tristar ii 3020 confirm installation instructions and

INSTALLATION INSTRUCTIONS ANDCHECKLIST

302-42870-04Sep 2017(Rev A)

TRISTAR® II 3020 CONFIRMSURFACE AREA AND POROSITY ANALYZER

TRADEMARKSAlconox is a registered trademark of the Alconox Company.Micromeritics is a registered trademark of Micromeritics Instrument Corporation.Microsoft, Windows, and Windows 7 are registered trademarks of Microsoft Corporation.Swagelok is a registered trademark of Swagelok.TriStar is a registered trademark of Micromeritics Instrument Corporation.

Copyright

The software described in thismanual is furnished under a license agreement andmay be used orcopied only in accordance with the terms of the agreement.

______________________________________________________________________________

Copyright © 2008 - 2017. Micromeritics Instrument Corporation. All rights reserved.

CONTACT USMicromeritics Instrument Corporation

4356 CommunicationsDriveNorcross, GA / USA / 30093-2901Phone: 1-770-662-3636Fax: 1-770-662-3696

www.Micromeritics.com

---------------

U.S. Inquiries

U.S. Sales Phone: 1-770-662-3636

[email protected]

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Quotes, Orders, and Customer Satisfaction

Customer Service Phone: 1-770-662-3636

[email protected]

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U.S. Instrument Service Department

U.S. Service Department Phone: 1-770-662-3666

[email protected]

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Micromeritics Scientific Services

Customer Support Portal

http://techsupport.micromeritics.com/portal

Contact Us

TriStar II 3020 Confirm Installation Instructions and Checklist302-42870-04 (Rev A)— Sep 2017 iii

http://www.micromeritics.com/

mailto:[email protected]?subject=Request for Sales Information

mailto:[email protected]?subject=Parts and Accessories Inquiry

mailto:[email protected]?subject=Request for Service

http://techsupport.micromeritics.com/portal

About thisManual

ABOUT THIS MANUAL

The following iconsmay be found in thismanual:

NOTE - Notes contain important information applicable to the topic.

CAUTION - Cautions contain information to help prevent actions that may damage theanalyzer or components.

WARNING - Warnings contain information to help prevent actions that may cause per-sonal injury.

iv TriStar II 3020 Confirm Installation Instructions and Checklist302-42870-04 (Rev A)— Sep 2017

Table of Contents

Contact Us iii

About this Manual iv

1 Overview 1 - 1Prepare for Installation 1 - 1

Dewar Precautions 1 - 2

2 Equipment Installation 2 - 1Connect Ethernet Cable 2 - 1

Install the VacuumPump 2 - 2

Apply Power to the Analyzer 2 - 2

3 Application Installation 3 - 1AddUsers toWindowsUser Groups 3 - 6

Record User Information 3 - 7

Create User Profiles in the Administrator Utility 3 - 8

Create Password Configuration Parameters 3 - 9

Create Application User Profiles 3 - 10

Create a Service User Account 3 - 12

Start the Application 3 - 13

4 Analyzer Preparation 4 - 1Manifold Evacuation 4 - 1

Specify Unit Selections 4 - 3

GasConnections 4 - 4

Guidelines for Connecting Gases 4 - 5

Connect a Regulator and aGas Line to aGasCylinder 4 - 6

Connect Gas to Analyzer 4 - 8

Clean and Verify the Gas Line 4 - 9

Specify Gas Ports 4 - 12

TriStar II 3020 Confirm Installation Instructions and Checklist302-42870-04 (Rev A)— Sep 2017 v

5 Operational Verification 5 - 1Transducer Verification 5 - 1

Verify 1000mmHgPressure Transducer Accuracy 5 - 1

Verify 10mmHgPressure Transducer Accuracy (Krypton Units only) 5 - 3

Create Sample Files 5 - 5

Step 1 - Clean and Label Sample Tubes 5 - 7

Determine the SampleMass 5 - 9

Degas Samples 5 - 10

Install the Sample Tube 5 - 11

Fill and Install the Dewar 5 - 12

ReferenceMaterial Analysis 5 - 14

6 Installation Checklists 6 - 1Exceptions 6 - 7

Signatures 6 - 8

Final Documentation 6 - 8

A Run Conditions A - 1Automatic BlankRunConditions A - 1

Manual BlankRunConditions A - 1

Carbon ReferenceMaterial Run Conditions A - 4

B Worksheets B - 1Sample DataWorksheet B - 2

User InformationWorksheet B - 3

vi TriStar II 3020 Confirm Installation Instructions and Checklist302-42870-04 (Rev A)— Sep 2017

1 OVERVIEW

Use these installation instructions and checklists to ensure that installation procedures arecompleted properly.

It is recommended that installation procedures be performed in the order presented inthis document.

PREPARE FOR INSTALLATIONBefore installation, ensure the operator has reviewed thoroughly the analyzer Pre-installationChecklist. Ensure all required equipment and supplies are unpacked and the required personnel areavailable.

When the equipment is received, unpack and inspect the contents of the shipping carton(s). Use thepacking list to verify that all products, accessories, software (if applicable), and documentation arereceived intact and in the correct quantity. The shipping carton(s) and contents should be inspectedwithin a few days of receipt in the event damage or loss has occurred. Sort through all packingmaterial before declaringmissing equipment or parts.

Save all shipping cartonswhere equipment is to be declared as damaged or lost. Theclaims investigator must examine the cartons prior to completion of the inspectionreport.

1 Overview

TriStar II 3020 Confirm Installation Instructions and Checklist302-42870-04 (Rev A)— Sep 2017 1 - 1

1Overview

DEWAR PRECAUTIONS

Always handle glass dewars with care. Any product incorporating a vacuum is a poten-tial safety hazard and should be treated with caution. If in doubt, contact your safetyofficer.

When handling dewars containing liquefied gases or cryogenic liquids:

l Wear protective equipment:o goggles or face shieldo an insulated or rubber aprono insulated gloves

l When pouring liquefied gases from one container to another:o cool the receiving container gradually to minimize thermal shocko pour the liquified gas slowly to prevent splashingo vent the receiving container to the atmosphere

FOR GLASS DEWARS

l Use a plastic stirring rod when stirring substances in a dewar containing liquefied gases (or othermaterials of extremely low temperature). Do not use a glass or metal stirring rod unless it has aprotective coating.

l Do not handle heavy objects above the dewar. If unavoidable, place a protective cover over thedewar opening. If an object of sufficient weight is accidentally dropped into the dewar, shatteringmay occur.

l If the dewar has a protectivemesh covering, do not remove it. This cover minimizes the risk of fly-ing particles should the dewar be knocked over, dropped, or broken.

