hplc instrumentation - chrom tech, inc.hplc instrumentation 296 chrom tech ® replaces dual piston,...

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HPLC Instrumentation

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Chrom Tech PumpsPump Model and Features GuideSingle Piston Isocratic PumpsDual Piston Isocratic PumpUltra High Pressure Isocratic PumpConstant Pressure Isocratic Pump Binary Gradient PumpHigh Flow Dual Piston PumpsSuper Critical Fluid PumpsFlash PumpsNext Generation Chrom Tech Replcement PartsModel LP-21 LO-Pulse Dampener

AutosamplerVacuum DegasserColumn HeatersDetectorsFixed WavelengthUV/VIS Variable WavelengthUV/VIS Multiple Wavelength & Diode ArrayRefractive IndexEvaporative Light Scattering

Isco Foxy® R1 & R2 Fraction Collectors

DataApex Clarity SoftwarePost Column DerivatizationPickering Post Column Reaction System & KitsSensivate Post-Column Reaction System

8 0 0 . 8 2 2 . 5 2 4 2 | 9 5 2 . 4 3 1 . 6 0 0 0 | w w w. c h r o m t e c h . c o m

HPLC

Inst

rum

enta

tion

Featured ProductsChrom Tech Pumps

ISCO Foxy® R1 & R2 Fraction Collectors

Detectors

Pickering Post Column Reactors

295

296

317

312

320

Vacuum Degasser

DataApex Clarity Chromatography Software

309

318

Notes from the Support Desk

AnalyticalPrepIsocraticGradient

2, 4 and 8 Channel available

Competitive pricing & free software updatesDirect control of many chromatography instruments

Merging equipment from two labs? Inherited legacy instrumentation? Have multi-vendor chromatography instrumentation in the lab?Is your IT Department requiring your lab to upgrade to a current operating system, but, your chromatograpny software is not compatible?If you answered yes to any of these, contact Chrom Tech to learn about DataApex Clarity Chromatography Software to Control and Collect Data from multiple instrument vendors.

Monitoring of the signal from detectors

Sequence Tab

Settings of directly controlled equipment

Single Analysis

Method setup Integration parameters

Information Table

Chromatogram review and

modify already measured chro-

matogram

Calibration use sample

as calibration standard

(calibrate or recalibrate)

Print custom-ized reports

from the analysis

Method setup calibrated calculations

DataApex Clarity Chromatography Software

H P L C I N S T R U M E N T A T I O N

296®Chrom Tech

“your chromatography specialists”

REPLACES Dual Piston, 1500 Series Prep 100, Prep 300 UHP Constant Pressure B2300Max flow rate/pressure 12 mL/6,000 PSI

36 mL/6,000 PSI100 mL/1,000 PSI

100 mL/4,000 PSI300 mL/1,000 PSI

5 mL/18,000 PSI 5 mL/25,000 PSI12 mL/18,000 PSI24 mL/10,000 PSI100 mL/5,000 PSI300 mL/1,000 PSI

5 mL/6,000 PSI10 mL/6,000 PSI40 mL/1,600 PSI

00 300 301 302 303Inlet: 1/8" OD, 1/4-28 Flat bottom

1/4" OD (300 mL)

1/4" OD (300 mL)

Outlet: 1/16" OD, 10-32 1/8" OD (100 mL)

1/8" OD (100 & 300 mL)

1/8" OD (100 & 300 mL)

FEATURES3 year warranty

Dual piston isocratic pump

Simple keypad control, LED display

Self-flushing pump heads

Pulse dampener

Prime purge valve

Real-time pressure monitoring

Set upper and lower pressure limits

Drip tray and leak sensor

REPLACES Series I, ISO-100 Series I, ISO-100 Series I+, ISO-100+ Series II, ISO-1000 Series III, ISO-2000Max flow rate/pressure 10 mL/2,000 PSI

