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Link¨ oping Studies in Science and Technology. Dissertations No. 1478 On Material Modelling of High Strength Steel Sheets Rikard Larsson Division of Solid Mechanics Department of Management and Engineering Link¨ oping University, SE–581 83, Link¨ oping, Sweden Link¨ oping, September 2012

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Page 1: On Material Modelling of High Strength Steel Sheets545669/... · 2012-09-25 · strength steel, and is often referred to as DP600. The number in the name indicates that the lowest

Linkoping Studies in Science and Technology.Dissertations No. 1478

On Material Modellingof

High Strength Steel Sheets

Rikard Larsson

Division of Solid MechanicsDepartment of Management and Engineering

Linkoping University,SE–581 83, Linkoping, Sweden

Linkoping, September 2012

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Cover:Results from a finite element simulation of the mid part of a notched tensile test.

Printed by:LiU-Tryck, Linkoping, Sweden, 2012ISBN: 978-91-7519-791-3ISSN: 0345-7524

Distributed by:Linkoping UniversityDepartment of Management and EngineeringSE–581 83, Linkoping, Sweden

c© 2012 Rikard LarssonThis document was prepared with LATEX, September 24, 2012

No part of this publication may be reproduced, stored in a retrieval system, or betransmitted, in any form or by any means, electronic, mechanical, photocopying,recording, or otherwise, without prior permission of the author.

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Preface

The work presented in this thesis has been carried out at the Division of SolidMechanics at Linkoping University. It was initially funded by the VINNOVAMERA ”FE simulation of sheet metal forming” project. During the last two years,the work has been a part of the SFS ProViking ”Super Light Steel Structures”project.

A number of people have been important to me during these years. First ofall, I am grateful to my supervisor Prof. Larsgunnar Nilsson for his support andfeedback, and for pushing me forward. My colleagues, especially my fellow PhDstudents, deserve a great acknowledgement for their friendship and support duringthese years. The cooperation with SSAB, and especially with my co-supervisor,Dr Joachim Larsson, and with Dr. Jonas Gozzi, has been very appreciated. Thesame gratitude goes to Outokumpu Stainless and Dr. Ramin Moshfegh.

All the assistance I have received from Bo Skoog, Ulf Bengtsson and Soren Hoffat Linkoping University has greatly facilitated the experimental part of this work.

Finally, I would like to thank my beloved girlfriend Katrin, my family and myfriends. This work would not have been possible without their support.

Linkoping, September 2012Rikard Larsson

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Abstract

The work done in this thesis aims at developing and improving material modelsfor use in industrial applications. The mechanical behaviour of three advancedhigh strength steel grades, Docol 600DP, Docol 1200M and HyTens 1000, hasbeen experimentally investigated under various types of deformation, and materialmodels of their behaviour have been developed. The origins of all these materialmodels are experimental findings from physical tests on the materials.

Sheet metal forming is an important industrial process and is used to producea wide range of products. The continuously increasing demand on the weight toperformance ratio of many products promotes the use of advanced high strengthsteel. In order to take full advantage of such steel, most product development isdone by means of computer aided engineering, CAE. In advanced product devel-opment, the use of simulation based design, SBD, is continuously increasing. WithSBD, the functionality of a product, as well as its manufacturing process, can beanalysed and optimised with a minimum of physical prototype testing. Accuratenumerical tools are absolutely necessary with this methodology, and the model ofthe material behaviour is one important aspect of such tools.

This thesis consists of an introduction followed by five appended papers. In thefirst paper, the dual phase Docol 600DP steel and the martensitic Docol 1200Msteel were subjected to deformations, both under linear and non-linear strain paths.Plastic anisotropy and hardening were evaluated and modelled using both virginmaterials, i.e. as received, and materials which were pre-strained in various mate-rial directions.

In the second paper, the austenitic stainless steel HyTens 1000 was subjectedto deformations under various proportional strain paths and strain rates. It wasexperimentally shown that this material is sensitive both to dynamic and staticstrain ageing. A constitutive model accounting for these effects was developed,calibrated, implemented in a Finite Element software and, finally, validated onphysical test data.

The third paper concerns the material dispersions in batches of Docol 600DP.A material model was calibrated to a number of material batches of the samesteel grade. The paper provides a statistical analysis of the resulting materialparameters.

The fourth paper deals with a simple modelling of distortional hardening. Thistype of hardening is able to represent the variation of plastic anisotropy duringdeformation. This is not the case with a regular isotropic hardening, where theanisotropy is fixed during deformation.

The strain rate effect is an important phenomenon, which often needs to beconsidered in a material model. In the fifth paper, the strain rate effects in Docol600DP are investigated and modelled. Furthermore, the strain rate effect on strainlocalisation is discussed.

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List of Papers

In this thesis, the following papers have been appended in chronological order:

I. Larsson, R., Bjorklund, O., Nilsson, L., Simonsson, K., (2011) A study ofhigh strength steels undergoing non-linear strain paths - Experiments andmodelling, Journal of Materials Processing Technology 211, 122–132.

II. Larsson, R., Nilsson, L., (2012). On the modelling of strain ageing in ametastable austenitic stainless steel, Journal of Materials Processing Tech-nology 212, 46–58

III. Aspenberg, D., Larsson, R., Nilsson, L., (2012). An evaluation of the statis-tics of steel material model parameters, Journal of Materials Processing Tech-nology 212, 1288–1297

IV. Larsson, R., Nilsson, L., (2012). On isotropic-distortional hardening, Sub-mitted.

V. Larsson, R., Nilsson, L., (2012). Strain-rate effects in a high strengths dualphase steel, Submitted.

Own contribution

I have been the main author of all papers except Paper III, in which I participatedin the writing. I have been responsible for the material modelling and calibrationprocedures in all the papers.

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Contents

Preface iii

Abstract v

List of Papers vii

Contents ix

Part I Theory and background

1 Introduction 3

1.1 Motivation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

1.2 Objective . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

1.3 Investigated steels . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

1.4 This thesis . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

2 Material modelling 5

2.1 Main equations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

2.2 Plastic strain hardening . . . . . . . . . . . . . . . . . . . . . . . . 6

2.3 Plastic anisotropy in sheet metals . . . . . . . . . . . . . . . . . . . 7

2.4 Anisotropic hardening . . . . . . . . . . . . . . . . . . . . . . . . . 14

2.5 Degradation of the unloading modulus . . . . . . . . . . . . . . . . 17

2.6 Strain rate sensitivity . . . . . . . . . . . . . . . . . . . . . . . . . 18

2.7 Strain ageing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20

2.8 Thermal effects . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23

2.9 Phase transformations . . . . . . . . . . . . . . . . . . . . . . . . . 24

3 Mechanical testing of sheet metal 27

3.1 Uniaxial tensile tests . . . . . . . . . . . . . . . . . . . . . . . . . . 27

3.2 Biaxial testing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30

3.3 Notched tensile tests . . . . . . . . . . . . . . . . . . . . . . . . . . 31

3.4 Shear tests . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35

3.5 Cyclic bending tests . . . . . . . . . . . . . . . . . . . . . . . . . . 36

3.6 Two stage testing . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36

3.7 Dispersion of material properties . . . . . . . . . . . . . . . . . . . 38

4 Finite Element modelling 41

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5 Calibration procedures 435.1 Inverse analysis . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 435.2 Trial and error procedure . . . . . . . . . . . . . . . . . . . . . . . 45

6 Future work 47

7 Review of appended papers 49

Bibliography 53

Part II Appended papers

Paper I – A study of high strength steels undergoing non-linear strainpaths - experiments and modelling . . . . . . . . . . . . . . . . . . 63

Paper II – On the modelling of strain ageing in a metastable austeniticstainless steel . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 77

Paper III – An evaluation of the statistics of steel material model parameters 93

Paper IV – On isotropic-distortional hardening . . . . . . . . . . . . . . 105

Paper V – Strain-rate effects in a high strength dual phase steel . . . . . 125

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Part I

Theory and background

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Introduction1

Simulation based design, SBD, including finite element, FE, analysis, is one of themost important methodologies in product development, and it has already sig-nificantly reduced the need for prototypes and physical tests. As a consequence,product development time has been shortened and product quality has been im-proved.

Many products, including automotive structures, are made from sheet metalparts produced by forming operations. During such forming operations, the mate-rial is subjected to complex deformations which in general include multiple strainpath changes. Successful forming operations require a correct tool geometry. Manyproblems associated with plastic forming operations, e.g. localisation and spring-back, can to a great extent be predicted and avoided early in the tool design processby using the SBD methodology, in which the tool designer can evaluate the conse-quence of design changes and optimise the process. However, there are still somediscrepancies between the prediction and the physical responses. These depend oninaccurate material models to some extent. Therefore, the development of moreaccurate material models is of a great importance in order to further improve theSBD process such that significantly better products can be developed at a lowercost.

Demands on improved weight to strength ratio motivates the use of highstrength steel.

1.1 Motivation

There are several important mechanical issues to consider in the development ofthe forming process of high strength steel. Major issues are springback and mate-rial failure. High strength steels, HSS, generally have a lower ductility comparedto conventional steel. This increases the risk for strain localisation, and a subse-quent rapid material fracture. The occurrence of strain localisation depends onplastic hardening, strain rate sensitivity and plastic anisotropy. Despite the highyield strength in HSS, the subsequent plastic hardening is comparatively lowerand thus, localisations may occur at lower strains. Furthermore, the strain ratesensitivity is lower in high strength steel, which further reduces the resistance tostrain localisation. Springback is often considered as an elastic phenomenon whichdepends on the strength to stiffness ratio and thus increases with the strengthof the material. In addition, the geometric distortion due to springback is morepronounced in thin sheet, and a common reason for using HSS is that a sheet ofregular steel can be replaced by a thinner one of HSS. This leads to a significantlyincreased degree of distortion during springback, and therefore effort must be madeto predict this accurately early in the design process of the forming tools.

3

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CHAPTER 1. INTRODUCTION

1.2 Objective

The main objective of this work is to develop material models that accuratelydescribe physical phenomena observed during deformation. The material modelsshould have an industrial applicability for detailed analyses of the product, i.e. bothfor its forming process and for its intended function. Another objective is to providean experimental set-up which is suitable for the calibration of the material modelparameters.

1.3 Investigated steels

Three specific steel grades have been investigated in this thesis. Two of these,Docol 600DP and Docol 1200M, have been provided by SSAB and are low alloyedhigh strength steels, see Olsson et al. (2006). Docol 600DP is a dual phase, DP, highstrength steel, and is often referred to as DP600. The number in the name indicatesthat the lowest guaranteed tensile strength of the material is RM = 600 MPa.The Docol 1200M is a martensitic steel, which has a much higher yield strengthand tensile strength, i.e. RM = 1200 MPa. However, the ductility of this steelis significantly lower. The third steel is HyTensX from Outokumpu Stainless.HyTensX is an austenitic stainless steel within the AISI 301 standard. The materialis cold rolled to a desired strength. In this thesis, a variant denoted HyTens 1000,i.e. AISI 301 C1000, has been investigated. C1000 indicates a tensile strengthof at least RM = 1000 MPa. Unlike Docol 1200M, this material displays greatformability. HyTensX is meta stable, and the austenite transforms to martensiteduring deformation. This phenomenon contributes to the plastic hardening andthus also to the improved formability.