1 - 2 TriStar II 3020 Confirm Installation Instructions and Checklist302-42870-04 (Rev A)— Sep 2017

2 EQUIPMENT INSTALLATION

CONNECT ETHERNET CABLE

CONNECT ONE ANALYZER1. Plug one end of the Ethernet cable into the analyzer Ethernet port.2. Plug the other end of the Ethernet cable into the computer Ethernet port.

CONNECT MULTIPLE ANALYZERS WITH AN ETHERNET SWITCH

Do not use the uplink port when using an Ethernet switch.

2 Equipment Installation


2 Equipment Installation

INSTALL THE VACUUM PUMPLog in to your customer portal to access the VacuumPumpGuide (part number 062-42804-00) forinstructions on installing the vacuum pump.

APPLY POWER TO THE ANALYZER1. Toggle the power switch to theON position.2. Check the power indicator on the front panel of the analyzer. The indicator will blink green to

indicate that power is applied to the analyzer. Once the application is running, the indicator willstop blinking and remain illuminated.


http://www.micromeritics.com/Customer-Login.aspx

3 APPLICATION INSTALLATIONConfigure an Ethernet port on the computer to communicate with the analyzer. The IP addressmustbe 192.168.77.100. Reference the computer operator manual for instructions on changing theIP address.

The person installing the applicationmust haveWindowsAdministrator rights.Theadministrator must create profiles for all users runningMicromeritics TriStar II Confirm.

The installationmedia contains theMicromeritics application and the Administrator Utility application.The following tasksmust be completed prior to application installation:

l The Ethernet port for the analyzer must be set to 192.168.77.100l Connect the analyzer to the configured portl The analyzer must be poweredON

If installingmultiple analyzers, connect the Ethernet switch to the configured port andthe analyzers to the Ethernet switch. Refer toConnect Ethernet Cable on page 2 - 1.

1. TheWindowsAdministrator must create profiles for all users running the Confirm application.Use the worksheetUser Information Worksheet on page B - 3 to record these profiles.

2. Insert the installationmedia into the computer. If the setup program does not immediatelystart, navigate to themedia device, then locate and double click the setup.exe file.

3. ClickNext on theWelcomewindow. Do not proceed with this installation until all listed taskshave been completed. ClickOK.

3 Application Installation



4. On theNew Installationwindow, select the default location for file installation.

5. If a shortcut icon should be placed on the desktop, select theAdd the application ... option.6. Select Install this application for all Users to enable or prohibit users other than the installer to

access the application. ClickNext.7. On the Auxiliary Path Setupwindow, clickBrowse to select a new path for the listed option -

or accept the default..

8. Use theSeat number field if the application is installed onmore than one computer. Enter anumber representing the computer. For example, if the application will only be installed on thiscomputer, enter 01. If installation will also be done on a second computer, enter 02, etc. The


Seat number is used by the application to create a separate log file for each computer. ClickNext.

9. In theStep 1 group box on theAnalyzer Configurationwindow, select the number of analyzersto be attached to this computer.

If... Then...

installing the analysis program dur-ing initial installation

Select the number of analyzers to be installed

using the analysis program for off-line data reduction

Select 0

moving an analyzer from anothercomputer to this computer

Select 0.Refer to the section onmoving a analyzerin theAdministrator's Utility for TriStar II 3020 Con-firmUser Guide.

10. In theStep 2 group box on theAnalyzer Configurationwindow, enter the serial number ofeach analyzer to be attached to this computer. ClickNext.

11. On theEthernet Portswindow, select one option from the following table:




If... Then...

the configured port is listed Select the port, then clickNext.

the configured port is not listed ClickSpecify and enter the remaining portion of theIP Address, then clickNext.

The IP Addressmust be 192.168.77.100.

12. Calibration files are installed next.

If installingmultiple analyzers, at the prompt, insert themedia containing the calibrationfiles for the next analyzer.

13. On the Installation Completewindow, read the notices, then clickFinish.


14. Remove the applicationmedia and store in a secure location. The original applicationmediacontains the calibration files specific to the installed analyzer. Upgrade applications do notcontain calibration files.

15. If prompted, restart the computer after application installation.




ADD USERS TO WINDOWS USER GROUPS

After reboot, theWindowsAdministrator must login and add application users to the four usergroups created during application installation. These user groups correspond to the four user profilesthat can be assigned in the Administrator Utility. Reference the computer operating systemmanualfor creating and editing user groups.

User Group Description

CfrAdministrator Contains the profile for the application Administrator.

It is recommended that at least two users tothis group.

MicDevelopers Contains users who will be assigned the Developer profile in theAdministrator Utility. The Developer profile enables users todevelop and enter analysismethods. A Developer has access to allfunctions of theMicromeritics application.

MicAnalysts Contains users who will be assigned the Analyst profile in theAdministrator Utility. The Analysts profile enables users to performanalyses using pre-defined analysismethods. An Analyst hasaccess to a limited set of theMicromeritics application features.

MicService Created for Micromeritics Service Personnel. These users will beassigned the Developer profile in the Administrator Utility and havefull access to the functions of theMicromeritics application.Although Service Personnel have the same access rights asDevelopers, a separate user group is created for them becauseService Personnel have different directory and file accesspermissions.

In addition to creating user groups, theMicromeritics application also sets theWindows directory andfile access permissions for each of these user groups.The default file permissions are included in theAdministrator Utility for TriStar II 3020 ConfirmUser Guide.


RECORD USER INFORMATIONIn addition to creating user groups, theMicromeritics application also sets theWindows directory andfile access permissions for each of these user groups.The default file permissions are included in theAdministrator Utility for TriStar II 3020 ConfirmUser’s Guide. These settingsmay bemodified asneeded.

Reference the computer operating systemmanual for creating and editing user groups.

Developer Analyst

Create sample records from templates ü ü

Analyze samples ü ü

Generate reports ü ü

List and print sample records and templates ü ü

Perform routine maintenance ü ü

Enable manual control when the analyzer is idle ü ü

Change limited analysis conditions prior to performing an ana-lysis

ü ü

Change report options after analysis ü ü

Create templates (analysis methods) for analyst use ü

Perform all other Micromeritics application functions ü

Record User Information



CREATE USER PROFILES IN THE ADMINISTRATOR UTILITY1. Go toStart > Programs > Micromeritics > Admin Util for TriStar II Confirm.

2. In theUser name field, enter cfradministrator.3. In thePassword field, enter Password. ClickOK.4. At the promptYour password has expired, clickOK and enter a new password. The pass-

wordmust contain aminimumof six alphanumeric characters. This password will be used tolog in to the Administrator Utility and theMicromeritics application. This will not affect theWin-dows password.

5. ClickOK.


CREATE PASSWORD CONFIGURATION PARAMETERSThe Password parameters entered here apply to all Micromeritics application users.

On theAdministrator Utilitywindow, click theConfiguration tab.

