mechanical behaviour of silica filled silicon rubber: an optical two-dimensional extensometer...

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Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS) Engineering Materials Center (CMGD) Ales School of Mines (EMA) M. Giton, P. Ienny, R. Piques

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Page 1: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

Mechanical Behaviour of silica filled Silicon Rubber:

an Optical two-dimensional Extensometer Application

Mechanics of Materials and Structures Lab (2MS) Engineering Materials Center (CMGD)Ales School of Mines (EMA)

M. Giton, P. Ienny, R. Piques

Page 2: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 2

Introduction

Tear Strength: Common Approach Principle: analytical model in Fracture Mechanics Drawback:

– no realistic approximation of the behaviour– dependency of the tear strength on

• specimen geometry• loading conditions (type of the test)

Local Approach Principle: stress concentration analysis

– Mechanical behavior of the material– Simulated test by FEA

ds

dfy

x

Page 3: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 3

Experiment Optimization processus

FiniteElementAnalysis

Load and Digitalkinematic field

constitutive law

Boundary Conditions

Mesh

Optimization Procedure

Experimental Datas

Digital Image Correlation

Image Analysis

Experimental Results

FEABC

ED

DIC

IA

ER

M

E(t)

F(t)

Page 4: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 4

Digital Image Correlation

F(t)

u(t)

Experimental setup

FEABC

ED

DIC

IA

ER

M

Image sequence

Page 5: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 5

Digital Image Correlation

Principle of the method

two-dimensional displacement measurements

t,XU i

mes

t,i

FEABC

ED

DIC

IA

ER

M

mes

tiF

,

Linear fit of displacement field

tIFFLi

Tmes

ti,

,

In-plane tensor of strain

Page 6: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 6

Digital Image Correlation

Image 2

X1

Y1

Y

XX2

Y2

P1 (x1 ; y1)

M1

M2

P2 (x2 ; y2)

Image 1

Processing method

FEABC

ED

DIC

IA

ER

M

•Elastomers: large strain

•Tear Study: local phenomena

Page 7: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 7

Digital Image Correlation

Image 2

X1

Y1

Y

XX2

Y2

[F]-1

P1 (x1 ; y1)

M1

M2

P2 (x2 ; y2)

Image 1

221

11 PMFPM

Improvement of the processing method

FEABC

ED

DIC

IA

ER

M

Page 8: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 8

Digital Image Correlation

New correlation functions

u

u

u

uPuPP

uFMuFMM

uPuFMPM

2Im2Im

1Im1Im

2Im1Im,

Where

2Im

111Im

12Im,1Im

PM

PMPMTc

2Im1Im

2Im,1Im ,,

Iterative fine search method:•lower number of intermediate images•better localisation measurement

u:Pattern of M

FEABC

ED

DIC

IA

ER

M

Page 9: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 9

Experimental Tests

V

UCUT

BT

B.C.

Homogeneous tests

FEABC

ED

DIC

IA

ER

M

Page 10: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 10

Experimental Tests

Exemple of experimental results in UT

FEABC

ED

DIC

IA

ER

M

0

1

2

3

4

5

6

7

-0.5 1.5 3.5 5.5

Experimental Strains

Nom

inal

Str

ess

(MPa

)

Exx

Exy

Eyy

Page 11: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 11

Experimental Tests

Non-homogeneous tests

L R

a

L

geometry

b

Alignment defaults

FEABC

ED

DIC

IA

ER

M

Page 12: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 12

Experimental Tests

Non-homogeneous tests

FEABC

ED

DIC

IA

ER

M

Realistic mesh

Realistic BC

Page 13: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 13

Experimental Tests

Non-homogeneous tests

FEABC

ED

DIC

IA

ER

M

Transverse profiles : axial stretch ratio

evolution

Page 14: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 14

Phenomenological modelFEA

BC

ED

DIC

IA

ER

M

4

8

2

4

14

Page 15: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 15

Experimental Study Numerical Study

EXPERI

MENT

Testing

Images

Collection

FiniteElementAnalysis

Load and Digitalkinematic field

viscous hyper-elastic law’sparametrersBoundary

Conditions

Mesh

Optimization Procedure

FiniteElementAnalysis

Load and Digitalkinematic field

constitutive law

Boundary Conditions

Mesh

Experimental Datas

Digital Image Correlation

Image Analysis

Experimental Results

FEABC

ED

DIC

IA

ER

M

Page 16: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 16

FiniteElementAnalysis

constitutive law

Boundary Conditions

Mesh

Optimization Procedure

Law cost Function

FEABC

ED

DIC

IA

ER

M

Page 17: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 17

Results and Discussion

Uniaxial Tensile Test

0

1

2

3

4

5

6

7

0.5 0.6 0.7 0.8 0.9 1

stretch ratio

No

min

al S

tre

ss

(M

Pa

)

0

1

2

3

4

5

6

7

1 2 3 4

stretch ratio

No

min

al S

tre

ss

(M

Pa

)

UT - v1

UT - v2

UT - v3

Page 18: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 18

Results and Discussion

Biaxial Tensile Test

0

1

2

3

4

5

6

0.85 0.9 0.95 1stretch ratio

No

min

al S

tre

ss

(M

Pa

)

0

1

2

3

4

5

6

1 1.5 2 2.5 3stretch ratio

No

min

al S

tre

ss

(M

Pa

)

BT - v1

BT - v2

BT - v3

Pure shear

Page 19: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 19

Results and Discussion

DENT Test

0

10

20

30

40

0 200 400 600 800 1000

time (s)

Lo

ad

(N

)

s imulation

experiment

Page 20: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 20

Results and Discussion

DENT Tests

Page 21: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 21

Concluding and remarks

Strain sollicitations diagram

1

1.5

2

2.5

3

3.5

4

0.5 1 1.5Transversal Stretch Ratio

Axi

al S

tre

tch

Ra

tio

DENT exp.

DENT sim.

UT

BT

Multiaxial tests with localisation zone

Fracture criteria

Page 22: Mechanical Behaviour of silica filled Silicon Rubber: an Optical two-dimensional Extensometer Application Mechanics of Materials and Structures Lab (2MS)

CompTest 2003 22

Concluding and remarks

FEA + Two-dimensional Digital Extensometer

•Realistic Boundary Conditions

•Identical meshes for FEA/DIC

•Identification bases on Multiaxial Tests

Inverse Approach