influ of tool pin and rotation speed on al alloy

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    Materials Science and Engineering A 459 (2007) 718

    Influences of pin profile and rotational speed of the tool on the formationof friction stir processing zone in AA2219 aluminium alloy

    K. Elangovan, V. Balasubramanian

    Department of Manufacturing Engineering, Annamalai University, Annamalai Nagar 608002, Tamil Nadu, India

    Received 23 October 2006; received in revised form 13 December 2006; accepted 27 December 2006

    Abstract

    AA2219 aluminium alloy has gathered wide acceptance in the fabrication of light weight structures requiring a high strength-to-weight ratio.

    Compared to the many fusion welding processes that are routinely used for joining structural aluminium alloys, friction stir welding (FSW) processis an emerging solid state joining process in which the material that is being welded does not melt and recast. The welding parameters and tool pin

    profile play a major role in deciding the weld quality. In this investigation an attempt has been made to understand the influences of rotational speed

    and pin profile of the tool on friction stir processed (FSP) zone formation in AA2219 aluminium alloy. Five different tool pin profiles (straight

    cylindrical, tapered cylindrical, threaded cylindrical, triangular and square) have been used to fabricate the joints at three different tool rotational

    speeds. The formation of FSP zone has been analysed macroscopically. Tensile properties of the joints have been evaluated and correlated with

    the FSP zone formation. From this investigation it is found that the square tool pin profile produces mechanically sound and metallurgically defect

    free welds compared to other tool pin profiles.

    2007 Elsevier B.V. All rights reserved.

    Keywords: AA2219 aluminium alloy; Friction stir welding; Rotational speed; Tool pin profile; FSP zone; Tensile properties

    1. Introduction

    AA2219 is most widely used material for the construction of

    liquid cryogenic rocket fuel tanks. It has a unique combination

    of properties such as good weldability, high strength-to-weight

    ratio and superior cryogenic properties [1]. The preferred weld-

    ing processes for AA2219 aluminium alloy are frequently gas

    metal arc welding (GMAW) and gas tungsten arc welding

    (GTAW) due to their comparatively easier applicability and bet-

    ter economy [2]. However, plasma arc welding (PAW) with a

    positive polarity electrode and high welding current allows alu-

    miniumcomponents to be joinedeconomically with an excellent

    weld quality [3]. In comparison with the TIG and MIG arcs,

    the electron beam is characterized by higher power density and

    thus permits the single pass welding of square butt joints with

    thickness up to approximately 8 mm in the flat position [4].

    Corresponding author. Tel.: +91 4144 239734;

    fax: +91 4144 239734/4144 238275.

    E-mail addresses: [email protected](K. Elangovan),

    [email protected] (V. Balasubramanian).

    ThoughAA2219 hasgot anedge over its6000and7000seriescounterparts in terms of weldability, it also suffers from poor as

    weldedjoint strength.Thejoint strength is only about 40%when

    compared to the base metal strength in T87 condition. This is

    true both in autogenous welds as well as those welded with the

    matching filler 2319, which contains slightly higher contents of

    Ti and Zr. The loss of strength is due to the melting and quick

    resolidification, which renders all the strengthening precipitates

    to dissolve and the material is as good as a cast material with

    solute segregation and large columnar grains [5].

    Compared to many of the fusion welding processes that are

    routinely used for joining AA2219 aluminum alloy, friction stir

    welding (FSW) is an emerging solid state joining process in

    which the material that is being welded does not melt and recast

    [6]. Friction stir welding (FSW) was invented at The Welding

    Institute (TWI), UK in 1991. Friction stir welding is a contin-

    uous, hot shear, autogenous process involving non-consumable

    rotating tool of harder material than the substrate material [7].