Field Description

Expire Enter the number of dayswhen a user password will expire. This num-ber of days goes into effect any time a password is changed. A zeroentry indicates the passwordswill not expire.

Warn Enter the number of days prior to password expiration that a user willbe notified to change his password. A zero entry indicates this warningwill not be given.

Remember Enter the number of previous passwords to be stored in the passwordhistory file for each user. This file is checked when a user enters a newpassword to ensure that the password is unique. A zero entry indicatesthis feature will not be used.

Disable account after Enter the number of times a user will be allowed to enter an invalidpassword when attempting to log in before the application is locked. Azero entry indicates this feature will not be used.

Must match Windowsuser

Select to indicate the User ID must match the user Windows ID andthe user must be logged in to theWindows application. This ensuresthat only the currentWindows user can operate theMicromeriticsapplication. Otherwise, any user with the same access level(Developer or Analyst) can log in to the application.

Application locked This field is selected when the application is locked. The applicationlocks automatically when the specified number of failed logon attemptsis reached.

Administrator Utility Fields

Create Password Configuration Parameters



CREATE APPLICATION USER PROFILESRefer toUser Information Worksheet on page B - 3 for the user names and profiles.

1. On theAdministrator Utilitywindow, click theUser tab.

2. ClickAdd.

Fields Description

User Name Enter the user'sWindowsUser ID.

Full Name Enter the name that will:

l display in the application,l be stored in the system log, andl used as an electronic signature. This field must be unique.

Password Enter password as a temporary password that can be used to accessthe application. This password is not saved in the password history file.

Add User Fields


Fields DescriptionWhen this password is entered by the user, the user will be promptedto change it. The new password will then be stored in the password his-tory file. The passwordmust contain aminimumof six alphanumericcharacters. This will not affect theWindows password.

Access level Select the user’s application access level.

Password change date This field is blank and disabled because this is a new user.

Change password onnext logon

Selected because the user’s assigned password is temporary andmust be changed when the user logs in to the application.

Add User Fields (continued)

3. ClickOK to save.

Create Application User Profiles



CREATE A SERVICE USER ACCOUNTA Service user account should be set up during installation to provideMicromeritics servicepersonnel access to system functions if a service call is required.

1. On theAdministrator Utilitywindow, click theUser tab, then clickAdd.

Field Description

User Name Enter the user'sWindowsUser ID.

Full Name Enter Service.

Password Enter password as a temporary password that can be used to accessthe application. This password is not saved in the password history file.When this password is entered by the user, the user will be promptedto change it. The new password will then be stored in the password his-tory file. The passwordmust contain aminimumof six alphanumericcharacters. This will not affect theWindows password.

Access level SelectDeveloper.

Add User Fields

2. ClickOK to save.


EXIT THE ADMINISTRATOR UTILITY

Click theWindowsClose icon in the upper right corner of the window.

START THE APPLICATIONTo start the application, click the application shortcut on the desktop or select the application from theWindows program list.

Start the Application


4 ANALYZER PREPARATION

MANIFOLD EVACUATIONPrior to the connection of the gas inlet lines to the analyzer, themanifolds are evacuated to preparethem for the installation of the gas lines.

1. Open the application and go to Start > All Programs > Micromeritics > TriStarII Confirm.

2. Go to File > Log In.3. Go toUnit [n] > Enable Manual Control. Ensure a checkmark displays to the left of the

menu item. If the analyzer schematic does not display, go toUnit [n] > Show InstrumentSchematic.

4. Verify that all ports have sample port plugs installed.

4 Analyzer Preparation



5. Open valves 10, 6, 1, 2, 3, 11, 12, and 13, by double-clicking on the valve. This will allow theanalysis components to be evacuated at the same time other installation tasks are completed.

6. All four transducer readings should begin to pull down. The transducer readings should allcome down to 0.00 ± 0.30.

l If the analyzer cannot pull down this low, check the vacuum pump connections for leaks,including oil vapor trap O-rings, and check oil level.

l If the transducer readings are within the tolerances, wait 15 to 20minutes to allow theman-ifold time to clean up under vacuum.

7. To zero the transducers, go toUnit 1 > Calibrate > Zero Pressure. Select the four trans-ducers and clickStart. Verify the pressure transducers have been zeroed.


SPECIFY UNIT SELECTIONSOptions > UnitsUse to specify how data should appear on the application windows and reports. Thismenu option isnot available if usingRestricted option presentation.

Specify Unit Selections



GAS CONNECTIONS

The TriStar II 3020 uses pressure relief valves to return the analyzer to a safe conditionin the event of a power failure or loss of cryogen. This protects the user from dangerouspressures on the sample tube. However, extra caution should be employed if toxic orflammable gases are used. The pressure relief valves vent into the analyzer cabinet.Additional venting of the cabinet may be required for use with flammable or toxic gases.

These instructions refer to the installation of a gas line, regulator, and gas cylinder foreach type of gas used. Expansion kits or other accessoriesmay be used in the lab. If so,special consideration should be given to these configurationswhen installing the gaslines.

Up to three gas cylinders containing analysis gas and one cylinder of helium can be connected to theTriStar II. The gas ports are located on the rear panel of the analyzer.

Steps are provided for each of the analysis gases and for the helium. These instructions apply tostandard installations only.Standardmeans that the gas cylinder is located within 6 feet (1.83m) ofthe analyzer and the gas lines used are those provided byMicromeritics with the analyzer.


GUIDELINES FOR CONNECTING GASES

l Place gas cylinders within 6 feet (2m) of the gas inlets of the analyzer. Using gas line extenderson gas cylinders located in remote areasmay degrade gas quality and reduce pressure. Gas linesare typically five to six feet long. Place the cylinders close enough to allow for proper connection atthe analyzer inlet.

l Use a retaining strap (or other appropriate tether) to secure the gas cylinder.l Always use the gas lines provided with the analyzer. It is very important that proper gas lines areused with the analyzer.

o Do not use polymer tubing for the gas line.o Do not use flexible gas lines. Some flexible linesmay appear to be appropriate, such as thosewith a herringbone covering, but the linemay be coated internally with a polymer.

l Long gas lines, such as those used with gas cylinders placed in remote areas, must be evacuatedfor an extended period of time to remove ambient gases.When possible, avoid placing gas cyl-inders in remote locations. It is always best to have gas cylinders located near the analyzer.

l Carefully route the gas lines from the cylinder to the analyzer avoiding overlapping or entanglinggas lines. This will help avoid confusion whenmaintenance is required.

l Label the gas line at the analyzer inlet for proper identification andmaintenance.l Replace gas cylinders before gas is depleted. It is best to replace a gas cylinder when the pres-sure reads approximately 500 psi (3500 kPa) on the high pressure gauge. Contaminantsabsorbed to the walls of the cylinder will desorb as the pressure decreases.

l Ensure the gas cylinder is closed before connecting to the analyzer.

