1517/7 - united states environmental protection agency · 2020. 12. 13. · e4711 station 2 - 1058...

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1517/7

Bridgeport Environmental Inc. uc«.ed A» yuc.i________________________________________________________________# 08555P.O. Box 247 609/467-0380510 Heron Drive Suite 107Bridgeport, NJ 08014-0247

WESTON

PROJECT: METRO CONTAINER

DATE RECEIVED: August 24, 1990

REPORT NO: E4696 - E4730

BRIDGEPORT ENVIRONMENTAL, INC.

RICHARD V. LYNCHLABORATORY MANAGER

SAMPLE LOCATION AMD IDENTIFICATION

ANALYSIS NO CLIENT ID

E4696 Station 1 - 1027E4697 Station 2 - 1045E4698 Station 3 - 1118E4699 Station 4 - 1208E4700 Station 5 - 1120E4701 Station 6 - 1208E4702 Station 7 - 1259E4703 Station 1 - 103(5 ' _E4704 Station 2 - 1047 "flE4705 Station 3 - 1122E4706 Station 4 - 1208E4707 Station 5-1124E4708 Station 6 - 1206E4709 Station 7 - 1300E4710 Station 1 - 1035E4711 Station 2 - 1058E4712 Station 3 - 1133E4713 Station 4 - 1215E4714 Station 5 - 1210E4715 Station 6 - 1215 cnE4716 Station 7 - 1303 _E4717 Station 1 - 1031 "**£*E4718 Station 2 - 1049 V°*E4719 Station 3 - 1127E4720 Station 4 - 1218E4721 Station 5 - 1125E4722 Station 6 - 1218E4723 Station 7 - 1301_E4724 Station 1 - 1036E4725 Station 2 - 1055E4726 Station 3-1134E4727 Station 4-1156E4728 Station 5-1157E4729 Station 6-1156E4730 Station 7 - 1303

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LABORATORY CHRONICLE

RECEIPT/REFRIGERATION________________8/24/90________

ORGANICSEXTRACTION

1. Acids 8/27/90-8/28/90

2. Base/Neutrals 8/27/90 - 8/28/90

3. Festlcides/PCB's/Herbicldes 8/27/90

4. Petroleum Hydrocarbons ______HA___________

ANALYSIS

1. Volatiles 8/27/90 - 8/30/90

2. Acids 9/7/90 - 9/11/90

3. Base/Neutrals 9/7/90 - 9/11/90

4. Pestlcides/PCB's/Herbicides 9/6/90 - 9/11/90

5. Petroleum Hydrocarbons _______^__________

6. Total Organic Carbon__________5^__________

Section SupervisorReview & Approval

INORGANICS

1. Metals__ 8/27/90 - 8/30/90

2. Cyanides,

3. Phenols

OTHER ANALTTES

es 8/28/90

s KA

Section SupervisorRevlev & Approval

Quality Control Supervisor O. iReview & Approval______________W COL -

If fractions are re-extracted and re-analyzed because initial endeavorsdid not neet quality control acceptance criteria, Include dates for *><tf • n n n n o

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METHODOLOGY SUMMARY

PURGEABLES U.S.E.P.A. Method 624 - This Is a purge andtrap Gas Chromatograph/Mass Spectrometer (GC/MS)method applicable to the determination of thecompounds listed in the U.S.E.P.A. Manualentitled " Test Procedures for the Analysis ofOrganic Pollutants'1.

An HP5996 GC/MS was used with a capillary column.

Method detection limits are as stated.

Soil samples are prepared for analysis as prescribedin Method 8240 from SWS46.

ACID EXTRACTABLESBASE NEUTRALS U.S.E.P.A. Method 625 - This method covers

the determination of a number of organic compoundsthat are partitioned in an organic solvent andamenable to gas chromatography. This is a gaschroma tography /mass spectrometer (GC/MS) methodapplicable to the determination of the compoundslisted In the U.S.E.P.A. Manual entitled "TestProcedures for the Analysis of Organic Pollutants".

A HP5970 was used with a DB-5 FSCC.

Method detection limits are as stated.

Soil samples were prepared for analysis asprescribed In Method 3550 from SW846.

PESTICIDES/PCB's U.S.E.P.A. Method 608 - This method covers thedetermination of pesticides and PCB's in samplesby ex tract Ion/concent ract ion with organic solventsand subsequent qualification/ quantification byGas Chromatography. The gas chromatograph utilizesan electron capture detector (ECD) which isapplicable for the determination of the compounds listedfor this method in the U.S.E.P.A. Manual entitle"Test Procedures for the Analysis of Organic Pollutants".

Soil samples were prepared as prescribed in Method3550 from SU846.

ARIOOOOlf

METHODOLOGY SUMMARY

METALS Soil Samples for metal analysis were run inaccording with the methods prescribed in SW846.This includes a nitric acid digestion followedby either Furnace, Flame Atomic absorption,Flameless Atomic Absorption, or InductivelyCoupled Plasma analysis.

Aqueous samples for metals analysis were runin accordance with the methods prescribed inMethods for Chemical Analysis of Water and Wastes,EPA-600/4-79-020 March 1983.

PHENOLS Analysis performed according to U.S.E.P.A. 420.1(Spectrophotometric, Manual 4AAP with distillation).Phenolic materials react with four (4) Antinoantipyrlneand Potassium Ferricyanide at pH 10. Red coloris read at 510 nm.

oCYANIDE Analysis performed according to U.S.E.P.A. 335.2

(Spectrophotometric with distillation). SampleIs reacted with Chloramine-T to produce Cyanogen,Chloride, CNC1. Red color develops when combinedwith Pyrldine/Barbituric Acid Reagent; which is redat 578 nm.

Soil samples are prepared for anlysis as prescribedin Method 9010 from SW846.

PETROLEUMHYDROCARBONS Aqueous samples were analyzed following Method 4.18.1

as prescribed in Methods for Chemical Analysis ofWater and Wastes, EPA-600/4-79-020 March 1983.

Soil Samples were extracted in accordance with themethods prescribed in Stf-846 and subsequentlyanalyzed as stated above.

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RESULT SUMMARY

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CERTIFICATE OF ANALYSISPRIORITY POLLUTANT

ANALYSIS NO; E 4696

CLIENT ID: Station 1 - 1027

SAMPLE DATE: 8/23/90

METALS HDL (mg/L) RESULT (mg/L)

Antimony 0.005 N"D"

Arsenic 0.005 N-D-

Beryllium 0.01 H-D-

Cadmium 0.01 N-D-

Chromium 0.01 N-D-

Copper 0.01 0-03

Lead 0.05 N-D-

Mercury 0.0005 N-D-

Nickel 0.05 N-D-

Selenium 0.005 N*D-

Silver 0.01 H-D-

Thallium 0.10 K-D-

Zinc 0.01 °-07

Cyanide 0.01 N.D.

RRIOOOIO

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Lab Name : Uastex Ind. of HJ I Sample Number ICase No : N/A I £4703 I

QRGANICS ANALYSIS DATA SHEET »————————*(Page 2)

Senivolatile Compounds

t ~~\Concentration: I Lojj>xnei'iui (Circle One ) GPC Cleanup _ Yes _ NoDate Extracted: 38/27/90 Separatory Funnel Extraction __ YesDate Analyzed: 09/08/90 13:50 Continuous Liquid-Liquid Extraction _ YesConc/Dil Factor: lOOOMmlPercent Koisture: NA

*s**~l\ „ A « f~ ^C.A.S. r ug/ or ug/Kg C.A.S. V. 9 X ug/KgKJumber ^* Tfircle One) Number lurcle One)

109-95-2 Phenol 10.U 83-32-9 Acenaphthene Ifl.U111-44-4 bis(-2-Chloroethyl)Ether 10.U 51-28-5 2,4-Dinitrophenol 50.U95-57-3 2-Chlorophenol 10.U 100-02-7 4-Nitrophenol 50.U541-73-1 1,3-Dichlorobenzene 10.U 132-64-9 Dibenzofuran 10.U106-46-7 1,4-Oichlorobenzene Ifl.U 121-14-2 2,4-Oinitrotoluene 10.U100-51-6 Benzyl Alcohol 10.U 606-20-2 2,6-Dinitrotoluene 10.U95-50-1 1,2-Oichlorobenzene 10.U 84-66-2 Diethylphthalate 10.U95-48-7 2-rtethylphenol Ifl.U 7005-72-3 4-Chlorophenyl-phenlyethar Ifl.U

39638-72-9 bis(2-chloroisopropyl)Ether 10.U 86-73-7 Fluorene 10.U106-44-5 4-Methylphenol 10.U 100-01-6 4-Nitroaniline 5Q.U621-64-7 N-Nitroso-Oi-n-Propylamine 10.U 534-52-1 4,6-Dinitro-2-dethylphenol 50.U67-72-1 Hexachloroethane 10.U 86-30-6 N-Nitrososdiphenylamine (1) 10.U98-95-? Nitrobenzene 10.U 101-55-3 4-Bromophenyl-phenylether 10.U78-59-1 Isophorone 10.U 118-74-1 Hexachlorobenzene 10.U98-75-5 2-Nitrophenol 10.U 87-86-5 Pentachlorophenol 50.U105-67-9 2,4-Dimethylphenol 10.U 85-01-8 Phenanthrene Ifl.U65-85-fl Benzoic Acid 50.U 120-12-7 Anthracene 10.U111-91-1 bis(-2-Chloroethoxy)rtethane 10.U 84-74-2 Di-n-Butylphthalate 10.U120-83-2 2,4-Oichlorophenol 10.U 206-44-0 Fluoranthene Ifl.U120-82-1 1,2,4-Trichlorobenzene 10.U 129-00-0 Pyrene 10.U91-20-3 Naphthalene 10.U 85-68-7 Butylbenzylphthalate 10.U106-47-8 4-Chloroaniline Ifl.U 1-94-1 3,3'-Oichlorobenzidine 20.U87-68-3 Hexachlorobutadtene 10.U 56-55-3 Benzo(a)Anthracene 10.U59-50-7 4-Chloro-3-«ethylphenol Ifl.U 117-81-7 bis(2-Ethylhexyl)Phthalate 3.J91-57-6 2-Methylnaphthalene 10.U 218-01-9 Chrysene 10.U77-47-4 Hexachlorocyclopentadiene 10.U 117-84-0 Oi-n-Octyl Phthalata 3.J88-06-2 2,4,6-Trichlorophenol 10.U 205-99-2 Benzo(b)Fluoranthene 10.U95-95-4 2,4,5-Trichlorophenol 50.U 207-08-9 Benzo(k)Fluoranthene **•91-58-7 2-Chloronaphthalene 10.U 50-32-8 Benzo(a)Pyrene 10.U88-74-4 2-Nitroaniline 50.U 193-39-5 Indeno(l,2,3-cd)Pyrene 10.U131-11-3 Dimethyl Phthalate 10.U 53-70-3 Dibenzo(a,h)Anthracene 10.U208-96-8 Acenaphthytene 10.U 191-24-2 Benzo(g,hli)Perylene 10.U99-09-2 3-Nitroaniline 50.U 92-87-5 Benzidine 20.U

A R i O O O l I(l)-Cannot be separated from diphenylamine

"•-Cannot be separated from Benzo(b)Fluoranthene •

+—————————————... 4

Lab Name : Bridgeport Environmental, Inc. I Sample Number ICase No : N/A I £4703 I

ORGANICS ANALYSIS DATA SHEET +—————————+(Page 3)

Pesticides/PCBs

Concentration: towy Medium ( Circle One ) GPC Cleanup _ YesDate Extracted/Prepared: 8/27/90 Separatory Funnel Extraction j YesDate Analyzed: 9/07/90 Continuous Liquid-Liquid Extraction _ YesConc/Dil Factor: 100«L/5«LPercent Moisture: N/A

C.A.S. Cig/L orNumber ug/Kg

319-84-6 Alpha-BHC. ....... 0.29 U319-87-7 Bata-BHC ........ 0.25 U319-66-8 Delta-BHC. ....... 0.2? U96-89-9 Ganma-BHC (Lindane). . . 0.2? U76-44-8 Keptachlor ....... 0.25 U309-00-2 Aldrin ......... 0.25 U1024-57-3 Heptachlor Epoxide . . . 0.25 U959-98-8 Endosulfan I ...... fl.25 U60-57-1 Dieldrtn ........ 0.25 U72-55-9 4I4'-DDE ........ 0.25 U72-20-8 Endrin ......... 0.25 U

33213-65-9 Endosulfan II. ..... 0.50 U72-54-6 4,4'-DDO ........ 0.50 U

1031-07-6 Endosulfan Sulfate . . . 0.50 U50-29-3 4,4'-DDT ........ 0.50 U72-43-5 nethoxychlor ...... 13 U

7421-93-4 Endrin Aldehyde. .... 0.50 U57-74-9 Chlordane. ....... 13 U

8001-35-2 Toxaphene. ....... 25 U12674-11-2 Arochlor-1016. ..... 13 U11104-28-2 Arochlor-1221. ..... 13 U11141-16-5 Arochlor-1232. ..... 13 U53469-21-9 Arochlor-1242. ..... 13 U12672-29-6 Arochlor-1248. ..... 13 U11097-69-1 Arochlor-1254. ..... 13 U11096-82-5 Arochlor-1260. ..... 13 U

Fort 1 7/85

flRioooia

- 50) UCERTIFICATE OF ANALYSIS .———

PRIORITY POLLUTANT

ANALYSIS NO. E 4710



METALS MDL (mg/kg) RESULT (mg/kg)

Antimony 0.13 N.D.

Arsenic 0.13 1-56

Beryllium 0.25 0-60

Cadmium 0.25 0.87

Chromium 0.25 *8-6

Copper 0.25 3»-8

Lead 1.3 157

Mercury 0.05 0-012

Nickel 2.5 19-*

Selenium 0.13 N'D-

Silver 0.25 N-D-

Thallium 2.5 N-D-

Zinc 0.25 I94

«• . * ~ ~ ** H.UaCyanide 0.10

Lab Name : Bridgeport Environmental, Inc. ! Sample Number iCase No : N/A 1 E4710 I

QRGANICS ANALYSIS DATA SHEET +-———————*(Page 2)

Seaivolatile Compounds

Concentration!^ Uy^lediua (Circle One ) GPC Cleanup _ Yes _ NoDate Extracted: 1/28/90 Separatory Funnel Extraction _ YesDate Analyzed: 09/11/90 20:54 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor: 3DG:lnilPercent Moisture: 32.0 *~~~\.

ug/L (r_uq/Kfl X C.A.S. ug/L(or ug/KgNumber (Circle One! Number (Circle

123-95-2 Phenol 490.U 83-32-9 Acenaphthene 490.U111-44-4 bis(-2-Chloroethyl)Ether 490.U 51-28-5 2,4-Dinitrophenol 2400.U95-57-8 2-Chloropnsnol 490.U 100-02-7 4-Nitrophenol 2400.U541-77-1 1,3-Dichlorobenzene 490.U 132-64-9 Dibenzofuran 490.U106-46-7 1,4-Dichlorobenzene 490.U 121-14-2 2,4-Oinitrotoiuene 490.U100-51-6 Benzyl Alcohol 490.U 606-20-2 2,6-Dinitrotoluene 490.U95-50-1 1,2-Dichlorobenzene 490.U 84-66-2 Diethylphthalate 490.U95-48-7 2-Hethylphenol 490.U 7005 72-3 4-Chlorophenyl-pheniyether 498.U

39638-32-9 bis(2-chloroisopropyl)Ether 490.U 86-73-7 Fluorene 490.U106-44-5 4-nethylphenol 490.U 100-01-6 4-Nitroaniline 2400.U621-64-7 N-Nitroso-Di-n-Propylamine 490.U 534-52-1 4,6-Dinitro-2-nethylphenol 2400.U67-72-1 Hexachloroethane 490.U 86-30-6 N-Nitrososdiphenylamine (1) 490.U

«8-95-3 Nitrobenzene 490.U 101-55-3 4-Bromophenyl-phenylether 490.U78-59-1 Isophorone 490.U 118-74-1 Hexachlorobenzene 490.U38-75-5 2-Nitrcphenol 490.U 87-86-5 Pentachlorophenol 2400.U105-67-9 2,4-Dimethylphenol 490.U 85-01-8 Phcnanthrene 490.U65-85-0 Bsnzoic ftcid 2400.U 120-12-7 Anthracene 490.U111-91-1 bis(-2-Chloroethoxy)nethane 490.U 84-74-2 Di-n-Butylpnthalate 490.U120-83-2 2,4-Dichlorophenol 490.U 206-44-0 Fluoranthene 490.U120-82-1 1,2,4-Trichlorobenzene 490.U 129-flfl-fl Pyrene 490.U91-20-3 Naphthalene 490.U 85-68-7 Butylbenzylphthalate 490.U

106-47-8 4-Chloroaniline 490.U 1-94-1 3,3'-Dichlorobenzidine 970.U97-68-3 Hexachlorobutadiene 490.U 56-55-3 Benzo(a)Anthracane 490.U59-50-7 4-Chloro-3-Methylphenol 49fl,U 117-81-7 bis(2-Ethylhexyl)Phthalate 390.J91-57-6 2-Kethylnaphthalene 490.U 218-01-9 Chrysene 490.U77-47-4 Hexachlorocyclopentadiene 490.U 117-84-0 Di-n-Octyl Phthalate 490.U88-06-2 2,4,6-Trichlorophenol 490.U 205-99-2 Benzo(b)Fluoranthene 64.J95-95-4 2,4,5-Trichlorophenol 24110.U 207-08-9 Benzo(k)Fluoranthene ••»•91-58-7 2-Chloronaphtha!ene 490.U 50-32-8 Benzo(a)Pyrene 73.388-74-4 2-Nitroaniline 2400.U 193-39-5 !ndeno(l,2,3-cd)Pyrene 490.U

131-11-3 Dimethyl Phthalate 490.U 53-70-3 Dibenzo(a,h)Anthr8cene 49Q.U2DB-96-8 Acenaphthyiene 490.U 191-24-2 8enzo(g,h,i)Peryiene 490.U99-09-2 3-Nitroaniline 2400.U 92-87-5 Benzidine 970,U

(l)-Cannot be separated fron diphenylamine AR I UUU I 4

"•-Cannot be separated from Genzo(b)Fluoranthene

t..._4.— -.,._-___*

Lab Name : Bridgeport Environmental, Inc. I Sample Number ICase No : N/A I E4710 I

ORGANICS ANALYSIS DATA SHEET *- ———————— *(Page?)

