reactor manual
TRANSCRIPT
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EXTRACTS FROM
INSTRUCTION MANUAL
CEX
CHEMICAL REACTORS TEACHING EQUIPMENT
CEX
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INSTRUCTION MANUAL
CEX
CHEMICAL REACTORS TEACHING EQUIPMENT
CEX
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CEX CHEMICAL REACTORS SERVICE UNIT
IMPORTANT SAFETY INFORMATION
All practical work areas and laboratories should be covered by local regulations which
must be followed at all times. If required, Armfield can supply a typical set of
laboratory safety rules.
Your CEX reactor bench has been designed to be safe in use, when installed, operated
and maintained in accordance with the instructions in this manual. As with any piece of
sophisticated equipment, dangers may exist if the equipment is misused, mishandled or
badly maintained.
Water-Borne Hazards
The equipment described in this instruction manual involves the use of water which
under certain conditions can create a health hazard due to infection by harmful micro-
organisms.
For example, the microscopic bacterium called Legionella pneumophila will feed on
any scale, rust, algae or sludge in water and will breed rapidly if the temperature of
water is between 20 and 45°C. Any water containing this bacterium which is sprayed or
splashed creating air-borne droplets can produce a form of pneumonia called
Legionnaires Disease which is potentially fatal.
Legionella is not the only harmful micro-organism which can infect water, but it serves
as a useful example of the need for cleanliness. Under the COSHH regulations, thefollowing precautions must be observed:
Any water contained within the product must not be allowed to stagnate, ie. the water
must be changed regularly.
Any rust, sludge, scale or algae on which micro-organisms can feed must be removed
regularly, i.e. the equipment must be cleaned regularly.
Where practicable the water should be maintained at a temperature below 20°C or
above 45°C. If this is not practicable then the water should be disinfected if it is safe
and appropriate to do so. Note that other hazards may exist in the handling of biocides
used to disinfect the water.
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CEX CHEMICAL REACTORS SERVICE UNIT
or contact Armfield. The equipment must not be operated with any of the panels
removed.
To give increased operator protection, the unit incorporates a Residual Current Device
(RCD), alternatively called an Earth Leakage Circuit Breaker, as an integral part of this
equipment. If through misuse or accident the equipment becomes electrically
dangerous, the RCD will switch off the electrical supply and reduce the severity of any
electric shock received by an operator to a level which, under normal circumstances,
will not cause injury to that person.
At least once each month, check that the RCD is operating correctly by pressing the
TEST button. The circuit breaker MUST trip when the button is pressed. Failure to trip
means that the operator is not protected and the equipment must be checked and
repaired by a competent electrician before it is used.
HOT SURFACES AND LIQUIDS
The unit incorporates a pumped electric water heater, and is capable of producingtemperatures that could cause skin burns.
Before disconnecting any of the pipes or tubing:
- Stop all the pumps.
- Leave time for the water to cool
- Check that the temperature is at a safe level
Do not touch any surfaces close to ‘Hot Surfaces’ warning labels, or any of the
interconnecting tubing, whilst the equipment is in use.
CHEMICAL SAFETY
Details of the chemicals intended for use with this equipment are given in the Product
Manuals for the different reactor options available with this equipment. Chemicals
purchased by the user are normally supplied with a COSHH data sheet which providesinformation on safe handling, health and safety and other issues. It is important that
these guidelines are adhered to.
