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Home Browse Search My settings My alerts Shopping cart Help Articles All fields Author Advanced search Images Journal/ Book title Volume Issue Page Search tips EuroCereal 2011, December 6-7, 2011 Food Chemistry Copyright © 2011 Elsevier Ltd. All rights reserved Sample Issue Online | About this Journal | Submit your Article | Shortcut link to this Title New Article Feed Alert me about new Volumes / Issues Your selection(s) could not be saved due to an internal error. Please try again. Add to Favorites < Previous vol/iss | Next vol/iss > Font Size: Add to my Quick Links Volume 127, Issue 2, Pages 379-892 (15 July 2011) ScienceDirect - Food Chemistry, Volume 127, Issue 2, Pages 379-892 (15 July 2011) http://www.sciencedirect.com/science?_ob=PublicationURL&_tockey=%2..._urlVersion=0&_userid=5943419&md5=64e88e841106e2774662ecfd710b6d90 (1 of 19) [19/4/2554 9:49:52] Hub ScienceDirect Scopus SciTopics Applications Register Login Go to SciVal Suite Articles in Press articles 1 - 78 Diet effects on AOC in beef muscle using FRAP and TEAC assay. AOC in hydrophilic and lipophilic extracts. Minimum of 30 min of reaction time is necessary using both assays. Volumes 121 - 128 (2010 - 2011) Volume 128, Issue 1 pp. 1-258 (1 September 2011) Volume 127, Issue 4 pp. 1409-1910 (15 August 2011) Volume 127, Issue 3 pp. 893-1408 (1 August 2011) Volume 127, Issue 2 pp. 379-892 (15 July 2011) Volume 127, Issue 1 pp. 1-378 (1 July 2011) Volume 126, Issue 4 pp. 1515-2016 (15 June 2011) Volume 126, Issue 3 pp. 821-1514 (1 June 2011) Volume 126, Issue 2 pp. 395-820 (15 May 2011) Volume 126, Issue 1 pp. 1-394 (1 May 2011) Volume 125, Issue 4 pp. 1131-1520 (15 April 2011) Volume 125, Issue 3 pp. 803-1130 (1 April 2011) Volume 125, Issue 2 pp. 277-802 (15 March 2011) | | | | Open all previews General Papers Research highlights = Full-text available = Abstract only Editorial Board/Aims & Scope Page IFC Antioxidant enzyme activities and antioxidant capacity in longissimus muscle from bulls fed diets rich in polyunsaturated fatty acids Original Research Article Pages 379-386 Liliana Mahecha, Karin Nuernberg, Gerd Nuernberg, Jörg Martin, Eva Maria Hubbermann, Sandra Knoeller, Erik Claeys, Stefaan De Smet, Dirk Dannenberger Show preview | Related articles | Related reference work articles Show preview | Related articles | Related reference work articles 1 2 Purchase Purchase

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EuroCereal 2011, December 6-7, 2011

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Add to my Quick Links Volume 127, Issue 2, Pages 379-892 (15 July 2011)

ScienceDirect - Food Chemistry, Volume 127, Issue 2, Pages 379-892 (15 July 2011)

http://www.sciencedirect.com/science?_ob=PublicationURL&_tockey=%2..._urlVersion=0&_userid=5943419&md5=64e88e841106e2774662ecfd710b6d90 (1 of 19) [19/4/2554 9:49:52]

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Articles in Press

articles 1 - 78

► Diet effects on AOC in beef muscle using FRAP and TEAC assay. ► AOC in hydrophilic and lipophilic extracts. ► Minimum of 30 min of reaction time is necessary using both assays.

Volumes 121 - 128 (2010 - 2011)Volume 128, Issue 1 pp. 1-258 (1 September 2011)Volume 127, Issue 4 pp. 1409-1910 (15 August 2011)Volume 127, Issue 3 pp. 893-1408 (1 August 2011)Volume 127, Issue 2 pp. 379-892 (15 July 2011)Volume 127, Issue 1 pp. 1-378 (1 July 2011)Volume 126, Issue 4 pp. 1515-2016 (15 June 2011)Volume 126, Issue 3 pp. 821-1514 (1 June 2011)Volume 126, Issue 2 pp. 395-820 (15 May 2011)Volume 126, Issue 1 pp. 1-394 (1 May 2011)Volume 125, Issue 4 pp. 1131-1520 (15 April 2011)Volume 125, Issue 3 pp. 803-1130 (1 April 2011)Volume 125, Issue 2 pp. 277-802 (15 March 2011)

| | | | Open all previews

General Papers

Research highlights

= Full-text available

= Abstract only

Editorial Board/Aims & Scope Page IFC

Antioxidant enzyme activities and antioxidant capacity in longissimus muscle from bulls fed diets rich in polyunsaturated fatty acids Original Research Article Pages 379-386 Liliana Mahecha, Karin Nuernberg, Gerd Nuernberg, Jörg Martin, Eva Maria Hubbermann, Sandra Knoeller, Erik Claeys, Stefaan De Smet, Dirk Dannenberger

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ScienceDirect - Food Chemistry, Volume 127, Issue 2, Pages 379-892 (15 July 2011)

http://www.sciencedirect.com/science?_ob=PublicationURL&_tockey=%2..._urlVersion=0&_userid=5943419&md5=64e88e841106e2774662ecfd710b6d90 (2 of 19) [19/4/2554 9:49:52]

► Indigenous siderophoregenic and probiotic strain Escherichia spp. (ST2) was isolated from healthy infant. ► Under artificial micro-aerophilic intestinal conditions, the isolate produced 2,3-dihydroxybenzoylserine which is catecholate type of siderophore. ► This isolate obeyed probiotic criteria according to the guideline of FAO/WHO (2002) and proved its sustenance in intestinal stressed in vitro conditions. ► Hence, this siderophoregenic culture may be useful in iron nutrition, but only after conducting proper animal and human trials.

► Nomilin and limonin from Citrus jambhiri peel. ► C. jambhiri extracts with strong DPPH* scavenging activity. ► Lipoxygenase inhibition indicates anti-inflammatory activity of C. jambhiri. ► Cytotoxicity of polymethoxyflavones against COS7, HeLa and Caco-2 cell lines.

► Rutin (50–100 μM) reduced proliferation of GL-15 glioblastoma cells. ► Rutin induced a decrease in levels of ERK1/2 phosphorylation in glioblastoma cells. ► The majority (87.4%) of glioblastoma cells exposed to 100 μM entered in apoptosis. ► Rutin induced astroglial differentiation in remaining glioblastoma cells.

