section: 11.3 background chapter 4 reference: 18 section: 11.3 background chapter reference: 4 18...
TRANSCRIPT
AP42 Section: 11.3
Background Chapter Reference:
4 18
Title: Particulate Compliance Analysis For The Coal-Fired Brick Kiln, The Mogul Corporation, Charloffe, NC, January24, 1978.
I I I I I I I I I I I I I I I
., . . . A P 4 2 Section Reference ~eportsect . Reference
MOGUL a envirof e fvice
MOGUL
ENVIRONMENTAL CONTROL SERVICES
THE MOGUL CORPORATION
' * +W4y
A!! e+ The Mogul Corporation W A T E R T R E A T M E N T PRODUCTS A N D SERVICES SINCE 1915
CHAGRIN FALLS onio 44022 I?lbl 2.17 SO00 TELEX NUMBER 980324
m0GUL @ 1
I , I I 1 1 I I
lV, I
February 13, 1978
REPLY TO:
Southern Division 1201 S. Graham Street Chwloffe. North Carolina 28203 17041 375-5726
t&. Paul S i e f f e r t Pullman-Swindell 4 4 1 Smi thf ie ld St. P i t t sbu rg , Pa. 15222
Subject: Pa r t i cu la t e Compliance Testing
Dear Mr. S i e f f e r t :
Enclosed are ,the r e s u l t s of the p a r t i c u l a t e compliance t e s t i n g performed on t h e b r i ck k i l n a t the Lee B r i c k and T i l e p l an t , Sanford, N. C. on January 24, 1978.
If you should have ques t ions which are not ' answered by. this ; r epor t , p l ease do no t hesitate ta con tac t me ,at our Char lo t te . . - of f i ce . . .
.~
i: . . .
Thank you raery much for u t i l i z i n g Mogul's Envi*oSeNices program . . .> , ' . - . . . , :. .
. . to obtain your p a r t i c u l a t e emission rates.. ... . ~ , . ~ .. . . . . . . . .
. .. , . . . ' yours very ..jxuly,', i . , . . . . . . .
. . ..
. . . .
Laboratory Manager . . . . .
WDF/sc . .
cc: In t r i p l i c a t e M r . Owen Foster Nr. B i l l McConnell
Enclosures
AIR QUALITY DIVISION CENTRAL OFFICE
I PLANTS AND LABORATORIES
Phoenix. Ar izona C A N A D A A U S T R A L I A Portland. Orcgon Winnioag, Manirnlls Thi3 Ni!ihling;~lc? Sul lo iv c o . . LKI. Inglewood. Cnli larnis M o n i r e ~ l , Qucl,crc S v d n r v . N. S. w .
Chagrin Fall%. Ohio Charlorlc. North Carolina Minnuaoolir. Minnesota Atlanta. Guorgia Arlingtori, Texas
Lconin. N e w Jersey I I
~
i
!
' ' j
i
i I
!
I
1
i
1 I
! ..
f
I I
\
I I I
- M OG u I, envirofe rvice
PREPARED ESPECIALLY FOR;
PDLLMAN-SWXNDJZLL LBE BRICK nt3fl TILE PLANT
8AtiFORD, Ep. C.
'PESTS: Parumlate Compliance Analysis fo r ths Cold P i r e d Brick Kiln
TESTS CONDUCTED BYa The C.4ogul Corporat$a blr . R. X. Pear-, Team Leader Mr. L e d 5 Frederick, Aesietant
TEST DATE: January 24, 1978
REPORT NUMBER1 5-12277-1
REPORT BY2 R. M. IJaaraa
TABLE OF CONTENTS
Introduction
Sampling & Analytical Procedures
Discussion
Summary of Results
Computer Printout
Raw Data
EPA Analytical Method
Calibration Data
Data From Records
.
PAGE 1
1
-
1
2
Appendix I
Appendix 11
Appendix 111
Appendix IV
Appendix V
I
I
i
!
I
- - I i
. I
1 i
I I
! !
1 j
-1 1
I
i ..
MOGUL enviroiervne
INTRODUCTION
Partiaulate laampling of the atack gasee emittad fm.m the cold f irad brick k i l n was parformed at the Lee Bfick and T i l e plant, Sanford, N. C. on January 2 4 , 1970.