Note:
- It is the user’s responsibility to handle chemicals safely
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CEX CHEMICAL REACTORS SERVICE UNIT
ARMFIELD LIMITED
OPERATING INSTRUCTIONS AND EXPERIMENTS
CEX CHEMICAL REACTORS TEACHING EQUIPMENT
1. INTRODUCTION 5
2. EQUIPMENT DESCRIPTION 7
2.1 Chemical storage vessels. 7
2.2 Feed pumps 8
2.3 Stirrer control panel 8
2.4 Hot water circulator 8
2.5 Temperature control of reactor 9
2.6 Conductivity measurement of reactor contents 10
2.7 Reactor fitment 10
2.8 Mainsplate at rear of plinth 10
3. OPERATION 11
3.1 Switching-on the unit 11
3.2 Filling the feed tanks 11
3.3 Controlling the feed pumps 11
3.4 Operation of the stirrer (CEM MkII and CEB MkII) 12
3.5 Operation of temperature controller 12
3.6 Operating the console 12
3.7 Calibrating the feed pumps 13
3.8 Operating the CEM MkII 13
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CEX CHEMICAL REACTORS SERVICE UNIT
5.3 Calibration of the conductivity sensor 16
5.4 Accessing the electrical circuits inside the plinth 17
5.5 Draining the hot water circulator 18
5.6 Temperature controller set-up 18
5.7 Priming the hot water circulator 19
6. APPENDIX 1: INSTALLATION GUIDES 20
6.1 CEM/CEX installation guide 206.2 CET/CEX installation guide 23
6.3 CEB/CEX installation guide 26
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CEX CHEMICAL REACTORS SERVICE UNIT
1. INTRODUCTION
The Armfield CEX Chemical Reactors Teaching Equipment demonstrates thecharacteristics of the important types of chemical reactor, batch stirred tank reactor
(batch reactor), continuous stirred tank reactor (CSTR) and tubular reactor. Other types
of reactor are demonstrated by separate equipment: CEU, packed bed chemical and
enzymic reactors; and CEP MkII, continuous stirred tank reactors in series.
The reactors available for use with CEX are as follows:
- CEB MkII batch reactor
- CEM MkII CSTR
- CET MkII Tubular reactor
There is a mounting position on CEX for any one of the reactors above. Reactors are
interchangeable. CEX is in effect the bench providing the services required by each of
the reactors such as dual peristaltic pumps for feed delivery, a hot water circulator or
chiller (optional) for constant temperature operation, and sensors – temperature and
conductivity. CEX can be operated with the IFD6 interface device to allow computer
data logging. Below CEX is shown with the CEM MkII:
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CEX CHEMICAL REACTORS SERVICE UNIT CEX CHEMICAL REACTORS SERVICE UNIT
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CEX CHEMICAL REACTORS SERVICE UNIT
2. EQUIPMENT DESCRIPTION
The chemical reactors service unit consists of a moulded ABS plinth which is used as a
mounting for the Chemical reactor to be used. It also provides the ancillary services for
the reactor.
armfield
CHEMICAL REACTOR SERVICE UNIT
CEX
FRONT VESSEL REAR VESSEL
TEMPERATURE CONTROL
1
0
CHILL
HEAT
DATA O/P
CONDUCTIVITY mS
SOL.
out 1
MTW11lae
°C
CEM CONTINUOUSSTIRREDTANK REACTORTemperature
probe
Conductivity probe
Stirrer plug
BOTTOMOF COIL
TO TOP OF COILAFTER PRIMING
CEX with CEM MkII reactor fitted Plinth
2.1 Chemical storage vessels.
The reagent tank module consists of two glass vessels mounted into a PVC base which
is located on studs in the plinth and held in position by thumbnuts. Drain valves are
fitted to the underside of each vessel and are accessible within the plinth trough.
Rigid standpipes are mounted
in the lids of the vessels
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CEX CHEMICAL REACTORS SERVICE UNIT
2.2 Feed pumpsTwo variable throughput peristaltic pumps are used to pump the reagents from the
storage vessels to the fitted reactor. The pumps are mounted on control plates mounted
on the front of the plinth.
A remote control facility allows the pumps to be driven from an external 0-5V dc
signal, via the data logging connector.
FRONT VESSEL REAR VESSEL
Manual speed control
Stirrer control panelData logging portsFeed pumps
2.3 Stirrer control panel
CEM MkII and CEB MkII reactors are equipped with agitators driven by electric motor.The control panel is located on the front of the plinth (see above).
2.4 Hot water circulator
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CEX CHEMICAL REACTORS SERVICE UNIT
R.C.C.B O/P HEATPUMP
STIRRERD.C. O/PCIRCULATOR
OUTPUT A.C. ~ 1A MAX
INPUT A.C. ~
MAINS INPUT240V/1PH/50HZ~
Priming vessel
Rear view showing
hot water circulator
2.5 Temperature control of reactor
Temperature control is achieved by circulation of heated or chilled water through
submersed coils inside the CEM MkII, CEB MkII reactors and the CET MkII. The hot
water circulator is supplied as standard with the CEX service unit whilst the chilled
water circulator (CW-16) can be supplied as an accessory.