40 mL/500 PSI10 mL/5,000 PSI 40 mL/900 PSI

10 mL/5,000 PSI 40 mL/900 PSI

5 mL/6,000 PSI10 mL/6,000 PSI 40 mL/1,600 PSI

5 mL/6,000 PSI10 mL/6,000 PSI 40 mL/1,600 PSI

Page 297 298 298 299 299Inlet: 1/8" OD, 1/4-28 Flat bottom

Outlet: 1/16" OD, 10-32

FEATURES3 year warranty

Single piston isocratic pump

Simple keypad control, LED display

Self-flushing pump heads

Pulse dampener

Prime purge valve

Real-time pressure monitoring

Set upper and lower pressure limits

Drip tray and leak sensor Drip tray only Drip tray only

NEW! Next Generation Pumps Replaces Chrom Tech Legacy Pumps

M1 CLASS

LD CLASS

ML CLASS

PR CLASS

MXT CLASS

LU CLASS

LL CLASS

CP CLASS

LST CLASS

LST BINARY

Chrom Tech Pumps

Pump accessory kit shipped with all pumps includes:

1/8" OD PTFE tubing (36" length) 20 µm inlet filter

TECH TIP

Outlet tubing sold separately:1/16" OD PEEK tubing (pg 253) 1/16" OD SS tubing (pg 257)



Flow Rate is dependent on solvent selection and operating pressure

Low Profile Single Piston Isocratic Pump | M1 ClassSelf-flushing pump headStainless steel or PEEK fluid pathSimple keypad controls, LED displaySingle pistonElectronic rapid refill mechanismMotor stall detector 3 year warranty

SPECIFICATIONSFlow Accuracy Within 2% of set flow rate*

Within 5% of set flow rate*10 mL40 mL

Flow Precision 1.0% RSDWetted Materials Synthetic Ruby, Sapphire, UHMWPE, PTFEDimensions (h x w x d)

5.5" x 3" x 10.5"(14 x 8 x 27 cm)

Weight 3.5 lbs (1.6 kg)Power To Supply: 100-240 VAC, 50-60 Hz, 1A

Supply to Pump: 24VDC, center positive, 2.1 mm post, 1.6 AMP

Control Micro USB Port with RS-232 communication, Run/Stop

*Seal Kits include: Self-flush seal, O-Ring, Primary Seal, and Removal Tool

REPLACEMENT PARTS MM HEAD MH HEAD

P-M110S P-M110B P-M140S P-M140BPiston Seal Kit*, Aqueous P-0103 P-0103B P-1295 P-1295BPiston Seal Kit*, Organic P-0109 P-0109B P-1299 —Check Valve Kit, Inlet & Outlet P-1085-2 P-1086 P-1085-2 P-1086

Repl Check Valve Capsules, 10/pk P-1075 P-1076 P-1075 P-1076Self-Flush Assembly P-1082 P-1088 P-1081 P-1089Replacement Piston P-0101 P-0101 P-1298 P-1298Inlet Filter Assy (Fitting & Element) 06-0110 06-0110 06-0110 06-0110Repl Inlet Filter Elements, 2/pk P-1170 P-1170 P-1170 P-1170

Standard vs Organic SealsThe standard seal is made of (UHMW-PE) Ultra High Molecular Weight Polyethylene for use with aqueous fluids. The organic seal is made of graphite-filled PTFE for use with harsh chemicals.

The recommended minimum back pressure is 200 PSI for optimum pump performance. If your application will not provide adequate back pressure, adding restrictive tubing to the outlet of the pump is recommended.

TECH TIP TECH TIP

ORDERING INFORMATION

PART NOSEAL TYPE

FLOW RATE (mL/min) MATERIAL

PRESSURE (PSI )

PUMP HEAD

P-M110S standard 10.00 SS 2,000 MM

P-M110B standard 10.00 PEEK 2,000 MM

P-M110S-O organic 10.00 SS 2,000 MM

P-M110B-O organic 10.00 PEEK 2,000 MM

P-M140S standard 40.0 SS 500 MH

P-M140B standard 40.0 PEEK 500 MH

P-M140S-O organic 40.0 SS 500 MH

*Flow rate range for flow accuracy specification: 10 mL—0.20 mL/min and above; 80:20 Water/IPA at 1,000 PSI40 mL—0.80 mL/min and above; 80:20 Water/IPA at 100 PSI

NEW!

