icp test report certification packet/media/electronics_technical/... · 2013-06-17 · for unit...

1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc. Product Series: PTC Product #: SMD, SL - 0603L, 0805L, 1206L, 1210L, 1812L, 2016L, 2920L Series

Issue Date: October 21, 2011 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.

Issued by:

<Global EHS Engineer>

(1) Parts, sub-materials and unit parts This document covers the SMD - 0603L, 0805L, 1206L, 1210L, 1812L, 2016L, 2920L RoHS-Compliant series products manufactured by Littelfuse, Inc. ＜ Raw Materials Used

Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1

Remarks：.

2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part

Number Raw Material Description Page(s) 1 HDPE/LR5900 Polyethylene 3-12 2 Raven 430UB Carbon Black 13-22 3 N/A Nickel Copper Foil 23-29 4 N/A Copper Foil 30-36 5 N/A Tin 37-41 6 ZSR-150W Ink Acrylic- White (with Phthalates) 42-49 7 ZSR-150W Ink Acrylic - White (Halogen) 50-53 8 PSR-550B Ink Acrylic- Green 54-60 9 PSR-550B Ink Acrylic - Green (Phthalates) 61-64 10 IT-140GBS Prepreg (with Phthalates) 65-79 11 N/A Plated Copper 80-84

Form 585-047 Rev. A 2/21/06

Validit nownFor QueSPtease u ith scs

t Itt||lIttt||l

Test Report No.: CE/2011122921Dale: 201110?,24 P a g e : 1 o f 1 0

EQUISTAR CHEMICALS, LPONE HOUSTON CENTER, SUITE 1600, 1221 IJCKINNEY ST, P. O. BOX 2583 HOUSTON,fExAx7t252-25A3

The following sample(s) was/wer submltted and identified by/on behatfofthe client as:

Sample DescriptionStyl€/ltem No.Sample Receiving DateTesting Period

POLYETHYLENEHDPE/LRsgOO2011t02t1A201 1 t O2t 1 I r O 201 1 tOZ24

Test Result(s) : Please refer to next page(s)

re l r csk bsrsn@odendb€cm@ Ll;irt1.'r...i irF, */{ilt ;11j1}..:1r . /.il:i3r.1-1\.: 3d;+:t. , ,ti U{!.n3d@hd€s3dbyh€ . .mFny ' r b i 6db6GgEE lcod Ibnsds

36 ] sd lo f * f u f ! co rn ims f t ) l €rma or b nb*$'Kin

rbf .ob6dd bd63ui6rhr€ nnd beqdud.xc.pr nrui. Mhd ry maunmd *darm

:rrn.r ?L rl .lr Lrias6loila

lorr

th.nH L-ado.V - T.h.l

scsTest Report No.:CEnO11n2921 Dalet2l l l t \2t24 page:2 of 1O

EQUISTAR CHEMICALS. LPOI]E HOUSTON CENTER, SUITE 1600, 1221 I.I|CKINNEY ST, P. O, BOX 2583 HOUSTON,rExAr< 77252-2583

Test Resultlsl

PART NAME No.1

Test ltom (s): Unit Method MDL RosultNo.'l

Cadmium (Cd) mgikg With reference to IEC 6232t: 20(E andperformed by ICP-AES.

2 n .d .

Lead (Pb) mg/Kg With reference to tEC 62321: 2008 andperformed by ICP-AES.

2 n.d.

Mercury (Hg) mg/Kg With reference to IEC 6232'1: 2008 andperfomed by ICP-AES.

2 n.d.

Hexavalent Chromium CrCy'l) byalkaline extraction

mg/Kg With reference to IEC 62321: 2008 andperformed by W-VIS.

2 n.d.

Hexabromocyclododecane(HBCDD) (CAS No.: 025637-994)

mg/Kg With reference to US EPA 3540Cmethod. Analysis was performed byGC/MS.

5 n.o.

Perfluor@ctane sulfonates(PFOS)PFOS - AcidPFOS - Metal SaltPFOS -Amide

mg/xg With reference to uS EPA 3540C:'1 996 method for PFOS Content.Analysis was performed by LC/MS.

1 0 n.d.

PFOA (CAS No.: 00033567-1) mg/Kg With reference to Us EPA 3540c1'1996 method for PFOA Content.Analysis wa5 perfomed by LC/[,S.

1 0 n.d.

Phthalat€6BBP (Benzyl butyl phthalate) (CASNo.: 000085€8-7)

'/o With reference to EN 14372. Analysiswas perfomed by GC/MS.

0.003 n.d,

DEHP (Di- (2-ethylhexyl)phthalate) (CAS No.: 0001 17{1-7)

o/o With reference to EN'14372. Analysiswas performed by GC/MS.

0.003 n.d.

DIDP (Di-isodecyl phthalate) (CASNo.:026761-4G0)

% With reference to EN 1 4372. Analysiswas performed by GC/irS.

0.01 n .d .

DINP (Di-isononyl phthalate) (CASNo.:02855312-0)

With referonce to EN 14372. Analysiswas performed by GC/MS.

0.01 n.d.

ONOP (Di-n-octyl phthalate) (CASNo.:000117-84-0)

% f,,/ith reference to EN 14372. Analysisl€s perfomed by GC/MS.

0.003 n.d.

DBP (Dibutyl phthalate) (CAS No.:000084-74-2)

% lL/ith reference to EN 14372. Analysisi.as performed by GC/l\rS.

0.003 n . d .

n lh 3 rar €pdldar ody b ik smpr6G)cdd rhs r6i.@n €nd b tscom@nyhr;tr.iir+q.t|11r,:rl11fr,:i!1;li'.e4.,1-.r++la1r:E-j::iJ..1.t:.,rli!.1

vsub ]d l o tG6m€cMd i66ds *

rd'ons. f 3ry h3cmFntsso6,3rb.,crcadd 0d 63 uid.r rh. t'

l[| |lI|t[l]|lll

WHITE POWDER

Test Report No.: CEn011l22g21 Da'.e:2011t'z24 page: 3 of 1O

EQUISTAR CHEMICALS, LPONE HOUSTON CENTER, SUITE 1600, 122'1 MCKINNEY ST, P. O. BOX2583 HOUSTON,rEx,x77252-25A3

Test ltem (s): Unit Mothod i,DL Re6ultNo.t

HalogenHalogen-Fluoine (F) (CAS No-014762-94-8)

mg/Kg With reference to BS EN 14582'2007.Analysis was pertomed by lC.

50 n.o.

Halogen-Chlo.ine (Cl) (CAS No.:022537 -15-1)

mg/Kg With reference to BS EN U5A22007 .Analysis was performed by lC.

50 n.d.

Halogen-Bromine (Br) (CAS No.:010097-32-2)

msik9 With reference to BS EN 14582''2cn7.Analysis was performed by lC.

50 n.d-

Halogenlodine (l) (CAS No.:01436244€)

mgfts with reference to Bs EN 14582:2007 .Analysis was perfo.med by lC.

50 n.d.

Sum of PBB9

mgikg With feference to IEC 62321: 2008 andpeformed by cC/lVS.

n.d.Monobromobiphenyl n.d.Dibromobiphenyl n.d.Tribromobiphenyl 5 n.d.Tetrabrcmobiphenyl 5 n.d.Pentabromobiphenyl 5 n.d.Hexabromobiphenyl 5 n . d .Heptabromobiphenyl 5 n.d-Octabromobiphenyl 5 n.d-Nonabromobiphenyl 5 n.d-Decabromobiphenyl 5 n.d-Sum of PBDES n . d .Monobromodiphenyl ether 5 n . d .Dibromodiph€nyl ether 5 n . d .Tribromodiphenyl ether 5 n.d.Tehabromodiphenyl ether 5 n.d.Pentabromodiphenyl ether 5 n.d.Hexabromodiphenyl ether 5 n.o,Hoptabromodiphenyl ether 5 n.d.Oclabromodiphenyl ether n.o.Nonabromodiphenyl other 5 n.d.Decabromodiphenyl ether n.d.

nlful€3l€p.nd€ro^91otbgampl€l'1ededThsla*rc@d€mdberecmpsny r I rj I :r.: . .1:t-t!- rr!fi1,; :;l!lrllij:9rf /-$F-h\1.1|- A r+:_. - i:,i,riq,ftsddn€[email protected]]condlbnso'sior 6odrdd 6n.r dddrB.ft s4

n s i b i t y 6 l o i s c e i l l d 6 s f u m e if t t r r ! f u a d d | ' g a 6 n s u e $ a b n o t b 3 E p d u d a e p l ' n l u l ' f u U l

Test Report No.: CE12011n2921 Date 2011t02,24 paoe:4 of 1O

EOUISTAR CHEMICALS, LPONE HOUSTON CENTER, SUITE 1600, 1221TEXAX 77252-25A3

Note :'1. mg/kg = ppm ;0.1wt% = i000ppm2. n.d. = Not Detected3. IVDL = l,Iethod Detection Limit4 . " - "=No tRegu ta ted

MCKINNEY ST, P. O. BOX 2583 HOUSTON,llm tll l]|ltt

L€l' b{d Th s r3d cPd €md b€ repdc m F r y r l l l r j t J r l l i l i ! ' ] l l ! ! : J i ; i n l l : : l { , - l i t s : h , l . ] : : m + r . 7 ! : r r i i q ,}Ed@frsdssdby'hecomp5dys6jodfoi,G*3E]cod1trsolsfor 66d,mc ftim.l doorn.ds suq ha rmbroi d ,'b rydsAtdion and judsddd cs6ddn y and w th n he his ol Cr€d s nsib e t r r ] g f u a d d | ' g d b n s u n e i b g , m n o l b e € p d U d a c e p l ' n f u r . w ] f u dt44oll.sndonol|| i6@ds1ol

PFOS Refer€nce Information : Dirocfive 2OO6/,t2ZEC({} lray not be pleced on the marker or used as a substance or constituent of preparations in a concentrationequalto or higherthan 0.005 % by mass.(2) May not be plac€d on the market in semi-finished products or articles, or parts thereof, if the concentration ofPFOS isequalto of higherthan 0.1 % by mass calculated with reference tothe mass of structuEllv ormicrostruclurally distinct parts that contain PFos or, for textiles or other coated matedals, if lhe amount of pFosis equalto or higher than 1pg/m'?ofthe coated material.

I : i r + ! ' 1 { i s6o?P}e t , ,

Menbs or rh. scs G/oup 66s 5A)

Test Report No.: CE12011t22921 Date:2011|t02t24 page: 5 of iO

EOUISTAR CHEMICALS, LPONE HOUSTON CENTER, SUITE 1600, 1221 IVCKINNEY ST, P. O, BOX 2583 HOUSTON,rExlJ< 77252-2583

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ICP.AES

Sample Material Digestion Acid

$eel, copper, aluminum, soldor Aqua regia, HNO3, HCl, HF, HrO,

Glass HNOy'HF

Gold, platinum, palladium, ceramic Aqua regia

Silver HN03

Pla6tic HrSO4, HrOr, HNOr, HCI

Others Any acid to total digeslion

cmFiv , r+Jr l i t ! r , . ! i t . x ! { , i , ; i r l t iq i f . i ! i t+ r r { : td , l r i I , r l : , l r tE tft9ddumdccsebyb6comts

$ b l e d l o T 6 f r 6 d d c m d i o B f u Eodamit don a! juffidEr d 55w5 d

i^db.j€p6du.6d€ic.pli iu|l ihod

1) Thes€ s€mples were dissotved tota y by pre-conditioning methoct according to betowflow cnan_( Cr- test method excluded )

2) Name of the person who made measurement: Climbgreatyang3) Name of the person in charge of measurement Troy Ch€ng

' r r , i r l ! r e l r r . ! i+s610r l ,e

Acid dig€stion by suitable aciddepended on different samolematerial {as below table)

Microwave digestion wilh

HNO3/HCI/HF

Add appropriate amolnt ofdigestion reagent

Heat to appropriate

tempe€ture to extract

Cool, filter digestate

through filter1) Alkal iFusion2) HCltodissolve

Add diphenyl-cabazide for

color development

measuae the absodance

at 540 nm by UV-VIS

Membo o/r^e 5cs6,o!p665 sAr

Test Report No.: CE12011122921Dai.e : 201110?,24 P a g e : 6 o f 1 0

EQUISTAR CHEMICALS, LPONE HOUSTON CENTER, SUITE 1600, 1221 MCKINNEY ST, P, O. BOX2583 HOUSTON,fExrx 77252-2583

Analwcal flow chart of halogen content1) Name ofthe person who made measurement Rita Chen2) Name of the person in charge of measureftent Troy Chang

rt]]l|t!tlItttt

Sample pretreatment / Separ€tion

Weighling and puttjng sample in cetl

Oxygen Bomb Combustton / Absorption

Dilution to fixed volume

Analy6is was performed by lC

0e(3)Gned rhs bd €tsn 6nd 6cmFiy *,: ,j ! ri!, . ]lri!*1l r!1*ir; rll'r1t.i:ei . .l.n*+lr.1'l:r ' :J i +i] . r 4: I'Jt Eun3dcqmd6]sd6ys€c.mp5

