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PANDIT DEENDAYAL PETROLEUM UNIVERSITY

SCHOOL OF TECHNOLOGY

COURSE STRUCTURE FOR B. TECH. CHEMICAL ENGINEERING

From Academic year (2016-2017)

SEMESTER III B.TECH CHEMICAL ENGINEERING

Sr.

No

.

Course

Code

Old

Code

Course Name Teaching Scheme Examination Scheme

L T P C Hrs/

Wk

Theory Practical Total

Marks

MS ES IA LW LE/Viva

1 MA201 Mathematics III 3 1 0 4 4 25 50 25 - - 100

2 CH201T Fluid Mechanics 3 1 0 4 4 25 50 25 - - 100

3 CH202 Chemical Process Calculations 3 1 0 4 4 25 50 25 - - 100

4 SC201 Engineering Chemistry 3 1 0 4 4 25 50 25 - - 100

5 CH205T Mechanical Unit Operations 3 1 0 4 4 25 50 25 - - 100

6 CH201L Fluid Mechanics Lab - - 3 1.5 3 - - - 25 25 50

7 CH205L Mechanical Unit Operations

Lab

- - 3 1.5 3 - - - 25 25 50

8 Civic and Social Service

Internship, CSSI (Evaluation)

1 100

Total 15 5 6 23+1 26 600+

100

MS = Mid Semester, ES = End Semester; * IA = Internal assessment (like quiz, assignments etc)

LW = Laboratory work; LE = Laboratory Exam

+ Marks for report writing

MA201T Mathematics III

Teaching Scheme Examination Scheme

L T P C Hrs/Week Theory Practical Total

marks MS ES IA LW LE/Viva

3 1 - 4 4 25 50 25 - - 100

Course Objective:

To impart knowledge of basic and applied sciences.

To connect linear algebra to other fields both within and without mathematics.

To introduce students the theory and concepts of linear algebra, Fourier Series, Special

Functions and Applications of Partial Differential Equations which will equip them with

adequate knowledge of mathematics to formulate and solve problems analytically.

Apply Fourier series expansion to different kind of wave forms and solve some partial

differential equations using Fourier series

Syllabus:

UNIT I Systems of linear equations : Matrices , Matrix Operations, Special matrices,

Elementary Matrices, Elementary transformation, Rank, Introduction to systems of Linear

Equations, Conditions for consistency of the system, Solution by Gauss and Gauss Jordan

Elimination Method, Solving system of equation using inverse of a Matrix and Cramer’s rule.

UNIT II Vector spaces: Euclidean n - space, Linear Transformations from Rn to R

m; Properties

Linear Transformations from Rn to R

m, Matrices of General Linear Transformations, Similarity;

Isomorphisim, Vector space and Subspaces, Linear dependence and Independence; Basis

Dimension, Row space; null space; column space and rank of a matrix, Rank and Nullity,

Dimension Theorem, Inner product spaces, Eigen values and Eigen vectors, Inner products ,

Angle and Orthogonality in Inner Product Spaces, Orthonormal Bases; Gram-Schmidt process;

Least squares approximation, Orthogonal Matrices, Eigen values and Eigen vectors,

Diagonalization.

UNIT III Fourier Series: Periodic functions, Euler's formulae, Dirichlet's conditions,

expansion of even and odd functions, half range Fourier series, Perseval's formula, complex form

of Fourier series.

Special Functions: Power series method to solve the equation, Frobenius method for solution

near regular singular points, Legendre’s equation, Legendre polynomials, Rodrigue’s formula,

Bessel’s equation and orthogonality..

UNIT IV Partial Differential Equations and its Applications: Classification of partial

differential equations, solutions of one dimensional wave equation, one dimensional unsteady

heat flow equation in Cartesian and polar coordinates by variable separable method with

reference to Fourier trigonometric series and by Laplace transform technique

Texts and References

11. Higher Engineering Mathematics, R. K. Jain & S. R. K. Iyernagar.

2. E.Kreyszig, Advanced engineering mathematics (8th Ed.), John Wiley (1999)

3 Ordinary and Partial Differential Equations by M.D. Raisinghania, 8th

edition, S. Chand

Publication (2010)

4. H.Anton, Elementary linear algebra with applications (8th ed.), John Wiley (1995)

5. G.Strang, Linear algebra and its applications (4rh Ed.), Thomson (2006)

Self Study: The course coordinator may assign a portion of the syllabus (max-10% of the

syllabus or equivalent to maximum 4 lecture hours) as self study by the students.

Course Outcomes:

Solve a system of linear equations by gauss elimination method and find the inverse of a

matrix.

Diagonalize a matrix using its eigenvectors.

Formulate Fourier series for various wave forms and solve some partial differential

equations using Fourier series.

Become familiar with various applications of partial differential equations and their

solution methods.

