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    Radiation-based process

    instrumentation

    Field service training 18. October 2010

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    Agenda

    Why nucleonic measurement?

    The nucleonic measuring principle

    Typical industries and markets

    Application examples

    Don't be afraid of gamma radiation

    PROTRAC: typically VEGA

    plics the idea with a future

    Configuration and parameter adjustment

    Source container shipping

    Page 2 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

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    Reliable measurement technology for extreme process condition

    Why nucleonic measurement?

    Suitable for extreme conditions

    Measuring principle works without

    contact to process medium

    High reliability of the measuring

    principle

    Some application areas still allowno other alternative to nucleonic

    measurement

    Page 3 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

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    A familiar measuring principle

    The principle is based on theradiation emitted by radioactive

    isotopes

    Isotopes are mounted into a source

    holder

    The radiation is damped when

    penetrating material

    A detector mounted to the tank

    receives the radiation and converts

    it into an electrical signal

    The detector calculates the level,

    density or concentration of themeasured product from the

    received (attenuated) radiation

    The nucleonic measuring principle

    Page 4 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

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    Application areas

    Level switching (1)

    Continuous level (2)

    Density and concentration

    as well as flow measurement

    of liquids (3)

    Interface measurement (4)

    Nucleonic measurement technology

    1

    2

    4

    3

    Page 5 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

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    Typical industries and markets

    Special application areas

    Chemical industry

    Petrochemical industry

    Metal processing

    Oil and gas

    Pulp and paper

    Energy productionAggregates and mining

    Cement industry

    Page 6 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

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    Flue gas desulfurization

    Emission protection through fluegas desulfurization in coal power

    stations

    Lime milk suspension binds sulphur

    dioxide

    Concentration measurement of the

    lime milk by means of density

    measurement

    Lime milk is very abrasive

    Application example density

    Page 7 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

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    Flue gas desulfurization

    Emission protection through fluegas desulfurization in coal power

    stations

    Lime milk suspension binds sulphur

    dioxide

    Concentration measurement of the

    lime milk by means of density

    measurement

    Lime milk is very abrasive

    Application example density

    Page 8 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

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    Cellulose production

    In cellulose production, wood chipsare broken down chemically with

    the help of a cooking liquor

    In a special reactor, the cooking

    liquor is regenerated so that it can

    be used again

    Temperature 160 C, pressure

    10 bar

    Aggressive process conditions

    The maximum level in the reactor

    must be monitored

    Application example point level

    Page 9 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

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    Cellulose production

    In cellulose production, wood chipsare broken down chemically with

    the help of a cooking liquor

    In a special reactor, the cooking

    liquor is regenerated so that it can

    be used again

    Temperature 160 C, pressure

    10 bar

    Aggressive process conditions

    The maximum level in the reactor

    must be monitored

    Application example point level

    Page 10 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

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    Polyester melt reactor

    Its almost impossible to imagineour lives without polyester

    This versatile plastic is created in a

    polyester melt reactor

    Process temperature 220 C

    The vessel is enclosed in a heatingjacket

    Rotation of the container

    Nucleonic measurement has

    proven itself worldwide in this

    application

    Application example level

    Page 11 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

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    Polyester melt reactor

    Its almost impossible to imagineour lives without polyester

    This versatile plastic is created in a

    polyester melt reactor

    Process temperature 220 C

    The vessel is enclosed in a heatingjacket

    Rotation of the container

    Nucleonic measurement has

    proven itself worldwide in this

    application

    Application example level

    Page 12 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

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    Measurement in cyclones in cement

    applicationsIn the lower part of the cyclone,

    buildup often occurs which results

    in blockage

    To avoid downtimes, the cyclone

    must be monitored for buildup and

    possible clogging

    Compressed air can prevent

    clogging, however, over a longer

    period can damage the refractory

    lining

    The thickness of the buildup mustbe monitored, to activate removal

    with compressed air, if necessary

    Application examples point switch

    Page 13 31 August 2011 Roland Bonath

    Radiation-based process instrumentation

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    Measurement in cyclones in cement

