solid - liquid phase separation - ucce sonomacesonoma.ucanr.edu/files/27768.pdf · extraction...

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1 OLIVE OIL PROCESSING COURSE OLIVE OIL PROCESSING COURSE Solid - Liquid Phase Separation

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Page 1: Solid - Liquid Phase Separation - UCCE Sonomacesonoma.ucanr.edu/files/27768.pdf · Extraction efficiencies per plant and operator Plant B 75.93% 83.20%-Plant A - 84.67% 90.10% Operator

1

OLIVE OIL PROCESSING COURSE

OLIVE OIL PROCESSING COURSE

Solid - Liquid Phase Separation

Page 2: Solid - Liquid Phase Separation - UCCE Sonomacesonoma.ucanr.edu/files/27768.pdf · Extraction efficiencies per plant and operator Plant B 75.93% 83.20%-Plant A - 84.67% 90.10% Operator

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Extraction efficiency

Very good efficiency: >90.0%

Benchmark efficiency: >85.0%

Unacceptable: <70 0%Unacceptable: <70.0%

Extraction efficiency

E.E.=1-(Oil pomace*(100-Oil fruit))/(Oil fruit*(100-Oil pomace)

Or

< 8.0% oil/dry matter in the pomace

With 50% moisture fruit = 3.0% oil/fresh in pomace

With 60% moisture fruit = 2.0% oil/fresh in pomace

Page 3: Solid - Liquid Phase Separation - UCCE Sonomacesonoma.ucanr.edu/files/27768.pdf · Extraction efficiencies per plant and operator Plant B 75.93% 83.20%-Plant A - 84.67% 90.10% Operator

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Fruit and moisture levels

Fruit moisture vs. extraction efficiency - Plant A

50.00%

60.00%

70.00%

80.00%

90.00%

100.00%

it m

oist

ure

& ex

trac

tion

effic

ienc

y (%

)

40.00%0 5 10 15 20 25

Samples

Fru

Moist Eff iciency Linear (Eff iciency) Linear (Moist)

Fruit and soil moisture

Fruit moisture vs. extraction efficiency - Plant BFruit moisture vs. extraction efficiency Plant B

50 00%

60.00%70.00%80.00%90.00%

100.00%110.00%

ruit

moi

stur

e an

d ef

ficie

ncy

(%)

40.00%50.00%

0 10 20 30 40 50

Samples

Fr

Fruit moisture Efficiency Poly. (Eff iciency) Linear (Fruit moisture)

Page 4: Solid - Liquid Phase Separation - UCCE Sonomacesonoma.ucanr.edu/files/27768.pdf · Extraction efficiencies per plant and operator Plant B 75.93% 83.20%-Plant A - 84.67% 90.10% Operator

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Decanter

Decanter

Page 5: Solid - Liquid Phase Separation - UCCE Sonomacesonoma.ucanr.edu/files/27768.pdf · Extraction efficiencies per plant and operator Plant B 75.93% 83.20%-Plant A - 84.67% 90.10% Operator

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Decanter

PomaceWater

OilPomace Oil

r

Decanter

• Capacity.

• Efficiency.

Page 6: Solid - Liquid Phase Separation - UCCE Sonomacesonoma.ucanr.edu/files/27768.pdf · Extraction efficiencies per plant and operator Plant B 75.93% 83.20%-Plant A - 84.67% 90.10% Operator

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Capacity of the Decanter

• Viscosity (Temperature).• Length.• Diameter.• Differential between screw and bowl.• Particle size (Crushing)• Particle size (Crushing).

Capacity of the Decanter

Page 7: Solid - Liquid Phase Separation - UCCE Sonomacesonoma.ucanr.edu/files/27768.pdf · Extraction efficiencies per plant and operator Plant B 75.93% 83.20%-Plant A - 84.67% 90.10% Operator

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Efficiency of the Decanter

• Density difference between phases (Talc – Water - Crushing).• Speed of rotation.• Size of phases (Decanter plates).• Separation time (Pumping speed).

Capacity vs. Equipment

Page 8: Solid - Liquid Phase Separation - UCCE Sonomacesonoma.ucanr.edu/files/27768.pdf · Extraction efficiencies per plant and operator Plant B 75.93% 83.20%-Plant A - 84.67% 90.10% Operator

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Pumping speed

13Speed 1 (65% TC) Speed 2 (80% TC)

9

10

11

12 p

om

ace

(%)

5

6

7

8

1 2 3Samples

Oil

in

Pumping speed

• How do I know if I am pumping too fast?p p g

• Oil losses above limit.• Oil comes out dirty (Not always).

• How do I know if I am pumping to slow?

• No problems apart from increased costs.• Do not go under 40% NC of the Decanter.

