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Ultra-Fast and High Resolution NEMS Thermal Detector Based on a Nano-Air-Gap Piezoelectric Resonant Structure Yu Hui and Matteo Rinaldi Dept. Electrical and Computer Eng., Northeastern University, Boston, MA, USA [email protected] [email protected] Abstract—This paper presents the theoretical modeling and experimental verification of an innovative Nano Electro Mechanical System (NEMS) technology suitable for the implementation of ultra-fast and high resolution un-cooled thermal detectors. Fundamental challenges associated to the implementation of mechanically resonant thermal detectors are overcome with the introduction of an innovative technology platform in which a temperature sensitive Aluminum Nitride (AlN) nano-plate resonator and a monolithically integrated micromachined suspended heat absorbing element are perfectly overlapped but separated by a sub-micron air gap. By placing the absorbing element outside the body of the resonator (but suspended over it) the electromechanical performance of the resonant device is not affected by the absorbing element and the material employed to implement it (quality factor, Q1800 and electromechanical coupling coefficient, k t 2 1%) enabling the use of a compact and low-power self-sustained oscillator circuit as direct frequency readout. At the same time, efficient and quick heat transfer from the absorbing element to the nanomechanical resonant device is achieved by minimizing the air gap between them. The detection capabilities of this first prototype were tested using an integrated resistive heat source in lieu of an absorber. Power level as low as 655 nW was readily detected and a limit of detection of 48 nW was experimentally extracted. In addition a thermal time constant of ~ 60 μs was predicted for this prototype through finite element simulation. I. INTRODUCTION An ideal thermal detector is defined as a temperature sensor which is optimized to result in maximum temperature change upon exposure to the measurand [1]. With the advances of Micro/Nano -Electro -Mechanical Systems (MEMS/NMES), such as small form factor, low power consumption, fast response and wafer scale batch fabrication, significant progress has been made on thermal sensors. The use of MEMS resonators as Infrared (IR) detectors has been recently demonstrated [2, 3]. Despite the high sensitivity of these devices, they suffer from either complex fabrication processes or slow response time [2, 3]. Furthermore, the conventional approach for the development of mechanically resonant thermal detectors involves the integration of a heat absorber directly into the resonant body of the device. Nevertheless, the introduction of an absorbing layer in the material stack forming the resonator should be compatible with the transduction mechanism of the mechanical structure and should not affect the electromechanical performance of the device. This poses stringent constrains regarding the design and the materials used to implement the absorber, limiting the overall performance and application range of MEMS/NEMS resonant thermal detectors. This fundamental challenge is addressed in this work with the introduction of an innovative NEMS resonant thermal detector technology in which a heat absorbing element and a temperature sensitive Aluminum Nitride (AlN) nano-plate resonator [4] are perfectly overlapped but separated by a sub- micron air gap (Figure 1). By placing the absorbing element outside the body of the resonator (but suspended over it) high electromechanical performance of the resonant device is maintained (quality factor, Q1800 and electromechanical coupling coefficient, k t 2 1%) enabling the use of a compact and low-power self-sustained oscillator circuit as direct frequency readout. An integrated resistive heat source is used, in lieu of an absorber, to verify the detection capabilities of the sensor demonstrating the possibility to detect absorbed power in the order of ~10s nW. In addition a thermal time constant of ~ 60 μs is predicted for this prototype through finite element simulation demonstrating the potential of the proposed technology for the development of ultra-fast and high resolution un-cooled resonant thermal detectors. Figure 1. Schematic illustration of the proposed NEMS thermal detector formed by a heat absorbing element suspended over an AlN nano-plate resonator. This work was partially supported by DARPA Young Faculty Award contract number: N66001-12-1-4221.