NEW!

NEW!

The compact M1 Class consists of single-headed, positive displacement piston pumps that deliver high-performance and precision at an affordable price. Applications include precise chemical metering, dispensing, and specific HPLC separation. Having the smallest possible footprint for a high pressure pump, the M1 Class will easily integrate into any laboratory or industrial environment.

NEW!Biocompatible SealsNow offering biocompatible seals which contain a fluoropolymer energizer (vs the Stainless Steel Energizer)

Clarity Software Compatible See page 318

Chrom Tech Pumps

Replaces Series I, ISO-100


298®Chrom Tech



Single Piston Isocratic Pump | ML & MXT ClassPressure monitoring with automatic pressure compensationIntegrated prime-purge valveStainless steel or PEEK fluid pathSimple keypad controls, LED displayLeak sensor 3 year warranty


Within 5% of set flow rate*10 mL40 mL

Pressure Accuracy ± 2% of full scale pressureFlow Precision 0.5% RSDWetted Materials Synthetic Ruby, Sapphire, UHMWPE, PTFEDimensions (h x w x d)

6.5" x 7" x 16"(17 x 18 x 41 cm)

Weight 15.3 lbs (6.9 kg)Power 100-240 VAC, (± 10%), 50-60 HzControl RS-232, Micro USB, Voltage Flow Control, Run/

Stop (ML Class: Micro USB & Run/Stop)

REPLACEMENT PARTS MM HEAD MH HEAD

P-ML10S P-MXT10S

P-ML10B P-MXT10B/P-MXT01B-MS

P-ML40S P-MXT40S

P-ML40B P-MXT40B

Piston Seal Kit*, Aqueous P-0103 P-0103B P-1295 P-1295BPiston Seal Kit*, Organic P-0109 P-0109B P-1299 —Check Valve Kit, Inlet & Outlet P-1085-2 P-1086 P-1085-2 P-1086Repl Check Valve Capsules, 10/pk P-1075 P-1076 P-1075 P-1076Self-Flush Assembly P-1082 P-1088 P-1081 P-1089Replacement Piston P-0101 P-0101 P-1298 P-1298Inlet Filter Assy (Fitting & Element) 06-0110 06-0110 06-0110 06-0110Repl Inlet Filter Elements, 2/pk P-1170 P-1170 P-1170 P-1170Repl Outlet Filter Elements, 2/pk P-1175 P-1171 (ea) P-1175 P-1171 (ea)Pulse Dampener Rebuild Kit P-1063 P-1063 P-1063 P-1063MXT Backpressure Coil Assy for MS applications — P-COIL — —

ML & MXT ORDERING INFORMATIONPART NO ML MODEL

PART NOMXT MODEL

FLOW RATE(mL/min) MATERIAL

PRESSURE(PSI)

PUMP HEAD

P-ML10S P-MXT10S 10.00 SS 5,000 MM

P-ML10B P-MXT10B 10.00 PEEK 5,000 MM

P-ML40S P-MXT40S 40.0 SS 900 MH

P-ML40B P-MXT40B 40.0 PEEK 900 MH

MXT-MS ORDERING INFORMATION— P-MXT01B-MS 1.000 PEEK 5,000 MM

*Flow rate range for flow accuracy specification: 10 mL—0.20 mL/min and above; 80:20 Water/IPA at 1,000 PSI40 mL—0.80 mL/min and above; 80:20 Water/IPA at 100 PSI

*Seal Kits include: Self-flush seal, O-Ring, Primary Seal, and Removal ToolNEW!

Biocompatible SealsNow offering biocompatible seals which contain a fluoropolymer energizer (vs the Stainless Steel Energizer)

NEW! NEW!

NEW!

ML MODEL MXT MODEL FEATURESX X Self-flushing pump heads & prime purge valve

X Real-time pressure monitoring

X Set upper and lower pressure limits

X X Drip tray

X Leak sensor on drip tray

X X Pulse dampener

X X Run/Stop

X X Micro USB with RS-232 communication

X RJ11 with RS-232 communication

X Voltage control

The MXT-MS pump includes an internal backpressure coil assembly (max flow rate of 1 mL/min) for mass spectrometry applications, i.e.: Flow Injection analysis, Infusion, Cone Wash.