Pesticides/PCBs

Concentration: Uu .) (ledius ( Circle One ) GPC Cleanup _ Yes ± NoDate Extracted/Prepered: 8/27/90 Separatory Funnel Extraction _ YesDate Analyzed: 9/10/90 Continuous Liquid-Liquid Extraction _ YesConc/Dil Factor: I0.02g/10nlsPercent Moisture: 32.0

C.A.S. ug/L orNu»ber >.ug/Kg ,;

319-84-6 Alpha-BHC. ....... 5.0 U319-87-7 Bet«-BHC ........ 5.0 U319-86-8 Delta-BHC. ....... 5.0 U58-69-9 Gaona-aHC (Lindane). . . 5.0 U76-44-8 Heptachlor ....... 5.0 U309-00-2 Aldrin ......... 5.0 U1024-57-3 Heptachlor Epoxide ... 5,0 U959-98-8 Endosulfan I ...... 5.0 U60-57-1 Dietdrin ........ 1072-55-9 4,4'-ODE ........ 1272-20-8 Endrin ......... 5.0 U

33213-65-9 Endosulfan II. ..... 10.0 U72-54-8 4,4t-OOD ........ 62

1031-07-8 Endosulfan Sulfate . . . 10.0 U50-29-3 V-DDT ........ 5072-43-5 Hethoxychior ...... 250 U


8001-35-2 Toxaphene. ....... 500 U12674-11-2 Arochlor-1016. ..... 250 U11104-28-2 Arochlor-1221. ..... 250 U11141-16-5 Arochlor-1232. ..... 250 U53469-21-9 Aroch lor- 1242. ..... 250 U12672-29-6 Aroch lor-1248. ..... 250 U11097-69-1 Arochlor-1254. ..... 250 U11096-82-5 Arochlor-1260. ..... 250 U

For* 1 7/85

AR100015

I -/03J1 Sample Number i

_0rgames Analysis Data Sheet I E4717 1(Pege 1) »—•————-——+

Laboratory Name: Bridgeport Environmental. Inc. Case No.: N/ALab Sample ID: >B9403::D2 ~ QC Report No.:Sample tlatrix: HATER /O i) • A Contract No.: N/AData release Authorized by: f rS uJr fl ^j \\*m+*S Date Samole Received:24 AUG 90

Uolatile CoopoundsConcentration: . Low/ Medium (Circle One )Date Extracted:Date Analyzed: 08/27/90 18:38Cone/Oil factor: I pH :Percent Jfcusture: ^ ^

C.A.S. (ug/J or ug/kg C.A.S. (ug/yor ug/kgNumber (Circle One) Number (TTfcle One)

74-87-5 Chloromethane 10. U 78-87-5 1,2-Dichloroprooane 5. U74-85-9 Bromomethane 10. U 10061-02-6 Trans-l,3-0ichloroprcpene 5. U75-01-4 Uinyi Chloride 10. U 79-01-6 Trichloroethene ' 5. U75-00-5 Chloroethane 10. U 124-48-1 Dibromochloromethane 5. U75-09-2 Hethylene Chloride 3. J.S 79-00-5 1,1.2-Trichloroethane 5. U67-64-1 Acetone 10. U 71-43-2 Benzene 5. U107-02-8 Acrolein 50. U 10061-01-5 cis-l,3-Dichloropropene 5. U167-13-1 Acrylonitrile 50. U 110-75-8 2-Chloroethylvinylether 10. U75-15-0 Carbon Disulfide 10. U 75-25-2 Browform ' 5. U

( . 75-35-4 1,1-Dichloroethene 5. U 108-10-1 4-Hethyl-2-Pentanone 10. U^ 75-34-3 1,1-Dichloroethane 5. U 591-78-6 2-Hexanone 10. U

156-60-5 Trans-l,2-Dichiotoethene 5. U 127-18-4 Tetrachloroethene 5. U67-66-3 Chloroform 5. U 79-34-5 1,1,2,2-Tetrachloroethane 5. U107-06-2 1,2-Dichloroethane 5. U 108-88-3 Toluene 5. U78-93-5 2-Butanone 10. U 108-90-7 Chlorobenzene 5. U71-55-6 i.l.l-Trichlcroethane 5. U 100-41-4 Ethylbenzene 5. U56-23-6 Carbon Tetrachloride 5, U 100-42-5 Styrene 5. U108-05-4 'Jinyl Acetate 10. U Total Xylenes 5. 'J75-27-4 Bromodichlorometnanfl 5. U Total Dichlorobenzenes 5. U

Data Reporting QualifiersFor reporting results to EPA the following results qualifiers are used. Additional flags or footnotesexplaining results are encouraged. However the definition of each flag must be explicit.

Value - If the result is a value greater than or equal to C - This flag applies to pesticide parameters wherethe detection limit, report the value. the identification has been confirmed by GC/MS.

U - Indicates compound was analyzed for but not detected. Single component pesticides >• 10 ng/ul in theReport the sum mum detection Unit for the sample with final extract should be confirmed by GC/I1S.the U (e.g. 10U) based on necessary concentration/dil- B - This flag is used when the analyte is found inution action (This is not necessarily the instrument the blank as well as a sample. It indicatesdetection limit). The footnote should read: U-Coapound possible/probable blank contamination and warnswas analyzed for but not detected. The number is the data the user to take appropriate action.minimum attainable detection limit for the sample. Other - Other specific flags and footnotes may be

J - Indicates en estimated value. This flag is used either required to properly define the results. Ifwhen estimating a concentration for tentatively identified used, they must be fully described and suchcompounds where a 1:1 response is assumed or when the mass description attached to the data summary report

I, spectral data indicated the presence of a compound thatmeets the identification criteria but the result is < than OPTIONAL FLAGSthe specified detection limit but > than zero • n I n fl n I C(e.g. 10J). If limit of detection is 10 ug/L and a N - Compound not present in Calibration RlJ.U U U I 0cement rat ion of 3.0 ug/L is calculated, report as 3J.

Font 1 7/85

I -t Sample Number I $&-[ I

Organics Analysis Data Sheet I E4724 '* (Page 1) *———————-

Laboratory Name: Bridgeport Environmental, Inc. Case No.: N/ALab Sample 10: >A8899::01 QC Report No.:Sample Matrix: SOIL /O 0/0 A Strict *°.i N/AData release Authorized by: *rxtC<A^^X /J Kyv O Date Sample Received: 24 AUG 90

volatile CompoundsConcentration: ( £OM Medium (Circle One )Date Extracted:Date Analyzed: 08/29/90 15:34Cone/Oil factor: 1 pH :Percent Moisture: 27,IX

C.A.S. ug/1 or llj/ta) C.A.S. ug/1 or (jo/kg*Number (Circle flntf- Number (Circle One

ig/kgneT

74-87-3 Chloromethane 14. U 78-87-5 1,2-Dichloropropane 7. U74-03-9 Bromomethane 14. U 10061-02-6 Trans-l,3-Dichloropropene 7. U75-01-4 Uinyl Chloride 14. U 79-01-6 Trichloroethene 7. U75-00-3 Chloroethane 14. U 124-48-1 Dibromochloromethane 7. U75-09-2 rtethylene Chloride 19. B 79-00-5 1,1,2-Trichloroethane 7. U67-64-1 Acetone 23. 8 71-43-2 Benzene 7. U107-02-8 Acrolem 69. U 19061-01-5 ^cis-l,3-0ichloropropene 7. U167-13-1 Acrylonitrile 69. U 110-75-8 2-Chloroethylvinylether 14. U75-15-0 Carbon Disulfide 14. U 75-25-2 Bromoform 7. U75-35-4 1,1-Dichloroethene 7. U 108-10-1 4-rtethyl-2-Pentanone 14. U75-34-3 1,1-Dichloroethane 7. U 591-78-6 2-Hexenone 14. U156-60-5 Trans-l,2-Dichlotoethene 7. U 127-18-4 Tetrachloroethene 7. U67-66-3 Chloroform 7. U 79-34-5 1,1,2,2-Tetrachloroethane 7. U107-06-2 1,2-Dichloroethane 7. U 108-86-3 Toluene 7. U78-93-3 2-Butanone 14. U 108-90-7 Chlorobenzene 7. U71-55-6 1,1,1-Trichloroethane 7. U 100-41-4 Ethylbenzene 7. U56-23-6 Carbon Tetrachloride 7. U 100-42-5 Styrene 7. U108-05-4 Uinyl Acetate 14. U Total Xylenes 7. U75-27-4 Bromodichloromethane 7. U Total Oichlorobenzenes 7. U


Ualue - IF the result is e value greater than or equal to C - This flag applies to pesticide parameters wherethe detection limit, report the value. the identification has been confirmed by GC/flS.

U - Indicates compound uas analyzed for but not detected. Single component pesticides >• 10 ng/uL in theReport the minimum detection limit for the sample with final extract should be confirmed by GC/ttS.the U (e.g. 10U) based on necessary concentration/dil- 8 - This flag is used when the analyte is found inution action (This is not necessarily the instrument the blank as well as a sample. It indicatesdetection limit). The footnote should read: U-Compound possible/probable blank contamination and warnsuas analyzed for but not detected. The number is the data the user to take appropriate action.minimum attainable detection limit for the sample. Other - Other specific flags and footnotes may be

J - Indicates an estimated value. This flag is used either required to properly define the results. Ifwhen estimating • concentration for tentatively identified used, they must be fully described and suchcompounds where a 1:1 response is assumed or when the mass description attached to the data summary reportspectral data indicated the presence of a compound thatmeets the identification criteria but the result is < than OPTIONAL FLAGSthe specified detection limit but > than zero(e.g. 10J). If limit of detection is 10 ug/L and • N - Compound not present in Calibration File.conentration of 3.0 ug/L is calculated, report as 3J. > A R I 0 0 0 I 7

Form 1 7/85

CERTIFICATE OF ANALYSISPRIORITY POLLUTANT , /£

ANALYSIS NO: £ 4697

CLIENT ID: Station 2-1045


METALS MDL (mg/L) RESULT (mg/L)

Antimony 0.005 N.D.

Arsenic 0.005 N.D.

Beryllium 0.01 N.D.

Cadmium 0.01 N.D.

Chromium 0.01 N.D.

Copper 0.01 0.02

Lead 0.05 N.D.

Mercury 0.0005 N.D.

Nickel 0.05 N.D.

Selenium 0.005 N.D.

Silver 0.01 N.D.

Thallium 0.10 N.D.

Zinc 0.01 0.06

Cyanide 0.01 N.D.

AR 1000 I 8

JL -

Lab Name : Uastex Ind. of NJ I Sample Number ICase No : N/A t £4704 I

QRGANICS ANALYSIS DATA SHEET * —— — —— ~*(Page 2)


Concentration^ ^Uwyfledium (Circle One ) 6PC Cleanup __ Yes _ NoDate Extracted! 08/27/90 Separatory Funnel Extraction _ YesDate Analyzed: 09/08/90 15:41 Continuous Liquid-Liquid Extraction _ YesCone /Oil Factor: lOOQUalPercent Moisture: NA

C.A.S. £ uq/ r ug/Kg C.A.S. ' ug/Ljfr ug/KgNumber --lurcle One) Number TTTfcle One)

108-95-2 Dhenoi 10.U 83-32-9 Acenaphthene 10.U111-44-4 bis(-2-Chloroethyl)Ether 10.U 51-28-5 2,4-Dinitrophenol 50.U95-57-3 2-Chlorophenol 10.U 100-02-7 4-Nitrophenol 58.U541-73-1 1,3-Dichlorobenzene 10. U 132-64-9 Dibenzofuran 10.U106-46-7 1,4-Dichlorobenzene 10. U 121-14-2 2,4-Dinitrotoluene 10. U100-51-6 Benzyl Alcohol 10. U 606-20-2 2,6-Dinitrotoluene 10. U95-50-1 1,2-Oichlorobenzene 10.U 84-66-2 Diethylphthalate 1Q.U95-48-7 2-Hethylphenol 10. U 7005-72-3 4-Chlorophenyl-phenlyether 10.U

39638-32-9 bis(2-chloroisopropyl)Ether 10. U 86-73-7 Fluorene 10. U106-44-5 4-Rethylpnenol 10.U 100-01-6 4-Nitroaniline 50.U621-64-7 N-Nitroso-Di-n-Propylamine Ifl.U 534-52-1 4,6-Oinitro-2-l1ethylphenol 50. U67-72-1 Hexachloroethane 10. U 86-30-6 N-Nitrososdiphenylamine (1) 10. U99-95-3 Nitrobenzene 10.U 101-55-3 4-Bromophenyl-phenylether 10. U78-59-1 Isaphorone 10. U 118-74-1 Hexachlorobenzene 10. U38-75-5 2-Nitropnenol 10. U 87-86-5 Pentachlorophenol 50. U105-67-9 2,4-Dimethylphenoi 10. U 85-01-8 Phenanthrene 10. U65-85-0 Senzoic Acid 50. U 120-12-7 Anthracene 10. U111-91-1 bis(-2-Chloroethoxy)dethane 10. U 84-74-2 Di-n-Butylphthalate 10. U120-83-2 2,4-Oichlorophenol 10.U 206-44-0 Fluoranthene 10.U120-82-1 1,2,4-Trichlorobenzene 10.U 129-00-0 Pyrene 10. U91-20-3 Naphthalene 10. U 85-68-7 Butylbenzylphthalate 10. U106-47-8 4-Chloroaniline Ifl.U 1-94-1 3,3'-Dichlorobenzidine 20.U87-68-3 Hexachlorobutadiene 10. U 56-55-3 8enzo(a)Anthracene 10. U59-50-7 4-Chloro-3-Hethylphenol 10.U 117-81-7 bis(2-Ethylhexyl)Phthalat6 3.J91-57-6 2-fethylnaphthalene 1Q.U 218-01-9 Chrysene 10. U77-47-4 Hexachlorocyclopentadiene 10. U 117-84-0 Di-n-Octyl Phthalate 10. U88-06-2 2,4,6-Trichlorophenol 10.U 205-99-2 Benzo(b)Fluoranthene 10.U95-95-4 2,4,5-Trichlorophenol 50. U 207-08-9 Benzo(k)Fluoranthene **»n-58-7 2-ChloronaphthaIene 10.U 50-32-8 Benzo(a)Pyrene 10.U68-74-4 2-Nitroaniline 50.U 193-39-5 IndenoU,2,3-cd)Pyrene 10.U131-11-3 Dinethyl Phthalate 10. U 53-70-3 Dibenzo(a,h)Anthracene 10. U208-96-8 Acenaphthylene 10. U 191-24-2 Benzo(g,h,i)Peryiene 10. U99-09-2 3-Nitroaniline 50.U 92-87-5 Benzidine 20.U

(l)-Cannot be separated from diphenylanine A P I H D H I Q

*»*-Cannot be separated from BenzoCbJFluoranthene

STATION

Lab Name : Bridgeport Environmental, Inc. I Sample NunberCase No : N/fi _ I £4704

ORSAWCS ANALYSIS DATA SrEET +———————-(Page 3)

Pesticides/PCBs

Concentration: (j-ou ' Medium ( Circle One ) GPC Cleanup _ Yes _i NoDate Extracted/Prepared: 8/27/90 Separatory Funnel Extraction _JrDate Analyzed: 9/06/90 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor: 10QiL/5tLPercent hoistore: N/A

C.A.S. Cug/LorNunber ug/Kg

319-84-6 Alpha-BHC. ....... 0.25 U319-87-7 Beta-BHC ........ 0.25 U319-86-8 Delta-BHC. ....... 0.25 U58-89-9 Gamma-BHC (Lindane). . . 0.25 U76-44-6 Keptachlor ....... 0.25 U309-00-2 Aldrin ......... 0.25 U1024-57-3 Heptachlor Epoxide . . . 0.25 U959-96-8 Endosulfan I ...... 0.25 U60-57-1 Dieldrin ........ 0.25 U72-55-9 4,4'-DDE ........ 0.25 U72-20-8 Endrin ......... 0.25 U

33213-65-9 Endosulfan II. ..... 0.50 U72-54-8 4,4'-ODO ........ 0.50 U

1031-07-8 Endosulfan Sulfate . . . 0.50 U50-29-3 4,4'-ODT ........ 0.50 U72-43-5 nethoxychlor ...... 13 U


6001-35-2 Toxaphene. ....... 25 U12674-11-2 Arochlor-1016. ..... 13 U11104-26-2 Arochlor-1221. ..... 13 U11141-16-5 Arochlor-1232. ..... 13 U53469-21-9 Arochlor-1242, ..... 13 U12672-29-6 Arochlor-1248. ..... 13 U11097-69-1 Arochlor-1254. ..... 13 U11096-82-5 Arochlor-1260. ..... 13 U

Form 1 7/85

a

BR I 0002-0

CERTIFICATE OF ANALYSIS

PRIORITY POLLUTANT $0 i L

ANALYSIS NO. E 4711



METAT.S MDL (mg/kg) RESDLT (ing/kg)

Antimony 0.13 *•!>•

Arsenic 0.13 6-32

Beryllium 0 . 25 * • 17

Cadmium 0.25 °-80

Chromium 0.25 32-8

Copper 0.25

Lead 1.3

Mercury 0.05 K-D-

Nickel 2.5 25-8

Selenium 0.13 N'D-

Silver 0.25 N'D-

Thallium 2.5

Zinc 0.25 25°N.D.

Cyanide 0.10

flRI0002l


ORGANICS ANALYSIS DATA SHEET *-————————»(Page 2)

Semivolatile Compounds

Concentration^ LOM ) fled tun (Circle One ) GPC Cleanup _ Yes _ NoDate Extracted: W5/90 Separatory Funnel Extraction _ YesDate Analyzed: 09/06/9020:19 Continuous Liquid-Liquid Extraction _ YesConc/Dil Factor: 3fl6:I»lPercent Moisture: 57,5 **~~~~*\ ^ ^

uq/L fcjjq/Ka C.A.S. ug/C or ug/Kg yNumber (Circle One) Nuiiber (Circle Une)

108-95-2 Phenol 53Q.U 83-32-9 Acenaphthene 93.3111-44-4 bis(-2-Chlorcethyl)Ether 530.U 51-28-5 2,4-Dinitrophenol 2600.U95-57-8 2-Chlorophenol 530.U 100-02-7 4-Nitrophenol 2600.U541-73-1 1,3-DichIorobenzene 530.U 132-64-9 Dibenzofuran 71.J106-46-7 1,4-Dichlorobenzene 53Q.U 121-14-2 2,4-Oinitrotoluene 530.U100-51-6 Benzyl Alcohol 530.U 606-20-2 2,6-Dinitrotoluene 530.U95-50-1 1,2-Dichlorobenzene 550.U 84-66-2 Diethylphthalate 530.U

O 95-48-7 2-nethylphenol 530.U 7005-72-3 4-Chlorophenyl-phenlyether 530.U39638-32-9 bis(2-chloroisopropyl)Ether 530.U 86-73-7 Fluorene 530.U106-44-5 4-l1ethylphenol 530.U 100-01-6 4-Nitroaniline 2600.U621-64-7 N-Nitroso-Di-n-Propylaaina 530.U 534-52-1 4,6-Dinitro-2-t1ethylphenol 2600.U67-72-1 Hexachloroethane 530,U 86-30-6 N-Nitrososdiphenylanine (1) 530.U°8-95-3 Nitrobenzene 530.U 101-55-5 4-Bromophenyl-phenylether 530.U78-59-1 Isophorone 530.U 118-74-1 Hexachlorobenzene 550.U39-75-5 2-Nitrophenol 570.U 87-86-5 Pentachlorophenol 2630.U105-67-9 2,4-DimethylphBnol 550.U 85-01-8 Phenanthrene 1400.65-85-0 Benzoic Acid 2600.U 120-12-7 Anthracene 520.J111-91-1 bis(-2-Chloroethoxy)ttethane 550.U 84-74-2 Di-n-Butylphthalate 530.U120-83-2 2,4-Dichlorophenol 550.U 206-44-0 Fiuoranthene 2600.120-82-1 1,2,4-Trichlorobenzene 550.U 129-00-0 Pyrene 5100.91-20-3 Naphthalene 66.J 85-68-7 Butylbenzylphthalate 550.U

106-47-8 4-Chloroaniline 550.U 1-94-1 5,5'-Dichlorobenzidine 1100.U87-68-3 Hexechlorobutadiene 550.U 56-55-5 Benzo(a)Anthracene 990.59-50-7 4-Chloro-5-rtethylphenol 530.U 117-81-7 bis(2-£thylhexyl)Phthalate 530.U91-57-6 2-Methylnaphthalene 550.U 218-01-9 Chrysene 1100.77-47-4 Hexachlorocyclopentadiene 530.U 117-84-0 Di-n-Octyl Phthalate 550.U88-06-2 2,4,6-Trichlorophenol 550.U 205-99-2 Benzo(b)Fluoranthene 900.95-95-4 2,4,5-Trichlorophenol 2600.U 207-08-9 Benzo(k)Fluoranthene »»«91-58-7 2-Chloronaphthalene 550.U 50-32-8 Benzo(a)Pyrene 810.88-74-4 2-Nitroaniline 26QO.U 193-59-5 lndeno(l,2,3-cd)Pyrene 530.U

131-11-3 Dimethyl Phthalate 550.U 55-70-5 Dibenzo(a,h)Anthracene 530.U208-96-8 Acenaphthylene 530.U 191-24-2 Benzo(g,h,i)Perylene 530.U

, 99-09-2 3-Nitroaniline 2600.U 92-87-5 Benzidine 1100.U

(l)-Cannot be separated from diphenylamine

•••-Cannot be separated from Benzo(b)Fluoranthene An I U U U CL

*....,—————+

Lab Name : Bridgeport Environnental, Inc. t Sample Number ICase No : N/A I E4711 t

ORGANICS ANALYSIS DATA SHEET *- ———————— *(Page 3)

Pesticides/PCBs

Concentration: (Low \t1ediun ( Circle One ) GPC Cleanup H Yea _^Date Extracted/Prepared: 8/27/90 Separatory Funnel Extraction _ YesDate Analyzed: 9/10/90 Continuous Liquid-Liquid Extraction _ YesConc/Dil Factor: 10.02g/10nlsPercent Moisture: 37.?