    Fig. 1 explains the working principle of FSW process. Defect

    free welds with good mechanical properties have been made in

    a variety of aluminium alloys, even those previously thought

    to be not weldable. When alloys are friction stir welded, phase

    transformations that occur during cool down of the weld are of a

    0921-5093/$ see front matter 2007 Elsevier B.V. All rights reserved.

    doi:10.1016/j.msea.2006.12.124

    mailto:[email protected]:[email protected]://dx.doi.org/10.1016/j.msea.2006.12.124http://dx.doi.org/10.1016/j.msea.2006.12.124mailto:[email protected]:[email protected]
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    8 K. Elangovan, V. Balasubramanian / Materials Science and Engineering A 459 (2007) 718

    Fig. 1. Schematic representation of FSW principle.

    solid state type. Due to the absence of parent metal melting, the

    new FSW process is observed to offer several advantages overfusion welding [8].

    FSW joints usually consist of four different regions as shown

    in Fig. 2. They are: (a) unaffected base metal; (b) heat affected

    zone (HAZ); (c) thermo-mechanically affected zone (TMAZ)

    and (d) friction stir processed (FSP) zone. The formation of

    above regions is affected by the material flow behaviour under

    the action of rotating non-consumable tool. However, the mate-

    rial flow behaviour is predominantly influenced by the FSW

    tool profiles, FSW tool dimensions and FSW process param-

    eters [9,10]. The available literature focusing on the effect of

    welding parameters and tool profiles on FSP zone formation in

    AA2219 aluminum alloy is very scant. Hence, in this investiga-tionanattempt has beenmade to understand the effectof tool pin

    profiles and rotational speed on FSP zone formation. This paper

    presents the relation between the FSP zone formation and ten-

    sile properties of friction stir welded AA2219 aluminium alloy

    joints.

    2. Experimental Work

    The rolled plates of 6 mm thickness, AA2219 aluminium

    alloy, were cut into the required size (300mm 150mm) by

    power hacksaw cutting and grinding. Square butt joint con-

    figuration, as shown in Fig. 3 was prepared to fabricate FSW

    joints. The initial joint configuration was obtained by securing

    the plates in position using mechanical clamps. The direction of

    welding was normal to the rolling direction. Single pass weld-

    Fig. 2. Different regions of FSW joint: (a) unaffected base metal; (b) heat

    affected zone (HAZ); (c) thermo-mechanically affected zone (TMAZ); (d) fric-

    tion stir processed (FSP) zone.

    Fig. 3. Dimensions of square butt joint.

    Fig. 4. FSW tool dimensions.

    Table 1a

    Chemical composition (wt%) of base metal

    Cu 6.7

    Mn 0.27

    Si 0.01

    Zn 0.04

    Ti 0.05

    Fe 0.13

    Zr 0.12

    Mg 0.01

    Al Bal

    ing procedure was used to fabricate the joints. Non-consumable

    tools made of high carbon steel were used to fabricate the joints.

    The tool dimensions are shown in Fig. 4. The chemical com-

    position and mechanical properties of base metal are presented

    in Table 1. An indigenously designed and developed machine

    (15HP; 3000 rpm; 25 kN) was used to fabricate the joints. Five

    different tool pin profiles, as shown in Fig. 5 were used to fab-

    ricate the joints. Using each tool, 3 joints were fabricated at 3

    different rotational speeds and in total 15 joints (5 3) were

    fabricated in this investigation. Trial experiments were carried

    out to find out the working limits of welding parameters. Three

    differentwelding speeds (0.32 mm/s, 0.76 mm/s and1.25 mm/s)

    and three different axial force levels (10 kN, 12 kN and 14 kN)

    were used to fabricate the joints. Then the joints were visually

    inspectedfor exteriorwelddefects andit was foundthat thejoints

    Table 1b

    Mechanical properties of AA2219-T87

    Yield strength (MPa) 310

    Ultimate tensile strength (MPa) 408

    Elongation (%) 23

    Vickers hardness (0.5 kg) 140

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    K. Elangovan, V. Balasubramanian / Materials Science and Engineering A 459 (2007) 718 9

    Fig. 5. FSW tool pin profiles.