TECH TIP

MXT-MS Applications include Flow Injection AnalysisInfusionCone Wash


Chrom Tech Pumps

ML Replaces Series 1, ISO-100 MXT Replaces Series 1+, ISO-100+



ORDERING INFORMATIONPART NOLL MODEL

PART NOLS MODEL

PART NOLST MODEL


PRESSURE (PSI)

PUMP HEAD

P-LL05S P-LS05S P-LST05S 5.000 SS 6,000 L

P-LL05B P-LS05B P-LST05B 5.000 PEEK 6,000 L

P-LL10S P-LS10S P-LST10S 10.00 SS 6,000 M

P-LL10B P-LS10B P-LST10B 10.00 PEEK 6,000 M

P-LL40S P-LS40S P-LST40S 40.0 SS 1,600 H

P-LL40B P-LS40B P-LST40B 40.0 PEEK 1,600 HFlow Rate is dependent on solvent selection and operating pressure

Single Piston High Performance Isocratic Pump | LS & LST Class

The reliable LS/LST Class consists of single-headed positive displacement piston pumps incorporating advanced cam designs for very low pulsation. With micro-stepping motor technology and a proven single-piston pump mechanism, the LS/LST Class exceeds the performance of more expensive units at a fraction of the cost. The pumps are ideal for a wide variety of HPLC applications (including biocompatible separations), semi-prep LC, metering & dispensing, and general lab use.

The recommended minimum back pressure is 200 PSI for optimum pump performance. If your application will not provide adequate back pressure, adding restrictive tubing to the outlet of the pump is recommended.

TECH TIP

SPECIFICATIONSFlow Accuracy Within 2% of set flow rate*Pulsation ≤ 2% at 1 mL/min and 1,000 PSIPressure Accuracy ± 2% of full scale pressureFlow Precision 0.2% RSD Wetted Materials Synthetic Ruby, Sapphire, UHMWPE, PTFEDimensions (h x w x d)

6.5" x 7" x 16"(16.5 x 18 x 41 cm)

Weight 15 lbs (7 kg)Power 100-240 VAC (± 10%), 50-60 HzControl RS-232, Micro USB, Voltage Flow Control, Run/Stop

(LL Class: Micro USB & Run/Stop)

Pulse dampenerSelf-flushing pump heads and prime purge valveStainless steel or PEEK fluid pathSimple front panel keypad controls with LED display 3 year warranty

Real-time pressure monitoringSet upper and lower pressure limits Drip tray and leak sensor

Additional features of LST models

*Flow rate range for flow accuracy specification: 5 mL and 10 mL—0.20 mL/min and above; 80:20 Water/IPA at 1,000 PSI40 mL—0.80 mL/min and above; 80:20 Water/IPA at 100 PSI

REPLACEMENT PARTS L HEAD M HEAD H HEAD

P-LL05S/P-LS05S/ P-LST05S

P-LL05B/ P-LS05B/ P-LST05B

P-LL10S/ P-LS10S/ P-LST10S


P-LL40S/ P-LS40S/ P-LST40S


Piston Seal Kit*, Aqueous P-1595 P-1595B P-1095 P-1095B P-1096 P-1096BPiston Seal Kit*, Organic P-1599 — P-1099 P-1099B P-3009 —Check Valve Kit, Inlet & Outlet P-1085-2 P-1086 P-1085 P-1086 P-1085 P-1086Repl Check Valve Capsules, 10/pk P-1075 P-1076 P-1075 P-1076 P-1075 P-1076Self-Flush Check Valve Kit P-1084 P-1084 P-1084 P-1084 P-1084 P-1084Replacement Piston P-1597 P-1597 P-1097 P-1097 P-1198 P-1198Inlet Filter Assy (Fitting & Element) 06-0110 06-0110 06-0110 06-0110 06-0110 06-0110Repl Inlet Filter Elements, 2/pk P-1170 P-1170 P-1170 P-1170 P-1170 P-1170Repl Outlet Filter Elements, 2/pk P-1175 P-1171 (ea) P-1175 P-1171 (ea) P-1175 P-1171 (ea)Pulse Dampener Rebuild Kit P-1063 P-1063 P-1063 P-1063 P-1063 P-1063*Seal Kits include: Self-flush seal, O-Ring, Primary Seal, and Removal Tool

NEW! NEW! NEW!