C.A.S. ug/t orNumber '

319-84-6 Alpha-BHC. ....... 5.0 U319-87-7 Beta-BHC ........ 5.0 U319-86-8 Delta-BHC. ....... 5,0 U98-89-9 Gauna-BHC (Lindane). . . 5.0 U76-44-8 Heptachlor ....... 5.0 U309-00-2 Aldrin ......... 5.0 U1024-57-3 Heptachlor Epoxide ... 5.0 U959-98-8 Endosulfan I ...... 5.0 U60-57-1 Dieldrin ........ 5.0 U72-55-9 4,4'-OOE ........ 5.0 U72-20-8 Endrin ......... 5.0 U

33213-65-9 Endosulfan M. ..... 10.0 U72-54-8 4,4'-DDD ........ 10.0 U

1031-07-8 Endosulfan Sulfate . . . 10.0 U50-29-3 4,4'-DDT ........ 10.0 U72-43-5 Methoxychlor ...... 250 U



Fora 1 7/85

ARI00023

I Sample Number iJDrgamcs Analysis Data Sheet I E4718 f

(Page i) *_______*Laboratory Name: Bridgeport Environmental, Inc. Case No.J N/ALab Sample ID: >B9404::02 . OC Report No.:Sample Matrix: UATER /J (] i ft Contract No.: N/ftData release Authorized by: f I >t *"ftW ^^ fvAy ^ f Data Saraole Receiveo:24 AUG 90

Volatile CoromjndsvConcentration: QLow) fled i urn (Circle One )Date Extracted: —^Date Analyzed: 38/27/90 19:26Cone/Oil factor: 1 pH IPercent flojsture: _^

C.A.S. (ug/yor ug/kg C.A.S. Ig/l or ug/(cgNumber (Circle One) Number TCTrcle One)

74-87-3 Chloromethane 10. U 78-87-5 1,2-Dichloropropane 5. U74-83-9 Bromomethane 10. U 10061-02-6 Trans-1.3-Dichloroprooene 5. U75-01-4 Vinyl Chloride 10. U 79-01-6 Trichloroethene 5. U5-00-3 Chloroethane 10. U 124-48-1 Dibroraochlorcmethane 5. U75-09-2 Metholene Chloride ?. U 79-00-5 1,1,2-Trichloroethane 5. U67-64-1 Acetone 10. U 71-43-2 Benzene 5. U107-02-8 Acrolein 50. U 10061-01-5 cis-l,3-0ichloropropene 5. U167-13-1 Acrylonitrile 50. U 110-75-8 2-Chloroethylvinylether ID. U75-15-0 Carbon Disulfide 10. U 75-25-2 Broaoform 5. U

j 75-35-4 1,1-DichIoroethene 5. u' 108-10-1 4-Hethyl-2-Pentanone 10. U75-34-3 l.i-Oichloroethane 5. U 591-7B-6 2-Hexanone 10. U156-60-5 Trans-l,2-Dichlotoethene 5. U 127-18-4 Tetrachloroethene 5. U67-66-3 Chloroform 5. U 79-54-5 1,1,2,2-TetrachIoroethane 5. U107-06-2 1.2-Dichiorcethane 5. U 108-88-3 Toluene 5. U78-93-3 2-Butenone 10. U 108-90-7 Chlorobenzene 5. U71-55-6 1,1,1-Trichloroethane 5. U 100-41-4 Ethylbenzene ?. U56-23-6 Carbon Tetrachloride 5. U 10D-42-5 Styrene 5. U

" 138-05-** Uinyl Acetate 10. U Total Xylenes 5. U7 -27-4 Bromooichloromethane 5. U Total Dichlorobenzenes ?. U

Data Reporting QualifiersFor reporting results to EPA the follouing results qualifiers ere used. Additional flags or footnotesexplaining results are encouraged. Houever the definition of each flag must be explicit.

alue - If the result is e value greater than or equal to C - This flag applies to pesticide parameters wherethe detection limit, report the value. the identification has been confirmed by GC'HS.

U - Indicates compound uas analyzed for but not detected. Single component pesticides >» 10 ng/uL in theReport the minimum detection limit for the sample with final extract should be confirmed by GC/flS.the U (e.g. 10U) based on necessary concentration/dil- B - This flag is used when the analyte is found inution action (This is not necessarily the instrument the blank as well as a sample. It indicatesdetection limit). The footnote should read: U-Co»pound possible/probable blank contamination and warnsuas analyzed for but not detected. The number is the data the user to take appropriate action.minimum attainable detection limit for the sample. Other - Other specific flags and footnotes may be

J - Indicates an estimated value. This flag is used either required to properly define the results. Ifuhen estimating a concentration for tentatively identified used, they must be fully described and suchcompounds where a 1:1 response is assumed or when the mass description attached to the data summary report

J spectral data indicated the presence of a compound thatmeets the identification criteria but the result is < than OPTIONAL FLAGSthe specified detection limit but > than zero(e.g. 10J). If limit of detection is 10 ug/L and a N - Compound not present in Caiibraiion fjU-oconentration of 3.0 ug/L is calculated; report as 3J. A n I U U U 2 *f

Fora 1 7/85

A -I Sample Nunber I

Organics Analysis Data Sheet I E4725 I(Page 1) *- —— ————— *

Laboratory Name: Bridgeport Environmental, Inc. Case No.: N/ALab Sample 10: >A890Q::D1 (£ Report No.:Sample Matrix: SOIL S\ D / 0 / Con*r«t No.: N/AData release Authorized by: ( lxi*J^A»M/ £J )x^>^^X Date Sample Received:Sample Received: 24 AUS 90

volatile CompoundsConcentration: (low/ fled i urn (Circle One )Date Extracted:Date Analyzed: 88/29/90 16:22Conc/Dil factor: 1 pH :Percent Hoisture^JUX

C.A.S. ug/1 or<ug/k(J' C.A.S. ug/1 ortjg/kgNunber (Circle One! Nunber (Circle One)

74-87-3 Chloronethane 15. U 78-87-5 1,2-Oichloropropane 7. U74-83-9 Bromomethane 15. U 10061-02-6 Trana-l,3-Dichloropropene 7. U75-01-4 Vinyl Chloride 15. U 79-01-6 Trichloroethene 7. U75-00-3 Chloroethane 15. U 124-48-1 Dibronochloronethane 7. U75-09-2 Hethylene Chloride 9. B 79-00-5 1,1,2-Trichloroethane 7. U67-64-1 Acetone 39. 8 71-43-2 Benzene 7. U107-02-8 Acrolein 71. U 10061-01-5 cis-l,3-Dichloropropene 7. U167-13-1 Acrylonitrile 71. U 110-75-8 2-Chloroethylvinyiether 15. U75-15-0 Carbon Disulfide 15. U 75-25-2 Bromoform 7. U75-35-4 1,1-Dichloroetnene 7. U 108-10-1 4-Hethyl-2-Pentanone 15. U75-34-3 1,1-Dichloroethane 7. U 591-78-6 2-Hexanone 15. U156-60-5 Trans-l,2-Dichlotoethene 7. U 127-18-4 Tetrachloroethene 7. U67-66-3 Chloroform 7. U 79-34-5 1,1,2,2-Tetrachloroethane 7. U107-06-2 1,2-Dichloroethane 7. U 108-88-3 Toluene 7. U78-93-3 2-8utanone 15. U 108-90-7 Chlorobenzene 7. U71-55-6 1,1,1-Trichloroethane 7. U 100-41-4 Ethylbenzene 7. U56-23-6 Carbon Tetrachloride 7. U 1(10-42-5 Styrene 7, U108-05-4 Uinyl Acetate 15. U Total Xylenes 7. U75-27-4 flromodtchloronethane 7. U Total Oichlorobenzenes 7. U


Uatue - If the result is a value greater than or equal to C - This flag applies to pesticide parameters wherethe detection Unit, report the value. the identification has been confirmed by GC/ttS.

U - Indicates compound was analyzed for but not detected. Single component pesticides >• 10 ng/uL in theReport the minima detection linit for the sample with final extract should be confirmed by GC/TtS.the U (e.g. 10U) based on necessary concentration/dil- 6 - This flag is used when the analyte is found inution action (This is not necessarily the instrument the blank as well as a sample. It indicatesdetection linit). The footnote should read: U-Compound possible/probable blanK contamination and warnswas analyzed for but not detected. The number is the data the user to take appropriate action.minimum attainable detection limit for the sample. Other - Other specific flags end footnotes may be

J - Indicates an estimated value. This flag is used either required to properly define the results. Ifwhen estimating a concentration for tentatively identified used, they must be fully described and suchcompounds where a I'-l response is assumed or when the nass description attached to the data summary reportspectral data indicated the presence of a compound thatBeets the identification criteria but the result is < than OPTIONAL FLAGSthe specified detection limit but > than zero(e.g. 10J). If liiit of detection is 10 ug/L and • N - Compound not present in Calibration File.conentration of 3.0 ug/L is calculated, report as 3J. fl R I ft fi fi 9 C

Form 1 7/85

I Sample Number I .i j Organics Analysis Data Sheet I £4725 R I S> V I

(Page 1) *————Laboratory Name: Bridgeport Environmental, Inc. Case No.: K/ftLab Sample ID; >A8909::01 QC Report Ho.:Sample Matrix: SOIL >2 fl / Q Contract Mo,: N/AData release Authorized b: K L J - jf L*J rx>L**x>l Date S m l e ReceiData release Authorized by: L^-^^j L*J rx>L**x> Date Sample Received: 24 AUG 90

volatile CompoundsConcentration: (l wy Medium (Circle One )Date Extracted:Date Analyzed: 08/30/90 12:24Conc/Dil factor: 1 pH iPercent Moisture: 33. 3X

C.A.S. ug/1 or /kg: C.A.S. ug/1 or/fig/KgNumber (CircleWf Number (Circled)

74-87-3 Chloromethane 15. U 78-87-5 1,2-Dichloropropane 7, U74-83-9 Bromomethane 15. U 10061-02-6 Trans-l,3-Dichloropropene 7. U75-01-4 Uinyl Chloride 15. U 79-01-6 Trichloroethene 7. U75-00-3 Chloroethane 15. U 124-48-1 Dibromochloromethane 7. U75-09-2 ftethylene Chloride 8. B 79-00-5 1,1,2-Trtchloroethane 7. U67-64-1 Acetone 3. B,J 71-43-2 Benzene 7. U107-02-8 Acrolein 71. U 10061-01-5 cis-l,3-Dichloropropene 7. U167-13-1 Acrylonitrile 71. U 110-75-8 2-Chloroethylvinyiether 15. U75-15-0 Carbon Oisulfide 15. U 75-25-2 Bromoform 7. U75-35-4 1,1-Dichloroethene 7. U 108-10-1 4-Methyl-2-Pentanone 15. U75-34-3 l;l-0ichloroethane 7. U 591-78-6 2-Hexanone 15. U156-60-5 Trans-l,2-Dichlotoethene 7. U 127-18-4 Tetrachloroethene 7. U67-66-3 Chloroform 7. U 79-34-5 1,1,2,2-Tetrachloroethane 7. U107-06-2 1,2-Dichloroethana 7. U 108-88-3 Toluene 7. U78-93-3 2-Butanone 15. U 108-90-7 Chlorobenzene 7. U71-55-6 1,1,1-Trichloroethane 7. U 100-41-4 Ethylbenzene 7. U56-23-6 Carbon Tetrachloride 7. U 100-42-5 Styrene 7. U108-05-4 Vinyl Acetate 15. U Total Xylenes 7, U75-27-4 Sromodichloromethane 7. U Total Dichlorobenzenes 7. U


value - If the result is a value greater than or equal to C - This flag applies to pesticide parameters wherethe detection limit, report the value. the identification has been confirmed by GC/HS.

U - Indicates compound was analyzed for but not detected. Single component pesticides >• 10 ng/uL in theReport the Minimum detection limit for the sample with final extract should be confirmed fay GC/MS.the U (e.g. 10U) based on necessary concent ration/dil- B - This flag is used when the analyte is found inution action (This is not necessarily the instrument the blank as well as a sample. It indicatesdetection limit). The footnote should read: U-Conpound possible/probable blank contamination and warnswas analyzed for but not detected. The number is the data the user to take appropriate action.minimum attainable detection limit for the sample. Other - Other specific flags and footnotes may be

J - Indicates an estimated value. This flag is used either required to properly define the results. Ifwhen estimating a concentration for tentatively identified used, they oust be fully described and suchcompounds where a 1:1 response is assumed or when the mass description attached to the data summary reportspectral data indicated the presence of a compound that

^ meets the identification criteria but the result is < than OPTIONAL FLAGSthe specified detection limit but > than zero(e.g. 10J). If limit of detection is 10 ug/L and a N - Compound not present in Calibration File.conentration of 3.0 ug/L is calculated, report as 3J. flRIQuQ26

Fort 1 7/85


ANALYSIS KO: E 4698




Antimony 0.005 N.D.

Arsenic 0.005 N.D.

Beryllium 0.01 N.D.

\J Cadmium 0.01 N.D.

Chromium 0.01 N.D.

CoPPer 0.01 0.04

Lead 0.05 N.D.

Mercury 0.0005 N.D.

*"•<**! 0.05 , N.D.

Selenium 0.005 N.D.

Silver 0.01 N.D.

Thallium 0.10 N.D.

Zinc 0.01 0.06

Cyanide 0.01 H.D.

flRI00027

Lab Name : Uastex Ind. of NJ I Sample Number ICase No : N/A I £4705 I

QRSANICS ANALYSIS DATA SHEET + ———————— *(Page 2)

Seaivolatile Compounds

Concentration:^ Loyx Medium (Circle One ) GPC Cleanup _ Yes _ NoDate Extracted: 08/27/90 Separatory Funnel Extraction _ YesDate Analyzed: 09/10/90 15:14 Continuous Liquid-Liquid Extraction _ YesCone /Oil Factor: IQOOUmlPercent Moisture: NA

C.A.S. f ug/^Ar ug/Kg C.A.S. C ug/Jr ug/KgNumber *-TTtrcle One) Number ^ "TTTfcie One)

108-95-2 Phenoi 10.U 83-32-9 Acenaphthene 10.U111-44-4 bis(-2-Chloroethyl)Ether 10.U 51-28-5 2,4-Dinitrophenol 50.U95-57-8 2-Chlorophenol 10.U 100-02-7 4-Nitrophenol 50,U541-73-1 1,3-Dichlorobenzene 10.U 132-64-9 Dibenzofuran 10.U136-46-7 1,4-Dichlorobenzene 10.U 121-14-2 2,4-Dinitrotoiuene 10.U

/ 100-51-6 Benzyl Alcohol 10.U 606-20-2 2,6-Dinitrotoluene 10.U^ 95-50-1 1,2-Dichlorobenzene 10.U 84-66-2 Diethylphthalate 10.U

95-48-7 2-ttethylphenol 10.U 7005-72-3 4-Chlorophenyi-phenlyether 10.U39638-32-9 bis(2-chloroisoprcpyl)Ether 10.U 86-73-7 Fluorene 10.U106-44-5 4-Hethylphenol 10.U 100-01-6 4-Nitroaniline 50,U621-64-7 N-Nitroso-Di-n-Propylanine 10.U 534-52-1 4,6-Dinitro-2-t1ethylphenol 50.U67-72-1 Hsxachloroethane 10.U 86-30-6 N-Nitrososdiphenylamme (1) 10.U99-95-3 Nitrobenzene 10.U 101-55-3 4-Bromophenyl-phenylether 10.U78-59-1 Isophorone 10.U 118-74-1 Hexachlorobenzene 10.U83-75-5 2-Nitrophenol 10.U 87-86-5 Pentachlorophenol 10.U105-67-9 2,4-Dimethylphenol 10.U 85-01-8 Phenanthrene 10.U£5-85-0 Benzoic Acid 50.U 120-12-7 Anthracene 10.U111-91-1 bis(-2-Chloroethoxy)ttethane 10.U 84-74-2 Di-n-Butylphthalete 10.U120-83-2 2,4-Dichlorophenol 10.U 206-44-0 Fluoranthene 10.U120-82-1 1,2,4-Trichlorobenzene 10.U 129-flfl-O Pyrene 10.U91-20-3 Naphthalene 10.U 85-68-7 Butylbenzylphthalate 10.U1Q6-47-8 4-Chloroaniline 10.U 1-94-1 3,3'-Dichlorobenzidine 20.U87-68-3 Hexachlorobutadiene 10.U 56-55-3 BenzotaJAnthracene 10.U59-50-7 4-Chloro-3-Hethylphenol 10.U 117-81-7 bis(2-Ethylhexyl)Phthalate 9.J91-57-6 2-flethylnaphthalene 10.U 218-01-9 Chrysene 10.U77-47-4 Hexachlorocyclopentadiene 10.U 117-84-0 Di-n-Octyl Phthalate 6.J88-06-2 2,4,6-Trichlorophenol Ifl.U 205-99-2 Benzo(b)Fluoranthene 10.U95-95-4 2,4,5-Trichlorophenol 50.U 207-08-9 Benzo(k)Fluoranthene ••*91-58-7 2-Chloronaphthalene 10.U 50-32-8 Benzo(a)Pyrene 10.U88-74-4 2-Nitroaniline 50.U 193-39-5 Indeno(l,2,3-cd)Pyrene 10.U131-11-3 Dimethyl Phthslate 10.U 53-70-3 Dibenzo(a,h)Anthracene 10.U

i , 208-96-8 Acenaphthylene 10.U 191-24-2 Benzo(g,h,i)Perylene 10.U^ 99-09-2 3-Nitroaniline 50.U 92-87-5 Benzidine 20.U

(l)-Cannot be separated from dtphenylamine fl R I fl fl fl 9 P

•"-Cannot be separated fron 8enzo(b)Fluoranthene

3 -Lab Nans : Bridgeport Environmental, Inc. I SanpU NumberCase No : N/A _ I E4705

ORGANICS ANALYSIS DATA SHEET *(Page 5)

Pesticides/PCBs

Concentration! J_o« ,-Hediuii ( Circle One ) 6PC Cleanup _ Yes _ .'NoDate Extracted/Prepared! 9/27/90 Separatory Funnel Extraction j/Date Analyzed: 9/06/90 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor! 100oL/5iLPercent Moisture: N/A

C.A.S.Nunber ug/Kg

319-84-6 Alpha-BHC. ....... 0.25 U319-87-7 Beta-BHC ........ fl.25 U319-86-8 Delta-BHC. ....... 0.25 U58-89-9 Ganma-BHC (Lindane). . . 0.25 U76-44-8 Heptachlor ....... 0.25 U309-00-2 Aldrin ......... fl.25 U1024-57-3 Heptachlor Epoxide . . . 0.25 U959-98-8 Endosulfan I ...... 0.25 U60-57-1 Dieldrin ........ 0.25 U72-55-9 4,4'-DDE ........ 0.25 U72-20-8 Endrin ......... 0,25 U

33213-65-9 Endosulfan II. ..... 0.50 U72-54-8 4,4'-DDO ........ fl.50 U

1031-07-8 Endosulfan Sulfata . . . 0.50 U50-29-3 4,4'-DDT ........ 0.50 U72-43-5 Methoxychlor ...... 13 U


8001-35-2 Toxaphene. ....... 25 U12674-11-2 ArochIor-1016. ..... 13 U11104-28-2 Arochlor-1221. ..... 13 U11141-16-5 Arochlor-1232. ..... 13 U53469-21-9 Arochlor-1242. ..... 13 U12672-29-6 Arochlor-1248. ..... 13 U11097-69-1 Arochlor-1254. ..... 13 U11096-82-5 Arochlor-1260. ..... 13 U

Forn 1 7/85

ARI00029

* CERTIFICATE OF ANALYSIS 50 ( L

PRIORITY POLLUTANT "3

ANALYSIS NO. E 4712



MPL (mg/kg) RESULT (mg/kg)

Antimony 0.13 N.D.

