98

86

99

98

120

114

t26

24.2

22.924.6)t'l25.2

L).4

22;7

25.9

23.'7

23.5

22.0

25.4

22.6

23.2

65.'l (7 .32)**'1.5

3.1 J

0.8

2.4

2.2

1.2

0.9

2.4

J.J

1À

10.0

2.0

5.0

1.0

0.38

0.48

l.l3 J

2.222.98 J4.40

0.23

0.440.54

0.60

0.44

0.89

0.3 r

4.77

0.45

r/2s/20064/2612006

7/26/2006t0/23/2006t/25/20074/19/20077/2s/2007t0t24/2007t/30/2008

MW-8RM\ry-8RMW-8RMW-8RMW-8RMW.8RMW-8RMW-8RMW-8R

1.6

2.0

J-q

J.+

).+2.9

2.5

2.9

2.1

5.29

4.86

4.86

4.93

5.03

).(r)5.1 8

4.7

4.94

120

90

94

86

94

94

105

t14109

24.8

24.6

23.8

z).+22.2

23.8

24.6

25.+

23.0

J.O

7.9

3.2Áa

r 0.9

6.2

3.5

6.5

1.4

2.6'7

1.08

0.290.38

0.32

0.33

0.440.93

0.34

2/s/2008 MW-9D ?o l0 87 249 40.2 219Notes:gal : gallonspmhos/cm : micromhos per centimeteroC: degrees centigrade

NTU : nephelometric turbidity unitsmg/L: milligrams per literI = Slabílity parameters where out ofSOP calibration ¡ange when checked.r = A verification sample was collected.** : Turbidity at the time the metals sample was collected.

Checked by: _RrilP_

FN: GXPrcj6cts\s93\s93-3e\993.39o2REPoRfsuanuary20o8\Rêrt\Tables\låblê3 FPrêv1 GOldgfASSOCiatgS 2oÍ2

April 2008

TABLE 4

SUMMARY OF DETECTED PARAMETERS IN GROLINDWATER - EVENT NO. 19

WACS Numbq 21251

Jmuary 28. 29, & 30. 2008

VEOLIA CYPRESS ACRES LANDFILL. INC

OCALA, FLORIDA

PARAMETEREPA

METHODUNTTS MCL ùl\il-2 M\ry-4 MW-S MW-6 MW-7 MW-8 lvnt-ER Mtv-gD EBOI TRJP BLANK

pn Field SU 6 5-8.5 l 7il 7 1' 730 7.38 7.22 4.E3 1.91 10.E7 NA NA

Volstile O¡s¡nic ComDounds (VOCS) bv EPA Method t2608 (reDortinq Danmeters l¡sted or EPA Methods 601 & 602)

Mahyløe Chloride

ChlorofomB@me

8260

8260

8260

pcIps/l

52

70

t:

0 t7u028 I

0058u

0.r7 u0.056 u0.0s8 u

0.17 u0.0s6 u0058u

0l7u0.056 u0058u

0.17 u0.056 u00s8u

0.17 u0056u062 I

NA

NA

NA

NA

NA

NA

0l7u0.056 u0058u

0,35 r

0.056 u0058u

Miscelloneoùs Inorguic Compounds

NitÉte

Chlo¡ide

Sulfate

Ammonia

Total dissolved solids

tst 2

325.2

315 4

350 I

t60.1

ns/lmgn

ñg/lmg/l

t0'250

l

250 !

28t{nn !

0.43

321.3 u

0 00s8 u120

048

92t2

0. 18 IV

220

0.47

57r3u

0 0088 rv200

0 3l44l3u

0 0046 rv160

0.42

5.6

t.3 u0 0052 rv

210

298.6

120

0 0t2 rv

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

0.1

2\l3u

0.0056 Iv50u

NA

NA

NA

NA

NA

Tot¡l Metsls

AluinumChromiM

I¡o¡Mscury

Sodim

6010

6010

6010

7470

6010

mg/l

mgllmg/r

mg/l

ñall

0.2'o. l'?

0.3 3

0.002 'z

t60 l

0 l20t0 0023 r

0 220v0 000072 u

28

0.080 r

0 0019 I0.087 v

0.000072 u74

0.021 u0.0019 IOOM6U

0 000072 u38

0.033 r

0.0026 I0 012 Iv

0 000072 u3.0

0.0s2 I

0 0019 r

0 031 rv0.000072 u

35

0.090 I0 0015 u0.0089 rv

0.0033

8l

NA

NANA

0.0055

NA

NA

NANA

0.000072 uNA

0021 u0 00ls u0 0065 IV

0 000072 uz8

NA

NANANANA

\oles:

I = Crcudwater CleÐup Taget Level in accordæcc with Chaptt 62-7'17 F AC.2 = Florid¿ P¡ima¡y D¡inking Wats StaDdùd in accordæce with Chaptq 62-550 F A C

3 = Fìorid¿ Sæondary Drinking Watø Stædad in accordece with Chaptø 62-550 F A.C

ng/l = milligrms pø litørgll = miaogrms per liter

J = Compoud wæ æalyzed for but Dot detected above the level shom.y' = Indicates dal)1e dctecled in both the smpl€ ed method blilk= The rsported value is between the laboratory method detection limit md the laboratory pËctical quiltitation limit

lB-01 = Equipmmt rinsate blank

Irip Blæk = Analyzed for VOCS oûly

),lA = Not applicable or not dalyzed,A,ll metals æalys6 repofed æ total metals (e.g.. wples were Dot filtæd),ihaded ud bolded results indicate the rÐorted concøtration 9xcæds the ¡6pætiv€ groudwats stmddd

993-3902-G

Chæked by: _RWP_

FN: C:\Prcjsrj\991\991-19\13-3902\REPORTSUailunry 2008R9þl\TablL\\Tîblo 4 Lilb Cyprcìs rcv I Golder Assoc¡ates Page I of I

Eor)nö

co

ON

o=Io

NonÐo

äi

o.çÈoô

LEGEND

PROPERTY BOUNDARY

--f--f--_l--f-h-r- RA|LRoAD TRACKS

TOPOGRAPHIC CONTOUR LINE

$uw-r

ACCESS ROAD

TREE LINE

GROUNDWATER ELEVATION

MONITORING WELL LOCATION

x ÊJJGROUNDWATER EQUIPOTENTIAL CONTOUR(0.10 FT. TNTERVAL)

GENERAL DIRECTION OF GROUNDWATERFLOW

PROPERTY BOUNDARY NOTES

Ao.'1.) LOCATTONS AND TOp OF CASTNG ELEVATTONS FOR

ON_SITE MONITORING WELLS SURVEYED BY CENTRALFLORIDA SURVEYING AND MAPPING, PLAT OFTOPOGRAPHIC SURVEY CELL 2 ONLY, DATEDMAY 5, 1999 AND REVISED JULY 2, 1999,

2.) ELEVATTON ARE REFERENCED TO THE NATTONALGEODETIC VERTICAL DATUM OF 1929.

REFERENCES

gs

ls1' 1.) AS-BU|LT S|TE SURVEY FOR J&B SERV|CES, SHEET 1

OF 1 PREPARED BY R.M. BARRINEAU & ASSOCIATES,INC. DATE OF FINAL SURVEY JANUARY 6, 1999.

2.) oVERALL BASE MAp ts FRoM AERTAL suRVEy oF7/2/O4 PERFORMED By l.F. ROOKS AND ACTTVE F|LLAREA WAS UPDATED BY CENTRAL FLORIDAsuRVEytNG AND MApptNc BASED ON 1/25/05GROUND SURVEY.

3.) LOCATTONS AND TOp OF CASTNG ELEVATTONS OFMW-3, MW_4, MW-8, MW_8R, AND MW-9DSURVEYED ON 1/3O/O8 By CENTRAL FLORTDAENGINEERING, SURVEYING, AND MAPPING.

xge.6

- EXIST¡NG ACCESS ROAD

-1 (

200 200

SCALE FEET

SI'I'E ENTRANCE

OFFICE LOCATION

À

DRAINAGE SWALE

EXISTING DRAINAGE SWALE

VEOLIA / CYPRESS ACRES O & M / FL

POTENTIOMETRIC MAPUPPER FLORIDAN AQUIFER

. JANUARY 30, 2OO8 .PROJECT No. 993-3902

FIGURE 1

E

Ðö

I

€OoN

o;

o

oÌ!N

N

onnooô

'=oô

PZ_240.65

ùs,

EDGE OF WASTE

\\

REFERENGES

1.) AS-BU|LT SITE SURVEY FOR J&B SERVICES, SHEET 1

OF 1 PREPARED BY R.M. BARRINEAU & ASSOCIATES,INC. DATE OF FINAL SURVEY JANUARY 6, 1999.

2.) LOCATTONS AND TOP OF CASING ELEVATIONS FORON_SITE MONITORING WELLS SURVEYED BY CENTRALFLORIDA SURVEYING AND MAPPING, PLAT OFTOPOGRAPHIC SURVEY CELL 2 ONLY, DATEDMAY 5, 1999 AND REVISED JULY 2, 1999.

LEGEND

5.) LOCATTONS AND TOP OF CASING ELEVATIONS REVISED

ON 1/3O/O8 BY CENTRAL FLORIDA ENGINEERINGSURVEYING AND MAPPING.

EOOEOSCALE FEEÏ

PROPERTY BOUNDARY

TOPOGRAPHIC CONTOUR LINE

ACCESS ROAD

40.668å3i^tiyîJiE^'ullj'oo'TlAlcoNToUR-Svw-r

^Pz-1

MONITORING WELL LOCATION

PIEZOMETER LOCATION

__> ESTTMATED GROUNDWATER FLOWDIRECTION

VEOLIA / CYPRESS ACRES O & M i FL

LOCAL GROUNDWATER FLOW DIRECTION (MW-3). JANUARY 30, 2OO8 -

APPEI\DD( A

Groundwater Collection and Instrument Calibration Field Records

SITE Cypress Acres Landfill 993-3902-c .0001NAMF.

SITELOCATION: OGALA, FLORIDA

wELLNo: fl,l - Z SAMPLEID: H-'td -Z pATE: 1lZ? 12008

DEP-SOP-001/01

Form FD 9000.24

GROUNDWATER SAMPLING LOG

2. SIABtLtzATtoNCRITERIA: pH=+0.2: Temperature=+0.2oC: _S¡eclficConductance=readinqsa_rewithin+51hDissolved Oxylren = A) < 20% saturation olB) readirlqs are within + QZ¡IS/L fiSf readi¡9912_¡rc111_o_r_l_Q%..úp¡_rc-a!lngp:__2_ndQl

__ rurìidi!y_=_Ð_S2QM_Us_oj Blreedjnss_arqrylt¡j¡_r 5_NT_U_s_(þ_rrç_a_dirus_ì20_e¡d s-5_O_NI.Ud!dq"¿-fl_o.rrcad!¡_s_s:_5!_NlUs.L

"J" = indicafes that the calibratlon result for the parameter of concern was outside of the acceptable criteria for standard range.

v\\- t?. \ R¿ z-s'.>*[ V.5:('! ¿-2' . t-r Ylt rt,r-¡ ì'l]C'fj- R P

vtw,'L |Pç; 5:c\-)'^\ ':- î Dç Rk-v .,,.? L A¿. i r- i\r!tt', - ^¿!'s ¡or},,uir Ltzrl.r fiÈ

NG DATA

PURGINGer.loeo ¡r' Ìoc.(o

AsAM H tLu_b_Il PElNLLl.8'Jl- I Lj4!L I u N :

Matthew Hamoton / Golder Assoclales lnc.John Kino / Golder Associates lnc,

ÞAM4EH(Þlè!-ej-! LU-!Lb_s i

rt.+tF:- SANIPLINGiñrl,qrEo ar, / u ti ¿

SAMP-L.ING t,--,o-EIIDEDAL / e5.)

E_u_I4P_orDEPTH IN P1,"",',. L{ 1 SAMPLE PUMPa, I

ffOW-n¡fe-frdåerminuteì: Ò' L. \ TUBINGMATERIALCODE: PE

FIELD DECONTAMINATION: Y TNIFIELD-FILTERED: Y t\N FILTER,Sl7F:

aUPLLçAIE:-..-Filkation EouiDment TvDe:

SAMPLE-EQNIAINE-BSPECIFICATION sÂlvP_LE PEE-SEBVAIIAN INTENDED

ANALYSIS AND/ORMETHOD

SAMP.[NGEQUIPMENT

CODESAMPLE ID

CODE CONTAINERS

MATERIAL

CODEVOLUME PRESERVATIVE

TJSEDTOTAL VOL

\DDED lN FIELD (mLF-INAL

OH

l4t+¿"2--7

L lí'ì ctt¡ .^ \ Hcr ¿ì_'I . Ð ËzlooP ;l,p

Vtu'7- I ??- ¿So*.1 ,SS.1., tt,t.,'ta Þ¡)Vw! :7-

Þr= t LS*l 595-,r,3 ts,'l Ri)

v\'\/'z \ Ìí: ¿çc,,^\ Hr.(o', ¿-2-r-l i\o.t '{,"nr''ri1 ,R()

¡\rt"W'L \ \-E z,so...\ ll-'rP-. ¿-> \) 3\'1. L - l'J, t rqt€ ,r)\

çv\)'v'L ì 1JË ¿s-o,*l l,f Ðs. 12. Ë øcr0r(-r\rÍ..(J GC-:'t\ ìKEMAKKS:

Fe+2 lmoil):C02 lmo/l) : -' H2S lmo/l):

MATERIAL EODES: _ AG = Amber Glass: GG = Cleelclassl ___Le__=__Psly_e_l¡ylCnel PP :_E9lyp¿o.pyle!el__E - Siljç9¡9l_I.=lclþ¡; __O_.-O_lher]ÞBecjly)

SAMPL¡NG/PURGING APP = AftelPeristaltic Pump: B = Ba¡ler: BP = Bladder Pumpi _ ESP = Eleçl¡çSuþ¡oç_ciþlc_furnp;_lP_ =_PçI¡stalric PumpEQUIPMENT CODES: RFPP = Reverggllq!y¿ej5.!Êlliqlqp:______S!U=_9traw Metho_d_(IgÞi!s_9re-yi!y_D6lrù;,____Vl=_Vs!g_ullfia!_i__. __Q: QtIerlS.pçsj¡¿)

N TFS. I hê ãhôve do nôt cônstttltte âll ôt thc intôrmât¡on rañilrrêrl hv {;hântcr fi

DEP-SOP-001/01

Form FD 9000'24


SITENAME

Cypress Acres Landfill 993-3902-G .0001 SITEt oCATloN: OCALA^ FLORIDA

wELLNo: Plb*I sAMpLE lp: f{UJ -q DATE: 1l?(i12008

PLINGs¿MP-t_E p_EY LP_BINIILAFEIIIA ì I o N :

Matthew Hampton i Golder Assocìates lnc.

John Klnq / Golder Associates lno. W. f#Hn^r. I ?4SSAMPLINGÈIoeoni l?c:Ò

F-U-MP-O.B_TUglNÊDEPTH lN WELL (feet): "YÉ P.3'{'näËiËn!,/Áou*t' ti', rá TUBING

MATERIAL CODE: PE

F I E LÞ.-Þ EçQNTA r4MIgNj-- gt--I E-E!Filtra

DUPLICATE: Y €)

SAMELE-C-9I!-TAITLE-EsPE_CJEAAILo. N

SA t\48!E I R EEE-RVA]IAN INTENDEDANAL.YSI9 ANryA.A

METHOD

SAMPLINGEQUIPMENT

CODE9AMBILIDCODE

FCONTAINERS

MATERIAL

CODEVOLUME PÅE-SEBV¿IIV-E

USEDTOTAL VOL

\NNFD IN FIEI D ImLFINAL

DH

.\\r-L-( t ('tô q$ lJ c\ L7-c g>úþD Fí5

I

l5Lr.-'.ÞÉ

1...:..ftrr u'

B-z-S-s-:r¿2.í-t ?V,o"rr)lS tt2.0.l

- .í)t:(¿i:)r --ì' .-;-. 'T-\t

1wl"v-u\ f [>É -¿,t? \^l !tr-1 .¡ ¡5 ¡|ç ri1, !ìrn

ì ?b '¿r;ç vl lr. so, ¿3¿ .1> SS3.z- i\),I.t'.ld) Kt'lJt¡)Fç ?'ç(u r.'l L{,.1ùi, /.2..Ç -{

5g, 1 ¡:¡*, n..,,, ",

la-kr**l I rr ¿,,4)_l ii\.( ,2, '3) s , K\,'

îg ?-<t ) r*l l+lJü". /-2. t) 6.oroß ltøk"l(, ß\.)REMARKS:hU i I r'; ¿,2 v l\5çç*'-.7 1,11ç11ì

_ H2S (ms/l)

_l) I

c02 (mq/l) i

tvtAfgglAt_SgDEÞ: _-Ac=ÂlTì-bsrcþsci_C_g_=_çþerclassl PE - P9ly9lh!þnei-l-P=f,o.lyEppylenq S = Silicon-e-;--.T = Teflon: --o. - O-lhsl (Sp.øfu)

re abovs do not constltute a rrmatlon reouired bv GhaÞter

Dissgl jcdlqxy_ge'¡1 mgi L (forleadinqs 'í

2 mq/L) or 10% (for ¡eadinqs l- 2 E^qlll

---.-TgIþJdltJ.L\L-<20

NTUq-or'EileadiDgs-a¡9lryLthi! +-5 XlU.s-(to-¡.rceqrn¡s-L2-0-a¡=d:l-0 NJ-Us)-srlgZ"-11-orleadi!.ssÌ- 50-NIUI.L

,,J,' = indlcates that the callbration regult for the parameter of concern was outslde of the acceptable criterÌa for standard range.

SITENAME

Cypress Acres Landflll 993-3902-G .0001 SITElocAT¡oN: OCALA.FLORIDA

WELL NO: F,!..\J 'S- SAMPLE lD: l-L\,J - S- DATE: 1lL4\ 12008

DEP-SOP-001/01

Form FD 9000'24

G LO_Ul'l DWATE R SAM P Ll N G LO g

,. Sr¡etLlz¡rlo¡lCntrenl¡: oH=+0.2; Î"mpãiãiure=+OZocl Speç¡ficConductance=readinqsarewithin+5%;

Dissolved oxvgen = A) < 20% saturation or B) readings are wjlhL¡-f-02r¡-s4=.fa.r-rcê-dtnss J¿nN/LLo!-q:éÍaIJ-e3diN!-ì-2-rn-dUj

____Turljdjly_¿I. 2Q_l!_T.u.s-o.rÐJeê-d-iD.ÇLs-ileyt[¡¡-t5Nl-us-1tø!-e-ad-rnssl2Q..ê.J.d-5..-5-Q.N-TLJdsl-l-07q-ÚerleadJ,lls.sl- sQNr-!Ð'

,,J" = lndicates that the calibration result for the parameter of concern was outside of the acceptabls criter¡a for standard range,

DATA

onlv fill out if aoolicable)

ffiff*or, t3Tø

3DASAMPLEÞ_BY]gBNr)l¡l=lllÂl loNìMatthew Hamoton / Golder Assoclates lnc,.lnhn Klno / GôlderAssocieles lnc.

sÁMÈE1slsrylÆç.( .+< iF- SANIPLINç ¡ Lrr\

JNIIJATEÞ_A.IJ I IL I

S¿MP_L|NQ .. ..2->-EIIDEDAT: /Y ))

P_ulúE_9R'ItJElN9 _ !.NFPTH IN WELL Ifeet): \ ò

SAMPLE PUIV )î. ¡ | TUBINGà'^o. -i.,,r"\. I rtiÁ-rrninr- coor: PEFLOW RATE

FIELD DECoNTAMINATION: (þ N _D UE!çAI_E : ----- Y

---(N.'SAMPLE CONUIINEB

SPECIFICATIONSAMPLE PRESERVAT]QI! INIENDI9

ANAI-Y-SLS_ANryAs.METHOD

SAMPLINGEQUIPÌúENT

CODE$aMtLllaCODE CONTAINERS

MATERIAL

CODEVOLUME

PRESESVJTIVEI ISFD

IQJA_I.-V-O-L\DDED lN FIELD lml

F..tNAtoH

l-'t^d -S)_) LE l-l c- I /-¿. L\ * Z¿,rtt ß BÞ

Ìt\^J . L 4A L- t+. SG, /^/..(: t^\ÉL^<J\9 c('Zar i

Y\/"J,S i>Ê \-¡](.).-.i-.NS

k\vr.ç \ ..í) í> z-So.-. 5S 't r fri\-' ; h(

Y\(¡-' 5ytrt'5

Þr: > S-ù.* !{ -Sc'r 35E ¿ ts\rt¡--f¡

\ çe zsu,*\ H ¿St) t'. y' l''ç'' -lJ-c,r Qe,,*,¿¡øì".

U,.l,v 'S 1ÞÉ" S(v"*l St s. ¿- ,37-s',i

i\dv.S l>\2 z fc* i{ñþ! /_.2 c Goru í\ ¡.n [-nt<¿ .2.ë

¡,Leccw1 ìcr)o/l ß p

co2 fma/l) ' '-- r"*z (

The above do not constltute a re irrformation requ bv rr 62-1 bu.

I

I

Lì]\'l\l

SITENAME

Cypress Acres Lendflll 993-3902-G .0001 SITElocATIoN: OCALA.FLORIDA

WELLNo: Ft.W.-(! SAMPLE lp: [-tw .-Q DATE: 1lL1 t2008

DEP-SOP-001i01

Form FD 9000-24


ã.- Sr¡ailz¡lo¡lCnrreni¡: pH=+0.2;_ Temperature=+0.2oC: SpeclficConductancg=readinqsarewithin+5%:

giss-q.ly9-d-QryçLel-*-AL<20%-sêlg@tia!-qlB-IrcAdinqs-4rc-wi.tilin + 0.2 mq/L lfqr-rcqdugs-i-2-m-d!)-o-tl-01/" 0qrc-qdj¡s!-f2-mduj

T¡rrþ.-rdXr-1l120 NTUg-o-r-pl-L€du-qs-?LefryLttrn-t 5 Nl-!ls-(!-olle-adir]g|l¡-20.end -'-Qq NÏ.tJsl.ç¡-i-0-"4-f-q[eÂdIs.s-ì-!Q..lLTu-i.

TOTALVOLUivIE r,,..ÞúnõE-orqailo*1,) 'Qc'

PURGING t _L.INITIATED AT: I )u )

PLING9¿ À/PIED-Ð1€ß,ND/ A F F-l uÀl I oN ;

Matthew Hempton / Golder Assoclates lnc.

John Kinq / Golder Associates lnc,

SA-MP-L-E3(ÞI.S]ENfl -q]E!JJ

q\.Á'Y=- SAMPLINGÑirt,qreonr: tt.(lra¿' Ètr"'Ìi r-ìes

zuMP--9.B]IJEINGntrPTH lN WELL lfeetì: \t- I

sat4P_LE-F!.tuE+.t ^ ,".FLow RATE (mL oer minule): u'- Jtu_Þ.tN9_MATERIALCODE: PE

FI ELD D EC ONTA M INA]LO.IIj Þ! P_LTQALE. -.- - -Y---ôFillration EouiÞment Tvoe:

SAMELE.ç-A.NTA]NEBSPECIFICATION

_s¡[4P!_íEB_ESEBVlll-QN INTENDED

ANÀL-YSIF-ANryO.AMETHOD

SAMPLINGEOUIPMENT

CODESAI\4PLE ID

CODE

#CONIA]NERS

MA-TEBI&LCODE

VOLUMEPRESERVATIVE

USEDIou!_v-o_l=

\DDED IN FIELD (mLEINAT

DN

Yr(\).-u ((. lb.- | pl-cl Å L.tl 8z-øc'5 ßf'Y(çu- LC

,z t-- l*l lJ",.50.r Lz <L -lvt\'J - t Þf tè b ø'l ìñ S

vL'-w -k þ¡= 7-.5-o u*l .(SLt .l tu,,lr,b

YLuv -q ?t ¿sê Þl lJ- 5.ì, z z.s 1ç( . ¿. Nt t-r-.,fo-:-a-: _._-. -,- ---:- ----ifO, t rJ*-o^0..

k_ -r::i '> (?rVwI Soq ¿ Z.c,

Kow-Q 'i>Ë: 1sr: þr \ ts ¿ ,.ll s-. t

t-!c\) ''\L t,;tÇ. ¿tc * li'^Jü. ¿-Z -(:' Iuf r' i( l(*'{¿.(J

MATE¡]AL çeDES: ____ Ag_=AmþcrG.l-as¡;---Çq=-eþerGlas-qi----IE -:-Pqlyethy!c¡ei.- PP = Polvplqpylcn-ej--S =-S.j!þ9-Dqi----T = teflon: - O = Otherlspsçjfv)

_=-,99¿istaltic !tl¡1p:..V-a-c.uunliaBi-.-.--o-:-QI!re-(S.psçilv)

1. rôV6l rrmation reouired bv Chaoter 62-160

'.J,, = lndicates that the calibration result lor the parameter of concern was outslde of the acceptable criteria for standard range'

SITENAMF

Cypress Acres Landfill 993-3902-G .0001 SITELoCATION: OCALA, FLORIDA

WELL NO: Ç{!- --l SAMPLE lD: tq-L1;z.--'? DATE: 1/>c /2008

DEP-SOP-001/01

Form FD 9000'24


-Dfsspl-vc-d.-Q¡yg9!-:- A) < 2Q%satqation-prB)resdjnqs-qle-lvlthj¡-+ 0.2 mq/LllgIgedjls-g 'r. 2I0g/L) or 10% (for re-Adinqs ì'2 mq/Ðj

--r.urþidj-tr=Jl*1-2.q1lTus-orpllsadinss are witþ.r¡_ú N]-U-sjf-olle-a{rn-sgÌ20-e-nd-s--ss-N-T.!-cþL1q% fþ11'ead1¡sc-> 5-SNI!J5-L

STATIC DEPTHro tn¿errn ri""O' 1'7 Uf,

¡.3 : I ,331

TON:tes lnc.

tnhn Kino / colder Associatss lnc,

SÁ i'/¡IEBGLSIGNÁIUB ESj

f<+{-<==SAMPLINGn1rL¡rep-¡r: l1'1 T

saM!!!N_a ¡,ãENDEDAT: I a I 0

PUMP OBj.UBIN9 r,, IDFPTH lN WELL lfeet): LL' t

SAMPLE PUMler. /Fl oW RATE lml oer minute): t.o1 TUBING

MATtrRIAI CODF: PE

FIELD DECONTAMINATION: ¿ì-T EILLD-IILT-E-¡|ED:_ Y ... -.d) - -l-LLIERgiZEL--_rmFiltralion EquiÞment TU--

p!P!eA-lEi-- Y 0)

SAMEIE_AANT-A]NEBsPEc_lFrç¿llQN_ SAMPLE PRESERVAI.!9N !I!_r_El!qEpANALY$]Ê¡NDLO-3

METHOD

SAMPLING

EAUIEI4ENICODESAivIPLE lD

IìÔDFtt

CONTAINERS

MATERIAL

CODEVOLUME EBESEAAÍ-IIE

USEDTOTAL VOL

\nntrn lN trlFl D lmlEIMt

oH

-t.r\--l _.) Let L(cr*" \ ì-\ ¿ t ¿:> , L) Sr"- t¿ O tì \3P

t|"J I z A(; lL--lJz

}j,L'- ¿-> , () st-e ¡{-ar' .-Tù 5 KI

tv\ru :1 I T't: Z-S L-,.* 3.Ç't -r loi'lr,t* Àr'

-v!4-(^L r' I

Ì>F 2-SO'n lì- .r(1,., ¿-2.Ò (S3.¿- rri{-r*É¿'¿{-L). t á"-*,v¡ ic.t

isP

\-E \-L) $r-'.rC , ,r,-'L 'lì- bT

V\l,.J '1 ?r 2:ço,-l 3¡s', z. '3 x. tl ßP

wN -1 I ÞÊ Z-<Ltt-.\ ,-l l\)c]{ ¿-z Ò \{ol uß ù('rl''l, br'

I hÞ ahôve o not constitute ¿ ,e information requlred bv Chapter 62'16+ 5"/ñ:

TtoN CR|TERIA: pH = t =+

,,J" = indicates that the callbration result for the parameter of concern was outslde of the acceptable criteria for standard range,

SITE Cypress Acres Landflll 993-3902-G .0001NAMF:

CITtr

I ONATION. OCAI A FLORIDA

wELL No: ì-Çt^-r..- ¡ç SAMPLE lD: /.^k, - ð DATE: 1/¿\ /2008.)v

DEP-SOP-001/01

Form FD 9000-24


2. STABILIZATION CRITERIA: PH = + 0.2:

DjSS-g¡te!_4ry!-etl_=_A[2Ay."¡eluration_olB) reac!_i¡gs are within + 0.2 mo/L (for readj¡gsl-Z!:n-S4þr--1-0% (for-Le-a--dltgtÌ-2-rn-dLii

__Jrrr_þjdi!v_:ll= 20 NTUs-o.r-B]-r.eadj¡ss-a¡e]{itbi¡-tl MT-U-s-llor-r-eadi-n-scì20--and'r-59I].Usl-q-1-0-"ó-(f.çll-e.adr¡g.q:--s!NTUd,

ffiN^r*or' ¡t1r'z-PURGINGENDED Ar: lT 5 {¿

NG DAs A M P L E LEYIPß!I!JJjj¡.E!!! ô I I oN :

Matthew Hampton / Golder Assooiates lnc,

John Klnq / Golder Associates lnc.