One two hour test was perfonwdl on ea& of the two stacks to deternine t \e pollutant mags rate aaaarding to the reg- ulations of the State of North Carolha. There ware no observers fran the State of North C a r o l i n a present.
Them 8ources were tested utilizing a Nutech Corporation, -1 261-300 particulats~staclc sampling syatm, which meets the &signed opacffLcaUon of tlm ~vLronmsuitcal Pmtection -cy. The method util ized fo r partlaulate m a l y ~ h wae the Envimmental Protaaotian Agency method as presented in the F&Er& -Volume 42, 168. August 8, 1977, Method V "mtennination of Particulate emissions for Stationary SOUrcn3B'.
RESULTS
For ease of interpretat ion, the'attachwl Wles out l ine the reeu l t s of each test perform@&. The couiputerlaed aalcula- t ions and raw data sheets bawd been included i n ttte report for specific calculat ion inforxiation.
DISCUSSION
%!he meximum allowable emission rate in lbs . /hr. of proaees w a s taken from the Ruculeeand Regulations t%verninq the Control of Air Pollution, Board of Water and Air Resources, Raleigh, N. C., January 2 3 , 1972, page c-30, 0-31.
... ..
C J H E, w 2 H x 0 m H
1 !
i
. !
I 1 I
I ’ 1: I
i I
I I I i i
_I i
I
W W N
p1 4 0 0 rl rl
m
a m
a W
3 z z 3 a
2
m
m
4
m W
r- N
,
P m
0 rl
N
W
m rl
d E+ 0 H
,
nrvision to Reference Mathod!, 1-8 A(:I;NCY: EnvlronmcnLnl rrotccllon AxcllCY. . .: AC-noN: FLnal Rule. : ,. , . . . SIlhfMARY: lhk nllC rCV16C8 Rrfrrence A r m & 1 through 8. Vlc detoJlcd re-
,. q u i r m ~ c ~ ~ l s used Lo rncasurc eirilsslons lr~m1 nllcctcd facilities to ,dclcnnlliC
. iv l :~ ihcr Uiey nre 111 complinticc m l l h n SIUI:!:I~CI 01 pcriormmce. n i c ~iieJlials ivt.rv wtj:ina1ly promulgnted December
1!l71, nnd'slnce U I R ~ unicseveinl re- <mi hrcnmc apparent whIc11 would
clrri l ,~. corrixt nnd lmprovc the mclli- ods. ' r h e c revirlons ,ninkc the niathods cu lc r to usc. ruidlmprovc thclr nccwncy nid roli:;blllly. ' "
EITTCI?VE DATE: September IS. 1077. ADDRESSES: COPlcs 01 .'the co~ ' ICI I t 1cttcw:trc available for public InSpcctloll nnd.cnimiiii: .:d I h c US. Envlroinientrd
.Protection Agency. .Public InlormaUon Rctcreiire Uniii'(EPA Libr:tiy). Room 29?2. . tflI. M Street, 8.W.. washliigton; D.C. ?0460. A summnry of Lhc ColnlnCnts and EP:\'s rewonses may be obtalncd uwn writkn rcquext from the EPA Pub-
~ lic Inlormntion' Center (PM-215J. 401 ' M Strect. S.w:. Washington. D.C. 20460 , (s11ccify "Publlc" Comnient' Summnry: Rcvkions to Relcrcncc Method? 1-8 In Aplh2nJi.y A 01 Stnndtirds 01 PCrformniiCC for s e w Stnllonnry Sources") . FOR FLIRTHER,'INFORMATION CON- TACT: ' " . . .
Don R. Goodwln. Ernlsslon StRndnrds and EnElncerlng DIvk$lnn. Envlron- nwiitnl ProLectlon Agency. Rqcwcll
: Trinni:lc Park. North CnroIlna.27711. . ' telephone No. 918-841-5311.
SUPPLEMENTARY' INFbRhrATION:. l l i e nmcndments wcrc proposed on 3unc R . i w ~ ' ( 4 0 En 23oGO). A totnl oe 55 eom- mcnt lcltcrs were rccclvcd durlnu the comn~riit period-34 from IndudrY. 15 lrom jiovcrnmentnl hficncirs. niid 6 froin othcr inlrrcsted purtlcs: Thry conlnlnc(l numrrom supgcslions wl~Ich mere incor- p0;ntcd In Llic fiiml revisions.