A temperature sensor is designed to be used individually with the CEM MkII and the
CET MkII in conjunction with the automatic temperature controller in the controlconsole. The sensor transmits a signal to the controller which then modulates power to
the heating element in the circulator, increasing or reducing the amount of heat put into
the circulating water. The CEB MkII is supplied with its own temperature sensor.
It is possible to run the reactors at temperatures below ambient by disconnecting the hot
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CEX CHEMICAL REACTORS SERVICE UNIT
Ensure Mains Switchis OFF
armfield
TEMPERATURE
CONTROL
1
0
CHILL
HEAT
DATAO/P
CONDUCTIVITY
mS
SOL.
out 1
MTW 11lae
°C
Temperature
controllerData logging
out ut
Output socket to
drive CW16 chiller
Conductivity
dis la
2.6 Conductivity measurement of reactor contents
A conductivity probe is supplied to be used individually with any of the reactors. The
conductivity is displayed on the meter in units of milliSiemens/cm. During a chemical
reaction, the conductivity of the reacting solution changes as more of the reactants are
converted. This can be monitored and used to determine the degree of conversion and
the rate of conversion.
The conductivity measurement is available for data logging.
2.7 Reactor fitment
Each of the three chemical reactor modules is mounted on identical PVC baseplates
which are designed to stand on the plinth in the space provided and to be secured to the
base by thumbnuts. Full fitment details for each of the reactors is given in theappropriate reactor manual.
2.8 Mainsplate at rear of plinth
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CEX CHEMICAL REACTORS SERVICE UNIT
3. OPERATION
The apparatus must be set up in accordance with the installation sheet supplied (see
Appendix A for details). Additionally, ensure that you have read the safety information
at the beginning of this manual.
3.1 Switching-on the unit
The unit is switched on using the
switch on the front of the unit. The
circuit breakers and RCD devicelocated at the rear of the unit
should be turned on beforehand.
Both the temperature controller and
conductivity display should
illuminate.
3.2 Filling the feed tanks
Lift the feed tank lids and pour
solutions in from above. A drain
tap is located at the base of each
vessel in order to drain residual
liquid.
3 3 Controlling the feed pumps
armfield
Lid
Drain valve for
each tank
On/off switch
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CEX CHEMICAL REACTORS SERVICE UNIT
3.4 Operation of the stirrer (CEM MkII and CEB MkII)
Operation is similar to the two feed
pumps. Speed is adjusted using the rotary
switch when the selector switch is set to
manual.
Speed
control
Manual/remote
Data logging
port
3.5 Operation of temperature control ler
TEMPERATURE
CONTROL
1
0
DATA
O/P
CONDUCTIVITY
mS
out 1
MTW 11lae
°C
1
3
24
Temperature is displayed in °C. The set- point temperature is shown by pressing
button 1 and the value adjusted up and
down using buttons 2 and 3 respectively.
The display will revert to the process
temperature after a short period. A light in
the top left hand corner of the display (4)
indicates when the controller output isactive.
3.6 Operating the console
When the CEX is used with the hot water circulator
then switch 9 should be positioned to heat It isTEMPERATURE
CONTROL
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CEX CHEMICAL REACTORS SERVICE UNIT
3.7 Calibrating the feed pumps
Both peristaltic pumps require calibration so that exact flow rates are known.Calibration should be carried out for both pumps since there may be small differences
between them.
Fill both reagent vessels. Set the feed pump to 2.0 and determine the flow rate by
measuring the volume collected for a defined period. Repeat the procedure for 4.0, 6.0,
8.0 and 10.0 and plot flowrate versus pump speed.
3.8 Operating the CEM MkII
The reactor has a turbine agitator (11)
and baffle (12) arrangement for efficient
mixing and heat transfer.
Temperature in the reactor is controlled
by circulating heating or cooling liquid
through the internal coil (13).
The liquid level in the reactor is
controlled by the position of the stand-
pipe (14). This can be adjusted by
loosening the back nut (15). To operate
at full volume the standpipe is pushed
upwards until the mark etched on thetube is level with the bottom of the back
nut. A stop on the standpipe limits the
lower operating limit to half the full
volume.
