origin of indian ocean seamount province by shallow ... · variable violations of the “closed...
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SUPPLEMENTARY INFORMATIONDOI: 10.1038/NGEO1331
NATURE GEOSCIENCE | www.nature.com/naturegeoscience 1
Origin of Indian Ocean seamount province by shallow recycling of continental lithosphere; Hoernle et al. 2011.
SupplementaryInformationGuide
SupplementaryInformationFile1:40Ar/39Aranalyticalmethods,agedataand
step‐heatingagespectradiagrams.Pages2‐10.
SupplementaryInformationFile2:Sr‐Nd‐Pb‐Hfisotopeanalyticalmethods.
Pages11‐13.
SupplementaryInformationFile3:Tectonicmodeldescription.Pages14‐15.
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Suppl. File 1: 40Ar/39Ar analytical methods and age data.
Thirty-four dredged rock samples (SO199) and eight land samples (Christmas Island)
were dated by 40Ar/39Ar laser step-heating. Crystals (plagioclase, K-feldspar, hornblende)
matrix and glass particles were hand-picked from crushed and sieved splits (250-500µm).
Feldspar separates were etched in 15% hydrofluoric acid for 5 minutes in order to remove
alteration surfaces and adhering matrix material. All samples were washed and cleaned using an
ultrasonic disintegrator.
Separates were irradiated in aluminum trays and cans lined by cadmium foil at the 5-MW
reactor of the GKSS Research Center (Helmholtz-Zentrum Geesthacht, Germany). The neutron
flux was monitored using Taylor Creek Rhyolite Sanidine (TCR-2: 27.87 ± 0.04 Ma; Lanphere
and Dalrymple, 2000). 40Ar/39Ar laser step-heating analyses were carried out at the IFM-
GEOMAR Geochronology Lab using a 20W SpectraPhysics Argon-Ion laser and an MAP 216
series noble gas mass spectrometer. Ar Isotope ratios from mass spectrometry were corrected
for mass discrimination, background and blank values, J-value gradients, and interfering
neutron reactions on Ca and K.
The step-heating data are evaluated in age spectra (apparent age and error vs cumulative
39Ar) trying to detect plateaus (>3 consecutive steps comprising >50% of the 39Ar released,
with ages overlapping within 2Sigma errors), plateau ages representing the inverse-variance
weighted mean of the plateau step ages and errors. The MSWD (mean square weighted
deviates; should be <<3) and POF (probability of fit; should be >0.05 at 2 Sigma / 95%
confidence levels) are calculated to test the statistical robustness of the plateaus and plateau
ages (Baksi, 1999). Because many of the SO199 marine and land samples are variably strongly
altered, the degree of alteration was monitored critically by calculating alteration indices based
on the measured 36Ar/37Ar ratios (plagioclase, hornblende, matrix, basaltic glass) or measured
36Ar/39Ar ratios (K-feldspar) following the methods established by Baksi (2007).
Results of step-heating analyses which yielded scattered age spectra, too small plateaus
(39Ar<<50%), statistically invalid plateaus (POF<<0.05), or large-error pseudo-plateaus were
rejected. All of these exhibit excessively high alteration indices (36Ar/37Ar) throughout the age
spectra, reflecting a significant uptake of (atmospheric) 36Ar during alteration, and indicating
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variable violations of the “closed system” assumption, such as gain or loss of the
parent/daughter after formation/closure.
Fourtythree step-heating analyses yield statistically valid plateau ages and plateau range
alteration indices around and close to the cut-off values for fresh sample material suggested by
Baksi (2007). Low-temperature heating steps generally yield 10 to 100 times higher alteration
indices, but are not included in the plateau age calculation. Results are summarized in Table 1.
References:
Baksi, A.K., 1999. Revaluation of plate motion models based on hotspot tracks in the Atlantic
and Indian oceans: Journal of Geology, v. 107, p. 13–26.
