s.y. adzaklo,* c.p.k. dagadu, i.i. mumuni, p.s. adu, h.a. affum, … · 2017. 4. 27. ·...

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S.Y. Adzaklo,* C.P.K. Dagadu, I.I. Mumuni, P.S. Adu, H.A. Affum, G.K. Appiah, A. Coleman

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Page 1: S.Y. Adzaklo,* C.P.K. Dagadu, I.I. Mumuni, P.S. Adu, H.A. Affum, … · 2017. 4. 27. · Introduction A good understanding of mixing operations in stirred vessels will enhance optimal

S.Y. Adzaklo,* C.P.K. Dagadu, I.I. Mumuni, P.S. Adu, H.A. Affum, G.K. Appiah, A.

Coleman

Page 2: S.Y. Adzaklo,* C.P.K. Dagadu, I.I. Mumuni, P.S. Adu, H.A. Affum, … · 2017. 4. 27. · Introduction A good understanding of mixing operations in stirred vessels will enhance optimal

INTRODUCTION

The main aim of industrial mixing is to provide mass transfer of material to promote better contact between reactor contents in order to obtain the required product quality in the shortest possible time (Kuncewicz et al., 2005).

However, many industrial mixing operations are either inefficient or more than enough, mainly as a result of improper reactor design.

ICARST 2017

Page 3: S.Y. Adzaklo,* C.P.K. Dagadu, I.I. Mumuni, P.S. Adu, H.A. Affum, … · 2017. 4. 27. · Introduction A good understanding of mixing operations in stirred vessels will enhance optimal

Introduction This is due to lack of understanding of the mixing

process which could be attributed to the complex nature of impeller-induced flows in stirred vessels (Delvigne et al., 2005).

This leads to poor product quality and overconsumption of energy that eventually results in high production costs

Therefore, there is the need for in-depth studies of mixing operations to determine the performance of mixing vessels.

ICARST 2017 3

Page 4: S.Y. Adzaklo,* C.P.K. Dagadu, I.I. Mumuni, P.S. Adu, H.A. Affum, … · 2017. 4. 27. · Introduction A good understanding of mixing operations in stirred vessels will enhance optimal

Introduction A good understanding of mixing operations in

stirred vessels will enhance optimal design and help modify existing processes in order to minimize capital and running costs (Dagadu et al., 2015).

This work was done to investigate the effect of impeller type on mixing and determine the fluid dynamics of the material in the vessels.

ICARST 2017 4

Page 5: S.Y. Adzaklo,* C.P.K. Dagadu, I.I. Mumuni, P.S. Adu, H.A. Affum, … · 2017. 4. 27. · Introduction A good understanding of mixing operations in stirred vessels will enhance optimal

EXPERIMENTAL SYSTEM

ICARST 2017, VIENNA, AUSTRIA, 24-28TH APRIL 2017

Fig. 4: axial impeller (b) radial impeller

(a) (b)

Page 6: S.Y. Adzaklo,* C.P.K. Dagadu, I.I. Mumuni, P.S. Adu, H.A. Affum, … · 2017. 4. 27. · Introduction A good understanding of mixing operations in stirred vessels will enhance optimal

EXPERIMENTAL SYSTEM

ICARST 2017, VIENNA, AUSTRIA, 24-28TH APRIL 2017

Fig. 1 Experimental set up

Page 7: S.Y. Adzaklo,* C.P.K. Dagadu, I.I. Mumuni, P.S. Adu, H.A. Affum, … · 2017. 4. 27. · Introduction A good understanding of mixing operations in stirred vessels will enhance optimal

EXPERIMENTAL SYSTEM

7 ICARST 2017, VIENNA, AUSTRIA, 24-28TH APRIL 2017

Experimental

Parameters

TK 1

(1 axial

impellers)

Tank2

(2 axial

impeller)

Tank3

(2 radial

impeller)

Tank 4

(no

impeller)

Tank height (cm) 61.0 61.0 61.0 61.0

Free board height

(cm)

10.0 10.0 10.0 10.0

Tank diameter

(cm)

38.2 38.2 38.2 38.2

Material volume

(lit)

58.4 58.4 58.4 58.4

Flow rate

(lit/min)

10 10 10 10

Page 8: S.Y. Adzaklo,* C.P.K. Dagadu, I.I. Mumuni, P.S. Adu, H.A. Affum, … · 2017. 4. 27. · Introduction A good understanding of mixing operations in stirred vessels will enhance optimal

PROCEDURE

ICARST 2017, VIENNA, AUSTRIA, 24-28TH APRIL 2017 8

Page 9: S.Y. Adzaklo,* C.P.K. Dagadu, I.I. Mumuni, P.S. Adu, H.A. Affum, … · 2017. 4. 27. · Introduction A good understanding of mixing operations in stirred vessels will enhance optimal

PROCEDURE

Mean Residence Time (MRT) and the variance were calculated by the method of moments.