Guidelines for Connecting Gases



CONNECT A REGULATOR AND A GAS LINE TO A GAS CYLINDER

1. Move the gas cylinder close to the analyzer.2. Secure the cylinder in place using straps or chains connected to a wall bracket or other fixed

surface, or use a cylinder stand.3. Use an appropriate cylinder wrench to remove the protective cap from the cylinder by turning

the protective cap counterclockwise.4. Attach the gas regulator to the connector on the gas cylinder. Hand-tighten the nut, then use

an appropriate wrench to tighten an additional 3/4 turn.5. Check for leaks at the high pressure side of the regulator and in the connector.

a. Turn the regulator control knob fully counterclockwise.b. Slowly open the gas cylinder shutoff valve, then close it.c. Observe the pressure on the high pressure gauge.d. If pressure drops, repair the leak.

6. Connect the gas line to the regulator.a. Connect the gas line to the regulator connector.


b. Use two 7/16 in. (11mm) wrenches to tighten the gas line connection: one to hold thefitting steady and one to tighten the connector nut.

7. Purge the air from the gas line.

This step applies to non-hazardous gases only.

a. Open the regulator shutoff valve.b. Open the gas cylinder shutoff valve and flow gas for 10 to 30 seconds.c. Close the gas cylinder shutoff valve and allow regulator pressure to go to zero.

Connect a Regulator and aGas Line to aGasCylinder



CONNECT GAS TO ANALYZER

Ensure the gas cylinder is closed before connecting the gas line to the analyzer.

Helium is connected to the He V7 port and up to three analysis gases can be connected to ports V14,V8, and V9.

1. Remove the plug from the port.2. Insert the gas line into the port and hand-tighten the connector nut.3. Use a 7/16 in (11mm) wrench to tighten the nut an additional 1/4 turn.4. Connect all the remaining gases in the samemanner.


CLEAN AND VERIFY THE GAS LINE

Always clean the gas lines and verify there are no leaks at the connections after a gas cylinder isconnected. This test examines the gas line from the analyzer to the gas cylinder, then from theanalyzer to the regulator shutoff valve. A report is generated at the completion of the test to verifythat it has passed or failed.

Before beginning, confirm that the state for valves and the low-pressure gauge are as shown below:

1. Go toUnit [n] > Enable Manual Control. Ensure a checkmark displays to the left of themenu item. If the analyzer schematic does not display, go toUnit [n] > Show InstrumentSchematic.

2. Go toUnit [n] > Diagnostics.3. Click the down arrow to the right of the Test field and selectClean and Verify Analysis Gas

Line [number] Rev. [latest revision letter].

Clean and Verify the Gas Line



.

4. Ensure thatReport after test is selected and that Screen is chosen as the destination.5. ClickNext.6. After the test is finished, a prompt indicates the test is complete. ClickOK.7. A test report displays. Click the Instrument to Regulator Shut-off Valve - 1 tab and observe the

Slope field on the report. It should displayPassed, indicating that the gas line is clean and leakfree.

If Failed is shown instead, a gas leak is indicated. Check all gas connections from the analyzerto the regulator shut-off valve. Tighten as necessary, then try the test again.

8. Click the Instrument to Gas Bottle Shut-off Valve - 2 tab and observe theSlope field on thereport. It should displayPassed, indicating that the gas line is clean and leak free.

If Failed is shown instead, a gas leak is indicated. Check all gas connections from the analyzerto the regulator shut-off valve. Tighten as necessary, then try the test again.

9. Click theGasPressure Test - 3 tab. This test checks tomake sure all valves are in the properstate. Observe theMinimum field. It should displayPassed, indicating that the valves are in theproper state for operation of the analyzer.

If Failed is shown instead, one or more valves is not in the correct position. Set the valves asshown below:


10. ClickClose to close the test report.11. ClickClose on the test dialog to close the test.

Clean and Verify the Gas Line



SPECIFY GAS PORTS

Unit [n] > Unit ConfigurationThe analyzer has gas inlets for up to three analysis gases and a dedicated inlet for helium. The gasesconnected to the inletsmust be specified in the analysis program. If the gases are changed on one ofthe inlets, make the same change on theUnit Configurationwindow. The analysis programmust bekept informed of any changes in gases.

Enter the gas selections and clickOK to save.

Fields Description

Configuration[group box]

Displays the IP address used by the analysis program, serial number,and type of analyzer.

Change IP. Displays theUnit IP Setupwindow. The IP address andsubnet mask assigned during installation display. Do not edit thesefields unless instructed by aMicromeritics service representative.

Board ID. Displays information from the electronic circuit boards in theanalyzer. These parameters cannot be edited.

Unit Configuration Fields Table


Fields Description

Gas Selections[group box]

Enter the gas connected to the specified port.

Options [group box] Displays options installed on the analyzer.

Servo Valve [group box] Displays the last calibration date for the servo valve.

Software Versions[group box]

Displays the software versions of theMIC BIOS, controller, and ana-lysis program.

Unit Configuration Fields Table (continued)

Specify Gas Ports


5 OPERATIONAL VERIFICATION

TRANSDUCER VERIFICATION

VERIFY 1000 MMHG PRESSURE TRANSDUCER ACCURACY

Verifying the 1000mmHg transducers’ accuracy requires the use of:

l 004-09814-00 Paroscientific Pressure Calibration Standard OR004-09603-00 Crystal Pressure Gauge

l 003-09623-01 VacuumCalibration Standard. (Super Bee)

1. Attach nitrogen gas at 10 to 15 psig to gas inlet port for Valve 9.2. Manually pressurize the system including the three sample ports and P0 port to 800mmHg ±

50 mmHg. If a 10mmHg transducer is installed, valve 15must also be open.3. Remove the sample port filter frits on ports 1 and 2.4. Install the pressure calibration standard on sample port 1. If using the Paroscientific gauge,

connect it to the analyzer's RS-232 port.5. Install the vacuum gauge on sample port 2.6. Install a blank tube or plug on sample port 3.7. Open valves 1, 2, 3, 4, 5, 6, and 15 (if present).8. Open valves 10, 11, 12, and 13.9. Wait until the vacuum gauge reads vacuum levels below 20 μmHg.10. Continue evacuation for 10minutes.11. Zero the pressure transducers.

a. Go toUnit [n] > Calibration > Zero Pressure.b. Select:

l Manifold Transducerl Port 1 Transducerl Port 2 Transducerl Port 3 Transducerl P0 Transducerl 10mmHg transducer (if present)

c. ClickStart. If no error messages display, continue to the next step.12. Select the pressure transducers.

a. Pressurize themanifold, sample ports and P0 port to 800 to 900mmHg.b. Go toUnit [n] > Calibration >Pressure Scale.c. Select:

l Manifold Transducer

5 Operational Verification


5Operational Verification

l Port 1 Transducerl Port 2 Transducerl Port 3 Transducerl P0 Transducer

d. ClickFrom Reference and enter the reading from the Paroscientific gauge, or enter thepressure reading from the pressure calibration standard. PressEnter.

e. Reduce the system pressure to 380mmHg ± 20mmHg. If the values for all 5 of the1000 mmHg transducers are within the tolerances shown on the Data Sheet, continue tothe next step.