Baksi, A.K., 2007. A quantitative tool for detecting alteration in undisturbed rocks and minerals
- I: Water, chemical weathering, and atmospheric argon. Geological Society of America Special
Paper 430, p. 285-303.
Lanphere, M.A. and G.B. Dalrymple, 2000. First-principles calibration of 38Ar tracers:
Implications for the ages of 40Ar/39Ar fluence monitors. U.S. Geological Survey Professional
Paper 1621, 10 p.
Suppl. File 1: 40Ar/39Ar step-heating results table
Step-heating plateau data Sample No Material
Dated Age (Ma)
± 2σ (Ma)
MSWD Prob. %39Ar Steps Alteration Index
Cocos-Keeling Volcanic Province
SO199-DR13-1 plagioclase 56.0 ± 0.2 0.81 0.66 97.4 6 to 20
0.0002 - 0.002
SO199-DR13-12C
hornblende 55.6 ± 0.2 1.19 0.31 81.2 13 to 18
0.0002 - 0.0003
SO199 DR16-1C
hornblende 46.7 ± 0.2 0.96 0.47 86.4 8 to 17
0.0002 - 0.0004
SO199-DR21-1 matrix 47.0 ± 0.2 0.86 0.56 84.0 8 to 17
0.0002 - 0.0004
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Outsider Seamount
SO199-DR1-10 glass 53.4 ± 0.3 1.40 0.22 50.0 6 to 10
0.0003 - 0.001
Vening-Meinesz Volcanic Province
SO199-DR35-1A
plagioclase 63.6 ± 2.5 1.60 0.10 76.3 7 to 18
0.0001 - 0.001
SO199-DR40-1 plagioclase 70.4 ± 0.3 0.7 0.60 85.8 15 to 20
0.0001 - 0.0005
SO199-DR40-2 plagioclase 69.5 ± 0.5 0.8 0.57 81.1 12 to 17
0.0001 - 0.0003
SO199 DR40-3 plagioclase 70.1 ± 0.4 0.14 0.99 46.7 10 to 16
0.0007 - 0.001
SO199-DR42-1 plagioclase 71.6 ± 0.5 0.79 0.58 55.6 11 to 17
0.0002 - 0.0005
SO199 DR42-3 plagioclase 70.9 ± 0.5 1.09 0.36 52.1 7 to 12
0.0001 - 0.0002
SO199 DR44-1 plagioclase 63.5 ± 0.3 0.24 0.98 86.4 8 to 15
0.0001 - 0.0006
SO199-DR45-1 K-feldspar 64.9 ± 0.1 1.2 0.31 69.9 13 to 17
0.0001 - 0.0002
SO199-DR49-1 plagioclase 85.0 ± 0.4 1.2 0.32 76.8 10 to 14
0.0001 - 0.0002
SO199-DR49-3 plagioclase 84.2 ± 0.7 0.53 0.81 82.6 13 to 20
0.0002 - 0.0005
SO199-DR50-1 plagioclase 82.1 ± 0.2 1.5 0.17 79.5 11 to 17
0.0002 - 0.0006
SO199-DR50-9C
K-feldspar 81.1 ± 0.2 1.60 0.15 96.2 1 to 16
0.00003 - 0.0002
SO199-DR87-1 plagioclase 95.6 ± 1.4 1.7 0.14 62.3 12 to 17
0.00015 - 0.0003
SO199-DR87-19C
K-feldspar 89.8 ± 0.2 0.33 0.86 80.7 16 to 20
0.00002 - 0.00003
Christmas Island (Lower Volcanic Series)
SO199-DR55-1 plagioclase 40.2 ± 0.2 1.2 0.31 96.2 7 to 11
0.00015 - 0.00035
SO199-DR55-3 plagioclase 39.6 ± 0.4 0.20 0.94 65.3 15 to 19
0.00015 - 0.001
SO199-DR55-3 hornblende 39.3 ± 0.4 0.89 0.54 87.5 8 to 17
0.00007 - 0.0004
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CH5A matrix 41.1 ± 0.1 1.50 0.10 86.1 5 to 19
0.003 - 0.004
CH9 matrix 37.0 ± 0.6 1.70 0.11 52.3 5 to 12
0.004 - 0.08
CH11 matrix 42.6 ± 0.4 1.60 0.09 53.1 7 to 18
0.004 - 0.01
CH13 matrix 43.6 ± 0.4 2.00 0.02 64.9 6 to 17
0.007 - 0.009
Christmas Island (Upper Volcanic Series)
CH1A matrix 4.31 ± 0.14 1.40 0.11 100.0 1 to 19
0.001 - 0.01
CH2 matrix 4.50 ± 0.18 0.48 0.96 100.0 1 to 18
0.0008 - 0.02
CH3 matrix 4.52 ± 0.18 1.30 0.17 97.5 2 to 19
0.0007 - 0.01
CH4 matrix 4.35 ± 0.24 0.69 0.66 58.0 4 to 10
0.002 - 0.009
Eastern Wharton Basin Volcanic Province
SO199-DR56-1 plagioclase 105.3 ± 2.0 1.2 0.29 74.4 6 to 9 0.0002 - 0.009
SO199 DR57-1 plagioclase 107.1 ± 4.1 1.90 0.09 69.5 8 to 13
0.00015-0.0005
SO199-DR58-1 plagioclase 94.9 ± 0.4 1.4 0.20 85.6 13 to 20
0.00015-0.00025
SO199-DR58-2 plagioclase 94.3 ± 0.3 0.04 0.97 50.5 17 to 19
0.00015-0.0002
SO199-DR59-3 plagioclase 96.6 ± 0.4 1.40 0.22 89.5 10 to 15
0.0002-0.0009
SO199-DR65-1 plagioclase 103.6 ± 0.7 0.7 0.60 93.5 6 to 10
0.00015 - 0.0003
SO199-DR66-5 plagioclase 111.8 ± 6.5 1.70 0.09 59.8 11 to 19
0.0004 - 0.002
SO199-DR73-5 plagioclase 115.9 ± 3.8 1.60 0.09 49.6 10 to 20
0.0002 - 0.0007
SO199-DR73-11C
K-feldpar 114.7 ± 0.3 0.72 0.72 79.7 1 to12 0.00002 - 0.01
SO199-DR75-2 plagioclase 115.2 ± 2.3 2.90 0.002 89.1 9 to 18