Ch:tnr.cs ci,ninion l o nll eight of tho rcrcrrncc methotls i:rc: ( 1 ) tl?! rlnllncn- (.ion ol proccdorcs ~ i i d noiliimcnt wec- i ~ i ~ ; , t . i u ~ ~ s rciulting. from t l ~ c comincnL% 1 2 ~ Uir adtlilioii 01 guldcllncs for &I-
nntl eiiui~xn~!iit lo 01 the Ailliihilslra- (3 ) Uic odditlori of
an inlrcxnhiction lo ench rclcrcilcc IIICCII- "d tit:.rw:iin,{ lhc wncral ILIC or tlic nicLImI :uld d~ll~!c:tllna the ~woccrlllrC i m W:,>IK nltcrnntlvc mcthoils hind cclulu- I l l C I I t .
sl,t~rlflc chnnfics to tho nirthods nrc: Mmion 1
1. Thr r,rovlslon for 'the u.w 01 IIIO~C t h i l ~ l LC'O Lrnvcrsc dlmiclerti. wlicn RIWC-
. '
, ,
i&\triinr; has h h tlelcl.ol. I f 11110 1rnren;c dlnniclrr b In n i h i u wnitdiilii~ lhc trrcnlwt rxrrrctcd w ~ ~ ~ r i ~ t r ~ ~ l i ~ i n vnrlnllon. LIic Inlciidrd
.. iwrrxma: ui thc i i c i ~ ~ e t i p11rtt~ru1111 wili h fll11111,.d ' '
3. JI1c::rd 011 rccilll dnln Iroin Fluldync tl'iwllriilnw Snintrllnr:' Strntwles for IAU'KO l'nwc!r P l n i i ~ ~ Incltidiuu .Nonut - lorin, Flow. EPA-GOQ/2-70-170, June 1070) nnd Enlrouy EnvlronmentnlL.ts (Lktcrmlnntion of Llrc Opllmum N u m h r Of Tritvcrsc k'oliib: A n Annlynls o f Mcllirul 1 CrlLcrln IdmIL). Coritrncl No. 68-Q1-3172)). the, number or Lravcrsc polnLI. for vclorlty inensurcnicnlr lips bccn reIJuccil und the ?:l lcnglh to uldL11 rallo rcriulreincrrt fur cros-secllonnl lny- 0111 01 r e # ! h n ~ ~ ~ I n ~ 'dilcts has bccn. rc- plncetl by n "bdlniicrd nintrix" scheme. 3. 0uldi:lluep . fo r sn1npUn8 In stncka
contntiiliic C ~ C I O I U C 'now nnd stncks smnller Llinn iiboiit 0.31 melrr in diam- ctcr or U.071 m' In craw-h~ctlonnl nrcx wlll ba liiibllslicd nt n Inter date. . 4. Clnrinu~tlon .Iir becn mndc NI .k,
when n elicck for cyclonlc llow Is ncccs- m y : nho. uio a s t : w L e d imwedure for delcrmiiintlon of unncceptuble flow con- dltlons hns bccn rcviscd.
'
. ' MrnloD 2 ' .
1. Thc cnllbrnllon of certain pltot tube8 h m bcen mnde optlond. ApProlwlnle con- ~ t r u c l l o n nnd oyiillcntloi~ guidelines have been Incllldcd.
' .z. A delnll?d cnlibrntlon bro&iire ror tenipernturc gnlwes bns becn Included. 3. A lcnk .check Procedure ior Pitot
: lln.c? lius bccii lncludcd. . -M&IIOD 3 ...
. .I
1: Tlie nvplicnitlllitrool the rneUiod has becn conrincd 'tu fos%ll-Iiicl roinbustloll procrssrs nnd to nlher proccsscs where I t hna b e n daltrrinlncd lhnt components othcr thnn 0:. CO,. CO. niid N, nre not present in conccntrntiom sufficient to .ancct tlic fliinl results.