    Table 2

    Welding parameters and tool dimensions

    Process parameters Values

    Rotational speed (rpm) 1500, 1600, 1700

    Welding speed (mm/s) 0.76

    Axial force (kN) 12

    D/dratio of tool 3.0

    Pin length (mm) 5.7

    Tool shoulder diameter, D (mm) 18

    Pin diameter, d(mm) 6

    Tool inclined angle () 0

    Shoulder deepness inserted into the surface

    of base metal (mm)

    0.2

    Included angle of taper pin 7.5

    Pitch (mm) and included angle () of

    threaded pin

    1 and 60

    fabricated at the welding speed of 0.76 mm/s and axial force of

    12 kN was free fromany externaldefects. Similar welding speed

    was used by the other investigator [8] also to weld AA2219 alu-

    minium alloy. The welding parameters and tool dimensions are

    presented in Table 2.

    The welded joints were sliced using power hacksaw and

    then machined to the required dimensions to prepare ten-

    sile specimens as shown in Fig. 6. American Society for

    Testing of Materials (ASTM) guidelines were followed for

    preparing the test specimens. Tensile test was carried out

    in 100 kN, electro-mechanical controlled Universal TestingMachine. The specimen was loaded at the rate of 1.5 kN/min

    as per ASTM specifications, so that tensile specimen under-

    goes deformation. The specimen finally fails after necking

    Fig. 6. Dimensions of tensile specimen.

    and the load versus displacement was recorded. The 0.2%

    offset yield strength, ultimate tensile strength and percentage

    of elongation were evaluated. Vickers microhardness testingmachine (Make: Matzusawa, Japan and Model: MMT-X7) was

    employed formeasuringthehardnessacrossthe joint with 0.5kg

    load.

    Macro- and microstructural analysis was carried out using

    a light optical microscope (VERSAMET-3) incorporated with

    an image analyzing software (ClemexVision). The specimens

    for metallographic examination were sectioned to the required

    sizes from the joint comprising FSP zone, TMAZ, HAZ and

    base metal regions and polished using different grades of

    emery papers. Final polishing was done using the diamond

    compound (1m particle size) in the disc polishing machine.

    Specimens were etched with Kellers reagent to reveal the

    macro- and microstructures. The fractured surface of the ten-

    sile tested specimens was analysed using digital scanner at

    low magnification to study the general mode of fracture pat-

    tern to establish the relationship between FSP zone and the

    fracture.

    3. Results

    3.1. Macrostructure

    In fusionwelding of aluminiumalloys, thedefects like poros-

    ity, slag inclusion, solidification cracks, etc. deteriorates the

    weld quality and joint properties. Usually, friction stir weldedjoints are free from these defects since there is no melting takes

    place during welding and the metals are joined in the solid

    state itself due to the heat generated by the friction and flow of

    metal by the stirring action. However, FSW joints are prone to

    other defects like pinhole, tunnel defect, piping defect, kissing

    bond, cracks, etc. due to improper flow of metal and insuffi-

    cient consolidation of metal in the FSP region. All the joints

    fabricated in this investigation are analysed at low magnifica-

    tion (10) using optical microscope to reveal the quality of FSP

    regions.

    The macrostructure of the joints and the observations (FSP

    zone shape, FSP zone height (H), FSP zone width (W) at three

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    Table 3

    Effect of rotational speed on macrostructure of the joints fabricated by straight cylindrical pin profiled tool

    Rotational

    speed (rpm)

    Macrostructure Size of FSP

    zone (mm)

    Shape of

    FSP zone

    Name of the

    defect and

    location

    Quality of

    weld metal

    consolidation

    Probable reasons

    RS AS W H

    1500 8.7 5.9 Inverted

    trapezoidal

    Tunnel in the

    bottom of the

    weld in the

    retreating side

    (RS)

    Poor Insufficient heat

    input and flow of

    the plasticized

    metal

    6.1

    4.1

    1600 9.2 5.9 Tunnel in the

    root of the weld

    in the retreating

    side

    No vertical flow

    of the metal6.3

    3.9

    1700 11.1 5.8 Pinholes in the

    retreating side

    and the root of

    the weld

    6.2

    4.6

    different locations, quality of the FSP zone, etc.) made from the

    macrostructure are presented in Tables 37. All the three joints

    fabricated using straight cylindrical pin profiled tool (Table 3)

    and tapered cylindrical pin profiled tool (Table 4) are found

    to be defective irrespective of rotational speeds used. In the

    case of threaded cylindrical pin profiled tool (Table 5) and tri-

    angular pin profiled tool (Table 7), the joints fabricated at a

    rotational speed of 1500 rpm are found to be defective. On the

    Table 4

    Effect of rotational speed on macrostructure of the joints fabricated by tapered cylindrical pin profiled tool