0.0002 - 0.001
SO199-DR79-3 K-feldpar 101.5 ± 0.2 1.7 0.13 86.3 15 to 20
0.00003 - 0.00007
SO199-DR79-4 K-feldpar 101.8 ± 0.3 1.7 0.16 80.5 13 to 16
0.00003 - 0.0001
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Argo Basin Volcanic Province
SO199-DR72-1 plagioclase 136.2 ± 1.7 1.9 0.11 80.6 6 to 10
0.00015 - 0.0002
Suppl. File 1: 40Ar/39Ar step-heating age spectra
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30
40
50
60
70
80
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 53.42±0.31 Ma(2 , including J-error of .185%)MSWD = 1.4, probability=0.22
Includes 50% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
1-10gls
30
35
40
45
50
55
60
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 47.00±0.19 Ma(2 , including J-error of .185%)MSWD = 0.86, probability=0.56
Includes 84% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
21-1mxs
20
30
40
50
60
70
80
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 46.74±0.17 Ma(2 , including J-error of .185%)MSWD = 0.96, probability=0.47
Includes 86.4% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
16-1hbs
40
50
60
70
80
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 55.55±0.19 Ma(2 , including J-error of .185%)MSWD = 1.19, probability=0.31
Includes 81.2% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
13-12hbs
30
40
50
60
70
80
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 56.04±0.22 Ma(2 , including J-error of .185%)MSWD = 0.81, probability=0.66
Includes 97.4% of the 39Ar
Plateau steps are magenta, rejected steps are cyan
Box heightsare 2σ
30
40
50
60
70
80
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 56.04±0.22 Ma(2 , including J-error of .185%)MSWD = 0.81, probability=0.66
Includes 97.4% of the 39Ar
13-1fss
Cocos-Keeling Volcanic Province
Outsider Seamount
fss = feldspar step-heating analysishbs = hornblende step-heating analysismxs = matrix step-heating analysisgls = glass step-heating analysis
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0
20
40
60
80
100
120
140
160
180
200
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 63.6±2.5 Ma(2 , including J-error of .185%)MSWD = 1.6, probability=0.099
Includes 76.3% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
35-1Afss
50
60
70
80
90
100
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 70.35±0.32 Ma(2 , including J-error of .148%)MSWD = 0.73, probability=0.60
Includes 85.8% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
40-1fss
20
40
60
80
100
120
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 69.45±0.49 Ma(2 , including J-error of .148%)MSWD = 0.77, probability=0.57
Includes 81.1% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
40-2fss
40
50
60
70
80
90
100
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 70.06±0.40 Ma(2 , including J-error of .185%)
MSWD = 0.14, probability=0.992
Includes 46.7% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
40-3fss
20
30
40
50
60
70
80
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 71.62±0.46 Ma(2 , including J-error of .185%)MSWD = 0.79, probability=0.58
Includes 55.6% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
42-1fss
40
50
60
70
80
90
100
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 70.90±0.53 Ma(2 , including J-error of .186%)MSWD = 1.09, probability=0.36
Includes 52.1% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
42-3fss
30
40
50
60
70
80
90
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 63.46±0.33 Ma(2 , including J-error of .173%)MSWD = 0.24, probability=0.98
Includes 86.4% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
44-1fss
60
61
62
63
64
65
66
67
68
69
70
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 64.89±0.11 Ma(2 , including J-error of .137%)MSWD = 1.2, probability=0.31