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Page 1: Ultra-fast and high resolution NEMS thermal detector based ...330427/fulltext.pdfMEMS/NEMS resonant thermal detectors. This fundamental challenge is addressed in this work with the

Ultra-Fast and High Resolution NEMS Thermal Detector Based on a Nano-Air-Gap Piezoelectric

Resonant Structure Yu Hui and Matteo Rinaldi

Dept. Electrical and Computer Eng., Northeastern University, Boston, MA, USA [email protected] [email protected]

Abstract—This paper presents the theoretical modeling and experimental verification of an innovative Nano Electro Mechanical System (NEMS) technology suitable for the implementation of ultra-fast and high resolution un-cooled thermal detectors. Fundamental challenges associated to the implementation of mechanically resonant thermal detectors are overcome with the introduction of an innovative technology platform in which a temperature sensitive Aluminum Nitride (AlN) nano-plate resonator and a monolithically integrated micromachined suspended heat absorbing element are perfectly overlapped but separated by a sub-micron air gap. By placing the absorbing element outside the body of the resonator (but suspended over it) the electromechanical performance of the resonant device is not affected by the absorbing element and the material employed to implement it (quality factor, Q≈1800 and electromechanical coupling coefficient, kt2≈1%) enabling the use of a compact and low-power self-sustained oscillator circuit as direct frequency readout. At the same time, efficient and quick heat transfer from the absorbing element to the nanomechanical resonant device is achieved by minimizing the air gap between them. The detection capabilities of this first prototype were tested using an integrated resistive heat source in lieu of an absorber. Power level as low as 655 nW was readily detected and a limit of detection of 48 nW was experimentally extracted. In addition a thermal time constant of ~ 60 μs was predicted for this prototype through finite element simulation.

I. INTRODUCTION An ideal thermal detector is defined as a temperature

sensor which is optimized to result in maximum temperature change upon exposure to the measurand [1]. With the advances of Micro/Nano -Electro -Mechanical Systems (MEMS/NMES), such as small form factor, low power consumption, fast response and wafer scale batch fabrication, significant progress has been made on thermal sensors. The use of MEMS resonators as Infrared (IR) detectors has been recently demonstrated [2, 3]. Despite the high sensitivity of these devices, they suffer from either complex fabrication processes or slow response time [2, 3]. Furthermore, the conventional approach for the development of mechanically resonant thermal detectors involves the integration of a heat absorber directly into the resonant body of the device. Nevertheless, the introduction of an absorbing layer in the

material stack forming the resonator should be compatible with the transduction mechanism of the mechanical structure and should not affect the electromechanical performance of the device. This poses stringent constrains regarding the design and the materials used to implement the absorber, limiting the overall performance and application range of MEMS/NEMS resonant thermal detectors.

This fundamental challenge is addressed in this work with the introduction of an innovative NEMS resonant thermal detector technology in which a heat absorbing element and a temperature sensitive Aluminum Nitride (AlN) nano-plate resonator [4] are perfectly overlapped but separated by a sub-micron air gap (Figure 1). By placing the absorbing element outside the body of the resonator (but suspended over it) high electromechanical performance of the resonant device is maintained (quality factor, Q≈1800 and electromechanical coupling coefficient, kt

2≈1%) enabling the use of a compact and low-power self-sustained oscillator circuit as direct frequency readout. An integrated resistive heat source is used, in lieu of an absorber, to verify the detection capabilities of the sensor demonstrating the possibility to detect absorbed power in the order of ~10s nW. In addition a thermal time constant of ~ 60 μs is predicted for this prototype through finite element simulation demonstrating the potential of the proposed technology for the development of ultra-fast and high resolution un-cooled resonant thermal detectors.

Figure 1. Schematic illustration of the proposed NEMS thermal detector

formed by a heat absorbing element suspended over an AlN nano-plate resonator.

This work was partially supported by DARPA Young Faculty Award contract number: N66001-12-1-4221.

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II. DESIGN According to the proposed approach, the input power to be

detected (i.e. incident IR radiation absorbed in the micromachined suspended absorber) is effectively dissipated into the structure inducing a rapid (~μs) temperature increase of both the absorbing element and the resonator given the nano-scale dimensions of the air gap (Figure 1). Such temperature increase is readily detected as a shift in the device resonance frequency due to its Temperature Coefficient of Frequency (TCF ~ -30 ppm/K) [5].