Fluid Mechanics




3 1 - 4 4 25 50 25 - - 100

Course Objective:

To develop an ability to apply knowledge of mathematics and physics to solve problems

in fluid flow operations in chemical process industries.

To Develop understanding of basic concepts of fluid flow and flow analysis leading to

systematic problem solving skills.

Understand the concept of designing a flow system involving various flow types.

Design and analysis of fluid transportation devices and systems including agitation and

mixing.

Gain an understanding of how the analysis of experimental data is carried out .

Syllabus:

UNIT I Definition and properties of fluid, Types of flow, steady and unsteady, laminar and

turbulent flows, relationship between shear stress and pressure gradient, Hagen Poiseuille

equation. Prandtl mixing length theory and eddy diffusivity, losses in pipes and fittings.

UNIT II Continuity equation for compressible and incompressible fluids. Bernoulli equation,

Euler equation. Equation of motion. Darcy-Weisbach equation for frictional head loss, friction

factor, Moody diagram. Velocity profile and boundary layer calculations for turbulent flow.

UNIT III Handling of fluids: Pumps, compressors and blowers for handling different fluids,

Standards for pumps, compressors and blowers, valves, pipe fittings and their standards, power

requirement for flow. Piping layout and economical pipe diameter. Mixing and agitation:

calculation of power numbers and mixing indices. Liquid-liquid and liquid solid mixing.

UNIT IV Flow metering devices: orificemeter, venturimeter, rotameter, pitot tube, anemometer

etc. Flow through open channels such as notches, weirs, nozzles. Vacuum producing devices; two

phase flow: basic principles and applications


1. W. L. McCabe and J. C. Smith, P. Harriot, Unit Operations of Chemical Engineering 7th ed.

McGraw Hill 2014.

2. J. M. Coulson and J. F. Richardson, Chemical Engineering Vol. I, 6th

Edition, Elsevier Press,

1999.

3. S. Foust, L. A. Wenzel, C. W. Clump, L. B. Andersen. Principles of Unit Operations, 2nd ed.

Wiley, New York, 2008

4. Y A Cengel and J M Cimbala, Fluid Mechanic: Fundamentals and applications, 3rd Edition,

Tata McGraw Hill, 2013

5. P N Modi and S M Seth, Hydraulics and fluid Mechanics, 19th

Edition, Standard Book House,

2009



Course Outcomes:

Basic Knowledge of principles of fluid flow operations

Ability to analyze fluid flow problems with the application of conservation principles of

mass, energy and the momentum

Understand design of fluid transportation systems such as pumps, compressors etc, and

ability to specify the fluid transportation devices for process applications

Fluid Mechanics Lab




- - 3 1.5 3 - - 25 25 50

Objective: Describe how to design experiments, perform experiments, and analyse and

interpret the observations yielded.

List of Experiments:

1. Study of flow regimes by Reynolds’s apparatus

2. Study of Bernoulli’s equation

3. Determination of Viscosity by efflux time measurement

4. Study of friction factor in close conduits

5. Study of minor losses and determination of equivalent length of pipe fittings

6. Study of venturimeter

7. Study of orifice meter

8. Calibration of rotameter

9. Studies of Pitot tube

10. Characteristics of centrifugal pump

11. Study of friction factor in annular flow

12. Determination of Viscosity by Stokes’s Law

Chemical Process Calculations




3 1 - 4 4 25 50 25 - - 100

Course Objective:

To develop an ability to apply the knowledge of basic sciences and basic engineering to solve

material and energy balance problems for unit processes and unit operations as preliminary

step of learning Chemical Engineering.

To accustom students with different process calculations in chemical engineering that makes

the base of any process design and evaluation.

To gain and apply the principles of mathematics, chemistry and thermodynamics to solve

energy balance of single and multiphase reaction systems.

To learn, Identify, formulate and analyze process calculations using different tools such as

computer aided calculations, spreadsheets.

Syllabus:

UNIT I Basic Concepts of processes - Units and Dimensions, Steady state and dynamic

processes, Lumped and distributed processes, Single and multiphase systems, unit processes and

unit operations.

Types of Variables - Intensive and extensive properties, Specific properties, State variables.

Types of Equations - Mass and energy conservation, equilibrium relations, Rate laws,

Constitutive equations for material behavior, Correlations for physical and transport properties.

UNIT II Thermodynamics of matter and properties of gases, liquids and solids, equations of

states, virial and cubic equations of state, generalized correlations, PVT behavior of mixtures.

phase equilibria for ideal mixtures, Reactions and stoichiometry.

Steady State Processes Material Balances: Reacting single phase systems - Single and multiple

units without recycle, systems with recycle, bypass and purge operations, non-reacting multi-

phase systems, processes involving vaporization and condensation.