NEW!

LL MODEL LS MODEL LST MODEL FEATURESX X X Pulse dampenerX X X Self-flushing pump heads & prime purge valve

X Real-time pressure monitoringX Set upper and lower pressure limits

X X X Drip trayX Leak sensor on drip tray

X X X Run/StopX X X Micro USB with RS-232 communication

X X RJ11 with RS-232 communicationX X Voltage control


LST model


Chrom Tech Pumps

LS Replaces Series II, ISO-1000 LST Replaces Series III, ISO-2000


300®Chrom Tech


*Does not come equipped with pulse dampener. 1/4" OD inlet (vs 1/8" OD).Flow Rate is dependent on solvent selection and operating pressure

Dual Piston Isocratic Pump | LD & PR Class

REPLACEMENT PARTS M HEAD H HEAD XH HEAD

P-LD12S P-LD36S

P-LD12B P-LD36B

P-LD100S P-PR100S

P-LD100B P-PR100B P-PR300S

Piston Seal Kit*, Aqueous P-1095 P-1095B P-1096 P-1096B P-1795Piston Seal Kit*, Organic P-1099 P-1099B P-3009 — —Check Valve Kit, Inlet & Outlet P-1085 P-1086 P-1085 P-1086 P-1781Repl Check Valve Capsules, 10/pk P-1075 P-1076 P-1075 P-1076 P-1785 (4/pk)Self-Flush Check Valve Kit P-1084 P-1084 P-1084 P-1084 P-1084Replacement Piston P-1097 P-1097 P-1198 P-1198 P-1798Inlet Filter Assy (Fitting & Element) 06-0110 06-0110 06-0110 06-0110 06-0110Repl Inlet Filter Elements, 2/pk P-1170 P-1170 P-1170 P-1170 P-1170Repl Outlet Filter Elements, 2/pk P-1175 (0.5 µm)*1

P-1172 (2 µm)*2P-1171 (ea) P-1172 P-1171 (ea) P-1172

Pulse Dampener Rebuild Kit P-1063 P-1063 P-1063 P-1063 P-10631) 0.5 µm outlet filter element standard with 12 mL pump 2) 2 µm outlet filter element standard with 36 mL pump*Seal Kits include: Self-flush seal, O-Ring, Primary Seal, and Removal Tool

Autoprime™ one button toggles flowrate to maximum for rapid solvent changeReal-time pressure monitoring with upper and lower pressure limitsDrip tray and leak sensorPulse dampenerSelf-flushing pump heads and prime purge valveStainless steel or PEEK fluid pathSimple front panel keypad controls with LED display 3 year warranty


PART NOSEAL TYPE

FLOW RATE(mL/min) MATERIAL

PRESSURE(PSI)

PUMP HEAD

TUBING OUTLET

P-LD12S standard 12.000 SS 6,000 M 1/16" OD

P-LD12S-O organic 12.000 SS 6,000 M 1/16" OD

P-LD12B standard 12.000 PEEK 6,000 M 1/16" OD

P-LD36S standard 36.00 SS 6,000 M 1/16" OD

P-LD36B standard 36.00 PEEK 6,000 M 1/16" OD

P-LD100S-8 standard 100.0 SS 1,000 H 1/8" OD

P-LD100B-8 standard 100.0 PEEK 1,000 H 1/8" OD

P-PR100S-8 standard 100.0 SS 4,000 H 1/8" OD

P-PR100S-O-8 organic 100.0 SS 4,000 H 1/8" OD

P-PR100B-8 standard 100.0 PEEK 4,000 H 1/8" OD

P-PR300S-8* standard 300.0 SS 1,000 XH 1/8" OD

Dual Piston Pump MaintenanceIn order to do maintenance on a dual piston pump, kits are sold per head, quantity two required.