13. Match the pressure transducers.a. Go toUnit [n] > Calibration > Match Transducers.b. Select:

l Manifold Transducerl Port 1 Transducerl Port 2 Transducerl Port 3 Transducerl P0 Transducer

c. ClickStart. If no error messages display, continue to the next step.d. If the analyzer has a 10mmHg transducer, continue with the calibration standards

attached to the analyzer, otherwise remove the vacuum gauge and pressure calibrationstandards.

e. If the system has a 10mmHg transducer, continue with the filter frits removed, otherwisere-install the filter frits in the sample port 1 and 2.


VERIFY 10 MMHG PRESSURE TRANSDUCER ACCURACY (KRYPTON UNITS ONLY)


l 004-09814-00 Paroscientific Pressure Calibration Standard OR004-09603-00 Crystal Pressure Gauge

1. Install the pressure calibration standard on one of the sample ports. If using the Paroscientificgauge, connect it to the analyzer's RS-232 port.

2. Manually pressurize the analyzer, including the one sample port, to 9mmHg ± 0.5mmHg.3. Go toUnit [n] > Calibration > Pressure Scale (10 mmHg).4. ClickFrom Reference and enter the reading from the Paroscientific gauge, or enter the pres-

sure reading from the pressure calibration standard. PressEnter.5. Reduce the system pressure to 4.50mmHg ± 0.25mmHg.6. Record the value for the 10mmHg transducer and the pressure calibration standard.7. Calculate the differences between the pressure calibration standard and the analyzer trans-

ducer.8. Record the serial number of the pressure calibration standard on the data sheet.9. Remove the vacuum gauge and pressure calibration standards.10. Re-install the filter frits in the sample port 1 &2.

Verify 10mmHgPressure Transducer Accuracy (KryptonUnits only)



VERIFY DOSING MANIFOLD TEMPERATURE SENSOR


l 003-09601-00 - Omega Thermometer

1. Remove the analyzer top cover.2. Locate themanifold with the temperature sensor (RTD).3. Place themeter thermocouple in the hole next to the RTD.4. Replace the analyzer top cover.5. Allow themeter thermocouple to thermally equilibrate for 10minutes. Check the temperature

on the computer monitor and compare it to themeter temperature. If different, calibrate theanalyzer temperature (only if the reference temperaturemeter has been calibrated within 1year.)

6. Go toUnit 1 > Calibration > Temperature.7. Enter current temperature. ClickOK.


CREATE SAMPLE FILESSample files can be created in advance or at the time of analysis by either the Developer or Analyst.

ANALYSTAn Analyst can create sample files by selecting predefined parameter files. An Analyst can switch toAdvanced presentation option to view details of the parameter files, but cannot edit the files.

1. Go to File > New > Sample Information.2. Select a template to use, then clickCreate.3. Complete the fields from the following table.

Fields Description

Sample Enter or edit the description for the analysis.

Mass Enter the samplemass.

Density Enter the sample density. This value is applicable only when using theCalculated free-spacemethod.

Analyst Fields

4. Click the down arrow to the right of each of the following to select parameter files:

l Sample Tubel DegasConditions (if using a SmartPrep degasser)l Analysis Conditionsl Adsorptive Propertiesl Report Options

ClickAdvanced to view the contents of the selected files.

5. ClickSave and complete theSave As options.6. ClickClose.

Create Sample Files



DEVELOPERA Developer is allowed to view and edit parameters of the sample file

1. Go to File > New > Sample Information.2. Select a template to use, then clickCreate. In theSample field, enter or edit the description .3. Complete the fields from the following table.

Fields Description

Sample Enter or edit the description for the analysis.

Operator Enter the name of the operator performing the analysis.

Submitter Enter the name of the department, company, etc. submitting thesample for analysis.

Mass Enter the samplemass.

Density Enter the sample density. This value is applicable only when using theCalculated free-spacemethod.

Developer Fields

4. Select if data will bemanually entered or automatically collected. IfManually entered is selec-ted, anEntered tab displays across the top of the window.

5. Click each parameter tab andmake any necessary edits. Refer to the TriStar II 3020 ConfirmOperator Manual for detailed instructions on these fields.

6. ClickSave and complete theSave As options.7. ClickClose.


STEP 1 - CLEAN AND LABEL SAMPLE TUBESSample tubes and filler rodsmust be clean and dry before samples are added and weighed. Thefollowing table indicateswhichmaterials are supplied byMicromeritics and which are supplied by theuser. The procedures following thematerials table are recommended.

Supplied by Micromeritics Supplied by User

l Filler rodl Sample data worksheetl Sample tubel Sample tube brushl Sample tube rackl Sample weighing supportl Stopper for sample tube

l Acetone or isopropyl alcoholl Analytical balancel Detergentl Drying ovenl Pipe cleanersl Rubber gloves or lint-free clothl Safety glassesl Ultrasonic cleaning unitl Waste container

1. Preheat drying oven to 110 ºC.2. Verify that the ultrasonic cleaning unit is clean.3. Use 5 grams of Alconox (or other suitable detergent) per 500ml of warmwater and fill the

ultrasonic unit with enough water to cover the sample tubes and filler rods (if used). If toomuch detergent is used, it may be difficult to rinse from the sample tubes. Ensure the deter-gent is dissolved before placing the sample tubes and filler rods into the water.

4. Fill the sample tubeswith warmwater and place them in the ultrasonic cleaning unit, thenplace the filler rods in the unit. Turn on the ultrasonic cleaning unit for approximately fifteenminutes.

Step 1 - Clean and Label Sample Tubes



5. Use rubber gloves to ensure no oils or residue are transferred to the clean tubes and fillerrods, then remove the sample tubes and filler rods from the unit.

6. Clean the interior of the sample tubeswith the brush supplied with the analyzer.7. Rinse the sample tubes and filler rods thoroughly with hot water. Rinse again with isopropyl

alcohol or acetone. If isopropyl alcohol or acetone is not available, deionized water may beused.

8. Stand the sample tubes on the sample tube rack and place the filler rods in a basket or in therack. Bake in a vacuum oven for two hours at 110 °C.

Samples tubes can also be cleaned with high purity acetone or isopropyl alcohol anddried for about 10minutes under heat. If using thismethod, continue with step10.