Arsenic 0.13 5.01

Beryllium 0 . 25 0.81

Cadmium ' 0.25 1.47

Chromium • 0*25 53.2

Copper 0.25 65.8

Lead 1.3 249

Mercury 0.05 N.D.

Nickel 2.5 31.7

Selenium 0.13 1-26

Silver 0.25 N.D.

Thallium 2.5 N-D-

Zinc 0.25 353

Cyanide 0.10 °*66

ARI00030

Lab Name : Bridgeport Environmental, Inc. I Samp la Number ICase No : N/A I £4712 I

ORGAWCS ANALYSIS DATA S*£ET +-————————*(Page 2)

Seaivolatile Cootpounds

Concentration^ lojjy Kediun (Circle One ) GPC Cleanup _ Yes _ NoDate Extracted: 8/58/90 Separatory Funnel Extraction _ YesDate Analyzed: 09/08/9021:15 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor: 3QG:lnlPercent Moisture: 32.6 S**~~*\ J

ug/L oTug/Kq) C.A.S. ug/L cug/KgNumber (Circle OhST"- Number (Circl

IU8-95-2 Phenol 49Q.U 33-52-9 Acenaphthene 490.U111-44-4 bis(-2-Chloroethyl)Ether 490.U 51-28-5 2,4-Oinitrophenol 2400.U*5-57-8 2-Chlorophenol 490.U 100-02-7 4-Nitrophenol 2400.U541-73-1 1,3-Dichlorobenzene 490.U 132-64-9 Dibenzofuran 490.U106-46-7 1,4-Oichlorobenzene 490.U 121-14-2 2,4-Dinitrotoluene 490.U100-51-6 Benzyl Alcohol 490.U 606-20-2 2,6-Oinitrotoluene 49Q.U95-50-1 1,2-Dichlorobenzene 490.U 84-66-2 Diethylphthalate 490.U

W 95-48-7 2-(1ethylphenol 490.U 7005-72-3 4-Chlorophenyl-phenlyether 490.U7963B-72-9 bis(2-chloroisopropyl)Ether 490.U 86-73-7 Fluorene 490.U106-44-5 4-Methylphenol 490.U 100-01-6 4-Nitroaniline 24QO.U621-64-7 N-Nitroso-Oi-n-Propylamine 490.U 534-52-1 4,6-Dinitro-2-Methylphenol 2400.U67-72-1 Hexachloroethane 490.U 86-30-6 N-Nitrososdiphenylaaine (1) 490.U

99-95-3 Nitrobenzene 490.U 101-55-3 4-Bromophenyl-phenylether 490.U78-59-1 Isophorone 490.U 118-74-1 Hexachlorobenzene 490.U98-75-5 2-Mitrophenol 490.U 87-86-5 Pentechlorophenol 2400.U105-67-9 2,4-Dimethylphenol 490.U 85-01-8 Phenanthrene 790.65-95-0 Benzoic Acid 2400.U 120-12-7 Anthracene 140.J111-91-1 bis(-2-Chloroethoxy)Methane 490.U 84-74-2 Di^n-Butylphthalate 490.U120-83-2 2,4-Oichlorophenol 490.U 206-44-0 Fluoranthene 650.120-82-1 1,2,4-Trichlorobenzene 490.U 129-00-0 Pyrene 1500.91-20-3 Naphthalene 490.U 85-68-7 Butylbeniylphthalate 490.U

106-47-8 4-Chloroaniline 490.U 1-94-1 3,3'-Oichlorobenzidine 980.U87-68-3 Hexachlorobutadiene 490.U 56-55-3 Benzo(a)Anthracene 490.U59-50-7 4-Chloro-J-Methylphenol 490.U 117-81-7 bis(2-Ethylhexyi)Phthalate 1700.91-57-6 2-nethylnaphtha!ene 210.J 218-01-9 Chrysene 490.U77-47-4 Hexachlorocyclopentadiene 490.U 117-84-0 Di-n-Octyl Phthalate 490.U88-06-2 2,4,6-Trichlorophenol 490.U 205-99-2 8enzo(b)Fluoranthene 280.J95-95-4 2,4,5-Trichlorophenol 2400.U 207-08-9 BenzotkJFluorenthene »*«?l-59-7 2-Chloronaphthalene 490.U 50-32-8 Benzo(a)Pyrene 330.J88-74-4 2-Nitroaniline 240Q.U 193-39-5 Indeno(l,2,3-cd)Pyrene 490.U

171-11-3 Dimethyl Phthalate 490.U 53-70-3 Dibenzo(a,h)Anthracene 490.U208-96-8 Acenaphthylene 490.U 191-24-2 Benzo(g,h,i)Perylene 730.U09-09-2 3-Nitrcaniline 2400.U 92-87-5 Benzidine 980.U

(l)-Cannot be separated from diphenylamine flRioooai•"-Cannot be separated fron Benzo(b)Fluoranthene

Lab Name : Bridgeport Environmental, Inc. I Sample Number ICasa No : N/A I E4712 I

ORSANICS ANALYSIS DATA SHEET + ————————— *(Page 3)

Pesticides/PCBs

Concentration: (HoiT flediun ( Circle One ) GPC Cleanup _ Yes J^ NoDate Extracted/Prepared: 8/27/90 Separatory Funnel Extraction M YesDate Analyzed: 9/11/90 Continuous Liquid-Liquid Extraction _ YesConc/Dil Tactor: 10.03g/10»UPercent Moisture: 32.6

C.A.S.Nunfaer

319-84-6 Alpha-BHC. ....... 10.0 U319-87-7 Bete-BHC ........ 10.0 U319-66-8 Delta-BHC. ....... 10.0 U98-89-9 Gawna-BHC (Lindane). . . 10.0 U76-44-8 Heptachlor ....... 10.0 U309-00-2 Aldrin ......... 10.0 U1024-97-3 Heptachlor Epoxide . . . 10.0 U999-98-8 Endosulfan I ...... 10.0 U60-57-1 Dieldrin ........ 5072-55-9 4,4'-DDE ........ 10.0 U72-20-8 Endrin ......... 10.0 U

33213-65-9 Endosulfan II. ..... 20.0 U72-54-8 4,4'-DDD ........ 320

1031-07-8 Endosulfan Sulfate . . . 20.0 U50-29-3 4,4'-DOT ........ 24072-43-5 flethoxychlor ...... 500 U

7421-93-4 Endrin Aldehyde. .... 20.0 U57-74-9 Chlordene. ....... 500 U

8001-35-2 Toxephene. ....... 1000 U12674-11-2 Arochlor-1016, ..... 500 U11104-28-2 Arochlor-1221. ..... 500 U11141-16-5 Arochlor-1232. ..... 500 U53469-21-9 Arochlor-1242. ..... 500 U12672-29-6 Arochlor-1248. ..... 500 U11097-69-1 ArochIor-1254. ..... 500 U11096-82-5 Arochlor-1260. ..... 500 U

Fort 1 7/85

3 -I Sample Mustier I

J3rganics Analysis Data Sheet I E4719 I(Page i) *-———————-*

Laboratory Name: Bridgeport Environmental, Inc. Case No.: N/ALab Sample ID: >B9405:*:D2 DC Report No.:Sample Matrix: UATER -O 0/1 1 Contract No.: N/AData release Authorized by: flNLcJ uf t *} JIA A /N flats Samoie Received:24 AUG 90

Volatile Compoundsjf 1 y\Concentration: (Lo.ii/ Medium (Circle One )Date Extracted:Date Analyzed: 08/27/90 20:13Cone/Oil factor: 1 pH :Percent ffeUture:

C.A.S. (fig/por ug/kg C.A.S. (ug/j/or ug/kgNumber iCTrcle One) Number TCTrcie One)

74-87-3 Chloromethane 10. U 78-87-5 1,2-Dichloropropane 5. U74-03-9 Sromomethane 10. U 10061-02-6 Trans-i.3-0ichloropropene 5. U75-01-4 I'inyl Chloride 10. U 79-01-6 Trichloroethene 5. U75-00-3 Chloroethane 10. U 124-48-1 Dibromochlororaethane 4. J75-09-2 flethylene Chloride 3. J,B 79-00-5 1,1,2-Trichloroethane 5. U67-64-1 Acetone 10. U 71-43-2 Benzene 5. U107-02-8 Acrolein 50. U 10061-01-5 cis-l,3-Dichloropropene 5. U167-13-1 Acrylonitrile 50. U 110-75-9 2-Chloroethylvinylether 10. U75-15-0 Carbon Oisulfide 10. U 75-25-2 Bronoform ' 5. U

> 75-35-4 1,1-Dichloroethene 5. U 108-10-1 4-l1ethvl-2-Pentanone 10. U^^ 75-34-3 i.l-Dichloroethane 5. U 591-78-6 2-Hexanone 10. U

156-60-5 Trans-1.2-Dichlotoethene 5. U 127-18-4 TetrachUroethene 5. U67-66-3 Chloroform 31. 79-34-5 1,1,2,2-Tetrachloroethane 5. U107-06-2 1.2-Dichloroethane 5. U 108-88-3 Toluene 5. U78-93-3 2-Butanone 10. U 108-90-7 Chlorobenzene 5. U71-55-6 i.Ll-Trichloroethane 5. U 100-41-4 Ethyibenzene 5. U56-23-6 Carbon Tetrachloride 5. U 100-42-5 Styrene 5. U138-05-4 vinyl rtcetate 10. U Total Xylenes 5, u??-27-4 Sromooichiorometnane 15. Total Oichiorobenzenes ?. u


'Jalue - If the result is a value greater than or equal to C - This flag applies to pesticide parameters wherethe detection limit, report the value. the identification has been confirmed by GC/flS.

U - Indicates compound was analyzed for but not detected.' Single component pesticides >• 10 ng/uL in theReport the minimum detection limit for the sample with final extract should be confirmed by GC/MS.the U (e.g. 10U) based on necessary concentration/dil- B - This flag is used when the analyte is found inuticn action (This is not necessarily the instrument the blank as well as a sample, tt indicatesdetection limit). The footnote should read: U-Compound possible/probable blank contamination and warnsuias analyzed for but not detected. The number is the data the user to take appropriate action.minimum attainable detection limit for the sample. Other - Other specific flags and footnotes may be

J - Indicates an estimated value. This flag is used either required to properly define the results. Ifuhen estimating a concentration for tentatively identified used, they must be fully described and suchcompounds where a 1:1 response is assumed or when the mass description attached to the data summary report

\^J spectral data indicated the presence of a compound thatmeets the identification criteria but the result is < than OPTIONAL FLAGSthe specified detection liait but > than zero(e.g. 10J). If limit of detection ia 10 ug/L and a N * Compound not present in Calibration File.conentration of 3.0 ug/L is calculated, report as 3J. . D • - n _

An IUU033Porn 1 7/85

-nayI Sample Number I 3 <9 l" (

\i Organics Analysis Data Sheet I E4726 I— (Page U *————————*

Laboratory Name: Bridgeport Environmental, Inc. Case No.: K/ALab Sample ID: >A3910::D1 QC Report No.:Sample Matrix: SOIL /^ fl * ft . Contract Mo.: N/AData release Authorized by: iKv^^d*rf Ltl 5> yc*A. Date Sample Received: 24 AUG 90

Volatile CoConcentration: u/ lied i urn (Circle One )Date Extracted:Date Analyzed: 08/50/90 13:12Cone/Oil factor: 1 pH :Percent Roisture: 30.OX

C.A.S. ug/1 or (tig/kg C.A.S. ug/1 ,.Hunber (Circle One) Number (CircleSJnW

74-87-3 Chloromethane 14, U 78-87-5 1,2-Oichloropropane 7. U74-83-9 Bromomethane 14. U 10061-02-6 Trans-l,3-Dichloropropene 7. U75-01-4 Umyl Chloride 14. U 79-01-6 Trichloroethene 7. U75-00-3 Chloroethane 14. U 124-48-1 Dtbromochloromethane 7. U75-09-2 netnylene Chloride 10. B 79-00-5 1,1,2-Trichloroethane 7. U67-64-1 Acetone 72. B 71-43-2 Benzene 7. U107-02-8 Acrolein 71. U 10061-01-5 cis-l,3-Dichloropropene 7. U167-13-1 Acrylonitrile 71. U 110-75-8 2-Chloroethylvinylether 14. U75-15-0 Carbon Oisulfide 14. U 75-25-2 Bromoform 7. U75-35-4 1,1-Dichloroethene 7. U 108-10-1 4-ttethyl-2-Pentanone 14. U

J 75-34-3 1,1-Dichloroethane 7. U 591-78-6 2-Hexanone 14. U156-60-5 Trans-l,2-DichIotoethene 7. U 127-18-4 Tetrachloroetnene 7. U67-66-3 Chloroform 7. U 79-34-5 1,1,2,2-Tetrachloroethane 7. U107-06-2 1,2-Dichloroethane 7. U 108-88-3 Toluene 7. U78-93-3 2-Butanone 14. U 108-90-7 Chlorobenzene 7. U71-55-6 1,1,1-Tricnloroethane 7. U 100-41-4 Ethylbenzene 7. U56-23-6 Carbon Tetrachlonde 7. U lflfl-42-5 Styrene 7. U108-05-4 Umyl Acetate 14. U Total Xylenes 7. U75-27-4 Browodichloromethane 7. U Total Dichlorobenzenes 7. U


Ualue - If the result is a value greater than or equal to C - This flag applies to pesticide parameters wherethe detection limit, report the value. the identification has been confirmed by GC/HS.

U - Indicates compound was analyzed for but not detected. Single component pesticides >• 10 ng/uL in theReport the minimum detection limit for the sample with final extract should be confirmed by GC/ttS.the U (e.g. 10U) based on necessary concentration/dil- B - This flag is used when the analyte is found inution action (This is not necessarily the instrument the blank as well as a sample. It indicatesdetection limit). The footnote should read: U-Compound possible/probable blank contamination and warnswas analyzed for but not detected. The number is the data the user to take appropriate action.minimum attainable detection limit for the sample. Other - Other specific flags and footnotes may be

J - Indicates an estimated value. This flag is used either required to properly define the results. Ifwhen estimating e concentration for tentatively identified used, they must be fully described and suchcompounds where a 1:1 response is assumed or when the mass description attached to the data summary report

J spectral data indicated the presence of a compound thatmeets the identification criteria but the result is < than OPTIONAL FLAGSthe specified detection limit but > than zero(e.g. 10J). If limit of detection is 10 ug/L and a N - Compound not present in Calibration File.conentration of 3.0 ug/L is calculated, report as 3J.

Form 1


ANALYSIS NO: E 4699




Antimony 0.005 N-D-

Arsenic 0.005 N.D.

Beryllium 0.01 N-D-

Cadmium 0.01 H-D-

Chromium 0.01 0.03

Copper 0.01 0-12

Lead 0.05 0-16

Mercury 0.0005 °-°013

Nickel 0.05 N-D-

Selenium 0.005 N*D*

Silver 0.01 K-D-

Thallium 0.10 N-D-

Zinc 0.01 °-36

Cyanide 0.01 N.D.

ARI00035

M-

Lab Name : Uastex Ind. of NJ I Sample Number ICase No : N/fl ! E4706 I

ORGANICS ANALYSIS DATA SHEET * ———————— »2)

Searivolatile Compounds

Concentration^ Apjrf/' tedium (Circle One > GPC Cleanup _ Yes _ NoDate Extracted: 08/27/90 Separatory Funnel Extraction _ YesDate Analyzed: 09/11/90 19:58 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor: 1000: tielPercent Moisture: NA

C.A.S. (uo/^r ug/Kg C.A.S. ( ug/L\r ug/KgNumber setfcla One) Number Mfiiftle One)

1QS-95-2 Phenol Ifl.U 33-52-9 ftcenaphthene Ifl.U111-44-4 bis(-2-CMoroethyl)Ether Ifl.U 51-28-5 2,4-Dinitrophenol 5Q.U95-57-8 2-Chlorophenol 10. U 10fl-fl2-7 4-Nitrophenol 50. U541-73-1 1,3-Dichlorofaenzene 10. U 132-64-9 Oibenzofuran Ifl.U106-46-7 1,4-Oichlorobenzene 10.U 121-14-2 2,4-Dinitrotoluene 10.U100-51-6 Benzyl Alcohol 10. U 606-20-2 2,6-Dinitrotoluene 10.U95-50-1 1,2-Dichiorobenzene 10. U 84-66-2 Diethylphthalate 10. U95-48-7 2-flethylphenol Ifl.U 7D05-72-3 4-Chlorophenyl-phenlyether 10.U

79638-32-9 bis(2-chloroisopropyl)Ether 10. U 86-73-7 Fluorene 10.U106-44-5 4-flethylphenol 10.U lflfl-01-6 4-Nitroaniline 50.U621-64-7 N-Nitroso-Oi-n-Propyla«ine 10. U 534-52-1 4,6-Dinitro-2-Methylphenol 50. U67-72-1 Hexachloroethane 10. U 86-30-6 N-Nitrososdiphenyiamine (1) 10. U93-95-3 Nitrobenzene 10.U 101-55-3 4-Bromophenyl-phenylether 10. U78-59-1 Isophorone 10. U 118-74-1 Hexachlorcbenzene 13. U93-75-5 2-Nitrophenol 10. U 87-86-5 Pentachlorophenol Ifl.U105-67-9 2,4-Dimethylphenoi 10. U 85-01-8 Phenanthrene 10. U65-85-0 Benzoic Acid 50. U 120-12-7 Anthracene 10. U111-91-1 bis<-2-Chloroethoxy)f1ethane 10. U 84-74-2 Di-n-Butylphthalate 10. U120-83-2 2,4-Dichlorophenol 10. U 206-44-0 Fluoranthene 10. U120-82-1 1,2,4-Trichlorobenzene Ifl.U 129-00-0 Pyrene Ifl.U91-20-3 Naphthalene 10. U 85-68-7 Butylbenzylphthalate 10.U106-47-8 4-Chloroaniline Ifl.U 1-94-1 3,3'-Oichlorobenzidine 20. U87-68-3 Hexachlorobutadiene Ifl.U 56-55-3 Benzo(a)Anthracene Ifl.U59-50-7 4-Chloro-3-Methylphenol 10,U 117-81-7 bis(2-Ethylhexyl)Phthalate Ifl.U91-57-6 2-rtethylnephthalene 10.U 218-01-9 Chrysene 10.U77-47-4 Hexachlorocyclopentadiene Ifl.U 117-84-0 Di-n-Octyl Phthalate 10. U38-06-2 2,4,6-Trichlorophenol Ifl.U - 205-99-2 Benzo(b)Fluoranthene 10.U95-95-4 2,4,5-Trichlorophenol 50. U 207-08-9 Benzo(k)Fluoranthene •••91-58-7 2-Chloronaphthalene 10. U 50-32-8 Benzo(a)Pyrene Ifl.U88-74-4 2-Nitroaniline 50.U 193-39-5 Indeno(l,2,3-cd)Pyrene 10.U131-11-3 Dimethyl Phthalate 10.U 53-70-3 Dibenzo(a,h)ftnthracene Ifl.U208-96-8 Acenaphthylene 10. U 191-24-2 Benzo(g,h,i)Perylene 10.U99-09-2 3-Nitroaniline 50.U 92-87-5 Benzidine 20.U

(l)-Cannot be separated froa diphenylanine ARI00036•••-Cannot be separated froa Benzo(b)FIuoranthene

ST/VT/o *> -13L oTLab Name : Bridgeport Environmental; Inc. I Sample Number ICase No : N/A I £4706 I

ORGANICS ANALYSIS DATA SHEET *____(Page 3)

Peaticides/PCBs

Concentration: (tpy tedium ( Circle One ) GPC Cleanup _ Yea _f NoDate Extracted/Prepared! 8/27/90 Separatory Funnel Extraction .YesDate Analyzed: 9/06/90 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor: 100al_/5§LPercent Moisture: N/A

C.A.S.Nunber ug/Kg

319-84-6 Alpha-BHC. ....... 0.25 U319-87-7 Beta-BHC , . . . , , . . 0.25 U319-86-8 Oelta-BHC. ....... 0.25 U58-89-9 Ganma-BHC (Lindane). . . 0.25 U76-44-8 Heptachlor ....... 0.25 U309-00-2 Aldrin ......... 0.25 U1024-57-3 Heptachlor Epoxide . . . 0.25 U959-98-8 Endosulfan I ...... 0.25 U60-57-1 Dieldrin ........ 0.25 U72-55-9 4,4'-DDE ........ 0.25 U72-20-8 Endrin ......... 0.25 U

33213-65-9 Endosulfan II. ..... 0.50 U72-54-8 4,4'-DDD ........ 0.50 U

1031-07-8 Endosulfan Sulfate . . . 0.50 U50-29-3 4,4'-DDT ........ 0.50 U72-43-5 flethoxychlor ...... 13 U


8001-35-2 Toxaphene. ....... 25 U12674-11-2 Arochlor-1016. ..... 13 U11104-28-2 Arochlor-1221. ..... 13 U11141-16-5 Arochlor-1232. ..... 13 U53469-21-9 Arochlor-1242* ..... 13 U12672-29-6 Arochlor-1248. ..... 13 U11097-69-1 Arochlor-1254. ..... 13 U11096-82-5 Arochlor-1260. ..... 13 U

Fora 1 7/85

~ CERTIFICATE OF ANALYSIS

PRIORITY POLLUTANT

ANALYSIS NO. E 4713




#

Antimony 0.13 N.D.