This unique approach results in the following exclusive advantages of the proposed NEMS thermal detector:

• By placing the absorbing element outside the body of the resonator, higher design flexibility is guaranteed and both resonator and absorber can be optimized individually.

• The electromechanical properties of the resonant structure are not affected by the absorbing element design and the material employed to implement it.

• High sensitivity and low thermal time constant can be achieved by scaling the overall volume of the structure.

A. Theoretical Modeling In order to properly model the device and optimize its

performance, the equivalent thermal circuit in Figure 2 was considered. The power to be detected Pin (i.e. the absorbed power or the power coming from a heat source) is dissipated into the device increasing both the absorbing layer temperature, TA, and the resonator temperature TR. The input power is dissipated through two thermal paths: RA1 (thermal resistance between the heat source and the heat sink through the length of the micromachined suspended absorbing element) and the series combination of RA2 (thermal resistance associated to the thickness of the absorbing element), Rair (thermal resistance between the heat source and the resonator through the air gap), and RR (thermal resistance associated to the length of the resonator). To achieve optimal device performance, it is necessary that TA≈TR, hence RR>>RA2+Rair. This translates in reducing the thickness of the micromachined suspended absorber (to reduce RA2), the air gap (to reduce Rair) and the thickness of the AlN resonant plate (to increase RR). A high value of RA1 is also desirable in order to maximize TA for a given Pin. This can be achieved by implementing the heat absorbing element with a high thermal resistivity material (i.e. SiO2). Efficient electromagnetic absorbers based on thin film dielectric layers have been demonstrated and are fully compatible with the technology presented in this work [6].

It is worth noting that the vertical scaling of the absorbing layer and the AlN plate causes an increase of the equivalent thermal resistance of the device, Rth, (hence the overall sensitivity) and a reduction of its thermal capacitance, Cth, maintaining its thermal time constant, τ, unchanged (τ= Rth⋅Cth). Nevertheless, lower values of thermal time constant can be achieved by scaling the overall volume of the device (vertical and lateral dimensions). By reducing the thickness of the AlN plate (i.e. implementing a nano-plate) the lateral dimensions of the device can be scaled maintaining high

transduction efficiency [7]. Therefore, in order to maximize the device performance it is crucial to scale the volume of the AlN resonant nano-plate maintaining, at the same time, high quality factor and power handling.

Figure 2. Equivalent thermal cricuit of the NEMS thermal detector.

According to the aforementioned design considerations, the thickness of the AlN nano-plate resonator of this work was set to 500 nm and its lateral dimensions were properly designed in order to maintain a low value of the device equivalent electrical impedance [7]. The device was designed to operate at high frequency (~ 1 GHz), which guarantees high power handling of the mechanical structure [8]. Lateral field excitation with floating bottom electrode (LFE-F) [5] was employed to excite a higher order contour-extensional mode of vibration in the AlN structure. In addition, the suspended AlN resonant body was fully anchored to the silicon substrate instead of partially anchored through narrow tethers. Such configuration improves power handling and overall robustness of the NEMS resonator. At the same time, since a large number of finger-electrodes (n=11) was used to excite a higher mode of vibration in the AlN plate, the acoustic energy remains confined in the body of the AlN resonator (which translates to high Q) [9]. The simultaneous achievement of high quality factor, Q, and high power handling is crucial for the implementation of a low noise resonant sensor [4].

To demonstrate the effectiveness of the proposed design solution a micromachined suspended nano-hot-plate [5] was designed in lieu of the absorbing layer. The power applied to the nano-hot-plate can be considered the equivalent of the power absorbed by a properly designed absorbing layer. According to the previous design considerations, the nano-hot-plate was composed of a platinum (Pt 100 nm thick) serpentine shaped heater deposited on top of a 600 nm thick SiO2 nano plate. It is worth noting that efficient electromagnetic absorbers based on patterned metal films deposited on top of thin film dielectric layers (structurally equivalent to the nano-hot-plate of this prototype) have been demonstrated and are fully compatible with the technology presented in this work [6].