Includes 69.9% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
45-1fss
40
50
60
70
80
90
100
110
120
130
140
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 84.98±0.40 Ma(2 , including J-error of .137%)MSWD = 1.17, probability=0.32
Includes 76.8% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
49-1fss
40
60
80
100
120
140
160
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 84.24±0.74 Ma(2 , including J-error of .156%)MSWD = 0.53, probability=0.81
Includes 82.6% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
49-3fss
70
80
90
100
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 82.05±0.21 Ma(2 , including J-error of .136%)MSWD = 1.5, probability=0.17
Includes 79.5% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
50-1Cfss
75
76
77
78
79
80
81
82
83
84
85
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 81.09±0.17 Ma(2 , including J-error of .173%)MSWD = 1.6, probability=0.15
Includes 96.2% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
50-9Cfss
0
40
80
120
160
200
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 95.6±1.4 Ma(2 , including J-error of .136%)MSWD = 1.7, probability=0.14
Includes 62.3% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
87-1fss
85
87
89
91
93
95
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 89.79±0.17 Ma(2 , including J-error of .142%)MSWD = 0.33, probability=0.86
Includes 80.7% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
87-19fss
Vening-Meinesz Volcanic Province
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0
50
100
150
200
250
300
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 105.3±2.0 Ma(2 , including J-error of .137%)MSWD = 1.2, probability=0.29
Includes 74.4% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
56-1fss
0
50
100
150
200
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 107.1±4.1 Ma(2 , including J-error of .161%)MSWD = 1.9, probability=0.087
Includes 69.5% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
57-1fss
50
100
150
200
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 94.87±0.41 Ma(2 , including J-error of .137%)MSWD = 1.4, probability=0.20
Includes 85.6% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
58-1fs2
0
40
80
120
160
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 94.26±0.33 Ma(2 , including J-error of .137%)
MSWD = 0.036, probability=0.97
Includes 50.5% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
58-2fs2
50
100
150
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 96.55±0.40 Ma(2 , including J-error of .161%)MSWD = 1.4, probability=0.22
Includes 89.5% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
59-3fss
50
100
150
200
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 103.61±0.74 Ma(2 , including J-error of .137%)MSWD = 0.69, probability=0.60
Includes 93.5% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
65-1fss
0
50
100
150
200
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 111.8±6.5 Ma(2 , including J-error of .161%)MSWD = 1.7, probability=0.090
Includes 59.8% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
66-5fss
0
40
80
120
160
200
240
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 115.9±3.8 Ma(2 , including J-error of .161%)MSWD = 1.6, probability=0.091
Includes 49.6% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
73-5fss
105
110
115
120
125
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 114.69±0.25 Ma(2 , including J-error of .161%)MSWD = 0.72, probability=0.72
Includes 79.7% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
73-11fss
0
50
100
150
200
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 115.2±2.3 Ma(95% conf.), including J-error of .161%)