Arsenic 0.13 4.18

Beryllium 0.25 1.02

Cadmium 0.25 4.31

Chromium 0.25 71.8

Copper 0.25 144

Lead 1.3 411

Mercury 0.05 0.16

Nickel 2.5 38.2

Selenium 0.13 0.36

Silver 0.25 N.D.

Thallium 2.5 N.D.

Zinc 0.25 493

Cyanide 0.10 1*05

ARI00038'


ORGANICS ANALYSIS DATA SHEET + ——— - ———— *(Page 2)

Semi volatile Compounds

Concentration: QUjjX Medium (Circle One ) 6PC Cleanup _ Yes _ NoDate Extracted: T/28/90 Separatory Funnel Extraction __ VesDate Analyzed: 09/08/9022:11 Continuous Liquid-Liquid Extraction _ YesConc/Dil Factor: 30G;lmlPercent Moisture: 55.0 ~~*\ ^ %.

ug/L on^g/KoX C.A.S. ug/L^rug/Kg )Nunber (Circle Srfrr Number (Circle Orwt

1C3-95-2 Phenol 730.U 83-32-9 Acenaphthene 150.J111-44-4 •bis(-2-Chloroethyl)Ether 730.U 51-28-5 2,4-Dinitrophenol 3600.U95-?7-8 2-Chlorophenol 730.U 100-02-7 4-Nitrophenol 3600.U541-73-1 1,3-Dichlorobenzene 730.U 132-64-9 Dibenzofuran 730.U106-46-7 1,4-Oichlorobenzene 730,U 121-14-2 2,4-Dinitrotoluene 730.U100-51-6 Benzyl Alcohol 730.U 606-20-2 2,6-Oinitrotoluene 730.U95-50-1 1,2-Dichlorobenzene O.U 84-66-2 Diethylphthalate 730.U

^ 95-48-7 2-Methylphenol 730.U 7005-72-3 4-Chlorophenyi-phenlyether 730.U39638-32-9 bis(2-chloroisopropyl)Ether 730.U 86-73-7 Fluorene 730.U1Q6-44-5 4-Ptethylphenol 730.U 100-01-6 4-Nitroaniline 3600.U621-64-7 N-Nitroso-Di-n-Propyiamine 730.U 534-52-1 4,6-Oinitro-2-Hethylphenol 3600.U67-72-1 Hexachloroethane 730.U 86-30-6 N-Nitrososdiphenylamine (1) 730.U98-95-? Nitrobenzene 730.U 101-55-3 4-Broinophenyl-phenylether 730.U78-59-1 Isophorone 730.U 118-74-1 Hexachlorobenzene 730.U99-75-5 2-Nitrophenol 730.U 87-86-5 Pentachlorophenol J6DO.U105-67-9 2,4-Diaiethylphenol 730,U 85-01-8 Phenanthrene 380.J•5-85-0 Benzoic Acid 3600.U 120-12-7 Anthracene 730.U111-91-1 bis(-2-Chloroethoxy)Hethane 730.U 84-74-2 Di-n-Butylphthalate 730.U123-83-2 2,4-Oichlorophenol 730.U 206-44-0 Fluoranthene 1200. '120-82-1 1,2,4-Trichiorobenzene 730.U 129-00-0 Pyrene 2300.91-20-3 Naphthalene 240.3 85-68-7 Butylbenzylphthalate 730,U

106-47-8 4-Chloroaniline 730.U 1-94-1 3,3'-Dichlorobenzidine 1500.U97-68-3 Hexachlorobutadiene 730.U 56-55-3 Benzo(a)Anthracene 720.359.50-7 4-Chloro-3-nethylphenol 730.U 117-81-7 bia(2-Ethylhexyi)Phthaiate 4300.91-57-6 2-Hethylnaphthalene 130.3 218-01-9 Chrysene 820.77-47-4 Hexachlorocyclopentadiene 730.U 117-84-0 Di-n-Octyl Phthalate 500.J98-06-2 2,4,6-TrichIorcphenol 730.U 205-99-2 Benzo(b)Fluoranthene 690.J95-95-4 2,4,5-Trichlorophenol 3600.U 207-08-9 Benzo(k)Fluoranthene »««»91-58-7 2-ChIoronaphthalene 730.U 50-32-8 Benzola)Pyrene 590.338-74-4 2-Nitroaniline 3600.U 193-39-5 Indeno(l,2,3-cd)Pyrene 73Q.U

131-11-3 Dimethyl Phthalate 730.U 53-70-3 Dibenzo(a,h)Anthracene 730.U208-96-8 Acenaphthylene 730.U 191-24-2 Benzotg^jiJPerylene 730.U


(l)-Cannot be separated from diphenylanine B D . n nflnIUU039

»»*-Cannot be separated from Benzo(b)Fluoranthene

Lab Name : Bridgeport Environmental, Inc. I Sample NumberCase No : N/A I E4713

ORGANICS ANALYSIS DATA SHEET *————(Pace 3)

Pesticides/PCBs

Concentration; / 'Loi£ , Hediun ( Circle One ) GPC Cleanup _ Yea _^Date Extracted/Prepared: 8/27/90 Scparatory Funnel Extraction _ YesData Analyzed: 9/10/90 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor: 10.02g/10mlsPercent Moisture: 99.0

C.A.S. ug/L orNunber

319-84-6 AIphe-BHC. ....... 20.0 U319-87-7 Beta-BHC ........ 20.0 UH9-86-8 Delta-BHC. ....... 20.0 U98-89-9 Gasuna-BHC (Lindane). . . 20.0 U76-44-8 Heptachlor ....... 20.0 U309-00-2 Aldrin ......... 20.0 U1024-97-3 Heptachlor Epoxide . . . 20.0 U999-98-8 Endcsulfan I ...... 20.0 U60-97-1 Dieldrin ........ 20. fl U72-99-9 4,4'-DOE ........ 20.0 U72-20-8 Endrin ......... 20.0 U

33213-69-9 EndosuUan II. ..... 40.0 U72-54-8 4,4'-DDO ........ 40.0 U

1031-07-8 Endosulfan Sulfate . . . 40.0 U50-29-3 4,4'-DDT ........ 40.0 U72-43-5 dethoxychior ...... 1000 U



Fon 1 7/89

,ARIOOOl»0

M -t Saocle Number I

JJrganics Analysis Data Sheet I E472Q I(Page 1) *- —————— ----+

Laboratory Name: Bridgeport Environmental, Inc. Case No.: N/ALab Sample ID: >B9406::D2 X Report No.:Sample Matrix: WATER /^ 0/0 A Contract No.: N/AData release Authorized by: f\^ U k t J A.3 *\ » U/A Date Sample Received:24 AUG 90

Uolatile CompouncConcentration: (Lojt/ Medium (Circle One )Date Extracted:Date Analyzed: 08/27/90 21:02Conc/Dil factor: 1 pH :Percent flpjsture:

C.A.S. /Cg/fir ug/kg C.A.S. (ug/bor ug/kgNumber TCTrcle One) Number lUTrcle One)

74-87-3 Chloromethane 10. U 78-87-5 1,2-Dichloropropane 5, U-74-85-9 Sromomethane 10. U 10061-02-6 Trans-1.3-Dichloropropene 5. U75-01-4 iJinyl Chloride 10. U 79-01-6 Trichloroethene 5. U75-00-3 Chloroethane 10. U 124-48-1 Dibromochloromethane 5. U75-09-2 rtcthylene Chloride 20. 6 79-00-5 1,1.2-Trichloroethane 5. U67-64-1 Acetone 10. U 71-43-2 Benzene 5. U107-02-8 Acrolein 50. U 10061-01-5 cis-l,3-Dichloropropene 5. U167-13-1 Acrylonitrile 50. U 110-75-8 2-Chloroethylvinylether 10. U75-15-0 Carbon Disulfide 10. U 75-25-2 Bromoforn ' ' 5. U

j 75-35-4 1,1-Dichloroethene 5. U 108-10-1 4-Methyi-2-Pentanone 10. U^ 75-34-3 1,1-Dichloroethane 5. U 591-78-6 2-Hexanone 10. U

156-60-5 Trans-1.2-Dichlotoethene 5. U 127-18-4 Tetrachloroethene 5. U67-66-3 Chloroform 3. J 79-34-5 1,1,2,2-TetracnIoroethane 5. U107-06-2 1,2-Dichloroethane 5. U 108-88-3 Toluene 5. U78-93-3 2-Butsnone 10. U 108-90-7 Chlorobenzena 5. U71-55-6 1.1,1-Trichloroethane 5. U 100-41-4 Ethylbenzene 5. U56-23-6 Carbon Tetrachloride 5. U 100-42-5 Styrene 5. U108-05-4 Uinyi Acetate 10. U Total Xylenes 5. U" 5-27-4 SromooichloroBethanB 5. U Total Dichlorobenzenes 5. U

Data Reporting QualifiersFor resorting results to EPA the following results qualifiers are used. Additional flags or footnotesexplaining results are encouraged. However the definition of each flag must be explicit.

Value - If the result is a value greater than or equal to C - This flag applies to pesticide parameters wherethe detection limit, report the value. the identification has been confirmed by GC/tlS.

U - Indicates compound was analyzed for but not detected. Single component pesticides >- 10 ng/uL in theReport the mnimun detection linit for the sample with final extract should be confirmed by GC/MS.the U (e.g. 10U) based on necessary concentration/dil- B - This flag is used when the analyte is found injtion action (This is not necessarily the instrument the blank as well as a sample. It indicatesdetection limit). The footnote should read: U-Coapound possible/probable blank contamination and warnswas analyzed for but not detected. The number is the data the user to take appropriate action.mininun attainable detection limit for the sample. Other - Other specific flags and footnotes may be

J - Indicates an estimated value. This flag is used either required to properly define the results. Ifwhen estimating a concentration for tentatively identified used, they must be fully described and suchcompounds where a 1:1 response is assumed or when the mass description attached to the data summary report

_^ spectral data indicated the presence of a compound thatmeets the identification criteria but the result is < than OPTIONAL FLAGSthe specified detection liaut but > than zero , _(e.g. 10J). If liait of detection is 10 ug/L and a N - CompouniAiR IrQe^Qnl^aflibration File.conentration of 3.0 ug/L is calculated, report as 3J.

Fore 1 7/85

I Sample Number IOrganics Analysis Data Sheet I E4727 I

* (Page!) » ————— ——— +Laboratory Name: Bridgeport Environmental, Inc. Case No.: N/ALab Sample ID: >A8903::D1 - QC Report No.:Sample Hatrix: SOIL jQ U I •* 0 * Contract No.: N/AData release Authorized by: ' Cv. tX SlA A. LJ *vy*s X Date Sample Received: 24 AUG 90

Volatile CompoundsConcentration: t wy tledium (Circle One )Date Extracted:Date Analyzed: 08/29/90 18:49Cone/Oil factor: 1 pH :Percent Moisture: 50. 4X

C.A.S. ug/1 oMjg/fo C.A.S. ug/lNumber (Circle UneT Number (Circle

74-87-5 Chloromethane 20. U 78-87-5 1,2-Dichloropropane 10. U74-83-9 Bromomethane 20. U 10061-02-6 Trans-1,3-Dichloropropene 10. U75-01-4 Uinyl Chloride 20. U 79-01-6 Trichloroethene 10. U79-00-3 Chloroethane 20. U 124-48-1 Dibromochloronethane 10. U75-09-2 Methylene Chloride 8. B,J 79-00-5 1,1,2-TrichIoroethane 10. U67-64-1 Acetone 26. B 71-43-2 Benzene 10. U107-02-8 Acrolein 100. U 10061-01-5 cis-l,3-0ichloropropene 10. U167-13-1 Acrylonitrile 100. U 110-75-8 2-CMoroethylvinylether 20. U

**- 75-15-0 Carbon Disulfide 200. 75-25-2 Bromoform 10. U75-35-4 1,1-Dichloroathene 10. U 108-10-1 4-hethyl-2-Pentanone 20. U75-34-3 1,1-Dichloroethane 10. U 591-78-6 2-Hexanone 20. U156-60-5 Trans-l,2-Dichlotoethene 10. U 127-18-4 Tetrachloroethene 10. U67-66-3 Chloroform 10. U 79-34-5 1,1,2,2-Tetrachloroethane 10. U107-06-2 1,2-Dichloroethane 10. U 108-88-3 Toluene 10. U78-93-3 2-8utanone 20. U 108-90-7 Chlorobenzene 10. U71-55-6 1,1,1-Trichloroethane 10. U 100-41-4 Ethylbenzene 5. J56-23-6 Carbon Tetrachloride 10. U 100-42-5 Styrene 10. U108-05-4 Uinyl Acetate 20. U - Total Xylenes 14.75-27-4 Bromodichloromethane 10. U Total Dichlorobenzenes 10. U

Data Reporting QualifiersFor reporting results to £PA the following results qualifiers are used. Additional flags or footnotesexplaining results are encouraged. However the definition of each flag must be explicit.

Ualue - If the result is a value greater than or equal to C - This flag applies to pesticide parameters wherethe detection limit, report the value. the identification has been confirmed by GC/HS.

U - Indicates compound was analyzed for but not detected. Single component pesticides >• 10 ng/uL in theReport the minimum detection limit for the sample with final extract should be confirmed by GC/ttS.the U (e.g. 10U) based on necessary concentration/dil- B - This flag is used when the analyta is found inution action (This is not necessarily the instrument the blank as well as a sample. It indicatesdetection limit). The footnote should read: U-Compound possible/probable blank contamination and warnswas analyzed for but not detected. The number is the data the user to take appropriate action.minimum attainable detection limit for the sample. Other - Other specific flags and footnotes may be

J - Indicates an estimated value. This flag is used either required to properly define the results. Ifwhen estimating a concentration for tentatively identified used, they must be fully described and suchcompounds where a 1:1 response is assumed or when the mass description attached to the data summary reportspectral data indicated the presence of a compound thatmeets the identification criteria but the result is < than OPTIONAL FLAGSthe specified detection limit but > than zero(e.g. 10J). If limit of detection is 10 ug/L and a N - Compound not present in Calibration File.conentration of 3.0 ug/L is calculated, report as 3J. A R I 0 0 0 2

Form 1 7/85

5CERTIFICATE OF ANALYSIS

PRIORITY POLLUTANT

ANALYSIS NO: E 4700




Antimony 0.005 N.D.

Arsenic 0.005 N.D.

Beryllium 0.01 N.D.

Cadmium 0.01 N.D.

Chromium 0.01 0.01

Copper 0.01 0.05

Lead 0.05 N.D.

Mercury 0.0005 N.D.

Nickel 0.05 N.D.

Selenium 0.005 N.D.

Silver 0.01 N.D.

Thallium 0.10 N.D.

Zinc 0.01 0.09

Cyanide 0.01 N.D.

10001*3

Lab Name : Uastex Ind. of NJ I Sample NumberCase No : N/A I £4707

QRGAWCS ANALYSIS DATA SHEET +-- ———(Page 2)

Setivolatile Compounds

Concentration^ .Loic/ Hediua (Circle One ) KC Cleanup _ Yes _ NoDate Extracted! 08/28/90 Separatory Funnel Extraction _ YesDate Analyzed: 09/08/90 14:45 Continuous Liquid-Liquid Extraction _ YesConc/Dil Factor! 1000: 1mlPercent Moisture: NA

C.A.S. f ugA^ir ug/Kg C.A.S. V ug/L )r ug/KgNumber ^ Circle One) Number ^ irrtfie One)

15B-95-2 Phenol 10.U 83-32-9 Acenaphthene 10.Ui11-44-4 bis(-2-Chloroethyl)Ether 10.U • 51-28-5 2,4-Dinitrophenol 59.U05.57-8 2-Chlorophenol 10.U 100-02-7 4-Nitrophenol 50.U541-73-1 1,3-Dichlorobenzene 10.U 132-64-9 Dibenzofuran Ifl.U106-46-7 1,4-Dichlorobenzene 10.U 121-14-2 2,4-Dinitrotoiuene 10.U100-51-6 Benzyl Alcohol 10.U 606-20-2 2,6-Dinitrotoluene 10.U95-50-1 1,2-Oichlorobenzene 10.U 84-66-2 Diethylphthalate 10.U95-48-7 2-Hethylphenol 10.U 7005-72-3 4-ChIorophenyl-phenlyether Ifl.U

39638-32-9 bis(2-chloroisopropyl)Ether 10.U 86-73-7 Fluorene 10.U106-44-5 4-flethylphenol 10.U 100-01-6 4-NitroaniHne 50.U621-64-7 N-Nitroso-Oi-n-Propylamine 10.U 534-52-1 4,6-Dinitro-2-nethylphenol 50.U67-72-1 Hexachloroethane 10.U 86-30-6 N-Nitrososdiphenylatnine (1) 10.U°8-95-3 Nitrobenzene 10.U 101-55-3 4-Bromophenyl-phenylether 10.U73-59-1 Isophorone . 10.U 118-74-1 Hexachlorobenzene 10.U99-75-5 2-Nitrophenol 10.U 87-86-5 Pentachlorophenol 50.U105-67-9 2,4-Oimethylphenol 10.U 85-01-8 Phenanthrene 10.U65-85-0 Senzoic Acid 50.U 120-12-7 Anthracene Ifl.U111-91-1 bis(-2-Chloroethoxy)nethane 10.U 84-74-2 Di-n-Butylphthalate Ifl.U120-83-2 2,4-Dichlorophenol 10.U 206-44-0 Fluoranthene 10.U120-82-1 1,2,4-Trichlorobenzene 10.U 129-00-0 Pyrene 10.U91-20-3 Naphthalene 10.U 85-68-7 Butylbenzyiphthalate 10.U106-47-8 4-Chloroaniline Ifl.U 1-94-1 3,3'-Dichlorobenzidine 20.U87-68-3 Hexechlorobutadiene 10.U 56-55-3 Benzo(a)Anthracene 10.U59-50-7 4-Chloro-3-Methylphenol 10.U 117-81-7 bis(2-Ethylhexyl)Phthalate 5.J91-57-6 2-flethylnaphthalene 10.U 218-01-9 Chrysene 10.U77-47-4 Hexachlorocyclopentadiene Ifl.U 117-84-0 Di-n-Octyl Phthalate Ifl.U88-06-2 2,4,6-Trichlorcphenol 10.U 205-99-2 Benzo(b)Fluoranthene Ifl.U95-95-4 2,4,5-Trichlorophenol 5fl.U 207-08-9 Benzo(k)Fluoranthene **«91-58-7 2-Chloronaphthalene 10.U 50-32-8 Benzo(a)Pyrene Ifl.U68-74-4 2-Nitroaniline 50.U 193-39-5 lndeno(l,2,3-cd)Pyrene Ifl.U131-11-3 Dimethyl Phthalate 10.U 53-70-3 Dibenzo(a,h)Anthracene 10.U208-96-8 Acenaphthylene 10.U 191-24-2 Benzo(g,h,i)Perylene Ifl.U99-09-2 3-Nitroaniline 50.U 92-87-5 Benzidine 20.U