& b , a d l o T 6 . m s e d c m d i ] o c b l E

lherlEhisaidoblga'ms6clbi6

:nl!r: tE!*r3i li + 3e 01)r@

Test Report No. I CE12011122921Dale .2011102124P a g e : 7 o f 1 0

EQUISTAR CHEMICALS. LPONE HOUSTON CENTER, SUITE 1600, 1221 I\4CKINNEY ST, P. O. BOX 2583 HOUSTOII,IEXAX 77252-25A3

l|l|t l| |ltltll

Analytical flow chart of Soxhlet extraction (GC/MS) procedure

1) Name ofthe person who made measurement Lydia Fu

2) Name ofthe person in charge of measurement: Shinjyh Chen

I Te6t ltems: Phthalate , Benzotriazote , HBCDD , Np , DBBT ,

Organic phosphoru6 compounds

Data

nhs|sll€M.€ldon|y1o1b3ampl€1'bddThsb{rupd€nndbaiqdcmFry rt+, jrj ii. . r ili :'!rrtlJ : jrirlrl::: ?j . r-kF,=!r.1.1\- :in+l . 4:i:,iu rj4

ny subrsd ro 6 G*ercond thns d ssuq6d b rems ad cturds 6r E

nsib]i'vtsiddcLei',ds"dhenrh6/ igtu aid dradpns ue ha ra iior b6 r.pdud scapr 'n ru I, wodfoa4ollasfelono'|h6@d3n1or

Test Report No. : CEnO11l22921Dale 2011102124 Page: 8 of 10

EQUISTAR CHEMICALS, LPONE HOUSTON CENTER, SUITE ,1600, ,1221 MCKJNNEY ST, P. O, BOX 2583 HOUSTOII.TEX-AJ,77252-2fi3

Analytical flow chart

1) Name ofthe person who made measurement Roman Wong2) Name of the person in charge of measurement Troy Chang

r TESI ITEMS: PBBi/PBDE, TBBP-A-b|S

Firsl lesling proc€ss -----' Oplionatscreenprocess....... Confhnalion prcc€ss -.>

lfl[tI][l]|lIl

Screen analysis

v

@V

@V

Analysis by GC/MS

vlssue Report

' ith3t*ll€pd'€1€rm|yloibgmp|e1s)le$dThsleslrepod€nm1bBcomFry !:lFritJs .ill i l l r!]}iJ,i;llnl..'ra ,]-ii+.twl. r. :i;li . r i: l.ltqrhdodiad3i3s€dbylhacohpanysuqedb6Gfficondltr3ois

dnt,id w rhn th€ imb or cr€d3 is dbrtEronscrsnradhs&mefrfFir. shre ard obr'gdron5 unk b6 ka nior b6 boodld ded in iu . w rd

Test Report No. : CE12011n2921Oale | 201110?,24 P a g e : 9 o f 1 0

EQUISTAR CHEMICALS, LPONE HOUSTON CENTER, SUITE 1600, 1221 MCKINNEY ST, P, O. BOX 2583 HOUSTOIT,rExN< 77252-2583

Analytical flow chart of Soxhlet extraction (LC/MS) procedure

1) Name ofthe person who made measurement: Lydia Fu

2) Name ofthe person in charge of measurement Shinjyh Chen

rTest ltems: PFOS/PFOA , Benzotriazote

Sample pretreatmenvseparation

I

tfl[It]rIl ]t

UAEI

comFry i.riJ:ii,i r. . .l:ll iej:' .r!1;lrt r-i4!riJr9* - ril++ q1\r f I F-.r'-! ui.c,1h€ fu3a3ss6dby lh6cdmp5 .ysuq6dbbGa@cond l t r 3o l s

ontand*rhinrturmisdcrbft\ isr p.i3b lysro bcrdandrrsddn

It,:, :i :!r r!:,r I rlt 1s6 @PD

Test Report No. : CE|2O11n2921Date :2011102124Page : 10 of l0

' * EndofReport '*

EQUISTAR CHEMICALS. LPONE HOUSTON CENTER, SUITE 1600, 1221 ITCKINNEY ST, P. O, BOX 2583 HOUSTOI\,rExN< 77252-2583

|l][ttt][tt tl

psGli€dd rh s rod 'eFd ennor bconFny d l r , ! i i i " . . r i - 1 r t 1 : i l 1 ! i , j : n ( r t : t r . , l . - l ' i 1 : 14 r - t \ , , i : j l . r ! , " r c l i : trnseum.m 6 6su6d by rh6 co'p,

FBb ' t s ro bc l d randh3d6un

Validit nownFor Ques-ljPlease Co ith scs

f,]ltllt|| ttI]l

Test Report No. : CEnO11l22922 Date | 2O11t0?,24 page : 1 of t O

COLUMBIAN CHEMICALS COMPANY'I8OO WEST OAK COMI,iIONS COURT I,ARIETTA, GEoRGIA 30062

The tollowing sample(s) was/werc submttted and identified by/on behetfofthe ctient as:

Sample DescriptionStyldltem No.Sample Receiving DateTesting Period

Test Result(s)

CARBON BLACKRAVEN43OUB2011t02t1A2011t02t1A rO 201I t12t24

: Please refer to next page(s).

nlh3Isitspddero]yblbsmdcompe^,4 l l , :q i t i ! , . , t l l i t r ! l !u ; r i ,1 r f t , . t6 r - i l++Nr41\ r ' l r ; r . t ,a , . -11 ,44 ,

n y s u h j e d b c G 6 @ c m d l t r s d s

" " o ' s o " " ' . o ' d o : . m a H t f umib 'v ts io '6 o sr ad 6s tufeifttrnstuaddraab$ue$ora nd b6 Bprdud *ced 'n ru I, stud

llrrN

ffiLnadort-T+.a

Men&'dlkscsGrelp{'65'{)

Test Report No. I CE1201122922 Date | 2011t02t24 pagej2of.lO

COLUIMBIAN CHEMICALS COIVPANY18OO WEST OAK COMMONS COURT MARIETTA, GEORGIA 30062

ELACK POWDER

rtlfl||ul ||t[|

Test R€6ultls)

PART NAIVE No.1

T€et ltem (s): Unit Method DL ResultNo.'l

Cadmium (Cd) mgikg With reference to IEC 62321: 2008 rndperformed by ICP+ES.

2 n.d.

Lead (Pb) mgKg With rcference to IEC 62321: 2008 andperformed by ICP-AES.

2 n.d.

lvercury (Hg) mg/Kg With reference to IEC 62321: 2008 anAperfomed by ICP-AES.

2 n.d.

Hexavalent Chromium Cr(Vl) byalkaline extraction

mg/Kg With reference to IEC 62321: 2008 andperfomed by W-VIS-

2 n.d.

Hexabromocyclododecane(HBCDO) (CAS No.: 025637-99-4)

mg/Kg With reference to US EPA 3540Cmethod. Analysis was perfomed byGC/l\rs.

5 n.d.

Perf luorooctane sulfonates(PFOS)PFOS - AcidPFOS - Metal SaltPFOS - Amide

mg/Kg With reference to US EPA 3540C:1996 method for PFOS Content.Analysis wEs p€rfomed by LC/[,S.

1 0 n.d.

PFOA (CAS No.: 000335€71) mg/kg With reference to US EPA 3540C:1 996 method for PFOA Content.Analysis was performed by LC/LilS.

'10 n.o.

Phthalat.sBBP (Benzyl butyl phthalate) (CASNo.:00008568-7)

o/o With reference to EN 14372. Analysisu€s performed by GC/MS.

0.003 n.d.

DEHP (Di- (2-ethylhexyl)phthalate) (CAS No.: 000117€1-7)

% With reference to EN 14372. Analysiswas perfomed by GC/MS.

0.003 n.o.

DIDP (Di-isodecyl phthalate) (CASNo.: 026761-40-0)

% With Gference to EN 14372. Analysiswes performed by GC/MS.

0 .01 n-d.

DINP (Di-isononyl phthalate) (CASNo.:028553-12-0)

% With reference to EN 1 4372. Analysiswas pertormed by GC/l!lS.

0.01 n.d-

DNOP (Di-n-octyl phthalate) (CASNo.: 000'1 17-84-0)

lo With reference to EN 14372. Analysiswas Derformed bv GC/MS.

0.003 n.d.

DBP (Dibutyr phthatate) (cAs No.0o0ou-74-2)

with reference to EN 14372. Analysiswas Derformed bv GC/MS.

0.003 n.o.

n ] ^ 1 h , 1 s l c p d ( r c l 3 r o n y b l h e $ m p e G ] l 6 i d r h 3 k 3 1 . @ d € o d sc o m F n y f i E r , r : j i q . l l r , l , , ; 1 : ; ! t ! i , , l i r r , ' d i i ] - 4 + * t s ^ l : F f l r : 4 . r . r r - - ] t | t t .Thseumd s Ro.d bylhg comFtu ekd d tu dndft. sebl

lbrfohEaddrioa]onsUnel66Ua

Test Report No. -. CEn011122922 Dale : 201'ltOZ24 P a g e : 3 o f 1 0

COLUMBIAN CHEMICALS COMPANY18OO WEST OAK COMMONS COURT IIIARIETTA, GEORGIA 30062

lllttIltt][tltl

T€t ltem (s): Unit Method MDL Ro€ultNo.l

HalogenHalogen-Fluodne (F) (CAS No.:014762-94-8)

mg/Kg With reference to BS EN 1458212007.Analysis was performed by lC.

50 n.o,

Halogen-Chlorine (Cl) (CAS No.:022537 -15-1)

mg/Kg With reference to BS EN 145E2:2007.Analysis w€s perfomed by lC.

50 n.d.

Halogen-Bromine (Br) (CAS No.l01 0097-32-2)

mg/x9 With reference to BS EN 145a2:20O7.Analysis ,.i€s performed by lC.

50 n .d .

Halogen-lodine (l) (CAS No.:01,{362-44J)

mdks With reference to BS EN 145822007 .Analysis wa6 performed by lC.

50 n.d.

Sum of PBBS

mg/Kg With reference to IEC 62321r 2008 andperfomed by GC/MS.

n.d.l\ronobromobiphenyl n-d.Dibromobiphenyl 5 n.d.Tribromobiphenyl 5 n.d.Tetrabromobiphenyl 5 n.d.Pentabromobiphenyl n.o,Hexabromobiphenyl 5 n.o.Heptabromobiphenyl n.d.Octabromobiphenyl 5 n.d.Nonabrcmobiphenyl 5 n.d.Decabromobiphenyl 5 n.d,Sum of PBOES n,d,Monobromodiphenyl elher 5 n.o.Dibromodiphenyl ether 5 n.o.Tribromodiphonyl ether 5 n.d.Tetrabromodiphenyl ether n.d,Pentabrcmodiphonyl ether n-d.Hexabromodiphenyl ether 5 n-d.Heptabromodiphenyl ether 5 n.d.Octabromodiohenvl ether n .d .Nonabromodiphenyl elher 5 n .d .Decabromodiphenyl ether n.d.