2. Dnpd on rcccnt rcsearch Inlormn- tlon (PnrLlculnte Snrniiliiig Strntcgles for Lnrpu Powr? rlnttb Inchulir~s Noiiunl- 'iornt Plow. EI'A-GOO~2-7G-liil. Jlinc ~ ' J ~ u I . (he rixwircincnt for Iwoi)ortlonnl saml)linpl Iiiu 1)ccn druriued nnd rcplnccd. U.IUI L lw rcqiilrciiienl for conslnnt rate S W I I ~ I I I I ~ : , l'rolmr'tlonnl nnd eor:stniit mtc s n ~ , ~ l , i ~ n g h ~ : brrn roittld to give CSSCII- Unity 1.11~ snmc rcwlt .
3. The "tlirce culisrcullvc" require- ment l i i u be?n rolilnwd by "nny three"
. .. . . . , .. . -. c: 'nie &IC oi 'polycl.liylcne wu11 I,,,,. 11. The ilse of deslrcalik uthrr li?,...
LIPS irnd sample StOrnKe CnntnlncF;. . . ...... -. ~~~ ~
silica a c ~ or cnlcium sulfnto. wi l l , , appropriate.
e. nit? use of stoiicock crcwe ntlirr Limn slliconc grexve. when ~ ~ I ) ~ o I M I : , I ~ I. The drylnc 01 fllwrs mid probc-liii,r
ciilcli~s nt clevntcd tclnl~craturcr. BIW,, npprourinte.
E. The comblnlng or the flltrr niid probc -mshcs intu one contnlncr. 2. The leak chcch Prlor to n tcsl ~ I I I I
hns been .inn& optlonnl. The iast.trst Icxk chcck remnins ninndntory. A niulli. od for correctlw anmple vol~iine lor rs . ccsslve lcakwe rnter I ins been Iricludnl
3. Dewled lenk.check nnd Cnlibrnliw~ 'proccdurcs for the metcrrirs sysleq Iiwr been Included.
1.. Possible interfering agents of lhe n~cthod hnve bccn dclineated. 3. The optlolls of: (8) using n Mcthnl
8 .Impingcr systen,. or (b) drlcnniillnn SO, 6lmulcnneously with Iinrtiriilntr matter. have been Included i n the method. :
'3. Cased on recent research dnta. llic rcqulrcnicnt for prowrtional snnii~llnu hnr becn dropped N I ~ replaced wilh the rcqulrernent lor constniit rmte sniii~linu.
4. Tests have shoun thnl Liolrroiinliul ab'lnlncd from conimerci:il sourcrs oc- cn!lonally hna peroxlde Impurities thnl ~1.111 cause erroneously low SO: nicnsitre- ments. Tlirrelnrc. n test tor deleclinr wroxldei in Lsoixopnnol lim bccn hi- cludcd In the method.
5. The leak clicck bcrore the k s t RIII Iins bccn ninde rWinnul: Uic lctik ell+ nltcr the nln reinalns tnnndntrry. .
'
6. A dctailed calibration 1,rocctlure lor the irieterinb: zyslmn has been incluclrd in the method.
. . METIIOU 'I I , For vnrinblc wiivc IrnqtIi P I I I - C I I I I -
yllintonielcrs. n sr:iiinii)i: i~ ro t~ t Iu~ 'c l ' w dclcrmiiilng the iu~i i t or mnxlniiitii nli- sorbancc h:is bcrii iii~orpor:~l('iI 11:; i l l l opt 1011.
blrrtl,>il 8
bwn Ilstcd to nvold ~ I I S ; I ~ ~ J ~ C ~ I ~ I I I I O f t h e nirllinl.
2. The deLermln;itlml of flllvrtlbh' ~ I I tii.uIutc innticr t i i w l i i ~ l l r i l : tw1d n t h f I
Wii nlluu,cd whon: ui8idIcnbic. 3. Slncc occns!.l~n:tlly somr comwr-
r l i i l lp nrniluble guniiUtira of kwroiu!!~~I
11. IV?? P
~ ' .M&Oo 8 . .