► Water extracts of P. cornucopiae fruiting body showed antihypertensive ACE inhibitory activity. ► Antihypertensive ACE inhibitor was purified by chromatography methods. ► Water extracts of P. cornucopiae fruiting body showed a clear antihypertensive effect on SHR. ► P. cornucopiae fruiting body can be used as the functional food or nutraceutical compounds.

Volume 125, Issue 1 pp. 1-276 (1 March 2011)Volume 124, Issue 4 pp. 1289-1776 (15 February 2011)Volume 124, Issue 3 pp. 697-1288 (1 February 2011)Volume 124, Issue 2 pp. 411-696 (15 January 2011)Volume 124, Issue 1 pp. 1-410 (1 January 2011)Volume 123, Issue 4 pp. 959-1356 (15 December 2010)Volume 123, Issue 3 pp. 563-958 (1 December 2010)Volume 123, Issue 2 pp. 203-562 (15 November 2010)Volume 123, Issue 1 pp. 1-202 (1 November 2010)Volume 122, Issue 4 pp. 937-1350 (15 October 2010)Volume 122, Issue 3 pp. 471-936 (1 October 2010)Volume 122, Issue 2 pp. 387-470 (15 September 2010) 5th Conference on Water in FoodVolume 122, Issue 1 pp. 1-386 (1 September 2010)Volume 121, Issue 4 pp. 923-1318 (15 August 2010)Volume 121, Issue 3 pp. 639-922 (1 August 2010)Volume 121, Issue 2 pp. 307-638 (15 July 2010)Volume 121, Issue 1 pp. 1-306 (1 July 2010)Volumes 111 - 120 (2008 - 2010)Volumes 101 - 110 (2007 - 2008)Volumes 91 - 100 (2005 - 2007)Volumes 81 - 90 (2003 - 2005)Volumes 71 - 80 (2000 - 2003)Volumes 61 - 70 (1998 - 2000)Volumes 51 - 60 (1994 - 1997)Volumes 41 - 50 (1991 - 1994)Volumes 31 - 40 (1989 - 1991)Volumes 21 - 30 (1986 - 1988)Volumes 11 - 20 (1983 - 1986)Volumes 1 - 10 (1976 - 1983)

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A potential probiotic culture ST2 produces siderophore 2,3-dihydroxybenzoylserine under intestinal conditions Original Research Article Pages 387-393 Jayesh J. Ahire, Kanchankumar P. Patil, Bhushan L. Chaudhari, Sudhir B. Chincholkar

Chemical composition and biological activity of Citrus jambhiri Lush Original Research Article Pages 394-403 Dalia Hamdan, Mahmoud Zaki El-Readi, Ahmad Tahrani, Florian Herrmann, Dorothea Kaufmann, Nawal Farrag, Assem El-Shazly, Michael Wink

Antiproliferative, proapoptotic and morphogenic effects of the flavonoid rutin on human glioblastoma cells Original Research Article Pages 404-411 B.L. Santos, A.R. Silva, B.P.S. Pitanga, C.S. Sousa, M.S. Grangeiro, B.O. Fragomeni, P.L.C. Coelho, M.N. Oliveira, N.J. Menezes-Filho, M.F.D. Costa, R.S. El-Bachá, E.S. Velozo, G.P. Sampaio, S.M. Freire, M. Tardy, S.L. Costa

Characterisation of a new antihypertensive angiotensin I-converting enzyme inhibitory peptide from Pleurotus cornucopiae Original Research Article Pages 412-418 Jeong-Hoon Jang, Seung-Chan Jeong, Jeong-Han Kim, Yun-Hae Lee, Young-Cheoul Ju, Jong-Soo Lee

In vitro scavenging capacity of annatto seed extracts against reactive oxygen and nitrogen species Original Research Article Pages 419-426 Renan Campos Chisté, Adriana Zerlotti Mercadante, Ana Gomes, Eduarda Fernandes, José Luís Fontes da Costa Lima, Neura Bragagnolo

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ScienceDirect - Food Chemistry, Volume 127, Issue 2, Pages 379-892 (15 July 2011)

http://www.sciencedirect.com/science?_ob=PublicationURL&_tockey=%2..._urlVersion=0&_userid=5943419&md5=64e88e841106e2774662ecfd710b6d90 (3 of 19) [19/4/2554 9:49:52]

► Annatto seed extracts as efficient in vitro scavengers of ROS and RNS. ► Bixin possesses high scavenging activity against ROS and RNS. ► Hypolaetin and caffeoyl acid derivative: the main phenolic compounds in annatto seeds.

► Phenolic profile and antioxidant properties of Dalmatian sage leaves. ► Influence of phenophase was explored. ► Sage leaves extracts are rich source of valuable phenolics, mainly phenolic acids. ► The presence of resveratrol or its derivatives was confirmed in all extracts. ► The best antioxidant properties were obtained for May sage extracts.

► A novel polysaccharide isolated from Acanthopanax senticosu. ► The characterisation was characterised. ► Demonstrated that had stronger immunomodulatory and antioxidant activities.

► Wild wine Saccharomyces strains consume less amino acids than commercial yeasts. ► Industrial dehydration process might increase yeasts nitrogen necessities. ► Some amino acids are released into the medium before autolysis phase. ► Mixed cultures modify amino acid uptake with regard to monoculture fermentations.

► UHPH prevent degradation of phenolic compounds. ► Vitamin C is preserved in UHPH treated samples. ► The antioxidant capacity do not decrease by effect of UHPH treatment. ► UHPH rends better product than thermal treatment does.

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Influence of the phenophase on the phenolic profile and antioxidant properties of Dalmatian sage Original Research Article Pages 427-433 Ivana Generalić, Danijela Skroza, Ivica Ljubenkov, Ana Katalinić, Franko Burčul, Višnja Katalinić

Antioxidant and immunobiological activity of water-soluble polysaccharide fractions purified from Acanthopanax senticosu Original Research Article Pages 434-440 Ruizhan Chen, Zhiqiang Liu, Jimin Zhao, Ruiping Chen, Fanlei Meng, Min Zhang, Wencheng Ge

Amino acid uptake by wild and commercial yeasts in single fermentations and co-fermentations Original Research Article Pages 441-446 N. Barrajón-Simancas, E. Giese, M. Arévalo-Villena, J. Úbeda, A. Briones

Influence of ultra-high pressure homogenisation on antioxidant capacity, polyphenol and vitamin content of clear apple juice Original Research Article Pages 447-454 Ángela Suárez-Jacobo, Corinna E. Rüfer, Ramón Gervilla, Buenaventura Guamis, Artur X. Roig-Sagués, Jordi Saldo

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ScienceDirect - Food Chemistry, Volume 127, Issue 2, Pages 379-892 (15 July 2011)

http://www.sciencedirect.com/science?_ob=PublicationURL&_tockey=%2..._urlVersion=0&_userid=5943419&md5=64e88e841106e2774662ecfd710b6d90 (4 of 19) [19/4/2554 9:49:52]

► Malva nut mucilage has been widely consumed in Thailand in the past few years. ► Little is known about health benefit of malva nut gum. ► Our laboratory has succeeded in producing dietary fibers extracted from malva nut seeds. ► Results in this study show the potential use in body if one uses it with suitable condition.