' n I h3 I6 l €pdda rm 'b i b9hp |e1s ) l e {d rh3 lo3 l@den@1br€comtsny iirr-r;Eji4 .l|i]rr 1_r!t{r ii Jiir,r:l ni ,l-:1+lprl\F:1r}r.,;!1},!L,ftsdumd ts tsodd bylfu comF

o^t,nd { rh'n th6 inns o, crFds ie p.nsb tErotrsosradbsemi io lbe€pdud6x4pl! i i !

rL rr r r.Lr ft* \ a s6 o.zrrTe rre ouBIT l!W{5(@

Test Report No.: CEl2O11n2922 Dale | 2011t02t24 page:4oflO

COLUMBIAN CHEMICALS COI\4PANY18OO WEST OAK COMMONS COURT MARIETTA, GEORGIA 30062

Note :1. mg/kg = ppm : 0.lwt% = lOOOppm2. n.d. = Not Detected3. IVDL = Method Detection Limit4 . " - "=No tRegu ta ted

Il| |lI|| [t][|l

PFOS Refercnce Information : Directive 2006/12ZEC(1) May not be placed on the ma*et or used as a substance or constituent of preparations in a concentrationequalto or higherthan 0.005 % by mass.(2) May not be placed on the market in 6emi-finished products or artictes, or pad6 thereof. ifthe con@ntEtion ofPFOS is equalto or higher than 0.1 % by mass calculated wilh €ference lo the mass of structura y ormicro8tructurally distinct parts that contain PFos or, for textiles or other coated materials, ifthe amount of pFosis equalto or higher than 1lg/m'?ofthe coated mateiat.

cmFiy f:F,,1r ir!, , li ++1r t11{t ,Jli,ii1rli "- i! i . l-,1+*lr14r r i ljt r:4 . .1.4:.,J11!+ftsd@!mdttr$uadbyfucmp'ysUb]dlotGa€€cmdi6€dS*

' € d ed 6d '^r.md m @dad *s maorGnbtud;np . i s b L t i s r o b c r d a d b s d m

jrrr ;1 +ir l*j?,,ni+$610r)rer7ef 1e1d2r2qd7 {-!{,<h

Test Report No. : Ce12O11122922 Date : 2O11\OZ24 paqe : S of 10

COLUMBIAN CHEMICALS COMPANY18OO WEST OAK COIUMONS COURT MARIETTA, GEORGIA 30062

ICP.AES

Sample Material Digestion Acid

Seel, copper, aluminum, 6older Aqua regia, HNO3, HCl, HE H,O,

Glass HNO3/HF

Gold, platinum, palladium, ceramic Aqua regia

Silver HNO]

Plastic HrSO1, HrOr, HNO3, HCI

Others Any acid to total dig6tjon

llt] tIltflfitttt

'1) Thesl? samples were dissotved totalty by pre-conditioning method according to betow flow chart.(Ci- tesl method excluded J

2) Name ofthe person who made measuremeat Climbgreat y€ng3) Name of the peron in charge of fie€surement: Troy Chang

srslrsdd Th s r€d r@i eind b €cdF ry { . r r r l j i ; ! , ! r i i : l : i { i , , ; ( ! l * r l i . : r l r i . t 4 / " j r + r : r ' L r I r ' . 4 } f i ' i l .rhEd@hdE]sdbyt€comts

g t ] adbTmsandcsd ioBbE

nndberqdu.detce,Iiful*ihod'oao.yollas{€1oiol|116@d.^tol

'., ,, lir l+i1 !i+s6 D!!etr trs6r0nzstt wle{on

Acid digestion by suitable aciddepended on differedt samptem€terial (as below table)

Microwave digestion with

HNO3/HCr/HFAdd appropriate amountof

digestion reagent

Heat to appropriate

temperature to extract

Cool, filter digestate

through filter1) Alkali Fusion2) HClto dissolve

Add diphenyFcarbazide for

color development

measue the absorbance

at 540 nm by UV-VIS

MMb€' or de sG5 6,@p 1565 r{)

Test Report No.: CE12011t22922 Date:2011t02t24 page:6 of 10

COLUMBIAN CHEMICALS CO[/|PANY18OO WEST OAK COMMONS COURT MARIETTA, GEORGIA 30062

Analytical flow chart of halogen content'1) Name of the person who made measuremenl: Rita Chen2) Name of the person in charge of measurement Troy Chang

tl| t[] t]|lIt

Sample pretreatment / Separation

Weighting and putting sample jn cetl

Oxygen Bomb Combustion / Absorption

Dilution to fixed volume

Analysis was performed by lC

b1o r6dd t sbe r@d ennd ba BcomtsnvN:lFl,,tiir!.rill+r:r1l1i:;liilrrd':ed r-il++}{r-1\E Jii;t1-, ? t!']rl,t4ft3fud 6 66ugd bylh6 conF

p . i 3 b ' 9Gro 6Cr61 'd6s tum

Test Report No.: CEl2O11n2922 Dale 2011t0i,24 page: 7 of 1O

COLUMBIAN CHEMICALS COMPANY18OO WEST OAK COMIVONS COURT MARIETTA, GEORGIA 30062

trl]tI|t][ttttll

Analytical flow chart of Soxhtet extraction (GC/MS) procedure

1) Name of the person who made measurement Lydia Fu

2) Name ofthe person in charge of measurement Shinjyh Chen

I Test ltems: Phthalate . Benzotriazote . HBCDD . Np , DBBT

Organic phosphorus compounds

DaE

comFn, rlrlj. ! i. i N: . I *+!l ilti lt r{lrjrii 9 6 - f-it++tr41\. .lt'1rr;t - . , i' ruirr{.ysuqdd b rGffi condrtrsor s

F i s b l y E l o | 9 c | { l a d b s ]

Test Report No. I CE12O11i22922 Date | 20'l1lOZ24 page:8oftO

COLUMBIAN CHEMICALS COMPANY,1800 WEST OAK COI,IIMONS COURT MARIETTA, GEoRGIA 30062

Analytjcal flow chaIt1) Name ofthe person who made measufement: Roman Wong2) Name of the person in charge of measuaement: Troy Chang

r Test |tems: PBB/PBDE, TBBP-A-bJS

FiFtlesling process ----.} Oplionalscreen process --... Confimalion prccess - .>

Screen analysis

rtll|ltl|][atlt|l

i@

vrt

tSample exfaction method

Analysis by GC/l'rS

lssue R€port

mpe(3lbdd rh€ r€d,.Fn 6nd b€c6€ ry ' l + / t t r : l r r ' r i 11 i : : 1 : , + ]L l : ; 4 : l r l i i ! f . L i i i l i r i i l - 11 . ] L , " dL r ' n l ' , 1 r t u : r 1 .n6d@ndF$u€dbyth€company&br.dlo6Gs.€|cddionsois

s*j.d b rms rd c6di dE ror E

fu04orfahfelmdde6Mtor

l:+r .r +:!, lirri, irt rss6lorrrre

Test Report No. : CE|2O11 n2922 Dale : 201 1 102124 page : 9 of .j0

COLUMBIAN CHEMICALS COI,1PANY18OO WEST OAK COMMONS COURT MARIETTA, GEORGIA 30062

Analtrtical flow chart of Soxhlet extraction (LC/MS) procedure

1) Namo of the person who made measurement Lydia Fu

2) Name of the person in charge of measurement: Shinjyh Chen

rTest ltems: PFOS/PFOA , Benzotriazole

Sample pretreatmenUsepa€tion

I

UEIA

ll][tIt Il]

mp6Glrerdd rh6 bd FFn 6nd bcmFry *r!,j!;tErl.i i!Fi:1:i{ir,; i\rlrl*, r: i . ,}itsi5rr4r:\ ' *r-+{. riI:rlrt!iil.f t 5 d d m d 6 s d b y m 6 c o m F n y & b ] a d l o i s G s s l a | c m d t r o i s d S

3uqed b ]m3 Td cndhoB br E

s F 6 b | l y s l o b c i a d a i d l h 6 d e unnd be r4roduoed erood ntun e Dur

.r.r!.: i:il l i ie ! t, M 10r!re rr r i s6 orrs rr !^ae<oD

Test Report No. I cEt2}11t22s22 Dile:2011to2t24 pase:10of 10COLUMBIAN CHEMICALS COMPANY18OO WEST OAK COMMONS COURT MARIETTA, GEORGIA 30062

"" End of Report "*

llLl[ t [t]|l

mp€ls) leied rhf r6d r6@d einor b€{:i i ;lrrrri::!r:. f .iliEiki.l :-\ lrJ,l, -:1 1rlfi.'r

3!oed 1o f*h6 nd cndi oc ror E

rh6,,'d'sandob 0aro3uid6.lbr€ ^ddbe@drdorcer nrur *rho!

Test Report Number : TWNC00190468

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 Of 7 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. ��114 �� 423� 8�

Tel: (+886-2) 6602-2888 2797-8885 Fax: (+886-2) 6602-2400 6602-2401

Applicant: Littelfuse Inc. Date : Feb 01, 2011 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description: One (1) group of submitted samples said to be : Part Description : Nickel/Copper foil (for RLD) Date Sample Received : Jan 28, 2011 Date Test Started : Jan 28, 2011

Test Conducted : As requested by the applicant, for details please refer to attached pages.

Number : TWNC00190468

Test Conducted


8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Testing Item Submitted Sample

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND


Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401



Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility Of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Jan 28, 2011 Testing Period : Jan 28, 2011 to Feb 01, 2011

(Ⅱ) RoHS Requirement:

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.


Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

(Ⅲ) Test Method: Testing Item Testing Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content


2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)


5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by ion chromatography

50 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample


Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

(Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List Of Appropriate Acid：

Material Acid Added For Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part


Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

(Ⅳ) Measurement Flowchart:

Test For Halogen Content Reference Standard：EN 14582

End Of Report

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the flask at room temperature

Transfer the absorbent into a volumetric flask


Sampling/grinding or cutting

Analyzed by ion chromatography


Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

Photo







Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401


Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : Copper Foil(for SMD) Date Sample Received : Jan 28, 2011 Date Test Started : Jan 28, 2011

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Number : TWNC00190474 Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401



Heavy Metal







Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401



Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected










Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401




2 ppm

Lead (Pb) content


2 ppm



2 ppm



1 ppm



5 ppm



5 ppm


50 ppm





Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401





Sample preparation



Cd/Pb/Hg

Analyzed by ICP-OES





Cr6+




PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample



Negative *2









Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401



End Of Report











Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

Photo







Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

Applicant: Littelfuse Inc. Date : Feb 10, 2011 LIMA Technology Center,

Lipa City, Malvar, Batangas

Sample Description: One (1) group of submitted samples said to be : Part Description : Tin(for SMD) Date Sample Received : Feb 01, 2011 Date Test Started : Feb 08, 2011

Test Conducted :



Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401


Testing Item Silvery Metal

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content 14 Mercury (Hg) content ND

Chromium VI (Cr6+) content (mg/kg with 50cm2) Negative

(< 0.02)(#)

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation

was not found at the time of testing. # = Due to the insufficient sample area, reduced total sample

surface of 10 cm2 was used and the dilution factor was adjusted accordingly.


Date Sample Received : Feb 01, 2011 Testing Period : Feb 08, 2011 To Feb 09, 2011



Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm)



Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401




2 ppm

Lead (Pb) content


2 ppm



2 ppm


With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer.

0.02 mg/kg with 50cm2



Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

(Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard：IEC 62321 edition 1.0:2008


Material Acid Added For Digestion

Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4


End Of Report




Cd/Pb/Hg

Analyzed by ICP-OES





Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

Boiling water extraction

Metal Polymers / Electronics

Negative*2 Confirm the tested samples are totally dissolved


Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

Photo

,r{a+E+Test Report i t & ( N " . ) , c E / 2 \ r r / 9 o r 2 a A S ( D a t e ) : 20l l109/08 FjR(Pase) : l o l 8

Validi nownith scs

tfl[ tru ||:||llnli6a*XqAA FAa 6lCHUNG YU II'DUSTRY CORPORATION

+bEitr+}lf €+t&:ft6r8&6]8, SEC. 3, I'EN.PING RD., PING-JENG. TAO-YIJAI{, TAI1',{N

&'?Zt8(S.rpl . Descript ion)

& , ? 4 l i ( S t y l . / I t . ' N o . )

4n4 E J& (s , .pL . Rcce iv ing Date)

t f l ! [ * ]E ( res t i hg Per iod)

, , .Ti i l i&e6*fP ' t&, LtstrP +4*.*.*P*tsieT (rh" forlo' i ls sarples eas/eeie subii t ted aldi de t r t i f ied by lon beha l f o f the c l ien t as) :

: IN((zSR-150)s

. zM- 40onT, Z{- { 00$l (HF). Z lF40ol IF- r , Zv- 40or tF(N),zM- 40oiB,s\ ry ,

{NA, l l l i , r r { , $ \ , rL ,$/H(N ) , f lH(H),13A089 , rc- l { ,PC-C , tC-$/ ,10otr ,9I ,SW. 2 0 l l / 0 9 / 0 1

| 2 0 L L / 0 9 / 0 1 T o 2 0 1 1 / 0 9 / 0 8

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p6(3) 16dad hE rad cpd €nm1 bacompany i i ; ! I t ] l , r r _ n t I i i J i t i j t [ i : 1 , : . ] t i i : i t l r . , r , . I i r \ 1 ( .

, rJr,rri rlrr,r_'.i!,\" l6eoarr

f r n - T - F ( P l " , " " . e f e r t o n e x t p a a e s ) .