All these three steels are of great industrial interest. DP600 has become astandard high strength steel for many applications, due its high strength and goodformability. Docol 1200M is used where yield stress and strength is more importantthan ductility, e.g. in door impact beams, see Olsson et al. (2006). For even moredemanding applications, the stainless steel HyTensX is useful. The mechanicalproperties and applicability of this steel has also been demonstrated in automotiveapplications, see e.g. Schedin (2012).

1.4 This thesis

The problems regarding material modelling of high strength steel sheet are pre-sented in the first part of the thesis, along with the mechanical testing proceduresused for parameter calibration, some issues regarding FE modelling of thin sheets,and a brief description of different calibration methodologies. In the second part,five papers are appended.

4

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Material modelling2

This chapter presents several typical phenomena considered in sheet metal mate-rials, and their incorporation into material models.

2.1 Main equations

Sheet metal forming operations result in large rigid body motions and large de-formations of the material. Therefore the material models must be defined inthis context. By using a co-rotational material frame, the material anisotropycan easily be accounted for, see e.g. Hallquist (2006) and Belytschko et al. (2000).Henceforth, all subsequent constitutive relations will be related to the co-rotatedconfiguration. Since the elastic deformations are considered to be small, an addi-tive decomposition of the rate of deformation tensor can be assumed, i.e.

D = De +Dp (1)

where De and Dp are the elastic and plastic parts, respectively. Also, as a con-sequence of the small elastic deformations, the update of the corotated Cauchystress can be assumed to be hypo-elastic, see Needleman (1985), i.e.

σ = C : De = C : (D −Dp) (2)

where C is the elastic material stiffness tensor, which in this work has been con-sidered to be isotropic with Young’s modulus E and Poisson’s ratio ν. The dotover σ indicates the material time derivative.

An important part of a material model is the yield function, f ,

f = σ − σf{≤ 0 elastic= 0 plastic flow

(3)

where σ and σf denote the effective stress function and the current flow stress,respectively. If the material obeys an associated flow rule, the direction of plasticflow is proportional to the gradient of the yield function with respect to the stresstensor σ, i.e.

Dp = λ∂f

∂σ(4)

where λ denotes the plastic multiplier.The yield function determines the elastic region in the stress space, and the

limit is given by f = 0, which constitutes the so called yield surface in the stressspace. The size of the yield surface is given by the flow stress, σf , and the shapeis governed by the effective stress function, σ.

5

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CHAPTER 2. MATERIAL MODELLING

The location of the origin of the yield surface is determined by the argumentof the effective stress function. A translation of the yield surface can be obtainedby changing the argument from the stress tensor, σ, to an over-stress tensor, Σ,defined by

Σ = σ −α (5)

where α is the back-stress tensor. The evolution of the back stress tensor is givenby the kinematic hardening law, see Section 2.4.

If σ is a first order homogeneous function of the stress tensor, the followingrelation holds

Σ :∂σ

∂Σ= σ (6)

where Σ ≡ σ if no kinematic hardening is present. The definition of equivalentplastic strain rate, ˙εp, yields

σ ˙εp = Σ : Dp (7)

Combining Eqs. (4), (6) and (7) gives

σ ˙εp = Σ : Dp = Σ :

(λ∂σ

∂Σ

)= σλ ⇒ ˙εp = λ (8)

and, thus,

εp =

t∫

0

λdt (9)

where t denotes time.

2.2 Plastic strain hardening

The flow stress, σf , is typically considered to depend on equivalent plastic strain,plastic strain rate, temperature and possibly also on other variables. The hardeningassociated with σf expands the yield surface homogeneously and is referred toas isotropic hardening. In this section, the component of the flow stress whichgoverns the plastic strain hardening is considered, denoted σy(ε

p), whereas othercomponents of the flow stress governed by plastic strain rate, temperature andphase transformations are discussed in subsequent sections.

The plastic hardening function can often be evaluated directly from experi-mental data. In general, such data is evaluated from uniaxial tensile tests, whichprovide the σ to εl relation, where σ is the true stress and εl = ln(l/l0) is thelongitudinal logarithmic strain evaluated over a length l, see Section 3.1. How-ever, the stress-plastic strain data obtainable from uniaxial tensile tests is limitedby plastic instability, denoted diffuse necking. Diffuse necking is an instabilityassociated with the uniaxial stress state, and there is a need to extrapolate thestress to strain relation beyond this instability. Furthermore, the quality of ex-perimental data is sometimes too poor to be used as input to a material modeldue to oscillations caused by the measurement equipment, dynamic effects in high

6

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2.3. PLASTIC ANISOTROPY IN SHEET METALS

speed testings, or a serrated stress-strain relation caused by dynamic strain ageing,DSA. Analytical functions can be used both to extrapolate the plastic hardeningbeyond diffuse necking and to represent the plastic hardening in cases of oscillatingexperimental data. Numerous analytical functions have been proposed over theyears. The powerlaw and exponential type of functions dominate. The powerlawhardening function, introduced by Hollomon (1945), often offers an unsatisfactoryfit to experimental data. Voce (1948) proposed an exponential hardening, whichcan be extended to several components in order give a close fit to experimentaldata. An extended Voce hardening function with m components is given as

σy(εp) = σ0 +

m∑

i=1

Qi(1− exp(−Ciεp)) (10)

where σ0, Qi and Ci are material constants. The Voce hardening function wasextended by Hockett and Sherby (1975) by adding an exponent to the plasticstrain. Both the Voce and the Hockett-Sherby functions often yield a good fitto experimental data for strains before diffuse necking. However, for large plasticstrains, the exponential type of functions saturate, and is often an underestimationcompared to experimental findings, cf. Lademo et al. (2009). To overcome thisshortcoming, two or more functions can be combined according to

σy(εp) =

σ0 +

m∑

i=1

Qi(1− e−Ciεp) εp ≤ ε(t)

A+B(εp)n ε(t) ≤ εp(11)

in which the second is a powerlaw function and where A,B, n and ε(t), are addi-tional material constants. The transition strain, ε(t) may be chosen arbitrarily inorder to obtain a good fit. A suitable choice may be to use the uniaxial plasticstrain close to diffuse necking. The hardening parameters, A, B and n, in thesecond function are obtained by applying continuity requirements and an addi-tional condition that controls the subsequent plastic hardening. However, otherpossibilities exist, e.g. to use a sum of an exponential term and a powerlaw termfor all plastic strain levels, see Sung et al. (2010).

An alternative extrapolation is to use experimental data from other tests, e.g. abulge test or a shear test, see Sections 3.2 and 3.4, respectively. A bulge test hasthe advantage that physical material data easily can be evaluated directly fromthe experimental data. The plastic strain level reached in a shear test is in generalhigher than in a bulge test. However, the evaluation of material properties fromsuch experiments is not straightforward, since inverse analyses are needed, seeSection 5.1.

2.3 Plastic anisotropy in sheet metals

Cold rolled metal sheet often has different material properties in different materialdirections, e.g. the yield stress may be higher in the rolling direction, RD, com-pared to other directions. The principal axes of orthotropy coincide with the RD,the transversal direction, TD, and the normal direction, ND. Variations with re-spect to the in-plane material direction is denoted planar anisotropy. In a materialmodel, plastic anisotropy is governed by the shape of the yield surface, i.e. by the

7

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CHAPTER 2. MATERIAL MODELLING

formulation of the effective stress function, which may include anisotropy param-eters. In the case of an associated flow rule according to Eq. (4), both anisotropicyield stresses and anisotropic plastic flow are described with an anisotropic ef-fective stress function, σ. A distortion of the yield surface may be achieved byletting the anisotropy parameters vary during the deformation. In such a case, theanisotropy parameters are denoted anisotropy functions, see Section 2.4.

Strictly speaking, the yield surface is a combination of the effective stress func-tion, the back-stress tensor and the flow stress. However, effective stress functionsfound in the literature are often referred to as yield surfaces. Important propertiesof the shape of the yield surface are discussed in this section. Focus lies on planestress states, since this is a good approximation for thin sheets.

Isotropic yield surfaces

A yield surface for a stress state in three dimensions is a convex surface in sixdimensions. Isotropic effective stress functions can be defined in terms of theprincipal stresses, σ1, σ2 and σ3. One family of such isotropic functions are givenby, see Hersey (1954),

2σa = |σ1 − σ2|a + |σ2 − σ3|a + |σ3 − σ1|a (12)

where a is the yield surface exponent. If a = 1 or a → ∞ the result is Tresca’syield surface, and if a = 2 or a = 4 the result is von Mises’ yield surface. Otherchoices of exponents result in different shapes of the yield surface, although itis still isotropic. The effective stress function (12) is independent of hydrostaticstress. That is, σ(Σ) = σ(Σ + λI), where λ is any real number. The yield surfaceis often visualised as a curve in two dimensions, which is denoted the yield locus.The yield loci for σ3 = 0 and a variety of exponents a are shown in Fig. 1.

10

11 Isotropic yield loci

σ1

σ2

σf

Material Characterization

Figure 1: Isotropic yield loci at plane stress. The dotted, dashed and solid curvescorrespond to the Tresca, von Mises and Hersey (a = 8) effective stress functions,respectively.

8

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2.3. PLASTIC ANISOTROPY IN SHEET METALS

Planar anisotropy

In this section, only plane stress states are considered. A yield surface for planestress is shown in Fig. 2. The corresponding yield locus for τRT = 0 is shown inFig. 3, where some typical stress states and normal directions for the evaluation ofplastic anisotropy are shown. τRT denotes the shear stress in the RD to TD plane.

1

−1

−0.5

0

0.5

1

Uniaxial tension, σ1 > 0, σ2 = 0

Balanced biaxial stress state, σ1 = σ2

Shear, σ1 = −σ2

σRD

σTD

τRT

Figure 2: Yield surface for plane stress state.

In the case of isotropy, the stress state under uniaxial tension can be consideredas a the intersection curve between the yield surface and a plane given by σRD +σTD = σf . However, this is not the case if the yield surface is anisotropic. Suchplanar anisotropy can be evaluated e.g. by the uniaxial yield stress ratios rφ,

rφ =σφσf

(13)

where φ is the material direction with respect to the RD. A usual choice of φ-directions in order to evaluate the plastic anisotropy is φ = 00, 45◦ and 90◦, whichcorrespond to the RD, DD (diagonal direction) and TD, respectively. σφ and σfdenotes the uniaxial flow stress in the φ-direction and the reference flow stress,respectively. Accordingly, the yield stresses in pure shear and plane plastic strainare given by the parameters rτ,φ and rpd,φ, see Fig. 3.