Based on the NMR spectral data of the irradiated beef samples: ► A trend toward an increase in the amount of saturated fatty acids was detected. ► A decrease in the amount of polyunsaturated fatty acids was established. ► An approach for estimation of the irradiation dose was proposed.

► TAG positional isomers in marine organisms were separated by polymeric ODS column. ► TAG positional isomers in marine mammals mainly bind DHA or EPA at the α position. ► TAG positional isomers in fish mainly bind DHA or EPA at the β position.

► pH and temperature affect the interaction of volatile compounds with yeast autolysates. ► Aromas can be fixed in model solution, while salting out effects occurred in wine. ► This was probably due to the presence of interfering compounds in wine. ► e.g., Highly concentrated wine volatile compounds can reduce aroma fixation. ► High temperatures (37 °C) can promote the release of the aromas previously bound.

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In vitro retardation of glucose diffusion with gum extracted from malva nut seeds produced in Thailand Original Research Article Pages 455-460 Anchalee Srichamroen, Visith Chavasit

Effect of gamma-ray irradiation on the fatty acid profile of irradiated beef meat Original Research Article Pages 461-466 Rayna Stefanova, Stoyan Toshkov, Nikola V. Vasilev, Nikolay G. Vassilev, Ilko N. Marekov

Actual ratios of triacylglycerol positional isomers consisting of saturated and highly unsaturated fatty acids in fishes and marine mammals Original Research Article Pages 467-472 Naohiro Gotoh, Yumiko Matsumoto, Toshiharu Nagai, Hoyo Mizobe, Ikuko Otake, Kenji Ichioka, Ikuma Kuroda, Hiroyuki Watanabe, Noriko Noguchi, Shun Wada

Interactions between yeast autolysates and volatile compounds in wine and model solution Original Research Article Pages 473-480 Piergiorgio Comuzzo, Lara Tat, Dennis Fenzi, Laura Brotto, Franco Battistutta, Roberto Zironi

Effect of ripening on protein content and enzymatic activity of Crimson Seedless table grape Original Research Article Pages 481-486 S. López-Miranda, P. Hernández-Sánchez, A. Serrano-Martínez, P. Hellín, J. Fenoll, E. Núñez-Delicado

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ScienceDirect - Food Chemistry, Volume 127, Issue 2, Pages 379-892 (15 July 2011)

http://www.sciencedirect.com/science?_ob=PublicationURL&_tockey=%2..._urlVersion=0&_userid=5943419&md5=64e88e841106e2774662ecfd710b6d90 (5 of 19) [19/4/2554 9:49:52]

► The year had an effect on the evolution of protein content, PPO and POD activity and °Brix in Crimson Seedless. ► The increase in protein synthesis observed after veraison is not related to PPO and POD activity. ► The maximum in specific activity at veraison may be correlated with changes in protein and anthocyanin content that take place during colour synthesis.

► The allergenic whey protein β-lactoglobulin was hydrolysed by L. bulgaricus CRL656. ► The strain cleaved three main epitopes of β-lactoglobulin (BLG). ► BLG allergenicity, assessed with sera from allergic children, was reduced in vitro. ► The studied strain could be used for formulating novel hypoallergenic foods. ► It is the first study on the allergenic response of hydrolysed BLG by Lactobacillus.

► Literature data lack of information about the nutraceutical power of new hybrids. ► This study aimed to evaluate the effect of the cv, tissue and storage on the antiradical activity. ► Results underlined the key role of the genotype on the content of the nutraceutical power of apples.

► Onion by-products are useful as dietary fibre ingredients. ► Sterilisation improve dietary fibre characteristics. ► Sterilisation is a good method to stabilise onion by-products.

► Indigenous proteases hydrolysed gelatin from skin of unicorn leatherjacket during extraction. ► Soybean trypsin inhibitor (SBTI) could prevent the degradation of gelatin during extraction. ► Gelatin extracted in the presence of SBTI had the improved functional properties.

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Proteolytic action of Lactobacillus delbrueckii subsp. bulgaricus CRL 656 reduces antigenic response to bovine β-lactoglobulin Original Research Article Pages 487-492 Micaela Pescuma, Elvira María Hébert, Hanitra Rabesona, Martine Drouet, Yvan Choiset, Thomas Haertlé, Fernanda Mozzi, Graciela Font de Valdez, Jean-Marc Chobert

Phenolic composition and free radical scavenging activity of different apple varieties in relation to the cultivar, tissue type and storage Original Research Article Pages 493-500 K. Carbone, B. Giannini, V. Picchi, R. Lo Scalzo, F. Cecchini

Effect of sterilisation on dietary fibre and physicochemical properties of onion by-products Original Research Article Pages 501-507 Vanesa Benítez, Esperanza Mollá, María A. Martín-Cabrejas, Yolanda Aguilera, Francisco J. López-Andréu, Rosa M. Esteban

Indigenous proteases in the skin of unicorn leatherjacket (Alutherus monoceros) and their influence on characteristic and functional properties of gelatin Original Research Article Pages 508-515 Mehraj Ahmad, Soottawat Benjakul, Mahmoudreza Ovissipour, Thummanoon Prodpran

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ScienceDirect - Food Chemistry, Volume 127, Issue 2, Pages 379-892 (15 July 2011)

http://www.sciencedirect.com/science?_ob=PublicationURL&_tockey=%2..._urlVersion=0&_userid=5943419&md5=64e88e841106e2774662ecfd710b6d90 (6 of 19) [19/4/2554 9:49:52]

► Cover crops in vineyard have the potential improvement of wine flavour. ► Eleven impact odorants were revealed in the wines from cover crops and clean tillage. ► Alfalfa cover crop was the best to enhance wine flavour, tall fescue was the next.

► High PPO and POD activities led to browning in water caltrop. ► Enzymatic browning is responsible for discolouration of caltrop. ► Food quality of light-coloured surface can be preserved during postharvest.

► All the techniques studied released total and neutral polysaccharides. ► The type and content of polysaccharides depended on the technique and the yeast derivative added. ► No clear effect was observed with the use of β-glucanase enzymes. ► The application of lees and micro-oxygenation enhances the formation of new pigments. ► From the sensorial point of view, some wines were better valued than the control wines.