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Chrob iun Cr (VI ) , PBBS and PBDES cohp ly v j lh the l im i ts as ser by RoHSD i . e c l j v e 2 0 l l / 6 5 / E U A n n e x I I i r e c a s t i n A 2 0 0 2 / 9 5 / E C . )

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nliaEt&aatE?i4clilJNG I'U II\'DUS'IRY @RPoMTIoN

,t Ei S. +Alii € +tA:fA6 r 8 *618, SEC. 3. ITN-FING RD., PING-JENG. TAO-\1JlN, TAIJfA\

rlrflt[lfl ||trr

t i * l ** (Te6t R€sur t s )

,q i{,q!& (PART Nd\n)No . 1 6 at$,g ($HrrE rN]()

;ul{{ a +'fq(uni r)

trlltti* ,*dxlfitr{t(r@L)

,* JF( R e s u l t )

ittE.{t

(L iE i t )N o . l,6 / cadmium (cd) re/kE ++rEc 62321,, 2oo8?:t, ,(&A*BA€

*.ff+*4l,t,*&&irl. / rvith rererencero IEC 62321: ?008 and per forned byICP-AES.

2 1 0 0

S / Lead (Pb) ng/ks +4IEL 6232r. 2008t*, 4&,6itA€*,F+44tt*&htd. / I l / i th rerereiceto IEC 62321: 2008 ahd Per fo rn€d byICP AES.

1 0 0 0

*. / Mercory (Hs) ++rEL 6232r. zoo8rii, ,x$^**e€{ ,F+&4}*,*A**, i1. / $i th rererencero IEC 62321: 2008 and per fo rned byICP AES.

1 0 0 0

n1f ,& / Hexava len t chron iuhc . (v r )

t-+rEc 6232r. 2oo8rli, r1w-Vlstf,iq./ w i th .e fe ren .€ ro IEc 62321: 2008and per fo rned by Uv-v IS .

2

7rtlt*+:q, /H€xabromocycrododec2ne (HBCDD)

( c A s N o - : 2 5 6 3 7 - 9 9 - 4 )

, !*us EPA 354ocr*. ' ,A^1anfr/g*A, l* , r1. / n i th ref€rence ro us EPA3540C nethod. Analys is was per f6.nedbv rc/MS.

5

,FX:P!TYf *T!B / BBP(Benzy l bu ty l !h tha la te ) (CAS

N o . : 8 5 _ 6 8 - 7 )

t+EN 113??, ,r. f,.*E,g +f d, / { r*{ '*;tl: . , / S i t b r e f e r e n c e r o E N 1 4 3 7 ? .Ana lys is was pe . fo r red by GCIMS.

0 . 0 0 3

t l iX:f &- (2-L*.2&)* /DEHP (Di- (2-ethy lh€xy1)p h t h a l a t e ) ( C A S N o . : I l 7 - 8 1 - 7 )

% +tut 14372, 4 *rlE,E{d,/L*&it,nla. / x i rh .ef€r€nce to EN 1. !3?2.Analvs is was Derforb€d bY C€/MS.

0 . 0 0 3

SX:P*.:.*.+& / DIDP (Di-i sodecy i p l tha la te ) (CAS No. :

2 6 7 6 t - 4 0 - A )

'+EN 143?2. / ft"*E & i.fd,/ f i$A&ixl<-. / f l i th reference to EN 14372.Analys is was per forned by CclMS.

0 . 0 1

con* i y + i r r l r i l , : i : r i ' i U ' r i l r r l r ' , l i i r , , l 3 * i i l L \ ' i ' ! . r . . - f . r n r i ! 'Thsdofumenl6'sdbybecompany&qedbbG€mraLcodloftolseM6pn^Eddvel*t,!'i,deo.cq

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nlntrf ,ta4'PEiN 51CHI,NG YU IN'DUSTRY CORPORATI O!"

}l6 *+ jItr'.re+!&:46 r8tt6T8, SEC. 3, YEN-PING XD., PING-JENG, TAO-\UAN, TA1WAN

3 0 f 8

l [ t]l[[tt]ll

,rl*{ a +&(Uni t )

agt*( € thod)

t;*{arltE!llt(uDL)

s*( R e 6 u l t

*{EC

N o . t$lt:Fd:++IE / DrNP (Di,isononyl pht ta lar€) (cAS No. :2 8 5 5 3 t 2 - o )

++EN r13iz, ,\ *"ta E tt&/ X t*lt &t l<- . / S i th .e fe ren .e to EN 14372.Ana lys is sas per fo rn€d by GC/MS.

0 , 0 1

*1i:fd:ra+!t / DNoP (Di n-octy l pr thalate) (cAS No. : t t7-8 4 - 0 )

++EN 14372, /ft&,? i6{,/frt*dt$rxl<-. / Wi th reterenc€ to lx \ r 14372.Analys is sas per fo.ned by rc /MS.

0 , 0 0 3

S*:f d:TrE / DBP (Diburylp h r h a l a t e ) ( C A S N o . : 8 4 - ? a - 2 )

++EN 14372, vzi 'EE fr&./ g1*6.*it lZ . / I f i t ! . e f e r e n c € t o E N 1 4 3 7 2 ,Ana lys is qas per fo rned by rc /MS.

0 , 0 0 3

ttrtfrl# / suD of PBB6

44IFL 6232rt 2008r)1, ,,t AlaE&l*/f *A, t* ,e | . / { i th rcrcrence to IEc6232Lt zAAa and pe. fore€d by GC/MS,

l 0 0 0- *S* / vonob.onoh ipheny l 5: i * t l * . / D ib ronob iphenyL 5: i l 4E / T r ib ronob iPhent t 5@it#S / Ter rabromobipheny I 5t i ^S l / Pe i tabronob ipncny l 5^*#* / l€sbromobip le ry l 5-L ; l tE / Hep iabronob ipheny l 5^- ; l# iF / o . tabromobiph€ny l 5/L;at+ / Nonabronob 5

+t*t:F / Decahrooob 5t*ttrr*fr / sud of PBDas 1 0 0 0-,!tt*at / rlonob.onodiphenyl etber 5: ; l4XEt / D is romodipheny l e rher 5: ;Ad$6 t / r ! i b roDod ipheny r e the . 5€&#*A { / Te t . ab roBod iphenyL e the r 5i t *SrAAt / Pentab iomodipheny l e ther 5n* t t *a t / f lexabromodip leny l e rher 5-LA#* l* / Heptab.oEodipnenyl e l !€r 5,\;l#tri6t / oclahronodiphenyl e th€r 5, t , ,1#*6 t / No 'a6ronod ipheny l € ther 5

+* ls f6t / De.abronodiphenyt ether 5

cmoany r : ; l | r t r : ] l i f t ' r . , r1 r ,1 . r l , i l l { L l i . , l ' l i i l t ! , | -1 - \ i r . ' r l l r th l -iy subled 1o r ceidaicdid rois d $

s d c m | o l h e l m i b i m o ' € b L l y .

spoisb' t sb b criad aid rh E do@

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*tEl #+,Irt'r€+r3:ft618fi,618, SEC. 3, ITN-PINC RD., PING-JENG, TAO,T]NN, TAISA]{

f i l i (Note) :

1. nglkg = ppn i 0 , l r t% = 1000ppn

2 . n . d . : N o t D e i € c i e d ( * . l b * )

3. vDL = M€t lod D€rect ion L imi ! ( t * lA i f l r l f&t&)

4. , ' - = Nor R"sulated (R{, }&{ i )

comoan! r : " r r l r , , i r l , r ! - { ' r r . r r , "J i i l n i i l i : r " ; ; i r : ! t ] i , 1 r . r i . , r r i ] ! * '

,d ddoic dmar doon$6. $bj i ro h. 'mrlalioi d 8bit.

|ll Ilr mru t

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fi|fi,*r+Test Report

ft6(No ) : cEl2011/s0128 E*(Dat€) '

nliaa*&AatEa4CI{I,NG }'I] INDUSTRY CORPOMTION

dBE ti+JIii €+r3:ft618fi618, SEC. 3, YEN-PING RD., PING-JENG, TAO-I'IJAN, TAII',11,I

r)

2011/09/08 q jk(Pase) : 5 ot 8

llr]|l]|l[[!trt]l

43)

iuertrT$)ff,anatFr+ , ilF giA8t+. (,rfir&rli{z*Srf ) / Th€6e sslnotes $€redissol!€d lotatty by pE{orditioning mehod according to betow iolv ch.n. ( Cf. rest mehod exctuded )

&^ I : *+1t / Name or the p€rson who made measurcment crimbgrear ya.gtri A I *^ r tt4i* / Name of the pelson in charge ot neasuremenr Trcy Chang

t5AlE+€f.fr +&41*,rld / rcP-AEs

*sitf / Samde Mareial ,filLa&fi / Diqslion Acid

stel. 6omr dumlnm sdliierrr<,4d, t*, 5.5.*, qt,^ /Aoua €oia. HNo' Hct. HE H,o,4*.inan / HNO,+IF

Gold. daiinum. D€lladium. ceramic,[ / Silver {ft / HNO!

4ft, ti,+ da, tit / H,so.. fr,G. HNor Hcltb ̂ &f,*4'.ZtEtf I Mt 3cid lo lotal digeslion

p3(s) 16rad rhsrad Gpd€nid6comD. r y , i l ! , r . i r , E_ , i i " r r i l J i ! , r - : l , i r : . l r i i : ! l - l i r 1 "

. , - . r i ' ! * .

tr*'*fr{s / Cutins . Plepa€tim

jtlg.ilsg! / smple M€asuMent

4&f ir Fl +ts 6trf f, 6 ttr!{f, Atlnit1i,fiL(r' T Irt,ii) / Add digeslion by cuitabte acid deDeftted ondm€.ed sarnple maleiat (as betow tabte)

,l.t/t */5.5.&6t fr*rtlr, /MicroMve dig€ston lnh HNoy'HcuHF

,"n!4Aftt&4li,flu++ / H€rt to app.oFiale

fller digBrare though filter

,'^*en]fia /Add

^xrtx-aLk'.**. 'tjrJ|{saitri 540 nm At4.

absolbance 61 540 nm by

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Mem6sd,hercscrclp6G55Al

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?b ffi tf + jF jt r€+ r&:ft6 r 8*618. SF'. 3, YEN-PING RD., PING-JENG, TAO-]'IJAN, TAIIIAN

*4+n+f&aD /Analytical flow chart of Soxhlet extraction (GC/ S) procedure

r flfi/i!F : fi$ry / Name of the person who made measurement Roman Wongr fl:t F l./. : tFEF / Name of the person in charge of measurcment: Troy Chang

(rifi,{ E: q!l,l' *J.:'ai{ua&. i*rt+:n ' *& ' + ?*:it:*,f ?R' '

6 &*YEh / Test ltems: Phthalato'Bonzotrlazole'HBCDD'NP'DBBT.Organic

phosphorus compounds)

*E / Data

npre(s) re*d frs ren 'epo^ enior bcomF iy h ; r I i ! . i l ' i , r ' 1 j : . : - 1 t ) i i : i . t l i { l i l l r ' , r " . ] - i l i t ! : 'rb";;'d6 $,ed by h. c"'p,.y $qed b b c$.,.rcod, dis or si.,."d.i, omd e"i'*ts *b"

m ! sd w hn sa,ifrB d ced! m' Mgbity6rorsc,eil5^dssdotumttu;

"rhb and os,od,oB dd* h" t,

&8"fr &tgt++*. ISample pretreatmenUseparation

6",i+ef(n * Ji+R* /Sample extraction by soxhlet method

+8k;R6iftf /ConcentEte/Dilute Extracted solulion

n./Bnfrn;*&.+& lAnalysis was perfomed by GC/MS

.: I:l l-:r I {liir,.:i+s6loaxee

rfla#+Test Report

fi6(N" ) ' cE/20t1'/sar28 E s(Dat") : 2 0 1 1 / 0 9 / 0 8 E * ( P a s e ) : 7 o f 8

,r l i6a*EDf B.a 4CIiIJNG YI' INTESTRY CORPORATION

+t tr 4i +iI i''r€ + !&:lt6 r 8!t618, SEC. 3, YEN-PING RD., PING-JENG, TAO-WAN. TAITAN

Im[tI| tttl|]t

+fi-ft€n / Analytical flow cha. iri*.,,.tl : ii'!9# / Name of the person who made measurement RomanWongr 4S F t/. : *8* / Name of he percon in charge of measuremeni: Troy chang

(ull't E (Te6t rtens): ,*t*Jtttt*n, ella'-A4 / pBB/pBoE, TBBpd-bis )t,ti|li{t* / FiEr 6rns p@$ ------t :t44**{4 joproErsc*np.o@ _n,r riea* /confimdon@@ _ r,

trrlrlf / Screen analysis

I +r.a,t*r** i concentat"io'tu" e"traa"oGi--l

+Rtt4E / Filter

knFrrtn*+*$.^ft / Analysis by GC/MS

lssue Report / i*tit+

or.G) 8d rh s ied @od €nnd bc o m D a n y ; r : ; l r , 7 r ' ! - 1 ' r . . i r r ' J : , i t r * i r . . r r i l : r t l \ I r ' , r l r r l r a .

chenc bF 13 wlchsd Fo?d wd! idri d zoDe N€! tdFi c]ly' t!'win rri"r ' ii ri, J:-i r-{1.; , ri,l + s610rr* rrTe i + 336 iori:ae r2r7 ww rg*on

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f i6 (No ) : cE/201r /e0r28 EJq(Date) :20 t r l0e l08 E* (Pase)

nl ,i6r- * x{Af IF.a 6fCHWG YU INDUSTRY CORMMTION

't Ei $+JI1r.r€+r5:.ft6r8th618, SEC. 3, YEI,i.PINC RD., PING-JENG, TAO-YUNN, TAIW,{N

- . #+ttL (End of Report) **

c @ € i y h " f r I i r i - f l ' i , r i r L i d l l i r 1 i . I f , 1 1 , ! 1 1 i i r . ' r l r t t l l 'ayaqedb G ceieGr cond r ons d s

s d'am ro rht rn'blm d 'ahL !