9. Remove the sample tubes and filler rods from the oven and allow to cool.

Do not insert the filler rods at this time. Filler rods are inserted before the sample tube isinstalled on the analysis port.

10. Blow out the sample tubeswith oil-free compressed air.11. Rinse the sample tube closure with isopropyl alcohol, then wipe the sample tube closure dry

with a clean, lint-free cloth.12. Label the sample tube and stopper for identification.13. Replace the rubber stopper, Check Seal, or TranSeal.


DETERMINE THE SAMPLE MASS

See also:

Sample Data Worksheet on page B - 2

Clean, dry sample tubes are essential for accurate results. How much sample to use can bedetermined best by experiment. In general, a sample providing 40 to 120 squaremeters of totalsurface area is recommended for nitrogen analysis. Less than 40 squaremetersmay causeunreliable results. More than 120 squaremeters will extend analysis time.

Smaller quantities are required for samples having high surface areas. These samples requirecareful weighing after degassing because a small error may represent a considerable percent oftotal weight. Proper weighing techniques aremost important in this case. Use no less than 100mg toreduce the effect of weighing errors.

Care should be taken when loading powders; the accessory funnel is useful for this purpose. Largegranules or chunksmay be loaded with forceps.

Analysis results are expressed in units of surface area per gram of sample; therefore, it is importantthe true samplemass be known.

Follow the instructions on theSample DataWorksheet and complete all fields to find the true samplemass.

1. Record theSample Tube Identification on theSample DataWorksheet.2. Tare the balance and allow it to stabilize at zero.3. Place the empty sample tube set on the balance.4. Record the stabilizedmass on theSample DataWorksheet as [A] Mass for empty sample

tube set. Remove the sample tube set from the balance.

Do not touch the sample with bare handswhile performing the following steps. Doing socould affect the accuracy of results.

5. Place a sample container on the balance. Tare the balance and allow it to stabilize to zero (0).6. Slowly pour the specified amount of sample into the sample container.7. Remove the rubber stopper, seal frit, or TranSeal from the sample tube.8. Use the sample tube funnel (provided in the accessories kit) and pour the sample from the

weighing container into the sample tube.

Determine the SampleMass



9. Replace the rubber stopper, Check Seal, or TranSeal.10. Weigh the sample tube set containing the sample and record the value on theSample Data

Worksheet as [B] Sample tube set plus samplemass (Before Degas).11. Subtract the [A] Mass for empty sample tube set from the [B] Mass of sample tube set plus

sample and record this value as the [C] Samplemass (Before Degas).

DEGAS SAMPLESAfter the sample has been weighed, use a degassing unit to remove any contaminants whichmayhave adsorbed to the surface or pores of your sample. Appropriate degassing units are availablefromMicromeritics. Log in to your customer portal to access parts and accessories.

If using the SmartPrep degasser, use theDegasConditions tab in the application to set degasparameters. Refer to the Smart PrepOperator Manual for operating instructions.

After degassing is complete, perform the following steps:

1. Weigh the sample tube set containing the sample; record the weight on the Sample DataWorksheet asSample tube set plus samplemass (After Degas).

2. Subtract theMass for empty sample tube set (Before Degas) from theSample tube set plussamplemass (After Degas) to obtain the sample’smass; record this value asSamplemass(After Degas).


http://www.micromeritics.com/Customer-Login.aspx

INSTALL THE SAMPLE TUBERepeat these steps for each sample tube to be installed.

If using... Then...

A rubber stopper Remove it.

An isothermal jacket Slide the jacket down over the stem of the sample tube until it touchesthe sample tube bulb.

A filler rod Hold the sample tube horizontally and carefully slide the filler rod into thetube.

Do not hold the rod vertically and drop the rod into the tube;this could break the rod and/or tube.

1. Remove the sample tube stopper.

l If using a filler rod, hold the sample tube horizontally and carefully side the filler rod into thetube.

l If using an isothermal jacket, slide the jacket down over the stem of the sample tube until ittouches the sample tube bulb.

2. Insert the P0 tube into the center hold of the dewar cover and slide the cover up. Ensure thetapered side of the cover is facing downward.

3. Insert the sample tube through one of the holes in the cover.

Install the Sample Tube



4. Place the connector nut, ferrule, andO-ring onto the sample tube stem.5. Attach the sample tube to the analysis port and ensure it is completely in the port. Securely

screw the connector nut onto the analysis port. Hand-tighten the connector nut.6. Slide the dewar cover upward until it stops.

FILL AND INSTALL THE DEWAR

The equipment images in this document may differ slightly from your equipment, how-ever the instructions are the same unless otherwise noted.

See also:

Dewar Precautions on page 1 - 2


1. Fill the dewar with the analysis bath liquid (such as liquid nitrogen) to no higher than 2 1/4 in.(5.7 cm) from the top. Filling the dewar higher than this will cause an error in the free spacemeasurement.

Incorrect fluid levels can lead tomeasurement errors. Check the level of the bath liquidbefore each analysis.

2. Insert the dipstick and check the level of the analysis bath liquid. Condensation should notexceed the level indicator mark.

3. For best results, if the dewar has not been used for a while, allow approximately 30minutesfor the temperature of the dewar to stabilize with the bath liquid, then recheck the level of thebath liquid. Add additional liquid if necessary.

4. If using isothermal jackets, slide the jackets down the sample tube until the jackets touch thesample tube bulbs.

5. Slide the dewar lid to ensure a proper seal on the top of the dewar.

Fill and Install the Dewar



REFERENCE MATERIAL ANALYSISA reference analysis is used to verify that the analyzer is operating properly and producing optimumresults. Thesemethods provide specifications for critical report quantities and reporting of whetherthe quantities are in or out of specification. The expected analysis results are shown on the referencematerial bottle. Analysis results should be with the stated tolerance level.

PERFORM A BLANK TUBE ANALYSIS

The equipment images in this document may differ slightly from your equipment, how-ever the instructions are the same unless otherwise noted.

1. Log in to Service Test Mode.2. Install blank tubeswith filler rods and isothermal jackets into each of the sample ports. Use

new O-rings on the sample tubes. Ensure the dewar cover is attached. (Verify that the iso-thermal jacket and filler rods are checked as being used in the sample tube file.)

3. Fill the dewar with LN2 and check the level using the dipstick.


4. Place the dewar on the elevator and close the sample compartment door.5. Go toUnit 1 > Service Test > PCP Analysis.6. SelectNitrogen Blank for Analysis Type, then clickStart.

Tube Size Tolerance

3/8 inch tubes Volume adsorbed to be ±0.073 std cm3 at any point. The isothermmust show a fairly smooth trace. No sudden peaks, except at sat-uration.

1/2 inch tubes Volume adsorbed to be ±0.2000 std cm3 at any point. The isothermmust show a fairly smooth trace. No sudden peaks, except atsaturation.