    Rotational

    speed (rpm)

    Macrostructure Size of FSP

    zone (mm)

    Shape of FSP

    zone

    Name of the

    defect and

    location

    Quality of

    weld metal

    consolidation

    Probable

    reasons

    RS AS W H

    1500 7.4 5.8 Inverted

    trapezoidal

    Tunnel in the

    bottom of the

    weld in the

    retreating side

    Poor Insufficient heat

    input and flow

    of the

    plasticized metal

    5.1

    3.1

    1600 8.4 5.9 Pinhole in the

    middle of the weld

    in the retreating

    side

    No vertical flow

    of the metal6.1

    4.3

    1700 11.3 5.9 Tunnel in the

    bottom of the

    weld in the

    retreating side

    6.7

    5.1

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    K. Elangovan, V. Balasubramanian / Materials Science and Engineering A 459 (2007) 718 11

    Table 5

    Effect of rotational speed on macrostructure of the joints fabricated by threaded cylindrical pin profiled tool

    Rotational

    speed (rpm)

    Macrostructure Size of FSP

    zone (mm)

    Shape of FSP

    zone

    Name of the

    defect and

    location

    Quality of

    weld metal

    consolidation

    Probable reasons

    RS AS W H

    1500 8.1 5.9 Inverted

    trapezoidal

    No defect Good Screw thread generate

    more heat and exerts

    an extra downward

    movement to the

    plasticized metal

    4.3

    3.1

    1600 10.3 5.8 No defect Good 5.2

    3.9

    1700 11.2 5.9 Pinhole in the

    middle of the

    weld

    Poor Excess turbulence of

    the plasticized metal

    due to higher

    rotational speed

    8.3

    7.1

    other hand, the joints fabricated using square pin profiled tool is

    found to be free from defects (Table 6). From the macrostruc-

    ture analysis, it can be inferred that the formation of defect

    free FSP zone is a function of tool profile and rotational speed

    used.

    3.2. Tensile properties

    Transverse tensile properties of FSW joints such as yield

    strength, tensile strength, percentage of elongation and joint

    efficiency were evaluated. Three specimens were tested at each

    Table 6

    Effect of rotational speed on macrostructure of the joints fabricated by square pin profiled tool

    Rotational

    speed (rpm)

    Macrostructure Size of FSP

    zone (mm)

    Shape of FSP

    zone

    Name of the

    defect and

    location

    Quality of

    weld metal

    consolidation

    Probable reasons

    RS AS W H

    1500 10.1 5.8 Inverted

    trapezoidal

    No defect Good Sufficient working of the

    plasticized metal due to

    the pulsating action of the

    pin profile

    4.1

    4.0

    1600 10.0 5.9 5.7

    3.3

    1700 12.1 5.9 Excess working of the

    plasticized metal with

    wider FSP due to high

    rotational speed

    8.4

    6.8

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    Table 7

    Effect of rotational speed on macrostructure of the joints fabricated by triangular pin profiled tool

    Rotational

    speed (rpm)

    Macrostructure Size of FSP

    zone (mm)