Normal anisotropy

The relation between the width strain, εw = ln(w/w0), where w denotes the widthof the specimen, and the longitudinal strain, εl, can be provided from uniaxialtensile tests. The normal strain component, εND = ln(t/t0), where t is the sheetthickness, is generally not measured. However, it can be evaluated by assumingnegligible elastic strains and plastic incompressibility. Thus, the through-thicknessstrain component can be evaluated from

εND = −εl − εw (14)

In an isotropic material, the contraction in the directions perpendicular to thelongitudinal one are equal, i.e. εND = εw. The deviation from isotropy is evaluated

9

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CHAPTER 2. MATERIAL MODELLING

10

11 Normalised yield locus

σRD/σf

σTD/σf

1

k00

1

k90

1

kb

‖ RD

‖ TD

ut

rs

rs

b

brs

rs

(r00, 0)

(0, r90)(rb, rb)

(rpd,00, rpd,00cpd,00)

(rpd,90cpd,90, rpd,90)

(rτ,45,−rτ,45)

(−rτ,45, rτ,45)

Material Characterization

Figure 3: yield locus for τRD−TD = 0. Uniaxial, biaxial, shear and plane strainstress states are indicated in the figures.

with the Lankford parameter. The rate version of the Lankford parameter isdefined as

R = − εpwεpl + εpw

(15)

Alternatively, the total Lankford parameter is defined as, see e.g. Hance (2005),

RεR = − εpwεpl + εpw

∣∣∣∣εl=εR

(16)

The total Lankford parameter RεR-value is evaluated at one specific longitudinalstrain, εR. If this strain is large enough, possible measurement errors can beignored.

A value of R = 1 implies isotropy. A value larger than one means that duringstretching contraction in the plane of the sheet is promoted rather than acrossthe thickness, and therefore the Lankford parameter is sometimes referred to asthinning resistance. This type of anisotropy in plastic flow is henceforth referredto as normal plastic anisotropy.

In Eqs. (15) and (16), uncertainties in the measurements are accumulated,especially at small strains. Thus, the error can be large for materials in whichdiffuse necking occurs at small plastic strains. As a consequence, the normalanisotropy has here been evaluated using the so called plastic strain ratio, k,

k =εpwεpl

; R = −εpwεpl

1 + εpwεpl

= − k

1 + k(17)

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2.3. PLASTIC ANISOTROPY IN SHEET METALS

where k corresponds to the normal direction of the yield surface, see Fig. 3. Thus,εND is not needed to calibrate the anisotropy parameters. The balanced biaxialplastic strain ratio coincides with the corresponding Lankford parameter, and isdefined by

Rb = kb =dεpTDdεpRD

(18)

Biaxial stress states

In addition to be planar and normal anisotropy, the material can be more or lesssensitive to a multi-axial loading. The following three in-plane multi-axial stressstates are considered important.

Balanced biaxial stress stateThe yield stress in a balanced biaxial stress state, i.e. σ1 = σ2, can be differentto the one in uniaxial tension. The yield stress under such biaxial stress stateis related to the reference flow stress by the yield stress ratio rb, see Fig. 3,

rb =σbσf

(19)

Plane strainPlane strain denotes a deformation mode in which the sheet is stretched inone in-plane direction, l, while no plastic deformation occurs in the transver-sal (width) direction, i.e. εpw = 0. Instead, the longitudinal plastic strainrate εpl rate is balanced by through-thickness contraction, i.e. εpND = −εpl .Such deformation occurs when the in-plane normal stress components arerelated by σw = cpdσl, where cpd is the ratio between the in-plane stressesrequired to obtain plane strain, see Fig. 3. The yield stress in plastic strain ishigher than it is in uniaxial tension, σl = rpdσf , where rpd denotes the planestrain yield stress ratio. Even though the material is isotropic, the value ofrpd depends on the curvature of the yield surface, cf. Figs. 1 and 3. Theplane strain deformation mode is important since it occurs within a strainlocalisation.

In-plane shearThe yield locus in pure shear is given by the intersection curve between theyield surface and a shear plane given by σTD = −σRD, see Figs. 2 and 3.In anisotropic yield surfaces, a pure shear stress state does not always resultin a pure plastic shear deformation, since the yield surface is not necessarilysymmetric across the shear plane.

Anisotropic yield surfaces

A difference between quadratic, i.e. a = 2, and non-quadratic yield surfaces isoften made in the literature. The first anisotropic quadratic yield surface wasproposed by Hill (1948). Since then it is mostly non-quadratic yield surfaces thatcan be found in the literature. By non-quadratic means that the exponent can beassigned a value a ≥ 1. The general recommendations are a = 6 and a = 8 for BCCand FCC crystal structures, respectively, see e.g. Hosford (1993). As previously

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CHAPTER 2. MATERIAL MODELLING

discussed, the exponent does not necessarily affect the isotropy, although it doesaffect the sensitivity to multi-axial stress states, see Fig. 1.

One widely used yield surface in industrial sheet metal forming simulations isthe three parameter yield surface proposed by Barlat and Lian (1989), denotedYLD89. In contrast to Eq. (12), YLD89 accounts for plane stress states only. TheYLD89 function can fit e.g. either k-values or uniaxial yield stresses in three mate-rial directions exactly. Karafillis and Boyce (1993) used a linear transformation ofthe stress tensor to describe the plastic anisotropy. Further development along thisline has led to the eight parameter yield surface YLD2000 proposed by Barlat et al.(2003). Later, Aretz (2004) proposed another eight parameter function, denotedYLD2003. Banabic et al. (2003) extended the YLD89 surface to a six parameteryield surface, BBC2002, which was further extended to the eight parameter sur-face BBC2003 in Banabic et al. (2005). Barlat et al. (2007) showed that YLD2000,YLD2003 and BBC2003 all represent an identical yield surface. In this thesis, theYLD2003 variant has been utilised. The BBC2002 surface is able to represent boththree uniaxial yield stress ratios and the corresponding directions of plastic flow.The YLD2003, and its variants, can also represent both the biaxial yield stressand the corresponding direction of plastic flow. A comparison of the yield loci forBBC2002 and the eight parameter surface YLD2003 is shown in Fig. 4. The sameuniaxial r and k values in the rolling, diagonal and transversal directions havebeen used in the calibration of both yield surfaces, whereas the experimental biax-ial data, rb and kb, have been used in the calibration of the YLD2003, in additionto the uniaxial data. The effective stress function in YLD2003 is given by

−1 −0.5 0 0.5 1

−1

−0.5

0

0.5

1

σRD/σref

σT

D/σ

ref

6 parameter model

8 parameter model

Figure 4: Comparison of the yield loci obtained with the 6- and 8 parameter modelsfor the same DP600 steel.

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2.3. PLASTIC ANISOTROPY IN SHEET METALS

2σa(σ) = |σ′1|a + |σ′2|a + |σ′′1 − σ′′2 |a

σ′1σ′2

}=A8σ11 +A1σ22

2±√(

A2σ11 −A3σ22

2

)2

+A24σ12σ21

σ′′1σ′′2

}=σ11 + σ22

2±√(

A5σ11 −A6σ22

2

)2

+A27σ12σ21

(20)

where Ai, i = 1 . . . 8, are anisotropy parameters. Equation (20) fulfills the condi-tions σ(σRD, σTD, τRT ) = σ(−σRD,−σTD, τRT ) and σ(σRD, σTD, τRT ) =σ(σRD, σTD,−τRT ). Thus, the material is assumed to have the same yield stressin compression as in tension. Cazacu et al. (2006) proposed an eight parameteryield surface which allows for tension-compression asymmetry.

The YLD89, YLD2003 and BBC2002 functions account for plane stress statesonly. One advantage of plane stress states is that the principal stresses can beexpressed explicitly. Thus, no eigenvalue problem needs to be solved, either in theevaluation of the effective stress or in the evaluation of the yield surface gradi-ent. The normal through thickness stress component can be incorporated in theplane stress functions by replacing the in-plane stress components σRD and σTDby σRD − σND and σTD − σND, respectively. This corresponds to removing theeffect of hydrostatic stress, and the yield surface will become a cylinder along thehydrostatic axis, σRD = σTD = σND. As a consequence, the principle stresses canstill be evaluated without solving the eigenvalue problem, since one of the eigen-values is equal to σND. If a full stress state is considered, the through thicknessshear stresses are included as well, and the evaluation of the principal stress can nolonger be expressed in a closed form. The evaluation of the eigenvalues, and theirderivatives with respect to the stress components, becomes more complicated thanin the plane stress case, see Barlat et al. (2005). Barlat et al. (1991) proposed a sixparameter yield surface for full stress states. Later, Barlat et al. (2005) proposedan extension with 18 parameters, YLD2004-18P. Recently, Aretz et al. (2010) ex-tended YLD2004-18P to a 27 parameter yield surface, YLD2004-27P. From thepoint of view of model calibration, difficulties may arise in finding appropriatemechanical experiments for thin sheet metals.

Equivalent plastic strain

The equivalent plastic strain rate is defined in Eq. (7). It coincides with thelongitudinal plastic strain rate in uniaxial tension, i.e. ˙εp = εpl , and the absolutevalue of the through thickness plastic strain rate in the balanced biaxial stress state,i.e. ˙εp = −εpND, in the case of plastic isotropy and incompressibility. However,in the case of plastic anisotropy, the following relations are obtained in uniaxialtension, plane strain and the balanced biaxial stress state

Uniaxial tension: σφεplφ = σ ˙εp =

σφrφ

˙εp ⇒ dεp

rφ= dεplφ

Plane strain: σφεplφ = σ ˙εp =

σφrpdφ

˙εp ⇒ dεp

rpdφ= dεplφ

Balanced biaxial stress state: σb(εpRD + εpTD

)= σ ˙εp =

σbrb

˙εp ⇒dεp

rb= dεpTD + dεpRD = −dεpND

(21)

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CHAPTER 2. MATERIAL MODELLING

The plastic hardening rate is affected accordingly, and should be accounted for inthe calibration of the anisotropy parameters.

2.4 Anisotropic hardening

The yield surface is usually calibrated to experimental data at the onset of plasticdeformation. Even though the initial yield stress may be isotropic, the subsequentplastic hardening rate can be anisotropic. This is not accounted for by the de-scription of the initial plastic anisotropy. However, anisotropic hardening has beenconsidered to be important for formability predictions, see Aretz (2007). Kine-matic hardening is a special case of anisotropic hardening, since the yield stresschanges differently in other stress states than in the state defined by the currentloading. This fact affects the stress response at non-proportional loading. Onewell known deformation induced anisotropic effect is the Bauschinger effect, whichis the phenomenon of a lower yield stress in the case of reversed loading.

Isotropic-kinematic hardening

Kinematic hardening means a translation of the yield surface during deformation,and is achieved by the introduction of a back-stress tensor, α, see Eq. (5). Ifthe yield surface expands and translates simultaneously, the hardening is referredto as mixed isotropic-kinematic. Kinematic hardening has a crucial effect on theresponse in cyclic loading. Therefore kinematic hardening should be considerede.g. in simulations of sheet metal forming, since the material is subjected to acyclic tension-compression deformation while it is drawn across the die radius orthrough the draw beads, see e.g. Weinmann et al. (1988).