ReferenceMaterial Analysis



PERFORM A REFERENCE MATERIAL ANALYSISPerform this analysis with carbon black referencematerial using nitrogen as the analysis gas.

1. Go to Unit [n] > Sample Analysis.2. In the Port 1 group box, clickBrowse. Locate and select theCarbon 1.SMP file. ClickOK.3. In the Port 2 group box, clickBrowse. Locate and select theCarbon 2.SMP file. ClickOK.4. In the Port 3 group box, clickBrowse. Locate and select theCarbon 3.SMP file. ClickOK.5. ClickStart.The analysis begins.6. When the analyses are complete, look at the reports for various ports to see if theBET Sur-

face Area shown on theSummaryReportmatcheswithin the tolerance level shown on the ref-erencematerial bottle.

7. If theBET Surface Area values do not match, refer to the causes and actions below.

Cause: The sample was not degassed properly.

Action: Degas the sample and try again.

Cause: The gas lines are not clean enough.

Action: Perform the procedure and verify gas lines, then try again.

Cause: Themeasured free space is too high, indicating that the helium is not pure enough.

Action: Use helium that is 99.999% pure, then try again.

8. Retain a copy of the sample information file to return to theMicromeritics Service SupportCenter.

9. Attach the printed reports to the Installation Checklist to be returned toMicromeritics.


6 INSTALLATION CHECKLISTSUse these codes to complete the tables in this section, then initial and date each section. If the tablehas an Initial / Date column, the person completing the procedure should enter their initials and thedate.

P Pass. Indicates that this procedure has been successfully completed without error.F Fail. Indicates that this procedure has been unsuccessful and prevents the analyzer

from being installed for use.Y Yes. Indicates that this procedure has been performed.N No. Indicates that this procedure has not been performed.N/A Not Applicable. Indicates that this procedure does not apply to your system.

Procedure Evaluation Code

Review thePre-installation Instructions and Checklist document and ensurethat the laboratory is prepared for installation. P F N/A

Ensure that the required personnel are available. P F N/A

Ensure that all equipment has been unpacked and verified using the packinglist. P F N/A

Analyzer is located in a suitable environment P F N/A

Line voltage has been verified to be within tolerances and changed if required. P F N/A

Prepare for Installation

6 Installation Checklists



Procedure Evaluation Code

The analyzer has been connected to a power source? P F N/A

Configure the Ethernet port P F N/A

Connect computer to analyzer. P F N/A

Connect the Ethernet switch, if applicable.

l If one Ethernet based analyzer was purchased, connect the Ethernet cableto the analyzer and the computer, or

l If more than one Ethernet based analyzer was purchased, connect an Eth-ernet cable from the computer to the Ethernet switch. Then connect the Eth-ernet based analyzers to the Ethernet switch.

P F N/A

Install application software. P F N/A

Setup Computer

Device Description

Computer(make / model / SN)

ComputerOperating System

Printer(make / model / SN)

Was the computer supplied by Micromeritics? Y N

Computer Information

Name:Date:Comments:

Computer Installed By:


Procedure EvaluationCode

Initial /Date

Confirm Application

l Install the application software. P F N/A

l Required personnel are available. P F N/A

l Type of installation (standard or non-standard has been determ-ined) P F N/A

l Standard installation requires personnel withWindowsAdmin-istrator skills available. P F N/A

l Network hardware is local. P F N/A

l Personnel with all Network Access rights is available. P F N/A

l Requirements for non-standard installations. Record issues con-sidered non-standard. P F N/A

l Network prepared byNetwork Administrator, if applicable. P F N/A

l File locations determined. P F N/A

l TriStar II 3020 application installed. P F N/A

Install the Software





Initial /Date

Start the Application

l Application users added toWindows user groups. P F N/A

l Administrator Utility program started. P F N/A

l Administrator user profile entered. P F N/A

l Password configuration parameters entered.

Expire: __________________________________Warn: ___________________________________Remember: ______________________________Disable: _________________________________Must matchWindows user: __________________

P F N/A

l Application user profiles entered. P F N/A

l Service user profile entered. P F N/A

l TriStar II 3020 Confirm application started. P F N/A

Install the Software (continued)


Initial /Date

Install the components of the vacuum pump. P F N/A

Connect the vacuum pump to analyzer. P F N/A

Install the Vacuum Pump



Initial /Date

Evacuatemanifold. P F N/A

Specify units of measure. P F N/A

Connect gas lines. P F N/A

Clean and verify gas lines. P F N/A

Connect Gases


Initial /Date

Gases entered in application? P F N/A

Specify Gases





Initial /Date

Create sample files for nitrogen analysis. P F N/A

Create additional sample files for krypton analysis, if applicable. P F N/A

Clean sample tubes P F N/A

Determine samplemass. P F N/A

Degas samples.

Install sample tubes.

Prepare the dewar.

Perform blank tube run. Blank tube runmust be within tolerances:

l 3/8 in. less than ± 0.073 STP cm3 at any pointl 1/2 in. tube less than ± 0.200 STP cm3 at any point

Perform carbon black referencematerial analysis with nitrogen gas.Use table below to record results.

Reference Material Analysis

Port 1: Carbon Black Initial / DateExpected BET results: _______________±_______________

Actual BET results: ________________±________________Y N N/A






EXCEPTIONSExplain the procedures that were categorized asFail orNo.

Procedure Comment Initial / Date

Exceptions



SIGNATURES

INSTALLER

Name: Date:Position:Company:Signed:Service Request Order (or FSR#)

CUSTOMER REPRESENTATIVE

Name: Date:Position:Company:Signed:

FINAL DOCUMENTATIONIn order to provide consistent analyzer service, Micromeritics retains records of installation,operational verification, and calibration data in its Service Support Center in Norcross, GA, USA.After completing the installation process, representatives of Micromeritics who install analyzers arerequired to send the following documents toMicromeritics for inclusion in the customer's analyzerhistory:

l Completed Service Request Order or Field Service Reportl Completed and signed Installation Checklist


A RUN CONDITIONS

AUTOMATIC BLANK RUN CONDITIONSThe TriStar II 3020 application contains an automated procedure of conducting the blank tube run.Use following steps to create blank tube run conditions and start the procedure.

1. Go toUnit 1 > Service Test > PCP Analysis.2. In theAnalysis Type group box, selectNitrogen Blank.3. ClickStart.4. When the run is complete, a report is created for each sample port. The Isotherm report con-

tains summary information about the run.

MANUAL BLANK RUN CONDITIONS

SAMPLE INFORMATION FILE SETTINGS

Field Enter

Sample Blank Tube Test

Operator Enter the Operator initials.