-S-AW!EB(ÐSIGNAIJELS-fr,Jlæ-¿4' ffi ftHo. tqla SAMPLINGExDEõ_Arj ¡ Ll.f Z

zuMP-9A-IUBIN-Ç r ^ rnFPTH lN WFI I lfeetl: \¿ ìSAMPLE PUMH,-"' Il.r-ow äÃrË'ifü o,ir ^(ur.rt

Ö @ \TERIAL CODE: PE

FIELD DECoNTAMI NATI oN l&_¡ DUPLICATE: .-- Y -€\Filtration EouiDment TvDe:

sÁllP_LE_CoNsrEclEl_ca

TAINERfloN OAMELE-PEESEBVA'TIQN INTENDED

ANALYSIS AND/ORMETHOD

SAMPLING

EqUJP.MENTCODESAMTL_E tQ

CODE I]ONfAINFRSMATERIAL

CODEVOLUME

PRESERVATIVEUSED

TOTAL VOL\DDFD lN FlFl ll lml

EINALnH

Þ\tu - 8 Þ\ r6 '10 t* I H-( ¿z .c) Y'z't¿ tt'i\ gf)'L

I_,4-6_._

lìr-: -tl.¿å"L-.r=r. - "*2:.Í)- '-Qh-r*::r:i s : ?¿.i I

't'ñc_ßrRÞ

\.\.\r'''K r\r-YT zç0,"-l qçLl ., Þr+r, lç fRP

[r.l-vz - $sIa h¡..$(

I \'Éj 'zSO*l7,{()'vl

il>_Ç(l,r ?-Þ-:,ó- n l.).A ¡.

RtrN<: l.l- Sa ¿-7,, O

Art^,-k' '?L '?to,*l 1ç<,¿,37S',1 BPt-4 t^r' {s' fË z-*O'" ìl-t'wl Lz. a tr0iO'll F(çJ¿r'ç ßÍ-r

F('s t tË. tL{ni Ht..xtïre+2(mgltf.

¿,2 ' ù ilto <¿-ur-r 7/7¿r lì¡

H2S (ms/l):

E[')

C02 (mo/l):

MAI_EBIAI_E-O!.EÞ: __.-A.G__=¿¡OþCfglC!_gL__CE_:ClearGlass: PE=Polvethvlene: PP=Polvorojo_vlène: S=Silicone:-T=Teflon: O=Other-(9peSUVJ

e above do not constitute all o re information reouired bv Ghanter 62-1 6

',J" = indicates that the calibration result for the parameter of concern was outslde of the acceptable criteria for standard range.

DEP-SOP-00'1/01

Form FD 9t¡{J0"24

GROUNDWATER SAMPLING I.OG

SITE CYPRESS ACRES LANDFILL 993.3902-G OOOI

NAME:SITELOCATION: OCALA. FLORIDA

WELLNo: t{b- I R SAMPLE lD: Ë,trO - gß DATE: l/þ/2008

,,J" = indlcates that the calibration ¡esult for the parameter ofconcern was outside ofthe acceptable criteria for standard range.

WELL 1 or þDIAMETER linches):

TUBING %

DIAMETER (inchesl:WELL SCREEN INTERVAL

DEPTH: (a¿ feet tof+bfeetsrATtc DEPTH I PURGE PUI,IP TYPE

rO WRrrR (teetl: I on netleR, -PF- RP

onìv fill out if aoplicable)=l fccl- feelì X oâllons/fool qallons

¡3 = /,3tf

(onlv f¡ll out if aopl¡cable)

FINAL PUMP OR TUBINGDEPTH lN WELL (feet): ¿¿\ ffiffi^.' ¿szz I ËfiËÊffi', t sHz TOTAL VOLUME

punc,¡o roãlloãrl' z. ro

TIMEVOLUMEPURGEDlqallons)

UUMUL.VOLUMEPURGED/õâllonsì

PURGERATE(qÞm)

DEPTHTO

WATERlfeet)

pHlstendard

units)

TEMP,E TURBIDìTY(NTUs) ORP

COLOR / ODOR

, çrû t, to /'St> ó.ro Ll.3.Íþ .t 9l 23.ò\ JbR o.3s /q, r 2,L3 r?t{.1 ¿l.c-..3o..¡.

{53? o.3Þ /.8"0 b,to .t<.8Ò q.15 z<.êe (Ò1 o,ir/9,9'/, , .1¿ ?.1 .t

t5*.{z o.3c> z.lo ô,ro \3 ,80 .{,gr ¡<oZ toj r,tr/.r,of /,'l () t7l.b

Fooll' /: 12" = 5.88' 51R"=nn16

Matthew Hamplon / Golder Associates lnc.John Kins / Golder Associates lno.

MAIEE]AI_SoSES]_ AG=AmberGlass: CG=ClearGlassi PE=.Polvelhvlene: PP=-P-plyp¡gpyle¡q S=Silicqrre: -T=I-efþ¡i-*-O.--Olh-e-l-ÍSp-eqrfu)

Page / of t

1L.6il8-)

u\çiL.

b.,

Field Instrument Dissolved Oxygen & Oxidation-Reduction Potential Calibration Records,

INSTRTINIENT (MAKE/MODELNO.) YSI 556MPS INSTRLME¡1¡g.Yl.¿s il/ r'¿t'trc)

STANDARD INFORMATION

Project Number:@Project Name: Cvpress Acres Lan

Standard Vendor: NÄ

Prepared Date: NA Where PrePared: NA

Grade: NÄ' DO-Units: me/L ORP Units: ntV

okP standard Lot # 720623 Exn Date JUL-08 Pur Date NOV-07

DO Sta.ndard Air Calibration Chamber in Air (Table FS 2200-2)

Standard

Standard

Acceptable calibration check is if the meter reads within +/- 0.3 mg/L of the value of appropriate

calibration standarcl. Need to recorcl DO readings in rng/L and use Table FS ZZ00-2 "Dissolved Oxygen

Saturation". ORP calibration reading must be within +/- 10 rnV from the theoretical redox stanclard value

at that temperatute.

Ci\DocùDìenls ¡ild Scltings\nrhurploÑDesktop\Projccts\Ficld Forr¡s2\DO-ORP-Cnlibrnlioil ForDr doc

ft:t.. Lt "ì

Golder Associates REV.3.11/07

^-rlLlyage ¿-of I

tr'ield Instrument Conductivity Calibration Records

TNSTRTJMENT (MAKEiIVIODEL NO.) YSI ss6 MPS INSTRUMENT NO'1"'i""'1

STANDARD INtrORMATION

project Number: 993-3902-G .0001 Project Name: Cvpress Acres LandfÏll i Veolia

Standard Vendor: GEOTECH

prepared Date: IIKN \ilhere Prepared: Golder Associates Inc.

Grade: NA Units: umhos/uS-cm

Standard

Standard

Standard

DATElru¡/dd/w)

TIMElhr:rninì

TEMPDEG CO

STDVALUE

INSTRTIMENTRESPONSE

%DEVPASS/FAIL

CALIBRATED(YES, No)

TYPE(rNrr, coNr)

SAMPLERINITIALS

1l¿1108 è'ì ZS t\ 1? 84 ìs )s% P lÇs INIT MH/JK

llzîl0B a>îz:1 IITLI s00 ql f t <_ 5% t Y*s INIT MH/JK

1t2108 ori¿1 ir .3R 2000 ZcrrS ¿5% Ê Nl U INIT MH/JK

Ilû/08 I r¿.f"] t1. u9 84 gl ¿- 5Yo s" xJ r) FINAI MH/JK

rlv1l08 \v.fi l'l,'ì3 500 r\11 ¿, 5% ñ1-" ñc) FINAL MH/JK

th1t08 t-Jo r¿ir.5t 2000 Z,vt{ ¿- 5o/o çr u\C FINAI MH/JK

rlgol cs ¡toIz t¿i-'\] 9ul 8z ¿- r'1, r.Þv l\ò "r: --.'J- ,".-tt' ]LC

r t)rl lI.s¿ góG t-tÇ \. ¿.. ( l, F ìvci 'î*,þ t.. tl fta

+ t oBil' Iq Lr,i iciri c./. 1-<'/ i¡\ ñs '1' --'.4 J.4FI It¿

,\s'-\aa¿ r s$t? '2;Z;-11 t"l fu ¿- ([ F \Jct -' I hh+ JV

Lsçt' zz.ø,a .çoc Tfl L <'l t\ ñrì f','t*,.,/ s.t!( ,lt"

+ l.S.-ltt'öz:\l "çn<ttJ 'LO tz. ô' 5/: t \.l¿t Ë- ¡l¡"'o'( r.r-tt [¡.¡r,,

Acceptable calibration check is if the meter reads within +l- 5% of the appropriate caliblation standarcl.

c:\DocÙ[rcDtsa¡dscll¡n85\llhrmPloD\Dcsklop\Projects\FieldFomts2\Conductivity-Calib¡0tionFom].29,07.doc

Golder Associates - REV-2-03/07

of-!-Golder

Associ;atesField Instrument Turbidity Calibration Records /

INSTRIIMENT (MAKE/I4ODEL NO.) 2100P Turbidimeter INSTRIIMENTNO. t+r-1 þz'Ssy

Project Number: 993-3902-G .0001 Project Name: Cypress Acres Lan


Prepared Date¡ IIKN 'Where Prepared:-IIACHPurchase Date; UKN Expiratlon Date: UKN Lot Number: 6100, 6108. 6101

Units :Nephelometric Turbidity Unit

Standard s-Lú ¿i Neohelometric Turbiditv Unit

Støndard (8.i NephelometricTurbidit)'Unit

Standard SG I Nephelometric Turbidity Unit

Standard Nephelometric Turbidit]¡ Unit

Calibration values for turbidity needs to be within 10% oÍ the standard for values between 0.1-1.0 NTU: B% forvalues between 1'1-40 NTU: 6.5% forvalues between 41-100 NTU and 5o/oforvalues >100 NTU.

C:\Docurnents nnd Scil irgs\¡nhaDplon\D6klop\l'rcjæts\Ficld Fo¡Ds2\Tut b¡dity-Cûlil¡r¡l ìon FonnJ '29 07.d0c

Golder Associates REV-2-03/07

DATElmm/dd/w')

TIME(hrrrnin)

TEMPDEG C

STDVALUE

INSTRUMENTRESPONSE

%DEVPASS/FAIL

CALIBRATED(YES, NO)

TYPE(rNrr, coNT)

SAMPLERINITIALS

u>1/08 Oê¿'ßu Ç,t¿ I S.-lo r0% Þ ño INIT MH/JK

tl75l08 q'¡rr 3i s k,'ì sk k,-6.5 % I tJ t: INIT MH/JK

1lz1t}B CftZz Sv. \ $tet" / 5o/o Þ XJ cr INIT MH/JK

tþ1/08 lvgz S. v'i î,'l'z s70% r" \J t) FINAI MH/JK

uzl l08 t\r.5 j )¿. \ .¿1 ,.> r.5 "6.5% f ñc, FINAL MH/JK

llzq l0B 1r".SI Çto r >v> 5% P ñcl FINAL MH/JK

i lse/ os{ tfssl 'î.b.Î :1 . þ'i ¿ tc'/. P \\0 -,{, '- r'è' b\K lrI o3g {8, < çq. r t o, <'l F ño '-t,.*.,þ i."rÉ-l.lþ

*" lorf çd,l S-G5 L-t/. q> ñ0 -L^.*' ül.çl' .llc

tìTctloV rgct) 5 , iê'1 S.r ( ¿: loÏ Þ Lio. Pì^*l rt lJ,JI:

\(L(8 -t.s.1 58,'r L i¿81^ tr i)r'. ç'ì.*l 14L+ \r-+ t 5\tc1 lbt S-to ¿ ¿- rl. Fl ñì) '?'l à^1 1"1.ü? 'Jv,

^ ,. ^

¡ Il,age L.l ol _\

GoldersocÍa'ftes

Field Instrument pH Calibration Records

INSTRUMENT O4AKE/IVIODEL NO.) YSI 556 MPS INSTRIIMENT NO.

STÄNDARD INFORMATION

project Number:@Project Name: cypress Acres Lan

Standard Vendor: GEOTECI{

PrepaíedDate:-UKN WherePrePared: Golder .A.ssociates Inc.

purchase Date: See Below Expiration Date:.1$ee þ!ow- Grade: UKN Units: Standard Units

Standard

Standard

Standard

Acceptable calibration check is if tlie meter reads within +l- 0.2 pH units of the value of appropriate

calibration standat'd,

C;\DocuDìc[(s înd sclthgs\[hnDplon\Dcsktop\Projccts\Field Forrrs2\pìl-Crlibratior Forrn3 ?9 0? doc

DATElmn/dd/w)

TIMElhr:rnin)

TEMPDBG C

STDVALUE

INSTRUMENTRESPONSE

%DEVPASSiFAIL

CALIBRÀTEDíYES. NO)

TYPE(INIT. CONT)

SAMPLERINITIALS

r&to& oç 3g l?.r'ì 7.00 -7 .13 > 0.2 Y-s INIT MH/JK

Llzql0S (,o11Ç ì2. k\l 4.01 t1.ot-[ ¿ 0.2 tr l.J (i INIT MH/JK

Utlos o6i31 i¿..7.2 10.0 I.sz <.0.2 r\ Ëo INIT MH/JK

r/2;7108 l.-ìo'i l'i.l\ 7.00 ì, if L 0.2 tr ñr FINAI MH/JK

rt?.1108 tlvl \tì'l\o 4.01 T.lla ¿ 0,2 Þ ñ0 FINAL MH/JK

t/7,|.108 Ilul r ti "'tK 10.0 '1.11 ", 0.2 F 1..\ \) FINAL MH/JK

rlQJ'o'Y rs39 t¿i.t8 '-l ^CIlr ). r? . 6,2 Û) FYr f *"L ',.tJ / irc-

tolt tq ,31 I"o '

¿-l, lf t-*(2,1 ç> Ì-I c; ,r, .l- (,-.vl lL+ lo$l ¡1,2x Io. ù q..91 1' t>,8 t\ Nrr 'T*.'k ,,n u. /.\l*

r\""o[¡g t{s-k Z:¿..t\("7

. crc 'f .0ç Z ar;t Þ 1..\ r\ rF,.'*"( r*di-l{¿

lr¿ cÒ z'¿--sT '1 .-rÞt ï. r(¡ ¿- Ð.'¿ F.. L\ò ç,"Å o.¡i/¡P

+ lt;'(Z z¿,3¡o r.o .. Ò 1.111 ¿*.0.\_ Þ $"t d Þ t l.+rl p,, /Jh-


DEP-SOP-001/01

Form FD 9000-24

GROUNDWATER SAM PLING LOG

SITE CYPRESS ACRES LANDFILL / VEOLIA 993.3902-G OOOI

ñtÀ firtr.SITElaìnÀTtôN. aì4.ÂlÀ trlôRInÂ

WELL NO: MW-9D SAMPLE lD: MW-9D pATE: 2t 6l2oo}

PURGING

SAMPLING DAT

2. STABtLtzATtoN CRITERIA: ÞH = + 0.2: Temþerature = + 0.2 nC: Specific Gonductance = readinqs are within + 5%:

Turbiditv=A)<20NTUsorBlreadinqsarewithin+5NTUs(forreadinqs>20ands50NTUS)or10%(forreadinqs>50NTUs-L

STATÍC DEPTH , .,.ro wnrun rr""Oi-l ¿

N/P VOLUME + (TUBING CAPACITY X TUBING LENGTH) + FLOW CELL VOLUME X3:- / Ltt6 oallons+(o.r.(2tt qallons/lootX ilt¡ feet) + O,2g- qallons=¿,f-]t'g¿llqns

PURGINGPr.lOeO ¡,f, / 'l \ .)

INITIAL PUMP OR TUBING -.DEPTH rr'r WEIL ft""ri Yo . s

COLOR / ODORldescribe)

¿ 1ç*¡' , âå.*-

'¿ tf lz¿, s /.

SAMPLINGlrnurcÞ-¿.rr /1 \ LaHampton / Golder Associates lnc.

H9 74704 - Filtered

Pase , of Ll

Field Instrument TurbÍdity Calibration Records 1

INSTRIIMENT (MAKEi\4ODEL NO,) 2100P Turbídimeter INSTRLIMENT NO. lt;fr /Project Number:@Project Name: Cvpress Acres Landfill / Veolia


Prepared Date: UKN 'Where Prepared: HACH

Purchase Date:-UKN-Expiration Date: IIKN Lot Number:

Units :Nephelometric Turbidity Unit

Standard f ,Ll L{ Nephelometric Turbidity Unit

Standard S I 'o Nephelometric Turbidity Unit

Standard S -l I Nephelometric TurbidÉnUs4

Calibration values for turbidity needs to be within 10% of the standard for values between 0.1-

1,0 NTU; Bo/o for values between 1 1-40 NTU; 6.5% for values between 41-100 NTU and 5% for

values >100 NTU,

c:',Docùnrenls ârd seltinüs\nhilnptoil\DesklopìProjccts\.Field FonnslrTilrbid¡ly-crliblnlion Form3 l9 0? dot

Golder Associates

6100. 6108. 6101

Standard Nephelometric Turbiditv Unit

DATE(mm/dd/vv)

TIMElhr:rninì

TEMPDEG C

STDVALUE

INSTRUMENTRESPONSE

%DEVPASS/FAIL

CAL]BRATED(YES, No)

TYPE(INIT. CONT)

SAMPLERINITIALS

2t6t08 Ir'3q S* ..-('\ .ç.'l o <10 % Þ ¡Ju INIT MH

2/&08 1tS-ì 5ì"C) c). ( /á3 % F fJ cr INIT MH

2/6/08 \ \'\A s-l I -s)*t , <o/^ tr N/U INIT MH

2/5/08 /5ls- s, .l L\ 5,'il t0% t- ñc FINAL MH

2/6t08 /s3þ s t.Ò ç-t .8 ¿ .6.s % P ño FINAL MH

2/6/08 lJSl <_ìI ç1t- s% f) Nù FINAL MH

REV-2-03/07

<t t"

Pase Zof Y

Field Instrument Dissolved Oxygen & Oxidation-Reduction Potential Calibration Records. ¡

TNSTRUMENT(MAKEIIIODELNO.) YSIs56MPS INSTRIIMENTNo. YSt* l/6zi? Q

STANDARD INF'ORMATION

Project Number:@Project Name

Standard Vendor: NA

Prepared Date: NA Where PrePared: NA

Grade: NA DO-Units: me/L ORP Units: mV

ORP Standard Lot# 120623 Exn Date JUL-08 Pur Date NOV-07

DO Standard Air Calibration Chamber in Air (Table FS 2200-2)

Standard

Standard

Acceptable calibration check is if the meter reacls within +l-0,3 mg/L of the value of appropriate

calibiation stanclard, Neecl to record DO readings inmgL and use Table FS 2200-2 "Dissolved Oxygen

Saturatio¡". ORP calibration reading must be within +/- 10 rnV fi-om the theoretical redox standard value

at that temperature,

Ci\Docurncnls 0nd Scllitrgsirnhnmptol\Dsktop,Pt oiects\Field Folnìs2ìDO-ORP-Crlibrål ¡ôh Fol [ì doc

DATElrrun/dd/w)

TIMEfhr':rnin)

TEMPDEGC

CHART IOO%

VALUEINSTRUMENT

RESPONSE%DEV

PASS/FAIL

CALIBRATED(YES, No)

TYPE(INIT. CONT)

SAMPLERIN]TIALS

2t6/08 l\31 2-rorR 8.otz- 8o 10.3 t\ ì-\5 INIT MH

26/oB'-13'7

zt.Í'ì 8l28 Í, I itl ¿: o'3 tr l'è c-¡FINAL MH

ORP

2tú08 t\,t1 Z\o-"(tl 'ZrT Ltv 5 l0 mV ç'" $<l INIT MH

2t6to\ r5.ÍO z<,'ì{ 'Z rt Z rS5 10 mV Þ N,s FINAL MH


Pase < of ¿/

Field Instrument Conductivity Calibration Records

TNsTRIIMENT (MAKE/N4oDELNo,) yslss6MPs INSTRTJMENT ¡7s. uisf

t

f o"t t a

STANDARD INFORMATIONproject Number:@Project Name: Cvpress Acres LandfÏll / Veolia

Standard Vendor: GEOTECII

Prepared Date: UKN Where Prepared: Golder Associates Inc.

Grade: NA Units:-@Standard

Standard

Standard

Acceptable calibration check is if the meter reacls within +l- 5% of the appropriate calibration stanciarcl,

c;\Doc['ncDts ud seltinBs\D]ltîil1plon\Dcsktop\l)¡o.ìeclslField FoDls2ìc:otrduclivity-c¡libralion !'orlnl ?9 07 doc

DATElmm/dd/w)

TIMElhr':rnin)

TEMPDEG CO

STDVALUE

INSTRUMENTRESPONSE

% DEVPASS/FAIL

CALIBRATED(YES, No)

TYPE(INIT, CONT)

SAMPLERINITIALS

z6toB I lL\( z.S;'ìl 84 q& )s% P þ: INIT MH

2t6t08 \ r-t3 24.é 500 -t'78 7 VLç INIT MH

216/08 I ìLtl Z{..l( 2000 '7tcoZ ç. bss INIT MH

216l0B f s-39 zÇ'1o 84 ft ¿5% P ñ6 FINAL MH

2ß108 , s-'f I zç.1"1 500 s-os ¿- 5% Þo FINAL MH

2t6108 tfr/( ¿S.elLl 2000 Zs oLL ¿_ 5% P Nd FINAL MH

Golder Associates - REV-z-03/07

Page I ofl

tr'ield Instrument pII Calibration Records d ITN5TRuMENT (MAKE/Ty1ODEL NO.) YSI ss6 MPS INSTRUMENT NO,trSj' t loztîrr

STANDARD INFORMATION

Project Number: 993-3902-G 0001 Project Name: cvpress Acres Lan


Prepared Date:-lKN Where Prepared: Golder Ässociates fnc.

Purchase Date: See Below Expiration Date: See Below Grade: UKN Units: Standard Units

Standard 4.01

Standard

Standard

DATElmrn/düwì

TIMElhl':¡nin)

TEMPDEG C

STDVALUE

INSTRUMENTRESPONSE

%DEVPASS/FAIL

CALIBRATEDIYES. NO)

TYPE(tNrr, coNT)

SAMPLER]NITIALS

216/08 lr\fl ¿s95 7.00 ì ,'?- O ¿.0.2 F Y*Ç INIT MH

2/6/08 ìf5'þ zí,98 401 3 ^81¿ <0.2 P \Þq INIT MH

216/08 (sL zkK- 100 ci.8 { <0.2 P V*S INIT MH

2t6t08 , sns )( ì'i '1.00 ?.1( ¿ 0.2 h'o FINAI MH

216108 r S{e t-( .8Y 401 LI t,t., ,1 0.2 ñc-, FINAL MH

2t6tj\ /s'(ì LS à\ 10.0 I ,is ¿- 0.2 't)h-¡cr FINAL MH

Acceptable calibration check is if the meter reads within +l- 0.2 pI{ units of the value of appropriate

calibration standard.

C:\DocumeDls 0Dd Sell¡tr8shhîrnploDìDesklopiPrcjccls\Field Fotrrs2\Ptl-Cûlibmt¡on Fomr3 29 0? doc


l.iqtrilrmcrrt St:r'vi ccs Pt'ogratr-tJack,sollviììe, FL

Calibration Stanclarcl s f)ata

Uscd drrtiug:tt/ztlo7 to current

NRTCO

TlìcrÌrolìreter4.O1 7 1o 8, 50( ?o0 0 220 o,1- 10 11.O-40 41 O-r00 >loo

Celcirrs pl.l DI-l )Ì mS/cnr trrS/cnr Drs/crì Dì\¡ NTU N I'U NTU NTU

1t0,o1Ç 2.50 250 250 250 250 IÕ 5

Dcgrces C nì/L Dì/L ur/L rr/l- rì/l lìì// l, nì/1, ¡/L ùiL ì/L Ìì/L

240r ZA,ttt4 7^lìo02 7^lo8tl TAKoqJ 7iU(0q3 7i\K092 72O62ij 6rlr 6r0o 6lo8 6r0l

f\fnr '04 I Ll uku t (ì kì lur ukì rkl Lu(n rk: ukn tì\ì

IUn) 'orl No\ -o7 No\ -(l; N0\-o7 No\-o7 No\ -07 No\-o7 Lhr r lur rhn

Oct'oó uli l Llir tJr rkl t tl tkl uit 200 b zÒo6 2oob :000

Oct'07 (jct-o9 AUA-o9 Sel)-o9 No\ -ou N(,,\ -otl J rì-otl /\l)r. oB ¿\l)r. ou Aì)r. otl Àpr, ull

lrf s¡:ient itic (ìeot('cl) (ì notcr:h (ìc0tü:l) (ìcol eclt (;n0lcclì (icotech (ìcolcch ticotcclì (ìcotcch (ieoteclt

hfscicntific tìoìdrr Goltlt'r ( ìoldel ("older (ìol(l('l (ìolrlc: (;ul(l('l llnch I lrr:lr I l¡ch

AccclrtiùìceCì:itèi'ia

r /- 0.2.c zT i IS . /- sli *¡'- t0t:t\¡ r /'- l(l'lô /Bo6 '/- 6 5rt l- i'ti

Nù rúlìtliûns ll i lDix( r'ì ol (r ¡ill rlrl ill (;ol(ìcl

U:\Matt Nagy\CALIBRATION\Caliblation Standalds lìecot'd 1|-21-07 to cunent.xls

APPENDIX B

Monitoring Well & Piezometer Installation Logs

STATE OF FLORIDA PEBMITAPPLICATION TO CONSTRUCT.REPAIR, MODIFY OR ABANDON A WELL

E Soulhwest THIS FOBM MUST BE FILLED OUT COMPLETELY.q Northwestd St. JOhnS RiVer ThewatetwellØn!Êdorisrespoæiblelorcompletìng- ^ lh¡slomandloryad¡ngthepemittotheappopíaleI'JOUInFl0rlOa debgetedæun¡ywheréappitiuøt.ú Suwannee BiverCHECX 8OX FORÁPPROPaIATE DISIRICTADORESS ON BÂCK OF PERMfT FORM

p6¡¡¡1¡6. 770127

Florida Unique l.D.