Several evolution rules for the backstress tensor have been proposed, see thereview by Chaboche (2008). Among such, one notes the rule by Frederick andArmstrong (2007), generally referred to as the Armstrong-Frederick, AF, function.It is given as

α = CX

(QX

Σ

σ−α

)˙εp (22)

where QX is the saturation value and CX governs the rate of saturation. TheAF model exhibits a hardening at monotonic loading similar to the Voce hard-ening function, see Eq. (10). In a similar manner, Eq. (22) can also be extendedwith several components. Kinematic hardening described by Eq. (22) is able todescribe the Bauschinger effect. However, it is unable to describe permanent soft-ening, a phenomenon where the yield stress at reverse loading remains significantlylower than in cases of monotonic loading. The back-stress tensor follows the stresstensor, and eventually, after monotonic loading, the back-stress tensor becomesproportional to the stress tensor, regardless of the initial value, see Fig. 5. Thesaturated back-stress tensor is obtained by setting α = 0, which gives

αsat =QXσ

Σ (23)

Geng and Wagoner (2002) addressed the issue of permanent softening by using anadditional bounding yield surface. Yoshida and Uemori (2002) considered the work

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2.4. ANISOTROPIC HARDENING

hardening stagnation effect at reverse loading, by using an additional hardeningsurface defined in the stress space.

Kinematic hardening affects the mechanical response during strain path changesas well as during cycling under proportional strain paths. Kim and Yin (1997) per-formed a three-stage deformation test where steel sheets were first pre-strained inthe RD. A second pre-straining was performed at several angles to the RD, fromwhich tensile test specimens were cut and tested in various directions. Hahmand Kim (2008) extended this work and found that the Lankford parameters didnot change in accordance with the change in yield stresses, an observation whichwas partly explained by kinematic hardening. Figure 5 shows an example of thegrowth and translation of the yield locus during a non-proportional strain path.The translation of the yield surface is described by Eq. (22). First, the material ispre-strained in the RD to εpl = 0.1, and then it is completely unloaded. Second,the material is loaded in uniaxial tension in the TD. The predicted effect of pre-straining is more pronounced at the beginning of the re-loading, and it fades outduring the subsequent deformation. Tarigopula et al. (2008) made similar exper-imental findings on a DP800 steel grade from SSAB, which was also the case inthe study in Paper 1. This motivates the use of a kinematic hardening rule of thetype given in Eq. (22).

0 0.05 0.1 0.150

200

400

600

800

Longitudin

alst

ress

σ[M

Pa]

Equivalent plastic strain εp[−]

Initial yield stress

Yield stress afterpre-straining unloading

Yield stress at reloading

Yield stress aftersubsequent straining

αασRD

σTD

initial yield locus

yield locus afterpre-straining

yield locusafterre-loading

pre-straining inthe RD

re-loadingin the TD

Figure 5: The predicted stress-strain relation and the corresponding growth andtranslation of the yield locus during pre-straining in the RD, unloading and sub-sequent reloading in the TD

Distortional hardening

The distortion of the yield surface during non-proportional loading has previouslybeen demonstrated experimentally. Ortiz and Popov (1983) reviewed a number ofexperimental findings which clearly showed that both a translation and a distor-tion of the yield surface take place during plastic deformation. Axelsson (1979)proposed a combination of a kinematic and distortional hardening. The sameapproach was later used by Ortiz and Popov (1983).

In the most general case, the shape of the yield surface may change arbitrarilydue to plastic deformation. However, a simple distortional hardening can be ob-

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CHAPTER 2. MATERIAL MODELLING

tained by allowing the parameters of the effective stress function to alter duringdeformation. Such a hardening approach is referred to as an isotropic-distortionalhardening, see Aretz (2008). Aretz (2008) showed that this type of distortionalhardening is important for predicting the anisotropy in forming processes. Thedistortion is then limited to the generality of the actual effective stress function.Plunkett et al. (2006) described the varying anisotropy by letting the anisotropyparameters of the effective stress function depend on the equivalent plastic strain.Such varying anisotropy parameters governing the plastic anisotropy are hence-forth denoted anisotropy functions. By using this approach, not only the initialplastic anisotropy, but also the subsequent anisotropic plastic hardening are rep-resented, as well as a possible change in the plastic strain ratios. The yield sur-face exponent a can change during deformation as well. An example of such anisotropic-distortional hardening is shown in Fig. 6. Aretz (2008) used a similarapproach with the eight parameter effective stress function YLD2003, in whichthe anisotropy functions depend on plastic work. The yield surface constitutes asurface with both a constant level of plastic work and with a constant equivalentplastic strain.

−1 0 1

−1

0

1

σT

D/σ

y,r

ef

σRD/σy,ref

εp = 0εp = 0.05εp = 0.1εp = 0.2εp = 0.3εp = 0.6

Figure 6: Example of evolution of the YLD2003 yield locus in the case of anisotropic-distortional hardening for HyTens 1000. The size of the yield surface isnormalised to the reference flow stress in order to elucidate the distortion.

Barlat et al. (2011) proposed a novel distortional hardening approach for de-scribing the Bauschinger effect both under cyclic loading and under non-proportionalstrain paths. Instead of altering the anisotropy parameters during loading, theyincluded an additional tensor in the effective stress function.

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2.5. DEGRADATION OF THE UNLOADING MODULUS

2.5 Degradation of the unloading modulus

In general it has been assumed that the elastic stiffness remains unaffected byplastic deformation. However, the strain increment from a loaded state to anunloaded stress state is found to be significantly larger than what is predicted bythe theory of elasticity. A detailed analysis of such tests indicates that such anunloading stress-strain relation is non-linear. A sketch of a stress-strain relationat a loading-unloading sequence is shown in Fig. 7. A tensile test is stretched upto a decided strain level, after which it is completely unloaded. This procedure isrepeated at various levels of longitudinal strains. A typical stress-strain relationfrom such a test is shown in Fig. 8. Yoshida et al. (2002) proposed a model that

0E

1

0E

1avE

1

u

up

l

Elastic

unloading

Figure 7: Sketch of a stress-strain relation during loading and unloading.

describes the decrease of the average elastic stiffness, which has become widelyused

Eav = E0 − (E0 − Esat)︸ ︷︷ ︸Edeg

[1− e−ξε

p]

(24)

where Eav = σu/∆ε denotes the degraded average elastic stiffness during unload-ing, E0 the initial elastic stiffness, Esat the saturation value of the degradation,and ξ governs the rate of degradation. The parameter Edeg governs the totaldegradation of elastic stiffness. Equation 24 can be extended in a similar way toEq. (10). In this work, Eav is denoted unloading modulus, however other notationscan be found in the literature, see Eggertsen (2011). A typical fit of Eq. (24) toexperimental data is shown in Fig. 8. The stiffness degradation of the type given inEq. (24) is a good approximation if the material is unloaded to a stress free state.This is generally not the case in the spring-back process of a formed metal sheet.Since the unloading path to a stress free state is non-linear, see Figs. 7 and 8, Eg-gertsen et al. (2011) developed a phenomenological elasto-plastic material modelin order to describe the hysteresis obtained in an unloading-reloading sequence.

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CHAPTER 2. MATERIAL MODELLING

0 0.02 0.04 0.06 0.08 0.1 0.12 0.14 0.160

200

400

600

800

Tru

est

ress

σ[M

Pa]

Logarithmic strain ε [-]0 0.02 0.04 0.06 0.08 0.1 0.12 0.14 0.16

150

160

170

180

190

200

Unlo

adin

gm

odulu

sE

av

[GPa]

stress−strain relationexperimental unloading moduliianalytical fit to unloading modulii

1

Eav

Figure 8: A fitted elastic stiffness degradation model for Docol 600DP. The un-loading modulus Eav is evaluated using the maximum stress before unloading andthe strain at zero stress.

The model is based on a two yield surfaces concept, an inner and an outer surface.A similar model was also presented by Sun and Wagoner (2011).

2.6 Strain rate sensitivity

Thermal activation leads to an increased flow stress with increasing loading rate,and thus steel usually display a positive strain rate sensitivity, SRS. However, somemetal alloys are sensitive to DSA, which affects the SRS, see Section 2.7. The SRSis lower for high strength steels, see Hosford and Cadell (1983), however, steelshows stronger strain rate dependency than aluminium, see Jie et al. (2009).

In addition to higher flow stresses at higher loading rates, such positive SRSact as a regularisation during deformation and postpones strain localisation, bothin reality and in FE analyses. Diffuse necking under uniaxial tension is relativelyindependent of the SRS, whereas the post-uniform elongation is highly affected,cf. Ghosh (1977). Therefore, a correct description of the SRS is of uttermostimportance in instability analyses. Zhang et al. (2008) incorporated SRS in anumerical instability analysis, and concluded that the onset of instability is notaffected by the strain rate itself, but on the SRS index m, which is defined by

m = lim˙εp2→ ˙εp1

ln (σf ( ˙εp2)/σf ( ˙εp1))

ln ( ˙εp2/ ˙εp1)(25)

which is the slope of the ln(σf ) to ln( ˙εp) relation. m depends on plastic strain,strain rate, temperature and possibly more variables. Thus, there is a need toevaluate the SRS index at a variety of loading conditions.

The contribution to the flow stress from the strain rate can be more or less com-plex. Two of the most commonly used assumptions are additive and multiplicative

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2.6. STRAIN RATE SENSITIVITY

contributions, i.e.

Additive σf (εp, ˙εp) = σy(εp) + σv( ˙εp) (a)

Multiplicative σf (εp, ˙εp) = σy(εp)H( ˙εp) (b)

(26)

where σv is a viscous stress and H is a multiplicative SRS function. An addi-tive contribution predicts a translation of the stress-strain relation in the stressdimension, whereas a multiplicative contribution results in diverging stress-strainrelations at different loading rates. In general, a multiplicative contribution, whichdepends on the plastic strain rate only, results in an SRS index which is indepen-dent of plastic strain. With an additive contribution, the SRS index will decreasewith the plastic strain, since the magnitude of the SRS function will decrease rel-ative to the flow stress due to plastic hardening. Such an additive contribution tothe yield stress was assumed in Paper 3, where

σv = S ln

(1 +

˙εp

εp0

)(27)

where S and εp0 are material constants.Multiplicative contributions prevaile in the literature, and several SRS func-

tions can be found. The so called powerlaw function, see e.g. Hosford (1993), isgiven by

Hp(εp) =

(˙εp

εp0

)q(28)

where εp0 and q are material parameters. The exponent, q, coincides with the SRSindex, m, see Eq. (25), and it is independent of the plastic strain rate. Severalvariants of the powerlaw function can be found in the literature, e.g. the Cowperand Symonds (1957), CS, function. Johnson and Cook (1983) proposed a mul-tiplicative flow stress function consisting of three factors, which depend on theplastic strain, plastic strain rate, and on the temperature, respectively

σf (εp, ˙εp, T ) = σy(εp)HJC( ˙εp)hJC(T ) (29)

The SRS part, HJC , is given by

HJC = 1 + C ln

(˙εp

εp0

)(30)

where C and εp0 are material parameters. Like Eq. (28), HJC will yield non-physicalvalues for very low plastic strain rates. A small modification to the HJC functionis proposed in Paper 5 in order to overcome this problem and get a closer fit to ex-perimental data. In the same paper, seven different SRS functions were calibratedto experimental uniaxial tensile test data. Although all of the investigated SRSfunctions give a close fit to the experimental data, the corresponding SRS indicesdiffer among the different functions.