SCOREMARK
CEM CONTINUOUS STIRRED TANK REACTOR
11
13
16
15
14
12
When the reactor is not being used it can
be drained through the valve (16).
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CEX CHEMICAL REACTORS SERVICE UNIT
4. SPECIFICATIONS
4.1 Overall dimensions:
Height: - 0.60m
Width - 1.00m
Depth - 0.50m
4.2 Electrical supply:
CEX-A CEX-B CEX-G
Green/yellow lead Earth (Ground) Earth (Ground) Earth (Ground)
Brown lead Live (Hot) Live (Hot) Live (Hot)
Blue lead Neutral Neutral Neutral
Fuse rating 13A 15A 13A
Voltage 220-240V 110-120V 220VFrequency 50Hz 60Hz 60Hz
4.3 Pin connections
Data logging connectors. Data logging via the telephone sockets is available for Pump
speeds, stirrer speed and conductivity. Pin connections are as follows:
Pin Pump 1 Pump 2 Stirrer speed Conductivity
1 Reserved Reserved Reserved Reserved
2 Not used Not used Not used +12V
3 Signal (0-5V) Signal (0-5V) Signal (0-5V) Signal (0-5V)
4 0V 0V 0V 0V
5 Not used Not used Not used -12V
6 Reserved Reserved Reserved Reserved
Hot water circulator connector has the following pin connections (See also electrical
drawing CBM29654):
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CEX CHEMICAL REACTORS SERVICE UNIT
4.4 Miscellaneous
Peristaltic pump flow rate: 0-95 ml/min per pumpFeed tank capacity 5 L per tank
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CEX CHEMICAL REACTORS SERVICE UNIT
5. ROUTINE MAINTENANCE
To preserve the life and efficient operation of the equipment it is important that theequipment is properly maintained. Regular maintenance of the equipment is the
responsibility of the end user and must be performed by qualified personnel who
understand the operation of the equipment.
5.1 General
The equipment should be disconnected from the electrical supply when not in use. After
use the feed tanks, reactor vessel, sump tray and pipework should be washed throughwith water to remove chemical residues and then drained.
5.2 RCD test
Test the RCD by pressing the TEST button at least once a month. If the RCD button
does not trip when the Test button is pressed then the equipment must not be used and
should be checked by a competent electrician.
5.3 Calibration of the conductivity sensor
The conductivity conditioning circuit (which provides the reading from the conductivity
probe supplied with the CEX service unit) is located on a printed circuit board inside
the electrical console. This circuit is calibrated before despatch and should not require
re-calibration. However, should re-calibration become necessary the appropriate
calibration potentiometers can be located using the diagram below.
Ensure the equipment has been connected to the electrical supply and switched on for at
least 20 minutes. To access the PCB remove the front panel from the electrical console
by removing the four fixing screws. It is not necessary to detach the PCB from the front
panel.
Disconnect the conductivity probe from the socket at the left-hand side of the electrical
console. Connect an AC Voltmeter (Range AC mV) to pins 1 and 2 of the vacant socket
and adjust potentiometer VR2 on the PCB to give a reading of 50 mV (RMS) on theVoltmeter (probe excitation voltage).
Disconnect the Voltmeter then reconnect the probe to the appropriate socket having
removed the probe from the appropriate reactor fitted to the CEX.
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CEX CHEMICAL REACTORS SERVICE UNIT
When the conditioning circuit has been re-calibrated replace the front panel of the
electrical console and re-install the probe in the appropriate reactor on the CEX service
unit.
5.4 Accessing the electrical circui ts inside the plinth
Maintenance of the CEX service unit does not require access to the electrical circuits or
components located inside the moulded plinth. However, in the event of an electrical
problem, it may be necessary for a competent electrician to gain access to the inside of
the mouldings as follows:
Ensure that the equipment is disconnected from the electrical supply (not just switched
off).
Drain any liquids contained in the reagent vessels or reactors.
Unscrew the channel drain valve located in the recess at the left hand end of the
moulded plinth.
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CEX CHEMICAL REACTORS SERVICE UNIT
Carefully remove the front panel from the electrical console by unscrewing the four
fixings.