1. xinowi ht~rrer1tv: r u n i p ~ ~ 1 1 1 i ~ 1 ~ hiiw
sIIIIuI1;III,~oIIsI." \ V l l h so, "1111 so. I W *
I.._.......__.. ~ ~
rctl~rrer. A s dcpied I n I Ell 2 or su!uarl A, lhc "AdmlnlulrnLcd' LIlvludcs nns nu- ll~orlmcl rfprcbclllnllw or Ule AdnilnlS- t.rnlor of tlie Envli'onln~:rrLnl ProlL'clInII Agrncy, AuthorlzCil rcI~rcs~:IlLntivcs nre ETA oln&lr 61 F:PA Ikcflnnnl OfBers or SLzlr. locnl. mid rceplnll:tl zovernnlenW otklnls who have bwn drlcmlcd llle re- sponsibility 01 enInrcillg I ' C A I I I ~ ~ I O I I S UII- der 40 CPR EO. T)lcrc nftlclnb 111 COIlSllltn- Won wltli othcr &lull nirlnbers lnllllllnr wlth tcchnlenl KqICcIS 01 SOIUCe ~ S l h l f i wlll mntlcr dreldons rrnnrcllng ncccpt- able alkrnnte l e s t prwnlurck. In ncrordnnce wiui sccLlon 111 of Lhc
Act. pUbllCnIIol1 of. Ulesc rnctllods wns prareddrd by consullnllon a i lh BPproLIrl- nlo advknIy rornmlttees. Independent experts. .and hdernl dcr)urlmenla m d anenclcs. , . .
?- , I 1 ,
I'
L
11756 RULES AND REGULATIONS
-n DUCT DIAMETERS UPSTREAM FROM'FLOW DISTURBANCE (DISTANCE A)
Figure
. . .
1-1. traverses.
. ,
. . .
. . . .
I( ......................... <...... .... I I: ...................... : ................... 4 u ,I .............................................. 4.4 1 ,. ........................................... 5-1 ................................................. n.n :Y) ............................................ : no .:u ............................................. *.a e:.. ....................... ..! ................ 1.a w .............................................. 1.1
3.x .......
I.' -. t
0 50
. a.
iJ i
4417.57 RULES AND REOUlhTION5
DUCT DIAMETERS UPSTREAM FROM FLOW DISTURBANCE (DISTANCE A) L. 2.5 ' 2.0 1 .o 1.5
I 1 1 - I 1 I I
-
- . . -
. .
" 0
traverses.
I - I I I ' 1 I 9 10. . : I I .; . .
- 7 8 . R 4 5 . 6 . .
RULES AND REGULATIONS
4 iRAvrnsE .I POIPIT
1 2 3 4 5 6
DISIANCC, 5 O f dlnnlrt lr
D 4.4 14 .7 29.5 70.5 85.3 95.6 ? q
3 J 4 9
Figure 1-3. Example Jiowing circular rlack'crai x i i o n divided into 12 equal areas, wiIh loCalion 01 IravelY poinll indicated.
. ' ' Table 1.2. LOCATION'OF TRAVERSE POINlS IN CIRCULAR STACKS . . .
{Percent of stack diameter from inside wall t o traverse point)
Traver pofn
nmbei on a
dlamett - - 24
1.1 3.2 5.5 7.9, 10.5 13.2..
-
16.1 19.4 !1.0 17.2 12.3 19.8 80.2 t7.7
'7.0 io. 6 ,3.9 6.8 9.5
4.5 6.8
.2: 8 '.
2.1,
0.3
r tr, 10
2.1 0.:
1 4 . 1
34;; 65.1 77.1 85.4 91 . E 97.4
- -
22: I
Int , 14
1 .I 5.; 9. ! 4.1 '0.1 '6.! 16.1 83.4 3.1 9 .1 5.4 0.1 4.3 8.2
- -
awl I8
1 . d
4.4 7.!
14.1 18.f 23.f 29.f
- -
10.:
!8.2 61 .8 70.4 16.4 11 .2
99.1 P2.5 95.6 98.6
35.4
rre - 12
2. 6.
11. 17. 25. 15. 54 * 75. 32. I B . , 13.. 17.1
- in a
16
1.6 4.3 8.5 12.5 16.9 22.0 20.3 37.5 62.5 71.7 78.0 01.1 87.5 91.5 95: 1 9 8 A
- - - 22
1 . I 3.5 6.0 8.1 11.6 14.6 18.0 21 .8 26.2 31.5 39.3 60.7 58.5
13.8 18.2
12.0 35.4 B.4 n . 3 14.0 16.5 10.1
- -
20
1. 3. .6.
. 9. 12. 16.' 20.' 25.1 30.1 38.1 61 .i 69.4 75.1 79.1 OI.! 37.1 90.2 93.2 9G.l 90.7
- 1 2 3 41 5' 1 , 6
8 $ 1
. . i
9 10 11
13 14 1 5 111 16 17
121
22
24 J 23
. . -
. , .