MSWD = 2.9, probability=0.002
Includes 89.1% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
75-2fss
90
95
100
105
110
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 101.52±0.19 Ma(2 , including J-error of .148%)MSWD = 1.7, probability=0.13
Includes 86.3% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
79-3fss
90
95
100
105
110
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 101.80±0.34 Ma(2 , including J-error of .137%)MSWD = 1.7, probability=0.16
Includes 80.5% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
79-4fss
50
100
150
200
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 136.2±1.7 Ma(2 , including J-error of .137%)MSWD = 1.9, probability=0.11
Includes 80.6% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
72-1fss
Argo Basin Volcanic Province
Eastern Wharton Basin Volcanic Province
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20
30
40
50
60
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 40.15±0.23 Ma(2 , including J-error of .137%)MSWD = 1.2, probability=0.31
Includes 96.2% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
55-1fss
0
20
40
60
80
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 39.64±0.43 Ma(2 , including J-error of .156%)MSWD = 0.20, probability=0.94
Includes 65.3% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
55-3fss
20
30
40
50
60
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 39.29±0.40 Ma(2 , including J-error of .156%)MSWD = 0.89, probability=0.54
Includes 87.5% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
55-3hbs
25
35
45
55
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 41.08±0.13 Ma(2 , including J-error of .234%)MSWD = 1.5, probability=0.098
Includes 86.1% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
X5Amxs
20
30
40
50
60
70
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 36.96±0.55 Ma(2 , including J-error of .195%)MSWD = 1.7, probability=0.11
Includes 52.9% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
X9mxsA
ge (M
a)
30
40
50
60
70
80
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 42.61±0.40 Ma(2 , including J-error of .195%)MSWD = 1.6, probability=0.091
Includes 53.1% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
X11mxs
30
40
50
60
70
80
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 43.61±0.38 Ma(2 , including J-error of .195%)MSWD = 2.0, probability=0.023
Includes 64.9% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
X13mxs
Christmas Island (Lower Volcanic Series)
Christmas Island (Upper Volcanic Series)
0
2
4
6
8
10
12
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 4.31±0.14 Ma(2 , including J-error of .234%)MSWD = 1.4, probability=0.11
Includes 99.95% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
X1Amxs
0
2
4
6
8
10
12
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 4.50±0.18 Ma(2 , including J-error of .234%)MSWD = 0.48, probability=0.96
Includes 100% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
X2mxs
0
2
4
6
8
10
12
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 4.52±0.18 Ma(2 , including J-error of .234%)MSWD = 1.3, probability=0.17
Includes 97.5% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
X3mxs
0
2
4
6
8
10
12
0.0 0.2 0.4 0.6 0.8 1.0
Cumulative 39Ar Fraction
Age
(Ma)
Plateau age = 4.35±0.24 Ma(2 , including J-error of .234%)MSWD = 0.69, probability=0.66
Includes 58% of the 39Ar
Plateau steps are magenta, rejected steps are cyan box heights are 2
X4mxs
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Origin of Indian Ocean seamount province by shallow recycling of continental lithosphere; Hoernle et al. Suppl. File 2: Sr-Nd-Pb-Hf Isotopes: Analytical methods and data for the Christmas Island Seamounts and Christmas Island.