Disconnect the electrical connections between the top and bottom plinth sections by
disconnecting the appropriate connectors.
Unscrew the six fixings around the periphery of the plinth top.
Carefully lift the top moulded section away from the bottom moulded section and place
the top section in a suitable location.
The electrical circuits inside the bottom moulded plinth section are accessible.
A circuit diagram showing the mains and DC electrical circuits inside the plinth is
included at the rear of this manual to assist in fault finding.
Should it be necessary to remove the PCB from inside the electrical console then the
PCB connections diagram on page 17 shows the location and function of the electricalconnectors on the PCB to aid re-assembly.
Re-assembly of the top and bottom moulded plinth sections is the inverse of the above
instructions.
5.5 Draining the hot water circulator
It is not necessary to drain the hot water circulator following use in normal
circumstances. However, if the ambient temperature may fall below freezing, especially
if it is intended to transport the equipment to a different location or the equipment is to
be placed in long term storage, then the circulator should be drained to prevent damage
simply by undoing the connections to the reactor and allowing the water to drain under
gravity.
5.6 Temperature control ler set-up
The temperature controller is a three term controller which has been set up and
configured to give the optimum control capability for all three reactor modules. As well
as the heating control for operating
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CEX CHEMICAL REACTORS SERVICE UNIT
When in configuration mode the parameters can be selected by pressing key (2). To
display the value press key (1) and if necessary change using keys (2) or (3). Store thenew value by pressing key (1).
No key activation within 10 seconds causes the instrument to switch over to basic
functioning.
The following are the correct parameters for the heating cycle:-
Parameter Heating Cooling
1Lo 0.0 0.0
1hi 50.0 50.0
1hy 0.0 0.0
1Pb -7.5 3.5
1it 90 90
1dt 60 60
1ar 35 351ct 04 04
1PF 00 00
2Lo -19.9 -19.9
2hi 99.9 99.9
2hy 0.0 0.0
2ct 05 05
2PF 00 00
dPS 01 01
5.7 Priming the hot water circulator
After draining the hot water circulator or changing the reactor vessels it will be
necessary to prime the pump again. Refer to the installation sheet supplied with the
reactor and also included in the appendix of this manual.
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CEX CHEMICAL REACTORS SERVICE UNIT
6. APPENDIX 1: INSTALLATION GUIDES
6.1 CEM/CEX installation guide
1MOUNTING THE FEED VESSEL ASSEMBLY
Locating studs
and fasteners
Connect the tubing on
the left hand side of
each of the two feed
pumps to the standpipe
located in each of thereagent vessels. (Left
feed pump to front
vessel, right feed pump
to rear vessel)
Fit the reagent vessel
assembly to the CEX
using the 4 locating
studs and black handnuts
2 MOUNTING THE HOT WATER CIRCULATOR (HWC)
Rear view of CEX showing positioning of HWC
Hoses on the HWC should be orientated as
shown in the diagram
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CEX CHEMICAL REACTORS SERVICE UNIT
3- Fit the CEM MkII assembly to
the CEX using the 4 locating
studs and black thumbnuts. The
reactor is supported by 3 pillars,
position the reactor on the CEX
so that a single pillar support is
foremost
- Connect the remaining two pipesfrom the feed pumps to the
connectors on the base of the
reactor as shown.
- Connect the conductivity probe
and temperature sensor plugs to
the sockets on the left hand edge
of the control console. Connectthe stirrer plug to the socket
located on the rear of the CEX.
- Fit the conductivity and
temperature sensors to the CEM.
Each probe fits in a gland. The
gland nut should be loosened to
fit the probes and then tightened
to secure them. Probes shouldreach the bottom of the reactor
armfield
CHEMICAL REACTORSERVICEUNIT
CEX
FRONT VESSEL REAR VESSEL
TEMPERATURE
CONTROL
1
0
CHILL
HEAT
DATA
O/P
CONDUCTIVITY
mS
SOL.
out 1
MTW11lae
°C
CEM CONTINUOUSSTIRREDTANK REACTORTemperature
probe
Conductivity
probe
Stirrer plug
BOTTOMOF COIL
TO TOP OF COILAFTER PRIMING
CONNECTION TO ELECTRICITY SUPPLY4
MOUNTING THE CEM MKII ONTO THE CEX
Brown - Live (hot)Blue - Neutral (hot)
Green/yellow - Earth (ground)
Check that the voltage specified on theequipment matches the supply voltage.