(l)-Cannot be separated from diphenylamine A R 1 0 0 0

***-Cannot be separated froii Benzo(b)Fluoranthene

-nay+_.**._....._——+

Lab Name : Bridgeport Environmental, Inc. I Sample Number ICase No : N/A _ I E4707 I

ORGANICS ANALYSIS DATA SHEET *-————————*(Page 3)

Pesticides/PCBs

Concentration: (Low . tedium ( Circle One ) GPC Cleanup _ Yea _L NoDate Extracted/Prepared: 8/27/90 Separetory Funnel Extraction _ YesDate Analyzed: 9/06/90 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor: lQOnL/5iLPercent Moisture: N/A

C.fl.S.Nunber ug/Kg

319-84-6 Alpha-BHC. ....... 0.25 U319-87-7 Beta-BHC ........ 0.25 U319-86-8 Delta-BHC. ....... 0.2? U98-89-9 Gawna-BHC (Lindane). . . 0.25 U76-44-8 Heptachlor ....... 0.25 U309-00-2 Aldrin ......... 0.25 U1024-57-3 Heptachlor Epoxide . . . 0.25 U959-98-8 Endosulfan I ...... 0.25 U60-57-1 Dietdrin ........ 0.25 U72-55-9 4,4'-DDE ........ 0.25 U72-20-8 Endrin ......... 0.25 U

332U-65-9 Endosulfan U. ..... 0.50 U72-54-8 4,4'-ODD ........ 0.50 U

1031-07-8 Endosulfan Sulfate . . . 0.50 U50-29-3 4J4'-DOT ........ 0.50 U72-43-5 Kethoxychlor ...... 13 U


B001-35-2 Toxaphene. ....... 25 U12674-11-2 Arochlor-1016. ..... 13 U11104-28-2 Arochlor-1221. ..... 13 U11141-16-5 Arochlor-1232. ..... 13 U53469-21-9 Arochlor-1242. ..... 13 U12672-29-6 Arochlor-1248. ..... 13 U11097-69-1 Arochlor-1254. ..... 13 U11096-82-5 Arochlor-1260. ..... 13 U

Forn 1 7/85

AR I 0001*5,


PRIORITY POLLUTANT

ANALYSIS NO. E 4714




Antimony 0.13 H-D-

Arsenic 0.13 6-88

Beryllium 0.25 N-D-

ffa/ltffitim • 0.25 J«J/

Chromium 0.25 *9'2

Copper 0.25 127

Lead 1.3 213

Mercury 0.05 • '

Nickel 2.5 32-9

Selenium 0.13 N'D'

Silver 0.25 N'D'

Thallium 2.5

Zinc 0.25 52°1.12

Cyanide 0.10

Lab Name : Bridgeport Environmental, Inc. I Sample NumberCase No : N/A I E4714

ORGANICS ANALYSIS DATA SHEET *—————(Page 2)

Senivolatile Compounds/ T\Concentration: ( Lpu> Medium (Circle One ) EPC Cleanup _ Yes _ No

Date Extracted: 3758/90 Separatory Funnel Extraction _ YesDate Analyzed: 09/07/90 19:19 Continuous Liquid-Liquid Extraction _ YesConc/Dil Factor! 30G:U1 1:2Percent Moisture'. 64.4 s*~*\

ug/L orfug/Ko) C.A.S. ug/L oAig/KeNumber (Circle mr^ Number (Circlr

108-95-2 Phenol 19QQ.U 83-32-9 Acenaphthene 1900.U111-44-4 bis(-2-Chloroethyl)Ether 1900.U 51-28-5 2,4-Dinitrophenol 9000.U95-57-8 2-Chlorophenol 1900.U 100-02-7 4-Nitrophenoi 9000.U541-73-1 1,3-Dichlorobenzene 1900,U 132-64-9 Oibenzofuran 1900.U106-46-7 1,4-Oichlorobenzene 1900.U 121-14-2 2,4-Dinitrotoluene 1900.U100-51-6 Benzyl Alcohol 1900.U 606-20-2 2,6-Dinitrotoluene 1900.U95-50-1 1,2-Oichlorooenzene 1900.U 84-66-2 Diethyiphthalate 1900.U

J 95-48-7 2-rtethylphenol 19QO.U 7005-72-3 4-Chlorophenyl-phenlyether 1900.U39638-32-9 bis(2-chloroisopropyl)Ether 1900.U 86-73-7 Fluorene 1900.U106-44-5 4-Methylphenoi 1900.U 100-01-6 4-Nitroaniline 90QQ.U621-64-7 N-Nitroso-Di-n-Propylamine 1900.U 534-52-1 4,6-Dinitro-2-(1ethylphenol 9000.U67-72-1 Hexachloroethane 1900.U 86-30-6 N-Nitrososdiphenylamine (1) 1900.U98-95-3 Nitrobenzene 1900.U 101-55-3 4-Bromophenyl-phenylether 1900.U73-59-1 Isophorone 1900.U 118-74-1 Hexachlorobenzene 1900.U38-75-5 2-Nitrophenol 1900.U 87-86-5 Pentachlorophenol 9000.U1Q5-67-9 2,4-Oimethylphenol 1900.U 85-01-8 Phenanthrene 370.J65-85-0 Benzoic Acid 9000.U 120-12-7 Anthracene 1900.U111-91-1 bis(-2-Chloroethoxy)r1ethane 1900.U 84-74-2 Oi-n-Butylphthalate 1900.U120-83-2 2,4-Oichlorophenol 1900.U 206-44-0 Fluoranthene 540.J120-82-1 1,2,4-Trichlorobenzene 1900.U 129-00-0 Pyrene 1900.U91-20-3 Naphthalene 19QQ.U 85-68-7 Butylbenzylphthalate 1900.U

106-47-8 4-Chloroaniline 1900.U 1-94-1 3,3'-Dichiorobenzidine 3800.U37-68-3 HexBchlorobutadiene 1900.U 56-55-3 Benzo(a)Anthracene 350.J59-50-7 4-Cnloro-3-Hethylphenol 1900.U 117-81-7 bis(2-EthyIhexyl)Phthalate 1800.J91-57-6 2-rtethyinaphthalene 1900.U 218-01-9 Chrysene 19QO.U77-47-4 Hexachlorocyclopentadiene 1900.U 117-84-0 Di-n-Octyl Phthalate 1900.U98-06-2 2,4,6-Trichlorophenol 1900.U 205-99-2 Benzo(b)FIuoranthene 1900.U95-95-4 2,4,5-Trichlorophenol . 9000.U 207-08-9 Benzo(k)Fluoranthene »«*•91-58-7 2-Chloronaphthalene 1900.U 50-32-8 Benzo(a)Pyrene 1900.U88-74-4 2-Nitroaniline 9000.U 193-39-5 Indeno(l,2,3-cd)Pyrene 1900.U

131-11-3 Dimethyl Phthalate 1900.U 53-70-3 Dibenzo(a,h»Anthracene 1900.U2D8-96-8 Acenaphthylene 1900.U 191-24-2 Benzo(g,h,i)Perylene 1900.U99-09-2 3-Nitroaniline 9000.U 92-87-5 Benzidine 3800.U

(l)-Cannot be separated from diphenylamine "** ' OQQif J

•••-Cannot be separated from Benzo(b)Fluoranthene

*....Lab Name : Bridgeport Environmental, Inc. I Sample NumberCase No : N/A I £4714

QRGAWCS ANALYSIS DATA S*€ET +•(Page3)

Pesticides/PCBs

Concentration: (low ' ttediut ( Circle One ) GPC Cleanup _ Yes _^NoDate Extracted/Prepared: 8/27/90 Separatory Funnel Extraction _ YesDate Analyzed: 9/11/90 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor: IQ.OQg/lOmlsPercent Moisture: 64.4

C.A.S. ug/L orNutber /tig/Kg "•"*

319-64-6 Alpha-BHC. ....... JO. 0 U319-87-7 Beta-BHC ........ 30.0 U319-86-8 Delta-BHC. ....... 30.0 U58-89-9 Gamu-BHC (Lindane). . . 30.0 U76-44-8 Heptachlor ....... 30.0 U309-00-2 Aldrin ......... 30.0 U1024-57-3 Heptachlor Epoxide ... 30.0 U999-98-6 Endosulfan I ...... 30.0 U

I j 60-57-1 Dieldrin ........ 750^ 72-55-9 4,4'-DDE ........ 76

72-20-8 Endrin ......... 30.0 U33213-65-9 Endosulfan U. ..... 60.0 U

72-54-8 4,4'-DDO ........ 14001031-07-8 Endosulfan Sulfate . . . 60.0 U50-29-3 4,4'-DDT ........ 270072-43-5 Methoxychlor ...... 1500 U


8001-35-2 Toxaphene. ....... 3000 U12674-11-2 Arochlor-1016. ..... 1500 U11104-26-2 Arochlor-1221. ..... 1500 U11141-16-5 Arochlor-1232. ..... 1500 U53469-21-9 ArochIor-1242. ..... 1500 U12672-29-6 Arochlor-1248. ..... 1500 U11097-69-1 Arochlor-1254. ..... 1500 U11096-62-5 Arochlor-1260. ..... 1500 U

Fort 1 7/85

ARIOOOii8

STAT/OA;i Sample Number 1

J]rganics Analysis Data Sheet I £4721 I(Page 1) *—————————*

Laboratory Name: Bridgeport Environmental, Inc. Case No.: N/ALab Sample 10: >B9407::D2 . QC Reoort No.:Sample Matrix: WATER jQ fl i J Contract No.: N/AData release Authorized by: f K L* Ml> £j" XUA<*f Date Sample Received:24 AUG 90

Uolatila CoamoundsConcentration: ("Lguy Medium (Circle One )Date Extracted:Date Analyzed: 08/27/90 21:51Cone/Oil factor: 1 pH iPercent ftawture:

C.A.S. ^jg/lyor ug/kg C.A.S. iig/l/or ug/kgNumber Turcle One) Number fCTrcle One)

74-87-5 Chloromethane . 10. U 78-87-5 1,2-Dichioropropane 5. U74-83-9 Sromomethane 10. U 10061-02-6 Trsns-1.3-Dichloropropene 5. u75-01-4 Uinyi Chloride ID. U 79-01-6 Trichioroethene 5. U."5-30-3 Chloroethane 10. U 124-48-1 Dibromochloromethane 4. j75-09-2 Methylene Chloride 13. 6 79-00-5 1,1,2-Trichioroethane 5. U67-64-1 ficetone 10. U 71-43-2 Benzene 5, U107-02-8 Acrolein 50. U 10061-01-5 cis-l,3-Dichloropropene 5. U167-13-1 Acrylonitrile 50. U 110-75-8 2-ChloroethyIvinylether 10. J75-15-0 Carbon Oisulfide 10. U 75-25-2 Bromoform ' 5. U

, 75-35-4 1,1-Dichloroethena 5. U IflB-lfl-l 4-Hethyl-2-Pentanone 10. U•^ 75-34-3 1.1-Dichioroethane 5. U 591-78-6 2-Hexanone 10. U

156-60-5 Trans-1.2-Dichlotoethene 5. U 127-18-4 Tetrachloroethene 5. Uo7-66-3 Chloroform 30. 79-34-5 1,1,2,2-Tetrachloroethane 5. U107-06-2 1,2-Dichloroethane 5. U 108-88-3 Toluene 5. U78-93-3 2-Butanone 10. U 108-90-7 Chlorobenzene 5. U71-55-6 1.1,1-Trichloroethane 5. U 100-41-4 Ethylbenzene 5. U56-23-6 Carbon Tetrachionde 5. U 100-42-5 Styrene 5. U138-05-4 Oinyl Acetate 10. U Total Xylenes 5. d75-27-4 Bromodichloromethane 14, Total Dichlorobenzenes ?, U

Data Reporting QualifiersFor reporting results to ERA the following results qualifiers are used. Additional flags or footnotesexplaining results are encouraged. However the definition of each flag must be explicit.

Value - If the result is a value greater than or equal to C - This flag applies to pesticide parameters unerethe detection limit, report the value. the identification has oeen confirmed by QC/MS.

U - Indicates compound was analyzed for but not detected. Single component pesticides >• 10 ng/uL in theReport the minimus detection limit for the sample with final extract should be confirmed by GC/HS.the U (e.g. 10U) based on necessary concentration/dil- B - This flag is used when the analyte is found inution action (This is not necessarily the instrument the blank as well as a sample, 'it indicatesdetection limit). The footnote should read: U-Coapound possible/probable blank contamination and warnswas analyzed for but not detected. The number is the data the user to take appropriate action.minimum attainable detection limit for the sample. Other - Other specific flags and footnotes may be

J - Indicates an estimated value. This flag is used either required to properly define the results. Ifwhen estimating a concentration for tentatively identified used, they must be fully described and suchcompounds where a 1:1 response is assumed or when the mass description attached to the data summary report

_^ spectral data indicated the presence of a compound thatmeets the identification criteria but the result is < than OPTIONAL FLAGSthe specified detection limit but > then zero(e.g. 10J). If linit of detection is 10 ug/L and a N - Compound not present in Calibration File.conentration of 3.0 ug/L is calculated, report as 3J.

For. lUR I 0001*9 7/85

I Sample Number IOrganic* Analysis Data Sheet I E4728 I

(Page 1) *————————+Laboratory Name: Bridgeport Environmental, Inc. Case No.: N/ALab Sample ID: >A8904::01 QC Report No.JSanple Matrix: SOIL >O fl . O « Contract No.: N/AData release Authorized by: I lSC<JyHl>.«/ 6*J ' yv cA- Oats Sample Received: 24 AUG 90

volatile CompoundsConcentration: (toy> Medium (Circle One )Date Extracted:Date Analyzed: 08/29/90 19:33Cone/Oil factor: 1 pH :Percent Moisture: 38.7%

C.A.S. , ug/1 or Ag C.A.S. ug/l orNumber (Circle One) Number (Circle tFeT

74-87-3 Chloromethana 16. U 78-87-9 1,2-Dichloropropane 8. U74-83-9 Bromoaethane 16. U 10061-02-6 Trans-l,3-Dichloropropene 8. U75-01-4 Uinyl Chloride 16. U 79-01-6 Trichloroethene 8. U79-00-3 Chloroethane 16. U 124-48-1 Dibromochlorofnethane 8. U75-09-2 rtethylene Chloride 8. B 79-00-5 1,1,2-Trichloroethane 8. U67-64-1 Acetone 74. B 71-43-2 Benzene 8. U107-02-8 Acrolein 82. U 10061-01-5 cis-l,3-Dichloropropene 8. U167-13-1 Acrylonitnie 82. U llfl-75-B 2-Chloroethylvinylether 16. U75-15-0 Carbon Disulfide 140. 75-25-2 Bromoform 8. U75-35-4 1,1-Dichloroethene 8. U 108-10-1 4-Hethyl-2-Pentanone 16. U75-34-3 1,1-Dichloroethane 8. U 591-78-6 2-Hexanone 16. U156-60-5 Trans-l,2-Dichlotoathene 8. U 127-16-4 Tetrachloroethene 8. U67-66-3 Chloroform 8. U 79-34-5 1,1,2,2-Tetrachloroethane 8. U107-06-2 1,2-Dichloroethane 6. U 108-88-3 Toluene 8. U78-93-3 2-Butanone 16. U 108-90-7 Chlorobenzene 8. U71-55-6 1,1,1-Trichloroethane 8. U 100-41-4 Ethylbenzene 8. U56-23-6 Carbon Tetrachioride 8. U 100-42-5 Styrene 8. U108-05-4 Uinyl Acetate 16. U Total Xylenes 8. U75-27-4 BromodichloroniBthane 8. U Total Dichlorobenzenes 9. U

Data Reporting QualifiersFor reporting results to ERA the following results qualifiers are used. Additional flags or footnotesexplaining results are encouraged. However the definition of each flag must be explicit.

value - If the result is a value greater than or equal to C - This flag applies to pesticide parameters wherethe detection limit, report the value. the identification has been confirmed by GC/tlS.

U - Indicates compound was analyzed for but not detected. Single component pesticides >* 10 ng/uL in theReport the minimum detection limit for the sample with final extract should be confirmed by GC/HS.the U (e.g. 10U) based on necessary concentration/dil- 8 - This Hag is used when the analyte is found inution action (This is not necessarily the instrument the blank as well as a sample. It indicatesdetection limit). The footnote should read: U-Compound possible/probable blank contamination and warnswas analyzed for but not detected. The number is the data the user to take appropriate action.minimum attainable detection limit for the sample. Other - Other specific flags and footnotes may be

J - Indicates an estimated value. This flag is used either required to properly define the results. Ifwhen estimating a concentration for tentatively identified used, they must be fully described and suchcompounds where a 1:1 response is assumed or when the mass description attached to the data summary reportspectral data indicated the presence of a compound thatmeets the identification criteria but the result is < than OPTIONAL FLAGSthe specified detection limit but > than zero(e.g. 10J). If limit of detection is 10 ug/L and a N - Compound not present in Calibration File.conentration of 3.0 ug/L is calculated, report as 3J. fl R I fl 0 fl C n

Form 1 7/85


ANALYSIS NO: E 4701




Antimony 0.005 N.D.

Arsenic 0.005 0.009

Beryllium 0.01 N.D.

, , Cadmium 0.01 0.01

Chromium 0*01 0.17

Copper 0.01 0.29

Lead 0.05 0.76

Mercury 0.0005 0.0007

Nickel 0.05 0.10

Selenium 0.005 N.D.

Silver 0.01 N.D.

Thallium 0.10 N.D.