TECH TIP


Within 2% of set flow rate*Within 2% of set flow rate*Within 3% of set flow rate*Within 4% of set flow rate*

LD 12LD 36LD 100PR 100PR 300

Pulsation ≤ 0.5% at 1 mL/min and 1,000 PSI ≤ 2% at 1 mL/min and 1,000 PSI≤ 4% at 50 mL/min and 250 PSI ≤ 4% at 50 mL/min and 500 PSI ≤ 4% at 50 mL/min and 500 PSI

LD 12LD 36 LD 100 PR 100PR 300

Pressure Accuracy ± 2% of full scale pressureFlow Precision 0.2% RSD (12 mL)

0.5% RSD (36 mL, 100 mL, 300 mL)Wetted Materials Synthetic Ruby, Sapphire, UHMWPE, PTFE, CeramicDimensions (h x w x d)

6.5" x 10" x 17"(16 x 25 x 43 cm)


*Flow rate range for flow accuracy specification: LD 12—0.200 mL/min and above; 80:20 Water/IPA at 1,000 PSILD 36—0.80 mL/min and above; 80:20 Water/IPA at 1,000 PSILD 100—2.0 mL/min and above; 80:20 Water/IPA at 1,00 PSIPR 100—2.0 mL/min and above; 80:20 Water/IPA at 1,000 PSIPR-300—5.0 mL/min and above; 80:20 Water/IPA at 100 PSI

NEW! NEW!

NEW!



Chrom Tech Pumps

LD Replaces Dual Piston, 1500 Series PR Replaces Prep 100, Prep 300




Ultra High Pressure Isocratic Pump | LU ClassSelf-flushing pump headReal-time pressure monitoring with upper and lower pressure limitsDrip tray and leak sensorPulse dampenerSimple keypad controls, LED displayAdvanced solvent select featureAutomatic pressure compensation3 year warranty

SPECIFICATIONSFlow Accuracy Within 1% of set flow rate*Pulsation ≤ 0.75% from 3,000 PSI – 8,000 PSIPressure Accuracy ± 2% of full scale pressureFlow Resolution 0.001 mLFlow Precision 0.5% RSD on > 30 sec. average flowsWetted Materials Synthetic Ruby, Sapphire, UHMWPE, PTFEDimensions (h x w x d)

6.5" x 10" x 17"(16 x 25 x 43 cm)



The analytical LU Class consists of dual-headed, positive displacement piston pumps, delivering accurate flow rates at extremely high pressures. The pumps are designed for fast, high pressure analytical HPLC, with increased peak resolution and exceptional retention time repeatability. The advanced solvent select feature provides very accurate flow rates at high pressures for a wide variety of solvents, particularly where compressibility is a major factor. With pulse-free performance and precise control, the LU Class provides the highest flow accuracy over the entire pressure range.

ORDERING INFORMATIONPART NO MAX FLOW RATE MATERIAL MAX PRESSUREP-LU05S 5.000 mL/min SS 18,000 PSI

REPLACEMENT PARTSSeal Kit*, UHP P-1895Check Valve Kit, double inlet/single outlet P-1885Repl Check Valve Capsules, 10/pk P-1875Self-Flush Check Valve Kit P-1084UHP Piston P-1897Inlet Filter Assy (Fitting & Element) 06-0110Repl Inlet Filter Elements, 2/pk P-1170Repl Outlet Filter Elements, 2/pk P-1175

Solvent Select FeatureDifferences in solvent compressibility factors can greatly influence flow accuracy, especially at ultra-high system pressures. The Solvent Select Feature optimizes pump performance with six preset compressibility settings for common solvents. For uncommon applications, an isothermal compressibility factor may be entered directly to assure accurate solvent delivery.