Permit Stipulations Requhed (See attached)

62-524 Quad #-Delinealion #

ABOVE THIS LIINE FOR OFFICIAL USE ONLY

Owner, Legal Name of Ent¡ty ¡l Cotporial¡on

Well Locatlon _ Address, Boad Name or number, Clty

Well Ddl¡lng Gontracto¡

35920 STATE FOAD 52

Telephone No.

4.- 1t1or

-lnorsection

22nft U09ðr

(tndt€to Weil on Chart)

5.Township 14 Range 22

tt

ttt-r-1-'t-

rtt-¡.-¡-{-rtt-J.-t-J-rtt

7. Number of proposed wells Check the uss of wèll: (sê. bad(or p€mr tDr sddir¡onol ch.iÉ) Domêstlc Monitor (typa) /

lrrigation (Type) Public Water Supply (type)(se! Brdr) {Sæ Bekl

List Other

Distance from septic system 0 ft. Descrlpllon of faclllty Estimaled start of construction date 1l28l2oo8I

8. Appllcatlon for: V New Construcllon

-

Repalr/tvlodlfy

-

Abandonment

'Fõã;õñõ¡ÃEã;Aõãñ;;ì_9. Estimaled: Well Depth e3 Casing Deplh 8a Screen lnterval from 8a to 93

Caslng Materlal: B¡øqXü / 6Xl / PVC Casing Diamet€r ,*ã¡õi Seal Mater¡al Bentonlte

0. lf appllcablo: Proposed From 0 to 05 Seal Materlal Cement Recelv€d: Frlday,

Grouting lnterval From_ lo _ Seal Matêrlal

From- to

-

searMarerrar ";:i"""ffi";:tr#tr:i:1,,#/Jfl*:Ei|#Ì#"i;!##.*"'"1. Telescope Casing

- or Liner- (check one) Diameter-

Blk-Steel / Galvanized / PVC Other (speclfyì-2, Method of Construcllon: / Rotury- Cable Tool- Combinalion

Auger

-

Other (specifyJ

lndlcate total No. ol wells on slte 9 List number of unused wells on slte o

ls thls well or any other woll or water withdrawal on lhe owner,s contlguous properly,coveredunderaConsumptiveMaterUsePermit(CUP/\Á/UP)orCUPI1VUpApptication? r/ No_yæ(IF YES, COMPLEIE THE FOLLOWNG) CUP/VVUP

District well l.D. No.

Latitude 2so 15'54.07" Longltude 62" s's7.27'

Data oblalned lrom GPS _ or map _ or survey _ (map datum NAO 27_ NAD gg )

5' I h'Þby ædify thal I 5 ol .tìllc

40. Fld¡.Ja Ádmíni:kålivc Cod. I cctify lhãl I om lho ohor of tho propdty. lhðt lho ¡ñlomat¡on p.ovidcd ¡s @u¡al€, ad that I sm ãwe ot mytnd lhâl ! w!l'r us ¡l n.sdôd. håsb€.n o.w¡ll b€ oblå¡nèd ispoí¡ib¡¡i¡e¡ un¿¡rc¡¡ptcrgzg, Flo¡idå Salutor, to mahuin'oiproporly ablndoi this woll¡ or, I ærtily thal í ampr¡or ùt ffiæh @rtfy lhel åll i¡lorm¡üh provid.d q thi! lhc'elou lor úre om¡r, ltr"t th" inio-utitn p.ø¿Ji""ã-r",

"'n¿ u*f I h¡È intftd lhê dfrr olhÌs ¡!-

rpp[cålion ¡s acur¡16 åñd thàt t w¡ll oblah¡êøgovdnhenb, ¡l€Fpl¡ebl€, I .gr.e to provide a wsllámùlíon ¡€port to th6 Oislrià wilhiñ 30 dar6atl.r drillng ø lhâ p€mit ôxpiåtion. whkhâv.¡æors lirs¡.

Dloltallv SIqn€d

Norlh

sSllc ls Norlh ol72nd Plece on NE

33rd

DO NOT WRITE BELOW THIS LINE . FOR OFFICIAL USE ONLY

Approval Granted By: GYNOI BELLINGAF STÄTUS: lssUED lssue Date: HydrologistApprou"l ¡;¡i¡;¡;

Owner Number: Fee Receivad: $ 25.00 Recelpt No.: 1N082746109 Check No.:

THIS PERMIT NOT VALID UNTIL PROPERLY SIGNED BYAN AUTHORIZED OFFICER OR REPRESENTATIVE OF THE WMD. IT SHALL BE AVAILABLE ATTHEWELL SITE DURING ALL DRILLING OPERATIONS. Iàrs perm il is vattd lor 90 davs from the dale ot issue.

WHITE: oBIGINALFILEYELLOW: DHILLINGCoNTFACTOBPINK: OWNEB

FoRl\r 41.10 - 410 (1) REV 12lO4

WELL COMPLETION REPORT (ptease comptete in btack ink ortype-)PERMTT#i 770127jlndicate the number of wellslndicate the number of wellscancelled:

WATER WELL CONÌRACTOR'S

License# 9342ft is accunle and true.

WELL LOCATION: Countlr Marion

_1l4of _'ll4 of Section 22 , Township 14 . Rrng"lz_-

COMPLEIION DATE: 01i29/2008 Florida Unioue LD.:Parcel#(Pin): 14864-001-00

oWNER's NAME: SUPERIOR SERVICES INC

WELL USE:

[ ]PublicSuppty [ ]tnþation[]lnjection[ ]Other

DRILL METHOD:

I lRotary [ ]CabteToot[ ]Jet ffiAuger

lDomestic ffi Monitor

lCombinationI Other

Latitude: 29" 15' 54.07"

DATE STAMP

Feb 07 2008

Official Use Onty

Longitude: -82" 5' 37.27"

Driller's Name (print or type): Kryin Reftuse

G¡ouf No. of Baqs From lft.l To lft.lNeat Cement: 25 0 88

Benlonite; 1 88 93(Other)

Measured Static Water Level: Measured pumping Water Level: _After _Hours at _GPM. Measuring pt. 1ò"j0"¡:Which is ff- [ ] above ffi belovv land surfaceCasing:[ ]BlackSteel [ ]GaÀ,anized XpVC [ ]Other:_[ ]Open Hole

[ ]ScreenDepür

(feet)DRILL CUTTINGS LOGExamine cuftings every 20 ft. or at

Casing Diameterand Deptì (ft.)

From To depth to producing zones.

Colú | craîn gze 1 Type ú Material

Diameter: 2F¡om: 0To: 88

) 60 oEnae rct appl¡q€bte dev

t0 70 oËnænetapplic€bleclavevllmestm

70 93 white not apoüæble limesloneDiameier: 2Fror: -8F-To: 93

Liner[ ]øCasing [ ]Diameter:From:_To: _

Chlorides: _ ppm TDSConductivitv'' ìmfiõ-s/cm-

Skelch of well localion on popøty

Give dishnces fiom septic bnk and house, orother reference points

PIEZOMETER INSTALLATION LOG

Cw¡ess Acres Lædfill / Veolia WELLNO PZ.l SHEET I OF

GROUNDELEV NA WATERELEV. 40

COLLARELEV NA DATE/TME

INVENTORY

CASING I in dia 4 lf. WELL SCREEN I in dia l0 I f. BENTONITE SEAI

ASING TYPE Schedule 40 PVC SCREEN ryPE Schedr¡le 40 PVC INSTALLATION METHOD

TYPE Fluh-th¡eaded SLOTSÍZE 0010'i¡chslot FILTERPACKQry

QUANTTTY@ CENTRALIZERS None FILTERPACKTYPE 2oßosilica

ROUT T\?E NONC DRILLING MUD TI?E NONC INSTALLATION METI{OD

ELEV./DEPTE

SOIL/ROCK DESCRIPTION WELLSKETCE INSTALLÂTION NOTES

30-

00-

l0 0-

20 0-

30 0-

G¡omd Surface

Monitoring wel I set to 50 0 ft bgs, I 0 ft Sqeen

I " d¡À.

Sch. 40PVC

l" dia. -0.01 0-inchslottedscfæn

500

IVELL DEVELOPMENT NOTES

50 0-

Date: NA

Development Time : NA

Developm€nt Raie: NA

PugeVolme: NA

Final Tubidig: NA

Boring Temimted at 50 0 feet bgs

Golder Assoc¡ates

PIEZOMETER TNSTALLATION LOG

No.j@li PRoJEcT---..lqyggrylcreslmdf¡ll/Vælia wELLNo Pz-2 sHEEr I oF I

INSPJLDNLLINGMETHoD@GRoUNDELEVNAITATERELEV

THER _.S.¡ggL DRILLINGCOMPANY _ P¡obeDomain CoLLARELEV NA DATE/TIME

65 F DRILLRIG 66loDT STARTED l:l1PMl t,28?0o8 COMPLETED 2:zoPMl 1128/29:08

CASING I in dia 4l lf WELLSCREEN I in dia l0 lf. BENTONITESEAL

TYPE Schedule4OPVC SCREENTYPE Schedule40PVC INSTALLAIONMETIIOD NA

TYPE Flwh-threaded SLOTSIZE 0O10-inchslot FILTERPACKQTY

QUANTITY

-@-

CENTRALTZERS- None FILTERPACKTYPE

T\?E None DRILLINGMUDTYPE None INSTALLATIONMETHOD

ELEVJnEpm SOIL/ROCK DESCRIPTION \ryELL SKEÎCE INSTALLATION NOTES

30-

00-

l0 0-

200-

30 0-

Gromd Surfaæ

Monitori¡g well set to 48.0 ft bgs, l0 ft Screm

l" dia.

Sch. 40PVC

l. diÀ -0 01o-inchslottedscreen

20ß0Smd Pack

480

WELL DE!'ELOPMENT NOTES

50 0-

Date: NA

Development Time: NA

Development Rat€: NA

PugeVolme: NA

Final Tubidity: NA

Boring Teminated at 50 0 feet bgs

Golder Assoclates

NO 993-3902-G PROJECT Cvpress Acres Lmdfill / Vælia WELLNO. PZ.3 SHEET I OF

rNsP___-lgg_ DRILLING METTIOD Direct Puh Technolow - DPT GROUNDELEV NA WATERELEV

COLLARELEV NA DATEÆIME

STARTED 2:4sPMl U2812o08 COMPLETED

Swy

65F

DRILLING COMPANY

DRILL RIG

Probe Domai¡

66 l oDTTIME/DATE TIME/DATE

PIEZOMETER INSTALLATION LOG

CASING I in dia 43 lî. I india l0 lf.

Schedule 40 PVCASINGTYPE Schedule40PVC

FILTER PACK QTY

FILTER PACK TYPE

ELEVJnnìm 1VELL SKETCH INSTALLATION NOTES

30-

o0-

l0 0-

20 0-

30 0-

40 0-

G¡omd Su¡face

Monitoring well set to 50.0 ft bgs, 1 0 ft Sc¡een

l" dia. -0.01o-inchslottodscreen

20t30Sod Pack

500

WELL DEVELOPMENT NOTES

Date: NA

Development Time: NA

DeYelopnmt Rate: NA

Puge Volme: NA

Final Tubidity: NA

Boring Teminaæd at 50 0 feet bgs

Golder Assoc¡ates

RECORD OF BOREHOLEPROJECT: Cypress Acres Landfill DRILL METHOD: Mud RotaryPROJECTNUMBER:993-3902-G.0001 DRILLRIG:Fa¡ling'1500DRILLEDDEPTH:93.0ft DATESTARTED: f/28/08

MW.gD SHEET'I of 2

DATUM: GeodeticCOORDS: notsurveyedGS ELEVATION:N/ATOG ELEVATION:N/ATEMPERATURE: 70. F

AZIMUTH: N/ALOCATION:

DATE COMPLETED:'l I29lO8WEATHER: Pafilv Cloudy

I

0-

5-

'10 -

't5 -

20-

25-

30-

J5-

40-

45-

50

z

keÈ-.d

SOIL PROFILE SAMPLES MONITORING WELUPIEZOMETER

DIAGRAM and NOIES

5'srickue- lil¡l ¡çlffi|l ffif

WELLCONSTRUCTION

DETAILSDESCRIPTIONtt,q <YÉ-o

ELEV. É.u@

fz

UÈBLOWSper 6 in

'l,l0lb hsmmer30 lnch droÞ

N

t-kC)uDEPTH

(fD

00-õ2.0no lilhology tsken

PortlandCsmênt Type+

,|

2" well casing-

6" cas¡ng4

WELL CASINGlnlervol: 6" diameter - 0-85 fl

bgs; 2" diam€ter- 0-88 ftDgs

Mster¡êlì Schedulê 40 PVColameter: 6' snd 2'Joint Typs: 6-- Slip Joinl; 2L

Flush lnter¡or Thresded

WELL SCREENlnlerval: 88-93 fl bgsMsterlsl: Schedule 40 PVcOlameter;2 lnchesSlol siz€r 0.010 inchEnd C€p:4.5" sump point

FILTER PACKlnteryal: 06-93 fl bgsTyp€: 20-30 slandard silica

sandQuantlty: 7 bags

FILTER PACK SEALlnteruâl: 84-86 fl bgsType: Bentonlte 3/8" Hole

Plug pelletsQuanlily: 2 bâgs

ANNULUS SEALlnteilal: 0-84 ft bgsType: Polland Cement TYpe

1

Quanlity:1 l bags

Development Notes'1550- lnitlate development'1640- End developmenl- 50 gallons purgedPurge rate = -'1 gpm

LOG SCALE: 1 in = 6.5 ftDRILLING COMPANY: Huss Drilling

DRILLER: Kevin/ Tony

GA INSPECTOR:

CHECKED BY: R,

DATE: 3/20/08

J. Klng

Poff

RECORD OF BOREHOLEPROJECT: Cypress Acres Landlill DRILL METHOD: Mud RotaryPROJECTNUMBER: 993-3902-G ,0001 DRILLRIG: Failinq 1500DRILLED DEPTH: 93.0 ft DATE STARTED: i/28/OS

MW-gD SHEET 2 of 2

DATUM: GeodeticGOORDS: notsurveyedGS ELEVATÍON: N/A

TOC ELEVATION: N/¡TEMPERATURE: 70. F

AZIMUTH: N/ALOCATION:

DATE COMPLETED: 1/29/08WEATHER: Pârllv Clôudv

I[ü

60

70

/þ-

*:

I-.1

Ie0 -l

IlI-l

-lI

1I*l

-lI-1

III

11oo -l

zokãu.¡

U

SOIL PROFILE SAMPLES MONITORING WELUPIEZOMETER

DIAGRAM and NOTES WELLCONSTRUCTION

DETAILSOESCRIPTION!)Ø <YÉ-

ELEV. É.U

f2

U

¡BLOWSper 6 in

140 lb hammlr30 Inch drop

N

r

UDEPTH(ft)

no llthology têkenlconløued)

Benton¡lep€ll€ts

20-30

sil¡ca ssnd

WELL CASINGlnterval:6" d¡ameter - 0-Bs fl

bgsi 2" dlâmetetr 0-88 ftbgs

Material: Schedule 40 PVCDiâmeter: 6" and 2 "Joinl Type: 6'! Slip Joint; 2a

Flush lntêr¡or Thresded

WELL SCREENlnteryÊl: 88-93 fl bgsMateriâl: Schedule 40 PVCOlamet€r: 2lnchesSlot Slze:0 010 lnchEnd Cap:4.5" sump po¡nt

FILTER PACKlntervel: 86-93 fl bgsType: 20-30 standard s¡l¡ca

san0Ouanlil.y: 7 bags

FILTER PACK SEALlnterual: 84-86 ft bgsTyps: Bentonlte 3/8" Hole

P¡ug pellelsQuant¡ty:2 begs

ANNULUS SEALlnlerval: 0-84 lt bgsType: Porlland Cement Type

1

Quantilyi 1 1 bags

tiz,u - b4,uposs¡blê VOID

62.0

no l¡lhology lakenö4.U

tu g - l4.t)light tan to very light Lan silty wealheredLIMEROCK, [rac€ gravsl sizêd limerockpices, trace fines from 71-72 ll bgs

70.0ss 17-17-31-13 48

ss 7-15-39-15 >50 20

74.0 - 80.0posslbl€ VOIÞ, no recovery

74.O

SS 19-15-25-30 40 20öu,u - Y1,ulight orange lo lighl tan LIMEROCK andLIMEROCK SAND, (% competenl limerockestlmated al2540%, in line to coarse gralnllmêrock matrlx. litlle flnë

80.0

ò

ãqI

2

(t)UÉ,ooÉ.

oU>UJcãU'

E3

ss 35-50/4 50/4 10

50t2 5012 10

ss 25-34-37-27 >50 20

f ss 7-35.50/3 >50 10

v Lu - Yó.u 91 0 ùù 34-5012 5012 10

vJ.u: oeorocKBoring complet€d at 93.0ít

LOG SCALE: 1 ln = 6.5 ftDRILLING COMPANY: Huss DrillingDRILLER: Kevin/ Tony

GA INSPECTOR: J. King

CHECKED BY: R. PoffDATE: 3/20108

APPEI\DIX C

Hyd raulic Gradient Calculations

,a

' N Ltt i. ..v Átt,

r 4-\c ii . 'i

"uo.., 4rJr-Jí. é*Jr.Å, Cr^Q,,^-Ç[r-rZJobN't 9gßgavGRst-

Dare Z/ tfls8-shoot

/ or

t

ü ?3ct fGtr

3-ú r tô-'t F{i- / îaoT

Þ .=L***.. \..-\** t*....{rr \f.^ 1¡J -16 R o,*-\\

c¿*\,=r oS- cç-æìt\, :

r..a\\ 5c-,t<-€ri*

,r-(-

APPENDIX D

Laboratory Analytical Reports and Chain of Custody Forms

TestAmericor}.lE LEAOËR IN IìNVIRONMËNTAL TäSTING

ANALYTIGAL REPORT

Job Numb er: 640-1 4947 -1

Job Description: Cypress Acres

For:Golder Associates lnc.

9428 Baymeadows RoadSuite 400

Jacksonville, FL 32256

Attention: Mr. Rich W Poff

Designee forChad Bechtold

Project Manager I

chad. [email protected]

These test results meet all the requirements of NELAC. All questions regarding this test report should be directed to theTestAmerica Project Manager who signed this test report.Measurement uncertainty data, as referenced in Section 8.6 of the TestAmerica Tallahassee LQM, are available uponrequest.

Florida Department of Health Certification No. E81005Mobile DOH Certification No. E87089

TestAmerica Laboratories, Inc,

TestAmerica Tallahassee 2846 lndustrial Plaza Drive, Tallahassee, FL

Tel (850) 878-3994 Fax (850) 878-9504 www.testannedeai¡ç.com

Page 1 of 30 02/08/2008

Job Nar¡ative640¿14947-1

CommentsNo additional comments.

ReceiptChain of Custody listed 8260, this analysis is not needed and no containers were submitted COC revised per client request

All samples were received in good condition within temperalure requirements

MetalsMethod(s) 200.7 Rev 4.4, 60108: ln method 60108, 200.7 the method blank for prep.batch # 64041340 contained Fe above the method

detection limit. This target analyte concentration was less than the reporting limit (RL); therefore, re-extraction and/or re-analysis ofsamples was not performed. Associated samples flagged "V".

No other analytical or quality issues were noted.

General ChemistryMethod(s) 350.1: The method blank for batch 41499 contained ammonia above the method detection limit. This target analyte

concentration was less than the reporting limit (RL); therefore, re-extract¡on and/or re-analysis of samples was not performed. All

associated samples were below the RL and are flagged "lV"

Method(s) 375.4: Batch 41527:The matrix spike / matrix spike duplicate (MS/MSD) recoveries (129%1129yo) for sample MW-5

(640-14947-3) were outside control limits (85-1 15%). The associated laboratory control standard and laboratory control standard

duplicate (LCS/D) met acceptance criteria. MS and MSD data flagged "J".


Page 2 of 30 02/08/2008

EXECUTIVE SUMMARY - Detections

Client Golder Associates lnc.

Lab Sample lD Glient Sample lD

Analyte Result / QualifierReporting

Limit Units

Job Number: 640-14947-1

Method

640-14947-l MW-2

Total Dissolved Solids

ChlorideAmmoniaNitrate Nitrite as N

Nitrate as N

Tolal Recoverable

AluminumChromiumtron

Sodium

640-14947-2 MW-7


ChlorideAmmon¡aNitrate Nitrite as N

Nitrate as N

Total Recoverøble

AluminumChromiumlronSodium

640-14947-3 MW-s



N¡trate as N

Total Recoverable

ChromiumSodium

I

IV

Àn

1.0

0.0200.0200.010

200'10

50

1 000

5.01.0

I V 0.0200.0200.010

I 10

1 000

1203.2

0,00580.43

043

1202.3

220

2800

2105.6

0.00520.420.42

5¿1q

31

3500

200F7

0.00880.470.47

1.9

3800

5.0

1.0

0.0200.200.010

20010tn

1 000

mg/Lmg/Lmg/Lmg/Lmg/L

ug/Lug/Lug/Lug/L

1 60.1

325.2

350.1

353.2

Nitrate by calc

601 0B

601 0B

601 0B

601 0B

1 60..1

325.2

350.1

353.2

Nitrate by calc

601 0B

601 0B

601 0B

601 0B



ug/Lug/Lug/LugiL

ug/Lug/L

1 60.1

325.2

350.1

353.2

Nitrate by calc

601 0B

601 0B

TestAmerica Tallahassee

Page 3of30 02 / o8 /2008

EXECUTIVE SUMMARY . DEtECtiONS

Client: Golder Associates lnc.

Lab Sample lD Glient SamPle lDAnalyte Result / Qualifier

ReportingLimit Units

Job Number: 64A44947-1

Method

640-149174 MW-6

Total Dissolved SolidsChlorideAmmoniaNitrate Nitrite as N

Nitrate as N

Tolal Recoverøble


160

4.40.00460,31

0.31

33

2.6tz3000

5.01.0

0.0200.0100.010

20010

1 000


160.1

325.2

350.1

353.2

Nìtrate by calc

601 0B

601 0B

601 0B

601 0BIV


Page 4 of 30 02/08 /2008

METHOD SUMMARY

Client: Golder Associates lnc. Job Number: 640-14947 -1

Matrix: Water

lnductively Coupled Plasma - Atomic Emission Spectrometry

Acid Digestion of Waters for Total Recoverable or

Mercury in Liquid Waste (Manual Cold Vapor Technique)

Mercury in Liquid Waste (Manual Cold Vapor

Residue, Filterable, Gravimetric, Dried at 180'C (TDS)

Chloride (Colorimetric, Automated Ferricyanide)

Nitrogen (Ammonia, Colorimetric, Automated Phenate)

Nitrogen, N¡trate-N¡trite (Colorimetric, Automated, CadmiumReduction)

Sulfate (Turbidimetric)

Phenolics (Spectrophotometric, Manual 4-AAP with Distillation)

Distillation/Phenolics

Nitrogen, Nitrate-Nitrite (Colorimetric, Automated, Cadmium

Reduction)

Lab References:

TAL SAV = TestAmerica Savannah

TAL TAL = TestAmerica Tallahassee

TAL TAM = TestAmerica Tampa

Method Refe¡ences:

MCA\ ^¡v

= "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.

SM-Online = Standard Methods Online

SWB46 = ',Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And lts Updates.