UNIT III Steady State Processes Energy Balances: Specific heat capacity, Enthalpy, Heat of

reaction, Thermo-chemistry, Isothermal systems, Adiabatic systems, Simultaneous material and

energy balances.

UNIT IV: Unsteady State Material and Energy Balances - Reaction rate laws, Transport laws.

Introduction to Computer Aided Process Calculations -Degrees of Freedom and Specifications,

Use of Spreadsheets, Tearing and Iterative techniques in Flow sheeting. Fuels and Combustion:

Combustion theory, Combustion equations, Theoretical excess air and equivalence ratio.


1. D.M. Himmelblau and J. B. Riggs, "Basic Principles and Calculations in Chemical

Engineering", 8th PHI Learning Pvt Ltd, 2014

2. B. I. Bhat and S. M. Vora, “Stoichiometry” Tata McGraw-Hill, New Delhi.

3. J. M. Smith and H. C. Van Ness “Introduction to Chemical Engineering Thermodynamics” 7th

ed. McGraw Hill, 2009.



Course Outcomes:

Understanding of the units, dimensions and performing basic chemical calculations based on

law of mass conservation and ideal gas law.

Able to find material balances of unit operations and processes with and without reactions

including recycle operations.

Able to find the heat of formation, heat of combustion, and make energy balances for a set of

reactions and the system.

Able to understanding the combustion process, air/oxygen requirement for the process. Able

to evaluate the mass and energy requirements of a process.

Engineering Chemistry




3 1 - 4 4 25 50 25 - - 100

Course Objective:

To form a basis for understanding behavior of substances through chemical means for

advanced study in engineering aspects.

To understand basic principles theories of electrochemistry and their application.

To understand the concept of different separation methods and the chemistry involve to

our surroundings.

To gain knowledge of different type of reactions and mechanism and to form a basis for

understanding behavior of surfaces for advanced study in engineering aspects.

To study the principles of nuclear chemistry and their application in different type of

instruments for analytical purpose.

Develop an ability to conduct qualitative and quantitative analysis using different

analytical instruments and solve problems using research-based knowledge,

interpretation of data and synthesis of information.

Syllabus:

UNIT I Electrochemistry: Specific, equivalent and molecular conductance, their determination,

theories of electrolytic conductance, Debye Huckel theory of strong electrolytes, Galvanic cells,

Reference electrodes and their potentials. Standard cell standard electrode potential determination

of dissociation constants of acids and bases, solubility product, hydrolysis constant hydrogen ion

concentration, Complex formation activity of electrolytes etc., theory of acid base indicators,

electrolytes etc., theory of acid base indicators, electro-metric titrations. Photochemical reactions,

Laws of Photo-chemistry.

UNIT II Separation methods: Concepts of precipitation, fractional distillation, fractional

crystallization, electro deposition, electro-dialysis, reverse osmosis, distribution (partition co

efficient),

Chromatography – Basic concepts; paper chromatography and thin layer chromatography with

suitable examples. Green Chemistry: Basic concepts, Factors affecting the environment like

ozone layer depletion, green house effect, acid rain etc, application of green chemistry to the

chemical industry processes

UNIT III Reactions and Mechanisms: Organic reactions and their mechanisms: types of organic

reactions; general methods of obtaining mechanisms, study of ionic, free radical and other

reactions Surface Chemistry: Interparticle forces, adsorption isotherms, determination of the

surface area of fine powders using BET theory, surface films. Colligative Properties and their

Experimental Determination: Boiling Point Elevation, Freezing Point depression, Osmotic

Pressure

UNIT IV Nuclear Chemistry: Nuclear fission and fusion, nuclear energy, nuclear reactors,

disposal of nuclear waste, radiation measurement and contentment Instrumental methods of

analysis: Basic principles and operations, applications, sampling techniques of gas

chromatographs, GCMS , FTIR, NMR, HPLC, spectroscopy etc., TGA, DTA, XRD, SEM


1. Atkins, Peter, ‘Physical Chemistry’, 8th ed New Delhi : Oxford & IBH Publishing House,

2006

2. Das, Ishwar, ‘An Introduction to Physical Chemistry’, New Age International (P) Limited;

New Delhi; , 2006

3. Manickam, Valli, ‘A Textbook of Analytical Chemistry’, Pharma Book Syndicate, 2006

4. Settle, Frank A, 'Handbook of Instrumental Techniques for Analytical Chemistry', Pearson

Education, 2004

5. Skoog, Douglas A, 'Fundamentals of Analytical Chemistry', 8th ed New Delhi : Cengage

Learning, 2004

6. Doble, Mukesh, 'Green Chemistry and Processes'New York : Elsevier, 2007

7. Jimenez-Gonzalez, Concepcion, 'Green Chemistry and Engineering: A Practical Design

Approach', New York, John Wiley and Sons, Inc, 2011



Course Outcomes:

Understanding the concepts of electrode potentials and electro chemical cells through the

theories of electrolytic conductance with an aim of achieving underlying electro-

analytical techniques

Establishing the principles of various separation methods with underlying principles for

targeted separations along with the basic concepts of green chemistry

Basics of reaction chemistry and mechanism are introduced with molecular interpretation

and surface chemistry of the molecules

Introduction to Nuclear chemistry and management and Introduction to various

characterization and sampling techniques for analysis of physics and chemistry of

substances

Mechanical Unit Operations




3 1 - 4 4 25 50 25 - - 100

Course Objective:

To identify the important physical mechanisms occurring in processes involving particles.