    applicationsIn the lower part of the cyclone,

    buildup often occurs which results

    in blockage

    To avoid downtimes, the cyclone

    must be monitored for buildup and

    possible clogging

    Compressed air can prevent

    clogging, however, over a longer

    period can damage the refractory

    lining

    The thickness of the buildup mustbe monitored, to activate removal

    with compressed air, if necessary

    Application examples point switch

    Page 14 31 August 2011 Roland Bonath

    Radiation-based process instrumentation

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    Highest sensitivity

    Detectors of the PROTRAC seriesare extremely sensitive

    Conventional Geiger-Mueller

    counters do not even respond here

    Remarkable measuring precision

    and quick response times

    Advantage

    Reduction of source activity

    Don't be afraid of gamma radiation

    Page 15 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

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    A high degree of safety

    Integrated safety functions

    Self monitoring and diagnosis

    Asset Management System

    Developed acc. to IEC 61508

    Qualified up to SIL2

    NEWVEGA is the first supplier to offer

    level, point level and density

    instruments with SIL

    PROTRAC: typically VEGA!

    Page 16 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

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    Simpler is better

    plics makes everything simpler

    From selection to ordering to setup

    The modular system can be exactly

    adapted to the measuring task

    plics allows unrestricted selection

    and combination of sensors,process fitting, electronics and

    housings

    Advantage:

    Simple planning, short delivery time,

    uncomplicated connection, fast setup

    and commissioning

    plics The idea with a future

    Page 17 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

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    plics Electronics

    Page 18 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

    Anzeige- und Bedienmodul

    4 20 mA

    HART

    Profibus

    PA

    Foundation

    Fieldbus

    FeaturesRelay output

    Analogue and digital inputs

    Serial multi-gauge communication bus

    Qualified up to SIL2

    Simple electronics exchange

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    plics Housing

    Page 19 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

    Stainless steelAluminium

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    plics Indicating and adjustment module

    Page 20 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

    VEGACONNECTPLICSCOM

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    One module for all plics

    instrumentsSimple adjustment via four

    compact membrane keys

    Measured value indication with unit

    Clear text with graphical elements

    Lighting (optional)Device information

    Diagnostics messages

    Configuration and parameter adjustment

    Page 21 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

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    Display

    Measured value indication with unitPlain text with graphic elements

    Multilingual menu

    Lighting

    Simple navigation

    Clear menu structures

    Tree structures

    Unambiguous terms

    PLICSCOM Easy and informative

    Page 22 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

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    plics Sensor system

    Page 23 August 31, 2011 Roland Bonath

    Radiation-based process instrumentation

    PVT

    scintillator

    Flexible

    plastic

    scintillator

    NaI crystal

    NEW

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    Source container VEGASOURCE

    Page 24 31 August 2011 Roland Bonath

    Radiation-based process instrumentation

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    Design of the source container VEGASOURCE

    Page 25 31 August 2011 Roland BonathRadiation-based process instrumentation

    Benchmarking data

    Small space requirement andsimple mounting

    Safe and easy source

    replacement

    Padlock for fixing the function

    settings

    Pneumatic switch-ON /

    switch-OFF

    Collimation angle 5, 20 and 40

    Fire-proof version

    821C / 30 min. (according ISO

    7205, IEC 60405, AERB/SS/2,ANS N538)

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    Design of the source container VEGASOURCE

    Page 26 31 August 2011 Roland BonathRadiation-based process instrumentation

    Benchmarking data

    Small space requirement andsimple mounting

    Safe and easy source

    replacement

    Padlock for fixing the function

    settings

    Pneumatic switch-ON /

    switch-OFF

    Collimation angle 5, 20 and 40

    Fire-proof version

    821C / 30 min. (according ISO

    7205, IEC 60405, AERB/SS/2,ANS N538)

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    Design of the source container VEGASOURCE