Samples selected for geochemistry were first crushed to small pieces, then
washed in de-ionized water and carefully handpicked under a binocular microscope.
Sr, Nd, and Double Spike (DS) Pb isotope analyses were determined on leached rock
chips (2N HCl at 70°C for 1 hour and triple rinsed with ultrapure water thereafter).
Powders used for Hf isotope analyses were not leached. The element chromatography
followed the methods of Hoernle and Tilton 1 and Hoernle et al. 2. Sr-Nd-Pb isotopic
ratios were analyzed in static multi-collection mode on the TRITON and MAT262
RPQ2+ thermal ionization mass spectrometers (TIMS) at IFM-GEOMAR. Sr and Nd
isotopic ratios are normalized within run to 86Sr/88Sr = 0.1194 and 146Nd/144Nd =
0.7219 respectively. All Sr isotope data are reported relative to NBS987 87Sr/86Sr =
0.710250 with an external 2s error (2 s.e.) of ±0.000016 (N=23) for the MAT262 and
2 s.e. of ±0.000011 (N=18) for the TRITON. Similarly the Nd isotope data
(exclusively determined on the TRITON) are reported relative to La Jolla 143Nd/144Nd= 0.511850± 0.000006 (N=30). Double Spike corrected NBS 981 values
(N=107) gave 206Pb/204Pb = 16.9420 ± 0.0029, 207Pb/204Pb = 15.4999 ± 0.0027, 208Pb/204Pb = 36.7257 ± 0.0071, 207Pb/206Pb = 0.91488 ± 0.00005 and 208Pb/206Pb =
2.16773 ± 0.00009. These values compare well with published double and triple spike
data for NBS981 3-7. For details of the Pb-DS technique see Hoernle at al. 8. Hf
chemistry was carried out following the methods of Blichert-Toft et al. 9 and isotope
ratios were measured in static mode on a VG Elemental AXIOM multi-collector
magnetic sector inductively coupled plasma mass spectrometer (MC-ICP-MS) at
IFM-GEOMAR. A subset of samples were measured on a Nu-Plasma II MC-ICP-MS
at IFM-GEOMAR. Our in-house SPEX Hf ICP standard solution (Lot #9) yields an
averaged, JMC 475-normalized value of 176Hf/177Hf = 0.282173 ± 0.000008 (n=132)
on the AXIOM and 176Hf/177Hf = 0.282170 ± 0.000007 (n=8) on the Nu Plasma II. A
detailed description of the Hf analytical procedures is found in Geldmacher et al. 10.
Total chemistry blanks were <100 pg for Sr, Nd, Hf and Pb and thus considered
negligible. Sr-Nd-Pb replicate analyses by means of separate dissolutions of SO199
DR57-1, SO199 DR35-1A and CH13 are within the external errors of the standards
except for a slightly larger offsets in 207Pb/206Pb for SO199 DR51-1 and 208Pb/204Pb
and 208Pb/206Pb for SO199 DR35-1A. The isotopic composition of the CHRISP
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Origin of Indian Ocean seamount province by shallow recycling of continental lithosphere; Hoernle et al. volcanic rocks covers a large range (e.g. 206Pb/204Pb = 17.3-19.3; 207Pb/204Pb = 15.49-
15.67; 143Nd/144Nd = 0.51220-0.51295; 176Hf/177Hf = 0.28246-0.28319; 87Sr/86Sr =
0.7036-0.7058). Trace element data (Rb, Sr, Sm, Nd, U, Th, Pb, Lu and Hf) were
determined on an Agilent 7500cs ICPMS at the Institute of Geoscience (Univeristy of
Kiel) after the methods of Garbe-Schönberg 11. A subset of samples marked with an
asterix were determined at AcmeLabs (http://acmelab.com/) by ICPMS following a
lithium metaborate/tetraborate fusion technique.
Table 2. Sr-Nd-Pb-Hf Isotope data.