TAL TAL

TAL TAL

TAL TAM

TAL TAM

TAL TAL

TAL TAL

TAL TAL

TAL TAL

TAL TAL

TAL SAV

TAL SAV

TAL TAL

sw846 60108

sw846 30054

sw846 74704

sw846 74704

MCA\ ^/\/

160.1

MCA\ A/V 325.2

MCA\ ^/v

350.1

MCA\ ^/V

353.2

MCA\^^/v 375.4

MCA\ ^/v420.'l Distill/Phenol

SM-Online N¡trate by calc


Page 5 of 30 02/08/2008

640-14947-1 MW-2

640-14947-2 MW-7

640-14947-3 MW-5

640-149474 MW-6

SAMPLE SUMMARY

Client Golder Associates lnc. Job Number: 640-14947-1

Date/Time Date/Time

Lab Sample lD Client Sample lD Client Matrix Sampled Received

01t2912008 1007 01/30/2008 0850

01t29t2008 1.149 01/30/2008 0850

01t2912008 1417 0'l/30/2008 0850

01t29t2008 1651 01130/2008 0850


Page 6 of 30 02/ o8 / 2Oo8

SAMPLE RESULTS

TestAmer¡ca Tallahassee

Page 7 of 30 02/ 08 /2008


Glient Sample lD:

Lab Sample lD:

Client Matrix:

MW.2

640-14947-'l

Water

Analytical Data

Job Number: 640-14947-1

Date Samoled: 0112912008 1007

Date Received: 01/30i2008 0850

60108 lnductively Goupled Plasma - Atomic Emission Spectrometry'Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Analyte

601 0B

300541.0

0210512008 1250

02t04t2008 0630

Analysis Batch: 64041437

Preo Batch: 640-41340

Result (ug/L)

lnstrument lD: ICP Trace

Lab File lD: FEBRO8

lnitial WeighWolume: 50 mL

Final WeighWolume: 50 mL

Qualifìer PQL

AluminumArsenicCadmiumChromiumlronLead

't20

4.20.462.3

220

2.0

sodium 2900

U

U

U

zt4.20.461.5

4.6¿-u

220

200l05.0

10

50

5.0

1 000

74704 Mercury in Liquid Waste (Manual Gold Vapor Technique)

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Analyte

74704747041.0

02/05/2008'150302/05/2008 0918

lnstrument lD:

Lab File lD:

lnitial WeighWolume:

Final WeighWolume:

Hg Analyzer

N/A

25.0 mL

25.0 mL

Analysis Batch: 660-571 94

Prep Batch: 660-57155

Result (mg/L) QualifÌer MDL PQL

Mercury 0.000072 0.000072 0.00020

TestAmerica Tallahassee Page I of 30 02/08/2008


Client Sample lD:

Lab Sample lD:

Client Matrix:

MW-7

640-14947-2

Water

Analytical Data

Job Number: 640-14947-1

Date Sampled: 0'112912008 1149

Date Received: 01/30/2008 0850

60108 lnductively Goupled Plasma - Atomic Emission spectrometry-Total Recove¡able

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Analyte


Sodium

601 0B

300541.0

0210512008 1252

02i04/2008 0630

Result (ug/L) Qualifìer MDL PQL

u 4.2 '10

u 0.46 50I 1.5 10

4.6 50



420.461.9

31

2.0


Lab File lD: FEBRO8



IVu 2.0 5.0

220 1000

7¡l7OA Mercury in Liquid Waste (Manual Cold Vapor Technique)

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Analyte

7470474704

1.0

02t05t2008 '1504

02l05i2008 0918

lnstrument lD:

Lab File lD:


Final WeighUVolume:

Hg Analyzer

N/A

25.0 mL

25.0 mL

PQL

0.00020


Prep Batch:660-57155

Result (mg/L) Qualifier MDL

ô-öôoii72 *

Mercury 0.000072

TestAmerica Tallahassee Page 9 of 30 02/ 08 / 20O8


Client Sample lD:

Lab Sample lD:

Client Matr¡x:

MW-5

640-14947-3

Water

Analytical Data

Job Number: 640-14947-1

Date Samoled: 0112912008 1417


60108 lnductively Goupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Analyte

601 0B

30054

1.0

02/05/2008 1309

02t04t2008 0630



Result (ug/L)


Lab File lD: FEBRO8



PQL

AluminumArsenicCadmiumChromiumtron

Lead

Sodium

21

4.20.461.9

4.62.0

3800

Qualifier MDL

4.2

0.464F

4.6¿.u

220

U

U

U

U

U

20010

5.0

10

50

5.0

1 000

74704 Mercury in Liquid Waste (Manual Cold Vapor Technique)

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Analyte

74704

7470Á'

1.0

02/05/2008 1506

02/05/2008 0918

lnstrument lD:

Lab File lD:


Final WeighWolume:

Hg Analyzer

N/A

25.0 mL

25.0 mL

PQL




Mercury 0.000072 0.000072 0.00020

TestAmer¡ca Tallahassee Page 10 of 30 02 / 08 /2008


Client Sample lD:

Lab Sample lD:

Client Matrix:

MW-6

640-14947-4

Water

Analytical Data

Job Number: 640-14947-1

Date Samoled: 0112912008 1651


60108 lnductively Goupled Plasma - Atomic Emiss¡on Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Analyte

601 0B

300541.0

02t05t2008 1311

02104/2008 0630

Analysis Batch: 640-41437

Preo Batch:640-41340

Result (ug/L)

lnslrument lD: ICP Trace

Lab File lD: FEBRO8



Qualifier MDL PQL


Sodium

4.20,462.6

12

2.03000

U

U

IVil

21

4.20.46,tÃ

4.62.0220

200

10

5.0

10

1 000

74704 Mercury ln Liquid Waste (Manual Cold Vapor Technique)

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Analyte

7470474704

1.0

02/05/2008 1508

02/05/2008 0918

lnstrument lD:

Lab File lD:


Final WeighWolume:

Hg Analyzer

N/A

25.0 mL

25.0 mL

PQL




Mercury 0.000072 0.000072 0.00020

TestAmerica Tallahassee Page 11 of 30 02/08/2008


Analytical Data

Job Number: 640-14947-1

Client Sample lD: MW-2

Lab Sample lD: 640-14947-1

Client Matrix: Water

Analyte

General Ghemistry

Date Sampled: 0112912008 1007


Result Qual Units MDL PQL Dil Method

Chloride

Ammon¡a

Nitrate Nitrite as N

Sulfate

.t¿ mg/L 0.22 '1 .0

Anly Batch: 640-41256 Date Analyzed 01/31/2008 '1033

0.0058 I V mg/L 0.00075 0.020 1.0 350'1

Anly Batch: 640-41499 Date Analyzed 02l07l2OOB 1252

0.43 mg/L 0.0022 0.20 20 353.2

Anly Batch: 640-41512 Date Analyzed 0210712008 1551

1.3 U mg/L 1.3 5.0 1.0 375'4

1.0 325.2

Anly Batch: 640-41257 Date Analyzed 01/31/2008 1016

Phenolics, Total Recoverable 0.025 U mg/L 0.025 0.050 1.0 420'1

Anly Batch: 680-97390 Date Analyzed 02i06/2008 0801

Preo Batch:680-97389 Date Prepared: 0210612008 0752

Nitrate as N 0.43 mg/L 0.0001 1 0.010 1 .0 Nitrate by calc


Analyte Result Qual Units PQL PQL Dil Method

Total Dissolved Solids 120 mg/L 5,0 5.0

Anly Batch: 640-41353 Date Analyzed (start) 02104/2008 1147 (End) 0210412008 1217

1 .0 1 60.1

TestAmer¡ca Tallahassee Page L2 of 30 02 / 08 /2008


Analytical Data

Job Number: 640-14947-1

Glient Sample lD: MW-7



Analvte

General Ghemistry

Date Sampled: 011291200A 1149



Chloride

Ammonia


Sulfate

J.b


0,0052 I V mg/L 0.00075 0.020 1.0 350'1


mg/L 0.00022 0.020 2 0 353.2

Anly Batch: 640-41512 Date Analyzed 0210712008 '1601

1.3 U mg/L 1.3 5.0 1.0 375'4


mg/L 0,22 1.0 1.0 325.2

042

Phenolics, Total Recoverable 0.025 U mgil 0.025 0.050 '1 0 420 1

Anly Batch: 680-97390 Date Analyzed 02106/2008 0801

Prep Batch:680-97389 Date Prepared: 0210612008 0752

Nitrate as N 0.42 mg/L 0.00011 0.010 1'0 Nitrate by calc



Total Dissolved Solids 210

Anly Batch: 640-41 353 Date Analyzed (start) 02/04/2008 1 1 47 (End]. 0210412008 1219

mg/L 5.0 5.0 1 .0 1 60.1

TestAmerica Tallahassee Page 13 of 30 02 / 08 /2008


Analytical Data

Job Number: 640-14947-1

Client Sample lD:

Lab Sample lD:

Client Matrix:

Analyte

MW-5

640-14947-3

Water

Result

General Ghemistry

Qual Units

Date Samoled: 0112912008 1417


D MethodPQLMDL

Chloride

Ammonia


Sulfate

Phenolics, Total Recoverable

Nitrate as N

mg/L 0.22

Date Analyzed 01/31/2008 1033

I V mg/L 0.00075

Date Analyzed 0210712008 1301

mg/L 0.00022


U mg/L 1.3


U mg/L 0.025

Date Analyzed 02/06/2008 080.1

Date Prepared: 0210612008 0752

mg/L 0.00011


5.7

Anly Batch: 640-41256

0.0088


0.47

Anly Batch: 640-4'1512

1.3


0.025


Prep Batch: 680-973890.47


1.0

0.020

0.020

þ.u

0 050

0.010

10 325.2

350.1

353.2

375.4

420.1

Nitrate by calc

l0

20

10

10

10

Dit MethodResult Qual Units PQL

200 mgil 5.0 50

Anly Batch: 640-41353 Date Analyzed (sên) 0210412008 1147 (End) 0210412008 1222

PQL

1.0 1 60.1Total Dissolved Solids

TestAmerica Tallahassee Page 14 of 30 02/ 08 /2008


Analytical Data

Job Number: 640-14947-1

Glient Sample lD: MW-6



Analyte

General Ghemistry

Date SamPled: 0112912008 1651



Chloride 4.4 mg/L 0.22 1.0 1.0 325.2

Anly Batch: 640-41256 Date Analyzed 01/31/2008 1033

Ammonia 0.0046 I V mg/L 0.00075 0.020 1.0 350.1


Nitrate Nitrite as N 0.31 mg/L 0.0001 1 0.010 1 .0 353 2


Sulfate 1.3 U mg/L 1.3 5'0 1 0 375'4

Anly Batch: 640-41257 Date Analyzed 0ll31i2008 1035

Phenolics, Total Recoverable 0.025 U mg/L 0.025 0.050 1.0 420'1

Anly Batch: 680-97390 Date Analyzed 02106/2008 080.1


Nitrate as N 0.31 mg/L 0.0001 1 0.010 1 '0 Nitrate by calc


Analyte Result Qual Units PQL PQL D¡l Method

Total Dissolved Solids 160

Anlv Batch: 640-41 353 Date Analyzed (Start) 02104/2008 1147 (Endl 0210412008 1224

mg/L 5.0 5.0 1 .0 160. 1


DATA REPORTING QUALIFIERS


Lab Section Qualifier Description

Job Number: 640-14947-1

U

I

lndicates that the compound was analyzed for but not

detected

lndicates the analyte was detected in both the sample and theassociated method blank.

The reported value is between the laboratory method detection

limit and the laboratory practical quantitation limit.

Estimated value; value may not be accurate.


detected.

lndicates the analyte was detected in both the sample and the

associated method blank.



General Chemistry

J

U

I


Page 16 of 30 02/ 08 /2008

QUALITY CONTROL RESULTS


Page 17 of 30 02/08/200s


Method BIank - Batch: 640-41340

Lab Sample lD: MB 640-41340/1-A


Dilution: 1.0

Date Analyzed: 0210512008 '1244

Date Prepared: 02104/2008 0630

Analyte



Units: ug/L

Result

Quality Control Results

Joþ Number: 640-14947-1

Method:60108Preparation: 30054Total Recoverable


Lab File lD: FEBRO8



PQL

AluminumArsenicCadmiumChromiumtron

Lead

Sodium

Lab Control Spike/Lab Gontrol Spike Duplicate Recovery Report - Batch:

21

4.20.464E

8.3

2.0220

640-41340

Qual MDL

¿t4.20.461.5

4.62.0220

U

U

U

U

I

U

U

20010Ãn

10

50

5.0

I 000

LCS Lab Sample lD: LCS 640-41340/2-A Analysis Batch: 64041437


Units: ug/L

Analysis Batch: 64041437Prep Batch: 640-41340

Units: ug/L

% Rec.

LCS LCSD



Lab File lD: FEBRO8

lnitial WeighWolume: 50

Final WeighWolume: 50


Lab File lD: FEBRO8



Client Matrix:

Dilution:

Date Analyzed:

Date Prepared:

LCSD Lab Sample lD:

Client Matrix:

Dilution:

Date Analyzed:

Date Prepared:

Water

1.0

02t05t2008 1246

02t04t2008 0630

LCSD 640-41340/3-A

Water

1.0

02t05t2008 1248

02/04/2008 0630

mL

ML

Analyte Lmt RPD Limit LCS Qual LCSD Qual

AluminumArsenic

Cadmium

Chromiumlron

Lead

Sodium

80 - 120

80 - 120

80 - 120

80 - 120

80 - 120

80 - 120

80 - '120

20

20

20

20

20

20

20

93

YJ

94

98

95o?

96

96

98

101

99

97oq

3

4

4

3

Calculations are performed before rounding to avoid round-off errors in calculated results.



Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 64041340

MS Lab Samole lD: 640-14947-2


Dilution: 1.0

Date Analyzed: 0210512008 1256

Date Preoared: 0210412008 0630

MSD Lab Samole lD: 640-14947-2


Dilution: L0Date Analyzed: 0210512008 1257


Analyte

Aluminum

Arsenic

Cadmium

Chromium

lron

Lead

Sodium

Duplicate - Batch: 640-41340



Dilution: 1.0


Date Prepared: 02/04/2008 0630

Analyte





Quality Gontrol Results

Job Number: 640-14947-1

Method: 60108Preparation: 30054Total Recoverable


Lab File lD: FEBRO8




Lab File lD: FEBRO8



Method: 60108Preparation: 30054Total Recoverable


Lab File lD: FEBRO8



% Rec.

MS MSD Limit RPD RPD Limit MS Qual MSD Qual

96 96 75-125 0 20

93 95 75-125 1 20

94 96 75-125 2 20

97 99 75-125 2 20

96 96 75-125 1 20

92 94 75-125 2 20

96 101 75 - 125 3 20



Units: ug/L

Sample ResulUQual Resull RPD Limit Qual

Aluminum

Arsenic

Cadmium

Chromium

tron

Lead

Sodium

52 I 48.9

4.2 U 4.2

0 46 u 0.46

1 .9 I 1.72

31 I 23.9

2.0 u 2.0

3500 3440

720NC20UNC20U12 20

25 20

NC20U120

Calculations are pelormed before rounding to avoid round-off errors in calculated results.

TestAmer¡caTallahassee Page 19 of 30 02/08/2008


Method Blank - Batch: 660-57155



Dilution: 1.0



Analyte



Units: mgi L

Result


Job Number: 640-14947-1

Method:74704Preparation: 74704

lnstrument lD: Hg Analyzer

Lab File lD: N/A

lnitial WeighWolume: 25.0 mL

Final WeighWolume: 25.0 mL

MDL PQLQual

Mercury

Lab Control Spike/Lab Gontrol Spike Duplicate Recovery Report - Batch: 660-57155

0.000072 u 0.000072 0.00020

Method: 74704Preparation: 74704

LCS Lab Sample lD: LCS 660-57155/2-A Analysis Batch: 660-57194 lnstrument lD: Hg Analyzer

Client Matrix: Water Prep Batch: 660-57155 Lab File lD: N/A

Dilution: 1.0 Units: mg/L lnitial WeighWolume: 25.0 mL

Date Analyzed: 02t0512008 1441 Final WeighWolume: 25.0 mL


LCSD Lab Sample lD: LCSD 660-57155/3-A Analysis Batch: 660-57194 lnstrument lD: Hg Analyzer



Date Analyzed: 0210512008 1443 Final WeighWolume: 25.0 mL


Analyte

% Rec.

LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual

Mercury 92 93 80-120 1 20

Calculations are performed before rounding to avoid round-off enors in calculated results.

TestAmericaTallahassee Page 20 of 30 02/08/2OOB



Lab Sample lD: MB 640-41353/1


Dilution: 1.0


Date Prepared: N/A

Analyte


Prep Batch: N/A

Units: mg/L

Result


Job Number: 640-14947-1

Method:160.1Preparation: N/A

lnstrument lD: No Equipment Assigned

Lab File lD: N/A



Qual PQL PQL

Total Dissolved Solids 5.0

Lab Control Spike/Lab Cont¡ol Spike Duplicate Recovery Report - Batch: 640-41353

5.0 5.0

Method: 160.1

Preparation: N/A

LCS Lab Sample lD: LCS 640-41353/2 Analysis Batch: 640-41 353 lnstrument lD: No Equipment Assigned

Client Matrix: Water Prep Batch: N/A Lab File lD: N/A

Dilution: 1.0 .Jnits: mg/L lnitial WeighWolume: 100 mL

Date Analyzed: 0210412008 1143 Final WeighWolume: 200 mL

Date Prepared: N/A

LCSD Lab Sample lD: LCSD 640-41353/3 Analysis Batch: 64041353 lnstrument lD: No Equipment Ass¡gned

client Matrix: water Prep Batch: N/A Lab File lD: N/A

Dilution: 1.0 Units: mg/L lnitial WeighWolume: 100 mL

Date Analyzed: O2!O412OOB 1'143 Final WeighWolume: 200 mL

Date Prepared: N/A

Analyte

% Rec.


Total Dissolved Solids 98 97 80-120 0 25


TestAmer¡caTallahassee Page 21 of 30 02/08/2008

Client; Golder Associates lnc.




Dilution: 1.0

Date Analyzed: 01/31/2008 1033

Date Prepared: N/A

Analyte


Prep Batch: N/A

Units: mg/L

Result


Job Number: 640-14947-1

Method: 325.2

Preparation: N/A

lnstrument lD: Konelab

Lab File lD: N/A



MDL PQL

0.22 1.0


Qual

Chloride 0.22

Lab Gontrol Spike/Lab Gontrol Spike Duplicate Recovery Report - Batch: 640-41256

Analyte

LCS Lab Sample lD: LCS 640-41256/2 Analysis Batch: 640-41256 lnstrument lD: Konelab


Dilution: 1.0 Jnits: mg/L lnitial WeighWolume: 2.0 mL

DateAnalyzed: 0113112008 1017 Final WeighWolume: 2.0 mL

Date Preoared: N/A

LCSD Lab Sample lD: LCSD 640-41256/3 Analysis Batch: 640-4'1256 lnstrument lD: Konelab

Client Matrix: Water Prep Batch: NiA Lab File lD: N/A



Date Prepared: N/A

% Rec.


Chloride 100 100 85-115 1 30


TestAmerica Tallahassee Page 22 of 30 O2/08/2OOB



MS Lab Sample lD: 640-14947-3


Dilution: 1.0


Date Prepared: N/A

MSD Lab Sample lD: 640-14947-3


Dilution: 1.0


Date Preoared: N/A

Analyte


Preo Batch: N/A


Preo Batch: N/A


Job Number: 640-14947-1

Method: 325.2Preparation: N/A


Lab File lD: N/A




Lab File lD: N/A



% Rec.


Chloride




Dilution: 1.0


Date Prepared: N/A

Analyte

95 95 85-1 15 1 30


Prep Batch: N/A

Units: mg/L



Lab File lD: N/A


Final WeightA/olume: 2.0 mL

Samole ResulUQual Result RPD Limit Qual

Chloride 5.72


030






Dilution: 1.0


Date Prepared: N/A

Analyte


Prep Batch: N/A

Units: mg/L


Job Number: 640-14947-1

Method: 350.1

Preparation: N/A

lnstrument lD: Astoria

Lab File lD: N/A



MDL PQLResu t Qual

Ammon¡a 0.0013

Lab Gontrol Spike/Lab Control Spike Duplicate Recovery Report. Batch: 640'41499

0.00075 0.020


LCS Lab Sample lD: LCS 640-41499/2 Analysis Batch: 640-41499 lnstrument lD: Astoria


Dilution: 1.0 Units: mg/L lnitial WeighWolume: 25'0 mL


Date Prepared: N/A

LCSD Lab Sample lD: LCSD 640-41499/3 Analysis Batch: 640-41499 lnstrument lD: Astoria



Date Analyzed: 0210712008 125'l Final WeighWolume: 25.0 mL

Date Prepared: N/A

Analyte

% Rec.


Ammonia 109 114 85- 115 4 30





Lab Sample lD: MB 640-4151211


Dilution: 1.0


Date Prepared: N/A

Analyte


Lab Control Spike/

Analysis Batch: 64041512Prep Batch: N/A

Units: mg/L

Resull

0.00011 u


Job Number: 640-14947-1



Lab File lD: N/A



MDL PQL

0.00011 0.010


Qual

Lab Cont¡ol Spike Duplicate Recovery Report - Batch: 640-4í512

LCS Lab Sample lD: LCS 640-41512/3 Analysis Batch: 640-41512 lnstrument lD: Astoria




Date Prepared: N/A



Dilution: 1.0 tJnits: mg/L lnitial WeighWolume: 25.0 mL

DateAnalyzed: 0210712008 1433 Final WeighWolume: 25.0 mL

Date Prepared: N/A

Analyte

% Rec


Nitrate Nitrite as N 107 106 90-110 1 30



elient: Golder Associates lnc.




Dilution: 2A

DateAnalyzed: 02/0712008 1559

Date Prepared: N/A

Analyte


Prep Batch: N1A

Units: mg/L


Job Number: 64444947-1



Lab File lD: N/A

Initial WeighWolume: 25.0 mL



Nitrate Nitrite as N 0.43

Calculations are performed before rounding to avoid round-off errors in caleulated results.

0.395 I 30

TestAmerica Tallahassee Page 26 of 30 02108/200,8





Dilution: 1.0


Date Prepared: N/A

Analyte


Prep Batch: N/A

Units: mg/L

Result


Job Number: 640-14947-1



Lab File lD: N/A

lnitial WeightA/olume: 2.0 mL

Final WeighUVolume: 2.0 mL

MDL PQL

-ïä*- - ""--"-îo "

Method: 375.4

Preparation: N/A


Lab File lD: N/A




Lab File lD: N/A



Qual

Sulfate 1.3

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 640-41257

LCS Lab Samole lD: LCS640-4125712 Analvsis Batch: 640-41257

LCSD Lab Sample lD: LCSD 640-41257/3 Analysis Batch: 640-41257


Dilution: 1.0


Date Prepared: N/A


Dilution: 1.0


Date Prepared: N/A

Analyte

Prep Batch: N/A

Units: mg/L

Prep Batch: N/A

Units: mg/L

% Rec.


Sulfate 102 102 85-115 0 30






Client Matrix: Watel

Dilution: 1.0


Date Prepared: N/A



Dilution: 1.0


Date Prepared: N/A

Analyte

Sulfate




Dilution: 1.0


Date Prepared: N/A

Analyte

Analysis Batch: 640*41257

PreD Batch: N/A


Preo Batch: N/A


Job Number: 640-14947-1



Lab File lD: N/A




Lab File lD: N/A



% Rec


128 128 85-115 0 30 J J


Prep Batch: N/A

Units: mg/L

Method: 375.4

Preparation: N/A


Lab File lD: N/A




Sulfate


1.3 U 1.3 NC30U






Dilution: 1.0

Date Analyzed: 02106/2008 0801


Analyte

AnalysisBatch: 680-97390


Units: mg/L


Job Number: 640-14947-1

Method:420.1Preparation : Distill/Phenol


Lab File lD: N/A



MDL PQLResu t Qual

Phenolics. Total Recoverable 0.025

Lab Control Spike/Lab Gont¡ol Spike Duplicate Recovery Report - Batch: 680-97389

Analyte

0 025 0.050

Method: 420.1

Preparation: Distill/Phenol

LCS Lab Sample lD: LCS 680-97389/2-A Analysis Batch: 680-97390 lnstrument lD: No Equipment Assigned



Date Analyzed: 02/06i2008 0801 Final WeighWolume: 100 mL


LCSD Lab Sample lD: LCSD 680-97389/3-A Analysis Batch: 680-97390 lnstrument lD: No Equipment Assigned



DateAnalyzed: 0210612008 0801 Final WeighWolume: 100 mL


% Rec.

LCS LCSD Limit RPD RPD Limit LCS QuaI LCSD QuaI

Phenolics, Total Recoverable 106 112 75 - 125 6 30



Jacksonville Service Center8933 Western Way Suite 1

Jacksonv¡llo, FL322æPhone (904) 519-9551 Fax 519-9s52

TestArnericachain of custod, *""TrÍ4 Ò_ ì,_t qq1

U0¡rqo(¡Joot-h

(to

oN

o@

Noo@

q) 3(¿3-3ttiô

-HCL M-H6Em-NaOH N-Nffi-ZnAætat€ O-AsNaO2

D-NiûicAdd P-Na2@SE-Nal-lSO4 Q-Na2SO3F-MeOH R-Na2S2SO3G-Amctìlq S-H2SO4H - Asdblc Add T - TSP Dodè€hvdEtel-hs U-AcetmJ-DIWaltr V-MCAAK-EDTA W-ph+sL - EDA Z -other (spec¡fy)

'f¿tlos

Z Non-Hazad I Ftammabte E "L,¡

lnitant E Poíson B E ,Jrkno*, tle Dísposal ( A fee rray be asçessed if samples dre retained longer than I month)

Retum To Ct¡ent E D¡soosat Bv Lab I Arch¡ve For Months

I, ll, lll, lV, Other (spec¡n

TestAmericct.IHE

LËAI]ËR IN ËNVIRONMËNI'AL TÈS IING

ANALYTICAL REPORT

Job Numb er: 640-14966-1


For:Golder Associates lnc.

9428 Baymeadows RoadSuite 400

Jacksonville, FL 32256

Attention: Mr. Rich W Poff


Project Manager I

chad. [email protected]

These test results meet all the requirements of NELAC. All questions regarding this test report should be directed to the

TestAmerica Project Manager who signed this test report.Measurement uncertainty data, as referenced in Section 8.6 of the TestAmerica Tallahassee LQM, are available upon

request.

Florida Deoartment of Health Certification No. E81005Mobile DOH Certification No. E87089

TestAmerica Laboratories, lnc.

TestAmerica Tallahassee 2846 lndustrial Plaza Drive, Tallahassee, FL 32301

Tel (850) 878-3994 Fax (850) 878-9504 www,testamericainc.com2

Page 1 of 38 02 / o8 /2008

Job Narrative640-J14966-1

GommentsNo additional comments.

Rece¡ptAll samples were received in good condition within temperature requirements.

GC/MS VOAMethod(s) 8260: Lab Control Standard and Lab Control Standard Duplicate (LCS-LCSD) recoveries for 2-chloroethyl vinyl ether were

outside the recovery limits. Target analyte not detected in fìeld samples, associated data flagged "J".

Method(s) 8260: Matrix spike and duplicate (MS-MSD) recoveries on sample MW-2 (640-14966-1)for 2-chloroethyl vinyl etherwere

outside the recovery limits. Target analyte not detected in field samples, associated data flagged "J".

No analytical or quality issues were noted.

MetalsMethod(s) 6010: The method blank contained lron above the method detection limit. This target analyte concentration was less than the

reporting limit (RL); therefore, re-extraction and/or re-analysis of samples was not performed. Associated data flagged 'V".


Field Service, Mobile LabNo analytical or quality issues were noted.

Genêral ChemistryMethod(s) 3S0.1: The method blank contained ammonia above the method detection limit. This target analyte concentration was less

than the reporting limit (RL); therefore, re-extraction and/or re-analysis of samples was not performed. Associated data flagged "V".

Method(s) 353.2: The method blank for batch 41514 contained Nitrate-Nitrited above the method detection limit. This target analyte

concentration was less than the reporting limit (RL); therefore, re-efraction and/or re-analysis of samples was not performed. Associated

data flagged 'V".


VOA PrepNo analytical or quality issues were noted.

Page 2 of 38 02 / 08 /2008



Lab Sample lD Client Sample lDAnalyte Result / Qualifier

ReportingLimit Units

Job Number: 640-14966-'l

Method

640-14966-r

Chloroform

640-14966-2 MW.4



SulfateNitrate as N

Tolal Recoverøble


640-149666

BenzeneMercuryTotal Dissolved Solids


SulfateNitrate as N

Díssolved

Mercury

Total Recoverable

AluminumlronSodium

640-14966-7


Nitrate as N

Total Recoverable

lronSodium

EB-01

0.28 10

5.0

1.0

0.0200.0205.0

0.010

20010

50

1 000

1.0

0.000205.01.0

0.0200205.0

0.010

0.00020

200CU

I 000

1.0

0.0200.0100.010

50

1 000

160.1

325.2

350.1

353.2

375.4

Nitrate by calc

601 0B

601 0B

601 0B

601 0B

826087470A'160.1

325.2

350.1

353 2

375.4

Nitrate by calc

74704

601 0B

601 0B

601 0B

82608

325.2

350.1

353.2

Nitrate by calc

601 0B

60r 0B

ug/L

2203.¿

0.180.4812

0.48

80.to

87

7400

0.620.0033JY

8.6

0.012z-Y

12

z-J

0.0029

90

8.9

81 00

ug/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L

mg/L

mg/Lmg/Lmg/Lmg/Lmg/Lmg/L

I

IV

IV

IV

IV

ug/Lug/Lug/Lug/L

2.1

0.00560.0550.055

6.52800

mg/Lmg/Lmg/Lmg/L

ug/Lug/Lug/L

ug/Lug/L


Page 3 of 38 02 / 08 /2008


Lab Sample lD Çlient Sample lD

Analyte


Job Number: 640-14966-1

ReportingResult / Qualifier Limit Units Method

640-14966{ TRIP BLANK

Methylene Chloride 0.35 I 5.0 ug/L 82608

640-14966-9 MW-8R

Mercury

Dìssolved

Mercury

0.00020 mg/L 74704

0.00020 mg/L 74704


Page 4 of 38 02 /08 /200s

METHOD SUMMARY

Client Golder Associates lnc. Job Number: 640-14966-1

Descriotion Lab Location Method Preparation Method

Matrix: Water

lnductively Coupled Plasma - Atomic Emission Spectrometry TAL TAL SW846 60108

Acid Digestion of Waters for Total Recoverable or TAL TAL

Mercury in Liquid Waste (Manual Cold Vapor Technique) TAL TAM SW846 74704

Volatile Organic Compounds by GC/MS

Purge-and-Trap

Sample F¡ltration performed in the Field


Residue, Filterable, Gravimetric, Dried at 180'C (TDS)

Chloride (Colorimetric, Automated Ferricyanide)

Nitrogen (Ammonia, Colorimetric, Automated Phenate)

TAL TAL SW846 82608

TAL TAL

TAL TAM

TAL TAM

TAL TAL MCA\A^iv 160 1

TAL TAL MCA\A^/V 325.2

TAL TAL MCA\ A/V 350.1

sw846 50308

sw846 30054

FIELD FLTRD

sw846 74704

Nitrogen, Nitrate-Nitrite (Colorimetric, Automated, Cadmium TAL TAL MCA\ ÂlV 353.2

Reduction)

Sulfate (Turbidimetric) TAL TAL MCA\ ^/V

375.4

Phenolics (Spectrophotometric, Manual 4-AAP with Distillation) TAL SAV MCA\ ^/V

420.1

Distillation/Phenolics TAL SAV Distill/Phenol

Nitrogen, Nitrate-Nitrite (Colorimetric, Automated, Cadmium TAL TAL SM-Online Nitrate by calc

Reduction)

Lab References:

TAL SAV = TestAmerica Savannah

TAL TAL = TestAmerica Tallahassee


Method References:

MCA\ A/r/ = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.