    Page 27 31 August 2011 Roland BonathRadiation-based process instrumentation

    Benchmarking data

    Small space requirement andsimple mounting

    Safe and easy source

    replacement

    Padlock for fixing the function

    settings

    Pneumatic switch-ON /

    switch-OFF

    Collimation angle 5, 20 and 40

    Fire-proof version

    821C / 30 min. (according ISO

    7205, IEC 60405, AERB/SS/2,ANS N538)

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    Design of the source container VEGASOURCE

    Page 28 31 August 2011 Roland BonathRadiation-based process instrumentation

    Engineering design

    Model A (Standard)

    Figure: VEGASOURCE 35 Figure: VEGASOURCE 31

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    Design of the source container VEGASOURCE

    Page 29 31 August 2011 Roland BonathRadiation-based process instrumentation

    Benchmarking data

    Weight with manual ON/OFF:SE31 app. 40 kg

    SE35 app. 87 kg

    Weight with pneumatic ON/OFF:

    SE31 app. 50 kg

    SE35 app. 97 kg

    Max. Cs-137 loading:

    SE31: 600 mCi /22,2 GBq

    SE35: 3.000 mCi / 111 GBq

    Max. Co-60 loading:

    SE31: 20 mCi / 740 MBq

    SE35: 100 mCi / 3,7 GBq

    Montingflange:

    DN100 PN16

    Ambient temperature:

    -40 C ... +200 C

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    Design of the source container VEGASOURCE

    Page 30 31 August 2011 Roland BonathRadiation-based process instrumentation

    Equivalent dose

    The equivalent dose defines theenergy dose taken in by the body

    through ionising radiation

    Measurement unit for the dose

    rate is the microsievert/hour

    (Sv/h)

    The sievert (Sv) unit is a measure

    of the biological effects of

    radiation

    The largest exposure results from

    a medical x-ray examination

    The dose rate a radiation sourcegenerates depends on the activity

    and the distance

    8,848 m

    1.0

    Mount

    Everest

    2,962 m

    0.1

    Zugspitze

    0 m

    0.01Venice

    Dose rate in Sv/h

    12,500 m

    5.0A

    ltitude

    Scintillation

    detector1.0

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    Mounting instructions

    Page 31 31 August 2011 Roland BonathRadiation-based process instrumentation

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    Mounting instructions

    Page 32 31 August 2011 Roland BonathRadiation-based process instrumentation

    Mounting position for cont. level

    The source container must bemounted at the height of, or

    slightly above, the max. level

    The radiation must be aligned

    exactly with the detector

    The source container and

    detector should be mounted as

    close as possible to the vessel to

    avoid control zones

    An gap between source container

    and vessel must be blocked off

    and marked.

    In general two or more source

    containers are used for large

    measuring ranges

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    Mounting instructions

    Page 33 31 August 2011 Roland BonathRadiation-based process instrumentation

    Mounting position for cont. level

    The source container must bemounted at the height of, or

    slightly above, the max. level

    The radiation must be aligned

    exactly with the detector

    The source container and

    detector should be mounted asclose as possible to the vessel to

    avoid control zones

    An gap between source container

    and vessel must be blocked off

    and marked.

    In general two or more source

    containers are used for large

    measuring ranges

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    Mounting instructions

    Page 34 31 August 2011 Roland BonathRadiation-based process instrumentation

    Mounting position for cont. level

    The source container must bemounted at the height of, or

    slightly above, the max. level

    The radiation must be aligned

    exactly with the detector

    The source container and

    detector should be mounted asclose as possible to the vessel to

    avoid control zones

    An gap between source container

    and vessel must be blocked off

    and marked.

    In general two or more source

    containers are used for large

    measuring ranges

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    Mounting instructions

    Page 35 31 August 2011 Roland BonathRadiation-based process instrumentation

    Mounting position for point level

    The source container version withan collimation angle = 5 is

    recommended for point level

    If larger collimation angle

    (20 or 40) are used, ensure that

    the ray is horizontal

    For this purpose, mount theradiation source container in such

    a way that the eyelet is

    positioned horizontally.