The fluid dynamics were obtained by modeling using

DTSpro and

RTD Software

9 ICARST 2017

Page 10: S.Y. Adzaklo,* C.P.K. Dagadu, I.I. Mumuni, P.S. Adu, H.A. Affum, … · 2017. 4. 27. · Introduction A good understanding of mixing operations in stirred vessels will enhance optimal

RESULTS AND DISCUSSIONS

10 ICARST 2017

Model

Parameters

TK 1

(1 axial

impellers)

PMSR

Tank2

(2 axial

impeller)

PMSE

Tank3

(2 radial

impeller)

PMSE

Tank 4

(no

impeller)

PMSE

Cum. tact(min) Tau 1 = 5 9.5 17.2 25.5

tm(min) J1 = 2.1 3.8 11.4 1

J Tau2 = 1 2.8 3.2 3.7

k J2 = 1, =

0.13

0.36 0.15 0.1

MRT Per tank

(min)

5.7 7.3 6.9 5.3

Variance , 2

Per tank (min2)

40.4 80.7 66.3 27.6

Page 11: S.Y. Adzaklo,* C.P.K. Dagadu, I.I. Mumuni, P.S. Adu, H.A. Affum, … · 2017. 4. 27. · Introduction A good understanding of mixing operations in stirred vessels will enhance optimal

RESULTS AND DISCUSSIONS

11 ICARST 2017

Experimental

Parameters

cont’d

TK 1

(1 axial

impellers)

Tank2

(2 axial

impeller)

Tank3

(2 radial

impeller)

Tank 4

(no

impeller)

Theoretical MRT

(min)

5.8 5.8 5.8 5.8

Exp. MRT per

tank (min)

5.3 7.5 7.1 5.1

Exp. Variance per

tank, 2 (min2)

42.4 86.3 57.7 26.6

Page 12: S.Y. Adzaklo,* C.P.K. Dagadu, I.I. Mumuni, P.S. Adu, H.A. Affum, … · 2017. 4. 27. · Introduction A good understanding of mixing operations in stirred vessels will enhance optimal

RESULTS AND DISCUSSIONS

12 ICARST 2017

0

0.02

0.04

0.06

0.08

0.1

0.12

0.14

0.16

0 20 40 60 80

E(t

) (

min

time (min)

Fig. 7 Tank 1 (1 axial impeller)

EXPERIMENTAL

PMSR MODEL

Page 13: S.Y. Adzaklo,* C.P.K. Dagadu, I.I. Mumuni, P.S. Adu, H.A. Affum, … · 2017. 4. 27. · Introduction A good understanding of mixing operations in stirred vessels will enhance optimal

RESULTS AND DISCUSSIONS

13 ICARST 2017

0

0.01

0.02

0.03

0.04

0.05

0.06

0 20 40 60 80

E(t

) (m

in-1

)

Time (min)

Fig. 8 Tank 2 (2 axial impellers)

EXPERIMENTALPMSE MODEL

Page 14: S.Y. Adzaklo,* C.P.K. Dagadu, I.I. Mumuni, P.S. Adu, H.A. Affum, … · 2017. 4. 27. · Introduction A good understanding of mixing operations in stirred vessels will enhance optimal

RESULTS AND DISCUSSIONS

14 ICARST 2017

0

0.005

0.01

0.015

0.02

0.025

0.03

0.035

0.04

0 20 40 60 80

E(t

) (m

in-1

)

Time (min)

Fig. 9 Tank 3 (2 radial impellers)

EXPERIMENTAL

PMSE MODEL

Page 15: S.Y. Adzaklo,* C.P.K. Dagadu, I.I. Mumuni, P.S. Adu, H.A. Affum, … · 2017. 4. 27. · Introduction A good understanding of mixing operations in stirred vessels will enhance optimal

RESULTS AND DISCUSSIONS

15 ICARST 2017

0

0.005

0.01

0.015

0.02

0.025

0.03

0.035

0 20 40 60 80 100

E(t

) (m

in-1

)

Time (min)

Fig. 10 Tank 4 (No impeller)

EXPERIMENTAL

PMSE MODEL

Page 16: S.Y. Adzaklo,* C.P.K. Dagadu, I.I. Mumuni, P.S. Adu, H.A. Affum, … · 2017. 4. 27. · Introduction A good understanding of mixing operations in stirred vessels will enhance optimal

CONCLUSION

The extent of material mixing in the tanks were inferred from the variances

Tank 2 (with 2 axial impellers) gave the highest variance as shown above and hence indicating a better mixing than the other tanks

The next is tank 3 (with two radial impellers)

Thank 4 gave the poorest mixing. This is expected since this tank has neither impellers nor baffles which aid in material mixing

16 ICARST 2017

Page 17: S.Y. Adzaklo,* C.P.K. Dagadu, I.I. Mumuni, P.S. Adu, H.A. Affum, … · 2017. 4. 27. · Introduction A good understanding of mixing operations in stirred vessels will enhance optimal

THANK YOU FOR YOUR ATTENTION

ICARST 2017, VIENNA, AUSTRIA, 24-28TH APRIL 2017 17