Page 9: Solid - Liquid Phase Separation - UCCE Sonomacesonoma.ucanr.edu/files/27768.pdf · Extraction efficiencies per plant and operator Plant B 75.93% 83.20%-Plant A - 84.67% 90.10% Operator

9

Pumping speed

Pumping speed

Page 10: Solid - Liquid Phase Separation - UCCE Sonomacesonoma.ucanr.edu/files/27768.pdf · Extraction efficiencies per plant and operator Plant B 75.93% 83.20%-Plant A - 84.67% 90.10% Operator

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Decanter plates

Decanter plates

Page 11: Solid - Liquid Phase Separation - UCCE Sonomacesonoma.ucanr.edu/files/27768.pdf · Extraction efficiencies per plant and operator Plant B 75.93% 83.20%-Plant A - 84.67% 90.10% Operator

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Decanter plates

Decanter platesPlate 99 Plate 100 Plate 101

8

9

10

11

5

6

7

Without water 6% WaterMarino Uceda – Australia 2005

Page 12: Solid - Liquid Phase Separation - UCCE Sonomacesonoma.ucanr.edu/files/27768.pdf · Extraction efficiencies per plant and operator Plant B 75.93% 83.20%-Plant A - 84.67% 90.10% Operator

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Decanter plates

• How do I know when to change the plate?g p

• Once you have tried everything else and the oil still comes out very dirty and with very low Decanter capacity. Put an smaller plate.

• Or if there is too much oil in the decanter. Stop the feeding pump into decanter, flush it with water and the amount of oil that is obtained should not exceed

f f1.5 % of the TC of the decanter. E.g.: 5 tn/hr should not produce more than 50-75 litres. Put a larger plate.

Processing

Page 13: Solid - Liquid Phase Separation - UCCE Sonomacesonoma.ucanr.edu/files/27768.pdf · Extraction efficiencies per plant and operator Plant B 75.93% 83.20%-Plant A - 84.67% 90.10% Operator

13

Extraction efficiencies per plant and operator

-83.20%75.93%Plant B

90.10%84.67%-Plant A

>2 years1-2 years< 1 yearOperator

92.15%89.31%-Plant C

OLIVE OIL PROCESSING COURSE

Liquid - Liquid Phase Separation

Page 14: Solid - Liquid Phase Separation - UCCE Sonomacesonoma.ucanr.edu/files/27768.pdf · Extraction efficiencies per plant and operator Plant B 75.93% 83.20%-Plant A - 84.67% 90.10% Operator

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Centrifugation

Centrifugation

Page 15: Solid - Liquid Phase Separation - UCCE Sonomacesonoma.ucanr.edu/files/27768.pdf · Extraction efficiencies per plant and operator Plant B 75.93% 83.20%-Plant A - 84.67% 90.10% Operator

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Centrifugation

Centrifugation

Page 16: Solid - Liquid Phase Separation - UCCE Sonomacesonoma.ucanr.edu/files/27768.pdf · Extraction efficiencies per plant and operator Plant B 75.93% 83.20%-Plant A - 84.67% 90.10% Operator

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Centrifugation

Centrifugation

Page 17: Solid - Liquid Phase Separation - UCCE Sonomacesonoma.ucanr.edu/files/27768.pdf · Extraction efficiencies per plant and operator Plant B 75.93% 83.20%-Plant A - 84.67% 90.10% Operator

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Centrifugation

Centrifugation

Oil in water:

Ideal: < 0.1%Unacceptable: > 0.3%

Water in oil:Ideal: < 0.2%Unacceptable: > 0.6%

Oil temperature:Oil temperature:Ideal: 1-2ºC higher than malaxing TºUnacceptable: Lower than malaxing Tº.

> 5ºC higher than malaxing Tº

Page 18: Solid - Liquid Phase Separation - UCCE Sonomacesonoma.ucanr.edu/files/27768.pdf · Extraction efficiencies per plant and operator Plant B 75.93% 83.20%-Plant A - 84.67% 90.10% Operator

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Centrifugation

• Accurate selection of regulation ring.g g• Check oil aspect at all times (Clean milky aspect).• Check foam aspect at all times (White as soon as it is formed).• Do not over feed the separator.• Do not add more than 40% of water/oil.• Temperature of water between 35-38ºC. Never colder than the oil.• Constant flow of oil and water.• Regulate discharge times (1-2 hours).• Maintain clean all parts.

Centrifugation

Page 19: Solid - Liquid Phase Separation - UCCE Sonomacesonoma.ucanr.edu/files/27768.pdf · Extraction efficiencies per plant and operator Plant B 75.93% 83.20%-Plant A - 84.67% 90.10% Operator

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Settling

Settling

• Maintain oil in settling for 24-48 h.g• Drain settlings every two hours.• Remove foam every six hours.• Avoid contact with open air or light.• If we drain more than 1% settlings for total oil produced we have to check the separator.• Maintain temperature above 18ºC.• Check acidity and peroxides before sending to final tank.