    Shape of FSP

    zone

    Name of the

    defect and

    location

    Quality of

    weld metal

    consolidation

    Probable reasons

    RS AS W H

    1500 7.4 5.9 Inverted

    trapezoidal

    Pinhole in the

    retreating side

    Poor Insufficient heat

    input and flow of

    the plasticized

    metal

    4.8

    3.3

    1600 8.6 5.9 No defect Good Adequate heat

    input and flow of

    the plasticized

    metal

    5.8

    4.3

    1700 9.1 5.9 No defect Good

    5.9

    3.4

    condition and average of the results of three specimens is pre-

    sented in Fig. 7. From the figure, it can be inferred that the

    tool profile and tool rotational speed are having influence on

    tensile properties of the FSW joints. Of the five joints, the

    joints fabricated by square tool profile exhibited superior tensile

    properties compared to other joints, irrespective of tool rota-

    tional speed. Similarly, the joints fabricated by threaded pin

    profiled tool are also showing almost matching tensile prop-

    erties to that of square tool profile. But the joints fabricated by

    straight cylindrical tool profile exhibited inferior tensile proper-

    Table 8

    Effect of rotational speed on fracture surface of the joints fabricated by straight cylindrical pin profiled tool

    Rotational speed (rpm) Fracture surface Location of

    fracture

    Fracture surface

    appearance

    Orientation of defects

    1500 Between FSP

    and HAZ of

    retreating side

    Coarse granular

    appearance with

    concave surface

    Groove corresponding

    to the tunnel in the

    weld cross section

    1600 Uneven surface with

    mixed mode pattern

    1700 Irregular surface with

    dull grey fibrous

    appearance

    Groove corresponding

    to the pinhole in the

    weld cross section

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    Fig. 7. Effect of rotational speed on tensile properties: (a) tensile strength; (b) yield strength; (c) percentage of elongation; (d) joint efficiency.

    tiescompared to theircounterparts, irrespectiveof toolrotational

    speed.

    The joints fabricated at the rotational speed of 1500 rpm have

    shown lower tensile strength and elongation compared to the

    joints fabricated at a rotational speed of 1600 rpm and this trend

    iscommonfor allthe tool profiles.Similarly, thejoints fabricated

    at therotational speed of 1700 rpmhavealso shownlowertensile

    strength and elongation compared to the joints fabricated at a

    rotational speed of 1600rpm. The effect of rotational speed is

    concerned, the joints fabricated at a rotational speed of 1600 rpm

    areshowing superior tensile properties compared to other joints,

    irrespective of tool profiles. The fractured surfaces of the tensile

    test specimens were scanned using a digital scanner and the

    fracture patterns of all the joints and observations made from

    the fractured surface are presented in Tables 712. From the

    fractured surface analysis, it can be inferred that the defect free

    welds are showing uniform deformation across the weld before

    failure (Table 11).

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    Table 9

    Effect of rotational speed on fracture surface of the joints fabricated by tapered cylindrical pin profiled tool

    Rotational speed (rpm) Fracture surface Location of

    fracture

    Fracture surface

    appearance

    Orientation of

    defects

    1500 Between FSP

    and HAZ of

    retreating side

    Irregular surface

    with fibrous

    appearance along

    with striations at

    the top

    Groove

    corresponding to

    the tunnel in the

    weld cross section

    1600 Uneven surface

    with fibrous dull

    grey appearance

    Insufficient

    consolidation

    corresponding to

    the pinhole in the

    weld cross section

    1700 Flat surface with

    coarse granular

    appearance

    Groove

    corresponding to

    the tunnel in the

    weld cross section

    4. Discussion

    From the experimental results (macrostructure, tensile prop-

    erties and fracture surface), it is found that the joint fabricated

    using square pin profiled tool at a rotational speed of 1600rpm

    exhibited superior tensile properties compared to other joints.

    The reasons for the better performance of these joints are

    explained below.

    4.1. Effect of tool pin profile

    The primary function of the non-consumable rotating tool

    pin is to stir the plasticized metal and move the same behind

    it to have good joint. Pin profile plays a crucial role in mate-

    rial flow and in turn regulates the welding speed of the FSW

    process [11,12]. The pin generally has cylindrical plain, frus-

    tum tapered, threaded and flat surfaces. Pin profiles with flat

    Table 10

    Effect of rotational speed on fracture surface of the joints fabricated by threaded cylindrical pin profiled tool

    Rotational

    speed (rpm)