SM-Online = Standard Methods Online

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And lts Updates.


Page 5 of 38 02/0e/2008

SAMPLE SUMMARY

Client: GolderAssociates lnc.

Date/TimeLab Sample lD Glient Sample lD Client Matrix Sampled

Joþ Number: 640-14966-1

640-14966-1

640-'14966-2

640.14966,3

640¡4966-4640-14966-5

640-14966-6

640-r4966-7640-14966-8

640-14966-9

MW:2

MW-4

MW-5

MW-6

MW-7

MW-8

EB-01

Trip Blank

MW.8R

Water

Water

Water

Water

Water

Water

Water

Water

Water

TestAmerica Ta I la hassee

SAMPLE RESULTS

TestAmer¡ca Tallahassee

Page 7 of 38 02 / 0s /2008


AnalYtical Data

Job Number: 640-14966-1

Date Sampled: 0112912008 1007

Date Received: 0113112008 1010

Client Sample lD:

Lab Sample lD:

Client Matrix:

MW.2

640-14966-1

Water

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

82608

50308

1.0

02t0712008 1453

02t0712008 1453

82608 Volatile Organic Gompounds by GC/MS

Analysis Balch: 64041 521 lnstrument lD: VME 5973N

Lab File lD: 18020713.D



mL

mL

ål"ervl9***- - .a"9Jvltle/ÐBenzene o o58

Bromoform o'13

Bromomethane 0.17

Carbon tetrachloride 0.078

Chlorobenzene 0.079

Chlorodibromomethane 0.080

Chloroethane 0.11

2-Chloroethyl vinyl ether 1.2

chloroform o'28

chloromethane o'o8o

cis-1 ,2-Dichloroethene 0.1 Icis-1,3-Dichloropropene 0.082

1,2-Dichlorobenzene 0 076

1,3-Dichlorobenzene 0.082

1,4-D¡chlorobenzene 0'14

Dichlorobromomethane 0.10

Dichlorodifluoromethane 0.075

1,1-Dichloroethane 0.067

1,2-Dichloroethane 0.082

1,1-Dichloroethene 0.11

1 ,2-Dichloropropane 0.1 0

Ethylbenzene 0.078

Methylene Chloride 0'17

Methyl tert-butyl ether 0.065

1,1,2,2-1el¡achloroethane 0.070

Tetrachloroethene 0.24

Toluene 0.063

trans-1,2-Dichloroethene 0.25

trans-1,3-Dichloropropene 0.077

I ,1 ,1 -Trichloroethane 0.1 1

1,1,2-Trichloroethane 0 20

Trichloroethene 0.13

Trichlorofluoromethane 0'12

Vinyl chloride 0.058

Xylenes, Total 0.'1 1

Qualifier PQL

1.0

1.0

1.0

1.0

1.0

1.0

1.0

10

1.0

1.0'1.0

1.0

1.0

1.0

1.0

1.0

1.0'1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

2.0

MDL

U

U

U

U

U

U

U

UJI

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.0580.130.170.0780.0790.0800.1 1

1.2

0.0560.0800.180.0820.0760.0820.'14

0.100.0750.0670.0820.11

0.100.0780.170.0650.0700.240.0630.250.0770.11

0.200.130.120.0580.1 1

Surrogate

4-BromofluorobenzeneDibromofluoromethaneToluene-dB (Surr)

%Rec

101

109

Acceptance Limits

83 - 123

78 - 126

TestAmerica Tallahassee Page 8of38 02 / 08 /2008


Client Sample lD:

Lab Sample lD:

Client Matrix:

MW4

640-14966-2

Water

Analytical Data

Job Number: 640-14966-1

Date Sampled: 0113012008 1245

Date Received: 01/31i2008 1010

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

82608 Volatile Organic Compounds by GC/MS

82608 AnalYsis Batch:640-41521

50308

1.0

02t0712008 1522

02t07t2008 1522

Result (ug/L) Qualifìer

lnstrument lD: VME 5973N




mL

ML

Analyte0.058

0.1 3

0.170.078

0.0790.0800.11

1,2

0.0560.0800.180.082

0.076

0.082

0.140.100.0750.0670.082

0.11

0.100.0780.170.0650.0700.240.0630.250.077

0.1 1

0.200.130.12

0.0580.11

%Rec

0.0580.130.170.0780.0790.0800.11

1.2

0.0560 0800.180.0820.0760.0820.140.100.0750.0670.0820.11

0.100.0780.170.0650.0700.240.0630.250.0770.1 1

0.200.130.120.0580.11

Þrìt

1.0

1.0

1.0

1.0

1.0

1.0

1.0

10

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0',l.0

501.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

2.0

BenzeneBromoformBromomethaneCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethane2-Chloroethyl vinyl ether

ChloroformChloromethanecis-1,2-Dichloroethenecis-1,3-Dichloropropene1 ,2-D¡chlorobenzene1 ,3-Dichlorobenzene1 ,4-DichlorobenzeneDichlorobromomethaneDichlorodifluoromethane1 ,1 -Dichloroethane

1 ,2-Dichloroethane1 ,1 -Dichloroethene

1 ,2-DichloropropaneEthylbenzeneMethylene ChlorideMethyl tert-butyl ether

1,1,2,2-f elrachloroetha ne

TetrachloroetheneToluenetrans- 1,2-Dichloroethenetrans-1,3-Dichloropropene1, 1, 1 -Trichloroethane1, 1,2-TrichloroethaneTrichloroetheneTrichlorofl uoromethane

Vinyl chlorideXylenes, Total

Surrogate

U

U

U

U

U

U

U

UJU

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

¿€romofl.'l"robe"teteDibromofluoromethaneToluene-dB (Surr)

9497

110

åe9:P"!'t9S,Iri970 - 11983 - 12378 - 126



Glient Sample lD:

Lab Sample lD:

Client Matrix:

MW-5

640-14966-3

Water

AnalYtical Data

Job Number: 640-14966-1

Date Sampled: 0112912008 1417


Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

82608

50308

1.0

02t0712008 1551

02t07t2008 1551

82608 Volatile Organic Gompounds by GG/MS

Analysis Batch: 640-41 521 lnstrument lD: VME 5973N

Lab File lD: 1E020715.D



mL

ML

Analyte

BenzeneBromoformBromomethaneCarbon tetrachlorideChlorobenzeneChlorodibromomethaneChloroethane2-Chloroethyl vinyl etherChloroformChloromethanecis-1,2-Dichloroethenecis-1, 3-Dichloropropene1 ,2-DichlorobenzeneI ,3-Dichlorobenzene1 ,4-DichlorobenzeneDichlorobromomethaneDichlorodifl uoromethane

I ,1-Dichloroethane'l ,2-Dichloroethane1 ,1 -Dichloroethene1 ,2-DichloropropaneEthylbenzeneMethylene ChlorideMethyl tert-butyl ether

1,1,2,2-l etrachloroeth a ne

TetrachloroetheneToluenetrans-1,2-Dichloroethenetrans-1,3-Dichloropropene1 ,1 ,1 -Trichloroethanel, 1,2-Trichloroethane

TrichloroetheneTrichlorofl uoromethaneVinyl chlorideXylenes, Total

Surrogate

4-BromofluorobenzeneDibromofluoromethaneToluene-d8 (Surr)

Result (ug/L)

0.0580.130.170.0780.0790.0800.11

1.2

0.0560.0800.180.0820.0760.0820.140.100.0750.0670.0820.11

0.100.0780.170.0650.0700.240.0630.250.0770.11

0.200.1 3

0.120.0580.11

Acceptance Limits

Qualifier MDL

0,0580.130.170.0780.0790.0800.11

1.2

0.0560.0800.180.0820.0760.0820.140.100.0750.0670.0820.1 1

0.100.0780.170.0650.0700.240.0630.250.0770.11

0.200.130.120.0580.11

PQL

1.0

1.0

1.0

1.0

1.0

1.0

1.0

10

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

2.0

U

U

U

U

U

U

U

UJilil

U

uU

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

%Rec-****-

91

100

114

70 - 11983 - 123

Ió - t¿o



Client Sample lD:

Lab Sample lD:

Client Matrix:

MW-6

640-14966-4

Water

Analytical Data

Job Number: 640-14966-1

Date Sampled: 0112912008 1651


Method:

Preparat¡on:

Dilution:

Date Analyzed:

Date Prepared:

Analyte


82608 AnalYsis Batch: 640-4'1521

50308

1.0

0210712008 1620

02t07t2008 1620


Lab File lD: 1 E02071 6.D



ML

ML


ChloroformChloromethanecis-1,2-Dichloroethenecis-1,3-Dichloropropene1 ,2-Dichlorobenzene1 ,3-Dichlorobenzene1 ,4-DichlorobenzeneDichlorobromomethaneDichlorodifl uoromethane1 ,l -Dichloroethane


I ,2-DichloropropaneEthylbenzeneMethylene ChlorideMethyl tert-butyl ether1,1,2,2-f etachloroethaneTetrachloroetheneToluenetrans-1,2-Dichloroethenetrans-1,3-Dichloropropene1 , I ,1 -Trichloroethane1, 1,2-TrichloroethaneTrichloroetheneTrichlorofl uoromethane


Surrogate

0.0580.130.170.0780 079

0.080

0.11

1.2

0.056

0.0800.180.082U.U/O

0.082o.140.100.0750.0670.082

0.11

0.100.078

0.170.0650.0700.240.0630.250.077

0.11

0.200.130.12

0.0580.11

%RecxÄ*--YÞ

98

110

0.0580.1 3

0.170.0780.0790.0800.11

1.2

0.0560.0800.180.0820.0760.0820.140.100.0750 067

0.082

0.1 1

0.100.078

0.17

0.065

0.0700.240.0630.250.0770.11

0.200.130.120.0580.11

Acceotance Limits

70¡ie --

Result (ug/L) PQL

U

U

U

U

U

U

U

UJU

U

Uil

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

Utt

1.0

1.0

1.0

1.0

1.0

1.0

1.0

10

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1,0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

¿.v


83 - 12378 - 126

TestAmerica Tallahassee Page 11 of 38 02/0e /2008

Client; Golder Associates lnc.

Client Sample lD:

Lab Sample lD:

Client Matrix:

MW-7

640-14966-5

Water

AnalYtical Data

Job Number: 640-14966-1

Date Sampled: 0112912008 1149


Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Analyte

82608

50308

1.0

02t07t2008 1649

02t07t2008 1649



Result (ugiL)





mL

mL


ChloroformChloromethanecis-1,2-Dichloroethenecis-1,3-Dichloropropene1 ,2-Dichlorobenzene1 ,3-Dichlorobenzene1 ,4-DichlorobenzeneDichlorobromomethaneDichlorodifl uoromethaneI ,1 -Dichloroethane

1 ,2-Dichloroethane1 ,1-DichloroetheneI ,2-DichloropropaneEthylbenzeneMethylene ChlorideMethyl tert-butyl ether

1,'1,2,2-T elr achloroethaneTetrachloroetheneToluenetrans-1,2-Dichloroethenetrans-1,3-Dichloropropene1, 1, 1 -Trichloroethane

1, 1,2-TrichloroethaneTrichloroetheneTrìchlorofl uoromethane


Surrogate

0.058

0.130.170.0780.0790.0800.11

1.2

0.0560.0800.180.0820.0760.0820,140.100.075

0.0670.082

0.11

0.100.078017u.uþc0.0700.24U.UOJ

0,250.0770.11

0.200.130.120.0580.11

Qualifìer

U"U

U

Uililil

UJU

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

MDL

0.0580.134.170.0780.0790.0800.11

1.2

0.0560.0800.180.0820.0760,0820.140.10

0.0750.0670.0820.11

0.100.0780.170.0650.0700.240.0630.250.0770.11

0.200.130.120.0580.'11

PQL

1.0

1.0

1.0

1.0

1.0

1.0

1.0

10

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

¿.v

Acceotance Limits

4-Bromofluorobenzene

%Rec--öö98

109

70 - 11983 - 123

78 - 126DibromofluoromethaneToluene-d8 (Surr)

TestAmerica Tallahassee Page L2 of 38 02 / 08 /2008


Glient Sample lD:

Lab Sample lD:

Client Matrix:

MW-8

640-14966-6

Water

Analytical Data

Job Number: 640-14966-1

Date Sampled: 0113012008 1440


Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Analyte MDL"'ò.öäB

0.130.'17

0.0780.0790.0800.11't.2

0.0560.0800.1 I0.0820.0760.0820.140.100.0750.0670.0820.11

0.100.0780.170.0650.0700.240.0630.250.0770.11

0.200.130.120.0580.11

-,-."-9l"qrI"l

U

U

U

U

U

U

UJU

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U


82608 Analysis Batch:640-41521

50308

1.0

02t0712008 1718

02t0712008 1718


Lab File lD: 1 E02071 8.D




ChloroformChloromethanecis-1,2-Dichloroethenecis-1,3-Dichloropropene1 ,2-Dichlorobenzene1 ,3-Dichlorobenzene1 ,4-DichlorobenzeneDichlorobromomethaneDichlorodifl uoromethane1 ,1-Dichloroethane1 ,2-Dichloroethane1 ,1 -Dichloroethene

1 ,2-DichloropropaneEthylbenzeneMethylene ChlorideMethyl tert-butyl ether

1,1,2,2-T eî achloroethaneTetrachloroetheneToluenetrans-1,2-Dichloroethenetrans-1,3-DichloropropeneI , I ,1 -Trichloroethane1, 1,2-TrichloroethaneTrichloroetheneTrichlorofl uoromethaneVinyl chlorideXylenes, Total

Surrogate

t":9"fsqt)" --0.620.130.170.0780.0790.0800,11

1.2

U.UCÞ

0.0800.1 I0.082

0.076

0.082

0.140.100.0750.0670.082

0.11

0.100.0780.170.0650.0700.240.0630.250.0770.11

0.200.1 3

0.12

0.0580.11

%Rec

'1.0

1.0

1.0

1.0

1.0

1.0

1.0

10

1.0

1.0

101.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0'1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

¿.u

AcceDtance Limits

70 - 119

83 -',123

78 - 126

PQL


82

86

100



Client Sample lD:

Lab Sample lD:

Client Matrix:

EB-01

640-14966-7

Water

Analytical Data

Job Number: 640-'14966-1

Date Sampled: 01/30/2008 1050


Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Analyte

82608 Volatile Organic Gompounds by GG/MS

82608 AnalYsis Batch:640-41521

50308

1.0

02t07t20a8 ß2402t07t2008 1424





ML

ML

Result (ug/L)

0 058

0.130,170.0780.0790.0800.11

1.2

0.0560.0800.180,0820.0760.0820.140.100.0750.0670.0820.1 1

0.100.078

0.170.0650.0700.240.0630.250.0770.11

0.200.130.12

0.0580.11

%Rec

POL

1.0

1.0

1.0

1.0

1.0'10

1.0

10

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

2.0

Acceotance Limits

Qualifier MDL

o.ösò0.130.170.0780.0790.0800.11

1.2

0.0560.0800.180.0820.0760.0820.140.100.0750.067

0.0820.11

0.100.0780.170.0650.0700.240.0630.250.0770.11

0.200.130.'t20.0580.11


ChloroformChloromethanecis- 1,2-Dichloroethenecis-1,3-Dichloropropene'1 ,2-Dichlorobenzene1 ,3-DichlorobenzeneI ,4-DichlorobenzeneDichlorobromomethaneDichlorodifluoromethane1 ,1-Dichloroethane1 ,2-DichloroethaneI ,1-Dichloroethene1 ,2-DichloropropaneEthylbenzeneMethylene ChlorideMethyl tert-butyl ether

1,1,2,2-I el¡ achloroeth a ne

TetrachloroetheneToluenetrans-1,2-Dichloroethenetrans-1,3-Dichloropropene1,1, I -Trichloroethane

1, 1,2-TrichloroethaneTrichloroetheneTrichlorofl uoromethaneVinyl chlorideXylenes, Total

:y"-o"g?q"_ "--.4-BromofluorobenzeneDibromofluoromethaneToluene-dB (Surr)

U

U

U

U

U

U

U

UJU

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

96ol

103

70-11983 - 12378 -'t26



Client Sample lD:

Lab Sample lD:

Client Matrix:

Trip Blank

640-14966-8

Water

Analytical Data

Job Number: 640-14966-1

Date Sampled: 01/30/2008 0000

Date Received: 01i31/2008 1010

Method:

Preparat¡on:

Dilution:

Date Analyzed:

Date Prepared:

Analyte

82608 Volatile Organic Compounds by GG/MS

82608 Analysis Batch: 64041521

50308

1.0

02t07t2008 1353

02t07t2008 1353

Result (ug/L) Qualifier


Lab File lD: 1E.0207',t1.D

lnit¡al Weighwolume: 40 mL


POLMDL

0,0580.130.170.0780.0790.0800.11

1.2

0.0560.0800.180.0820.0760.0820.140.10

^ ^aE0.0670.0820.11

0.100.0780.350.0650.0700.240 063

0.250.0770.1 1

0.200.130.120.0580.11

U

U

U

U

U

U

U

UJU

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.0580.130.170.0780.0790.0800.11

1,2

0.0560.0800.180.0820.0760.0820.140.100.0750.0670.0820.11

0.100.0780.170.0650.0700.240.0630.250 077

0.11

0200.1 3

0.120.0580.1'1

1.0

1.0

1.0

1.0

1.0

1.0

1.0

10

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

2.0

Acceotance Limits


ChloroformChloromethanecis-1,2-Dichloroethenecis-1,3-Dichloropropene1 ,2-Dichlorobenzene1 ,3-Dichlorobenzene1 ,4-DichlorobenzeneDichlorobromomethaneDichlorodifl uoromethane1 ,1-Dichloroethane1 ,2-Dichloroethane1 ,1-Dichloroethene1 ,2-DichloropropaneEthylbenzeneMethylene ChlorideMethyl tert-butyl ether

1,1,2,2-1 eîachloroethaneTetrachloroetheneToluenetrans-1,2-Dichloroethenetrans-1,3-Dichloropropene1 .1 .1 -Trichloroethane


Surrogate %Rec

90


70 - 11983 - 12378 -'t26

TestAmerica Tallahassee Page 15 of 38 02/ 0e /2008


Glient Sample lD:

Lab Sample lD:

Client Matrix:

MW.4

640-14966-2

Water

Analytical Data

Job Number: 640-14966-1

Date Sampled: 0113012008 1245


60lOB lnduct¡vely Goupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Analyte

601 0B

30054

1.0

02105/2008 1659

02/05/2008 0900

Analysis Balcht 64041 442


Result (ug/L)

lnstrument lD:

Lab File lD:


Final WeighWolume:

Qualifier MDL

ICP Trace

FEBROS

50 mL

50 mL

POL


Sodium

80

4.20.461.9

87

2.0

7404

21

u 4.2

u 0.461.5

v 4.6

u 2.0220

20010

5.0

l050

5.01 000

7470A Mercury in Liquid Waste (Manual Cold Vapor Techn¡que)

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

7470A.

7470A.

1.0

02t05t2008 1512

02/05/2008 0918



lnstrument lD:

Lab File lD:


Final WeighWolume:

Hg Analyzer

N/A

25.0 mL

25.0 mL

Þôt

- ""-"--" o.tioòzo

Analyte

Mercury

MDL'ö.oooo?ã

Result (mg/L)

õ.o"oooz *-

TestAmerica Tallahassee Page 16 of 38 02 / o8 /2008


Glient Sample lD:

Lab Sample lD:

Client Matr¡x:

MW-8

640-14966-6

Water

Analytical Data

Job Number: 640-'14966-1

Date Samoled: 0113012008 1440



Method:

Preparat¡on:

Dilution:

Date Analyzed:

Date Prepared:

Analyte


601 0B

300541.0

0210512008 1704

02/05/2008 0900

An alysis B atch'. 640 41 442


Result (ug/L)


Lab File lD: FEBRO8



PQLMDL

90

4.20.461t

Rq

2.0

81 00

"::*:._"__U

U

U

IVU

21

420.46l5

4.62.0220

20010

5.0

10

50

5.0

I 000

74704 Mercury in Liquid Waste (Manual Gold Vapor Techn¡que)

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Analyte

7470474704

1.0

0210512008 1514

02/05/2008 0918

lnstrument lD:

Lab File lD:

lnitial WeighWolume:Final WeighWolume:

Hg Analyzer

N/A

25.0 mL

25.0 mL



Result (mg/L) Qualifier

7470A Mercury in Liquid Waste (Manual Gold Vapor Technique)'Dissolved

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Analyte

747047470Á.

1.0

02t0512008 15't6

02/05/2008 0918

lnstrument lD:

Lab File lD:


Final WeighWolume:

Hg Analyzer

NiA

25.0 mL

25.0 mL

Þôt




Mercury 0.0029 0.000072 0.00020

TestAmerica Tallahassee Page 17 of 38 02 / 08 /200e


Client Sample lD:

Lab Sample lD:

Client Matrix:

EB-01

640-14966-7

Water

Analytical Data

Job Number: 640-14966-1

Date Samoled: 01/30/2008 1050



Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

601 0B

30054

1.0

02t05t2008 '1705

02/05/2008 0900

Analysis Balch: 64041 442



Lab File lD: FEBRO8



Analyte

Air.ñrtArsenicCadmiumChromiumlronLead

Sodium

Result (ug/L) Qualifier

21

4.2

0.4644

6.5

2.0

U

U

Uil

IVU

MDL

21

4.20.4614

4.62.0

2800 220 1000


Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Analyte

747047470A'

1.0

02t0512008 1518

02/05/2008 0918

lnstrument lD:

Lab File lD:


Final WeighWolume:

Hg Analyzer

N/A

25.0 mL

25.0 mL



Result (mg/L) Qualifier

U

MDL

Mercury 0.000072

TestAmerica Tallahassee Page 18 of 38 02/08 /2008


Analytical Data

Job Number: 640-14966-1

Glient Sample lD: MW-BR

Lab sample lD: 640-14966-9 Date sampled: 0113012008 1545

client Matrix: water Date Received: 01/31/2008 1010

7470A Mercury ín Liquid Waste (Manual Cold Vapor Technique)

lnstrument lD: Hg AnalYzer

Lab File lD: N/A



Result (mg/L) Qualifier MDL PQL

Method: 74704

Preparation: 74704

Dilution: 1.0



Analyte

Method: 74704

Preparation: 74704

Dilution: 1.0



Analyte





Mercurv 0.0055 0'000072 0'00020

-

74704 Mercury in Liquid Waste (Manual Cold Vapor Technique)-D¡ssolved


Lab File lD: N/A



Result (mg/L) Qualifìer MDL PQL

Mercury 0.000072 0.000200 0050

TestAmerica Tallahassee Page 19 of 38 02/oe/2008


Analytical Data

Job Number: 640-14966-1

Glient Sample lD:

Lab Sample lD:

Client Matrix:

Analyte

MW4

640-14966-2

Water

Result

General Chemistry

Qual Units

Date Samoled: 0113012008 1245


MethodPQLMDL

Chloride

Ammonia


Sulfate

Phenolics. Total Recoverable

Nitrate as N

9.2


0.'18


0.48


12


0.025


Prep Batch: 680-973890.48


0.22


V mg/L 0.00075


V mg/L 0.00022


mg/L 1.3


U mg/L 0.025

Date Analyzed 02106/2008 080'l


mg/L 0.0001 1


10

10

20

10

10

10

mg/L 1.0

0.020

0.020

5.0

0.050

0.010

325.2

350.1

óaó.¿

375.4

420.',|

Nitrate by calc

Result Qual Units POL PQL

220 mg/L 5.0 c.u

Anly Batch: 640-41 353 Date Analyzed (start) 02104/2008 1 1 48 (End) O2lO4l2OO8 1227

Dit Method

1.0 1 60.1Total Dissolved Solids

TestAmerica Tallahassee Page 20 of 38 02/ 08 / 2OO8


Analytical Data

Job Number: 640-'14966-1

Client Sample lD: MW-8



Analyte

General Chemistry

Date Sampled: 0113012008 1440



Chloride

Ammonia


Sulfate

mg/L 0.22 1.0 1.0 325.2


0.012 I V mg/L 0.00075 0.020 1.0 350 1

Anly Batch: 640-41499 Date Analyzed 02l07l2oo$ 1305

2.9 V mg/L 0'0022 0'20 20 353 2

Anly Batch: 640-415'14 Date Analyzed 0210712008 1634

12 mg/L 1.3 5.0 1.0 375'4


Phenolics, Total Recoverable 0.025 U mg/L 0.025 0.050 1.0 420.1


Preo Batch:680-97389 Date Prepared: 0210612008 0752

Nitrate as N 2.9 mg/L 0.0001 1 0.010 1 .0 Nitrate by calc


Analyte Result Qual Units PQL PQL D¡l Method

Total Dissolved Solids 59 mg/L 5.0 5.0 1'0 160.1

AnlyBatch: 640-41353 DateAnalyzed(Start)02104/2008 1148 (End)o2l04l2ïO8 122s

TestAme¡ica Tallahassee Page 2L of 38 02 / o8 /2008


Analytical Data

Job Number: 640-14966-1

Glient Sample lD: EB-01



Analyte

General Ghemistry

Date Samoled: 01/30/2008 1050



Chloride

Ammonia


Sulfate

2.1

Anly Batch: 640-41256 Date Analyzed 01i31/2008 1913

0.0056 I V mg/L 0.00075 0.020 1'0 350.1


0.055 V mg/L 0.00011 0.010 1.0 353.2


1.3 U mg/L 1.3 5.0 1.0 375.4

mg/L 0.22 1.0 1.0 325.2


Phenolics, Total Recoverable 0.025 U mg/L 0.025 0.050 1.0 420 1



N¡trate as N 0.055 mg/L 0.00011 0.010 1.0 Nitrate by calc



Total Dissolved Solids 5 0 U mg/L 5.0 5.0 1.0 160.1

Anly Batch: 640-41353 Date Analyzed (start) 02/04/2008 1149 (End) O2lO4l2O08 1232

TestAmerica Tallahassee Page 22 of 38 02 / o8 /2008

Client Golder Associates lnc


Descriotion

Job Number: 640-14966-1

Lab SectÍon Qualifier

GC/MS VOA

J Estimated value; value may not be accurate.