Zinc 0.01 1.70

Cyanide 0.01 0.13

Aft I 0005 I

Lab Nans ; Uastex Ind. ef NJ I Sample NumberCase No : N/A I £4703

ORGANICS ANALYSIS DATA SHEET(Page 2)


Concentration^ bjj^Hedium (Circle One ) GPC Cleanup _ Yes _ NoDate Extracted 08/58/90 Separator^ Funnel Extraction _ YesDate Analyzed: 09/08/9019:24 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor: 1000: Ira 1Percent Moisture: NA

C.A.S. /^ ugA> ug/Kg C.A.S. ( ug/^p/ug/KgNumber V ^fircle One) Number TCtrcie One)

108-95-2 Phenol 73. 83-32-9 Acenaphthene 10.U111-44-4 bis(-2-Chloroethyl)Ether 10.U 51-28-5 2,4-Dinitrophenoi 50.U95-57-8 2-Chlcrophenol 10.U 100-02-7 4-Nitrophenol 50.U541-73-1 1,3-Dichlorobenzene 10.U 132-64-9 Dibenzofuran 10.U1G6-46-7 1,4-Dichlorobenzene 10.U 121-14-2 2,4-Dinitrotoluene 10.U100-51-6 Benzyl Alcohol 10.U 606-20-2 2,6-Dinitrotoluene Ifl.U95-50-1 1,2-Dichlorobenzene 10.U 84-66-2 Oiethylphthalate 10.U95-48-7 2-ttethylphenol 10. 7005-72-3 4-Chlorophenyl-phenlyether 10.U

79638-32-9 bis(2-chloroisopropyl)Ether 10.U 86-73-7 Fluorene 10.U106-44-5 4-flethylphenoi 51. 100-01-6 4-Nitroaniline 50.U621-64-7 N-Nitroso-Oi-n-Propylemine 10.U 534-52-1 4;6-Dinitro-2-t1ethylphenol 50.U67-72-1 Hexachloroethane Ifl.U 86-30-6 N-Nitrososdiphenylamine (1) 10.U°9-95-3 Nitrobenzene 10.U 101-55-3 4-Bromophenyl-phenyiether Ifl.U78-59-1 laophorone 5.J 118-74-1 Hexachlorobenzene 10.U58-75-5 2-Nitrophenol 10.U 87-86-5 Pentachlorophenoi 9J105-67-9 2,4-Dimethylphenol 18. 85-01-8 Phenanthrene l.J65-85-0 Benzoic Acid 50.U 120-12-7 Anthracene 10.U111-91-1 bis(-2-Chloroethoxy)Methane 10.U 84-74-2 Di-n-Butylphthalate 10.U120-83-2 2,4-Dichlorophenol 10.U 206-44-0 Fluoranthene 10.U120-82-1 1,2,4-Trichlorobenzene 10.U 129-00-0 Pyrene 10.U91-20-3 Naphthalene 2.J 85-68-7 Butylbenzylphthalate 10.U106-47-8 4-Chloroaniline 10.U 1-94-1 3f3'-DichtorobenzidinB 20.U87-68-3 HexacMorobutadiene 10.U 56-55-3 Benzo(a)Anthracene 10.U59-50-7 4-Chloro-3-Methylphenol Ifl.U 117-81-7 bis(2-Ethylhexyl)Phthalate 10.U91-57-6 2-?1ethylnaphthalene 10.U 218-01-9 Chrysene 10.U77-47-4 Hexachlorocyclopentadiene 10.U 117-84-0 Di-n-Octyl Phthalate 10.U88-06-2 2,4,6-Trichlorophenol Ifl.U 205-99-2 Benzo(b)Fluoranthene 10.U95-95-4 2,4,5-Trichlorophenol 50.U 207-08-9 Benzo(k)Fluoranthene *«1-58-7 2-Chloronaphthalene 10.U 50-32-8 Benzo(a)Pyrene 10,U89-74-4 2-Nitroaniline 50.U 193-39-5 Indeno(l,2,3-cd)Pyrene Ifl.U131-11-3 Ditethyl Phthalate 10.U 53-70-3 Dibenzo(a,h)Anthracene 10.U208-96-8 Acenaphthylene Ifl.U 191-24-2 Benzo(g,h,i)Perylene Ifl.U99-fl9-2 3-Nitroaniline 50.U 92-87-5 Benzidine 20.U

(D-Cannot be separated from diphenylanine

«*«-Cannot be separated from Benro(b)Fluoranthene An I U U U D C

c, -Lab Name '• Bridgeport Environmental, Inc. I Sample Number ICase No : N/A I E47Q8 I

QRGANICS ANALYSIS DATA SHEET *(Page 3)

Pesticides/PCBs

Concentration: Cj-Oj Mediua ( Circle One ) GPC Cleanup _ Yes -ftaDate Extracted/Prepared: 8/27/90 Separator Funnel Extraction ^ YeaDate Analyzed: 9/07/90 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor: 100nL/5eLPercent Moisture! N/A

C.A.S.Nunber ug/Kg

319-84-6 Alpha-BHC. ....... 0.25 U319-87-7 Bete-BHC ........ 0.25 U319-86-8 Delta-BHC. ....... 0.25 U58-89-9 Ganina-BHC (Lindane). . . 0.25 U76-44-8 Heptacnlor ....... 0.25 U309-00-2 Aldrin ......... 0.25 U1024-57-3 Heptachlor Epoxide . . . 0.25 U959-98-8 Endosulfan I ...... 0.25 U60-57-1 Dieldrin ........ 0.25 U72-55-9 4,4'-ODE ........ 0.25 U72-20-8 Endrin ......... 0.25 U

33213-65-9 Endosulfan II. ..... 0.50 U72-54-8 4,4'-DDO ........ 0.50 U

1031-07-8 Endosulfan Sulfate . . . 0.50 U50-29-3 4,4'-DOT ........ 0.50 U72-43-5 ttethoxychlor ...... 13 U


8001-35-2 Toxaphene. ....... 25 U12674-11-2 Arochlor-1016. ..... 13 U11104-28-2 Arochlor-1221. ..... 13 U11141-16-5 Arochlor-1232. ..... 13 U53469-21-9 Aroch lor- 1242. ..... 13 U12672-29-6 Arochlor-1248. ..... 13 U11097-69-1 Arochlor-1254. ..... 13 U11096-82-5 Arochlor-1260. ..... 13 U

Fora 1 7/85

flRIOOOSS

CERTIFICATE OF ANALYSISS*

PRIORITY POLLUTANT

ANALYSIS NO. E 4715




Antimony 0.13 N.D.

Arsenic 0.13 2.14

Beryllium 0.25 N.D.

Cadmium . 0.25 2.65

Chromium • 0*25 61.7

Copper 0.25 86.8

Lead 1.3 263

Mercury 0.05 N-D-

Nickel 2.5 31.8

Selenium 0.13 N-D-

Silver 0.25 H-D-

Thallium 2.5 N'D-

Zinc 0.25 438

Cyanide 0.10 N"D*

ARI0005I*

o

Lab Name : Bridgeport Environmental, Inc. I Sample Number !Case No : N/A I £4715 I

ORGANICS ANALYSIS DATA SHEET *———-—————*(Page 2)


Concentration:^ Lowxnediufli (Circle One ) EPC Cleanup _ Yes _ NoDate Extracted: 3755/90 Separatory Funnel Extraction _ YesDate Analyzed: 09/07/90 20:15 Continuous Liquid-Liquid Extraction _ YesConc/Dil Factor: 30G:1»1 1:2Percent Moisture: 50.9 *~~*\ -

ug/L o ug/KjX C.A.S. ug/L (Tug/Kg)Number (CircleNlnej Nunber (Circle UffiT

1C3-95-2 Phenol 320.J 83-32-9 Acenaphthene 970.J111-44-4 bis(-2*Chloroethyl)Ether 1300.U 51-28-5 2,4-Oinitrophenoi 6500.U°5-57-B 2-ChIorophenol 1300.U 100-02-7 4-Nitrophenol 6500.U?41-73-l 1,7-Dichlorobenzene 1300.U 132-64-9 Dibenzofuran 250.0106-46-7 1,4-Dichlorobenzene 1300.U 121-14-2 2,4-Dinitrotoluene 1300.U100-51-6 Benzyl Alcohol 1300.U 606-20-2 2,6-Dinitrotoluene 1300.U95-50-1 1,2-Dichlorobenzene 1300.U 84-66-2 Diethylphthaiate 1300.U95-48-7 2-Hethylphenol 1300,U 7005-72-3 4-Chlorophenyl-phenlyether 1300.U

39638-32-9 bis(2-chloroisopropyl)Ether 1300.U 86-73-7 Fluorene 800.J106-44-5 4-Netnylphenoi 13QQ.U 10Q-01-6 4-Nitroaniline 6500.U621-64-7 N-Nitroso-Di-n-Propylamine 1300.U 534-52-1 4,6-Dinitro-2-ftethylphenol 6500.U67-72-1 Hexachloroethane 1300.U 86-30-6 N-Nitrososdiphenylamine (1) 1300.U°8-95-3 Nitrobenzene 1300.U 101-55-3 4-Bromophenyl-phenylether 1300.U7B-59-I Isophorone 1300.U 118-74-1 Hexachlorobenzene 1300.U99-75-5 2-Nitrophenol 1300.U 37-86-5 Pentachlorophenol 6500.U105-67-9 2,4-Oimethylphenol 1300.U 85-01-8 Phenanthrene 2800.65-85-0 Benzole Acid 6500.U 120-12-7 Anthracene 670.J111-91-1 bis(-2-Chloroethoxy)(1ethane 1300.U S4-74-2 Di-n-Butylphthalate 1300.U120-83-2 2,4-Dichlorophenol 1300.U 206-44-0 Fluoranthene 1400.120-82-1 1,2,4-Trichlorobenzene 1300.U 129-00-0 Pyrene 3300.91-20-3 Naphthalene 240.J 85-68-7 Butylbenzylphthalate 1300.U

106-47-8 4-Chloroaniline 1300.U 1-94-1 3,3l-0ichlorobenzidine 2700.U87-68-3 Hexachlorobutadiene 1300.U 56-55-3 Benzo(«)Anthracene 1300.59-50-7 4-Chloro-3-Hethylphenol 1300.U 117-81-7 bis(2-Ethylhexyl)Phthalate 1300.U91-57-6 2-nethylnaphthalene 520.J 218-01-9 Chrysene 1200.J77-47-4 Hexachlorocyclopentadiene 1300.U 117-84-0 Di-n-Octyl Phthalate 1300.U88-06-2 2,4,6-Trichlorophenol 1300.U 205-99-2 Benzo(b)Fluoranthene 1200.J95-95-4 2,4,5-Trichlorophenol 6500.U 207-08-9 Benzo(k)Fluoranthene «»«91-58-7 2-Chloronaphthalene 1300.U 50-32-8 Benzo(a)Pyrene 960.J88-74-4 2-Nitroaniline 6500.U 193-39-5 lndeno(l,2,3-cd)Pyrene 1300.U

131-11-3 Dimethyl Phthalate 1300.U 53-70-3 Dtbenzo(a,h>Anthracene 1300.U208-96-8 Acenaphthylene 1300.U 191-24-2 BenzoCg^h^JPeryiene 1300.U


(l)-Cannot be separated from diphenylatine

•••-Cannot be separated from 6enzo(b)Fluoranthene ARI00055

30, 1

Lab Name : Bridgeport Environmental, Inc. I Sanple Number ICase No : N/A I 54715 |

ORGANICS ANALYSIS DATA SHEET + ———————— *(Page 3)

Pesticides/PCBs

Concentration: low > Medium ( Circle One ) GPC Cleanup _ Yes _i NoDate Extracted/Prepared: 8/27/90 Separately Funnel Extrection _ YesDate Analyzed: 9/11/90 Continuous Liquid-Liquid Extraction _ YesConc/Dil Factor: Id.OOg/lOnlsPercent ftoisture: ?0.9

C.A.S. ug/L orNumber

319-84-6 Alpha-BHC. ....... 20.0 U519-87-7 Beta-BHC ........ 20.0 U319-86-8 Delta-BHC. ....... 20.0 U58-89-9 Gamma-BHC (Lindane). . . 20.0 U76-44-8 Heptachlor ....... 20.0 U309-00-2 Aldrin ......... 20.0 U1024-57-5 Heptachlor Epoxide . . . 20.0 U959-98-8 Endosulfan I ...... 20.0 U

(j 60-57-1 Dieldrin ........ 20.0 U72-55-9 4,4'-ODE ........ 8872-20-8 Endrin ......... 20.0 U

33213-65-9 Endosulfan II. ..... 40.0 U72-54-8 4,4'-DOD ........ 640

1031-07-8 Endosulfan Sulfate . . . 40.0 U50-29-3 4,4'-ODT ........ 76072-43-5 Hethoxychlor ...... 1000 U



Form 1 7/85

ARI00056

| Sample Nunber |Organic* Analysis Data Sheet | E4722 |

- (Page 1) *................+Laboratory Name: Bridgeport Environmental, Inc. Case No.: N/ALab Sample ID: >B9411::D2 ^> QC Report No.:Sample Matrix: WATER /V Q f ft I Contract Mo. i N/AData release Authorized by: f fS L*J *J*X f ,J fX-AM. ** Data Sample Received: 21 AUG 90

ft IfX-AM. **

^Volatile CompoundsConcentration: ([Low* Medium (Circle One >Data Extracted: N/ADate Analyzed: 08/28/90 01:14Conc/Dil factor: 1:5 pH :Percent Moisture: ^ ^

C.A.S. (tig/Dor ug/Kg C.A.S. por us/KgNumber (Circle One) Number (Circle One)

74-87-3 Chloromethane 50. U 78-87-5 1,2-Dlchloropropana 25. U74-83-9 Bromomethane 50. U 10061-02-6 Trans-1,3-D1chloropropene 25. U75-01-4 Vinyl Chloride 50. U 79-01-6 Trlchloroethene 25. U75-00-3 Chloroethane 50. U 124-48-1 Dlbromochloromethane 25. U75-09-2 Methylene Chloride 45. B 79-00-5 1,1,2-Trichloroethane 25. U67-64-1 Acetone 50. U 71-43-2 Benzene 25. U107-02-8 Acroleln 250. U 10061-01-5 cls-1,3-01chloropropene 25. U167-13-1 Acrylonitrile 250. U 110-75-8 2-Chloroethylvlnylether 50. U75-15-0 Carbon Bisulfide 8000. D 75-25-2 Bromoform 25. U75-35-4 1,1-Dlchloroethene 25. U 108-10-1 4-Methyl-2-Pentanone 50. U75-34-3 1,1-Dichloroethane 25. U 591-78-6 2-Hexanone 50. U156-60-5 Trans-1,2-D1chloroethene 25. U 127-18-4 Tetrachloroethene 25. U67-66-3 Chloroform 25. U 79-34-5 1,1,2,2-Tetrachloroethane 25. U107-02-2 1,2-Dlchloroethane 25. U 108-88-3 Toluene 30.78-93-3 2-Butanone 50. U 108-90-7 Chlorobenzene - 25. U71-55-6 1,1,1-Triehloroethane 25. U 100-41-4 Ethylbenzene 25. U56-23-6 Carbon Tetrachlorlde 25. U 100-42-5 Styrene 25. U108-05-4 Vinyl Acetate 50. U Total Xylenes 25. U75-27-4 Bromodichloromethane 25. U Total Dichlorobenzenes 25. U


Value • If the result Is a value greater than or equal to C • Thia flag applies to pesticide parameters wherethe detection limit, report the value. the identification has been confirmed by GC/HS.

U - Indicates compound was analyzed for but not detected. Single component pesticides >- 10 ng/ul in theReport the minimum detection limit for the sample with final extract should be confirmed by GC/HS.the U (e.g. 10U) based on necessary concentratlon/dU- B • This flag is used when the analyte is found inutlon action (This Is not necessarily the Instrument the blank as well as a sample. It indicatesdetection limit). The footnote should read: U-Compound possible/probable blank contamination and warnswas analyzed for but not detected. The number Is the data the user to take appropriate action.minimum attainable detection limit for the sample. Other - Other specific flags and footnotes may be

j • Indicates an estimated value. This flag is used either required to properly define the results. Ifwhen estimating s concentration for tentatively identified used, they must be fully described and suchcompounds where a 1:1 response is assumed or when the mass description attached to the data summary reportspectral data indicated the presence of a compound that

i j meets the Identification criteria but the result Is < than OPTIONAL FLAGS^"^ the specified detection limit but > than zero

(e.g. 10J). If limit of detection Is 10 ug/L and a D • Compound quanitiated on diluted sample.conentratlon of 3.0 ug/L la calculated, report as 3J.

J V 1»i Sample Number !Jlrganics Analysis Data Sheet I £4729 I

(Page U *————————+Laboratory Name! Bridgeport Environmental, Inc. Case No.: N/ALab Sample ID: >B9445::02 -_ -. QC Report No.:Sample Matrix: WATER /J I) * A I Contract No.: N/AData release Authorized by: f IS U A u CJ 'SA*"** Date Sample Received: 24 AU6 98

Volatile CompoundsConcentration: Low) Medium (Circle One )Date Extracted: "R7?Date Analyzed: 08/29/90 18:42Cone/Oil factor: 1:50 pH ;Percent flajature:

C.A.S. (5 D°r U9/K9 C.A.S. QJg/Uor ug/KgNumber (Circle One) Nunber TCTrcle One)

74-87-3 Chloronethane 500. U 78-87-5 1,2-Dichloropropene 250. U74-83-9 Bronomethane 500. U 10061-02-6 Trans-1.3-Dichlorooropene 250. U75-01-4 Uinyl Chloride 500. U 79-01-6 Trichloroethene ' ' 250. U75-00-3 Chloroethane 500. U 124-48-1 Dibromochloromethane 250. U75-09-2 flethylene Chloride 250. U 79-00-5 1,1.2-Trichloroethane 250. U67-64-1 Acetone 500. U 71-43-2 Benzene 250. U107-02-8 Acrolein 2500. U 10061-01-5 cis-l,3-Dichloropropene 250. U167-13-1 Acrylonitrile 2500. U 110-75-8 2-Chloroethylvinvlether 500. U75-15-0 Carbon Disulfide 3300, 75-25-2 Browjform ' ' 250. U

(^1 75-35-4 1,1-Dichloroethene 250. U 108-10-1 4-Methyi-2-Pentanone 500. U75-34-3 1,1-Dichloroethane 250. U 591-78-6 2-Hexanone 500. U156-60-5 Trans-1.2-Dichloroethene 250. U 127-18-4 Tetrechloroethene 250. U67-66-3 Chloroform 250, U 79-34-5 1,1,2,2-Tetrachioroethane 250. U107-06-2 1,2-Oichloroethene 250. U 108-88-3 Toluene 250. U78-93-3 2-Butanone 500. U 108-90-7 Chlorobenzene 250. U71-55-6 1.1,1-Trichloroethane 250. U 100-41-4 Ethylbenzene 250. U56-23-6 Carbon Tetrechloride 250. U 100-42-5 Styrene 250. U108-05-6 Umyl Acetate 500. U Total Xylenes 250. U" -27-4 Bromodichlororaethane 250. U Total Dichiorobenrenes 250. U

Oata Reporting QualifiersFor reporting results to ERA the following results qualifiers are used. Additional flags or footnotesexplaining results are encouraged. However the definition of each flag must be explicit.

l/alue - If the result is a value greater than or equal to C - This flag applies to pesticide parameters wherethe detection limit, report the value. the identification has been confirmed by GC/MS.

U - Indicates compound was analyzed for but not detected. Single component pesticides >• 10 ng/uL'in theReport the minimum detection limit for the sample with fine! extrect should be confirmed by GC/MS,the U (e.g. 10U) based on necessary concentration/dil- B - This flag is used when the analyte is found inution action (This is not necessarily the instrument the blank as well as a sample. It indicatesdetection limit). The footnote should read: U-Compound possible/probable blank contamination and warnsuas analyzed for but not detected. The number is the data the user to take appropriate action.minimum attainable detection limit for the sample. Other - Other specific flags and footnotes may be

3 • Indicates an estimated value. This flag is used either required to properly define the results. If, when estimating a concentration for tentatively identified used, they must be fully described and suchV_y compounds where a 1:1 response is assumed or when the mass description attached to the data summary report

spectral data indicated the presence of a compound thatmeets the identification criteria but the result is < than OPTIONAL FLAGSthe specified detection limit but > then zero(e.g. 10J). If Unit of detection is 10 ug/L and a ([ Pcf Wft1/ KMent in Calibration File.conentration of 3.0 ug/L is calculated, report as 3J.


ANALYSIS NO: E 4702




Antimony 0.005 N.D.

Arsenic 0.005 N.D.

Beryllium 0.01 N.D.

(i Cadmium 0.01 N.D.

Chromium 0.01 N.D.

Copper 0.01 0.03

Lead 0.05 0.05

Mercury 0.0005 N.D.

Nickel 0.05 N.D.

Selenium 0.005 N.D.

Silver 0.01 N.D.

Thallium 0.10 N.D.