B. Finite Element Simulation 3-Dimensional Finite Element Method (3D FEM)

simulation using COMOL Multiphysics was performed to verify and optimize the proposed design solution. For the FEM simulations, both conductive and convective heat transfers were considered. The thermal conductivity of AlN

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was set to 80 W/(m·K) [5], and the convective heat transfer coefficient of air was set to 10 W/(m2·K). A fixed temperature of 20°C was set as the boundary condition for the edges of the device.

Figure 3. Heat transfer efficiency for different air gaps.

The effect of air gap dimensions on the device performance was studied in terms of heat transfer efficiency, which is defined by the ratio between the temperature of AlN resonator TR and one of the heat absorbers TA. Figure 3 shows that smaller air gaps guarantee significantly more efficient heat transfer. Therefore, the air gap of the prototype presented in this work was set to 250 nm (TR > 0.8· TA).

Figure 4. FEM simulated temperature rise with different levels of power

applied to the heat absorbing element.

Figure 5. FEM simulated thermal time constant for the device (10 mW input

power).

For a given air gap of 250 nm, the temperature rise factor and the time constant of the device were simulated and are shown in Figure 4 and Figure 5, respectively. The simulation results clearly indicate that few mWs of power applied to the heat absorbing element cause 10s °C increase of the resonator temperature and the associated thermal time constant is only about 63 μs. This demonstrates that ultra-fast and sensitive

NEMS thermal sensor can be achieved with the proposed technology.

III. EXPERIMENTAL RESULTS A six-mask post-CMOS-compatible microfabrication

process [5] was employed to fabricate the device. Figure 6 shows a Scanning Electron Microscopy (SEM) image of the fabricated device.

Figure 6. SEM image of the fabricated AlN nano-plate resonator (NPR) with integrated suspended nano-hot plate. The air gap between the resonant device

and the nano-hot plate (designed to be 250nm) is larger in the center of the device because of residual stress in the SiO2 layer.

The electrical response of fabricated device was tested by an Agilent E5071C network analyzer after performing a short–open–load calibration on a reference substrate. Figure 7 shows the admittance curve of experimental data and its corresponding Butterworth–van Dyke (BVD) fitting. The resonance frequency of the device was measured to be 962 MHz and its quality factor Q and electromechanical coupling factor kt

2 were extracted to be 1805 and 0.9%, respectively. Such high Figure of Merit (FOM= kt

2· Q >15) is among the best measured for 500nm thick AlN contour-mode resonators (CMRs).

Figure 7. Given the opportunely designed device geometrical dimensions (device capacitance, C0=220 fF) and the achieved high value of FOM a

motional resistance, Rm, of only 56 Ω is obtained for the fabricated 962 MHz NEMS resonator.

The achievement of a high value of device FOM is of crucial importance for the direct connection of the ovenized MEMS resonator to a compact and low-power oscillator circuit. In fact, the primary power loss in an oscillator circuit is due to the motional resistance, Rm, of the resonator, the value of which is inversely proportional to the device FOM (Rm∝1/(C0⋅kt

2⋅Q)) [7].

The fabricated resonant thermal detector was directly wire-bonded to a Pierce oscillator implemented with an ATF-

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551M4 E-pHEMT GaAs transistor. The use of such high gain amplifier (GaAs technology) allowed exploiting the extended dynamic range of the fully-anchored AlN resonator [4].

To test the sensitivity of the device, different power levels (from 655 nW to 690 µW) were applied to the nano-hot-plate and the corresponding oscillator output frequency shifts were recorded with a frequency counter. Figure 8 shows the measured frequency shifts for different levels of power supplied. The sensitivity of the device was found to be 0.54 ppm/µW (520 Hz/µW). In order to examine the limit of detection of the device, the short term frequency stability of the oscillator output signal was characterized by measuring its Allan Deviation [4]. The frequency measurements were taken with an Agilent 53230A frequency counter keeping the oscillator bias constant at 1.2 V. The limit of detection was evaluated by dividing the Allan Deviation (which is a measure of the noise-induced frequency fluctuation) by the measured device sensitivity (520 Hz/µW). Figure 9 shows the minimum detectable power for different measurement integration times. The limit of detection of the device is only 48 nW for 0.1 s integrating time indicating the great potential of this prototype to be used for detecting extremely small levels of power.