@ i3b l y ] 9b t c l ed ,nd lhsdoam

8 0 f 8

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dtEi ti+4f €+a:$6r8fi618, SEC. 3, ITN-PI\G RD., PING JENG. TAO-YUAI{, TAII'AN

&t€(No.) : CE/?01r/67429 ES(Date) | 2077/07/04 F l * . ( P a 8 e ) : r o i a

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||]u|||| lttt$l

trTd*,*s46*Pt!t, -8- A *t +*nf,*P 4l l8{pT Gre folro' i !8 sarpr€s 'as/ '€r€ subuitr€d andi d e n t i f i € d b y l o n h e h a l f o I t h e c l i e n t a s ) :

I t&**(s, 'pr. Des.r ipt ion)

i i .S4f i(sryLe/I ren No. )

4t{+ E S(sahple Receivins Date);(3iSE:(Test irs Per i od)

rNI( (zsR-t 50 )i{zl!-40ori lF, zv-4001rF-1, an-100$I (N), z{-400sts, 13A089, rc-iy, Pc-G,IC-W, 100$, StV2 0 L t / 0 6 / 2 7

20LL/06/21 rO 2At t /0? /04

; i t - 'F -F (P l " r . . ie fe r ro n€x i paces)l l 'g*(Test Resul ts)

$in$lrdttSlfnrd for

Chc|dr.l labo|tto.t - T.lDCa

mPr.(s) bsEd rh 3 b3k@od enior &comp.ny f : | , , . : l r ' L1 l i i i r . ' r j i i r r r l t l i : , .111 ic r r ' r in .4 .J ' !1 , r i i1 r !_r l ' i t i ' . . . , * "aq* .co .o" ry4qsdbb@isra |co id ld i3o ls€

s.;ruhamd d,qd.B m#h6 ra ..d ba €prclu@d€tGpr Ln,u, wsou

- r r r r ; t r r : - 1 l 64a r r o i qNe f r rF . { , t aw iD , r ' L i l , r ! l ? - r a . l s i { , 1+e6€ '? ) ' ee t r ' } s

,r{H,*E+Test Reportnli$a*&rlatE?aCHIJNG YIJ INDIJSTRY CORPOMTION

'tEirG+*lF€+t&:&618t8618, sEc. 3, YUq-PING RD., PING-JENG, TAo-wAN, TAIWAN

tJl l ** . (TeBt ReBul ts )

* 4 ( N o . ) : C E / 2 0 1 r l 6 ? 4 2 9E S ( D a t e ) : 20rr /a1/01 F*(PaEe) . 2 or 4

tl][tttlffi tt

r'Jit$y'n (PIRT Nr'l'lE) No. r 6 e.f {{# (sHrrE PAsrE)

iri{{ E(TeBt I teos)

+e(U! i t )

i{t* t*{t jdfiFE(MDL)

s*(R€s ! l t )

N o . l

i * / I la losea

f i t ( f r , ) / Halose!-Fl lor ine(F) (cAs No.: r1762-91-a)

4+Bs El.r r4s82:2ooz, D(*+EI t&,+*8. / { i th reference ioB S E N 1 4 5 8 2 : 2 0 0 7 , A n a l y s i s w a s

50 a2

Ai (5") / Hal osen-c! lor ine( C l ) ( C A S N o . : 2 2 5 3 1 - 1 5 - L )

5 0 5 8 6

&* ( i1) / Harosen-Bronine(Br) (CAS No. : 10097-32-2)

5 0

& * ( d f ) / H a l o g e n - I o d i n e ( I )

(CAS No. : 14362_44-8)

5 0

f t i i ( N o t e ) :1. mglkg = pph ; 0 .1rr% = 1000ppmz . n . d . = N o t D . t . . r . d ( * r * * )

3. l lDL = M€thod Derect ion L in i t (Z*{RUEPEId)

p6(3Jbr.d rhs bn repd diior becom@y i i r f r l i l t i ! - l ' r . l r l i i l ! n l r r l 1 ! , : - ! i 1 i r ! r t : r i : r . , 1 . r . r l : l t r r * .

iy subred b h 6eneE condsoB d s

h€r€oi Gi.cG rhe comFrv s ind'nos d

nndbaEFdu€d3l6plnlu]w]b@

rF|l'd,*t+Test Reportnl#t*&rlArE1i 61CHUNG YIJ INDIISTRY @RPOMTION

dtE ti+4t r€+r&:&6 18!f,618, SEC. 3, \EN PING RD., PING-JENG, TAO-WAN, TAII!'AN

ah4(No.) : CE/2011/67429 Es(Date) | 2 ' r r /07/01 F*(pase) : 3 of 4

tlff[]|l Ilttr||l

i *+fi'fref / Analytical flow chart of halogen content1) Xld\,,\F : *g* / Narno ofthe person who dlade rneasurerEnt Rita Chen2) :r{dt & ll. : 'i-*4 / Name of the peEon in charge of rEasurenEntr Trcy Chang

*+E )f(6.Nfi tAmlysis was perforred by lC

conpa i y : : l l r r l t r i - r l ' i , r 1 ' , 1 : l n i l q i r , r ' 2 ' i r ; i 1L1 r 1 r . i 1 . . . l r j r j { ] ! .iysubledrdbGe^a6 cmdddnsd setoepldadda,eata!a'6deon€q

.L , r : 1 r . : , r i l i l , . l + s6o r r r ee tTe r l s6LDAree t t ww$*on

,rl|-d,+R+Test Reportnl ila * xqrla rF.a ;fCHUNG \U INDUSTRY @RPORATION

ttE *i+Al'F€+t6-1+1618ti618, SEC. 3, IEN-PING RD., PING JENG, TAO-WAN, TAI\]'AN

f t4(No.) , cE/2011/6?42e E&(Date) : 2 0 r 1 l 0 7 l 0 4 F * { P r g e ) : 4 o f 4

l I |||lU tt]lrr

c n o a n y r : r l ! / t r r , r L n ' : , r r - j ; i - j t : . " i

^ , : , , L . , . . . i i p r l

' " iR***E(n'a or Repo.t) **

--L ltl-,r f :i.f11,,i+4610?lreetTer+s6io?l:,ett wrlsi.on

67429







Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401


Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : Ink (Acrylic) Green(for SMD) Date Sample Received : Jan 28, 2011 Date Test Started : Jan 28, 2011

Test Conducted :



Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401



Heavy Metal





Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401



Halogen Content Fluorine (F) ND Chlorine (Cl) 283 Bromine (Br) ND Iodine (I) ND

Remarks: ppm = Parts per million based on wet weight of tested sample =

mg/kg ND = Not detected








Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401




2 ppm

Lead (Pb) content


2 ppm



2 ppm



1 ppm



5 ppm



5 ppm


50 ppm



Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401





Sample preparation



Cd/Pb/Hg

Analyzed by ICP-OES





Cr6+




PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample



Negative *2







Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401



End Of Report









Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

Photo

Validi

Please

xlBt#+TeSt RepOft

tt6(No ): cE/2011/652s5 Eli(Dat€) '! 2ar/a6/23 F*(Pase) : l or a

&!tt+i{e?r}aR't 4ADVANCE MATERIAIS CORPORATION LTD.

it El tf &i64 f ,1, Jt t*:+42 5 6 61 6 8*NO. 168, LANE 256, CHUANG SAN NORTH RD., SEC- 2, YANG [IEI, TAO YIJAN HSIEN, TAIlll,AI

, ' r -F,r l {{ [$4*8P€*, E * 5P +#-i t lE+,P r l* trT (rh. for lor ins sadples,aslv€'€ 6qboitre<l andi d e l t i l i e d b y l o D b 6 h a 1 f o f t h e c l i e n t a . ) :

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: PSR-550B/[S-558 GREEN

. 2 0 L L / 0 6 / L 6

t 20 l l /06 /16 TO 20 l l /06 /23

; 6 , { T - q ( P l . , " . . e r e r t o n e x t p a g e s )

r l . h e n c L F 4 I a p e . r r i v s / t ' . 1 l i r r ?

rtlr [tllllfl]I

&S2iS(sanpte D€sdipt ion)

l lg416,(sty l e / I r€n No- )

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jdt l rgJR(r.s t R€,u I ts)

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p 3G) €srd rh 3 rsd €pon cinor *cmp . i y ' t : i f r i 9 t , . f -F i , r l l i ' j l ! f i r , l i . I : l , L i r . l r t \ . i n - n l | t u l .rhs doonsl 6 sEd by se conPa

nd6mnfdonandiunsddm'sesd3ps jb ' l }E l o { sc |€dand lh3doa

ntH,#+Test Report i t ( N o . ) : C E / 2 0 r l 6 s 2 9 5 E J q ( D " t . ) : 2 0 1 1 / 0 6 / 2 3E * ( P a s e ) : 2 o f 4

&*+*te/rlf Ra 4ADVANCE MATERIAIS @RPORATION LTD.

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irl-its{n(PAxr NA\E)No. I

rlltl||tti |lnl[

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{{{ a +&(Uni t )

j{idtri tr*.fir'1*E E{toDL)

e*

N o . l'rtA*+:e, /sera6.oEocyc Lodod€cane (HBCDD)(CAS No. : 25637-99- , t )

t+us EPA 354octii, ,tnaaEfi/q*&it , r i . / wi th refe.ence ro us EPA35.10c nethod. Anzlys is ,as per lo.nedby @/MS.

5

Strij.PliY*ATlE / BBP(B€nzy l bu ty l pn tha la te ) (cAS

N o , : 8 5 - 6 8 - 7 )

++EN r4s72, r,( $,r€,8 +td, / f j*d'i*'rla. / Wi lh re fe r€n .€ 16 EN 1 . t372.Ana lys is was t€ i fo rncd by rc /NS.

0 . 0 0 3

f f i i :Y&:TEB / DBP (Di buiyrp h t h a i a t e ) ( C A S N o . : 8 4 - ? 4 - 2 )

+tEN 14372, ')( {r,1EE*4.4,/ tr;gt*,iA'rla. / I i rh r€ fe rence io !N 14372_Ana lys is was per lo rncd by rc /MS.

0 . 0 0 3

!ftf,:F&: (2-L&.a*)& /DEHP (D i - (? -e thy lhexy l )p h t h a l a t e ) ( C { S N o . : 1 1 7 - 8 1 - ? )

++EN M372, 't nla E *t 6./ F !&#./dtalZ , / $ i i n r e f e r e n c e t o E N 1 4 3 7 2 .A.a lys is was pe . fo rned by C ic /MS.