NOTE: this unit MUST be earthed.
Ensure that circuit breakers
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CEX CHEMICAL REACTORS SERVICE UNIT
5 PRIMING THE HOT WATER CIRCULATOR
- Connect suction pipe of the HWC
to a cold water supply (preferably
deionised).
- Switch on the mains switch on the
front of the CEX.
- Adjust the temperature controller
set-point to a temperature below
ambient (see Operation
instructions overleaf).
- Then switch on the pump switch at
the side of the temperature
controller.
Suction pipe
CONNECTING THE HWC TO CEM MKII6
Priming vessel
CEM CONTINUOUS STIRRED TANK REACTOR
1
2
- Connect suction pipe of the HWC (1) to the
connection for the top of the coil (rear).
- Connect the supply pipe of the HWC (2) to
the connection for the bottom of the coil(front).
- Turn on the mains switch and then the pump
switch and refill the HWC expansion tank as
required.
7 CONNECTING TO THE DATA LOGGER (OPTION)
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CEX CHEMICAL REACTORS SERVICE UNIT
6.2 CET/CEX installation guide
1 MOUNTING THE FEED VESSEL ASSEMBLY
Locating studs
and fasteners
Connect the tubing on
the left hand side of
each of the two feed
pumps to the standpipe
located in each of the
reagent vessels. (Left
feed pump to front
vessel, right feed pump
to rear vessel)
Fit the reagent vessel
assembly to the CEX
using the 4 locating
studs and black hand
nuts
2 MOUNTING THE HOT WATER CIRCULATOR (HWC)
Rear view of CEX showing positioning of HWC
Th l d f h HWC l i h k
Hoses on the HWC should be orientated as
shown in the diagram
CEX CHEMICAL REACTORS SERVICE UNIT
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CEX CHEMICAL REACTORS SERVICE UNIT
armfield
TEMPERATURE
CONTROL
1
0
CHILL
HEAT
DATA
O/P
CONDUCTIVITY mS
SOL.
out 1
MTW11lae
°C
CHEMICAL REACTORSERVICE UNIT
CEX
TEMPERATUREPROBE
AT REAR
FRONT VESSEL REAR VESSEL
TEMP
COND
CEB(OPTION)
3 MOUNTING THE CET MKII ONTO THE CEX
- Fit the CET MkII assembly to the CEX using the 4 locating studs and black
thumbnuts. Position the reactor so that the non-return valve is on the left hand side
of the reactor towards the rear.
- Connect the remaining
two pipes from the feed
pumps to the connectors
on the lid of the reactor
as shown.- Connect the conductivity
probe and temperature
sensor plugs to the
sockets on the left hand
edge of the control
console.
- Fit the conductivitysensor into the housing
on the top of the reactor
as shown. The
temperature sensor fits into a gland on the reactor lid. In both cases the gland nut
should be loosened to fit the probes and then tightened to secure them. Probes
should be inserted fully so that they are submerged and flow holes in the
conductivity probe glass should be positioned so that liquid flows through.
4 CONNECTION TO ELECTRICITY SUPPLY
Brown - Live (hot)
Blue - Neutral (hot)
Green/yellow - Earth (ground)
Check that the voltage specified on the
equipment matches the supply voltage.
NOTE: this unit MUST be earthed.
TEMPERATURE CONTROL
1
0
out 1
MTW11lae
°C
Ensure that circuit breakers
and RCCD are ON (up)
CEX CHEMICAL REACTORS SERVICE UNIT
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CEX CHEMICAL REACTORS SERVICE UNIT
5 PRIMING THE HOT WATER CIRCULATOR
- Connect suction pipe of the HWC
to a cold water supply (preferably
deionised).
- Switch on the mains switch on the
front of the CEX.
- Adjust the temperature controller
set-point to a temperature below
ambient (see Operation
instructions overleaf).
- Then switch on the pump switch at
the side of the temperature
controller.