► Prepared rice starch gels mixed with konjac glucomannan, xanthan gum, and agar. ► Effects of NSP on the starch digestibility and rheological properties were investigated. ► Clarified that added NSP suppressed starch hydrolysis in the starch gel. ► The impact of NSP on the rheological properties of starch gels depended on the type of NSP. ► The suppressive effect of NSP on starch digestibility was not only due to the gel rigidity.

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Impact of cover crops in vineyard on the aroma compounds of Vitis vinifera L. cv Cabernet Sauvignon wine Original Research Article Pages 516-522 Zhu-mei Xi, Yong-sheng Tao, Li Zhang, Hua Li

The role of polyphenol oxidase and peroxidase in the browning of water caltrop pericarp during heat treatment Original Research Article Pages 523-527 Jhih-Ying Ciou, Hsin-Hung Lin, Po-Yuan Chiang, Chiun-C. Wang, Albert Linton Charles

Techniques for improving or replacing ageing on lees of oak aged red wines: The effects on polysaccharides and the phenolic composition Original Research Article Pages 528-540 Rubén Del Barrio-Galán, Silvia Pérez-Magariño, Miriam Ortega-Heras

Effect of non-starch polysaccharides on the in vitro digestibility and rheological properties of rice starch gel Original Research Article Pages 541-546 Tomoko Sasaki, Kaoru Kohyama

Evaluation of different Saccharomyces cerevisiae strains on the profile of volatile compounds and polyphenols in cherry wines Original Research Article Pages 547-555 Shu Yang Sun, Wen Guang Jiang, Yu Ping Zhao

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ScienceDirect - Food Chemistry, Volume 127, Issue 2, Pages 379-892 (15 July 2011)

http://www.sciencedirect.com/science?_ob=PublicationURL&_tockey=%2..._urlVersion=0&_userid=5943419&md5=64e88e841106e2774662ecfd710b6d90 (7 of 19) [19/4/2554 9:49:52]

► Different strains exhibited diverse volatile and polyphenol profiles in cherry wines. ► RA17 and GRE wines had more esters and acids; D254 wine contained more alcohols. ► BM4×4 and D21 extracted most phenolics; RA17 and GRE had similar polyphenol profiles. ► RC212 and D254 cherry wines were characterised by the abundance of anthocyanins. ► Each two strains performed similarly: (1) RA17, GRE; (2) RC212, D254; (3) BM4×4, D21.

► Antioxidant capacity of rapeseed varieties was determined. ► Antioxidants content in rapeseed differ significantly. ► Total glucosinolates and erucic acid contents varied among rapeseed cultivars. ► Total phenolics in rapeseed varieties correlated with their antioxidant capacity. ► Darker rapeseed cultivars contain higher levels of antioxidants.

► Leaves of five Ligustrum plants are described in Taiwan flora and used as health tea. ► Ligustrum plants leaves exhibit appreciate radical-scavenging capacity against ROS. ► Ligustrum plants leaves inhibit lipid peroxidation and haemolysis in cell-based models. ► Ligustrum morrisonense is a potential source of natural antioxidants.

► Ethylene gas is encapsulated into α-cyclodextrin. ► Ethylene concentration remains unchanged in inclusion complex but complex yield increases over pressure and time changes. ► Crystalline complex is characterised by X-ray diffractometry, solid-state NMR, thermal analysis, scanning electron microscopy and Fourier transform infrared spectroscopy.

► Lippia multiflora herbal tea is a good source of phenylethanoid glycosides (PhGs). ► PhGs constituted ca 15% of the hot water-soluble solids. ► Verbascoside was present in the highest concentration. ► Steam pasteurisation of the leaves did not affect the PhG content of the infusion.

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Antioxidant capacity, total phenolics, glucosinolates and colour parameters of rapeseed cultivars Original Research Article Pages 556-563 Aleksandra Szydłowska-Czerniak, Iwona Bartkowiak-Broda, Igor Karlović, György Karlovits, Edward Szłyk

Evaluation of the antioxidant activity of five endemic Ligustrum species leaves from Taiwan flora in vitro Original Research Article Pages 564-571 Chi-Rei Wu, Wen-Hsin Lin, You-Cheng Hseu, Jin-Cherng Lien, Yung-Ta Lin, Tzu-Ping Kuo, Hui Ching

Encapsulation of ethylene gas into α-cyclodextrin and characterisation of the inclusion complexes Original Research Article Pages 572-580 Binh T. Ho, Daryl C. Joyce, Bhesh R. Bhandari

Phenylethanoid glycosides as major antioxidants in Lippia multiflora herbal infusion and their stability during steam pasteurisation of plant material Original Research Article Pages 581-588 Hanson Arthur, Elizabeth Joubert, Dalene De Beer, Christiaan J. Malherbe, R. Corli Witthuhn

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ScienceDirect - Food Chemistry, Volume 127, Issue 2, Pages 379-892 (15 July 2011)

http://www.sciencedirect.com/science?_ob=PublicationURL&_tockey=%2..._urlVersion=0&_userid=5943419&md5=64e88e841106e2774662ecfd710b6d90 (8 of 19) [19/4/2554 9:49:52]

► The stability of intermediate moisture green tea apple products was studied at 30 °C. Stability rankings were dihydrochalcones, chlorogenic acid > flavan 3-ols > ascorbic acid. The half-life for antioxidant activity was 165 d at aw of 0.75. The anti-glycoxidative properties did not change over 2 months. Consumption of these

products could inhibit oxidative- and glycoxidative-related diseases.

► Pressure inhibit the browning of glucose–ammonium sulphite caramel solutions. ► Pressure could promote the condensation reaction between

/ammonium and glucose. ► Pressure increases dissociative

content and limits N-glucosamine formation. ► Pressure leads to a retardation of the degradation of the ARP.

► Identical the thousand achenes weight and achene yield in organic and conventional farming. ► Higher level of rutin and epicatechin gallate in organic groats. ► Rutin and epicatechin dominant flavonoids in buckwheat groats. ► Presence of catechin and epicatechin gallate in buckwheat groats.

► Two new cucurbitane triterpenoids have isolated from Momordica charantia ► Several constituents were identified as XO inhibitor or displayed ABTS + or O2•−

scavenging activity or indicated ORAC-PGR values. ► These findings showed that these constituents may be used as antioxidant.