U lndicates that the compound was analyzed for but not

detected.

I The reported value is between the laboratory method detection


Metals


detected.

lndicates the analyte was detected in both the sample and theassociated method blank.



General Chemistry


detected,

lndicates the analyte was detected in both the sample and the

associated method blank.



U

I

U

I


Page 23 of 38 02 / o8 /2008

QUALITY CONTROL RESULTS


Page 24 of 38 02 / o8 /2008




Prep Batch: N/A

Units: ug/L

Result


Job Number: 640-14966-1






POL

Lab Sample lD:

Client Matrix:

Dilution:

Date Analyzed:

Date Prepared:

Analyte

MB 640-4152115

Water

1.0

02t07t2008 1318

02t07t2008 1318

Qual MDL


ChloroformChloromethanecis-1,2-Dichloroethenecis-1,3-DichloropropeneI ,2-Dichlorobenzene1 ,3-Dichlorobenzene1 ,4-DichlorobenzeneDichlorobromomethaneDichlorodifl uoromethane1 ,1-Dichloroethane1 ,2-Dichloroethane1 ,1-Dichloroethene1 ,2-DichloropropaneEthylbenzeneMethylene ChlorideMethyl tert-butyl ether1,1,2,2-I elrachloroethaneTetrachloroetheneToluenetrans-1,2-Dichloroethenetrans-1,3-Dichloropropene1 ,1 ,1 -Trichloroethane


Surrogate

0.058

0.130.170.078

0.0790.0800.11

1.2

0.056

0.080

0.1 I0.082

0.076

0.082

0.140.10

0.075

0.067

0.082

0.11

0.100.078

0.170.065

0.0700.240.063

0.25

0.077

0.1 1

0.20

0.130.12

0.058

0.11

% Rec

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

U

0.0580.r 3

0.170 078

0.0790 0800.11

1.2

0.0560.0800.180.0820 0760.0820.140.100.0750.0670.0820.11

0.100.0780.170.0650.0700.240.0630.250.0770.11

0.200.130.12

0.0580.11

Acceptance Limits

1.0

1.0

1.0

1.0

1.0

1.0

1.0

10

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

1.0

5.0't.0

101.0

1.0

1.0

1.0

1.0

1,0

1.0

1.0

1.0

2.0

4-BromofluorobenzeneDibromofluoromethaneToluene-d8 (Surr) tuo

70-11983 - 12378 - 126




Lab Control Spike/Lab Gontrol Spike Duplicate Recovery Report. Batch: 640-41521


Job Number: 640-14966-1










RPD Limit LCS Qual LCSD Qual

LCS Lab Sample lD:

Client Matrix:

Dilution:

Date Analyzed:

Date Prepared:

LCSD Lab Sample lD:

Client Matrix:

Dilution:

Date Analyzed:

Date Prepared:

LCS 640-41 521l3

Water

1.0

02t07t2008 1151

02t07t2008 1151

LCSD 640-4'1521/4

Water

1.0

02t07t2008 1220

02t0712008 1220


Prep Batch: N/A

Units: ug/L


Prep Batch: N/A

Units: ug/L

% Rec.

LCS LCSD LmtAnalyte

Benzene

Bromoform

Bromomethane

Carbon tetrachloride

Chlorobenzene

Chlorodibromomethane

Chloroethane2-Chloroethyl vinyl ether

Chloroform

Chloromethanecis-1,2-Dichloroethene

cis-1,3-Dichloropropene

1 ,2-Dichlorobenzene1 ,3-Dichlorobenzene1 ,4-DichlorobenzeneDichlorobromomethane

Dichlorodifl uoromethane

1 ,1 -Dichloroethane


1 ,2-DichloropropaneEthylbenzeneMethylene Chloride

Methyl tert-butyl ether

1,1,2,2-T elrachloroethane

Tetrachloroethene

Toluene

trans-1,2-Dichloroethene

trans-1, 3-Dichloropropene

I ,1 ,1 -Trichloroethane

1,1,2-Trichloroethane

Trichloroethene

100'100

106

82

107

98

vo

44102

103

100

93

92

98

92

79

98

97

84

96

101

108

98

103q1

95

98

/oQ7

92

97

99

84

90

101

101

100

26

100

99

94

YO

80

ó¿

97

84

96

94

84105

102

103

88

107

95

95

94

74

94oq

ao

2

1

23

þ

4

50

1

4

15

l017

2

41

q

I

5

11

4

4

1

4

4

2

¿¿

25

44

19

2024

38

21

30

34

29

24zz21

21

30

28

29

202430

3022

38

245¿

20

21

zz¿¿

59 - 132

62 - 140

22 - 179

53 - 134

63 - 132

55 - 134

53 - 144

36 - 152

60 - 126

oz - tJU

49 - 127

49 - 141

60 - 154

55 - 147

58 - 151

60 - 134

28 - 133

54 - 132

51 - 167

43-11860 - 138

57 - 130

52 - 132

67 - 128

63 - 148

48 - 136

59 - 130

46 - 125

52 - 140

58 - 136

60 - 140

59 - 129

J




Lab Gontrol Spike/Lab Control Spike Duplicate Recovery Report - Batch: 640-4'1521

LCS Lab Sample lD: LCS 640-41521/3 Analysis Batch: 64041521


Job Number: 640-14966-1






Prep Batch: N/A

Units: ug/LClient Matrix: Water

Dilution: 1.0

Date Analyzed: 0210712008 115'l

Date Preoared: 0210712008 115'l

Analyte

LCSD Lab Sample lD: LCSD64O-4152114 Analysis Batch: 640-41521 lnstrument lD: VME 5973N

Client Matrix: Water Prep Batch: N/A Lab File lD: 1E020708.D

Dilution: '1.0 Units: ug/L lnitial WeighWolume: 40 mL

DateAnalyzed: OZ\OT\2OOB 1220 Final WeighWolume: 40 mL


% Rec.


Trichlorofl uoromethane

Vinyl chloride

Xylenes, Total

98 101 62 - 138 3 40

98 101 66 - 121 3 31

101 102 52 - 128 1 25

LCS % Rec LCSD % RecSurrogate


103 102

92 94

100 103

Calculations are peformed before rounding to avoid round-off errors in calculated results.



Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 6404152'l


Preo Batch: N/A


Preo Batch: N/A


Job Number: 640-14966-1








lnitial We¡ghWolume: 40 mL


RPD RPD Limit MS Qual MSD Qual

MS Lab Sample lD:

Client Matrix:

Dilution:

Date Analyzed:

Date Prepared:

MSD Lab Sample lD:

Client Matrix:

Dilution:

Date Analyzed:

Date Prepared:

Analyte

640-14966-1

Water

1.0

02t07t2008 2208

02t07t2008 2208

640-l 4966-1

Water

1.0

02t07t2008 2237

02t07t2008 2237

% Rec,

MS MSD Lmt

Benzene

Bromoform

Bromomethane

Carbon tetrachloride

Chlorobenzene

Chlorodibromomethane

Chloroethane

2-Chloroethyl vinyl ether

Chloroform

Chloromethane

cis-1,2-Dichloroethene

cis-1, 3-Dichloropropene

1 ,2-Dichlorobenzene



Dichlorobromomethane


1 , 1-Dichloroethane

1 ,2-Dichloroethane

1 ,1-Dichloroethene

1 ,2-Dichloropropane

Ethylbenzene

Methylene Chloride

Methyl tert-butyl ether

1,1,2,2-T et¡achloroethane

Tetrachloroethene

Toluene

trans-.1,2-Dichloroethene

trans- 1,3-Dichloropropene

97

112

o¿

99

105

101

102

0

111

oo

107

86

79

79

86

100

76

104

109

YO

104

106

75

111

Yó

102

101

68

OA

106

73

J¿

100

100

97

0

to81

94

Ió

71

YC

78

89

97

84

89

98

o4

86

103

96

on

87

71

1

l67

4

1

5

NC

13

20

12

4

I10

16

16

12

10

I

16

13

7

IJ

16

4

19

20

41

28

23'18

45

50

21

16

¿¿

25

24

24

¿Ò

z¿

?,1

29

19

22

25

21

¿¿

23

¿o

24

21

¿c

65 - 130

49 - 150

23 - 140

50 - 162

70 - 125

58 - 131

43 - 165

20 - 149

70 - 124

56 - 137

70 - 122

46 - 131

70 - 142

70 - 137

70 - 137

65 - 135

37 - 139

70 -126

65 - 150

60 - 127

66 - 135

63 - 124

61 - 134

51 - 132

41 - 149

62 - 128

68 - 122

64 - 127

40 - 137

UJUJ




Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 6404152'l



Dilution: 1.0

DateAnalyzed: 0210712008 22Oa

Date Preoared: 0210712008 22AB



Dilution: 1.0

Date Analyzed: 0:210712008 2237


Analyte

Anaìysis Batch: 640-41521

Prep Batch: N/A


Prep Batch: IVA


Job Number: 640-14966-1

Method:82608Preparation; 50308


Lab Fífe lD: 1E.020728.D


Final WeighWolumer 40 mL



ln¡tiâl Weighwolume: 40 mL

Final WeþhWolume: 40 mL

1 , 1 ,1-Trichloroethane


Trlchloroethene


Vinyl chloride

Xylenes, Total

Surrogate

% Rec.

MS MSD Limit RPD RPD Lim¡t MS Qual MSD Qual

109 98 61 -',152 11 21

97 93 60-132 4 22

94 93 70-131 I 28

100 98 60 - 157 2 2ß

92 84 63-126 I 23

101 98 67 - 119 3 26

MS % Rec MSD % Rec Acceptance Limits

105 94

101 87

104 94

Calculations are performed before rounding to avoíd round-off enors in calculated results.

TestAmerica Tallahassee Page 29 of 38 02/08/2ooe





Dilution: 1.0

Date Analyzed: 02105/2008 1616


Analyte

Analysis Batch: 64041 442


Units: ug/L

Result


Job Number: 640-14966-1



Lab File lD: FEBRO8



Qual POL


Sodium

Lab Gontrol Spike/Lab Cont¡ot Spike Duplicate Recovery Report'Batch: 640-41390

LCS Lab Sample lD: LCS 640-41390/2-A

21

4.20.461.5

7.1

2.0

220

Analysis Balch: 64041 442


Units: ug/L

Analysis Balcht 64041 442


Units: ug/L

% Rec.

LCS LCSD

Method:60108Preparation: 30054Total Recove¡able


Lab File lD: FEBRO8




Lab File lD: FEBRO8



U

U

U

U

U

U

MDL

21-*4.20.461.5

4.62.0220

20010

5.0

10

50

5.0

1 000

Client Matrix:

Dilution:

Date Analyzed:

Date Prepared:

Client Matrix:

Dilution:

Date Analyzed:

Date Prepared:

Analyte

Water

1.0

02t05t2008 1620

02105/2008 0900

Water

1.0

0210512008 1621

02105/2008 0900

ML

ML

LCSD Lab Sample lD: LCSD 640-41390/3-A

RPDLmt RPD Limit LCS Qual LCSD Qual

Aluminum

Arsenic

CadmiumChromium

lron

Lead

Sodium

80 - 120

80 - 120

80 - 120

80 - 120

80 - 120

80 - 120

80 - 120

20¿v¿U

2020

20

20

2

J

z

93

97

98

9807

94OA

95

100

101

101

100

97

100







Dilution: 1.0





Units: mg/L

Result


Job Number: 640-14966-1



Lab File lD: N/A



MDL PQL

0.000072 0.00020



Lab File lD: N/A



Analyte

Mercury 0.000072 u

Qual

Lab Gontrol Spike/Lab Gontrol Spike Duplicate Recovery Report - Batch: 660-57155

LCS Lab Sample lD: LCS 660-57155/2-A Analysis Batch: 660-57194


Dilution: 1.0



Analyte


Units: mg/L

LCSD Lab Sample lD: LCSD 660-57155/3-A Analysis Batch: 660-57194 lnstrument lD: Hg Analyzer



Date Analyzed: 0210512008 1443 Final WeighWolume: 25'0 mL


% Rec.


Mercury 92 93 80-120 1 20


TestAmerlca Tallahassee Page 31 of 38 02 / 08 /2008





Dilution: 1.0


Date Prepared: N/A

Analyte


Prep Batch: N/A

Units: mg/L

Result


Job Number: 640-'14966-1

Method: 160.1

Preparation: N/A

lnstrument lD: No Equipment Ass¡gned

Lab File lD: N/A



PQL PQLQua

Total Dissolved Solids 5.0

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 640'41353

5.0 5.0


LCS Lab Sample lD: LCS 640-41353/2 Analysis Batch: 640-41353 lnstrument lD: No Equipment Assigned


Dilution: 1 .0 Jnits: mg/L lnitial WeighWolume: 100 mL

Date Analyzed: O2lO4l2OO8 1143 Final WeighWolume: 200 mL

Date Preoared: N/A

LCSD Lab Sample lD: LCSD 640-41353/3 Analysis Batch: 64041353 lnstrument lD: No Equipment Assigned


Dilution: l.O Jnits: mg/L lnitial WeighWolume: 100 mL

Date Analyzed: 0210412008 1143 Final WeighWolume: 200 mL

Date Prepared: N/A

Analyte

% Rec.


Total Dissolved Solids 98 97 80-120 0 25




Method BIank - Batch: 640-41256



Dilution: 1.0


Date Prepared: N/A

Analyte


Prep Batch: N/A

Units: mgil

Result


Job Number: 640-14966-1

Method: 325.2

Preparation: N/A


Lab File lD: N/A



MDL PQLOual

Chloride 0.22

Lab Control Spike/Lab Gontrol Spike Duplicate Recovery Report - Batch: 640'41256

Analyte

0.22 1.0


LCS Lab Samole lD: LCS 640-41256/2 Analysis Batch: 640-41256 lnstrument lD: Konelab



DateAnalyzed: O1t31l2OO8 1017 Final WeighWolume: 2.0 mL

Date Prepared: N/A

LCSD Lab Sample lD: LCSD 640-41256/3 Analysis Batch: 640-41256 lnstrument lD: Konelab



DateAnalyzed: O1l31t2OO8 1017 Final WeighWolume: 2.0 mL

Date Prepared: N/A

% Rec.


Chloride 100 100 85-115 1 30

Calculations are performed before round¡ng to avoid round-off errors in calculated results.

TestAmericaTailahassee Page 33 of 38 02/0g/2008

Client: Golder Assodates lnc.




Dilution: 1.0


Date Prepared: N/A

Analyte


Prep Batch: N/A

Units: mg/L

Result


Job Number: 640-',l4966-1

Method: 350.1

Preparation: N/A


Lab File lD: N/A




0.0013

Qual

Ammonia

Lab Control Spike/Lab Control Spike Duplicate Recovery Report'Batch: 640-41499

LCS Lab Sample lD: LCS 640-41499/2 Analysis Batch: 64041499 lnstrument lD: Astoria



DateAnalyzed: O2tO7l2OO8 1249 Final WeighWolume: 25.0 mL

Date Prepared: N/A




Date Analyzed: O2lO7l2OO8 1251 Final WeighWolume: 25 0 mL

Date Prepared: NiA

Analyte

% Rec

LCS LCSD Limil RPD RPD Lim¡t LCS Qual LCSD Qual

Ammonia 109 114 85 - 115 4 30


TestAmer¡ca Tallahassee Page 34 of 31 02 / 08 /2008





Dilution: 1.0


Date Prepared: N/A

Analyte


Prep Batch: NiA

Units: mg/L

Result

QualltY Control Results

Job Number: 640-14966-1

Method: 353.2

Preparation: N/A


Lab File lD: N/A

lnitial Weighwolume: 25.0 mL


MDL PQLQual


Lab Control Spike/

0.00061 I 0.0001 1 0.010

Method: 353.2

Preparation: N/ALab Gontrol Spike Duplicate Recovery Report - Batch: 640-41514

LCS Lab Sampte lD: LCS640-4151412 Analysis Batch: 640-41514 lnstrument lD: Astoria


Dilution: 1.0 Units: mg/L lnitial WeighWolume: 25 0 mL

DateAnalyzed: O2tO7l2OO8 1502 Final WeighWolume: 25'0 mL

Date Preþared: N/A

LCSD Lab Sample lD: LCSD 640-41514/3 Analysis Batch: 64041514 lnstrument lD: Astoria


Dilution: 1.0 Units: mg/L lnitial WeighWolume: 25 0 mL

DateAnalyzed: O\\OT\^OOB 1503 Final WeighWolume: 25'0 mL

Date Prepared: N/A

Analyte

% Rec.


Nitrate Nitr¡te as N 110 108 90-110 1 30


TestAmericaTallahassee Page 35 of 38 02/08/2009



Lab Sample lD: MB 640-4'125711


Dilution: 1.0


Date Prepared: N/A

Analyte

Analysis Balch: 64041257

Prep Batch: N/A

Units: mg/L

Sulfate

Resull

i t'*

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 640'41257

LCSD Lab Sample lD: LCSD 640-41257/3 Analysis Balch: 64041257


Job Number: 640-'14966-1

Method: 375.4

Preparation: N/A


Lab File lD: N/A



MDL PQLQua

LCS Lab Sample lD: LCS 640-4125712 Analysis Batch: 640-41257 lnstrument lD: Konelab


Dilution: l.O Units: mg/L lnitial WeighUVolume: 2 0 mL

Date Analyzed: O1l31t2OOB 1016 Final WeighWolume: 2 0 mL

Date Prepared: N/A

1.3 5.0

Method: 375.4

Preparation: N/A


Lab File lD: N/A

lnitial Weighwolume: 2.0 mL



Dilution: 1.0


Date Prepared: N/A

Prep Batch: N/A

Units: mg/L

Analyte

% Rec.


Sulfate 't02 102 85 - 1 15 0 30


TestAmericaTallahassee Page 36 of 38 02/08/2008



Lab Sample lD: MB 680-97389/l-A


Dilution: 1.0





Units: mg/L

Result


Job Number: 640-14966-1

Method: 420.1

Preparation: Distill/Phenol


Lab File lD: N/A



MDL PQLQualAnalyte

Phenolics, Total Recoverable

Lab Control Spike/

0.025 0.025 0.050

Method: 420.1

Preparation: Distill/PhenolLab Control Spike Duplicate Recovery Report'Batch: 680-97389

LCS Lab Sample lD: LCS 680-97389/2-A Analysis Batch: 680-97390 lnstrument lD: No Equipment Assigned

client Matrix: water Prep Batch: 680-97389 Lab File lD: N/A


Date Analyzed: 02106/2008 0801 Final WeighWolume: 100 mL


LCSD Lab Sampte lD: LCSD 680-97389/3-A Analysis Batch: 680-97390 lnstrument lD: No Equipment Assigned


Dilution: 1 .O Units: mg/L lnitial WeighWolume: 100 mL

Date Analyzed: 02106/2008 O8O1 Final WeighWolume: 100 mL

Date Prepared: A210612008 0752

Analyte

% Rec.


Phenolics, Total Recoverable 106 '112 75 - 125 6 30

Calculations are performed before rounding to avoid round-off errors in calculated results


fesfÅrn@gJaclsonville Service Cenfer

Ghain of tustodY Record

Phone(904) 519'05s1 Fax 519-s552

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TestAmericoIHË LËAOËR IN ÈNVIRONMTN I'At

ANALYTICAL REPORT

Job Number: 640-15103-1


For:

Golder Associates lnc.942SBaymeadows Road

Suite 400Jacksonville, FL 32256

Attention: Mr, Rich W Poff


Project Manager I

chad. [email protected]: 1

These test results meet all the requirements of NELAC. All questions regarding this test report should be directed to the

TestAmerica Project Manager who signed this test report'Measurement uncertainty dãta, as referenced in Section 8.6 of the TestAmerica Tallahassee LQM, are available upon

request.

Florida Department of Health Certifìcation No. E81005TestAmerica Tampa DOH Certification No. E84282

TestAmerica Laboratories, lnc.

TestAmerica Tallahassee 2846 lndustrial Plaza Drive, Tallahassee, FL 32301

Tel (850) 878-3994 Fax (850) 878-9504 www.testamerlcainc.com

Page 1 of L2 o4/ o8 /2008

Job Narrative640-J1 51 03-l

GommentsNo additional comments.

ReceiptAll samples were received in good condition within temperature requirements

MetalsNo analytical or quality issues were noted.

Page 2 of t2 04/ 08/2008


Lab Sample lD Glient Sample lDAnalyte


Job Number: 640-15103-1

ReportingResult / Qualifier Limit Units Method

640-15103-2 lDw

Mercury 0.000099 I 0.00020 mg/L 74704


Page 3 of, L2 04 / 08/ 2OO8

METHOD SUMMARY

Client: Golder Associates lnc. Job Number: 640-15103-1

Matrix: Water

Mercury in Liquid Waste (Manual Cold Vapor Technique)

Sample Filtration performed in the Field


Lab References:


TAL TAM

TAL TAM

TAL TAM

sw846 74704FIELD FLTRD

sw846 74704

Method References:

SWB46 =,'Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And lts Updates.


Page 4 of L2 04/ 08 / 2008

SAMPLE SUMMARY

Client: Golder Associates lnc. Job Number: 640-15103-1

Date/TimeDate/Time

640-151 03-1

640-151 03-2

MW-gDIDW

Client Matrix


Page 5 of. L2 04/ 08 /200s

SAMPLE RESULTS


Page 6 of. L2 04 / 08 /2A08


Analytical Data

Job Number: 640-15103-1

Client Sample lD: MW-9D

Lab Samole lD: 640-15103-1 Date Sampled: 0210612008 1456

Client Matrix: Water Date Received: 02i08/2008 0931

74704 Mercury in Liquid Waste (Manual Cold Vapor Technique)

Method: 7470A Analysis Batch: 660-57779 lnstrument lD: Hg Analyzer

Preparation: 7470A Prep Batch:660-57713 Lab File lD: N/A

Dilution: 'l.O lnitial WeightA/olume: 25.0 mL

DateAnalyzed: O2l15l2OO8 1443 FinalWeighWolume: 25.0 mL


T*:: --- * - - -T:::l:1T9**---*Îr151- " *y?: -*- --lÎ: -74704 Mercury in Liquid Waste (Manual Gold Vapor Technique)-Dissolved

Method: 7470A Analysis Batch: 660-57779 lnstrument lD: Hg Analyzer

Preparation: 7470A Prep Batch:660-57713 Lab File lD: N/A

Dilution: 1.0 lnitial WeighWolume: 25.0 mL

Date Analyzed 0211512008 1445 FinalWeighWolume: 25.0 mL

Date Preoared. 0211512008 0918

Analyte'Meräury


o¡ooo72*** ît "îööó"2ö


Analytical Data

Job Number: 640-15103-1Client: Golder Associates lnc.

Glient Sample lD: IDW

Lab Sample lD: 640-15'103-2


Date Sampled: 0210612008 1530


Method: 7470P.

Preparation: 74704Dilution: 1.0

Date Analyzed: 0211512008 1446Date Prepared: 0211512008 0918

Analyte


Analysis Batch: 660-57779 lnstrument lD: Hg Analyzer

Preo Batch: 660-57713 Lab File lD: N/A




Mercury

TestAmerica Tallahassee Page I of t2 04 / 08 /2008



Lab Section Qualifier Description

Job Number: 640-15103-1

lndicates that the compound was analyzed for but notdetected.

The reported value is between the laboratory method detectionlimit and the laboratory practicalquantitation limit.


Page 9 of 72 04 / 0e /2a08

QUALITY GONTROL RESULTS


Page 10 ot L2 o4/ o8/2008




Job Number: 640-15103-1

Method:74704Preparation:7470Á.

Lab Sample lD: MB 660-5771311-A Analysis Batch: 660-57779 lnstrument lD: Hg Analyzer

Client Matrix: Water Prep Batch: 660-57713 Lab File lD: NiA

Dilution: 1.0 Units: mg/L lnitialWeighUVolume: 25.0 mL

DateAnalyzed: Q2l15l2OO8 1357 FinalWeighWolume: 25.0 mL

Date Prepared: 02115120O8 0918

Analyte Result Qual MDL PQL

Mercury ^ *-- 0-ooôò?î*"-

"'-*"u * -ö:ö00ö7ä-" *"öö020 - -

Lab Gontrolspike/ Method: 7470A.

Lab Gontrolspike Duplicate Recovery Report - Batch: 660-57713 Preparationl.74704

LCS Lab Sample lD: LCS 660-5771312-A Analysis Batch: 660-57779 lnstrument lD: Hg Analyzer


Dilution: 1.0 Units: mg/L lnitialWeighWolume: 25.0 mL

DateAnalyzed: O2t15l2OO8 1359 FinalWeighWolume: 25.0 mL

Date Prepared . 0211512008 0918

LCSD Lab Sample lD:LCSD 660-57713/3-A Analysis Batch: 660-57779 lnstrument lD: Hg Analyzer


Dilution: 'l.O Units: mg/L lnitialWeighWolume: 25.0 mL

DateAnalyzed: O2l15l2OO8 1401 FinalWeighWolume: 25.0 mL

Date Preoared'. 0211512008 0918

Analyte

% Rec.


Mercury 99 98 80-120 1 20


TestAmerica Tallahassee Page 11 of L2 04/08/2008

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APPENDIX E

FDEP Parameter Monitoring Report Forms (Form 62-522.900(2))

ACRES C&D LANDTTLL

)NITORING REFORT70t.730(2Xb)

rter Monitoring (P¡ge I of 3l

SAMPLE DATE 1/2912008

MONITORING WELL WACS# 12976 ANALYSIS DATE I/3Il08 Io 2/07/08

WELL NAME MV/-2

CLASSIFICATION OF GROUNDWATER G-II(DE) Detecrion(CE) Compliance(OT) OtherWell Purged* prior ro

Sample Colleccion (Yes/No) Groundwater Elevation (NGVD) 41. l3Yes

STORETCODE

PARAMETERMONITOREI)

SAMPLINGMETTIOD

ANALYSISMnlf¡ôn

ANALYSIIRESTJLT

ANALYSISn/t Tn/TlÀ'l*' I,JNITS

TTLTERED/lWMDDT

TRESER,VATTVEIADDED

082545

000010

o'00299

000406

000094

082078

000610

000940

000ó20

032730

000945

070300

001 105

001002

ffi1027

001034

001045

001051

071900

000929

MNTAI.S

Aluminum

Arsenic

Cadmium

Chromium

Iron

Lead

Mercury

Sodium

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

350. I

325.2

353.2

420,1

375.4

160. I

6010

6010

6010

ó010

6010

6010

7470

6010

35.53

¿1.)

4.1

7 .tt

203

5.37

0,0058 IV

3.2

0.43

0.025 u

1.3 u

t20

120 |

4.2 U

0.46 U

2.3 t

220V

2.0 u

0.072u

2.8

v29t2008

tl29l2M8 lO:01

112912008 10:07

t/2912008 lO:07

ll29l2û08 10:07

112912008 10:07

AO7l2AO8 D:52

l/31/2008 l0:33

210712008 17:30

2/06/2008 08:01

l/31/2008 10:16

210412008 1l:47

FT NGVD

'c

mglL

STD

pmhos/cm

NTUs

mglL

mglL

mglL

mg/L

mglL

Unfilrered

Unfiltered

Unfilte¡ed

Unfìlte¡ed

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfilte¡ed

Unfiltered

Unfiltered

Unf,ltered

Unfiltered

Unfiltered

Unf¡ltered

Unfiltered

Unfiltered

None

None

None

None

None

H2SO.