The initial yield stress shows a stronger SRS than the flow stress at largerplastic strains for some steels, i.e. converging stress-strain relations at differentloading rates. In order to account for this phenomenon, Peixinho and Pinho (2007)proposed a multiplicative SRS function which depends both on the plastic strainrate and on the plastic strain itself.

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CHAPTER 2. MATERIAL MODELLING

2.7 Strain ageing

Dynamic strain ageing, DSA, denotes the interaction between mobile solute atomsand temporarily arrested dislocations during plastic deformation, cf. van den Beukeland Kocks (1982). Solute atoms diffuse to temporarily arrested dislocations andstrengthen them, cf. Fressengeas et al. (2005). In the special case of a constantplastic strain rate, the average ageing time, ta, of the arrested dislocation is as-sumed to be constant and inversely proportional to the plastic strain rate. Alonger ageing time implies a stronger resistance to dislocation glide, due to the dif-fusion of solute atoms to temporarily arrested dislocations. Since the higher plasticstrain rate implies a shorter ageing time, with an increasing plastic strain rate adecreasing contribution from DSA to the flow stress will be found. This leads to acompetition between the positive instantaneous SRS and the DSA, cf. Mesarovic(1995), and the material can display a negative steady state SRS, ∆σss, althoughthe instantaneous SRS response, ∆σi, at a strain rate change is positive. In thecase of a strain rate jump, the instantaneous stress increase, ∆σi, is followed bya transient stress regime, with a significantly lower hardening rate compared tothe reference hardening rate, see Fig. 9. The transient stress response can be ex-plained by the successive release of arrested dislocations. Altogether, the smallercontribution from DSA at the higher strain rate can lead to negative steady stateSRS, i.e. ∆σss < 0.

Tru

est

ress

σ

Equivalent plastic strain εp

˙εp(1)

Δσi

Positive instanteneous SRS

˙εp(2)

Sudden strainrate increase:˙εp(1)

< ˙εp(2)

Transientperiod

|Δσss|Negative steady state SRS

Figure 9: Stress response in the case of a jump in the equivalent plastic strain rate.

A negative SRS, leads to temporal strain localisations since the homogeneousdeformation is unstable, cf. McCormick (1988). In the special case of uniaxialtension, a negative SRS leads to a force singularity, i.e. dF = 0, and the plasticstrain rate will localise into a band. However, unlike in the case of diffuse necking,the localisation of the plastic strain rate will propagate along the tensile specimenduring deformation, see Fig. 10(a). The assumed temporal distribution of longi-tudinal strain is shown in Fig. 10(b). Whether the strain distribution outside thestrain rate localisation is homogeneous or not cannot be determined without fur-ther measurements. The repetitive birth and propagation of such bands result in a

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2.7. STRAIN AGEING

serrated stress-strain relation, also called ”jerky flow”, and a staircase like relationbetween the strain measured by the extenso-meter, εl, and the total elongation ofthe specimen, δ, see Fig. 10(c). This effect is usually referred to as the Portevin-LeChatelier, PLC, effect. It is important to note that the birth and propagationof such PLC bands are associated with the special case of a uniaxial tensile test,and do not occur in a general stress state. In sheet metal forming, however, thenegative SRS can lead to premature localisations, see Hopperstad et al. (2007).The Portevin-Le Chateliereffect has been the subject of many research studies,2

cross headdisplacement

δ

repetitive strain rate

band propagation

b b

l

extensometer

location

Temporal strain distribution

εl

Location on specimen

εl

δ

Elasticdeformation

Initial homogeneous plastic deformation

Repetitive strain rateband propagation

(a)

(b)

(c)

Material Characterization

Figure 10: Schematic sketch of the Portevin-Le Chatelier effect in the case of auniaxial tensile test. (a) Propagating plastic strain rate band, (b) the temporaldistribution of longitudinal strain over the parallel length of the specimen, and (c)the resulting obtained strain-displacement relation.

and has been identified experimentally for a variety of materials, e.g. aluminium,see Clausen et al. (2004), TWIP steel, see Zavattieri et al. (2009) and austenitic

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CHAPTER 2. MATERIAL MODELLING

stainless steel, see Meng et al. (2009). Several incorporations of the DSA effectin FE simulations have previously been made. McCormick (1988) developed amodel based on the concentration of solute atoms at pinned dislocations, hence-forth denoted the MC model, which is a function of the ageing time, ta, of suchdislocations. The evolution of the ageing time depends on the plastic strain rate,where the steady state value, ta,ss, depends on strain rate and acts as a targetvalue for ta. An instantaneous strain rate change is followed by a transient periodwhere ta changes towards its new steady state value. The model was further devel-oped by Mesarovic (1995). Zhang et al. (2001) used the MC model to investigatethe morphology of the PLC bands by FE analyses. Hopperstad et al. (2007) usedthe MC model in order to investigate the influence of the PLC effect on plasticinstability and strain localisation in an aluminium alloy. It was shown that thePLC effect reduces strain to necking under both uniaxial and biaxial stress states.This work was extended by Benallal et al. (2008), where Digital Image Correlationwas used in order to detect the PLC bands, follow their propagation, and validatethe proposed material model.

The lack of mesh convergence in FE analyses of propagating instabilities haspreviously been shown e.g. by Benallal et al. (2006) and Maziere et al. (2010).Maziere et al. used the MC model and found that the band width, and thus alsothe maximum plastic strain rate within the band, is mesh dependent, whereas theband propagation speed and the plastic strain increment carried by the band arenot. They suggested a non-local approach as a regularisation in order to overcomethis mesh dependency.

Static strain ageing

Strain ageing may take place in an unloaded state after pre-straining as well asduring plastic deformation. Like DSA, static strain ageing, SSA, is related to thepinning of dislocations, see Leslie and Keh (1962). However, it is different fromDSA since it occurs while the material is unloaded. The ageing time is prescribedin the case of SSA, whereas in the case of DSA it depends on the plastic strainrate. The increment in increased stress at yielding depends both on the level ofpre-strain as well as on the ageing time, see Kubin et al. (1992). Ballarin et al.(2009) used an additional term, ∆σ, in the plastic hardening function in order tomodel the SSA

∆σ = Ra +Qa[1− exp(−ba(εp − εp0))] (31)

where Ra, Qa and ba are material constants and εp0 is the equivalent plastic strainat unloading. In Paper 2, the dependency on the ageing time, τ , was introduced.The contribution from the SSA, denoted σSSA, was given by

σSSA = [σsat − (σsat − στ ) exp(−Cε(εp − εp0)](1− exp(−Cττ)) (32)

where τ denotes the ageing time from unloading to reloading, and Cτ governs therate of the SSA. The increase of the inital yield stress, στ , is followed by a transientstress response after which a permanent effect, σsat, remains, see Fig. 11. The rateof change during the transient period is governed by Cε.

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2.8. THERMAL EFFECTS

Tru

est

ress

σ

Longitudinal strain εL

unloading, ageingand reloading

pre-straining

permanenteffect

yield stressincrease

Figure 11: Principal effect of static strain ageing on the stress-strain relation.

2.8 Thermal effects

Plastic deformation gives rise to a heating of the material. If the deformation pro-cess is rapid, less energy can be transferred to the surroundings, and the processbecomes close to adiabatic. Thus, even if no external heat is added, the temper-ature increase can locally be significant in rapid deformation processes. The heatgeneration is usually evaluated from

T = ησ ˙εp

ρCp(33)

where ρ, η and Cp are the density, fraction of plastic work converted to heatand specific heat capacity, respectively. Among the most commonly used modelsfor thermal thermal effect on the yield stress is the Johnson and Cook (1983),JC, model. The complete JC model consists of three factors, see Eq. (29). Thetemperature dependence is governed by hJC(T ) = (1 − (T ∗)m). m is a materialconstant and T ∗ = (T − TR)/(TMELT − TR) where TR and TMELT are the roomand melting temperatures, respectively.

Other multiplicative contributions to the flow stress can be found in the lit-erature, see Sung et al. (2010), who proposed a flow stress function of the sametype as the JC model. However, in their model, the temperature was taken intoaccount in the plastic hardening function, i.e. σy = σy(ε

p, T ), in addition to thefactor corresponding the h(T ) in Eq. 29. The plastic hardening was assumed totransform from a powerlaw type of hardening to a Voce type of hardening duringa temperature increase. At small plastic strain levels the effect is thereby limited,whereas it is more pronounced at larger plastic strain, since the Voce type of func-tion saturates and the powerlaw function does not. A similar plastic hardening

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CHAPTER 2. MATERIAL MODELLING

function was proposed in Paper 5, i.e.

σy(εp, T ) = α(T )σP (εp) + (1− α(T ))σV (εp) where

α(T ) = α1 − α2(T − TR),

σP (εp) =

σ0 +

2∑

i=1

Qi(1− exp(−Ciεp)) εp < εpu

A+B(εp)n εp ≥ εuand

σV (εp) = σ0 +

2∑

i=1

Qi(1− exp(−Ciεp))

(34)

An example of the corresponding plastic hardening curves σP , σV and σy, underthe assumption of adiabatic heating according to Eq. (33), is shown in Fig. 12,

0

50

100

150

200

250

Tem

per

atu

rein

crea

seT−

T0

[K]

0 0.2 0.4 0.6 0.8 1

400

500

600

700

800

900

1000

Pla

stic

har

den

ing

σP

,σV

[MPa]

Equivalent plastic strain εp [-]

σP (εp)

σV (εp)

σy(εp, T ) (adiabatic heating)

T − T0 (adiabatic heating)

Figure 12: Stress-plastic strain relations σP and σV , corresponding to σy at α = 0and α = 1, respectively, together with the plastic hardening σy under adiabaticheating.

The temperature also affects the flow stress via possible phase transformations.

2.9 Phase transformations

The high strength and deformation hardening in austenitic stainless steels aremainly due to phase transformations during plastic deformation. Martensitictransformation can be spontaneous, stress-assisted, or strain induced, see Seethara-man (1984). The transformation depends on the temperature, and decreases withincreasing temperature. The γ-austenite, FCC, transforms to ε-martensite, HCP,and to α′-martensite, BCT, during deformation. Transformation to α′-martensitecauses a volume expansion, since the FCC structure is more close packed than theBCT-martensite. The magnitude of the volume expansion depends on the car-bon content, see Krauss (2008). Furthermore, the transformation also depends on

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2.9. PHASE TRANSFORMATIONS

strain rate, see Hecker et al. (1982), and hydrostatic pressure, see Lebedev andKosarchuk (2000).

Ramırez et al. (1992) suggested a model for martensitic transformation basedon an energy assumption, where the martensitic fraction was determined by thetemperature and plastic strain. They also presented a non-linear mixture rulebased on the strains of the two phases and their individual hardening. In a laterwork, Tsuta and Cortes (1993) reformulated this model into an incremental for-mulation to be used in plasticity applications. Further development resulted inthe Hansel et al. (1998) model, where the rate of transformation depends on thecurrent martensitic fraction, VM , and on the temperature, T ,

∂VM∂εp

= V pM

B

2A

(1− VMVM

)B+1B

eQ/T [1− tanh(C +D · T )] (35)

where A,B,C,D,Q, and p are material constants. The transformation rate doesnot explicitly depend on strain rate, but high strain rates will affect the temper-ature due to adiabatic heating, and thus also affect the transformation rate. TheHansel model was used e.g. by Schedin et al. (2004) in order to predict the marten-sitic fraction in a deep drawing operation on the austenitic stainless steel HyTensX.The plastic hardening was a function of equivalent plastic strain, temperature andmartensitic transformation, i.e.