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Stability and anti-glycation properties of intermediate moisture apple products fortified with green tea Original Research Article Pages 589-595 Vera Lavelli, Mark Corey, William Kerr, Claudia Vantaggi

Effects of pressure on the glucose–ammonium sulphite caramel solutions Original Research Article Pages 596-601 Yong-Guang Guan, Pei Yu, Shu-Juan Yu, Xian-Bing Xu, Wen-Hui Shi, Wei-Wei Sun

The influence of organic and conventional crop management, variety and year on the yield and flavonoid level in common buckwheat groats Original Research Article Pages 602-608 Jana Kalinova, Nadezda Vrchotova

Antioxidant constituents from the stems and fruits of Momordica charantia Original Research Article Pages 609-614 Kai-Wei Lin, Shyh-Chyun Yang, Chun-Nan Lin

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ScienceDirect - Food Chemistry, Volume 127, Issue 2, Pages 379-892 (15 July 2011)

http://www.sciencedirect.com/science?_ob=PublicationURL&_tockey=%2..._urlVersion=0&_userid=5943419&md5=64e88e841106e2774662ecfd710b6d90 (9 of 19) [19/4/2554 9:49:53]

► First analysed the main nutrients and phenolic composition of S. gracilis root. ► First studied the antioxidant activity and DNA damage protective effect of the root. ► Microstructure of S. gracilis root was observed by SEM. ► Compared the phytochemicals and biological activities of S. gracilis roots harvested at different time.

► Enzymatic pomace treatment had a positive effect on the production of puree-enriched cloudy apple juices. ► Puree-enriched cloudy apple juices were high in antioxidant phenolics. ► After enzymatic treatment of pomace there were increased contents of polymeric procyanidins in puree-enriched cloudy juices. ► The use of apple pomace as a technological alternative to mechanical press. ► This processing is promising for the production of new beverages or drinks as a good source of natural bioactive compounds.

► The first study of heavy metals in Mytilus galloprovincialis and sediments. ► The coastal area of Montenegro, southeastern Adriatic Sea, in two seasons. ► Correlation analysis between metals found in mussels and sediments. ► The study data were compared with data from the south to northeast Adriatic Sea. ► Evaluation of the mussels quality and possible risks of their consumption.

► Non-previously described tomato allergen (ARP60S) obtained by molecular biology. ► ARP60S is related with allergic sensitisation and shows IgE binding capacity. ► Tomato ARP60S shares high homology with previous described allergens in almond and moulds.

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Main nutrients, phenolics, antioxidant activity, DNA damage protective effect and microstructure of Sphallerocarpus gracilis root at different harvest time Original Research Article Pages 615-622 Chun-yan Gao, Yue-hong Lu, Cheng-rui Tian, Jian-guo Xu, Xiao-peng Guo, Rui Zhou, Guo Hao

Effect of pectinase treatment on extraction of antioxidant phenols from pomace, for the production of puree-enriched cloudy apple juices Original Research Article Pages 623-631 Jan Oszmiański, Aneta Wojdyło, Joanna Kolniak

Trace metal concentrations in Mediterranean blue mussel and surface sediments and evaluation of the mussels quality and possible risks of high human consumption Original Research Article Pages 632-637 Danijela Joksimovic, Ilija Tomic, Ana R. Stankovic, Mihajlo Jovic, Slavka Stankovic

Acidic ribosomal protein 60S: A new tomato allergen Pages 638-640 M.A. López-Matas, A. Ferrer, C.H. Larramendi, A.J. Huertas, J.A. Pagán, J.L. García-Abujeta, J. Bartra, C. Andreu, J.R. Lavín, J. Carnés

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ScienceDirect - Food Chemistry, Volume 127, Issue 2, Pages 379-892 (15 July 2011)

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► Starfruit is a popular tropical fruit, with potential health promoting properties. ► This is the first report on the effects of ultraviolet (UV) radiation on starfruits. ► UV was effective in reducing the microbial load of starfruit juice. ► UV enhanced some of the bioactive antioxidant compounds in starfruit juice. ► Results obtained will be useful for the implementation of UV technology on a pilot scale.

► Moisture and fat contents two important parameters in quality evaluation of fried chicken nuggets. ► VIS/NIR spectral analysis a straightforward and fast method for Prediction. ► VIS/NIR instrument capable of doing the analysis in few min.

► A RF-MEKC method for green tea catechins was developed and validated. ► It allowed baseline separation of five catechins in 4 min. ► Demonstrating excellent performance, it was applied to Brazilian green tea samples.

► The %metMb in tuna extract was estimated using equations derived from horse Mb. ► The results showing different %metMb were obtained with the different equations. ► This discrepancy was due to difference in absorption spectra of horse and tuna Mb. ► New set of equations derived from absorption spectra of tuna Mb was established.

Research highlights

Analytical Methods

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Quality attributes of starfruit (Averrhoa carambola L.) juice treated with ultraviolet radiation Pages 641-644 Rajeev Bhat, Suhaida Binti Ameran, Han Ching Voon, A.A. Karim, Liong Min Tze

VIS/NIR hyper-spectroscopy technique for the measurement of moisture and fat contents of breaded-fried chicken nuggets Original Research Article Pages 645-650 A. Yavari, A. Heshmati, M. Hamedi, S. Haghbin

Determination of catechins in green tea infusions by reduced flow micellar electrokinetic chromatography Original Research Article Pages 651-655 Renato G. Peres, Fernando G. Tonin, Marina F.M. Tavares, Delia B. Rodriguez-Amaya

Equations for spectrophotometric determination of relative concentrations of myoglobin derivatives in aqueous tuna meat extracts Original Research Article Pages 656-661 Chotika Viriyarattanasak, Naoko Hamada-Sato, Manabu Watanabe, Kazuhito Kajiwara, Toru Suzuki

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► Volatiles of fermented Antrodia camphorata were analysed by HS-SPME–GC–MS. ► Aroma of fermented A. camphorata was evaluated by HS-SPME–GC–O. ► HS-SPME condition for the volatiles was extensively optimised by a D-optimal design.

► Both protein extraction and immunoreactivity are affected by the baking process. ► The use of ELISA for the detection of milk proteins is severely compromised for incurred samples. ► The method used for sample dilution can affect the quantitative result by ELISA.

► Caseins and other chelatants differently bind calcium. ► We measured ionic calcium during titration of the molecules. ► We fitted the calcium-binding isotherms using a modelling approach. ► We determined the calcium-binding parameters of the different molecules.

► Only small quantity of organic solvent was used in analytical process. ► It was a rapid, sensitive, convenient and practical method. ► Used cloud point extraction for determination of organophosphorus pesticides.