To understand the role of unit operations in Chemical industries, and the characteristics of

particulate solids, Principles of size reduction, particle dynamics and separation of particles.

To provide an overview of the methods and techniques of Mechanical Operations and use of

mechanical forces.

To understand the mineral processing techniques for the handling of raw materials for

different chemical industries.

UNIT I Particulate Solids - Particle Characterization, Particulates in Bulk, Blending of Solid

Particle, Classification of Solid Particles, sieving operation.

Size Reduction of Solids:- Mechanism of Size Reduction. Energy for Size Reduction, Methods

of Operation of Crushers, Nature of Material to be Crushed, Types of Crushing and pulverization

Equipments,

Settling and Sedimentation- Gravitational Sedimentation (free and hindered settling), Centrifugal

Separation, Flocculation. Clarifications and classification

UNIT II Fluidization - Characteristics of Fluidized Systems, Liquid-Solid and Gas-Solid

Systems, Application of Fluidization Technique.

Packed Columns - Flow of a Single Fluid through a Granular Bed, Dispersion,

UNIT III

Filtration - Theory of Filtration. Filtration Practices, Filtration Equipments, Centrifugation and

Filtration Calculations.

Gas Cleaning, principles and operation Gravity Separators, Centrifuge, cyclone separators,

Electrostatic Precipitators, gas scrubbers etc.

UNIT IV Solid handling - Pneumatic and Hydraulic Conveying, Flow of solids through silos and

hoppers. Storage and transport of powders. Particle size and shape measurement and analysis,

shape factor,. Principles of agglomeration, palletizing (cone and disk), press and tablelating

machines and extrusion and granulating machines.


1. J. M. Coulson and J. F. Richardson, Chemical Engineering, Vol. 2 (Particle Technology And

Separation Processes), 5th

Edition , Elsevier, 2006

2. W. L. McCabe and J. C. Smith, P. Harriot, Unit Operations of Chemical Engineering 7th ed.

McGraw Hill 2014.

3. W. L. Badger and J. T. Banchero, “ Introduction to chemical engineering”, McGraw-Hill

Education, 1st edition, 2001

4. L. A. Wenzel, C. W. Clump, L. Maus, L. B. Andersen, A. S. Foust, “ Principles of unit

operations”, Wiley, 2nd

edition, 2008

5. C. M. Narayanan and B. C. Bhattacharya , “Mechanical Operation for Chemical Engineers –

Incorporating Computer Aided Analysis”, Khanna Publishers, 3rd

edition, 2016



Course Outcomes:

Apply the techniques of mechanical operations to meet the need of chemical Industries.

Ability to select suitable size reduction equipment, solid-solid separation method and

conveying system.

Understanding fluid flow through packed and fluidized beds.

Able to identify the different types of mixing, agitation and conveying of solids; and

estimating the power requirement.

Acquaintance of the principles of separating ores for chemical industries.

Mechanical Unit Operations Lab




- - 3 1.5 3 - - - 25 25 50


1. Study of sedimentation

2. Determination of screen effectiveness

3. Study of cyclone separator

4. study the laws of crushing and grinding using ball mill

5. Study of fluidization

6. Power consumption in agitator

7. Study of screen analysis

8. Study of Vacuum leaf filter

9. Study of Conveyors

10. study the laws of crushing and grinding using jaw crusher

11. Study of friction factor in packed column

12. Pressure drop and characteristic studies of Fluidized Bed

XX XXXP Civic and Social Services Internship


L T P C Hr/week Report writing V/V Total

- - - 1 80 20 100

Duration: three weeks after second semester

Examination of CSSI will be conducted in III semester

PANDIT DEENDAYAL PETROLEUM UNIVERSITY

SCHOOL OF TECHNOLOGY

COURSE STRUCTURE FOR B. TECH. CHEMICAL ENGINEERING

SEMESTER IV B.TECH CHEMICAL ENGINEERING

Sr.

No

.