TECH TIP

*Flow rate range for flow accuracy specification:0.100 mL/min and above; 80:20 Water/IPA at 5,000 PSI


Chrom Tech Pumps

Replaces UHP pump


302®Chrom Tech


Flow rate is dependent on solvent selection and operating pressure

Constant Pressure Isocratic Pump | CP Class

Complete Pack in a Box (PIAB Models) system includes:

Pressure monitoring with automatic pressure compensationSelf-flushing pump heads and integrated prime-purge valveStainless steel or PEEK fluid pathSimple keypad controls, LED display3 year warranty

SPECIFICATIONSPressure Accuracy ± 2% of full scale pressureWetted Materials Synthetic Ruby, Sapphire, UHMWPE, PTFE, CeramicDimensions (h x w x d)

6.3" x 10" x 17"(16 x 25.5 x 43 cm)

Weight 30 lbs (14 kg)Power 100-240 VAC, (± 10%), 50-60 HzControl RS-232, Micro USB, Voltage Flow Control, Run/Stop

The CP Class pumps are widely used for LC Column packing, as well as many process applications. Advanced pressure control algorithms ensure consistent bed density and prevent pressure over-shoot by allowing the user to select a wide range of process parameters, including desired pressure set point, ramp rate, and upper flow rate limit. Control software included. Pressure Control Accuracy is dependent on hydraulic system parameters. Pump automatically adjusts fluid flow to maintain constant system pressure under typical column-packing usage. Pump does not contain an automatic pressure-relief valve.


PART NO

FLOW RATE

(mL/min) MATERIAL

MAX PRESSURE

(PSI)

PUMP HEAD

MODELP-CPU05S 5.000 SS 25,000 XUHP

P-CP12S 12.00 SS 10,000 L

P-CPU12S 12.00 SS 18,000 UHP

P-CPU12S-PIAB 12.00 SS 18,000 UHP

P-CP24S 24.00 SS 10,000 M

P-CP24S-NF-PIAB 24.00 SS 10,000 M

P-CP100S-8 100.0 SS 4,000 H

P-CP300S-8 300.0 SS 1,000 XH


REPLACEMENT PARTS XUHP HEAD UHP HEAD L HEAD M HEAD H HEAD XH HEAD

P-CPU05S P-CPU12S P-CP12S P-CP24S P-CP100S P-CP300SPiston Seal Kit*, Aqueous P-1895 P-1895 P-1595 P-1095 P-1096 P-1795Piston Seal Kit*, Organic P-1899 P-1899 P-1596 P-1099 P-3009 —Check Valve Kit, Inlet & Outlet P-1881 P-1985 P-1085-2 P-1085 P-1085 P-1781Repl Check Valve Capsules, 10/pk — P-1875 P-1075 P-1075 P-1075 P-1785Self-Flush Check Valve Kit P-1084 P-1084 P-1084 P-1084 P-1084 P-1084Replacement Piston P-1897 P-1597 P-1597 P-1097 P-1198 P-1798Inlet Filter Assy (Fitting & Element) 06-0110 06-0110 06-0110 06-0110 06-0110 —Repl Inlet Filter Elements, 2/pk P-1170 P-1170 P-1170 P-1170 P-1170 —Repl Outlet Filter Elements, 2/pk P-1175 (ea) P-1175 (ea) P-1175 (ea) P-1175 P-1172 P-1172

Dual Piston Pump MaintenanceIn order to do maintenance on a dual piston pump, kits are sold per head, quantity two required.

TECH TIP

Chrom Tech Pumps

Next Generation CP Class Constant Pressure Pump with pressure transducer, RS-232, and Micro USB control; Stainless Steel; non-flushing pump heads; 110/220 Volt20 mL packing reservoir assembly with inlet & outlet caps attached4.6 mm pre-column assembly with packing adapter for 4.6 mm columnsTwo (2) 4.6 mm x 150 mm columns10 g bottle of C18 stationary phaseBracket assembly to mount Packing Reservoir to the pumpQuick-Set Disk to allow full control of the packing process through a computerStep by step instructions explaining how to set up and pack columnsSet of tubing to connect the system for useSet of cables to connect the pump to a computerAll necessary fittings and ferrules for tubing connections

Replaces Constant Pressure pump



ORDERING INFORMATIONPART NO w/o degasser

PART NOw/degasser


PRESSURE(PSI)