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Analysis of volatile compounds of Antrodia camphorata in submerged culture using headspace solid-phase microextraction Original Research Article Pages 662-668 Zhen-Ming Lu, Wen-Yi Tao, Hong-Yu Xu, Joanne Lim, Xiao-Mei Zhang, Li-Ping Wang, Jing-Hua Chen, Zheng-Hong Xu

Influence of baking time and matrix effects on the detection of milk allergens in cookie model food system by ELISA Original Research Article Pages 669-675 Linda Monaci, Marcel Brohée, Virginie Tregoat, Arjon van Hengel

Determination of calcium-binding constants of caseins, phosphoserine, citrate and pyrophosphate: A modelling approach using free calcium measurement Original Research Article Pages 676-682 Omar Mekmene, Frédéric Gaucheron

Cloud point extraction coupled with ultrasonic-assisted back-extraction for the determination of organophosphorus pesticides in concentrated fruit juice by gas chromatography with flame photometric detection Original Research Article Pages 683-688 Wei-jun Zhao, Xiao-ke Sun, Xiao-ni Deng, Lin Huang, Ming-min Yang, Zhi-ming Zhou

Volatile compounds of leaves and fruits of Mangifera indica var. coquinho (Anacardiaceae) obtained using solid phase microextraction and hydrodistillation Original Research Article Pages 689-693 Sâmya Soler Gebara, Wellyta de Oliveira Ferreira, Nilva Ré-Poppi, Euclésio Simionatto, Eduardo Carasek

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ScienceDirect - Food Chemistry, Volume 127, Issue 2, Pages 379-892 (15 July 2011)

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► The HS-SPME offers net advantages in term of isolation time and contributes with “green chemistry”. ► Some components of leaves and fruits varied significantly according to maturation periods. ► The cluster analysis showed low correlation among the extraction techniques HS-SPME and HD.

► The electrochemical behaviours of luteolin was investigated at MWNTs modified glassy carbon electrode (MWNTs/GCE) ► The detection limit of 6.0 × 10−11 M is achieved based on MWNTs/GCE, which is much lower than that reported in literature. ► The modified GCE have a good stability and repeatability for the detection of luteolin. ► The analytical performance of this sensor has been evaluated for detection of luteolin in peanut hulls as a real sample.

► The flavones were irreversibly oxidised at the platinum electrode. ► The first step includes the electrooxidation of hydroxyl groups in the ring B. Oxidation of one –OH group proceeds with an exchange of one electron. ► Hydroxyl groups in the rings A and C are probably oxidised in subsequent steps. ► If the number of –OH groups increases, a slower oxidation rate is observed.

► Partial binding parameters of vanillin to HSA were revealed by molecular docking. ► Physicochemical properties of vanillin to HSA were detected by fluorescence. ► Secondary structure of HSA were measured by CD and FT-IR spectroscopic methods.

► In a conventional method for the microbiological determination of water-soluble vitamins, the growth of the microorganism in relation to the vitamin is measured as turbidity. ► The WST-8 colorimetric method has been applied to the rapid proliferation assay of microorganisms. ► Compared with a conventional method, the application of WST-8 colorimetric method to a microbiological determination of water-soluble vitamins could lead to a decrease in incubation times and a good reproducibility in the assay. ► The WST-8 colorimetric assay is a useful method for the rapid and accurate determination of vitamin B6, biotin, folic acid, niacin, and

pantothenic acid in a 96-well microtiter plate.

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Sensitive electrochemical determination of luteolin in peanut hulls using multi-walled carbon nanotubes modified electrode Original Research Article Pages 694-698 Dongming Zhao, Xiuhua Zhang, Lijun Feng, Qiong Qi, Shengfu Wang

Electrooxidation of flavonoids at platinum electrode studied by cyclic voltammetry Original Research Article Pages 699-704 Anna Masek, Marian Zaborski, Ewa Chrzescijanska

Application of molecular modelling and spectroscopic approaches for investigating binding of vanillin to human serum albumin Original Research Article Pages 705-710 Xiaoru Wang, Xiaoyun Xie, Cuiling Ren, Ying Yang, Xiangmei Xu, Xingguo Chen

Determination of water-soluble vitamins using a colorimetric microbial viability assay based on the reduction of water-soluble tetrazolium salts Original Research Article Pages 711-715 Tadayuki Tsukatani, Hikaru Suenaga, Munetaka Ishiyama, Takatoshi Ezoe, Kiyoshi Matsumoto

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ScienceDirect - Food Chemistry, Volume 127, Issue 2, Pages 379-892 (15 July 2011)

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► Iron and zinc dialyzability were measured with a newly proposed in vitro setup. ► Iron or zinc dialyzability from meals was correlated with published absorption data. ► Iron or zinc dialyzability correlated well with iron or zinc absorption. ► The new setup can be employed for the prediction of iron or zinc bioavailability.

► A novel method for detection of glufosinate in maize samples was developed by ion-pair reversed-phase liquid chromatography with derivatisation. ► The effect of different ion exchange conditions on separation efficiency was studied and 10 mM DTAB and pH 4.0 was used for better and quicker separation. ► The mechanism of ion exchange of glufosinate-CNBF with ion-pair reagent was discussed.

► Three compounds are tentatively as new compounds based on the fragmentation behaviours of HPLC/(+)ESI-MSn. ► The relative abundance of two key product ions are utilised for the key structure identification of a resveratrol dimer. ► Based on their HPLC/DAD-UV spectra, two compounds were tentatively identified as cis and trans-configuration, respectively.

► The potential of Raman spectroscopy for glucose quantitative determination was investigated. ► Micro-Raman spectra in the 600–1600 cm−1 region of four sport drinks were recorded. ► A multivariate analysis based on the interval Partial Least Square approach was used. ► Glucose concentration results were in good agreement with the values given by a biochemical assay.

Research highlights

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Research highlights

Iron or zinc dialyzability obtained from a modified in vitro digestion procedure compare well with iron or zinc absorption from meals Original Research Article Pages 716-721 K. Argyri, E. Theophanidi, A. Kapna, C. Staikidou, G. Pounis, M. Komaitis, C. Georgiou, M. Kapsokefalou

A rapid liquid chromatography method for determination of glufosinate residue in maize after derivatisation Original Research Article Pages 722-726 Kun Qian, Shun He, Tao Tang, Tianyu Shi, Jianqiang Li, Yongsong Cao

Identification of isomers of resveratrol dimer and their analogues from wine grapes by HPLC/MSn and HPLC/DAD-UV Original Research Article Pages 727-734 Q.J. Kong, X.Y. Ren, N. Hu, C.R. Sun, Y.J. Pan

Visible micro-Raman spectroscopy for determining glucose content in beverage industry Original Research Article Pages 735-742 I. Delfino, C. Camerlingo, M. Portaccio, B. Della Ventura, L. Mita, D.G. Mita, M. Lepore

Mid infrared and fluorescence spectroscopies coupled with factorial discriminant analysis technique to identify sheep milk from different feeding systems Original Research Article Pages 743-748 Romdhane Karoui, Moncef Hammami, Hamadi Rouissi, Christophe Blecker

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ScienceDirect - Food Chemistry, Volume 127, Issue 2, Pages 379-892 (15 July 2011)

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► Monitoring ewe’s milk during lactation period by rapid spectroscopic techniques. ► Concatenation of MIR and fluorescence spectra allow good discrimination of milk. ► MIR and fluorescence could be used as efficient tool for authenticating milk. ► These two techniques could be adopted for on line measurements.