Course

Code

Old Codes Course Name Teaching Scheme Examination Scheme

L T P C Hrs/

Wk

Theory Practical Total

Marks

MS ES IA LW LE/

Viva

1 MA203T Probability, Statistics and

Numerical Analysis

3 1 0 4 4 25 50 25 - - 100

2 CH406T Environmental Engineering 3 1 0 4 4 25 50 25 - - 100

3 CH206T Chemical Engineering

Thermodynamics

3 1 0 4 4 25 50 25 - - 100

4 CH208T Chemical Process

Technology I

3 0 0 3 3 25 50 25 - - 100

5 CH207T Elements of Heat Transfer 3 1 0 4 4 25 50 25 - - 100

6 CH406L Environmental Engineering

Lab

- - 3 1.5 3 - - - 25 25 50

7 CH207L Heat Transfer Lab - - 3 1.5 3 - - - 25 25 50

8 Industrial Orientation

(3 weeks)

Total 15 5 6 22 25 600

MA202T Probability, Statistics and Numerical Analysis




3 1 - 4 4 25 50 25 - - 100

Course Objective:

Learning the technique to solve ordinary differential equations, integrals, algebraic and

transcendental equations using Numerical methods.

The course will develop an understanding of the elements of error analysis for numerical

methods.

Thus the course will further develop problem solving skills as Ordinary differential

equations occur in many scientific and engineering disciplines.

This course provides an introduction to probability theory and random variables.

The course also covers various distributions – discrete as well as continuous.

The students get to know about the theory of least squares and statistical averages. They

also learn about to collect and analyze the data that help in decision making.

Syllabus:

UNIT I Numerical Solution of System of linear equations & non-linear equations: Solution

of transcendental and non-linear equations by Bisection, RegularFalsi, Newton’s Raphson and

Secant method. Solution of a system of linear simultaneous equations by LU Decomposition,

Cholesky Decomposition, Jacobi and Gauss Seidel methods.Concept ofIll conditioned system.

UNIT II Interpolation and Numerical Integration: Introduction of Finite differences,

Operators, Newton Gregory Forward Interpolation Formula, Newton Gregory Backward

Interpolation Formula, Gauss’s Forward and Backward Interpolation Formula, Stirling’s Central

Difference Formula, Lagrange’s Interpolation Formula for unevenly spaced data, Inverse

Interpolation, Divided Differences, Properties of Divided Differences, Newton’s Divided

Difference Formula, Relation between Divided Differences and Ordinary Differences. Formulae

for Derivatives, Newton-Cotes’s Quadrature Formula, Trapezoidal rule, Simpson’s one-third

rule, Simpson’s Three-Eighth rule, Weddle’s rule, Romberg’s method, Double Integration.

Numerical solution of first order ordinary differential equation by Taylor series method, Picard’s

method, Euler’s method, Modified Euler’s method and Runge-Kutta (4th

order only) method.

Multi step methods: Adams-Moulton method and Milne’s method.

UNIT III Various approaches of probability-classical, frequency (statistical), subjective and

axiomatic. Theorems on probability, conditional probability, Independence, Baye’s Theorem.

Random variable-discrete and continuous. Distribution function and their properties, probability

mass and density functions.

UNIT IV Statistics: Mathematical Expectation, Moment Generating Function and its properties.

Probability distributions: Bernoulli, Binomial, Negative Binomial, Poisson and Normal

Distributions. Theory of least squares and curve fitting. Correlation-Simple, Multiple and Partial,

Regression lines and Regression coefficients.


1. B.S. Grewal, Numerical Methods in Engineering and Science with Programs in C &

C++,Khanna Publishers (2010).

2. S.S. Sastry, Introductory Methods for Numerical Analysis,4th

Ed., Prentice Hall of India

(2009).

3. M.K. Jain, S.R.K. Iyenger and R.K. Jain, Numerical Methods for Scientific and

Engineering Computation, 5th

Ed., New Age International (2007).

4. S.C. Gupta and V.K. Kapoor, Fundamentals of Mathematical Statistics, S. Chand

Publisher (2007).

5. R.K. Jain & S.R.K. Iyenger,Advanced Engineering Mathematics, 3rd

Ed., Narosa (2002).



Course Outcomes:

Common numerical methods and how they are used to obtain approximate solutions to

otherwise intractable mathematical problems.

Apply numerical methods to obtain approximate solutions to mathematical problems.

Derive numerical methods for various mathematical operations and tasks, such as

interpolation, differentiation, integration, the solution of linear and nonlinear equations,

and the solution of differential equations.

Analyze and evaluate the accuracy of common numerical methods.

Basic probability axioms and rules and the moments of discrete and continuous random

variables as well as be familiar with common named discrete and continuous random

variables.

How to derive the probability density function of transformations of random variables and

use these techniques to generate data from various distributions.

How to calculate probabilities, and derive the marginal and conditional distributions of

bivariate random variables.

Distinguish between different types of data.

Construct the probability distribution of a random variable, based on a real-world

situation, and use it to compute various raw and central moments of higher order.