?SDDoAL L€Ul$l~1, VOL. '41. NO. IbO-THUISDAI. AVOUIl lI,"l977
i:
. ~ .. . . . . .. '2 ........... -.
c . .
RULES AND HtbUlAlIUNS U,.J.,
i
tll
Figure 2.1. Type S pitot tube manometer assembly.
, . .. .. . . ... ..
...
Figure 2.2. Properly constructed Type S pitot tube, shown in: (a) end view; face opening planes perpendicular to t r a w vcrsc axis; (b) top vicw; face opcnillg planes parallel to lon- gitudinal axis; (c) side view; both legs of equal length and centerlincs coincident, whcn viowed from both sides. Base- line cocflicient values of 0.84 may be assigiled to pitot tubes constructed . . , . this way., , , , ,
. . I
.
a a
CURVED OR MITERED JUNCTION
I)
STATIC HOLES\ I
(-0.10)
I I 12.. , HEM!SPHERICAl *
TIP
Figure 2.4.. Standard pitot tube design specifications.
RULES AND REGULAIIONS
-_- -.- P L A N T D A T E - R U N NO.
B A R O M E T R I C PRESSURE. mm Hy (in. 119)
OPERATORS PITOT TUBE 1.0. NO. --
STACK OIAP;ETCR O R I I I M E N S I O N S , m(ie.)
CROSS SECTIONAL A R E A , 1112(112) - -
-
A V G . C O i F F I C I E N T , C p = -- LAST D A T E CALIBRATED _-- S C I I C M A T I C O F S T A C K
CROSS S C C T I O N
’ . Averaga
1
Figure 2.5. Vclocity travcrse data. . . .
R D E U L ECGlSlEl, VOI. 42. NO. lOO--TIIUI5DAY. AUGUST 18, lW7
! RULES AND RCGULATIONS I
' I . ":
. . . . . . . . . . .
. . A. .BOTTOM VIEW; SHOWING MINIMUM PITOT-NOZZLE SEPARATION.' , . . ' . .
. . . . . . . . .
. ,
-.A,-
--.-. . . . .
. . . . .. STRf AMLINES APPROACHING THE
' . , '..NOZZLE,THE IMPACTPRESSURE , . . i
. . OPENING PLANE OFTHE PITOT TUBE SIIALL BE EVEN WITH OR ABOVE THE NOZZLE ENTRY PLAIIE.
, ,
Figure.2.6. Proper pitot'tube - sampling nozzle configuration to pr&eht aerodynamic interference; buttonhook - type nozzle:,centen of nozzle
318 in.). c
. . ,. and pitot opening aligncd; Dt between 0.48 and.0.95 cm (3/16 : . and ., .
:.. FEDLIAL UtOlSlII, V0l.I 41. NO. lbO-lHUI1DAV. AUOu$l la , 1Pr7 ' ' - '
. . . . . . . . : .I . . . . . . . . . . . . . . . . . . . , . . I , . . . . . . - ~. I . 2 . . .
1 ! , " . '. . . . , . . . . . . . . . . .. w. . . . . I.. , . .
,.-. d,,'..' .: . . .
. A . , . . I , ,. , . . . , .. ,. . 4 ;, .'.,, . . . *, . :
Ca m
, .. i , .
r I i .
TYPE SP1101 TUUC , Q bI Ot
RULES AND REGULATIONS $17(i>
Figure 2.7. Proper therrnocouplc placemcnl io prevent inlcrference: Dt bclween 0.48 and 0.95 c m I3/16 and 318 in.).
I
TYPES PITOTTUBE . I I I 1 - Y 27.62 cm (3 in.)
I I
Figure 2-8. Minimum pitot-sample probe separation needed to prevent interference; Dt between 0.48 and 0.95 cm (3/16 and 3/8 in.).
/
FEDIDAL RCGljlFl. VOL 42, NO. lb&lllURSOAV, A W U S l I D , I P 7 7 0
417tiG RULES AND REGLllATlONS
. . . .. . .
' . 3
' . . . T: IC,il).Z,IA OR 611 -C MUST BE (0.01 AVERAGE DEYlATlON 8 u IA OR 6 )
3 . "
..' Figure 2.9. Pilot tube calibrpiiondata. ..