► Development of screen-printed biosensors for glucose, fructose and ethanol. ► Application of the biosensors to the monitoring of alcoholic fermentations. ► Evaluation of the fermentation profiles obtained using two different yeast strains. ► Highlighting of the differences in metabolic behaviour of the two strains. ► Biosensor data in good agreement with spectrophotometric analyses.

► HPLC method was developed to assess the quality of cinnamon bark and twig. ► Seven bioactive components including cinnamic acid were separated and quantified. ► Fingerprint analysis was carried out to discriminate cinnamon bark from twig. ► Partial least-squares discriminant analysis showed good classification.

► Suitable for high-throughput screening of total antioxidant content in edible items. ► Satisfactorily quantification of most hydrophilic and lipophilic antioxidants. ► Most extensive reaction within the first 4 min for most compounds and foods. ► Four minutes reaction time is appropriate.

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Graphical abstract

Real time monitoring of alcoholic fermentation with low-cost amperometric biosensors Original Research Article Pages 749-754 S. Piermarini, G. Volpe, M. Esti, M. Simonetti, G. Palleschi

Discrimination of cinnamon bark and cinnamon twig samples sourced from various countries using HPLC-based fingerprint analysis Original Research Article Pages 755-760 Yan Ding, En Qi Wu, Chun Liang, Jianbo Chen, Minh Ngoc Tran, Chong Hui Hong, Yuseon Jang, Kyung Lae Park, KiHwan Bae, Young Ho Kim, Jong Seong Kang

Validation of a quantitative assay for the total content of lipophilic and hydrophilic antioxidants in foods Original Research Article Pages 761-768 Bente L. Halvorsen, Rune Blomhoff

Micelle mediated extraction and simultaneous spectrophotometric determination of vanadium(V) and molybdenum(VI) in plant foodstuff samples Original Research Article Pages 769-773 Tayyebeh Madrakian, Abbas Afkhami, Reza Siri, Masoumeh Mohammadnejad

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ScienceDirect - Food Chemistry, Volume 127, Issue 2, Pages 379-892 (15 July 2011)

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► Procedure based on emulsification for metals determination in vegetable oils. ► Fast alternative in relation to the traditional digestion procedures. ► Method does not require the sample to be subjected to any drastic pre-treatment. ► Method does not require the sample to be subjected to time-consuming pre-treatment.

Research highlights

► The concentration of V and Mo in foodstuffs samples is in the order of μg L−1. ► The method gives selective, very sensitive, simple, and environmentally friendly. ► The method was validated by determination elements in different complex mixtures. ► This is the first report of simultaneous analysis of V and Mo in foodstuff samples.

Graphical abstract

Highlights

► Two enzymatic methods for assay of formaldehyde have been developed. ► An applicability of both methods for formaldehyde assay in fish was demonstrated. ► Oxidase-peroxidase-based method is the most sensitive for formaldehyde analysis. ► Hake and cod contain high formaldehyde concentrations (up to 100 mg/kg wet weight).

Research highlights

Alcohol oxidase- and formaldehyde dehydrogenase-based enzymatic methods for formaldehyde assay in fish food products Original Research Article Pages 774-779 Vladimir Sibirny, Olha Demkiv, Halyna Klepach, Taras Honchar, Mykhailo Gonchar

Multi-element determination of Cu, Fe, Ni and Zn content in vegetable oils samples by high-resolution continuum source atomic absorption spectrometry and microemulsion sample preparation Original Research Article Pages 780-783 Luana S. Nunes, José T.P. Barbosa, Andréa P. Fernandes, Valfredo A. Lemos, Walter N.L. dos Santos, Maria Graças A. Korn, Leonardo S.G. Teixeira

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► A fast and sensitive multi-residue analysis method in grapes is developed. ► SiO2 hollow fiber was applied in analysis of multi-pesticides in grape samples. ► A new

pretreatment method involves extraction and clean-up in one step.

► Mushroom β-1,3-1,6-glucans were determined with a new colorimetric method. ► The dye Congo red interacts with the triple helix of the glucans. ► The total- β-1,3-glucan content in mycelia and fruiting bodies was measured. ► Fruiting bodies have higher amounts of β-1,3-1,6-glucans and total-β-1,3-glucans.

► Rapid CZE method for determining phenolic compounds in broccoli. ► A SPE step introduced to replace liquid–liquid extraction. ► Method applied to several Brassica vegetables. ► Method validated with HPLC.

► The original percentage in weight of polar compounds %PC0 depends on oil composition. ► Time to reach 25% in weight of polar compounds T25%pc depends on the

oil composition. ► %PC0 and T25%pc are very closely related. ► T25%pc can be predicted from %PC0.

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Monitoring multi-class pesticide residues in fresh grape by hollow fibre sorptive extraction combined with gas chromatography–mass spectrometry Original Research Article Pages 784-790 Jia Li, Hong-Fei Zhang, Yan-Ping Shi

A new colorimetric method to quantify β-1,3-1,6-glucans in comparison with total β-1,3-glucans in edible mushrooms Original Research Article Pages 791-796 Jörg Nitschke, Hendrik Modick, Ekkehard Busch, Reimund Wantoch von Rekowski, Hans-Josef Altenbach, Helga Mölleken

A rapid quantitative determination of phenolic acids in Brassica oleracea by capillary zone electrophoresis Original Research Article Pages 797-801 Iris S.L. Lee, Mary C. Boyce, Michael C. Breadmore

A very simple, fast, and non-destructive approach to predict the time at which edible oils submitted to high temperature reach the established limits of safety Original Research Article Pages 802-806 Maria Dolores Guillén, Patricia S. Uriarte

Identification and quantification of phenolic compounds from pomegranate (Punica granatum L.) peel, mesocarp, aril and differently

produced juices by HPLC-DAD–ESI/MSn Original Research Article Pages 807-821 Ulrike A. Fischer, Reinhold Carle, Dietmar R. Kammerer

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►Forty-eight phenolic compounds were detected in pomegranate peel, mesocarp and arils. ►Ellagitannins predominate in pomegranates and pomegranate-derived products. ►Antioxidant capacity is highly correlated with the contents of phenolic compounds. ►Raw material and processing markedly affects juice phenolic profiles and contents.