None

None

H2S04

None

None

HNOr

HNO3

HNOI

HNO,

HN03

HNOs

HNOs

HNO.

*well Pur8¡ng is lhe process ofpumping the well prio¡ to sampling in order to obtain a represenàtive g¡oundwater sampleDEP Forn ó2-522.900(2) Effecrive Aprit 14, 1994

VEOLIA CYPRESS ACRES C&D LANDFTLL

PARAMETER MONITORING REPORT(Rule ó2-701.730(2Xb))

FACILITY WACS# 21251 SAMPLE DATE U29t2m8

MONITORING WELL WACS# 12976 ANALYSTS DATE 7t24t07 to 8t04to7

WELL NAME MI¡/-2

CLASSIFICATION OF GROUNDWATER G-II

tilell Purged* prior to

Sample Collection (Yes/No)

ìJI¡ELL TYPE:

Yes Groundwater Elevation (NGVD) 41.11

(BG) Background(DE) Detection(CE) Compliance(OT) Other

BG

STORETl-ônF. PARÂMETER MONITORED

ùA]v TL¡Nt'METHOI)

AÑAl,IùIÙMETHOD

¡INA¡J I SI¡RESI.JLT

ANALYSISDATE/TIME T]NITS

FILTERED/fÌNÍ'II,'TTNf.I

PRESE.RVATIVEIADDEI)

032 l0r

032104

0344t3

032t02

034301

0343 I 1

034576

032106

03,1418

032r05

034536

034566

03457 I

034668

034496

03453 I

034501

077093

034546

034541

Bromodichloromethane

B¡omoform

Bromomethane

Carbon Tetrachlo¡ide

Chlorobezene

Chloroethane

2-Chloroethyl vinyl erher

Chlo¡oform

Chloromethane

Díb¡omochloromethane

I,2-DichÌorober¿ene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

Dichlo¡odifl uoromethane

1,1 -Dichloroethane

1,2-Dichloroethane

l, l-Dichloroethene

cis- 1,2-Dichloroethene

trans- 1,2-Dichloroelhene

I .2-Dichlorooronane

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bfadder Pump

Bladder Pump

Rl¡¡lãe¡ Þrmn

82608

82608

82608

82608

82608

82608

8260B

82ó08

82608

82608

82608

82608

82608

8260B

82ûB

82ó08

82608

82608

82608

trÁnR

0.10 u

0.13 U

0.17 U

0.078 u

0.079 u

0.11 U

1.2 UJ

0.28 I

0.080 u

0.080 u

0.076 u

0.082 u

0.14 u

0.075 u

0.0ó7 u

0.082 u

0.ll u

0.18 U

0.25 U

rì ln rT

210712008 14:53

2107 12008 14:53

2107 12008 14:53

2lO7l20O8 14:53

2lO7l2O08 14:53

2107/2008 14:53

210712008 t4:53

2l0'll2N8 14:53

210712008 t4:53

210712008 14:53

210712008 t4:53

2107l20OB 14:53

2107 12008 14:53

2107 l20OB 14:53

2/0712008 l4:53

2lO7l2OO8 14:53

2lO7 12008 14:53

210712ffi8 14:53

210712008 14:53

2lO7 12008 14:53

pgll

pgll

p9ll

pcll

pcll

pglt

pgll

Itgll

þgll

þgll

pgll

ttgll

p9ll

pcll

pcll

pgll

pgll

ttgll

pgll

Unfiltered

Unñltered

Unfiltered

Unfìltered

Unfilte¡ed

Unfiltered

Unfilte¡ed

Unfil¡ered

Unhltered

Unfiltered

Unfiltered

Unhltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

Hl.I

*Well Purging ¡s the process of pumping the well pr¡or to sampling ¡n order to obtain a represenøtive groundwter sample.

DEP Form ó2-522.900(2) Effective April 14, 1994

I'EOLIA CYPRESS ACRES C&D LANDFILL

PARAMEÏER MONITORING REFORT(Rule 62-?01.730(2Xb))

IACILITY WACS# 21251 SAMPLE DATE U29t2008

{ONITORINGV/ELLWACS# 12976 ANALYSIS DATE ll3ll08 rozl07/08

YELL NAME MW-2

:LASSIFICATION OF GROUNDV/ATER G-II

WELL TYPE: BG (BG) Background(DE) Detection(CE) Compliance(OT) Other

[ell Purged* prior toSample Collection (Yes/No) Yes Groundwater Elevation (NGVD) 41.13

STORETf!ftnF PARAMETTR MONITORED

ù,¿tI/tfLTN(;METHOI)

AIìALIJIJMETTIOD

ANALY¡'IIREST]LT

ANALYSISfìÂTE'./TIMü' T-INITS

FILTERED/ PRESERVATTYEIADDED

034704

034699

034423

034516

034475

034506

03451 I

0391 80

034488

039175

034030

03437t

034010

034020

ug91



Methylene Chloride

l, 1,2,2-Telrachloroethane

Tet¡achloroethene

l, l, 1-Trichloroethane


Trichlo¡oethene

Trichlorofl uo¡omethane

Vinyl Chloride

Beuene

Ethylbeüene

Toluene

Xylenes

Merhyl tert-butyl ether

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

82608

82608

82608

82608

82608

82ó08

82608

82608

8260B

82608

82608

82608

82608

82608

82ó08

0.082 u

0.077 u

0.17 U

0.070 u

0.24 U

0.ll u

0.20 u

013u

0.12 u

0,058 u

0.058 u

0.078 u

0.063 u

0.ll u

0.065 u

2lO7l2OO8 14:53

2lO7l2OO8 14:53

2lO7/2008 l4:53

2lO7l2O08 14:53

2lO7|2OOB 14:53

210712008 14:53

210712408 14:53

2107 12O08 t4:53

210712008 14:53

21O712008 14:53

210712408 ß:53

21O712008 14:53

210712ffi8 14:53

2lO7l2OO8 14:53

2lO7l20O8 14:53

pgll

pgll

pïll

þcll

pcll

pcll

pcll

Itgll

pgll

Itgll

ttgll

p$ll

Æll

pgll

p9ll

Unfilte¡ed

Unfiltered

Unfil¡e¡ed

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unñltered

Unfiltered

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

*Well Purging is the process of pump¡ng the well prior to sampl¡ng in order to obta¡n a represenbt¡ve Broundwater sample

DEP Form 62-522 900(2) Effærive April 14, 1994

VEOLIA CYPRESS ÀCRES C&D LANDTILL

PARAMETER MONITORING REPORT(Rule 62-701.730(2)(b))

FACILITY V/ACS# 21251 SAMPLE DATE U30t2û8

MONITORING WELL'IYACS# 12977 ANALYSIS DATE ll3ll2û08 to 2/0712008

WELLNAME MW4


Well Purged+ prior toSample Collection (Yes/No)

WELL TYPE:

Yes Groundwater Elevation (NGVD) 40.61

(BG) Background(DE) Detection(CE) Compliance(OT) Other

CE

STORETt-ôDú'.

PARAMETERMONITORÍ"D

ò,¡II} TLIN('METHOD

A¡IALIJIÙMETHOD

ANALYSI!RESI]LT

ANALYSISIìÄTM/TÌMN IJNITS

FILTERED/ PKT;ST'RVATIVETADDEI)

082545

000010

0'00299

000,106

000094

082078

000610

000940

000620

032730

000945

070300

001 105

001002

00t027

001034

001045

00105 I

071900

æ0929

NiraÞ as N

Phenols

Sulfate

To¡al Dissolved Sotids

MFTÀTS

Aluminum

Arsenic

Cadmium

Chromium

Iron

Lead

Mercury

Sodium

Grab

Grab

Grab

Grab

Grab

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

BIadde¡ Pumn

350. I

325.2

353.2

420.1

375.4

I 60.1

60r0

6010

6010

6010

6010

6010

7470

fflln

40.29

22.16

1.5

7.12

416

7.12

0.18 v

9.2

0.48 V

0.025 u

12

220

80 I

4.2 tJ

0.46 U

1.9 I

87V

2.0u

0.012 u

7.4

t/30t2008

113O/2408 2:45

ll30l2008 12:45

113012008 12:45

ll30l2û08 12:45

ll30l2A08 0:45

21O712008 13:04

ll3ll2ffi8 19:12

210712008 17:30

2106/2008 O8:01

ll31l20O8 l6:47

2lMl2O08 11:48

210512008 16:59

2lO5l2A08 t6:59

210512008 16:59

210512408 ß:59

2105120f8 16:59

2/O512008 16:59

2105l20OB l5:12

2lO5l2OO8 16:59

FT NGVD

"C

mg/L

STD

¡¿mhos/cm

NTUs

mglL

mglL

mglL

mglL

mglL

mglL

pgll

tLgll

pgll

þcll

pgll

pcll

pcll

mplf.

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfil¡ered

Unfilte¡ed

Unhltered

Unfilte¡ed

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfilte¡ed

Unfiltered

Unfiltered

Unfìltered

Unfiltered

Unfiltered

None

None

None

None

None

H2SO4

None

None

H2S04

None

None

HNOI

HN03

HN03

HN03

HN03

HN03

HNOs

HNO"

*Well Purging is the præess of pump¡ng the well prior lo sâmpling in order to obain a represenhtive groundwater sample

DEP Form 62-522 900(2) Effective April 14, I994

FACILITY WACS# 21251

MONITORING WELL WACS# 12977

WELL NAME Mtù/4


VEOLIA CYPRESS ACRES C&D LANDFILL

PAR.AMETTR MONITORING REFORT(Rule 62-701.730(2)(b))

Seni-Annul Grounrlweter Moniloring lPage 2 of 3)

Yes

SAMPLE DATE II3OI2OO8

ANALYSIS DATE II3V2m8 þ 2IO7I2OO8

WELL TYPE: CE (BG) Background

Groundwater Elevation (NGVD)

(DE) Detection(CE) Compliance(OT) Orher

40.6t

Well Purged+ prior toSample Collection (Yes/No)

STORETnônÍ' PARAMETER MONITORED

SAMPLINGIlifNTTIôN

ANALYSISMÍ'TTTTìN

ANALYSIIRESTJLT

ANA¡JY¡'I¡iDATE/TIME IJNITS

FILTERED/I lNf'tr .Tf'Dnr

PRDSERVATTVEIADDÍ:,T)

032101

032104

034413

032102

034301

03431 I

034576

032106

03441 8

032105

034536

034566

03457 |

034668

034496

03453 I

034s01

077093

034546

034541


Bromoform

Bromomethane

Carbon Tetrachloride

Chlorobemene

Chlo¡oethane

2-Chloroe¡hyl vinyl ether

Chlo¡oform

Chloromethane

Dìbromochloromethane

1,2-Dichlorobeuene

1,3-Dichlorobeuene

1,4-Dichlorobenzene


1,1-Dicblo¡oethane

1,2-Dichloroethane

1, l-Dichloroethene

cis-1,2-Dichlo¡oethene

trans- 1,2-Dichloroethene

I ?-fli¡hln¡n¡¡nnqnp

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

82608

82608

82ó08

82ó0B

82608

82608

82608

82608

82608

82608

82608

82608

0.10 u

0.13 u

0,17 u

0.078 u

0.079 u

0.ll u

1.2 ut

0.056 u

0.080 u

0.080 u

0.076 u

0.082 u

0.14 u

0.075 u

0.067 u

0.082 u

0.11 U

0.18 U

0.25 U

nl0lt

210712008 15:22

2lO7l20O8 15:22

210712008 15:22

2107/2008 t5:22

2lO7l2NB 15:22

210712008 15:22

210712008 15:22

210712008 15:22

210712008 15:22

210712008 15:22

2/0712008 15:22

2lO7/2008 15:22

2/0712008 t5:22

2/0712008 15:22

210712008 15:22

rgll

pgll

pcll

p*ll

pcll

pc/l

pell

pgll

þc/l

pgll

pgll

p\ll

Ælt

þgll

tïll

þgll

p}ll

pgll

ttgll

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfilte¡ed

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfilre¡ed

Unfiltered

Unfilte¡ed

Unfiltered

Unfilte¡ed

Unfiltered

Unfiltered

Unfilte¡ed

Unfiltered

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

Hl-I

+Well Purging is the process of pumpin8 the well prior to samplin8 ¡n order to obtain a represenht¡ve groundwater sample,

DEP Form 62'522.900(2) Effective April 14, 1994

I VEOLIACYPRESSACRESC&DLANDFILLI

PARAMETER MONITORING REFORT(Rute 62-701.730(2Xb))

Semi-Annul Groundwaler Moniforing lPage I of 1)

FACILITY WACS# 2125I SAMPLE DATE II3OIzcf,ï

MONITORING ìVELL WACS# 12977 ANALYSIS DATE l/31/2008 ro 2/0?/2008

V/ELL NAME MW-4 WELL TYPE: CE (Bc) Background

CLASSIFICATION OF GROUNDÌ/ATER G-II(DE) Detecrion(CE) Compliance(OT) Orhe¡

Groundwater Elevation (NGVD) 40.61Yes

Well Purged* prior toSample Collection (Yes/No)

STORETCODE PARAMETER MONITORED

SAMPLINGMN-TT¡IID

ANALYSIStilú'TTTôN

ANALYSI!RftslIf .T

ANALYSISDATE/TIME TJNITS

FILÏERED/lllû'fr.rTnÍ't

PRFSERVATIVEIADIIEI)

03470/.

034699

034423

034516

034475

034506

0345 I I

0391 80

034488

039175

034030

03437t

034010

034020

a4&91


trans- 1,3-Dichlo¡opropene

Methylene Chloride

l, 1,2,2-Tetrachìoroerhane

Telrachloroethene

1, I , l-Trichloroethane

1, 1,2-T¡ichlo¡oetbane

Trichloroethene


Vinyl Chloride

Benzene

Ethylbeuene

Toluene

Xylenes

Methyl Tert-Buryl Erher

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

8260B

82608

82608

82608

8260B

82608

82608

82608

8260B

82608

82608

82608

82608

82608

82608

0.082 u

0.077 u

0.17 u

0.070 u

0.24 U

0.ll u

0.20 u

0.13 u

0.12 U

0.058 u

0.058 u

0.078 u

0.063 u

0.ll u

0.065 u

210712008 15:22

210712008 t5:22

2107/2008 t5:22

210712008 15:27

210712008 15:22

210'112008 15:22

210712008 15:22

210712008 15:22

210712008 15:22

210712008 15:22

t|gll

þgll

pgll

þgll

þgll

þgll

pgll

Fcll

pgll

pcll

p8/l

Itgll

Itglt

ttgll

ttgll

Unfiltered

Unfilrered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unhltered

Unflltered

Unfiltered

Unfiltered

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

*Well Purging ¡s the prccess of pump¡ng the well prior to såmpl¡nB in order to obtain a representative groundwter sample

DEP Form 62-522.900(2) Effective Ap¡il 14. 1994

FACILITY WACS# 2t251 SAMPLE DATE U29t2008

VEOLIA CY?RESS ACRES C&D LANDFILL

PAR,A,METER MONITORING REPORT(Rule 62-701.730(2)(b))

Semi-Annml Groundwater Monitoring lPage I of 3)

MONITORING V/ELL WACS# 129'18

WELL NAME MW.5

CLASSIFICATION OF GROUNDÏVATER G.II

ANALYSIS DATE IIf |I2OOE TO 2IO7I2OO8

WELL TYPE: cE (BG) Background(DE) Detection(CE) Compliance(OT) Other

Groundwater Elevation (NGVD)Yes 40 69

Well Purged+ prior toSample Collection (YeVNo)

STORETCODE

PARAMETERMO¡lITORED

SAMPLINGMETTIOD

ANALYSISMETl{OI)

ANALYSIfRESTII,T

ANALYSIsDATTiTIME UNITS

FILIERED/TNT¡ff .TT'NÍ'T

PRF,SERVATÏVETADDED

082545

000010

0'00299

000406

000094

082078

000610

000940

000620

032730

000945

070300

001 105

001002

001027

001034

001045

00105 I

07 1900

000929

Spec. Conductance (field)

Turbidity (field)

Ammonia as N

Chlorides

Nitrate as N

Phenols

Sulfate


METAI,S

Aluminum

Arsenic

Cadmium

Chromium

Iron

Lead

Mercury

Sodium

Grab

Grab

Grab

Grab

Grab

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pumo

350. I

325.2

353.2

420.1

37s.4

160.1

60r0

6010

6010

6010

6010

6010

7470

Ánln

39.70

2l.16

3.92

7.30

366

1.07

0.0088 rv

5.7

0.47

0.025 u

1.3 U

200

21 U

4.2U

0.46 U

1.9 I

4.6U

2.0 u

o.o72 u

3.8

u29t2008

ll29l2NB 14:17

112912008 14:17

Il29l20f9 14:17

112912008 14:17

112912008 14:17

210712008 13:01

l/3112û8 10:33

210712008 I7:30

2106l2NE 08:01

I13I12008 10:28

2lMl2ffi8 ll:47

210512008 l3:O9

2105120[,8 13:09

21O512008 13:09

2/0512008 13:O9

2/05/2008 13:09

210512A08 ß:O9

210512ffi8 15:06

210512008 13:09

FT NGVD

"c

mglL

STD

pmhos,/cm

NTUs

mglL

nglL

mglL

mglL

mg/L

pEll

pgll

pgl'l

pgtl

pgll

ttgll

us.ll

msll.

Unfìltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfìltered

Unfiltered

Unfìltered

UnFrltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfilte¡ed

Unfil¡ered

Unfiltered

Unfiltered

None

None

None

None

None

HrSQ

None

None

H2S04

None

None

HN03

HN03

HNOs

HNO3

HNOs

HN03

HNO3

HNO-

*Well Purging ¡s the process of pump¡ng the well pr¡or to sampling in order to obtain a represenbt¡ve groundwater sample

DEP Form 62-522 900(2) Effective April 14, 1994

VEOLIA CYPR-ESS ACRES C&D LAI|IDFILL

PARAMETER MOMTORING REPORT(Rule 62-701.730(2)(b))

Semi-Annml Groundwater Monitoring (Page 2 of 3l


MONTTORTNG V/ELL WACS# 12918

WELL NAME MW-5


Welì Purgedt prior toSample Collection (Yes/No)

SAMPLE DATE II29I2OO8

ANALYSIS DATE 1/31/2008 TO 2/07/2008



(DE) Derecrion(CE) Compliance(OT) Other

40.69Yes

STORETCODE PARAMETER MOMTOREI)

SAMPLINGMETHOD

ANALYSISMETTIOD

ÄNALYSI!RF',ST]I,T

ANALYSISDATE/TIME I'MTS

FILTT,RED/IINF'TT,TE"RET

PRESERVAITVEIannÍ'.D

032101

032tM

034413

032102

034301

0343 1 1

034576

032t06

03441 8

03210s

034s36

034s66

03457r

034668

034496

034531

034501

077093

034546

î7Á.<L1


Bromoform

Bromomethane

Carbon Te¡rachloride

Chlorobenzene

Chloroethane


Chloroform

Chloromethane

Dibromochloromethane

1,2-Dichlo¡obenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

Dichlorod ifl uoromethane

I ,1 -Dichloroethane

I ,2-Dichloroethane

1,1-Dichloroethene



I -2-I)ichloronronane

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Btadder Pump

82608

82608

8260B

82608

82608

82608

82608

82608

82608

82608

82608

82608

82608

82608

82608

82ffi8

82608

82ñB

82608

.RtÁnR

0.10 u

0.13 U

0.17 U

0.078 u

0.079 u

0.11 u

I.2 UJ

0.0s6 u

0.080 u

0.0E0 u

0.076 u

0.082 u

014U

0.075 u

0.067 u

0.082 u

0.11 u

0.18 U

0.25 U

ô lN TI

2107l20OB L5:51

2107/2008 15:51

210712008 15:51

210712008 15:51

210712008 15:51

210712008 15:51

2107120[8 15:51

2/0712008 15.51

210712008 15:51

2107l20OB 15:51

210712008 15:51

210712Cf8 15:51

210712008 15:51

2lO7l2N8 15:51

2107/2008 15:51

210712008 15:51

210712408 ß:51

210712008 15:51

2/07 12008 15:51

210712008 15:51

pgll

pgll

pgll

þgll

pg^

Itgll

pgll

þgll

þgll

pgll

pgll

þgll

Pgll

pgll

þgll

þgll

ttEll

pEll

pgll

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfrltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfìlte¡ed

Unfiltered

Unfiltered

Unfrltered

Unfiltered

Unfiltered

Ilnfiltered

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

t{cI

+\ilell Purging ¡s the process of Pump¡ng the well prior to sampling in order to obtain å representât¡ve groundMter sample

DEP Form 62-522,900(2) Etfecr¡ve April 14, 1994

I VEOLIACYPRESSACRESC&DLANDFILL

I

I PARAMETERMOMTORINGREPORT(Rule 62-701.730(2)(b))

Semi-Amul Groundweter Monitoring lPage 3 of 3)

FACILITY Iù/ACS/ 21251 SAMPLE DATE II2}I2OO8

MONITORING WELL WACS# 12978 ANALYSIS DATE I/31/2008 TO 2/0?/2008

WELL NAME MW-5 WELL TYPE: CE (BG) Background

CLASSIFICATION OF GROUNDWATER G-II(DE) Detectjon(CE) Compliance(OT) Other


rly'ell Purged* prior toSample Collection (YeVNo)

STORETCODE PARAMETTR MONITOREI)

SAMPLINGMETHOI)

ANALYSISMETHOI)

ANALYSISRESTlI,T

ANALYSISDATE/TIME UNITS

FILTERED/lNTnMDDI

PRESERVAITVE{ADDET)

0347M

034699

034423

034516

0344'15

034506

0345 I I

039180

03448E

039175

034030

0f437 1

034010

034020

046/91



Methylene Chloride

l, 1,2,2-Tetrachloroethane

Tetrachìoroethene

l, l, I -Trichloroethane

1, 1,2-Trichloroethane

Trichloroethene


Vinyl Chloride

Benzene

Ethylbenzene

Toluene

Xylenes

Methyl Tert-butyl Ether

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

82608

82608

82608

8260B

82608

82608

E260B

82608

82608

82608

8260B

82608

82608

82608

82608

0.082 u

0.077 u

0.17 U

0.070 u

o.24U

0.11 U

0.20 u

0.13 U

o.l2 u

0.058 u

0.058 u

0.078 u

0.063 u

0.11 u

0.065 u

210712008 15:51

210712008 15:51

210712008 15:51

210712008 15:51

210712û8 15:51

210112008 15:51

210712008 15:51

210712008 15:51

210712008 15:51,

2/0712008 15:51

210712008 15:51

210712008 15:51

210712008 75:51

210712ffi8 15:51

210'112008 15:51

þEll

pïll

þgll

Fcll

pgll

þgll

tlglI

pgll

pgll

ttgll

ttgll

pgll

pgll

pgll

pgll

Unfiltered

Unfiltered

Unfiitered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Uofiltered

Unfiltered

Unfiltered

Unfiltered

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

*rivell Pu¡ging is the process ofpump¡ng the well prior to sampling in order to obtain a representative groundwater sample

DEP Form 62-522.900(2) Effective April 14, 1994


PAR.AMETER MONITORING REPORT(Rule 62-701.730(2Xb))

Semí-Annml Groundwater Monitoríng lPage 1 of 3l

ILITY WACS# 21251 SAMPLE DATE II29I2OO8

IITORING WELL \¡ÍACS# 190 t8 ANALYSIS DATE 1l3ll2û08 ro2l0'll2Ù08

L NAME MV/-6

JSIFICATION OF GROUNDWATER G.N

Purged* prior tole Collection (Yes/No)

WELL TYPE: CE (BG) Background(DE) Detection(CE) Compliance(OT) Other


ST'OR.ETCODE

PARAMETERl.lÔNITÍìRNr)

SAMPLINGl\rfE,TI¡IIN

ANALYSISMü''ITTrlN

ANALYSIIP[.SIfl T

ANALYSTSn^m/T|.m TJNITS

IÏLTERED/tNf,fr ,lFDf.f

t'¡f"ËÁìt tl'vAIIvtf¿tÀDDEI)

082545

000010

0'00299

000406

000094

082078

000610

000940

000ó20

032730

000945

070300

001 105

00 1002

001027

00 1034

001045

00105 I

071900

000929

'Water Level

Temperature (field)

Dissolved Oxygen (held by probe)

pH (field)


Turbidity (fìeld)

Amonia as N

Chlorides

Nitrate as N

Phenols

Sulfate


MF'-TAf .S

Aluminum

Arsenic

Cadmium

Cbromium

Iron

Lead

Mercury

Sodium

Grab

Grab

Grab

Grab

Grab

Bladder Punp

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

350. r

325.2

353.2

420.1

375.4

160. I

6010

6010

6010

6010

6010

6010

7470

6010

42 89

20.87

J.IJ

7.38

2.98

6.34

0.0046 IV

4.4

0.31

0.025 u

1.3 U

160

33r

4.2U

0.46 U

2.61

12 IV

2.0 u

0.072 u

3.0

1n9t2m8

112912008 16:51

ll29/20f8 16:51

112912008 16:51

112912008 16:51

112912008 16:51

210712088 13:03

l/31/2008 l0:33

210712008 t7:30

2/06/2008 08:01

1/3 1/2008 10:35

2lM/02008 ll:41

210512ffi8 13:11

210512ffi8 13:11

2lO5l20OB 13:11

2105120[8 l3:ll

210512008 13:11

2105120f8 13:ll

2/05/2008 l5:08

210512Cf8 l3:ll

FT NGVD

.C

mglL

STD

¡rmhos/cm

NTUs

nglL

mg/L

mglL

mglL

mglL

mglL

pcll

Pcll

pcll

þcll

ttgll

ttgll

þgll

mo/T

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfilte¡ed

Unfiltered

Unfrlte¡ed

Unfiltered

Unfiltered

Unf¡ltered

Unfiltered

Unfilte¡ed

Unfiltered

Unfiltered

Unfiltered

Unfillered

Unfiltered

None

None

None

None

None

H2S04

None

None

H2S04

None

None

HN03

HN03

HNO3

HN03

HNOs

HNOI

HNO3

T{NÔ.