    Fracture surface Location of

    fracture

    Fracture surface

    appearance

    Orientation of

    defects

    1500 Between FSP and

    HAZ of retreating

    side

    Flat and smooth

    surface with bright

    granular appearance

    No defect

    1600 Irregular surface with

    fibrous dull grey

    appearance

    No defect

    1700 Uneven surface with

    fibrous appearance

    along with striations

    at the top

    Groove

    corresponding to

    the pinhole in the

    weld cross section

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    Table 11

    Effect of rotational speed on fracture surface of the joints fabricated by square pin profiled tool

    Rotational

    speed (rpm)

    Fracture surface Location of

    fracture

    Fracture surface

    appearance

    Orientation of defects

    1500 Between FSP

    and HAZ of

    retreating side

    Coarse granular

    appearance with striations

    at top and bottom

    No defect

    1600 Concave surface with

    granular appearance (like

    cup and cone fracture)

    1700 Granular appearance with

    striations at the bottom

    Table 12

    Effect of rotational speed on fracture surface of the joints fabricated by triangular pin profiled tool

    Rotational

    speed (rpm)

    Fracture surface Location of

    fracture

    Fracture surface

    appearance

    Orientation of defects

    1500 Between FSP

    and HAZ of

    retreating side

    Uneven surface with

    coarse granular

    appearance along with

    striations at the bottom

    Groove corresponding to

    the pinhole in the weld

    cross section

    1600 Flat surface with bright

    granular appearance

    No defect

    1700 Irregular surface with dull

    grey fibrous appearance

    along with striations at

    the bottom

    No defect

    Fig. 8. Effect of pin profiles on FSP zone hardness.

    faces (square and triangular) are associated with eccentricity.

    This eccentricity allows incompressible material to pass aroundthe pin profile. Eccentricity of the rotating object is related to

    dynamic orbit due to eccentricity [13]. This dynamic orbit is

    the part of the FSW process. The relationship between the static

    volume and dynamic volume decides the path for the flow of

    plasticized material from the leading edge to the trailing edge of

    the rotating tool. This ratio is equal to 1 for straight cylindrical,

    1.09 for tapered cylindrical, 1.01 for threaded cylindrical, 1.56

    for square and 2.3 for triangular pin profiles. In addition, the

    triangular and square pin profiles produce a pulsating stirring

    action in the flowing material due to flat faces. The square pin

    profile produces 100pulses/s and triangular pin profile produces

    75 pulses/s when the tool rotates at a speed of 1500 rpm. There

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    Fig. 9. Effect of tool pin profiles on FSP zone microstructure: (a) straight cylindrical; (b) taper cylindrical; (c) threaded cylindrical; (d) square; (e) triangular.

    is no such pulsating action in the case of cylindrical, tapered and

    threaded pin profiles.

    During tensile test, most of the specimens failed in the FSP

    region but the exact location of failure is either at the retreating

    side (RS) or at the advancing side (AS) and it is also evident

    from the fracture surface analysis. Hence, microhardness mea-

    surement and microstructural analysis have been carried out in

    the FSP region of all the joints. Fig. 8 shows the microhardness

    values and Fig. 9 displays themicrostructure of FSPregionof all

    the joints fabricated at a rotational speed of 1600rpm for com-

    parison purpose. Of the five joints, the highest hardness value

    of 105 Hv has been recorded in the joint fabricated using square

    pin profiled tool and the lowest hardness value of 82 Hv has

    been recorded in the joint fabricated using straight cylindrical

    pin profiled tool. Similarly, the FSP region of the joint fabri-

    cated using square pin profile tool contains finer grains (Fig. 9d)

    compared to other joints. The higher number of pulsating action

    experienced in the stir zone of square pin profiled tool produces

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    K. Elangovan, V. Balasubramanian / Materials Science and Engineering A 459 (2007) 718 17

    finer grained microstructure and in turn yields higher strength

    and hardness.

    4.2. Effect of tool rotational speed

    Rotational speed appears to be the most significant process

    variable since it also tends to influence the translational velocity.