Zinc 0.01 0-04

Cyanide 0.01 N.D.

flR!00059

7 -

Lab Name : Uastex Ind. of NJ I Sample NumberCase No : N/A | E4709

ORGAWCS ANALYSIS DATA SHEET *(Page 2)


(Circle One ) GPC Cleanup _ Yes _ NoDate Extracte 08/28/90 Separatory Funnel Extraction _ YesDate Analyzed! 09/11/9019:03 Continuous Liquid-Liquid Extraction _ YesCone/Oil Factor: 1000: 1mlPercent Koisture: NA

C.A.S. ug/Ldr ug/Kg C.A.S. ( ug/L o> ug/KgNumber MGiirie One)

1*38-95-2 Phenol Ifl.U 83-J2-9 Acenaphthene Ifl.U111-44-4 bis(-2-Chloroethyl)Ether 10.U 51-28-5 2,4-Dinitrophenoi 50.U95-57-8 2-Chlorophenol Ifl.U 100-02-7 4-Nitrophenol 50.U541-73-1 1,3-Dichlorobenzene Ifl.U 132-64-9 Dibenzofuran Ifl.U1Q6-46-7 1,4-Oichlorobenzene 10.U 121-14-2 2,4-Dinitrotoluene 10.U

. ( 100-51-6 Benzyl Alcohol 10.U 606-20-2 2,6-Dinitrotoluene 10.UW °5-50-l 1,2-Dichlorobenzene 10.U 84-66-2 Diethylphthalate 10.U

95-48-7 2-nethylphenol Ifl.U 7005-72-3 4-Chlorophenyl-phenlyether 10.U39638-32-9 bis(2-chloroisopropyl)Ether 10.U 86-73-7 Fluorene 10.U106-44-5 4-fethylphenol 10.U 100-01-6 4-Nitroaniline 50.U621-64-7 N-Nitroso-Di-n-Propylamine Ifl.U 534-52-1 4,6-Dinitro-2-ttethylphenol 50.U67-72-1 Hexachloroethane Ifl.U 86-30-6 N-Nitrososdiphenylamine (1) 10.U98-95-3 Nitrobenzene 10.U lfll-55-3 4-Bromophenyl-phenylether 10.UTg-59-1 laophorone 10.U 118-74-1 Hsxachlorobenzene 10.U38-75-5 2-Nitrophenol Ifl.U 87-86-5 Pentachlorophenol Ifl.U1D5-67-9 2,4-Dimethylphenol 10.U 85-01-8 Phenanthrene 10.U65-85-0 Benzoic Acid 50.U 120-12-7 Anthracene 10.U111-91-1 bis(-2-Chloroethoxy)Hethane 10.U 84-74-2 Di-n-Butyiphthalate 10.U120-83-2 2,4-Dichlorophenol Ifl.U 206-44-0 Fluoranthene 10.U120-82-1 1,2,4-Trichlorobenzene Ifl.U 129-00-0 Pyrene 10.U91-20-3 Naphthalene 10.U 85-68-7 Butylbenzylphthalate Ifl.U106-47-8 4-Chtoroaniline 10.U 1-94-1 3,3<-Dichlorobenzidine 20.U87-68-3 Hexachlorobutadiene 10.U 56-55-3 6enzo(a)Anthracene 10.U59-50-7 4-Chloro-3-t1ethylphenol 10.U 117-81-7 bis(2-Ethylhexyl)Phthalate 4.J91-57-6 2-Hethylnaphthalene 10.U 218-01-9 Chrysene 10.U77-47-4 Hexachlorocyclopentadiene 10.U 117-84-0 Di-n-Octyl Phthalate Ifl.U38-06-2 2,4,6-Trichlorophenol 10.U 205-99-2 8enzo(b)Fluoranthene 10.U95-95-4 2,4,5-TrichlorophenoI 50.U 207-fl8-9 Benzo(k)Fluoranthane •«91-58-7 2-Chloronaphthalene 10.U 50-32-8 Benzo(a)Pyrene 10.U88-74-4 2-Nitroaniline 50.U 193-39-5 IndenoU,2,3-cd)Pyrene 10.U131-11-3 Dimethyl Phthalate 10.U 53-70-3 Dibenzo(a,h)Anthracene 10.U

( , 208-96-8 Acenaphthylene 10.U 191-24-2 Benzo(g,h,i)Perylene 10.Us 99-09-2 3-Nitroaniline 50.U 92-87-5 Benzidine 20.U

(l)-Cannot be separated from diphenylamine

•••-Cannot be separated froa Benzo(b)Fluoranthene " " ' U U U D U

t—Lab Name : Bridgeport Environmental, Inc. j Sample NunbarCase No i N/A _ |

ORGANICS ANALYSIS DATA SHEET *--(Page 3)

Pesticides/PCBs

Concentration: iLoM^xllediuni ( Circle One ) 6PC Cleanup _ Yea J NoDate Extracted/Prepared: 8/27/90 Separatory Funnel Extraction J^YesDate Analyzed: 9/07/90 Continuous Liquid-Liquid Extraction „ YesCone/Oil Factor: 100«L/5*LPercent Hoistures N/A

C.A.S.Nunber ug/Kg

319-84-6 Alpha-BHC. ....... 0.25 U319-87-7 Bata-BHC ........ 8.25 U319-86-0 Oelta-BHC. ....... 0.25 U58-89-9 Ganma-BHC (Lindane). . . 0.25 U76-44-8 Heptachlor ....... fl.25 U309-00-2 Aldrin ......... 0.25 U1024-57-3 Heptachlor Epoxide . . . 0.25 U959-90-8 Endosulfan I ...... 0.25 U

I ) 60-57-1 Ditldrin ........ 0.25 U^ 72-55-9 4,4'-DOE ........ 0.25 U

72-20-8 Endrin ......... 0.25 U33213-65-9 Endosulfan II. ..... 0.50 U

72-54-8 4,4(-DOO ........ 0.50 U1031-07-8 Endosulfan Sulfate . . . 0.50 U50-29-3 4,4'-DDT ........ 0.50 U72-43-5 Methoxychlor ...... 13 U

7421-93-4 Endrin Aldehyde. .... fl.50 U57-74-9 Chlordane. ....... 13 U

8001-35-2 Toxaphene. ....... 25 U12674-11-2 Arochlor-1016. ..... 13 U11104-28-2 Arochlor-1221. ..... 13 U11141-16-5 Arochlor-1232. ..... 13 U53469-21-9 Arochlor-1242. ..... 13 U12672-29-6 Arochlor-1248, ..... 13 U11097-69-1 ArochIor-1254. ..... 13 U11096-82-5 Arochlor-1260. ..... 13 U

Fon 1 7/85

f *


PRIORITY POLLUTANT

ANALYSIS NO. E 4716




Antimony 0.13 N.D.

Arsenic 0.13 3.65

Beryllium 0.25 0.78

Cadmium 0.25 1.65

Chromium 0 . 25 53.8

Copper 0.25 93.4

Lead 1.3 194

Mercury 0.05 0.10

Nickel 2.5 33.0

Selenium 0.13 N.D.

Silver 0.25 K.D.

Thallium 2.5 N-D-

Zinc 0.25 383

Cyanide 0.10 N.D.

flRI00062

S+ii

U

Lab Name : Bridgeport Environmental, Inc. t Sample Number ICase No : N/ft I £4716 I

ORGANICS ANW.YSIS DATA SHEET * ———————— *(Page 2)


Concentration^ Lou j Medium (Circle One ) GPC Cleanup _ Yes _ NoDate Extracted: 8728/90 ' Separatory Funnel Extraction _ YesDate Analyzed: 09/07/90 21:11 Continuous Liquid-Liquid Extraction _ YesConc/DU Factor: 3QG:lnl 1:2Percent tloisture: 48.5 -—

ug/L or(ug/Kj) C.A.S. ug/L of ug/KgNumber (Circle fitter^ Number (Circle*

108-95-2 Phenol 1300.U 33-32-9 Acenaphthene 1300.U111-44-4 bis(-2-Chloroethyl)Ether 1300.U 51-28-5 2,4-Dinitrophenol 6200.U95-57-8 2-Chlorophenol 1300,U 1QO-02-7 4-Nitrophenol 6200.U541-73-1 1,3-Dichlorobenzene 1300.U 132-64-9 Dibenzofuran 1300.U106-46-7 1,4-Dichlorobenzene 1300.U 121-14-2 2,4-Dinitrotoluene 1300.U100-51-6 fienzyl Alcohol 1300.U 606-20-2 2,6-Dinitrotoluene 1300.U95-50-1 1,2-Qichlorobenzene 1300.U 84-66-2 Diethylphthalate 1300.U95-48-7 2-fathylphenol 1300.U 7005-72-3 4-Chlorophenyl-phenlyether 1300.U

39638-32-9 bis(2-chloroisopropyl)Ether 1300.U 86-73-7 Fluorene 1300.U106-44-5 4-MethyIphenol 1300.U 100-01-6 4-Nitroaniline 6200.U621-64-7 N-Nitroso-Di-n-Propylemine 1300.U 534-52-1 4,6-Dinitro-2-t1ethylphenol 6200,U67-72-1 Hexachloroethane 1300.U 86-30-6 N-Nitrososdiphenylaaine (1) 13QO.U98-95-? Nitrobenzene 1300.U 101-55-3 4-Bromophenyl-phenylether 1300.U78-59-1 Isophorone 1300.U 118-74-1 Hexachlorobenzene 1300.U?3-75-5 2-Nitrophenol 1300.U 87-86-5 Pentachlorophenol 6200.U105-67-9 2,4-Oimethytphenol 1300.U 85-01-8 Phenanthrene 1200.J65-85-0 Bsnzoic Acid 6200.U 120-12-7 Anthracene 240.J111-91-1 bi9(-2-Chloroathoxy)Kethane 1300.U 84-74-2 Di-n-Butylphthalate 1300.U120-83-2 2,4-Dichlorophenol 1330.U 206-44-0 Fluoranthene 1400.120-82-1 1,2,4-Trichlorobenzene 1300.U 129-00-0 Pyrene 1900.91-20-3 Naphthalene 1300.U 85-68-7 Butylbenzylphthalate 1000.J

106-47-8 4-Chloroeniline 1300.U 1-94-1 3,3'-Dichlorobenzidine 2600.U37-68-3 Hsxachlorobutadiene 1300.U 56-55-3 Benzo(a)Anthracene 860.359-50-7 4-Chloro-3-«ethylphenol 1300.U 117-81-7 bis(2-Ethylhexyl)Phthalate 3800.91-57-6 2-hethylnaphthalene 350.3 218-01-9 Chrysene 800.377-47-4 Hexachlorocyclopentadiene 13QO.U 117-84-0 Di-n-Octyl Phthalate 1300.U88-06-2 2,4,6-Trichlorophenol 1300.U 205-99-2 Benzo(b)FIuoranthene 810.395-95-4 2,4,5-Trichlorophenol 6200.U 207-08-9 Benzo(k)Fluoranthene «»«91-58-7 2-Chloronaphthalene 1300.U 50-32-8 BenzotaJPyrene 570.388-74-4 2-Nitroaniline 6200.U 193-39-5 Indenod^^-cdJPyrene 1300.U

131-11-3 Dimethyl Phthalate 1300.U 53-70-3 Dibenzo(a,h)Anthracene 1300.U208-96-8 Acenaphthylene 1300.U 191-24-2 Benzo(g,h,i)Perylene 1300.U99-09-2 3-Nitroaniline 6200.U 92-87-5 Benzidine 26QO.U

(l)-Cannot be separated from diphenylanine

***-Cannot be separated from 6enzo(b)FluorantheneARI00063

Lab Name : Bridgeport Environmental, Inc. I SaopU Number t < t "^ rCase No : N/ft I E4716 I

ORGAWCS ANALYSIS DATA SHEET *—————————*(Page 3)

Pesticides/PCSs

Concentration: (Logy Median ( Circle One ) 6PC Cleanup _ Yea _^NoDate Extracted/Prepared: 8/27/90 Separatory Funnel Extraction _ YesDate Analyzed: 9/10/90 Continuous Liquid-Liquid Extraction _ YesConc/DU Factor! 10.19g/10nlsPercent Moisture: 48.5

C.A.S. ug/L orNuiber (tig/Kg

319-84-6 Alpha-BHC. ....... BO U319-87-7 Beta-BHC ........ 20.0 U319-86-8 Delta-BHC. ....... 20.0 U98-89-9 Ganma-BHC (Lindane). . . 20.0 U76-44-8 Heptachlor ....... 20.0 U309-00-2 Aldrin ......... 20.0 U1024-97-3 Heptachlor Epoxide . . . 20.0 U959-98-8 Endosulfan 1 ...... 20.0 U60-97-1 Dialdrin ........ 20.0 U72-55-9 4,4'-DOE ........ 11072-20-8 Endrin ......... 20.0 U

33213-65-9 Endosulfan II. ..... 40.0 U72-54-8 4;4'-DDO ........ 990

1031-07-8 Endosulfan Sulfate . . . 40.0 U50-29-3 4,4'-DDT ........ 84072-43-5 netnoxychlor ...... 1000 U



Forn 1 7/85

. STATION 3- - ISO/*•.»««-..„»«- +I Sample Number !

JJrganics Analysis Data Sheet I E4723 f(Page 1) * ———————— *

Laboratory Name: Bridgeport Environmental, Inc. Case No.: N/ALab Sample ID: >B94()8::02 - X Report No.:Sample Matrix: WATER fj \) . A . Contract No.: N/AData release Authorized b: ix LaJ W / J \^A^. Date Samle RData release Authorized by: fx La^ \ ^ ^ . Date Sample Received:24 AUG 90

Uolatile CojapundsConcentration: (j.oiT) Medium (Circle One )Date Extracted:Date Analyzed: 08/27/90 22:41Conc/DU factor: 1 pH :Percent Moisture:

C.A.S. (ug/Por ug/kg C.A.S, (ug/l/)r ug/kgNumber (Circle One) Number TCTrcle One)

74-97-3 Chloromethane 10. U 78-87-5 1,2-Dichloropropane 5. U74-83-9 Sromomethane 10. U 10061-02-6 Trans-1.3-0ichloropropene 5. U75-01-4 Uinyl Chloride 10. U 79-01-6 Trichloroethene 5. U75-00-3 Chloroethane 10. U 124-48-1 Dibrornochloromethane 5. U75-09-2 fathylene Chloride 12. B 79-00-5 1,1,2-Trichioroethane 5. U67-64-1 Acetone 10. U 71-43-2 Benzene 5. U107-02-8 Acrolein 50. U 10061-01-5 cis-l,3-Dichloropropene 5. U167-13-1 Acrylonitrile 50. U llfl-75-B 2-Chloroethylvinylether 10. U75-15-0 Carbon Disulfide 10. U 75-25-2 Broncfora ' 5. U

, j 75-35-4 1,1-Dichloroethene 5. U 108-10-1 4-t1ethyl-2-Pentanone 10. U^-^ 75-34-3 1,1-Dichloroethane 5. U 591-78-6 2-Hexanone 10. U

156-60-5 Trans-1.2-Dicnlotoethene 5. U 127-18-4 Tetrachloroethene 5. U67-66-3 Chloroform 5. U 79-34-5 1,1,2,2-Tetrachloroethane 5. U107-06-2 1,2-Dichloroethane 5. U 108-88-3 Toluene 5. U73-93-3 2-Butanone 10. U 108-90-7 Chlorobenzene 5. U71-55-6 1,1,1-Trichloroethane 5. U 100-41-4 Ethylbenzene 5. U56-23-6 Carbon Tetrachlonde 5. U 100-42-5 Stwrene 5. U103-05-4 Uinyl Acetate 10. U Total Xylenes 5. U7?-27-4 Bromodichloromethanc 5. U Total OichloroDenzenes 5. U

Data Reporting QualifiersFor reoorting results to EPA the following results qualifiers are used. Additional flags or footnotesexplaining results are encouraged. However the definition of each flag must be explicit.

'Jalue - If the result is a value greater than or equal to C - This flag applies to pesticide parameters wherethe detection limit, report the value. the identification has been confirmed by GC/tlS.

U - Indicates compouno was analyzed for but not detected. Single component pesticides )• 10 ng/uL in theReport the minimum detection limit for the sample with final extract should be confirmed by GC/tlS.the U (e.g. 10U) based on necessary concentration/dil- B - This flag is used when the analyte is found in•jtion action (This is not necessarily the instrument the blank as well as a sample. It indicatesdetection limit). The footnote should read: U-Compound possible/probable blank contamination and warnsuias analyzed for but not detected. The number is the data the user to take appropriate action.minimum attainable detection limit for the sample. Other - Other specific flags and footnotes may be

J - Indicates an estimated value. This flag is used either required to properly define the results. Ifwhen estlasting a concentration for tentatively identified used, they must be fully described and suchcompounds where a 1:1 response is assumed or when the nass description attached to the data summary report

(> spectral data indicated the presence of e compound thatmeets the identification criteria but the result is < than OPTIONAL FLAGSthe specified detection limit but > than zero(e.g. 10J). If limit of detection is 10 ug/L and a N - Compound not present in Calibration File.conentration of 3.0 ug/L is calculated, report as 3J. _ K

^R100065Fori 1 w 7/85

o

I Sample Number t O<?ii Qrganics Analysis Data Sheet 1 E473Q I

IrQUO 4 J *••• •••••• •• •.• ••**mm»

Laboratory Name: Bridgeport Environmental! Inc. Case Ho.: N/AUb Sample ID: >A8911::D1 _ X Report No.:Sample Hatrix: SOIL /J Q J 0 I Contract No.: N/AData release Authorized by: flN UJPVl \jj TvjL / Oatt Sample Received: 24 AUG 90

Volatile Compounds ^"^Concentration: (\g»s fadium (Circle One )Date Extracted:Data Analyzed: 08/30/90 14:02Cone/Oil factor: 1 pH :Percent floistura: 64.2k

C.A.S. ug/1 orxfg/kj C.A.S. ug/1 orNumber (Circle UnV) Number (Circle if

74-87-3 Chloromethane 28. U 78-87-9 1,2-Oichloropropane 14. U74-83-9 Bromomethane 28. U 10061-02-6 Trans-l,3-Dichloropropene 14. U79-01-4 Uinyl Chloride 28. U 79-01-6 Trichloroethene 14. U79-00-3 Chloroethane 28. U 124-48-1 Dibromochlorometnana 14. U79-09-2 ttethylene Chloride 24. 8 79-00-9 1,1,2-Trichloroethane 14. U67-64-1 Acetone 39. B 71-43-2 Benzene 14. U107-02-8 Acrolein 140. U 10061-01-9 cis-l,3-Dichloropropene 14. U167-13-1 Acrylonitrile 140. U 110-79-8 2-Chloroethylvinylether 28. U79-19-0 Carbon Oisulfide 28. U 79-29-2 Bromoform 14. U79-39-4 1,1-Dichloroethene 14. U 108-10-1 4-fothyl-2-Pentanone 28. U79-34-3 1,1-Dichloroethene 14. U 991-78-6 2-Hexenone 28. U196-60-9 Trans-l,2-Dichlotoathene 14. U 127-18-4 Tetrachloroethene 14. U67-66-3 Chloroform 14. U 79-34-9 1,1,2,2-Tetrechloroethane 14. U107-06-2 1,2-Dichloroethane 14. U 108-88-3 Toluene 9. J78-93-3 2-Butanone 28. U 108-90-7 Chlorobenzene 14. U71-99-6 1,1,1-Trichloroethane 14. U 100-41-4 Ethylbenzene 8. J96-23-6 Carbon Tetrachloride 14. U 100-42-9 Styrene 14. U108-09-4 Uinyl Acetate 28. U Total Xylenes 39.79-27-4 Bromodichloromethane 14. U Total Dichlorobenzenes 14. U

Data Reporting Qualifiersfor reporting results to EPA the following results qualifiers are used. Additional flags or footnotesexpleining results are encouraged. However the definition of each flog must be explicit.

Value - If the result is a value greater than or equal to C - This flag applies to pesticide parameters wherethe detection limit, report the value. the identification has been confirmed by EC/US.

U - Indicates compound was analyzed for but not detected. Single component pesticides >* 10 ng/uL in theReport the minimum detection limit for the sample with final extract should be confirmed by GC/tlS.the U (e.g. 10U) based on necessary concentration/dil- B - This flag is used when the analyte is found inution action (This is not necessarily the instrument the blenk as well as a sample. It indicatesdetection limit). The footnote should read: U-Compound possible/probable blank contamination and warnsuas analyzed for taut not detected. The number is the data the user to take appropriate ection.minimum attainable detection limit for the sample. Other - Other specific flags and footnotes may be

J - Indicates en estimated value. This flag is used either required to properly define the results. Ifwhen estimating a concentration for tentatively identified used, they must be fully described and suchcompounds where a 1:1 response is assumed or when the mass description attached to the data summary report

U spectral data indicated the presence of a compound thatmeets the identification criteria but the result is < than OPTIONAL FLAGSthe specified detection limit but > than zero(e.g. 10J). If limit of detection is 10 ug/L and a N - Compound gptj pMHr& w Calibration File.conentration of 3.0 ug/L is calculated, report as 30. An I UUUbO

Form 1 7/89

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