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    Mounting instructions

    Page 36 31 August 2011 Roland BonathRadiation-based process instrumentation

    Mounting position for density

    The most constant conditions fordensity measurement in pipes

    are achieved if the unit is

    mounted on vertical pipes

    If only horizontal pipes are

    accessible, the path of the ray

    should also be arrangedhorizontally to reduce the

    influence of air bubbles and

    build-up.

    In order to achieve a longer path

    of the radiation through the

    medium and thus a largermeasuring effect

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    Pipe mounting bracket KV31

    Page 37 31 August 2011 Roland BonathRadiation-based process instrumentation

    Figure: Pipe mounting bracket KV31 - vertical detector mounting

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    Pipe mounting bracket KV31

    Page 38 31 August 2011 Roland BonathRadiation-based process instrumentation

    Figure: Pipe mounting bracket KV31 - horizontal detector mounting

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    Pipe mounting bracket KV31

    Page 39 31 August 2011 Roland BonathRadiation-based process instrumentation

    Figure: 30 pipe mounting bracket KV31with diagonal beam

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    Mounting accessoires

    Page 40 31 August 2011 Roland BonathRadiation-based process instrumentation

    Figure: L-bracket PTB3 for FIBERTRAC and MINITRAC

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    Setup / Adjustment

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    Configuration and parameter adjustment

    Page 42 31 August 2011 Roland BonathRadiation-based process instrumentation

    Communication with all systems

    Standard communication protocolsare available for adjustment and

    connection in process automation

    4 20 mA /HART

    Profibus PA and

    Foundation Fieldbus

    All settings can be made with oneadjustment software (DTM or EDD)

    Simple setup is also possible via

    the indicating and adjustment unit

    PLICSCOM

    PLS/SPS

    VEGAMET

    DTM EDD

    AMS/

    PDM

    EDD

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    Service and diagnosis Asset Management

    Page 43 31 August 2011 Roland BonathRadiation-based process instrumentation

    Asset management functions

    Standardized status messages acc.to NE 107 or VDI/VDE 2650

    Detailed diagnosis in the

    instrument with cleartext display

    Digital transmission via HART,

    Profibus and Foundation Fieldbus

    Preventive maintenance

    Early recognition of malfunctions

    Diagnosis evaluation with

    PACTware 4.0

    Simplified servicing

    Failure

    Maintenance

    Function control

    Out of specification

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    Background calibration

    The background calibration isnecessary in order to register the

    natural background radiation

    The pulse rate of this background

    radiation is automatically

    subtracted from any other

    measured pulse rate

    Configuration and parameter adjustment

    Page 44 31 August 2011 Roland BonathRadiation-based process instrumentation

    80

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    Full calibration

    The radiation is switched onMost of the Gammaphotones will

    be blocked by the liquid

    The pulse rate is low

    Background pulse rate of the

    background radiation is

    automatically subtracted

    Configuration and parameter adjustment

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    185

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    Configuration and parameter adjustment

    Page 46 31 August 2011 Roland BonathRadiation-based process instrumentation

    Empty calibration

    The radiation is switched onWithin the measuring range, the

    vessel is emptied as far as possible

    Ideally: 0%, maximum 40%

    Background pulse rate of the

    background radiation is

    automatically subtracted

    3891

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    Configuration and parameter adjustment

    Page 47 31 August 2011 Roland BonathRadiation-based process instrumentation

    Measuring mode

    The amount of pulse rate dependson the filling level

    An low number of pulses means an

    high filling level of the vessel

    The measured pulse rate is inverse

    proportional to the filling level

    An detailed relation between filling

    level and pulse rates is defined by

    the Linearization curve

    1941

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    Configuration and parameter adjustment

    Page 48 31 August 2011 Roland BonathRadiation-based process instrumentation

    Density measurement

    For density and concentrationmeasurements the MINITRAC

    needs the two parameters:

    The absorption coefficient of the

    measured material

    The reference pulse rate Io

    For many applications an one-pointcalibration is sufficient

    This calibration point should be

    located as near as possible to the

    operating point

    If high accuracy is required over

    the complete measuring range twoor more calibration points should

    be applied.