    Veryhighrotationalspeeds (>10,000 rpm)couldraisestrain rate,

    andthereby influence therecrystallisationprocess;whichin turn

    could influence the FSW process [14]. Higher tool rotational

    speed resulted in a higher temperature and slower cooling rate

    in the FSP zone after welding. A higher rotational speed causes

    excessive release of stirred materials to the upper surface, which

    resultantly left voids in theFSP zone. Lowerheat input condition

    dueto lowerrotational speed resulted in lack of stirring.Thearea

    of the FSP zone decreases with and decreasing the tool rotation

    speed and affect the temperature distribution in the FSP zone

    [15].

    As the rotational speed increases, the strained region widens,

    and the location of the maximum strain finally moves to theadvancing side from the original retreating side of the joint.

    This implies that the fracture location of the joint is also affected

    by the rotational speed [16]. The tensile properties of the joints

    madewithdifferentwelding conditionsresulted in lowest tensile

    strength and ductility at lowest spindle speed for a given tra-

    verse (welding) speed. As the spindle speed increased, both the

    strength and elongation improved, reaching a maximum before

    falling again at high rotational speeds. It is clear that, in FSW,

    as the rotational speed increases, the heat input also increases.

    However, the calculated maximum temperatures are nearly the

    same in all the rotational speeds. This phenomenon can be

    explained by the following two reasons: first, the coefficient offriction decreases when a local melt occurs, and subsequently

    decreases when a local input; secondly, the latent heat absorbs

    some heat input.

    Moataz and Hanadi [17] have opined that at very high rota-

    tional speeds, second phase (strengthening) particles would

    suffer more fragmentation and leads to segregation of par-

    Fig. 10. Effect of rotational speed on FSP zone hardness (tool profile: square

    pin).

    ticles in other parts of the TMAZ. As the rotational speedis decreased, and the temperature within the nugget becomes

    lower and the volume fraction of coarse second phase particles

    increases. Hence, the tool rotation speed must be optimized to

    getFSPregionwith fineparticlesuniformlydistributedthrough-

    out the matrix. Of the three different tool rotational speeds,

    the joints fabricated at a rotational speed of 1600 rpm exhib-

    ited superior tensile properties, irrespective of tool pin profiles.

    For comparison purpose, the microhardness and microstructure

    of FSP regions produced by square pin profiled tool at different

    rotational speedsarepresented in Figs. 10 and 11. Higher micro-

    hardness and finer grain diameter have been obtained at the FSP

    region of the joint fabricated at 1600 rpm using square pin pro-

    filed tool. The combined effect of higher number of pulsating

    stirring action during metal flow and an optimum tool rotational

    speed may be the reason for superior tensile properties, higher

    hardness and finer microstructure at the FSP region of the joint

    fabricated at a rotational speed of 1600rpm using square pin

    profiled tool.

    Fig. 11. Effect of rotational speed on microstructure of FSP zone (tool profile: square pin).

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    18 K. Elangovan, V. Balasubramanian / Materials Science and Engineering A 459 (2007) 718

    5. Conclusions

    In this investigation an attempt has been made to study the

    effect of tool pin profile and tool rotational speed on the forma-

    tion of friction stir processing zone in AA2219aluminium alloy.

    From this investigation, the following important conclusions are

    derived:

    (i) Of the five tool pin profiles used in this investigation to

    fabricatethe joints, squarepinprofiled tool produced defect

    free FSP region, irrespective of rotational speeds.

    (ii) Of the three tool rotational speedsused in this investigation

    to fabricate the joints, the joints fabricated at a rotational

    speed of 1600 rpm showed better tensile properties, irre-

    spective of tool pin profiles.

    (iii) Ofthe15 jointsfabricatedin this investigation, thejointfab-

    ricated using square pin profiled tool at a rotational speed

    of 1600 rpm showed superior tensile properties.

    Acknowledgements

    The authors are grateful to the Department of Manufacturing

    Engineering, AnnamalaiUniversity, AnnamalaiNagar, Indiafor

    extendingthefacilitiesof Metal Joining Laboratory andMaterial

    Testing Laboratory to carryout this investigation. The authors

    wish to place their sincere thanks to Aeronautical Research &

    Development Board (ARDB), New Delhi for financial support

    rendered through a R&D project No. DARO/08/1061356/M/I.

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