Ages (bold) are from Supplementary File 1, Table 1. For undated samples the average
age (italic) of the respective volcanic province or unit is used to calculate the initial
isotopic ratios. For sample numbers marked with an asterix (*) the trace element
concentrations were determined at AcmeLabs. “_R” denotes replicate analyses in
terms of separate sample dissolution.
References:
1 Hoernle, K. A. & Tilton, G. R. Sr-Nd-Pb isotope data for Fuerteventura (Canary Islands) basal complex and subaerial volcanics: applications to magma genesis and evolution. Schweiz. Mineral. Petrogr. Mitt. 71, 3-18 (1991).
2 Hoernle, K. et al. Arc-parallel flow in the mantle wedge beneath Costa Rica and Nicaragua. Nature 451, 1094-1097 (2008).
3 Baker, J. A., Gamble, J. A. & Graham, I. J. The age, geology and geochemistry of the Tapuaenuku Igneous Complex, Marlborough, New Zealand. New Zeal. J. Geol. and Geophys. 37, 249-268 (1994).
4 Baker, J. A., Peate, D. W., Waight, T. E. & Thirlwall, M. F. Reply to the: Comment on "Pb isotopic analysis of standards and samples using a 207Pb-204Pb double spike and thallium to correct for mass bias with a double focusing MC-ICP-MS" by Baker et al. Chem. Geol. 217, 175-179 (2005).
5 Galer, S. J. G. & Abouchami, W. Practical application of lead triple spiking triple spiking for correction of instrumental mass discrimination. Mineral. Mag. 62A, 491-492 (1998).
6 Thirlwall, M. F. Inter-laboratory and other errors in Pb isotope analyses investigated using a 207Pb-204Pb double spike. Chem. Geol. 163, 299-322 (2000).
7 Thirlwall, M. F. Multicollector ICP-MS analysis of Pb isotopes using a 207Pb-204Pb double spike demonstrates up to 400 ppm/amu systematic errors in Tl-normalization. Chem. Geol. 184, 255-279 (2002).
8 Hoernle, K. et al. On- and off-axis chemical heterogeneities along the South Atlantic Mid-Ocean-Ridge (5-11°S): Shallow or deep recycling of ocean crust and/or intraplate volcanism? Earth Planet. Sci. Lett. 306, 86-97 (2011).
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Origin of Indian Ocean seamount province by shallow recycling of continental lithosphere; Hoernle et al. 9 Blichert-Toft, J., Chauvel, C. & Albarede, F. Separation of Hf and Lu for
high-precision isotope analyses of rock samples by magnetic sector-multiple collector ICP-MS. Contrib. Mineral. Petrol. 127, 248-260 (1997).
10 Geldmacher, J. et al. Origin and geochemical evolution of the Madeira-Tore Rise (eastern North Atlantic). J. Geophys. Res. 111, B09206, doi:10.1029/2005JB003931 (2006).
11 Garbe-Schönberg, C.-D. Simultaneous determination of thirty-seven trace elements in twenty-eight international rock standarts by ICP-MS. Geostand. Newslett. 17, 81-97 (1993).
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Origin of Indian Ocean seamount province by shallow recycling of continental lithosphere; Hoernle et al. Suppl. File 3. Tectonic model description.