    899

    DTM

    sample 1

    sample 1

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    Configuration and parameter adjustment

    Page 49 31 August 2011 Roland BonathRadiation-based process instrumentation

    Density measurement

    The calibration points for anmultiple point calibration should be

    located as far from each other as

    possible

    The calibration points should be

    uniformly distributed over the

    measuring range

    1491

    DTM

    sample 2

    sample 2

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    Configuration and parameter adjustment

    Page 50 31 August 2011 Roland BonathRadiation-based process instrumentation

    Density measurement

    After the calibration points havebeen entered, the MINITRAC

    automatically calculates the

    linearization curve

    For recalibration (e.g. buildups in

    the pipe) the parameterreal value

    correction can usedThe absorption coefficient is

    kept unchanged from the original

    calibration

    I = 10 * e - * roh * d

    1491

    sample 2

    sample 1

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    DTM Device Type Manager

    Device DTMDriver for field devices and

    Remote I/O

    Communication DTM

    Driver for communication protocols

    such as Profibus, Foundation

    FieldbusProvides all instrument-specific

    data and functions

    Runs in different frame applications

    such as PACTware, ABB, etc.

    Configuration and parameter adjustment

    Page 51 August 31, 2011 Roland BonathRadiation-based process instrumentation

    LIVE

    Demo

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    Electrical connection

    Two connection chambers areavailable

    Depending on the instrument

    version the signal output is either in

    the primary or in the secondary

    chamber

    Configuration and parameter adjustment

    Page 52 August 31, 2011 Roland BonathRadiation-based process instrumentation

    Secondary terminal connections

    Primary terminal connections

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    Primary terminal connections

    1. Power supply

    2. Power supply

    3. 4 20 mA active output

    (only explosion protected devices)

    4. 4 20 mA passive output

    (only explosion protected devices)

    5. 4 20 mA input

    6. Switching input open collector

    7. Switching input relay contact

    8. Switching output (NPN transistor

    9. Multisensor communication bus

    10. 2x address switches for MGC

    Secondary terminal connections

    1. 4 20 mA output option (IS safe devices)

    2. PLICSCOM connection

    3. Connections for external indication (VEGADIS)

    4. Ground connection

    Configuration and parameter adjustment

    Page 53 August 31, 2011 Roland BonathRadiation-based process instrumentation

    Secondary terminal connections

    Primary terminal connections

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    Density calibration example

    Density calibrationOne point calibration

    Min. process value: 1,5 kg/m

    Max. process value: 3,0 kg/m

    Pipe diameter 200 mm

    Pulse rate for density 3,0 kg/m:

    1000 ct/s

    Pulse rate for density 1,0 kg/m:

    3000 ct/s

    Lesson:Setup the gauge

    Build an linearization curve

    Configuration and parameter adjustment

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    Source container shipping

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    Source loading

    Eckert & Ziegler load theVEGASOURCE container

    Eckert & Ziegler labels the type

    plate

    Eckert & Ziegler ship the source

    container direct to the end user

    Source container shipping

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    Source container shipping

    Page 57 August 31, 2011 Roland BonathRadiation-based process instrumentation

    1. Serial number VEGASOURCE container2. Order code3. Document ID4. Radiation angle5. Local dose rate at a defined distance from the surface

    6. Wording "Hochradioaktive Strahlenquelle"(highly radioactive source), depending on activity

    7. Isotope (Cs-137 orCo-60)8. Serial number of the source capsule9. Source activity in Bq and mCi10. Manufacturing date of the source capsule

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    Editorial

    Field service training radiation-based process instrumentation

    Version: EN 18 October 2010

    VEGA Grieshaber KG

    Am Hohenstein 11377761 Schiltach

    Germany

    Phone +49 7836 50-0

    Fax +49 7836 50-201

    E-mail [email protected]

    www.vega.com

    R di ti b d i t t ti