Assess which distribution for summarizing a data set are most appropriate and highlight

interesting features of the data.

Environmental Engineering




3 1 - 4 4 25 50 25 - - 100

Course Objective:

To introduce the knowledge about different environment regulations, standards and norms

and apply this contextual knowledge to assess societal, health, safety, legal and cultural

issues and the consequent responsibilities relevant to professional engineering practice.

To introduce the knowledge about the cause of air and water pollution, to understand the

methodology of primary, secondary and tertiary treatment of waste water.

To understand different treatment techniques for the control of air, water and soil

pollution.

To give basic understandings of solid waste management system.

To give understandings of noise pollution, its effect and control methods.

Syllabus:

UNIT I Environmental regulations in India, Environmental Standards, Classification of

pollutants, Cleaner production practices, GPCB & CPCB norms

Air Pollutants - Various pollutants (like SOx, NOx, CO, organic vapors and particulate matter)

and their permissible limits

Air pollution control processes – settling chamber, Cyclone separators, dust collector, fabric

filters, venturi scrubbers, Electrostatic precipitators, wet scrubber, adsorption, absorption,

Catalytic reduction.

UNIT II Sources of water, Impurities in water, Indian & WHO standards for drinking water,

Water borne diseases and their control, Physical, chemical and biological characteristics of water

and waste water,

Sources of waste water and industrial effluents from fertilizer, petrochemical, pulp and paper,

caustic soda, tanning and sugar industries

Effluent Treatment methodologies Primary treatment processes -Sedimentation, Coagulation and

flocculation, filtration

Secondary treatment processes: (Biological treatment) - Design procedures for HRT, CRT, SVI,

MLSS, Activated Sludge Process, trickling filters, Drying of sludge & use of sludge for

designated & approved landfill sites and possibility of using as fertilizer.

UNIT III Tertiary Treatment Processes: Membrane processes, Adsorption and ion exchange,

chlorination, ozonation, Aeration, Softening, fluoridation, Recarbonation, Lime soda softening,

Desalination, Demineralization.

Solid Waste Management: Quantity, Composition and characteristics of solid waste, Methods of

solid waste treatment and disposal (Open dumping, Land filling, incineration, composting and

recycling)

Treatment of plastic and e-waste, recovery of valuable intermediates from plastic waste and e-

waste.

UNIT IV Noise Pollution: Definition, characteristics of sound and its measurement, Definition of

noise frequency, noise pressure, noise intensity, and noise threshold limit value, equivalent noise

level Sources, Effects and control of noise pollution, Noise level and its standards, Noise

pollution control

Alternate routes of manufacture and/or sequencing of operations as means pollution control and

recovery of chemicals. Alternate use of byproducts waste as means of pollution abatement.


1. C. S. Rao, “Environmental Pollution Control Engineering”, New Age International Publishers;

2nd edition, 2006

2. H. S. Peavy, D. R. Rowe and G. Tchobanoglous, "Environmental Engineering", McGraw-Hill

Education, India Edition, 1st Edistion, 2013.

3. Metcalf & Eddy, "Waste Water Engineering: Treatment, Disposal, Reuse", McGraw Hill

Education; 4th edition, 2002.

4. S. P. Mahajan, "Pollution Control in Process Industries", Tata McGraw Hill, New Delhi, 1st

Edition, 2001

5. N.M. Rao and H. V. N. Rao, " Air Pollution", Tata McGraw Hill, New Delhi, 1st Edition, 2001



Course Outcomes:

Able to understand air, water, noise and solid waste pollution sources, regulations and

standards

Able to apply knowledge for the design of water and waste water treatment process

Able to design and monitor air and water pollution control systems

Able to select and use suitable waste treatment techniques

Environmental Engineering Lab




- - 3 1.5 3 - - - 25 25 50


1. Determination of pH and conductivity of water and waste water

2. (a) Determine the normality and strength of a solution using conductivity meter

(b) Determination of Turbidity and Hardness

3. Determination of Acidity and Alkalinity

4. Determination of fluoride and sulphate

5. (a) Measurement of residual chlorine

(b) Determination of chloride

6. Determination of coagulant dose by jar test apparatus

7. Determination of DO and BOD and determination of rate kinetics constant of aerobic

reactions

8. Determination of COD and Solids

9. Presumptive test for coliform bacteria

10. Ambient air quality measurement using High Volume sampler

11. To study the principle, working, construction and operation of various instruments like

FTIR, Gas chromatograph, spectrophotometers, conductivity meter etc.

12. To verify the Beer’s Lambert’s law using UV/visible scpectrphotomenter.

13. Measurement of noise at different sources using sound meter

Chemical Engineering Thermodynamics




3 1 - 4 4 25 50 25 - - 100

Course Objectives:

To understands the basic concepts of chemical engineering thermodynamics,

To grasp principles of ideal and non ideal solution thermodynamics and various models

for non-ideal solutions.