Figure 3 was created using GPlates, a no-cost, interactive plate-tectonic and raster
visualization package (see http://www.gplates.org/ and 1 for more details). The
tectonic model 2,3 is based upon the identification of marine magnetic anomaly picks
from the Argo, Gascoyne, Cuvier and Perth abyssal plains, offshore Western
Australia, using gravity and magnetic potential field data and comparison with a
synthetic magnetic model. Rotation poles were derived iteratively invoking the best
visual fit and ensuring compliance within the available constraints such as fracture
zones and ODP/DSDP drill site minimum ages. The plate motion vectors in figure 3
are from 4-6 and references therein. Here are the rotation poles for Greater India 3, except 10.9 Ma 7, and 20.1 Ma 8: Time (Ma) Latitude Longitude Angle Relative plate 0.0 0.0 0.0 0.0 India-Central Indian Basin 10.9 -8.7 76.9 2.75 India-Central Indian Basin 20.1 -5.2 74.3 5.93 India-Central Indian Basin 83.5 23.25 -16.38 3.02 India-Central Indian Basin 83.5 16.6 24.66 -53.43 India-Madagascar 100.0 20.34 26.01 -57.43 India-Madagascar 106.0 23.01 26.85 -55.79 India-Madagascar 121.0 24.07 25.33 -54.75 India-Madagascar 124.0 23.04 25.03 -55.73 India-Madagascar 126.7 22.08 24.27 -56.61 India-Madagascar 126.7 0.87 -170.31 85.14 India-Antarctica128.96 1.29 -169.52 85.52 India-Antarctica129.5 1.45 -169.38 85.78 India-Antarctica136.0 2.79 -167.32 87.49 India-Antarctica600.0 2.79 -167.32 87.49 India-Antarctica And Argoland (West Burma Block): Time (Ma) Latitude Longitude Angle Relative plate 0.0 0.0 0.0 0.0 West Burma-India 80.0 0.0 0.0 0.0 West Burma-India 80.0 27.37 24.66 67.43 West Burma-India 85.0 34.06 44.26 76.32 West Burma-India 121.0 34.06 44.26 76.32 West Burma-India 136.0 -31.1 -127.86 -81.57 West Burma-India 136.0 14.91 102.95 73.6 West Burma-Australia
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Origin of Indian Ocean seamount province by shallow recycling of continental lithosphere; Hoernle et al. 146.0 8.44 112.29 86.24 West Burma-Australia 146.75 8.39 112.59 86.3 West Burma-Australia 148.12 8.12 113.42 86.47 West Burma-Australia 150.43 7.89 114.13 86.6 West Burma-Australia 150.7 7.74 114.51 86.67 West Burma-Australia 152.11 7.56 114.97 86.75 West Burma-Australia 153.54 7.42 115.37 86.83 West Burma-Australia 154.1 7.26 115.74 86.9 West Burma-Australia 155.0 7.13 116.06 86.98 West Burma-Australia 155.36 6.96 116.52 87.07 West Burma-Australia 600.0 6.96 116.52 87.07 West Burma-Australia
1 Boyden, J. A. et al. Next-generation plate-tectonic reconstructions using GPlates. in: Geoinformatics: Cyberinfrastructure for the Solid Earth Sciences, Keller G.R. and Baru, C., eds., Cambridge University Press, pp 388, ISBN: 9780521897150 (2011).
2 Gibbons, A., Whittaker, J. & Müller, R. D. Composite tectonic model for the early Indian Ocean. Geophysical Research Abstracts 13, EGU2011-5179, EGU General Assembly (2011).
3 Gibbons, A., et al. Constraining the Jurassic extent of Greater India: tectonic evolution of the West Australian margin: G3, submitted (2011). 4 Cande, S. C., Patriat, P. & Dyment, J. Motion between the Indian, Antarctic
and African plates in the early Cenozoic. Geophys. J. Int. 183, 127-149 (2010).
5 Eagles, G. & König, M. A model of plate kinematics in Gondwana breakup. Geophys. J. Int. 173, 703-717 (2008).
6 Whittaker, J. M. et al. Major Australian-Antarctic Plate Reorganization at Hawaiian-Emperor Bend Time. Science 318, 83-86, (2007).
7 Müller, R. D., Roest, W. R., Royer, J. -Y., Gahagan, L. M., and Sclater, J. G. Digital isochrons of the world's ocean floor. Journal of Geophysical Research 102, 3211-3214 (1997).
8 Royer, J. Y. & Chang, T. Evidence for relative motions between the Indian and Australian plates during the last 20 m.y. from plate tectonic reconstructions: implications for the deformation of the Indo-Australian plate. Journal of Geophysical Research 96, 11779-802 (1991).
© 2011 Macmillan Publishers Limited. All rights reserved.