:rilell Purging is the process of pumping the wll pr¡or to sâmpl¡ng in order to obtain a represenøtive groundwater sample

DEP Fotm 62-522 900(2) Effetive April 14, 1994

VEOLIA CYPRESS ACRES C&D LA¡IDFILL


Semi-Annrr¡l Groundwafer Monitoring lPage 2 of 3ì

FACILITY WACS# ZIZ5I SAMPLE DATE II29I2OO8

MONITORING WELL WACS# 19018 ANALYSIS DATE 1131t2008to210712008

WELL NAME MW-6 WELL TYPE: CE (BG) Backeround(DE) Detection(CE) Compliance(oT) othe¡

Well Purged* prior toSample Collection (Yes/No) Groundwater Elevation INGVD) 40.58


STORETñôfìú' PARAMETER MONITOR-ED

SAMPLINGMETHOD

ANALYSISMnTt{ôn

ANALYSI¡PF'.SITI T

ANALYSISÍì Ä TE'/TIÀIF TJNITS

FILTERED/IJNI¡ILTEREI

r'¡(öùt,|l'vatlvI,iADDEI)

032101

032t04

0344t3

032\02

034301

0343 I I

034576

032 106

034418

032105

034536

034566

0345'7 |

034668

034496

03453 r

034501

077093

034546

n?45¿1


Bromoform

Bromomethane

Carbon Tetrachloride

Cblorobenzene

Chloroethane


Chloroform

Chloromethane



I ,3-Dichlorobenzene

1,4-Dichloroberzene


l, l-Dichloroethane

I ,2-Dichloroethane

I ,1-Dichloroethene



1 )-lli¡hlnrnn¡nn¡np

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

iRbdder Èrmn I

82608

82ó08

82ó0B

82608

8260B

82608

8260B

8260B

82608

82608

82608

82608

82608

82608

82608

82ó08

82608

8260B

82608

R260R

0.10 u

0.13 u

0.17 u

0.078 u

0.079 u

0.ll u

I.2 UJ

0.056 u

0.080 u

0.080 u

0.076 u

0.082 u

0.14 U

0.075 u

0.067 u

0.082 u

0.11 u

0.18 u

0.25 U

0.10 u

210712008 16:20

210712008 16:20

210'112008 t6:20

210712008 16:20

210712008 16:20

2l07l2NB 16:20

210712008 16:20

2lO7l2N8 16:20

2lO7l20O8 16:20

210712008 16:20

UO7|2A08 16:20

2/0712008 16:20

210712008 16:20

2107120f8 16:20

2/0712008 16:20

210712008 16:20

þgll

pçll

pgll

þEll

pgll

þgll

pcll

pcll

ttgll

pgll

ttgll

pgll

pcll

pcll

þEIT

þcll

pgll

pgll

ttcll

Unfil¡ered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unhltered

Unfiltered

Unfilte¡ed

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfil¡ered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

I Tnfilta¡p¡l

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCt_

ÌWell Purging ¡s the process of pumping the El¡ prior to sâmpl¡ng in order to obtain a representative groundwter sample.

DEP Form 62-522.900(2) Effætive April 14, 1994


PARAMETER MONITORING REFORT(Rule 62-701.730(2)(b))

Semi-Annml Grounrlwater Moniloring lPage 3 of 3l


MONITORING V/ELL WACS# 19018

V/ELL NAME MW-6

CLASSIFICATION OFGROUNDWATER G-N


SAMPLE DATE 1IZ9I2OO8

ANALYSIS DATE ll3llzffi9 to 210712008

TilELL TYPE: q-(BG) Background


(DE) Detection(CE) Compliance(OT) Other

40.58

STORETCODE PARAMETER MONITOREI)

SAMPLINGMÍ'TITôIì

ANALYSISME'nt¡ôn

ANALYSIfRESTrI,7

ANALYSISDATT/TIME UNITS

FILTERED/l TMDDT

PRESERYATIVEIADDED

034'tu

034699

034423

034516

034475

034506

0345 I I

039180

034488

039175

034030

034371

034010

034020

ug91


trans-1,3-Dichloropropene

Methylene Chloride


Tefrachloroethene

l, l, l-Trichloroethane

l, 1,2-Trichloroethane

T¡ichloroethene

Trichlo rofl uoromethane

Vinyl Chloride

Benzene

EthylbeMene

Toluene

Xylenes

Methyl Tert-Butyl Ether

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

82608

82ó0B

82608

82608

8260B

82608

82608

82608

82608

82608

82ó08

82608

82608

82608

82608

0.082 u

0.077 u

0.17 u

0.070 u

0.24 U

0.11 U

020u

0.13 u

0.12 u

0.058 u

0.058 u

0.078 u

0.063 u

0.11 U

0.065 u

210712008 16:20

2107120f8 t6:20

2107l2NB 16:20

2t0712008 16:20

2107120f8 16:20

210712008 16:20

2107/2008 16:20

2107l2NB 16:20

210'7|2OOB 16:20

2/07 12008 16:20

210712008 16:20

210712008 16:20

210712008 t6:20

2107120[8 16:20

210712008 16:2O

Pgll

pgll

pgll

pcll

pgll

þgll

ttgll

ttgl'l

pcll

ttgll

pgll

pgll

pgll

FCII

p9ll

Unfil¡ered

Unfilte¡ed

Unfiltered

Unfìltered

Unfilrered

Unfiltered

Unfiltered

Unfiltered

Unfilte¡ed

Unfil¡ered

Unfiltered

Unfiltered

Unfillered

Unfiltered

Unfillered

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

*Well Purging is the process ofpump¡ng the well prior to sampling in order to obtain â representâtive groundwater sample

DEP Form 62-522.900(2) Effective April 14, 1994



Semi-Annul Grorndwater Mon¡toring lPâge I of 3l

FACILITY WACS# 21251 SAMPLE DATE \Izglzffil

MONITORING V/ELL WACS# 19019 ANALYSIS DATE l/31/2008 ro 2/07/2008

WELL NAME MV/-7 TüELL TYPE: L(BG) Background

CLASSIFICATION OF GROUNDV/ATER G-II(DE) Detection(CE) Compliance(OT) Other

Well Purgedr prior toSample Collection (Yes/No) Groundwater Elevation (NGVD)Yes 40.&

STORETCODE

PARÂMETTRMôNITôPÍ'TI

SAMPLINGMETIIOD

AITALYSISMETIIOD

ANALYSISRÍ'sIN.T

.ANALYSISDATT/TIIIIE TJNITS

}-ILTERED/lwMDEI

PRF.SERVATIVEIADDED

082545

000010

0'00299

000406

000094

082078

000610

000940

000620

032730

000945

070300

001 105

001002

001027

001034

001045

001051

071900

w0929

'Water Level

Temperarure (field)

Dissolved Oxygen ltield by probe)

pH (field)

Spec. Conductance (fi eld)

Turbidiry (field)

Amonia as N

Chlorides

Nitråte as N

Phenols

Sulfate


METAI.S

Aluminum

Arsenic

Cadmium

Chromium

Iron

Lead

Mercury

Sodium

G¡ab

Grab

Grab

Grab

Grab

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump ]

I

Bladder Pumo I

350 I

325.2

J)J.Z

420.1

375.4

160. I

6010

6010

6010

6010

6010

6010

't470

6010

4'1.66

21.&

2.t4

7.22

9.84

0,0052 IV

5.6

0.42

0.025 u

l3u210

52r

4.2 U

0.46 U

1.9 I

3l rv

2.0u

0.072 u

J.)

u29/2008

112912008 ll:49

ll29l2Ñ8 ll:49

'l/2912008 1l:49

112912008 11:49

112912008 ll:49

2107l20OB 12:53

I /3 1/2008 10:33

210712008 17:30

a06t2m8 080t

u31t2æ8 tO16

210412008 ll:47

210512008 12:52

210512008 12:52

210512008 12:52

FT NGVD

'cmglL

STD

¡rmhos/cm

NTUs

mg/L

mglL

mg/L

mg/L

mg/L

mg/L

Unfiltered

Unfiltered

Unfiltered

Unfil¡ered

Unfiltered

Unfilte¡ed

Unfiltered

Unfiltered

Unhlte¡ed

Unfiltered

Unfilrered

Unfilte¡ed

Unfiltered

Unfiltered

Unfilte¡ed

Unfiltered

Unfiltered

Unfiltered

ITnfiltere¿l

None

None

None

None

None

H2SOa

None

None

H2S04

None

None

HN03

HN03

HN03

HNO3

HNOs

HNO3

HN03

HNO.

*Well Purging is the præess of pumping lhe we¡l pr¡or lo sampling in order to obtain å representative groundwaler sampleDEP Fotm 62-522.900(2) Effective April 14. 1994

VEOLIA CYPRESS ACRES C&D LANDFTLL

PARAMETER MONITORING R-EPORT(Rule 62-701.730(2)(b))

Semi-Annrrrl Gmrmdwaler Monitoring lPage 2 of 1ì

ìACILITY WACS# 21251 SAMPLE DATE I/2412007

íONITORING WELL WACS# 19019 ANALYSIS DATE l/31/2008 to 2/07/2008

VELL NAME M\¡/-7 WELL TypE: CE (BG) Background

:LASSIFICATION OF GROUNDI/ATER G-II(DE) Derection(CE) Compliance(OT) Orher

G¡oundwater Elevation (NGVD) 40.64

Vell Purged+ prior toSample Collection (Yes/No)

ù I Ut(¡; ICODE PARAMETER MOMTOREI)

SAMPLINGMETHOD

ANALYSISMnTI{ôn

ANALYSITPE SIII T

ANALYSISDÂTWTIMI" T,INITS

FILTERED/ PRDSERVATIVEIADDED

032101

032104

034413

032102

034301

0343 I I

0345'76

032 106

034418

032 105

034536

034566

034571

034668

034496

03453 I

034501

077093

034546

^al\11


Bromoform

Bromomethane

Carbon Tet¡achloride

Chlorobeuene

Chloroethane

2-Cbloroerhyl vinyl ether

Chloroform

Chloromethane

Dibromochlo¡omethane

I ,2-Dìchlorobemene

I ,3-Dichlorobeuene

I ,4-Dichlorobenzene

Dichl orodifl uo¡omethane

1, 1 -Dichloroethane

1,2-Dichloroerhane

l, l-Dichloroethene

cis-1,2-Dichlo¡oethene

trans- 1,2-Dichloroetbene

1.2-Dichloroorooane

Bladder Pump

Blâdder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

82608

82608

82608

82608

82608

82608

82608

82608

82608

82608

82608

82608

82608

82608

8260B

82608

82608

82608

82608

82608

0.10 u

0.13 U

0.17 u

0.078 u

0.079 u

0.ll u

1.2 U

0056u

0.080 u

0.080 u

0.076 u

0.082 u

0.14 u

0.075 u

0.067 u

0.082 u

0.ll u

0.18 u

0.25 U

0.10 u

210712008 16:49

210712008 16:49

2lO'112008 t6:49

2107 12008 16:49

2107 12008 16:49

2/07 12008 16:49

210712008 16:49

2107l20OB 16:49

210712008 16:49

210712008 16:49

2107l2OO8 16:49

2107120f8 16:49

210712008 t6:49

p9ll

pcll

pgll

Itgll

pgll

Itgll

pgll

Pgll

pgll

pgll

Fcll

Unfiltered

Unfiltered

Unfiltered

Unfilte¡ed

Unfiltered

Unfiltered

Unfilrered

Unfiltered

Unfilte¡ed

Unfiltered

Unfiltered

Unfiltered

Unfille¡ed

Unfiltered

Unñltered

Unfìltered

Unfiltered

Unfilte¡ed

Unfiltered

T Infiltercd

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

Hl-I

*Well Purging is the præess of pumping lhe well prior to sampling ¡n order to obtåin â representat¡ve groundwater sâmpl€DEP Fotm 62-522 900(2) Effect¡ve April 14, 1994

VEOLIA CYPRESS ACRES C&D LAIIDF]LL


Semi-Annul Grorrndwater Monitoring lPage 3 of 1l

FACILITY V/ACS# 21251 SAMPLE DATE II29I2OO8

MONITORING !ù/ELL WACS# 19019 ANALYSIS DATE lt31l2mï ß2t07t2|f,B

WELL NAME MW-7 WELL TYPE: L(BG)Background3LASSIFICATION OF GROUNDWATER G-N

(DE) Detection(CE) Compliance(OT) Other

Well Purged+ prior toSample Collection (Yes/No) G¡oundwater Elevation (NGVD) 40&

STORETl-fltì[' PARÂMETER MONITORED

SAMPLINGMETIIOD

ANALYSISÑfF'.TI¡'ìN

ANALYSI!Pü'SI II -T

ANALYSISDATE/TIME TJNITS

I-ILTEß.ED/WMDEÍ

PRESERYATIVFIADDED

034704

034699

034423

03451ó

034475

034506

03451 1

039f80

034488

039 175

034030

034371

034010

034020



Methylene Chloride


Tetrachloroethene

l, l, 1-Trichìo¡oerhane

l, 1,2-Trichloroethane

Trichloroethene

T richlorofl uo rome¡hane

Vinyl Chloride

Benzene

Ethylbenzene

Toluene

Xylenes

Methyl Tert-Butyl Ether

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

82608

82608

82608

82608

82608

82608

82608

82608

82608

82608

82608

8260B

82ûB

82608

82608

0.082 u

0.077 u

0.17 u

0.070 u

0.24 U

0.ll u

0.20 u

0.13 U

0.12 u

0058u

0.058 u

0.078 u

0.063 u

0.ll u

0.065 u

210712008 16:49

210112008 16:49

210712008 16:49

2107l2NB 16:49

210712008 16:49

210712008 16:49

210712008 t6:49

210712008 t6:49

2107120[8 t6:49

2101120f8 16:49

210112008 16:49

210712008 16:49

21071200816:49

2107 12008 16:49

2107l20OB 16:49

pgll

pcll

Fcll

ttgll

þgll

þgll

pgll

pgll

pgll

p}ll

Fcll

pcll

pgll

Itgll

ttgll

Unfilte¡ed

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfille¡ed

Unfiltered

Unf¡ltered

Unfilte¡ed

Unfiltered

Unfiltered

Unhltered

Unfil¡ered

Unfiltered

Unfiltered

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

.Well Purging is the process of pumping the well prior to sampling in order to obta¡n a represenht¡ve groundMte¡ sample

DEP Foß 62-522 900(2) Effect¡ve Apri¡ 14, 1994


PARAMETER MONITORING REFORT(Rute 62-701.730(2Xb))

Semi-Ànnu¡l Groundweter Monitoring (Page I of 3l


MONITORING V/ELL WACS# I9O2O

YELL NAME MV/-8


\ryell Purged* prior toSample Collection (Yes/No)


ANALYSIS DATE I/3V2M810 2IO7I2M8

WELL TYPE: CE (BG) Background(DE) Derecrion(CE) Compliance(OT) Other

Groundwater Elevation (NGVD) 40.76

STORETCODE

PARÀMETERMONITORED

SAMPLINGMETHOD

ANALYSISll,lN.TTIôIì

ANALYSI!RDSTIT;T

ANALYSISDATF"/TIMT: TJNITS

rILTERED/ITNTrr.TNNNT

PRESERVATryESADDNÍ)

082545

0000r 0

0'00299

000406

0m094

082078

0006r0

000940

000620

032730

000945

070300

001 105

001002

00t027

001034

001045

00105 I

071900

071900

0æ929

Chlorides

Nitrate as N

Phenols

Sulfate

Total Dìssolved Solids

MÍ'.TÂI,S

Aluminum

Arsenic

Cadmium

Chromium

Iron

Lead

Mercury

Mercury

Sodium

G¡ab

G¡ab

Grab

Grab

Grab

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

350. I

325 2

353.2

420 I

375.4

r60. I

6010

6010

6010

6010

6010

6010

7470

7470

6010

44.86

23,2

0.45

4.83

t26

0.95

0.12 IV

8.6

2.9

0.025 u

t2

)v

90 I

4.2 U

0.46 U

1.5 U

8.9 IV

20u

3.3

2.9

8.1

I

v30t2008

l130/2008 14:40

113012408 14:40

113012008 l4:40

113012008 14:4O

113012008 14:40

2/0712008 13:05

1l3ll20f8 19:12

2t07/2008 17:30

2/06/2008 08:01

2/06/2008 08:01

210412008 ll:48

210512008 17:04

210512008 l7:04

FT NGVD

"c

mglL

STD

¡¡mhos/cm

NTUs

mg/L

mglL

mglL

mg/L

mg/L

mglL

ttgll

Unfilte¡ed

Unfiltered

Unfiltered

Unfiltered

Unfrltered

Unfiltered

Unfìltered

Unfilte¡ed

Unhltered

Unfiltered

Unfiltered

Unhltered

Unfillered

Unhltered

Unfrltered

Unfiltered

Unfiltered

Unfilte¡ed

Filtered

Unfilte¡ed

None

None

None

None

None

HzSO¡

None

None

HzSQ

None

None

HN03

HN03

HN03

HNO3

HN03

HNOI

HNO3

HNOs

HNO.

*Well Purging ¡s lhe process of pumping the well prior to sampling in order to obtain a represenEt¡ve groundwater sample

DEP Fotñ 62-522.900(2) Effective April 14, 1994


ì4ONTTORTNG WELL WACS# tn20

WELL NAME MV/-8

CLASSIFICATION OF GROUNDWATER G.II

VEOLIA CYPR-ESS ACRES C&D LANDFILL

PARAMETER MONITORING REPORT(Rule 62-701.730(2Xb))

Semi-Annuql Groundweter Monitoring (Page 2 of 3ì

Yes


ANALYSIS DATE I/3II2OO8TO2IO1I2OO8



(DE) Detection(CE) Compliance(OT) Orber

40.76

Well Purged* prior toSample Collecrion (Yes/No)

sl oRI4'fCODE PARAMETER MONITOREI)

SAMPLINGMETTIOD

ANALYSISMETHOD

ANALYSI!NN,SIfI T

ANALYSISDATE/TIME IJNITS

FILTERED/ PRESERVATIVEIÄ nnÍ,rì

032101

032104

034413

032102

034301

0343 I I

034576

032 106

034418

032 105

034536

034566

034571

034668

034496

03453 1

034501

077093

034546

ô1áS¿ 1


Bromoform

Bromomethane

Carbon Tet¡achloride

Chlorobeuene

Chlo¡oethane


Chlo¡oform

Chloromethane


1 ,2-Dichlorobeuene

I ,3-Dichlorobeuene

I ,4-Dichlorobeüene

Dichlo¡odifl uoromethane

I, I-Dichloroethane

1,2-Dichloroerhane

1,1-Dichloroethene

cis- 1,2-Dichloroethene

trans- 1,2-Dichloroethene

I .2-Dichloroorooane

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Btadder Pump

Bladder Pump

Bladder Pump

82608

82ûB

82608

82608

82608

82608

82608

82608

8260B

82608

82608

82608

82608

82608

82608

82608

82608

82608

82608

ctÁrìp

0 t0u

0.13 u

0.17 u

0.078 u

0.079 u

O.il u

t.2u

0.056 u

0.080 u

0.080 u

0076u

0082u

0.14 U

0.075 u

0.067 u

0.082 u

0.11 U

0.18 U

0.25 U

0.10 u

2107 12008 l'l:18

210712008 17:18

210712008 17:18

210712008 17:tB

2lO7 12008 t7:18

2107 12008 17:18

210712008 l7:18

2/0712008 17:18

210712008 17:18

210712C08 17:18

2107l20OB 17:18

2107 12008 t7:r8

2lO7 /2008 17:18

2107120f8 17:18

pgll

þgll

ItBll

pg/l

þcll

pcll

pcll

pgll

tlgll

ttgll

p+ll

Itgll

Fc/l

pcll

pell

ttgll

ttgll

ttgll

pgll

Unfilte¡ed

Unfiltered

Unfìltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfilte¡ed

Unfil¡ered

Unfilrered

Unfiltered

Unfiltered

Unfilte¡ed

Unfiltered

Unñltered

Unfiltered

Unfiltered

Unfiltered

I InfilterPri

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HCL

HI-I

*Well Purging is the process ofpumping the well prior to s¿mpling in order to obta¡n â representat¡ve groundwaler sâhpleDEP Form ó2-522.900(2) Effætive Apr¡l 14, 1994

VEOLIA CYPRESS ACRES C&D LANDTTLL

PARAMETER MONITORING REFORT(Rule 62-701.730(2Xb))

Semi-Annuql Groundwete¡ Monitorin&lP¡ge 3 of 3ì

FACILITY WACS# 2I25I SAMPLE DATE 7I25I2OO7

MONITORING Iù/ELL WACS# 19020 ANALYSIS DATE I/31/2008 TO 2/07/2008

WELL NAME MW-8 !ilELL TypE: CE (BG) Background

]LASSIFICATION OF GROUNDWATER G.II(DE) Detecrion(CE) Compliance(OT) Orher


fy'ell Purged* prior toSample Collection (Yes/No)

STORETcônF. PARAMETER MONITORED

SAMPLINGIl/ltr'.TT¡ÕN

ANALYSISME lfrrìn

ANALYSIIRESTJLT

ANA¡rf ¡t.tù

DATE/TIME TJNITSFILTERED/

f tNü'r¡.Tr.DÍ'rPRtrSERVATTVET

ADDF"II

034704

034699

034423

0345 16

034475

034506

0345 I I

039180

034488

039175

034030

034371

034010

034020

04&91



Methylene Chloride

I , I ,2,2-Tetrachloroerhane

Tetrachloroethene

l, l, l-Trichloroethane

I , I ,2-Trichloroethane

Trichloroethene


Vinyl Chloride

Benz ene

EthylbeEene

ToÌuene

Xylenes

Methyl Terr-Buryl Erher

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

Bladder Pump

82608

82608

82608

8260B

8260B

82608

82608

82608

82608

82608

82608

8260B

82608

82608

8260B

0.082 u

0.077 u

0.17 u

0.070 u

0.24 U

0.11 u

0.20 u

0.13 u

0.12 u

0.058 u

0.62 |

0.078 u

0.063 u

0.ll u

0.065 u

210712008 17:18

210'll20OB 17:18

2/0712008 17:18

A07DA08 17:18

2107120f8 17:18

210712008 17:18

210712008 17:18

2107/2008 l'l:18

2107 l2OO8 17:18

2lO7|2OOB 17:18

210'112008 17:18

210712008 17:18

2lO7l2O08 t7:18

210112M8 17:t8

210712008 17:18

pgll

Pgll

pgll

pgll

Fcll

pgll

þgll

pgll

ttgll

þcll

pgll

pgll

pgll

Fcll

pcll

Unfiltered

Unfiltered

Unfìltered

Unfiltered

Unfilte¡ed

Unfilte¡ed

Unfiltered

Unfil¡ered

Unfiltered

Unfiltered

Unfiltered

Unfilte¡ed

Unfiltered

Unñltered

Unfitte¡ed

HCL

HCL

HCL

HCL

HCL

tIU L

HCL

HCL

HCL

HCL

HCL

HCL

¡tUL

HCL

HCL

tWell Purging ¡s the Process of pumping the well prior to sampling ¡n order to obtain a representat¡ve groundw¡ter sample

DEP Fotm 62-522.900(2) Effæ!¡ve Apr¡l 14. 1994

I VEOLIACYPRESSACRESC&DLANDFILLI

PARAMETER MONITORING REFORT(Rule 62-701,730(2Xb))

Semi-Annu¡l Grounrlweter Monitoring lPage I of lì

FACILITY WACS# 2I25I SAMPLE DATE 1/30/2008

MONITORING WELL WACS# ANALYSIS DATE 2t0512008 ro 0Zß5næ8

V/ELL NAME MW-8R TilELL TYPE: OT (BG) Background

CLASSIFICATION OF GROUNDWATER G-II(DE) Detection(CE) Compliance(OT) Other

G¡oundwater Elevation (NGVD) 40.80Yes


STORETCODE

PÄRAMETERMOMTORED

SAMPLINGMü'Tl¡ôN

ANALYSISMÍ'îI¡fìN

ANALYSI!RF^SI,JLT

AIlALTÙIDDATE/TIME IINITS

FILTERED/ PRESERVATIVEIADDÍ]I)

082545

000010

0'00299

000406

000094

082078

07r900

071900

\ry'ater Level

Temperature (field)

Dissolved Oxygen (field by probe)

pH (field)


Turbidity (field)

MFTÀT,S

Mercury

Mcrnrrrv

Grab

Grab

Grab

Grab

Grab

Bladder Pump

Bladder Pumo

7470

7470

43.11

230

0.34

4.94

109

1.4

5.5

5.0

U30t2008

I l3Ol2OO8 15:45

1/30/2008 15:45

l13012008 15:45

l13012008 15:45

113012008 t5:45

2/0512008 15:19

2/05/2408 t5:21

FT NGVD

"C

mglL

STD

¡mhos/cm

NTUs

t/gll

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Unfiltered

Filtered

None

None

None

None

None

HNOs

HNO¡

*Well Purging is the process of pumping the well prior to sampl¡ng in o¡der to obtain a represenbtive groundmter sample

DEP Form ó2-522.900(2) Effætive April 14. 1994

VEOLIA CYPRESS ACRES C&D LANDTILL


Semi-Ànnrrl Gronndwater Monitoring lpage I of lì

]ILITY WACS# 2I25I SAMPLE DATE 2/06/2008

NITORTNGIVELLWACS# ANALYIISDATE 2t15l2008TO 2n5t2008

WELL TYPE: OT (BG) Background

\SSIFICATION OF GROUNDWATER G.II(DE) Derecrion(CE) Compliance(OT) Orher

G¡oundwater Etevarion (NGVD) 40.61

I Purgedx prior tople Collection (Yes/No) Yes

STORETlìñnF

PARAMETERMONITORED

SAMPLINGMETTIOD

ANALYSISMETIIOD

ANALYSITREST]LT

ANALYSISDAT'E/TIME TJNITS

FTLTERED/ rxüùt ¡f'Y¡¡lllv¡tADDED

082545

000010

0'00299

000406

000094

082078

071900

071900

Wate¡ Level

Temperanrre (field)

Dissolved Oxygen 1field by probe)

pH (fietd)


Turbidity (fìeld)

METÂT.S

Mercury

Mercurv

G¡ab

Grab

Grab

Grab

Grab

Bladder Pump

Bladder Pumn

7470

7470

42.55

24.9

2.19

10.87

773

40.2

0.72 U

0.72 U

2t6t2008

2l6l2N8 14:56

216l2NB 14:56

21612OO8 14:56

21612008 14:56

21612008 t4:56

2115/2008 14:43

211512008 14:45

FT NGVD

"c

mglL

STD

irmhos/cm

NTUs

p\ll

Unfilrered

Unfiltered

Unfiltered

Unfiltered

Unfilrered

Unfiltered

Filtered

None

None

None

None

None

HNOI

HNO.

¡we¡l Purging is the process of pumping the well prior to sampling in order to obh¡n a representrtive groundqrer sampleDEP Form 62-522.900(2) Effect¡ve Apr¡t 14. 1994

APPENDIX F

DER Form 62-522.900Q)

ATTACHMENT F

Florida Department of Environmental Protection3319 Maguire Boulevard, Suite 232, Orlando, Florida 32803-3767

GROUND WATER MONITORING REPORTRule 62-522.600(11)

PART I GENERAL INFORMATION

(1) Facility Name: Superior Cypress Acres C&D Landfill

Address: 7424 NE 33'o Court

City Ocala

Telephone Number: (352) 351-8886

WACS_Facilily: 21251

DEP Permit Number: SO-420019903-006

Zip 34479 County: Marion

E-mail address: Jeffrev. [email protected]

(2)

(3)

(4) Authorized Representative's Name: Jeff lnglehart Title

Address 5111 South Pine Avenue. Suite M

Site Manaoer

City

Telephone Number (352) 351-B886

Zip 34480 County: Marion

E-mail address : Jeffrev. [email protected]

Type of Discharge: None(5)

(6) Method of Discharge: N/A

CERTIFICATION

I certify under penalty of law that I have personally examined and am familiar with the information submitted in thisdocument and all attachments and that, based on my inquiry of those individuals immediately responsible for obtainingthe information, I believe that the information is.true, accurate, and complete. I am aware that there are significantpenalties for submission of false information incl of fìne and imprisonment.

-"?ol ttlosRepresentative's Signatu re

PART II QUALITY ASSURANCE REOUIREMENTS

Sampling Organization Comp QAP #: FDEP-SOP-001/01

Analytical Lab Comp QAP #/ HRS Certification: ES81005

Lab Name: TestAmerica Laboratories

Address: 2846 lndustrialPlaza Drive. Tallahasse. FL 32301

Phone Number: (850)878-3994

E-mail Address [email protected]

DER Form 62-522.900(2)Effective April 14, .1994

fgolder - florida department of environmental protection

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