σy = σy,γ(εp)(K1 +K2T ) + VM∆σγ⇒α′ (36)

where a constant difference in yield stress between the austenitic phase (γ) andthe martensitic phase (α′) was assumed. The plastic hardening model by Hockettand Sherby (1975) was used in order to represent σy,γ , but any analytical functioncan be used.

In Paper 2, the stress to plastic strain relation under close to isothermal con-ditions was evaluated from a uniaxial tensile test. The martensitic transformationwas predicted with the Hansel model (35). The plastic hardening in the austeniticphase was evaluated by subtracting the assumed martensite and temperature con-tributions from the stress found in the uniaxial tensile test.

Several other models can be found in the literature for martensitic transforma-tion in austenitic stainless steel. Olson and Cohen (1975) related the martensitictransformation to the formation of shear bands by a probability function. Stringfel-low et al. (1992) included the stress state in the probability function. The formationof shear bands is assumed to depend on the triaxiality parameter, temperature andstrain rate, see Tomita and Iwamoto (2001).

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Mechanical testing of sheet metal3

In this chapter mechanical material testing procedures for sheet metals are de-scribed and discussed. If the experimental data should be used to calibrate amaterial model, it is important that relevant data can be easily evaluated fromthe experiment. If not, the experiment is a component test rather than a mate-rial test. Uniaxial tensile test is the prevailing mechanical test method for mostmaterials, including sheet metals. The advantage of uniaxial tensile tests is thatphysical material data directly can be evaluated from the test data. Other types oftest, such as notched tensile tests, do not result in homogeneous stress and straindistributions. Physical material data from such tests can only be evaluated bynumerical methods, such as inverse modelling, see Section 5.1, and must there-for be considered as component tests. In fact, even uniaxial tensile tests are tobe considered as component tests for deformations beyond the limit of uniformelongation.

It is almost impossible to perform in-plane compression tests of thin sheetmetals to adequate plastic strain levels due to buckling. Thus, other types of testsin which the material is subjected to a compression must be used, e.g. a three-point bending test. Such a set-up can also be used as a cyclic tension-compressionloading test.

3.1 Uniaxial tensile tests

A schematic sketch of the uniaxial tensile test is shown in Fig. 13. Such a testprovides a uniaxial stress-strain relation, i.e. σ(εl). Usually, the longitudinal strainεl and the transversal strain εw are measured continuously during the test, fromwhich the plastic strain ratio, kφ, can be evaluated, see Eq. (17). This data is validto the limit of homogeneous plastic deformation, εu.

11

12 Prestrain geometry with measure-points

b b b b b b b

b b b b b b b

L x

Figure 1: Schematic picture of the tensile test geometry

13 SSAB Tensile Tests - fel radier!

b b

t 0, t

l0, l

w0, wF F

Figure 2: Schematic picture of the tensile test geometry

Material Characterization

Figure 13: Sketch of the uniaxial tensile tests.

Planar plastic anisotropy can be evaluated by conducting uniaxial tensile testson specimens cut in several material directions. The uniaxial yield stress ratios,rφ, are introduced in order to relate the flow stress in the φ-direction with respectto e.g. the RD.

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CHAPTER 3. MECHANICAL TESTING OF SHEET METAL

Peak strain rates in forming applications are normally in the order of 10/s,cf. Kim et al. (2011). These strain rates might be achieved in a servo-hydraulictensile test machine. In a car crash, peak strain rates in the order of 1000/smay develop, cf. Thompson et al. (2006). Material testing at these strain rates isdominated by the split-Hopkinson bar method, see e.g. Lindholm (1964).

Diffuse necking

Diffuse necking occurs when the softening caused by the decrease of cross sectionalarea no longer is balanced by strain hardening, i.e.

d(σwt)

σwt=

σ+

dw

w+

dt

t=

σ+ dεw + dεND = 0 (37)

For steels, plastic incompressibility is generally assumed, and the volume changedue to elastic deformations is assumed to be negligible. Thus, in this context therelative volume change is ignored, i.e. lwt = l0w0t0. Using the definition of thelogarithmic strains in Eq. (37) one finds the Considere condition

dεl= σ (38)

from which the limit of uniform elongation, εu, can be solved. The condition (38)is independent of normal plastic anisotropy.

Post-uniform deformation

The geometry of the test specimen and the length of the extenso-meter do nothave an influence on strain measures as long as the stress is uniaxial and the straindistribution is uniform. The deformation mainly takes place at the location ofthe neck, which has approximately the same length in the longitudinal directionas the width of the specimen. Thus, the strain measured by the extenso-meterduring the post-uniform deformation depends on the measure length l0. A shortmeasure length will result in a larger strain since a larger part of the measurelength is located within the neck. Furthermore, if diffuse necking takes placeoutside the measure length, the extenso-meter will exhibit a negative strain dueto elastic unloading. The strain distribution during the post-uniform deformationis complex and the stress is no longer uniaxial. Eventually, a strain localisation,denoted localised necking, occurs within the neck, followed by material rupture.Figure 14 shows a specimen which is aborted close to rupture.

Strain rate jump test

The most common method for evaluating the strain rate effects is to conduct mono-tonic tests at different loading rates. However, some researchers have promotedso called strain rate jump tests. Both negative and positive strain rate jump testscan be conducted. Figure 15 shows the stress-strain relations obtained from threesuch strain rate jumps in Docol 600DP at ε∗ = 0.02, 0.06 and 0.1. The cross headvelocity was rapidly increased from 3 mm/min to 300 mm/min. A strain rate jumpis followed by an instantaneous stress response. The instantaneous response willbe followed by a transient stress response if the material is sensitive to DSA, seeFig. 9. Thus, such a test can be used to evaluate both the instantaneous and the

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3.1. UNIAXIAL TENSILE TESTS

(a)

(b)

Figure 14: (a) A uniaxial tensile test unloaded close to rupture and (b) a detailedview of the localisation.

steady state SRS. Furthermore, strain rate jump tests are less sensitive to specimenvariation, since the flow stress at the different strain rates are compared to eachother using the same specimen. Although the flow stress may differ from specimento specimen, the SRS is believed to display a smaller dispersion, as demonstratedin Paper 5. However, this is not the case if several specimens are subjected toindividual loading rates. In such a case, it is recommended that several tests ateach loading rate are conducted, in order to evaluate a mean value and possibledispersion of the flow stress.

0 0.02 0.04 0.06 0.08 0.1 0.12 0.14

400

500

600

700

800

Tru

est

ress

σ[M

Pa]

Logarithmic strain εl [-]

Figure 15: Stress-strain relations obtained from strain rate jump tests on Docol600DP. The loading rate was rapidly increased by a factor of 100 at ε∗ = 0.02(dash-dotted line), at ε∗ = 0.06 (solid line) and at ε∗ = 0.1 (dashed line).

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CHAPTER 3. MECHANICAL TESTING OF SHEET METAL

Loading-unloading tests

Cyclic loading-unloading tests, using uniaxial tensile test specimens, give infor-mation concerning the strain increments during unloading, see Section 2.5. Inaddition, other effects can also be analysed, e.g. the sensitivity to SSA. Typicalexperimental results from such ageing tests on HyTens 1000 are shown in Fig. 16.As seen, the ageing time strongly affects the initial yield stress at the second load-ing.

0 0.02 0.04 0.06 0.08 0.1 0.120

200

400

600

800

1000

1200

Longitudinal strain εL [-]

Tru

est

ress

σ[M

Pa]

0 days3 days11 days56 days

0.09 0.1 0.11

1050

1100

1150

1200

Figure 16: Experimental results from ageing tests on HyTens 1000.

3.2 Biaxial testing

Material testing at arbitrary in-plane stress states can generally not be achieved ina standard uniaxial tensile test machinery. Biaxial test equipment for use in suchone dimensional test machines has been developed by e.g. Ferron and Makinde(1988). This type of test can also be performed in order to evaluate anisotropy,since a great variety of deformations can be applied, see e.g. Kuwabara et al.(1998). A drawback may be that the geometry of the cruciform specimen is ofgreat importance in order to obtain homogeneous strain distributions.

Bulge test

A balanced biaxial stress state can be achieved in a so-called viscous bulge test.The blank is clamped between a die and a blank-holder at its periphery, andsubjected to a pressurised fluid. Such loading will lead to a bulge on the sheet.In addition to the pressure p, the in-plane strains, εRD and εTD, and the radiusat the top of the bulge, R, are also measured during the test using Digital Image

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3.3. NOTCHED TENSILE TESTS

Correlation, DIC. The biaxial stress can be evaluated from

σb =pR

2t(39)

where t is the sheet thickness, which is evaluated by assuming a close to isochoricdeformation, i.e.

t = t0 exp(εND) ≈ t0 exp(−εRD − εTD) (40)

In addition to the biaxial stress to thickness strain relation, a relation between thein-plane strain components, εRD and εTD, is provided. A punch made of relativelysoft silicone can be used instead of a fluid to facilitate the testing, cf. Sigvant et al.(2009). The sheet is then loaded with a close to homogeneous pressure. A sketch ofsuch a test set-up is shown in Fig. 17. A drawback with the bulge test, compared

4

5 Bulge test

Punch

Sheet

Blankholder

Die

Material Characterization

Figure 17: A bulge test set-up. The dashed line is the axis of axi-symmetry.

to an in-plane biaxial test, is the problem that can occur when measuring thesheet radius at small curvatures. Furthermore, the sheet is initially subjected tobending, which results in an inhomogeneous strain and stress distribution throughthe thickness. However, the latter effect decreases as the bulge grows larger and aclose to membrane state is achieved.

3.3 Notched tensile tests

A variety of notched tensile tests can be found in the literature. Many of thesetests are referred to as plane strain tensile tests, see Kuwabara (2007).

In general, the material in the centre of the notched part will be subjectedto deformations close to plane strain, whereas the stress state close to the notchboundary will be close to uniaxial tensile stress. Thus, the evaluation of test datais not straight-forward as in the case of a uniaxial tensile test. In the notchedtensile test, inverse modelling of the test process is required.

The geometries of three such notched tensile test specimens are shown inFig. 18. The geometry in Fig. 18(a) is similar to the one used by e.g. Gryttenet al. (2008), however its dimensions have been uniformly scaled. The other twogeometries presented in Fig. 18 have been developed within this work. The geome-tries in Figs. 18(a) and (b) are designed to achieve plane strain deformation. Thespecimens can be clamped close to the center in order to achieve a plane straindeformation path. Efforts must be made to achieve a rigid clamping, and someresearchers have used bolts in addition to the clamping, see e.g. Suh et al. (1996).