To apply the principles of phase equilibrium and chemical equilibrium to analyze the

equilibrium problems.

Develop the ability to apply knowledge of physics and chemistry for the prediction and

modeling of equilibrium processes.

Syllabus:

UNIT I Thermodynamic Analysis of Chemical Process: Gibbs energy and its role in generating

function, Helmholtz free energy, relation between properties, Phase rule, phase diagrams, Phase

equilibrium and stability, Criteria of equilibrium, Vapour liquid equilibrium (VLE), liquid liquid

equilibrium (LLE), solid vapour equilibrium (SVE), solid liquid phase behavior characteristic

and qualitative behavior of these equilibrium systems

UNIT II Solution Thermodynamics, Ideal and non ideal solutions, Raoult’s law, Henry’s law,

Fugacity and fugacity coefficient, Excess properties, activity and activity coefficient, Activity

Coefficients from Excess Functions in Binary Mixtures, Application of Gibbs-Duhem Equation,

bubble point and due point calculation, heat effect of mixing process. Systems of Liquid-liquid

phase miscibility.

UNIT III Chemical Reaction Equilibrium- Equilibrium constant and equilibrium conversion and

their estimation, single reactions and multi reactions, phase rule and Duhem’s theorem for

reacting system. Electrochemical reactions.

UNIT IV Non-ideal solutions: Calculation of vapor liquid equilibria using equations of state and

activity coefficient approach. Fugacities in high pressure Redlich-Kwong and P-R equation of

state, Classical and excess free energy based mixing rules; Theories of solutions; Partition

function of a perfect Gas, Estimation of thermo physical properties especially by group

contribution methods


1. J. M. Smith and H. C. Van Ness “Introduction to Chemical Engineering Thermodynamics” 7th

ed. McGraw Hill, 2009.

2. K. V. Narayanan, “ A text book of chemical engineering Thermodynamics”, Prentice Hall

India Learning Private Limited, 2nd edition, 2013

3. S. I. Sandler. “Chemical, Biochemical and Engineering Thermodynamics”, John Wiley &

Sons; 4th Revised edition, 2006

4. J. M. Prasusnitz, R. N. Lichtenthaler, and E.G.de Azevedo, "Molecular Thermodynamics of

Fluid-Phase Equilibria", Prentice Hall; 3rd edition, 1998

5. B. E. Poling, J. M. Prausnitz, J. P. O'Connell, “ The properties of liquids and gases”, McGraw

Hill, 2001



Course Outcomes:

Understanding the properties and relationships among thermodynamic properties and

establishing fundamental property relations. Behavior of systems at equilibrium (VLE,

LLE and SVE).

Establishing the concept of chemical potential, fugacity and activity coefficients.

Determination of activity coefficient through excess Gibbs energy models.

Understanding the principles of chemical multiphase equilibrium and chemical reaction

equilibrium. Determining equilibrium constants and equilibrium compositions for

multiple reaction systems.

Up on successful completion of course the student should be able to understand properties

and relationships of fluids in equilibrium and interpret the behavior of real fluids through

development of thermodynamic models for engineering applications.

Elements of Heat Transfer




3 1 - 4 4 25 50 25 - - 100

Course Objective:

To develop an ability to apply knowledge of mathematics, physics, basic engineering and

to solve problems related to heat transfer in chemical process industries

To understand the different modes of heat transfer (conduction, convection and radiation)

and their application in process industries.

To understand heat balance equations and principles of heat exchangers.

To understand heat transfer with phase change involving in evaporation and condensation.

To understand combined heat transfer, this involves all modes of heat transfer.

UNIT I Fundamentals of heat transfer, types of heat transfer, mechanism of heat transfer, heat

transfer rate, flux, resistances.

Conductive heat transfer: Conduction through a single homogeneous solid, thermal conductivity

of solids, liquids and gases. Conduction through objects (flat surfaces, cylindrical bodies,

spherical object, finned surfaces) in series. Contact resistances. Composite walls, heat losses and

insulation, types of insulation materials. Concept of critical insulation thickness.

UNIT II Convective Heat transfer: Natural and forced convection Film and overall heat transfer

coefficients, Resistance concept, solid-fluid heat transfer, Laminar and turbulent flow heat

transfer, Coefficients for scale deposits, concept of L.M.T.D. in heat exchangers with co and

counter current flow. Effectiveness – N T U method in finned tube heat exchangers

UNIT III Heat transfer with phase change: Nucleation and boiling, Film wise and drop wise

condensation, film wise condensation on vertical and inclined surfaces, condenser design,

fundamentals of pervaporation Unsteady state heat conduction, lumped heat capacity system,

transient heat flow in a semi-infinite solid.