Suction pipe
CONNECTING THE HWC TO CET MKII6
Priming vessel
- Connect suction pipe of the HWC (1)
to the overflow pipe mounted high on
the side of the reactor
- Connect the supply pipe of the HWC
(2) to the non-return valve mounted
low down on the left rear side of thereactor.
- Fill the reactor with water, preferably
deionised, using the fill plug on the
top plate of the reactor. Refit the plug.
- Turn on the mains switch and then the
pump switch and refill the HWC
expansion tank as required.1
2
Connect inlet
pipe (1) to here
Connect outlet pipe (2) to here
7 CONNECTING TO THE DATA LOGGER (OPTION)
CEX CHEMICAL REACTORS SERVICE UNIT
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CEX CHEMICAL REACTORS SERVICE UNIT
6.3 CEB/CEX installation guide
1 MOUNTING THE CEB ONTO THE CEX
armfield
TEMPERATURE
CONTROL
1
0
CHILL
HEAT
DATA
O/P
CONDUCTIVITY mS
SOL.
out 1
MTW11lae
°C
CHEMICAL REACTORSERVICEUNIT
CEX
TEMPERATUREPROBE AT REAR
FRONT VESSEL REAR VESSEL
TEMP
COND
CEB(OPTION)
The reactor vessel is set on
a baseplate which is itself
located on four studs on theservice unit and secured by
thumbnuts. The hot water
circulator and feed tanks
provided with CEX are not
required with the batch
reactor configuration.
- The CEB is supplied with its own temperature sensor which fits in the socket on
the side of console dedicated to this purpose. The sensor will not fit any other
socket. Plug in the sensor then insert the sensor into the vessel through the
appropriate gland on the reactor lid.
- The standard conductivity sensor provided with CEX is used with CEB. Plug this
in to the appropriate socket on the side of the control console then insert the
sensor through the remaining gland into the reactor.
- Ensure that both sensors are inserted fully into the vessel without fouling the wall
or other components. Both sensors are secured in the correct position by
tightening the gland nut.
2CONNECTING TO THE ELECTRICITY SUPPLY
Check that the voltage specified on the
equipment matches the supply voltage.
NOTE: this unit MUST be earthed.
Brown - Live (hot)
Blue - Neutral (hot)
Green/yellow - Earth (ground)
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CEX CHEMICAL REACTORS SERVICE UNIT
The chiller unit is used when operating temperatures at or below ambient are
required.
- The feed and return hoses for the chiller are connected to the heating coilwithin the reactor. Connections are made through the reactor lid.
- The plug for the chiller solenoid valve connects to the socket on the front of
the control console (see ‘OPERATING THE CONSOLE’ page 12).
- Switch the switch on the control console to ‘CHILL’
N h lli h (I h l i ) i i
CONNECTING THE CEB TO THE CHILLER3
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- To enter configuration mode, sequentially press keys (3), (1) and (2) and keep them
pressed for 3 seconds.
- Parameters are selected using key (2) and the parameter value by pressing key (1).Changes are made by pressing keys (2) or (3) and the new value stored by pressing
key (1).
- Parameter values required for chiller operation are:
Param Value Param Value Param Value Param Value
1Lo 0.0 1it 90 1PF 00 2ct 05
1hi 50.0 1dt 60 2Lo -19.9 2PF 00
1hy 0.0 1ar 35 2hi 99.9 dPS 01
1Pb 3.5 1ct 04 2hy 0.0
TEMPERATURE
CONTROL
1
0
DATA
O/P
CONDUCTIVITY
mS
out 1
MTW 11lae
°C
1
3
2
CONNECTING TO THE DATA LOGGER (OPTION)5
CEX CHEMICAL REACTORS SERVICE UNIT
4
TEMPERATURE CONTROL
1
0
CHILL
HEAT
DATA O/P
CONDUCTIVITY mS
SOL.
out 1
MTW11lae
°C
IFD6INTERFACE CONSOLE
armfield
4
8MAINS
SOCKET 1POWER
1
5
2
6
3
7
WARNING240V~
240V 2A~ SOCKET 2 POWER 240V 2A~
o
I
o
I
o
I
CONFIGURING THE TEMP CONTROLLER FOR OPERATION WITH CHILLER
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Electrical diagram of the hot water circulator
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