If a small notch radius is used, the localisation and the subsequent crack tendto start from the notch, while if the notch radius is larger, the localisation will start

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CHAPTER 3. MECHANICAL TESTING OF SHEET METAL

from the center. The localisations in specimens made from Docol 600DP with thegeometries presented in Figs. 18(a), (b), and (c) are shown in Figs. 19(a), (b),and (c), respectively. Note that the same specimen geometries may fail in otherfailure modes for other steel grades. If strain localisations are under investigation,a localisation in the middle of the material is preferable, since the roughness of theedge can affect the localisation.

The specimen shown in Fig. 18(c) was primarily designed to obtain a highstrain rate within the notched area, see Paper 5. Instead of being rigidly clampedthis specimen should be mounted with clevis pins far from the center. Thus, theinfluence from the mounting on the deformation behaviour is minimised, whichfact simplifies the FE analysis of the test. Moreoever, efforts were made in orderto avoid a global instability prior to the localised necking.

An et al. (2004) used plane strain tests in order to evaluate plastic hardeningat large strains. Aretz et al. (2007) proposed a method to calibrate the anisotropyparameters in the YLD2003 effective stress function. Instead of using experimentaldata from a bulge test, they used notched tensile tests in the rolling and transversaldirections.

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3.3. NOTCHED TENSILE TESTS

(a)

(b)

(c)

Figure 18: Three specimen geometries of notched tensile tests. [mm]

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CHAPTER 3. MECHANICAL TESTING OF SHEET METAL

(a)

(b)

(c)

Figure 19: Localisations in Docol 600DP, starting from (a,c) the center and (b)from the notch.

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3.4. SHEAR TESTS

3.4 Shear tests

A pure in-plane shear deformation can be described by εRD + εTD = 0. Thus, thecross sectional area in such a test does not decrease as in a uniaxial or notchedtensile test. The absence of geometric softening due to decreasing cross sectionalarea leads to a higher resistance to plastic instability, and large plastic strainlevels can be achieved before failure. A variety of shear test specimen geometriescan be found in the literature, see e.g. Lademo et al. (2009) and Tarigopula et al.(2008). Carbonniere et al. (2009) used a cyclic shear test to evaluate the kinematichardening.

In this work, the specimen geometry shown in Fig. 20 has been used and it issimilar to that one used by Tarigopula et al. (2008). This geometry is designedfor use in a regular tensile testing machinery. The specimen is mounted withclevis pins through the holes, in the same way as the notched tensile test specimenpresented in Fig. 18(c). The clevis pins are lubricated in order to minimise frictionand permit possible rotations. The force, F , and the displacement, δ, at theclevis pins are continuously recorded during the tests. For small displacements,the deformation in the shear zone is close to pure shear. However, the shear zonerotates during deformation, and the deformation gradually turns towards tensionas the specimen deforms. Very large strain gradients are obtained at the notches inthe shear zone and, eventually, thinning close to the notch radius leads to materialrupture, see Fig. 21.

Figure 20: Geometry of the shear test specimen. [mm]

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CHAPTER 3. MECHANICAL TESTING OF SHEET METAL

Figure 21: Picture of the shear zone close to failure.

3.5 Cyclic bending tests

One way to achieve in-plane compression in thin sheets is to use bending tests,where the material can be subjected to cyclic loads, which is useful for evaluatingkinematic hardening. Weinmann et al. (1988) developed a test apparatus in whichthe specimen is subjected to pure bending. They found that the strains at thetension and compression sides were to some extent equal. Yoshida et al. (1998)developed another pure bending test machine where the sheets were subjected tocyclic loading. The moment to curvature relations were used in order to evaluatethe kinematic hardening coefficients. Omerspahic et al. (2006) used a three-pointbending to subject the sheet to cyclic bending deformation. However, with sucha test equipment only very limited levels of plastic strain can be achieved, unlikethe levels obtained using the test equipments proposed by Weinmann et al. (1988)and Yoshida et al. (1998). Also, the plastic strain is concentrated to the mid ofthe strip. Finite element simulations were used in Paper 3 in order to evaluate thekinematic hardening parameters in the AF model, see (22). The test apparatusshown in Fig. 22 was used, and is similar to the one used by Omerspahic et al.(2006).

3.6 Two stage testing

Tensile, plane strain, shear and bulge tests all result in rather linear strain paths,however, this is generally not the case in sheet metal forming processes. Thus,there is a need to evaluate the material behaviour under such loading conditions.Non-linear strain paths can be obtained in a number of ways, e.g. by utilising ageneral biaxial testing machine. Another approach is to strain a large sheet underuniaxial tension, and then cut small test specimens out of it. A large variety ofnon-linear strain paths can be achieved in this way. In Paper 1, large specimens

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3.6. TWO STAGE TESTING

(a) (b)

Figure 22: Bending test apparatus: (a) 3D view of the set-up. (b) Sketch of thebending behaviour. The upper and lower figures in (b) show the undeformed stateand a deformed state. The displacement of the mid support was controlled in thetest machine.

as shown in Fig. 23(a) were pre-strained under uniaxial tension both in the RDand in the TD. Uniaxial tensile and shear test specimens were cut out in differentdirections after pre-straining, see Fig. 23(b). Plastic deformation during the pre-

(a)

(b)

Figure 23: (a) Geometry of the pre-strain specimen. (b) Sketch including examplesof cut out specimens. [mm]

straining tends to increase the overall yield stress of the material and the plasticanisotropy can become larger than in the virgin material. Figure 24(a) shows

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CHAPTER 3. MECHANICAL TESTING OF SHEET METAL

stress-strain relations in the RD, DD and TD, both of a virgin material and of apre-strained material. Figure 24(b) shows the corresponding εw to εl relations inthe DD and in the TD. The initial normal anisotropy as well as the initial planaranisotropy is changed during deformation. However, after a transient period inthe beginning of the re-loading, the plastic anisotropy is similar to the anisotropyof the virgin material.

0 0.05 0.1 0.15350

400

450

500

550

600

650

700

750

800

Tru

est

ress

σ[M

Pa]

Logarithmic strain εl [-]

RDDDTDVirginPre-strained in the RD,εp

RD = 0.05

0 0.05 0.1 0.15−0.07

−0.06

−0.05

−0.04

−0.03

−0.02

−0.01

0

Wid

thst

rain

ε w[-]

Longitudinal strain εl [-]

(a) (b)

Figure 24: Uniaxial tensile test results in various material directions from a virgin(solid lines) or pre-strained material (dashed lines). Stress-strain relations areshown in (a) and the εw to εl relations are shown in (b).

3.7 Dispersion of material properties

In several studies, e.g. Chen and Koc (2007), Del Prete et al. (2010) and Aspenberget al. (2011), the assumed flow stress variation is described by a simple scaling ofthe flow stress. Alternatively, model parameters in the hardening description,e.g powerlaw parameters, have been varied individually without accounting forpossible parameter correlations, e.g. Ledoux et al. (2007), Jansson et al. (2008),and Marretta and Di Lorenzo (2010). Presumably, these approximations are toorough for many applications. Thus, an investigation of the true characteristics ofthe variations of material parameters is of major interest.

Fyllingen et al. (2009) performed detailed measurements of geometric imperfec-tions, the spatial thickness variations and the spatial material property variationsin five high-strength steel batches. The objective was to investigate if the bucklingbehaviour of dynamically axially crushed top-hat profiles was related to the mea-sured variations in these steels. As a part of their study, the linear correlationsamong parameters from the engineering stress-strain curves from uniaxial tensiletests were studied. A strong linear correlation was found between the stress at

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3.7. DISPERSION OF MATERIAL PROPERTIES

0.2% plastic strain, Rp02, the ultimate stress, Rm, its corresponding strain, eu,and the ultimate strain at rupture, A80. However, the study did not indicate howthe variations and correlations observed should be interpreted as material modelparameters.

In Paper 3 extensive mechanical testing was conducted on 13 material batchesof Docol 600DP. A material model was calibrated to each of the experimentaldata sets, resulting in 13 individual parameter sets. Strong correlations among thephysical properties and the parameter values for the material model were found. Asa result, approximate linear relations between several material model parameterscould be identified with a certain degree of statistical confidence. For example, thesaturation value of the kinematic hardening, i.e. QX in Eq. 22, was found to becorrelated to Rp02. With this correlation, a good guess of the value for QX can bemade based on uniaxial tensile test data only, i.e. the cyclic bending test can beomitted from the calibration procedure of a new batch.

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Finite Element modelling4

Shell elements have traditionally been used for modelling thin sheets. This typeof elements are computationally cheaper than continuum elements, i.e. solid ele-ments, see Belytschko et al. (2000). The reason is that several through-thicknessintegration points can be used in shell elements, which would correspond to severalsolid elements through the thickness. Moreover, with an explicit FE methodologythe critical time step is related to the element length. Thus, several solid elementsacross the sheet thickness would result in a short maximum time step. Further-more, a large number of solid elements within the plane of the sheet would berequired in order to avoid poor aspect ratios.

A drawback with plane stress shell elements is that no constraint can be appliedto the thickness variation. This implies that the thickness in one shell element isindependent from the thickness in the neighbouring elements. Thus, the thicknesscan vary stepwise in a shell model, see Fig. 25(a), which can result in a non-physicalthickness variation, and to an inability to account for some 3D-effects. Plane stressshell theory works well when the elements are larger than the shell thickness, theout-of-plane curvature is small, and possible 3D effects are negligible. However, inthe context of strain localisation, small elements are needed to resolve the strainand stress distribution. Furthermore, 3D effects in the sheet will postpone strainlocalisations. Thus, it is necessary to regularise the thickness in an FE shell model.One way to do this is to include the through thickness normal stress componentin the material model. Without the plane stress assumption, constraints can beapplied to the element thickness, and continuous thickness across the elementboundaries can be obtained, see Fig. 25(b). Because the anisotropic effective stressfunctions are mostly formulated for plane stress states only, the through thicknessstress component is included by replacing the in-plane normal stress componentsaccording to σ′RD = σRD−σND and σ′TD = σTD−σND. This modification removesthe dependence of hydrostatic stress, see Section 2.3. Shell elements with through-thickness stretch for use with this type of semi-plane stress effective stress functionsare available in LS-DYNA, see Hallquist (2007). The stress update in a hypo-elasticcontext follows the elastic predictor and elasto-plastic corrector methodology, seeOrtiz and Simo (1986). The predictor stress is evaluated according to

σtrialn+1 = σn + C : D∆t (41)

where n denotes the current integration cycle and ∆t is the time step. In the caseof shell elements, the through thickness shear stresses are updated elastically witha scale factor κ. The recommended value is κ = 5/6 for isotropic materials inLS-DYNA. At the end of the time step, the stress state is approximately given by

σtrialn+1 = σn + C :

(D∆t−∆εpn+1

∂σ

∂σ

)(42)

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CHAPTER 4. FINITE ELEMENT MODELLING

(a) (b)

Figure 25: Thickness distribution in shell element meshes. The center line consti-tutes the center of the element in the normal direction. (a) Plane stress elementswithout any thickness coupling in-between adjacent elements and (b) shell elementswith a through thickness stress component.