. . I
I r;
1 " " / . . ,." PULES AND REGULATIONS
SHEATH .
(XI
.Figure 2-10. Projectdnrea models
EXTCRNAL 1
(bf
100
for typical phot tube assemblics.
EW"lh 2 5 -.v,(l-lf"J+lP.o 11,
FtDrIAL DWlS11R, VOl. 41. NO. :IbOcTHUISOAY, AUGVSl l D , 1 V T I
............. . . . . . . . . . . a'. i ? ....
, .,..
I l i M RULES AND RtGULATlONS
' Pirur T U D L IDINTIFICATION NUMBER: - , __ OAT€:--
-J I
-' I
. . ,..-... .̂" u r n " . ,
RULES AND REGULATIONS I
SOUEEZE D U L B '
Figure 3.1. Grabsampling train. . .
. . . , . .
. .
PRO
OUlCK DISCONNECT-
RIGID CONTAINER
E
Figure 3.2, Integrated gar.sampling train.
3 - i
.. . . ,.GI;.& . . . .
. .
RULES AND REGULATIONS
. . . .
\ . .
. ., . . ;:.
<; . . .
. . .
c e- .-. -
*I1771
. . . . .
R U L t S AND REGULATIONS . ' . . . . ,
. .
. ' . . r .
. . ,:. . . . . . . . . .
. 1 _I . I. . . . . . . : . . . . . . . . . ..' .
. . , . .I
. . I . . , . . - . , . , . . . . . .
. . .
. . . . . . . . . ,
" > ! . : , . .
. , . .
. . ,. ., ,. . ... , .:, ._I
. . . . . . . . : ,
. . . . . . .
. . . . . . . . . . . . . .. , . . , . ., ~.
. . . . . . . . . . . . . . . . .
. . . . . . . . . .
. . . . ...
. . . . . . /
. .
. . . . . . . . . . . . . . . . ,. i - . . , . .: . .
, . .,-. . I . . . .
' I I . . . . . . . . . . . . , , . . , .
. .
. .
I ! ' i . : .
1 1 . , !
, '1
I
!
f .' I '
. . , : . . . , -
. . . . . GAS VOLUME THROUGH
, ' METER. IVm). .,. RATE r i c ~ i x SETTING . .
mWiirin. (~GVrnin,) . . . .
. , ,3 (113) :. CLOCK TIME . .
. ..
. .
. .
. .
I
I I
I
I t
I
I
I
I
I
METER TEMPERATURE. OC (OF)
. .
. , . .
' 41775 RULES AND RCGULATIO~S
. . MIDGET, IMPINGERS . ,
. . .
. .
, :
. . . .
. . . . . . . . . . .
. , . .
. . . . . .
. .
.' . COMMENTS . . . ' ~ ' LOCATION . .
. . .
. . . . TEST : . ' \
. . . . .'. DATE . .
. ' OPERATOR . . . .
. . . . , . . . . .,
8AROMETRlC PRESSURE .. . . .
' . .' . : . ,
41770
. . . . . . ;. . I .
.; ::. . . . .i . . . . . .
. . . . . . . .
. " . . ..... . .
! , " : . . . . - . . . . . .
. . . . . . . , .
. . .
. .
. . .
. . .
. . RULES AND REGULATIONS
. . . . . ".' . ,
. . . .
. .
. . . . . .
. . . . . ...... ? . :(.s\: . . . . . . * ......
. .
. . . . . .
. . . . : . . . . . . . .
. . . . . . .
. . . > . : . . ,
. . . . . . . . .
I . . . . . .
, . . . . .
' I ' . . . . . . . . , .
. . . . .
. . , . . . I . . , . ' ,:/: , : , . . . . . . . . . . . . . . . . . . M u A L UOIIIH. (ioL;44 YQ 1W-IWfi~DAV;AUQWl I & 1 V n ,. . . . . . . . : ,
. . , , . . . .
pt
..
* 41777 i RULES AND REGULATIONS
IMPINGER TRAIN OPTIONA1.MAY BE REPLACEO TEMPERATUnE SENSOR
BY AN EOUIVALENT CONOCNSER
THERMOMETER CHECK VALVE
VACUUM LINE
IIEATEO AREA THEnMDMCTER
BY4'ASS VALVE
. .