UNIT IV Radiation: Black and gray body radiations, plank’s law, Stephen-Boltzmann law, view

factor, luminous and non-luminous gases. Combined heat transfer, i.e. conduction, convection

and radiation together.


1 J. M. Coulson and J. F. Richardson, Chemical Engineering Vol. I and II, 6th

Edition, Elsevier

Press, 1999.

2. W. L. McCabe and J. C. Smith, P. Harriot, Unit Operations of Chemical Engineering, 7th ed.

McGraw Hill 2014.

3. D. Q. Kern, “Process Heat Transfer”, McGraw Hill, 2014.

4. J. P. Holman and S. Bhattacharyya, “Heat Transfer”, McGraw Hill Education, 10th edition,

2011



Course Outcomes:

Ability to comprehend and solve conduction, convection and radiation heat transfer

problems .

Able to explain the mechanism of heat transfer to a fluid in motion over a solid surface.

Able to perform a general Heat balance for various types of heat exchangers given that

the heat exchange process involves convection between two fluids and conduction

through the wall separating them.

Evaluate heat transfer with phase change during boiling and condensation.

Calculate radiation heat transfer between ‘black’ surfaces using electromagnetic radiation

principles and blackbody definitions of emissivity, absorptivity, reflectivity, and

tranmissivity on spectral and total basis.

Heat Transfer Lab




- - 3 1.5 3 - - - 25 25 50


1. Determination of thermal conductivity of solids

2. Studies in heat transfer by natural convection

3. To compare overall heat transfer coefficients for parallel flow and counter flow in double pipe

heat exchanger

4. To study the performance of 1-2 fixed tube sheet heat exchanger and calculate overall heat

transfer coefficient

5. Study of Effectiveness of fin tubes

6. Determination of Heat transfer coefficient in laminar flow

7. Study of Heat transfer in turbulent flow

8. Study of Heat transfer in agitated vessel/coils

9. Study of Radiation heat transfer

10. Heat transfer studies in plate heat exchanger

11. Heat Transfer studies in fluidized bed

Chemical Process Technology I




3 - - 3 3 25 50 25 - - 100

Course Objective:

Develop the ability to apply the knowledge of fundamental of chemical engineering to the

solution of complex problems of chemical process industry.

To understand basic knowledge of oxidation, reduction, alkylation, halogenations,

sulphonation, nitration and polymerization processes carried out in chemical industry.

To understand various production technologies of petrochemicals and organic chemicals

To understand the various process flow diagrams for the production of pharmaceuticals

and the salient features of the process.

To understand various production processes of fine and specialty chemicals.

Syllabus:

UNIT I Unit Processes: Principles of a few selected unit processes such as oxidation, reduction,

alkylation, halogenations, sulphonation, nitration and polymerization and important organic

products related to the same.

UNIT II Petrochemicals: Raw materials and principles involved in the production of olefins and

aromatics. C1, C2, C3, C4, compounds, Aromatics, Acetylene, butadiene and typical

intermediates from olefins and aromatics such as ethylene glycol, ethyl benzene, phenol, cumene,

and DMT.

UNIT III Organic chemicals: Importance in synthesis of organic chemicals, Resins, Plastic and

rubber chemicals, Dyes and intermediates, coal chemicals. Soap and detergents, starch, alcohol,

cellulose, paper, vegetable oils soaps, detergents. Manufacture of alcohol. Process economics

UNIT IV Surface coatings: Paints, varnishes lacquers, surfactants, resins.

Pharma and Biotech industry: - Introduction to enzymes. Basic concepts of drug design; some

drug types (antimalarials, antibiotics, antiseptic), structure and synthesis; Single cell protein

(SCP), and major pharmaceuticals, Enzymatic hydrolysis of cellulosic substances, penicillin,

paracetamol etc, manufacturing of biological products like insulin


1. George T. Austin, Shreve’s Chemical process Industries, McGraw Hill, 5th

edition, 2012

2. M. Gopala Rao and Marshall sitting, Dryden’s outlines of chemical technology , East-West

press, New Delhi, 3rd

edition, 1997

3. D. Venkateswarlu, Chemical Technology III manual of chemical technology, chemical

engineering education curriculum development center, I. I. T. Madras, 1977.

4. Kirk-Othmer, Encyclopedia of chemical Technology, Wiley-Blackwell, 4th

edition, 1998.

5. McKetta, Encyclopedia of Chemical Processing and Design, Marcel Dekker Inc., New York,

1994.



Course Outcomes:

Able to understand the basic knowledge of the different process carried out in chemical

industry.

Able to identify different unit operations and unit processes in a given process flow

diagram

Acquire thorough knowledge about some important process industries (petrochemicals,

soaps and detergents, dyes and intermediates, pharmaceuticals, etc.)

Able to recognize the importance of process economics in the industry

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