If the through thickness shear components are included in the effective stressfunction, σ, all stress components are updated elasto-plastically. However, if thethrough thickness shear components are excluded from σ, these shear componentswill not be further updated during the iteration back to the yield surface, andthus, the trial values will remain. This leads to a non-physical magnitude forthese stress components. This works well when it is used for out of plane shearingof shell elements. However, in the current implementation in LS-DYNA, thesethrough thickness shear components affect the geometric constraints on the thick-ness coupling between elements as well. Thus, the κ-value has an impact on theregularisation.

A positive SRS included in the FE model actually works as a regularisation oflocalised straining, see Needleman (1988). The importance of the SRS is shownin Paper 5. Notched tensile tests were simulated both with and without the SRSincluded. Despite the fact that solid continuum elements were used, the thicknessvariation within the strain localisation was dependent on whether the SRS wastaken into account or not.

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Calibration procedures5

The calibration procedures have in general been formulated as optimisation prob-lems, where the mean square difference between the numerical predictions, F , andthe experimental data, F , has been minimised by using an optimisation procedure.The standard formulation of such a minimisation problem yields

find xi

minimise e =

m∑

j=1

(Fj(xi)− Fj)2

subject to xi ∈ Xi for all i

(43)

where Xi denotes the feasible ranges for the sought variables xi, and m denotesthe number of quantities considered in the problem.

In some cases, the numerical prediction can be evaluated at a very low com-putational cost. One example is the calibration of the extended Voce hardeningparameters, see Eq. (10). In such a case, both the evaluation of the function value,F , and the optimisation procedure have been conducted in MATLAB, see MAT-LAB (2007). However, other calibrations require FE simulations and, thus, alsosome computational effort. In such optimisation problems, a so called meta modeloptimisation procedure has been utilised, see Stander et al. (2009).

5.1 Inverse analysis

In this section, an example of an optimisation procedure based on inverse anal-ysis is presented. In Papers 1 and 3, an optimisation procedure was developedin order to find the value of the yield surface exponent, a, and the flow stress atεp = 100%, denoted σ100 = A+B, see Eq. (11). This optimisation was built up byone outer major optimisation loop with two variables, where the objective func-tion, es, was the mean square deviation between the numerical and experimentalforce-displacement relations obtained from shear test simulations and experiments,respectively. However, two inner optimisation problems were required in order toobtain the complete set of material model parameters. A sketch of the optimisationprocedure is shown in Fig. 26.

Firstly, the plastic hardening function was given by Eq. 11. The extendedVoce parameters were assumed to be known, whereas the values of A, B and nwere determined from the continuity requirement of the plastic hardening and thatA+B = σ100. In Paper 1, this latter optimisation was conducted internally using∗MAT 135 in the LS-DYNA software, and by using a MATLAB routine in Paper3.

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CHAPTER 5. CALIBRATION PROCEDURES

Secondly, if the yield surface exponent, a, is changed, so are the anisotropyparameters, Ai, i = 1...8, see Eqs. (20). Thus, for each value of a, a new set ofanisotropy parameters must be found. The set of experimental plastic anisotropyvalues, i.e. r00, r45, r90, rb, k00, k45, k90 and kb, was evaluated prior to this optimi-sation, and worked as target values in the optimisation of Ai. The sub-optimisationproblem to find the anisotropy parameters was solved in MATLAB.

Yes

No

Solution

Evaluate deviation

Run simulations

Create in-data file

Find Ai

Create hardeningcurve

Set up problem

Convergence

Find A, B and n

Create new DOE

a 100

b

b

kkkkrrrr,,,

,,,,

904500

904500

)(22110 ,,,,, tCQCQ

Figure 26: Graphical representation of the optimisation procedure used to find thevalues of σ100 and a in Papers 1 and 3.

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5.2. TRIAL AND ERROR PROCEDURE

5.2 Trial and error procedure

Not all calibration procedures can be formulated as well-posed mathematical min-imisation problems. In Paper 2, all parameters but one governing the DSA inthe material model were found from a minimisation problem of the same type asEq. (43). The parameters identified were used to describe the variation of the flowstress with respect to the plastic strain rate. However, the last parameter valuecould not be identified, either from this type of minimisation problem, or from aregular inverse modelling procedure. The sensitivity to DSA leads to repetitivepropagation of strain rate bands along the specimen in a uniaxial tensile test, seeFig. 10. The birth and propagation of such bands are somewhat random, and theonly experimental data available the for evaluation of these bands was the εl to δrelations, see Fig. 10(c). In order to evaluate this last parameter, several valueswere used in an FE simulation of the tensile test. The corresponding relation wasevaluated from the FE simulation, and compared to the experimental relation.The value giving the same characteristic behaviour was considered to be the bestone. The final result is shown in Fig. 27.

0 5 10 15 20 250

0.05

0.1

0.15

0.2

0.25

0.3

Lon

gitu

din

alst

rain

ε L[-]

Crosshead displacement δ [mm]

Numerical, Le = 0.25 mmExperimental

Figure 27: Experimental and numerical εl to δ relations from a uniaxial tensiletest on HyTens 1000.

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Future work6

In this thesis several mechanical phenomena occurring in high strength steel sheetshave been investigated and reported. Much effort has been put on modelling ofplastic anisotropy and plastic hardening and new insight has been gained on somephenomena. Further understanding of the mechanics can be gained from micro-and meso-mechanical modelling, and such studies are proposed for further work.It is also important to transfer these results to macro-mechanical models, for usein industrial applications.

Prediction of failure in high strength steel is an important issue, and is alsothe main subject in one part of the ProViking SLSS research project.

Although the materials studied in this work just display a small anisotropyduring deformation, the failure of these materials may exhibit anisotropic effects.A future study of these effects is recommended. In order to predict failure accu-rately, a major issue is the strain rate effects. The nature and onset of materialfailure depend to a large extent on the loading rate, and the loading rates in manyengineering applications, e.g. in car crashes, are significantly higher than the strainrates studied in this work. High strain rates also cause a temperature increase dueto adiabatic heating. Thus, there is a need to improve the understanding of thethermo-mechanics in the materials under high strain rates as well as increasedtemperature.

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Review of appended papers7

Paper I

A study of high strength steels undergoing non-linear strain paths - experi-ments and modelling.

This paper concerns two advanced high strength steels, Docol 600DP and Docol1200M. Plastic anisotropy and its evolution during deformation was experimentallyinvestigated. A material model, which accounts for the observed behaviours, wassubsequently developed.

In addition to tests on virgin materials, tensile and shear tests were performedon pre-strained materials. The resulting deformation induced plastic anisotropywas evaluated and modelled with a mixed isotropic-kinematic hardening functioncombined with a high exponent yield surface. The anisotropy found from theshear tests was well predicted by the anisotropy evaluated from tensile tests anda bulge test. It was concluded that an isotropic-kinematic hardening is necessaryfor accurate hardening predictions in the case of non-linear strain paths.

Paper II

On the modelling of strain ageing in a metastable austenitic stainless steel.

The mechanical behaviour of the austenitic stainless steel HyTens 1000 was inves-tigated. Three tensile tests, three plane strain tests and a bulge test were used inorder to evaluate the plastic anisotropy and hardening. A significantly differentplastic hardening in the rolling direction compared to the transversal directionwas found. A model with a combination of a high yield surface exponent andan isotropic-distortional hardening assumption was successfully used in order torepresent the anisotropic plastic hardening.

Additionally, two series of experiments were conducted in order to evaluatethe sensitivity of the steel both to dynamic and to static strain ageing. Dynamicstrain ageing was evaluated by conducting so-called jump tests, from which boththe instantaneous and the steady state strain rate sensitivities were evaluated. Thedynamic strain ageing was accounted for in the material model by introducingadditional terms in the yield function. The prediction of mechanical behaviour inthe tensile tests agreed well with the experimental results.

Static strain ageing was evaluated by pre-straining a series of tensile tests,which were aged at room temperature. The yield stress after pre-straining andageing was found to depend on the ageing time, whereas the over-stress effectpartly vanishes during the recurring deformation. A term was added to the plasticstrain hardening function in order to account for this phenomenon. This function

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CHAPTER 7. REVIEW OF APPENDED PAPERS

made it possible to predict the main characteristics of the static strain ageingphenomenon.

Paper III

An evaluation of the statistics of steel material model parameters.

Variations in material properties are often described by a simple non-physicalscaling of the stress-strain relation or of the parameters included in the plastichardening function. This method can be too rough, and no physical coupling be-tween the material model parameters are taken into account. In this third paper,material from 13 different material batches of DP600 was analysed. Extensive me-chanical testings were conducted on each material batch, providing equally manyexperimental data sets. A material model was calibrated to each one of the sets.The result was consequently 13 different sets of material model parameters. Thecorrelations between both physical properties, such as thickness and yield stress,and the material model parameters obtained were studied. Several strong linearcorrelations were found. As a result, some model parameters can be approximatedfrom others and, thus, some identification tests may be excluded for this steel.

Paper IV

On isotropic-distortional hardening.

Isotropic hardening provides a plastic hardening which is similar in all directions.By letting the anisotropy parameters depend on plastic strain, a distortion of theyield surface is obtained during deformation. If the anisotropy functions dependon the equivalent plastic strain only, the distortion will be the same regardless ofstress state. This type of hardening is denoted isotropic-distortional hardening.Such hardening allows for arbitrary plastic hardening in several directions. Thenumber of directions depends on the formulation of the effective stress function.In this work, the 8 parameter effective stress function YLD2003 was utilised. Thisspecific function allows for an individual yield stress, and thus individual plastichardening, in three uniaxial tensile stress states and in the balanced biaxial stressstate. A novel methodology was presented in order to evaluate the variation of theplastic anisotropy with respect to the equivalent plastic strain. Furthermore, twopossible solutions were found in the calibration of the anisotropy functions. Bothsolutions represented the correct plastic anisotropy in all stress states included inthe calibration procedure. However, these two solutions predicted different plasticanisotropy in other stress states. By using additional experiments, one of the twosolutions could be rejected.

Paper V

Strain rate effects in a high strength steel.

A positive strain rate sensitivity postpones strain localisation, and gives a higherflow stress at elevated plastic strain rates. A number of issues associated withstrain rate sensitivity were addressed, e.g. the variation of the strain rate sensitivity

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index with respect to plastic strain rate. An experimental testing program onDocol 600DP was carried out, including uniaxial and notched tensile tests, andshear tests at various loading rates. Uniaxial strain rate jump tests in additionto monotonic uniaxial tensile tests were also conducted. It was concluded that amultiplicative contribution to the flow stress was a good approximation. Severalsuch strain rate sensitivity functions were calibrated to the experimental data, andthe one giving the closest fit was chosen for subsequent FE simulations. Severalimportant conclusions were drawn. The strain rate sensitivity index increases inthe range of strain rates of the study, implying a stronger resistance to strainlocalisation at higher strain rates compared to lower strain rates. It was shownthat the scaling of the stress-strain relation is insufficient to account for the effectof plastic strain rate. Furthermore, it was concluded that adiabatic heating at highstrain rates may affect the plastic hardening of the material, which in turn affectsthe total elongation at material rupture e.g. in shear tests.

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