Figure 8. The oscillator output frequency shift for different levels of power

applied to the nano-hot plate.

Figure 9. Limit of detection for different measurement times extracted from

the measured Allan Deviation (oscillator biased at 1.2) and sensitivity.

IV. CONCLUSION In this paper, an innovative NEMS resonant thermal

detector technology suitable for the implementation of ultra-fast and high resolution NEMS thermal detector was

introduced. A new design solution in which a heat absorbing element and a temperature sensitive nanomechanical resonator are perfectly overlapped but separated by a sub-micron air gap, was theoretically modeled and experimentally demonstrated. By placing the absorbing element outside the body of the resonator (but suspended over it), a 962 MHz resonant thermal detector with high electromechanical performance (Q≈1800 and kt

2≈1%), was fabricated and connected to a compact and low-power self-sustained oscillator circuit as direct frequency readout. An integrated resistive heat source was used, in lieu of an absorber to verify the detection capabilities of the sensor showing a sensitivity of 520 Hz/µW and a limit of detection of only 48 nW. A thermal time constant as low as 63 μs was predicted for this prototype through FEM simulation demonstrating the potential of the proposed technology for the development of ultra-fast and high resolution un-cooled resonant thermal detectors.

ACKNOWLEDGMENT The authors wish to thank Professor Gianluca for the

precious discussion regarding the device fabrication and the staff of the Wolf Nanofabrication Facility at the University of Pennsylvania.

REFERENCES [1] K. L. Ren, M. B. Pisani, P. Kao and S. Tadigadapa, “Micromachined

quartz resonator-based high performance thermal sensors,” IEEE SENSORS 2010 Conference, pp. 2197-2210, November 2010.

[2] M. B. Pisani, K. L. Ren, P. Kao and S. Tadigadapa, “Application of micromachined Y-cut-quartz bulk acoustic wave resonantor for infrared sensing,” J. Microelectromech. Syst., vol. 20, pp.288-296, February 2011.

[3] V. J. Gokhale, J. Roberts and M. Rais-Zadeh, “Sensitive uncooled IR detectors using gallium niride resonators and silicon nitride absorbers,” Proc. Solid-State Sensors, Actuators and Microsystems Workshop (Hilton Head 2012), June 2012, in press.

[4] M. Rinaldi and G. Piazza, “Effects of volume and frequency scaling in AlN contour mode NEMS resonators on oscillator phase noise,” Proc. IEEE International Frequency Control Symposium, pp. 1-5, May 2011.

[5] M. Rinaldi, Y. Hui, C. Zuniga, A. Tazzoli and G. Piaaza, “High frequency AlN resonators with integrated nano hot plate for temperature controlled operation,” Proc. IEEE International Conference on Frequency Control Symposium, pp. 1-5, May 2012.

[6] C. M. Watts, X. L. Liu and W. J. Padilla, “Metamaterial electromagnetic wave absorbers,” Advanced Materials, vol. 24, pp. 98-120, 2012.

[7] M. Rinaldi, C. Zuniga, C. J. Zuo and G. Piazza, “Super-high-frenquency two-port AlN contour-mode resonators for RF applications,” IEEE Transactions on Ultrasonics, Ferroelectrics, and Frequency Control, vol. 57, pp. 38-45, January 2010.

[8] C. Zuo, M. Rinaldi and G. Piazza, “Power handling and related frequency scaling advantages in piezoelectric AlN contour-mode MEMS resonators,” Proc. IEEE International Ultrasonics Symposium, pp. 1187-1190, September 2009.

[9] M. Rinaldi, A. Tazzoli, J. Segovia-Fernandez, V. Felmetsger and G. Piazza, “High power and low temperature coefficient of frequency oscillator based on a fully anchored and oxide compensated AlN contour-mode MEMS resonator,” Proc. IEEE 25th Conference on Micro Electro Mechanical Systems (MEMS), pp. 696-699, 2012.