► Application of MSPD in mycotoxin analysis. ► Monitoring aflatoxins and OTA in tiger nuts. ► Evaluation of quality of raw material (tiger nuts) and one of its derivates. ► Risk for the consumers.

► PARAFAC2 models in a fast analytical process for LC-DAD analysis of aflatoxins. ► Using a mixture calibration design as a calibration set. ► Examination of synthetic and real contaminated samples as validation set. ► Satisfactory quantitative and qualitative results by correct determination of factors.

► We developed a duplex real-time PCR detection method for soya and lupin in food. ► We established the performances of the method using flours and baked cookies. ► Detection limits in the low milligrams per kg range are considered to be appropriate. ► The method was successfully applied to food products that may contain soya or lupin. ► We concluded that the developed method was suitable for the application.

► A novel FI-CL method was developed for determination of melamine in milk products. ► Parameters affecting reproducibility and CL detection were optimized systematically. ► A assay produce takes only 25 s and the sampling rate is about 120 samples h−1.

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One-year monitoring of aflatoxins and ochratoxin A in tiger-nuts and their beverages Original Research Article Pages 822-826 J. Rubert, N. Sebastià, J.M. Soriano, C. Soler, J. Mañes

Exploiting second-order advantage using PARAFAC2 for fast HPLC-DAD quantification of mixture of aflatoxins in pistachio nuts Original Research Article Pages 827-833 Maryam Vosough, Amir Salemi

Development of a real-time PCR method for the simultaneous detection of soya and lupin mitochondrial DNA as markers for the presence of allergens in processed food Original Research Article Pages 834-841 Antonio M. Gomez Galan, Marcel Brohée, Eugénia de Andrade Silva, Arjon J. van Hengel, Hubert Chassaigne

Determination of melamine by flow injection analysis based on chemiluminescence system Original Research Article Pages 842-846 Hua-jin Zeng, Ran Yang, Qing-wen Wang, Jian-jun Li, Ling-bo Qu

Analysis of nisin A, nisin Z and their degradation products by LCMS/MS Original Research Article Pages 847-854 N. Schneider, K. Werkmeister, M. Pischetsrieder

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ScienceDirect - Food Chemistry, Volume 127, Issue 2, Pages 379-892 (15 July 2011)

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► Development of an LCMS/MS method to quantify nisin A and nisin Z in cheese matrix. ► Analysis of the prevalence of nisin in commercial processed cheese samples. ► Identification of nisin Z as the predominant variant in commercial products. ► Identification and quantification of nisin degradation products in processed cheese.

► The focus is simultaneous determination of 88 pesticides in berry with SPE-GC-MS. ► It is a rapid and reliable method that we have developed to analyze 88 pesticides. ► It is the first time to analyze 88 pesticide residues in raspberry and blueberry.

► The study quantifies the effects of green and black tea quality parameters using statistical modelling, remote sensing and NIR spectroscopy. ► Relationships could be observed between Normalised Difference Vegetation Index (NDVI), NIR spectroscopy and the green and black tea quality parameters. ► Statistical analysis showed that liquor brightness is affected by the levels of catechins, theaflavins and caffeine content. ► NDVI and Near Infrared (NIR) spectroscopy have a large potential to be used for monitoring tea quality in the future.

► There are only few reports about the determination of cyanuric acid in infant formula. ► MAE can reduce both extraction time and solvent consumption. ► Many cases have proved that MAE is a viable alternative to conventional techniques. ► In the present work, we combined MAE with LCMS for analysis of CYA in infant formula.

► A new method was established for the simultaneous analysis of three groups of analytes. ► More qualitative information can be attained by the proposed HPLC-DAD–ESI/MS method. ► The method was first used to determine the amount of 10 bioactive components in citrus. ► The results provide the proof for evaluating the quality of citrus newly cultivated. ► Products containing the above bioactive components can be evaluated by the method.

Research highlights

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Short Communications

Research highlights

Multiresidue method for determination of 88 pesticides in berry fruits using solid-phase extraction and gas chromatography–mass spectrometry: Determination of 88 pesticides in berries using SPE and GC–MS Original Research Article Pages 855-865 X. Yang, H. Zhang, Y. Liu, J. Wang, Y.C. Zhang, A.J. Dong, H.T. Zhao, C.H. Sun, J. Cui

Integrating satellite images and spectroscopy to measuring green and black tea quality Original Research Article Pages 866-874 R. Dutta, A. Stein, R.M. Bhagat

Microwave-assisted extraction and determination of cyanuric acid residue in infant formula samples by liquid chromatography–tandem mass spectrometry Original Research Article Pages 875-879 Chao Han, Cuiping Liu, Yongfang Zhou, Biqi Xia, Zhenou Zhu, Xinxiang Lei, Yan Shen

Simultaneous determination of flavanones, hydroxycinnamic acids and alkaloids in citrus fruits by HPLC-DAD–ESI/MS Pages 880-885 Dongxiu He, Yang Shan, Yuehui Wu, Guozhu Liu, Bo Chen, Shouzhuo Yao

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► HS-SPME-GC/MS method is reliable to monitor the stability of lipid fraction in butter. ► High extraction temperatures induce the ex-novo formation of hexanal. ► The storage temperatures are critical factors to maintain the quality of butter. ► Butter samples at the end of shelf-life (180 days) showed the highest hexanal content.

► There are only very few reports about the determination of Gibberellin A3 residue. ► In this paper, a simple method has been developed for the determination of Gibberellin A3. ► Analysis is performed by LC–MS/MS operated in the multiple reaction monitoring mode. ► The proposed method is rapid and simple. ► This method could be utilised for the routine analysis of Gibberellin A3 in fruit samples.

Research highlights

Research highlights

A headspace solid-phase microextraction gas-chromatographic mass-spectrometric method (HS-SPME–GC/MS) to quantify hexanal in butter during storage as marker of lipid oxidation Pages 886-889 Sara Panseri, Silvia Soncin, Luca Maria Chiesa, Pier Antonio Biondi

Determination of Gibberellin A3 residue in fruit samples by liquid chromatography–tandem mass spectrometry Pages 890-892 Wen Xie, Chao Han, Ziqiang Zheng, Xiaomei Chen, Yan Qian, Huiying Ding, Lei Shi, Chunhua Lv

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