' . . DRYGASMETER AIR:TIC.HT PUMP
i . I
RULES AND REGULATIONS
Plant-', --
Run No. -
Amoun: liquid lost,duting tiansport -
Date ' ,
F h r No.
. . .
Acetone wash volume. ml
Acstone . . blank conccntration;mg/mg (equalio11'54) . .
. . . Acetone wash blank, . . mg (equation 5.5) , '
: . .
. . . . Weight of pa+date :mat tw
. . .. .. . . . . . : ,
, . . . . . .
... . ., . ... . . . . , .
. . . . VOLUME OF LIOUID
... . WATER COLLECTED .... . . .
TOTAL VOLUME COLLECTED I ml
. CONVERT WEIGHT OF WATER TO VOLUME BY DIVIDING TOTAL WEIGHT INCREASE BY DENSITY OF WATER (lg/mlj.
INCREASE' ' r'VOLUhlE WATZR. ml 1 drnl
Flgure 5-3. Analytical dala.
. ,
. . . . . :
. . ~.
_ . . : I ._ 8 . . . . . . . . . . . . . [ 18-y .: .'. . :
. . . . . . . . -. . . . . . .
. .
. . . , . . . .
. .
. . . . - .._ ,
, . . . . . . .
. . ~ ~ . ~ . . . . . . . .
. .
. .
. . . . . . . . . . . . . . , . . . . . . .. . . . . .
RULllS AND REGULATIONS
... , . ..... , .
I I e e t
1 .
LOCATION
OPERATOR L " DATE
RUM YO.
SAMPLE BOX NO.
. . ,, . METERBOXNO.
METERAHB
417W
. ,
I '
.. . , .
. .
RULES AND RECUIA~IONS
I
I
WIBlfNTTEMPFRATURE BAROMETRIC PRESSURE
LSIUMEOM0ISTURE.X
CROBE LENGTtl.m ( I d , '
~ V E R A G E CALIBRATEO N O n L E DIAMETER.cmlin.)- . . , .
PROBE HEATERSETTING LEAK HATE, m~/nin,bfm)
PROBE LINER MATERIAL'
NOZZLE IOENTIFICATION NO.
Q
i L 1 , .
L
. ., 1 . . . . . $ .
... .
L
j ! , i' .,
RULES AND REGULATIONS
. .. Equntion 6-1
Equnlios 8-2
. . . .E:oualion 8-4
. flOCRA1 RfOlSlfR. VOL. 42, NO, lbO.--IHURSDAY,~AUOUSl, 18, 1977 I ' ,:..':: " . . . . . . .
~ . . , . . _ _ . i . .. J I ' .
. 4171M
4 JSTOMER ADDRESS .
JOR NO. '7 ; ) > ! J , CUSTOMER N O . , L O C A T I O N
R U N N O .
P w m # VM I PG
/ / - I ' ' ~ I ~ , DATE O F TEST
VCB , VCD Meter t3ox (f
V B F , VBG , VBH , V B I
A , cp , Y WAK , Y A J , WAL
, WTT 0 Engl 1 '-h l l n i t s
O!\!t.tK I C [ I t Its I A N . e u Pa (COMBUST 1 ON ONLY ) 0 I n c i n e r a t o r
. . I -., ,..
./!--A 1 Y ";7 -
_. . T i n R E A D I N G P R E S S . PITOT T E M P . ACT.
-- -
I a p I I ! . I I
I I I !
__- I
_._.- I ___.- I --I
JSTOMER A IIDK ES S
CUSTOMER NO. , L O C A T I O N --i
J O P N O :
RUN N O . // I f , DATE OF TEST
PBAR I VM I PG VCB , VCD
Meter Hox X
V B F , VBG , VBH , V B I
A , C P , y WAK , Y A J , WAL
, w r ~ , A N , e i UPR (COMBUST 1 ON ONLY )
a C o m b u s t i o n 0 Yetr I!:iits
MI:I' 1:l< i ' CI.OCK GM S T A C K S T A C K Oi< 11: I C E
T . r n A C T . TIFlt? POINI' R E A D I N G PRESS. P l T G T T E M P .
i TS I AH
I . . . . .
i I
. ._ -A-
. - ,.- .