0 . 0 0 3

f f i i ( N o t e ) :L n g l k g = p p m ; 0 . l w t % = t 0 0 0 p p b

2 . n . d . : N o t D . r . " t . d ( i l A * )

3. MDL = Met lod D€tect ion L in i r ( t ; i lA in l r t tF ld)

c d m p a o y ; ! 1 r r l j l t _ i ' ! I ' r l J i i l l r i , i r , i N , r . + t r r I i " . . r r i , r a r i .ry subted ro b Gene6 condrons or s

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fla#+Test Report f f46(No.) : CE/2011/652e5 E*(Dar€) : 2ai /a6/2x F*(paa") , 3

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ll[| llll tltlt

t*.+rr+&fian /Analytical tlow chart of Soxhlet extraction (cc/lrs) pioc€dure

l g{:{/t'F : il!**, / Name of the peFon who made measurementt Roman Wongr jflA F l,l' : t&.** / Name of the person in charge of measu€ment Troy Chang

()rl*,{ E: qA, . *jr.:"!ltt+4, ',r*rl+:n. +$. +f 4:*:84yn '

6 A4ft+b / Test ltems: Phthalate'Benzotriazole'HBCDD'NP'DBBT.Oryanicphospho.us compounds)

&f i Data

mr!.(s) r.sbd Th 3 bi rsPod €nnor bc o m F f i + J , I r j , . I l i ' i , r i j i l , i r j ' i : i . t l i , l t ! 1 1 : . i n . I r l r n r ' i ! .T h 5 d o a m m l E 3 s e b y h g c o m p a n ' s b j e a b c c s e € | c o ^ d ' d i 3 b l s

s p o n j b ' t i c l o l s c l e i l , ^ d h 3 d @

Lfir-r:. r: i.rii-:.,:ir + s6 o.ree

*fs fi-.€.rcl+t{ /Sample pretreatmenvsepa€tion

&g+4LRE *n +4(}+ /Sample extraction by soxhlet method

+4(ntiG/ti# /Concentrate/Dilute Extracted solution

^1afr&Fi*#.*& |Analysis was performed by GC/MS

rfla*E+Test Report s4(N".) , cE/2011/6i2es ES(D.t .) , 201106/23 F*(pase) : 4 or 4

s*r+&xlDa FF,r 4ADVINCE I,TATERIATS CORPOMTION LTD.

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trrfltI| [t[]r

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p€19 kdad *r ra$ rcpod enior bacompany + r ' , 1 / . l j I q , l r t , r . n j i i : : l , i r 1 , : . tP * i , i i r ! t I 1 . , . i , i r r , ! .

ont ard wLhin ih6 linis or c ren' s ns

, tir: i+dq u)2F,ro f+e

65295

Mfl srdde(s€roup (9{r sAr

Validi nownForPlease

,r{'d,#+Test Report f t 4 ( N o . ) : C E / 2 0 1 1 / 9 4 1 7 9a S ( D a t e ) : 2 0 u l r o l 0 7 F.q(Page) : 1 of 15

st{.€+ItDtrPE?i€1 |r]tIl ][ttt[tlITEO @&PORATION

)ttr rf+3!tJ.* Ea* -tA??*22, KUNG YEH 1ST RD., PING CI€II IN'DUSTR]AL ZONE, PING CHEN, TAOYIJAN. TAINA}I. R. O. C.

t TNl i l* .S. l f 6*,n!&, .E6+,P+*nit* ,P*@trT (rhe fol loei ls san?le. ' .s/eer. subl i t te.r andi d e r t i l i e a l b y l o ! h e h a l f o t t h . . l i e l t a E ) :

# .S2{* (sanpte Desd ip t ion)

* [94* , (s ty le / I te . N . . )

' l (+ t E S(sanpte R€ce iv ins Date)

jr,lii,JH P.1(Tes t ine Per ioa)

: PREPREC

: IT-140GBS

| 2 0 l l / 0 9 / 2 7

| 2 0 L L / 0 9 / 2 7 T O 2 0 l l / L 0 / A 7

;6e-F-F (Pr . . " . refer to ne*r pases) .I i f i , |* j t ( rcst Resur ts)

com@d Nrrltr,r;rrd , .{ i l i i r j.t!!.rD ;l l lngn 9rr i*F^!}1.1:;3rrrr, l.z,I jr l i1xl.ny suq6d b b ctrseicod r ons ol s

l € . . g h c a d e € d 0 ^ 6 u . d 6 1 6 6 t 6

:-,5, ;1 +:r l|ri:rtr36LDrrst, f +s6ior)rreraT {w4'.on

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Clto aC L.6ot to.V-T4d

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sli.€+xqg)trFE.r a rl|l|||afl |ltttllITEO @RPOMTION

dEEi li+ jlii r.* E.r*-r&22#,22, KUNG YEH 1ST RD., PING CHIN IN'DUSTRIAL ZONE, PING CIIEN, TAOYUAN, TAIINN, R. O. C.

l l$*(Test Resur i s )

,ll;{,S{n(PAItr NAl6)No. I

eG)r6dd ftsiee@d€mdb'4cm€ry *i:ri!n4 ..8.'l+:' +ltii : ;i lrli ts-. - 1..1.!+F^rr\E ii+t. I r-'| 11414f tsddmd€sdbys€comts

g ] h ] . d b r e f f s s n d c m d i | o B b l E

sFEbLq sb k crsl and h s 6m

lLlaJr :ur{it il rs6 uPreta.+3e or)rBrt \!@e!@m

*e.4ii (\€tl,jl SHEE"I) (€gw€isht: 16s)

rld,{ € +ti( U n i t )

d$,rn ,r*dJ*r E4tool)

sltr

N o . 1

J l / c a d m i , , ( c d ) +trw 623211 2008t;i. ,x6&ttA€*,F+*4+rt *d,Ajr l - / with rererenceto IEC 62321: 2008 and per lo rned byICP-AES.

tE / Lead (Pb) 2

*. / Ner .ury (Hs) 2

^ l l r ' / Hexavalent chroni"hc r (v t )

++rEc 6232\ : 2oo8rii, 4w-vrsl6jtl./ l r i t ! fe fe rence to IEC 62321: 2008and pe . fo rned by UV VIS.

2

4 / A r s e n i c ( A s ) ng/kg 4+us DPA 3o52tii, 46&l*e€f,F+**tt'+f;,lhtrl4*t. / lvi th.e fe rence to US EPA Method 3052 fo r

Arsen ic Conten t . Ana lys i s wasperfo.hed by Ic.P AEs.

lF / Ant ino.y (sb) 4+us EPA 3osoBtil, r/AA*A€*.&+*#t:*d,&)tl$At - / witnre fe rence to US EPA Method 30508 fo r

A n t i h o n y C o n t e n t . A n a l y s i s v a s

pe.forned by ICP-AES.

a^|L: - l f / Ant imony t r iox ide(Sb?o3) (#) (cAS No. : 1309-61-1)

4+us EPA 3o5oBtti, r/6&*tA€{,F+44tt i*AAirlS6&. ./ nJithre f€ rence to US EPA Method 30508 fo r

A n l i n o n y C o n t e n t . A n a l y s i s s a s

per fo .ned by ICP-AES.

4 / Nickel (Ni ) 4+us EPA 3osoBtii, nrSfr+*A€'{,n+*4tt l*&ii,r!4+!. / withre f€ rence to US EPA ve thod 30508 fo r

N ick€ l Conren i . Ana lys is was per fo rned

by ICP AES,

2

,r{-d,*E+T e s t R e p o r t & E q ( N o ' ) : c E / 2 0 1 1 / e 4 1 ? e E J k ( D a i e ) t 2 a r r / r a / a l F j k ( P a s e ) : 3 ' f r 5

#iEE+M.hA&.ra l [tr]t ttlt lITEQ @RPORATION

' tE*+4lFa*El.f -t422lt2?, KUNC \EH lST RD., PING CHEN II\'DUSTRIAI Z,ONE, PING CHDN. TAOYUAN, TAIWA}I. R. O. C.

rt{ E( les t I te05)

+&(Uni t )

rlrtr*( l te thod)

tti{t jrlbBt(r{DL)

$ *(R€sul t )

N o . l

ld / Bery l I i um (Be) +fus EpA 3osoBril, %t$G*46fi.fr+&4t,t;*d,lixl&+t. / ll,i ihr€ference to us F:PA l {ethod 30508 forBery l I ium content . Analys is *asperforned by ICP-AIS.

2

fr , ' {Edt / nery lL iun ox ide (Beo)t t * 4€us EpA 3o5oBr*, /B6FA€*.&+*4 {,*d,*ajrl&+t. / withreference ro us EPA Method 30508 forB e r y l l i u n C o n r € n r . A n a l y s i s w a sperforned by ICP-AES.

efr,+H,r* l l . / Perf ru6.ooctanes ! l fo .a tes (PFOS Ac id , Meta l

nglkg t+us EPA 3540C: r996ri1, '} ,&laE*t/ f *d,F rlafr.+R-*&ag. / vrirhre fe .ence to US EPA 3540C: t996 m€thodfor PmS Content . Ana lys is wasper fo rn€d by rc /Ms.

1 0

en+* (r*) / PFoA (cAs No.3 3 s - 6 7 - 1 )

ng/ka 4+us EPA 3540c, r999t)8, ,)t *+EE&/tr*Al*d4fi.+.t(J*) 6*. / wirhre fe .ence to US EPA 3540C: 1996 method

fo . P IOA Conte . t . Ana lys is uas

p€r fo rmed by LCI IS .

l 0

*5,alF / Pvc t t t** ,1* ' i f t 4$6)t i* ;r '1. / Analysisvas pe.fofned by FIIR and FL.U'iE Test.

FiAEAf, -A / Tetrabromobi sphenolA ( ' IBBP_A) (CAS No. : ?9 94 7)

4+DrN 533r3ti*, r^^*aEfr&,/\*&l * i i l . / q l i th re fe re .c€ to DIN 53313

nethod. Ana iys is was p€r fo rned by

cic/Ms.

l 0

'r*t*+:&, /Hexabrono.yctododecane (HBCDD)(cAs No. : 25637_99_4)

n8/ Kg t-tus wA 354t)c)i.*, ,]rfi,finfi/f iE&lf i i l . / Yi i rh r€feience to IJS EPA35.10C eethod. Ana lys is was per fo rned

bY GC/MS.

5

oklt6{d rM bd r4n ennor b r€comFry irl Ji ri:iir. . :l il if r l:]{]li ;11!lli!9* . /-l}Fih!-!} r!:L:;r I ? i J:,11} ft;l .Tn3d€mad3€su.dbylh.comp,ny3uqedb6c53€lconntdn6ols

rhd r ridib and d sar os und6r h ta

l : r r . r + i , 4 r1 : . , r {+s6or ) re

fil|a#+Test Report i f ( N " . ) , c E / 2 n t t / 9 4 1 ? e E S ( D a t e ) , 2 0 l r l 1 0 / 0 2 q * ( p , s " ) , . r o r r 5

&|*.X+kttl&x4 l|tlfl|:ll|||| trITEQ @RPOMTION

,tEl tr+lilir* E!*-t422fi22, IiUNG YEH lST RD., PING CHEN INDUSTRIAI- ZOI\E, PING CHEN, TAOI'I]AN, TAI\I'AN. R. O. C.

cmtsry airlJ.!r+!, n*51:,!l{iJt ;1ijtt--,gt NlrFi$tl-! ill ; "+iI ril:ilrtll'ir.'i*i,mo"**aovrt..c"npaiysuqdb6GsE]cond1trso,sr", a.*-" o*" d'*r .'.ibi;1 b r.'"

"d c"d,b.. b. E Ated on s d,*. ro rha rimtuld or 'ab' tv

M.mddssdiu sddh^ $,6ibi- y *d - , h " b . i . €

" r c ed " . *

h6trgh,so'dd,'sdssmcglh6,6 nd&6pd!.€n.x@p,inru.wd

lL-!t =:!t Ei't lirrsstNrrr*t7e,'e pr,etrT 'l0s!@m

g,t E +to( U ! i t )

rl*,rr*(Uethod)

ttt.firdF&noDL)

* *(ReE! l t )

N o . l

6* (S,) / H"1og."-chlor ine (c l )( C A S N o . : 2 2 5 3 7 - 1 5 - r )

+*Bs EN 14582:2007, ,/a&+ntf i&.+* r ' . / q i th .e fe rence to Bs EN

14582:2007. Ana lys is was p€ i fo rn€d by

I C .