Submitter Analyzer Serial Number

Mass 1.0000 g

Density 1.0000 cm3/g

Type of Data Automatically Collected

SAMPLE TUBE FILE SETTINGS

Field Enter

SampleTube Default 3/8 in. Sample Tube

Stem Diameter 3/8 in.

Physical volume below mark 4.8608 cm3

User Isothermal Jacket Yes

Use Filler Rod Yes

A RunConditions

TriStar II 3020 Confirm Installation Instructions and Checklist302-42870-04 (Rev A)— Sep 2017 A - 1

A RunConditions

DEGAS CONDITIONS FILE SETTINGS

Leave these settings at the default. Do not modify.

ANALYSIS CONDITIONS FILE SETTINGS

Field Enter

Description RunConditions

Isotherm Collection Target Pressure

Pressures - Dp not adjust

Options -

l Use first pressure fixed dose:Nol Use maximum volume increment:Nol Absolute pressure tolerance: 3.0000mmHgl Relative pressure tolerance: 3.0%

Preparations l Fast evacuation: Yesl Evacuation time: 0.30 hoursl Leak test:No

Free Space l Free space group:Measuredl Lower dewar after free space: Nol Evacuation time: 0.02 hoursl Outgas test: No

P0 and T l P0 type:Measurel P0: 745.000mmHgl Temperature: 77.30 K

Equilibration l Equilibration interval: 6 secl Minimum equilibration delay at P/P0 > 0.995: 600 secs

Backfill Do not adjust

A - 2 TriStar II 3020 Confirm Installation Instructions and Checklist302-42870-04 (Rev A)— Sep 2017

ADSORPTIVE PROPERTIES FILE SETTINGS

Field Enter

Adsorptive Nitrogen

Mnemonic N2

Psat vs Temperature Do not adjust

Maximum manifold pressure 1050.00mmHg

Non-ideality factor 0.000062

Density conversion factor 0.0015468

Molecular cross-sectional area 0.162 nm2

REPORT OPTIONS FILE SETTINGS (ISOTHERM ONLY)

Field Enter

Isotherms Yes

Tabular Report Selected Yes

Plot Adsorption Branch No

Plot Description Branch No

Linear Plot Selected Yes

Plot Curve No

Plot Points No

Overlay Samples No

Autoscale X Axis Yes

Autoscale Y Axis Yes

Logarithmic Plot Selected No

Plot Curve No

Manual BlankRunConditions


A RunConditions

CARBON REFERENCE MATERIAL RUN CONDITIONS

SAMPLE INFORMATION FILE SETTINGS

Field Enter

Sample Carbon ReferenceMaterial

Operator Enter the Operator initials.

Submitter Analyzer Serial Number

Mass To be entered g

Density To be entered as cm3/g

Type of Data Automatically Collected

SAMPLE TUBE FILE SETTINGS

Field Enter

SampleTube Default 3/8 in. Sample Tube

Stem Diameter 3/8 in.

Physical volume below mark 1.0000 cm3

User Isothermal Jacket Yes

Use Filler Rod Yes

DEGAS CONDITIONS FILE SETTINGS

Field Enter

Description DegasConditions

Stage 1

Soak Temperature (°C) 30

Ramp Rate (°C/min) 10

Soak Time (min) 10


ANALYSIS CONDITIONS FILE SETTINGS

Field Enter

Description Referencematerial

Isotherm Collection

Pressures

Options -

Target Pressure

Do not adjust

l Use first pressure fixed dose:Nol Use maximum volume increment:Nol Absolute pressure tolerance: 5.0000mmHgl Relative pressure tolerance: 5.0%

Preparations l Fast evacuation: Nol Evacuation time: 10.0mmHg/secl Unrestricted evacuation from: 5.0mmHgl Evacuation time: 0.30 hoursl Leak test:No

Free Space l Free space group:Measuredl Lower dewar after free space: Yesl Evacuation time: 0.10 hoursl Outgas test: No

P0 and T l P0 type:Measurel P0: 760.000mmHgl Temperature: 77.30 K

Carbon ReferenceMaterial Run Conditions


A RunConditions

ADSORPTIVE PROPERTIES FILE SETTINGS

Field Enter

Adsorptive Nitrogen

Mnemonic N2

Psat vs Temperature Do not adjust

Maximum manifold pressure 1050.00mmHg

Non-ideality factor 0.000062

Density conversion factor 0.0015468

Molecular cross-sectional area 0.162 nm2

REPORT OPTIONS FILE SETTINGS (ISOTHERM ONLY)

Field Enter

Isotherms Yes


Plot Adsorption Branch No

Plot Description Branch No

Linear Plot Selected Yes

Plot Curve Yes

Plot Points Yes

Overlay Samples No



Logarithmic Plot Selected

BET Surface Area:

No

Yes


Plot Report Selected Yes

Overlay Samples No



Langmuir Surface Area NoNo


Field Enter

t-PlotBJH AdsorptionBJH DesorptionOptionsSummaryPore SizeSingle Point BETMulti Point BET

NoNoNoYes

YesYes

Equilibration

Equilibration interval

Minimum equilibration delay atP/P0 ≥ 0.995

5 sec

600secs

Backfill Do not adjust

Carbon ReferenceMaterial Run Conditions


B WORKSHEETS

Worksheets in this sectionmay be copied as needed.

See also:

Sample Data Worksheet on the next page

User Information Worksheet on page B - 3

BWorksheets

TriStar II 3020 Confirm Installation Instructions and Checklist302-42870-04 (Rev A)— Sep 2017 B - 1

BWorksheets

SAMPLE DATA WORKSHEET

Sample Tube Identification:_________________________________

Sample Data (g)

Record all values in gramsBefore Degas After Degas After Analysis

A. Mass for empty sample tube set:

B. Sample tube set plus samplemass:

C. Sample mass (B - A):

Degas Information

Degas apparatus:

Temperature (ºC):

Time (hours):

Actual time started:

Actual time finished:

Degas Notes:

B - 2 TriStar II 3020 Confirm Installation Instructions and Checklist302-42870-04 (Rev A)— Sep 2017

USER INFORMATION WORKSHEET

Enter the user names assigned to each group.

Developer Analyst Service **

User Name*: ______________________________

Full Name: ________________________________

User Name*: ______________________________

Full Name: ________________________________

User Name*: ______________________________

Full Name: ________________________________

User Name*: ______________________________

Full Name: ________________________________

User Name*: ______________________________

Full Name: ________________________________

User Name*: ______________________________

Full Name: ________________________________

User Names and Groups

* User Name:WindowsUser ID

** Service: Users should be added to theMicServiceWindowsUser Group and assigned aDeveloper User Profile in the Administrator Utility.

User InformationWorksheet

TriStar II 3020 Confirm Installation Instructions and Checklist302-42870-04 (Rev A)— Sep 2017 B - 3

tristar ii 3020 confirm installation instructions and

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