5 0 3 6 7

f t ( tA) / Ealosen-Bionine (8. )(CAS No. : 10097-32 2)

mslkg 5 0

t[l+*+ / su! or PaBs

**rFr. 6232r' 2oo$r:ih, ,\^+aE ft&/T*d,&;Fl . / x i th r€ference to rEc6232r: zaat and pe. form€d 6y C'C/MS.

- t *4 f / Mo iobronob iphe iy l

: * f , l i / D ' b romobr phenyr

: *# f / T r ib romobipheny l 5

€ i *#* / re r rabroEoh i phe ly l 5

' . r r r$* / Pe i tabronoh iPhe i r l 5

n* # / Hex ,b rooob i pheny l 5

t * * f / sep tabronob ip leny l 5

^ i l$ f / o . tabrorob jpheny l 5

,L , lT+ / Nonzbrobob, pbeny l 5

+i * f l * / Decabroaob iphe iy l 5

t*tti,t+ / sun .r PBDE.- ; t4 fA t / $ tonob.omdipheny l e ther 5

: * # *A€ / D ib ronod ipheny l € the . 5

: *S*ad / T r ib ronad iphcny l e tner 5

€A*+& / Te ! rabronod iph€ny l e ther 5

nA | fS6 t / P .n tab ronod iphenyL e the r 5

i i *$*a6 / Hexabromodipheny l e ther 5

!A**a i / Heptabronod iph€ny l e rhcr 5

, \A#*R / ocrzbronod iphenyL e th€r 5

r'LtltXtat / Nonab!osodipi.nyL ether 5

+A#fa t / Decahromodiph€ny l e ther 5

,F{-d,#.+TeSt RepOft

f i '6(N" ) ' cE/201r/e1r7s EJh(D't ') ' 2011/10/02 Fjk(Pae€) : s or 15

#X, €+rtr.)A rEa El f,fi||rr]mttf,llITEQ CORPOMTION

tEEl *+4irr-* Er* -r422*22, (WG YEII lST RD., PING CHEN INDUSTRIII ZONE, PING CI]EN, TAOYUNN. TAII'AN. R. O. C.

g,t E +'ls(Uni t )

tit* t*d*r Eli(ror)

* *(R€sul t )

N o . 1SiS:F69:l*Tg / BBP(Benzy l bu ty l Ph tha la te ) (cAs

N o . : 8 5 - 6 8 - ? )

++v1 t4372, r ^l1n&/,fr*&lhi l<_./ $ / i t ! re fe ienc€ to EN 14372. Ana lys is

ras per fo rned by @/MS.

0 - 0 0 3

t$x:F&- (2-a4.eil)!5 /DEI{P (Di- (2 ethyrhexyl )p h r n a l a t e ) ( c A S N o . . 1 1 7 8 r - 7 )

0 . 0 0 3

t$X:F*.:*r+aE / DIDP (Di-i s o d € c y 1 p ! t h a l a t e ) ( C S N o . :

26761-40-0)

0 . 0 1

f iX:Y*:*+G / DINP (Di-isonooyl Phrhalate) (cAs No. :28553-12-0)

0 . 0 1

Sf:F*:ia+ai / DNoP (Di-n-o c t y l p h t h a l a t e ) ( c A s N o . : 1 1 ? -8 4 - 0 )

0 . 0 0 3

t tX:F*:Tt.: / DBP (Di burylp h t h a l a t e ) ( C A S N o . : 8 4 - 7 1 - 2 )

% 0 . 0 0 3

wosrF*t t l f . (Rsf€r .nc€ hfornar ion) , lE+ 2oo6/122lEc (Direct ive 2006/122lEc)(l) arirff Tir,[+t4]d.&n,A]+4&f d.!r,,E.&+€iXA+,i!*.i+o.oo5%.

( M a y i o t b e p l a c e d o n t h e f r a r k e t o . u s € d a s a s u b s t a n c e o t c o n s t i t u e n ! o f p r € p a . a t i o n s i n a

( o n . . 1 r r r r i o r . q r a l r o o ' \ i g \ e r h a n 0 . 0 0 5 ' ! b y m a s s . )

(2) ri4tf 4rrfi,ais-L6t+rja,""q.fi sd.4rr.r+, &is4r+-Lat&r4d pFoslttf€-***ra&.eif€jt+-fPFosf l tUi+'Ad. n,Ao. r%, it'rt*,"sd.4{etr}'&f , {'RProsAt6{b{ f 6t?;Ad.n:tttue/n':.( M a y n o t b e ! l a c e d o n t h e n a r k e t j ! s € n i - l i n i s l e d P r o d u c t s o r a r t i c l e s , o r p : r r s t h e . e o f , i f t h €

.oncent .a t ion o f PrcS is equa i to o r h iAher than 0 .1% 6y nass ca lcu la t€d w i th re fe rence io lhe

n a s s o f s l r u c t u r a l l y o r n i c r o s ! r ! c t ! r a l l y d i s t i r c l P a r t s t h a t c o n t a i n P F I S o r , f o r t € x t i l e s o r

o t le r coa ted Mt€r ia ls , i f the anounr o f PFGS is equa l to o r h iaher lhan lUg/o '1o f the coated

n a t e r i a l . )

mpreG)rsdd $ 3 bn Gpoi €md bcmtsry Fil. jr ;r'i . n t i1'irl x:i{iir) ;i.rrAr.e n l rl:,*A-{r]\' J::!r'f ;:- F{{h8d;6a3$d'1bcohp.iy9qedbdG6nala|ctrdibBofSfltu

"e'-" t-d d."i'"d" .6i"d b r-.' -d cddiD* tu Ertu rhs mbton 0t 'b't

spoBb rq s ro Gc rs i adhsenhi,sh6 add,sd,o^s u.da, 66 raj*

,',r,+*r..ltrrc;:tjll'. [+r:.: =:I]rti'l 1l's6ozr2et7erre{0nretr7 "*re(on

Member of rhe s6s 6ldp (565 5A)

x{a#+Test Report i l4(No.) : cE/2011/e4t?e ES{Dut") | 2orr/ro/07 Fi t(paae) : 6 or l5

',fr.E+ ,k ltr6 &x aITEQ MRPOMTION

#t Ei t*+rtrfi .af Ea*-!t22*22, KUNG \'EH IST RD., PING CHIN ]]$DUSTR]AL ZONE, PING CI{EN, TAOYIJAN, TAIi{AX, R. O.

f , i i (Not.) :1 . n g l k g = p p m ; 0 . 1 u t % = 1 0 0 0 p p n

? . n . d . = N o l D e t e c r e d ( , t l d * )

3. MDL : Melhod Detecr ion L in i l ( r * j ix l iEBia)

4. " - , ' = Noi Recl lared (d**q8iA)

s . * * : Q u a l i t a t i v e a n a l y s i s ( N o u " i r ) . t , E . r > t t ( * + & )

6. Negat iv€ = underecra6le l * , l * ' ( * {Axr l t l ) ; posi r ive : Detectable f r ,E(g lAr l t ' l )t. (*): Lii4b\ ah&z_xl*t***++€*o. *rDl€1+tt4z+tb. (rhe slbstance va.

resr l r o f Ant inony . The MDL was eva lua ted fo r A i r inony . )

llfl lrr]rrt]tl

c .

c a l c u l a t e d b y t h e t e s r

AX

a( - l t : - t * | An t 'nony r ox ide (sbror ) I . 1 9 7 1

8. ** ' , ?r l rJf . { .&&.xl :{ t }* i t41+*o. *IDL€Att&<E+t*. (rhe srbstance vas carcurai€d by tLe resrresr l t o f Bery l l iun . The I4DL u ,s eva lua ted fo r Bery t t iun . )

Prqs) bdsd thE r6d rcFd 6nd bcmFry 4,:rjiji ir. ri nF,itll$ir, i ' ldl,4 ' ri J , ,1..1++la?-1\ . 1ri.'l - ^i:ru64'fr" ;;'d ; *B by b" c.'p,iy sub,a b € ca€€ csdt€6 d sr* €sd'ic rom., dodin6* slbl,dbnr.d m ad lcdd d soA ijon ' " na " rn i n r * i , . a "ao .n "n l l udoc iedy f recmp ' ' s so6 l s5pBb l t yE ld6c ]61 ' dhs&@rbi., Eh6 d d {aom m6 'h. !a

',r**Fr,:, ;ie,-,t: rl'f-,r rii!'lrt ills6iDr,ae

kmb€ o/ Fs636'o!pl56ssAr

rnlH,+E+Test Report ! t4(No. ) : cE/2011/9a179 S ( D a t e ) : 2 0 1 r l 1 0 / 0 7 F j k ( P a g e )

I]|||tt]fittt[#i\E+wtie'raITEQ CORPOMTION

tuEl*+*f l.* El.*-r322*22, (UNG YEH lST RD., PING CIEN INDUSTRIIT" Z!NE, PING CHEN, TAO}'I]AII, TAII,N, R. O. C.

D FdirtrT$rnaEa#?f ilg cttaf,l.( ifir}'i&z*r$rl ) / rhese sampt€s re€dissolved tolaly ry pre{rnditio. ng method accordirE to betow Rd chan. ( Cf' t€st merhod oxctuded lrl !t^ I : $ t Jt / Nme of the pe|s who made mduremenr: ctimbgreat yangrdqt l^ : tt*4 / Name orlr€ p€Gon in charge ot measuremenr: Tfoy Chang

2)3)

56*+t*.f +**lJt ttd / ICP-aES

&sar / sampre Malenal fi iLrtfttt / oisGtion Acid.a*, ,Ba, aat, l"nan, tt^ /Adua rsia HNO. HCI HF H,a',

4a,tfi.rt / HNoJHF

Gold, olalinLn. Dalladiom. ceramiclt / Srlver 4* / HNO3

tt*, lt+,4rrt, -lr4/ HZSO.. Hzo:, HNO\ HCI," *+nr',,az*r* I Mt acid to lotal dig€stion

6G l te i d r hs rd r@.€ddsecnp€iy +lFr;q;t:r,: .t lli l i ' rr!l{:rl,; ;1;ii.li 9r5 .iitsif!,l l\,. i:lin 14:,]]Jli.:]'rhsih;.d""*.dbyrh.c"ip,.y3uqdb 6css.rcondlionsd s

id6md els md iu sd d d $6&n rM€4'ehcompanvsfl^dn$artmy 'ddhnhe inGorc s ' 3h * ndb ' t s l obc edhdubdcumaduot nohrs and obr,a,*" -d* th€ ta

i,,r I l"i1kr-!i:|l 1eoztree

!{.. {fr{{s / Culting . Prepararion

jrit{*sll / Sample Mealurcment

e.le:i. Fl tl.s rtil t 6,;{ iit sAt!i!liifiL(}r'[ t4 +) / A.id dige€lion by suitable acid depended ondiffe€nl sample material (as betowtabte)

sa{/Irt/{.t *r1&;tr{iE /Mico*€ve dagertionsith HNo./HcuHF

,9n!-ar4f art,tridrL+fi. / H€al to apFoFiate

1) *t6liil /AlkaliFusion2) ,**l+ /Hcllodisolve

,+i,ti!&l}&s / coot,fller d{€€late thragh nl|er

,"^f e ta /Add

'If tl.rL-rI4,ti,rlfl'l'r!{s,*it* 540 nm .04

absobance at 540 nm by

fi{a+E+TeSt RepOft

te€(No ): cEl2orllear7e ES(D'te) | 2ai/ro/o? F*(Pae") ' s o{ ls

&ft.$+MtSi B'r: A Il]t||tr][ttt[ITEO CORMMT]ON

dtEl rd+44It r* E.!f -rAz2!t,22, (UNG YEH lST RD.. PING CHEN IIiDUSTRIAL ZO\E, PING CIiEN, TAOI'I]AN, TAII'AN, R. O. C.

1 ) i * d t r T a i , F . A E z i * f t , * 1 " " c e 4 , 5 t 1 ' / r h e s e s a n p t e s w e r e t l i s s o r v e d t o r a l l y o yp r e - c o n d i t i o . i n g n e t h o d a c c o r d i n g t o h € l o w f l o s c h a f t .

2) tdJ{- \F : r+- fF ' l+ / Nane of the person 'ho &de n€asurenent : cr iobsreal yans3) t i l i l iE l ' : t i , ** / N. ' " o f the p€rson i . charse of f reasu.enent : r roy chans

Air,. tcp-fis +fi itfirbri,€n

6rUStSt*F + *4t,t +{ / rcP-Ars

n,k ,E ,F l t / s tee l , copper , a lun inun, so lder rn{,dri, ltd,6,n&.E5.n( /Aqua !eaia, IINO,, HCL, IIF, I{?O,

,f,t* 4*,4*!* / mio./HF

&, tA .H, l4 f . / co ld , p l : r iDur , pa l lad iun , cer :n ic

'E 4ff / IlNo:

a6 4h.*,* i.,*.,4d, {tt / Hso,, r{or, Hfro,. Hcr

*ld n ^EFt&4- i4 j , *& / Any ac id to tota l d isest ion

sG)rsdd rhs '6d r*n end h Bconoad !irtrntq! . -rilF,:l:1t':l :i-ti+!r5 r.iltts*,!t1.11 =i-:, I j I:,1trii+rh3& insn3€&dbys6cohpany3uq6dbb6$sE ]cond1o*dsi*

"M-. r",-d ddm.c. *br"ii b r." ."d cdldtns l., e d*

6 y , d * d , l h " i . c . f c . . d ! . * n s i b i l y s i o i s c e n | a n d l h i 5 d @ m e irhoir ohh and obLoar d3 unds rh6 i,afqgeryorfab|fi€t6oflh€@nlenltr

r " r " r , ' : t ! . , " , ; 1 6 * - , h F r w @ v * " n . r n n l L : , r i + 5 r l p ; i ' r i + 3 3 6 i 0 4

(F lor Cha. t of d igest iod for the e leo€nts analys is per foroed by ICP-AXS)

4 d, ' { f t i*" ' i / curr i 's 'preparat ion

, f l i { , i t "%Eg / sanple veasurehent

&&:Fq&:"etdf ts' , / i i66i*Gtit l i . lL (r 'T*. f i+) / ^c\d digestio. bys u i t a b l e a c i d d e p e n d e d o n d i l f e r € n ! s a n p l e m a t e r i a l ( a s b e l o u 1 a b 1 e )

4 t s / F i l t r a t i o n

4iA / Residu€j8 i t / Solut i on

1)& l8#* / A lka l i F ls ion2) ! r&84 / Hcr to d issorve

rfla#+Test RepOft

t€6(N'') ' cu/2a11/s41?s Erh(D't") ' 2 0 1 r / 1 0 / 0 i F * ( P a 8 e ) : 9 o f r s

,fifr.$+Mtrl e^ 4ITEQ CORPOMTION

ttElrf +*lF r* Er*-r&22fi22, I(!I{C YEH IST RD., PINC CIIEN INDUSTRIAL ZONE, PINC CHDi, TAO\,IJAN, TAI1,,{N, R. O. C.

|l][||tr lIt[tl

,ft{+*+fiAan /Analttical flow chart of Soxhtet extraction (LC/MS) procedure

r ,rldr'.q : ti'q# / Name ofthe person who made measurement: Roman Wonqr xli{ ft t ,/- : ti +R / Name of the person in charge of measurement: Troy Cha;g(, ri{a: 4fi.+r,**./an+|t(*). f,&-1*.t/u+# /Test ltonr8: PFOS/PFOA , Benzotriazole I

*.d / Data

€19 r*6 rhs 6d rcFn ennd e €rl i[1,:ll:M ; ilrtt:i9 d u.i:i]:n.1-1r., I : lli] r' I- rlril:]

f t s e i n a d 3 € s € d b , l h 6 c o m t s n y 3 g q 6 d b b c d s E ] c o d 1 o n s o i s

c i 6 ] i y s l o c c e d e d s b d d c u m g n

-: ,r. : fii!hr!-rlaelo)rs

ssri€4/ri* /Sample preteatnenuseparalion

+te+**E R j.+Rlt /Sample extraction by soxhlet method

+Birx*/ft# /Concenbate/Dilute Extracted solution

,]*.ta E frq*E'!.;fr4&,*- |Analysis was pedomed by LC/lllS

rrl'd,+E+Test Report * . 6 ( N o . ) , c E / 2 0 1 r l 9 a r 7 9 * ( D a t e ) : 2 o r r l 1 0 / o ?q*(Pase) : 10 of 15

Stq€+It't lAP&a61ITEQ CORPOMTION

t[Erf **f r* El.*-r&22fr22, (UNG YIII 1ST RD., PING CHEN INDUSTRIAL ZONE, PING CHEN. TAOYUAN, TAI[A]{, R. O. C.

*-*L*bfAE *frfien tAnalysis flow chart for determination of PVC in matedal

|l]ll][fltttlt]l

I

I

jl{;t^,F : **:iq / Name of the person who made measurementi GinnyChenxl;t t t,/- : ,tts4 / Name of the person in charge of measurement Troy Chang

ttt i Data

con€ry r.!rl, j1rj,. ' ,r i. i1'.::1:,{i j ,: i j ]]rtt.r ' l i .-ri: lFl!. ' l i l i l r ' i ' .".1t.1ft6ei'.ad ' *d by se comFny &b,.d,o $ GseE, csdtr o6 d sk aetri. romd @mstu s46d 1o rems trd Cmdi oB ro, Ertu

hi,sh6add€d6mmd66ka .d berqducedolcepr iM *ihod

*a etith-xl / Flame test

}!rl.tt*rl]f / Sampte anat}/zed by FT|R

,{a#+.Test Report ! E € ( N o . ) : c E / 2 0 1 1 / e ! r 7 9E J h ( D a t € ) , 2 0 1 1 / 1 0 / 0 7F j k ( P a s e ) : 1 1 o r 1 5

&it X+ehi e^ 4ITEQ CORPORATION

dt E tt+JAt.r- tF Er*-Ez2lh22, (UNG YEH IST RD., PING CISII

||]mlrr rlll[

IIIDUSTRIAL ZONE, PING CHEN, TAOYLIAN, TAI{AN. R. O. C.

I

I

t&*,An I Analytlcal flow chart

,qJA./.F : it'Ih# / Name ofthe person who made measurement Roman Wongt4$q */. : tF,*e / Name ofthe person in charge of measurement: Troy Chang

(,rlil{ E (Test ttems): qitla}-A, ttt A/ TBBP.A, BtsphenotAl

*Ji.+e,*+R/Sample extraclion by Soxhlet extraction

*.fil / Daia

' I r l f , , r r ! 1M , ; i . , ! ! L l i ' i r r - l r F^b !1 -1 3 i : , l , I r r r J t i l .Th3 fuum* l s " susdby lhscomFny5uqsdbb6*61cond1 .nsds

lh6rrLghGa.dobga'msUndsrfuta

fialLE-R, SAR,tNB/#r*/Defived by acetic acid

Concentrate/Dilute Extracled solution

rF{a+E+TeSt RepOft

ia46(No' ) : cEl?011/ea1?s aS(D't") | 2ai/n/01 Fik(Pas€) : 12 or rs

&itX+Mt*4W'r:4 trr|ffirlrflrtuITEQ @RPORATION

,tEilt+4iF'r*Eaf -rt22S22, KUNG YEH lST RD., PING CHEN INDUSTRIA! ZO\!, PING CHEN, TAOYIJAN. TAII'AN. R. O. C.

*Ji+rR+fi')n€f /Analytical flow chart of Soxhlot extractlon (GC/MS) procedurc

r ,nl:t^fi : frFt*t / Name ofthe person who made measurement Roman Wongr tilS\, A */! : tEr'3* / Name of the pe6on in charge of measurement Troy Chang

tide4 a: {!t{ . *.i!.:,}.ri{bAS ' ,r*rl+:8,' +&' + F*:i*:*AFB, .+ **U+h / Test ltemsr Phthalate.Benzotrtazote,HSCDO,NP.DBBT.Organicphoaphorus compounda)

&E / Data

€G)r6rd Th€ id €Fn en^d b IcomFry iirtrj!;ji3 -1]]i=il1M!1.1i;.;iirlI ,lti.,li[]!+!,1.1\'rFf:+il.l!l il lfi;].Th3fuumsdtsEsuadbylhsconpa.ysuqedbbcs66jcodionso.s

rha, fd'h and ob oar ms uodsihs ta

! ndsu rz .N N?s r rF i . { r h iw$ /n1 , , , . r + t r ! lX ! . ] r ' , r i rM D rze

&sii Erc/+* /Sample prctrealmenvseparation

+fs+F*4 +i,+n(ii /Sample extraction by soxhlet method

+4u{)X$/ffirf /Concentrate/Dilute Extracted solution

&4anftYr*&,t>fr |Analysis wES perfomed by GC/MS

,n{-d,+E+Test Report n&(N" ) ' ca, /2011/94t79 s ( D a r e ) : 2 0 1 1 / 1 0 / 0 7Fg(Pase) : 13 of 15

#iq€+wttd&24 |r][tll |l||r]tiTEQ CORPORATION

,t Ei S.+l1ifi r* Er*-rSz?*22, KUNG YEH lST RD.. PING CHEN INDUSTRIAI- ZONE, PING CHEN. TAOYLIAN. TAIJXAN. R. O. C.

i *+*f n€f, / Analttical flow chart of halogen content)!i';tl,F : fjl,g+ / Name ofthe pe.son who made measurement Rita Chen,tl d A t/\ : ,irg* / Name of the person in charge of measurementi Troy Chang

*+E &d\'Slt tAnalysis was perfomed by lC

1 )

2')

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r i " d . ; . d " * d b ' l E c . ' F n y s b j € d l d h c d n e 6 L c m d i o B d stu

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,i6nf.cl m a^d !6d.dtr f*3;*t.d *{h. rh.l,niB or cbdt *1h ; , , h 6 . d d o d - " * e , b " " .

,lr !r ;nr{B n 1s6i02lrret, t+M r0r)2etr7 !#l9(dm

Membs of rhe lcs6,o!p(scs rA)

rfla#+Test Report i i6(No.) : cE/2011/941?9 S ( D a t e ) : 2 0 1 1 / l o l 0 7 F * ( P a g e ) : 1 4 0 f 1 5

rllffI|t||lflt||nrS;{. € + rtr,}6 FA'li 4ITES CORMTITION

dt Ei,i+rtr6 r-* Er-i -r&22*22, KUNG YEH 1ST RD., PING CHE}I

'fi*,eI / Analytlcal tlow chanr , ii./'l : 4iltly / Name ofhe pefson who made measu€ment Roman wongr &A *,?\ : tt,*R / Name of lhe pe6on in chaEe of measurement Trcy Chang

I Nlit{ E (Test rtems): t;ltflt;tt*r, €*tr}.A{ / PBB/pBDE, raBp-A-bis)i 'nllLa4 / FiGI bsii.ro p@s -----t ltfnttas/t /oproB s@npo6s -..-. **at /confdjm!rces.-.|'

II\'DUSTRIAL ZONE, PINC CHDN, TAOI'IJAN, TAII{AN, R. O. C.

. . . . . ' . . . . . . . . . . . . . .

-I ttS f &* / Sample exlraclon merhod

+RR€8 / Filler

r r r r r r . . . . . . . . , , . . r . . . . . . . . . . . ' ' ' t ' ' . . . . r r . r . i

rrhr)fi / Scre€n analysis

fi"{€q}4f .*d.ttf / AnalysE by GC/lvlS

lssue Repod / &+rrE*

prelt €ned t srad ruFd €nnd sc@Fry nr ' r j l , r ie r 'b r l : l+1 : ] ] ! r+ i r , : i l l ' t t r t i 1 - 1E+tc^1 \ . : - - : l : : 7 r r l1 ]qfttrd@m€dts sdby$€compa

s4ed b t6n6 and cond,toB hr E'foe.,rdmad!6ddo6s6dm y a d . h ^ h e i m 6 d c r e d s m r u d o G i a r y h e c m p n t s s d e r c s p o B u r t s r o b c l s r ' n d s s t u 6lb,, sh6 ad d!'ea5ns ue ha h

fi{-d,+E+T e s t R e p o r t i t € ( N o . ) : c E l 2 0 1 1 / 9 a 1 7 9 e s ( D a t e ) : 2 0 1 1 / 1 0 / 0 7 F ' - * ' ( P a g e ) : 1 5 o f 1 5

#A,€+&DtrRaa t||| ][ltt[tlITEQ @RPOMTION

itEl '4+liiFa* Er* -t&22&22, KUNG YEH IST RD., PING CI]EN INDUSTRIAL Z!NE, PING CHEN, TAOYIJAN, TAIS'Itr\, R. O. C.

' F'4 fr!trft*R+ ' qii^AtlF** i&e/${i' '(Tbe tes ted saop le / par t i s oa tked by an ar io r i f i t ' s shorn on tbe photo . )

- - #*J*A (End or Report ) **

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Mnbqdtuhescs6rclp66ssAr







Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

Applicant: Littelfuse, Inc. Date : Feb 10, 2011 LIMA Technology Center,

Lipa City, Malvar, Batangas

Sample Description: One (1) group of submitted samples said to be : Part Description : Plated copper(for SMD) Date Sample Received : Feb 01, 2011 Date Test Started : Feb 08, 2011

Test Conducted :



Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401


Testing Item Coppery Metal

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content (mg/kg with 50cm2) Negative (< 0.02)

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected < = Less than mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre Negative = A negative test result indicated positive observation

was not found at the time of testing.


Date Sample Received : Feb 01, 2011 Testing Period : Feb 08, 2011 To Feb 09, 2011



Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm)



Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401




2 ppm

Lead (Pb) content


2 ppm



2 ppm


With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer.

0.02 mg/kg with 50cm2



Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

(Ⅳ) Measurement Flowchart: Test For Cd/Pb/Hg/Chromium (VI) Reference Standard：IEC 62321 edition 1.0:2008


Material Acid Added For Digestion

Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4


End Of Report




Cd/Pb/Hg

Analyzed by ICP-OES





Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

Boiling water extraction

Metal Polymers / Electronics

Negative*2 Confirm the tested samples are totally dissolved


Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

Photo

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