PUMP HEAD

PB-LST05S PBD-LST05S 5.000 SS 6,000 L

PB-LST05B PBD-LST05B 5.000 PEEK 6,000 L

PB-LST10S PBD-LST10S 10.00 SS 6,000 M

PB-LST10B PBD-LST10B 10.00 PEEK 6,000 M

PB-LST40S PBD-LST40S 40.0 SS 1,600 H

PB-LST40B PBD-LST40B 40.0 PEEK 1,600 HFlow Rate is dependent on solvent selection and operating pressure

High Performance Binary Gradient Pump | LST ClassPulse dampenerSelf-flushing pump heads and prime purge valveStainless steel or PEEK fluid pathSimple front panel keypad controls with LED display Real-time pressure monitoring with upper and lower pressure limitsDrip tray and leak sensorLow volume mixing chamber3 year warranty

The customizable Binary Gradient Pumping System is an advanced pumping system for two-solvent high-pressure gradient applications. The system is designed with two single-head positive displacement piston pumps integrated into a functional enclosure. Equipped with belt drive pump mechanisms with shaped cam and electronic fast refill, the system produces very low pulsation. The included Gradient Board allows for autonomous binary gradient formation without the need for continuous computer monitoring and control. Serial commands may be used to directly set pump flow rates, start/pause, or monitor status. Additional features include control of two solvent-selection valves, multiple timed events, and leak detection.

SPECIFICATIONSFlow Accuracy Within 2% of set flow rate*Pulsation ≤ 2% at 1 mL/min and 1,000 PSIPressure Accuracy ± 2% of full scale pressureFlow Precision 0.2% RSD Wetted Materials Synthetic Ruby, Sapphire, UHMWPE, PTFE, PFADimensions (h x w x d)

9" x 10" x 17" (22.9 x 25.4 x 43.2 cm)


Gradient Method Development

Pump shown with degasser option

*Flow rate range for flow accuracy specification: 5 mL—0.20 mL/min and above; 80:20 Water/IPA at 1,000 PSI10 mL and 40 mL—0.80 mL/min and above; 80:20 Water/IPA at 1,000 PSI

REPLACEMENT PARTS L HEAD M HEAD H HEAD

PBD-LST05S PB-LST05S

PBD-LST05B PB-LST05B





Piston Seal Kit*, Aqueous P-1595 P-1595B P-1095 P-1095B P-1096 P-1096BPiston Seal Kit*, Organic P-1599 — P-1099 P-1099B P-3009 —Check Valve Kit, Inlet & Outlet P-1085-2 P-1085-2 P-1085 P-1086 P-1085 P-1086Repl Check Valve Capsules, 10/pk P-1075 P-1076 P-1075 P-1076 P-1075 P-1076Self-Flush Check Valve Kit P-1084 P-1084 P-1084 P-1084 P-1084 P-1084Replacement Piston P-1597 P-1597 P-1097 P-1097 P-1198 P-1198Inlet Filter Assy (Fitting & Element) 06-0110 06-0110 06-0110 06-0110 06-0110 06-0110Repl Inlet Filter Elements, 2/pk P-1170 P-1170 P-1170 P-1170 P-1170 P-1170Repl Outlet Filter Elements, 2/pk P-1175 P-1171 (ea) P-1175 P-1171 (ea) P-1175 P-1171 (ea)Pulse Dampener Rebuild Kit P-1063 P-1063 P-1063 P-1063 P-1063 P-1063*Seal Kits include: Self-flush seal, O-Ring, Primary Seal, and Removal Tool

NEW! NEW! NEW!

NEW!



Chrom Tech Pumps

Replaces B2300


304®Chrom Tech


REPLACEMENT PARTSPiston Seal Kit*, Aqueous P-1795Check Valve Capsules, 4/pk P-1785Self-Flush Check Valve Kit P-1087Replacement Piston P-1697Repl Outlet Filter Element, ea P-1172

HF 300 PUMPPART NO MODEL FLOW RATE MAX PRESSURE* SELF FLUSHP-5300CFNF Constant flow 0.1 – 300 mL/min 10,000 PSI

P-5300CFSF Constant flow 0.1 – 300 mL/min 10,000 PSI

P-5300CPNF Constant pressure 0.1 – 300 mL/min 10,000 PSI

P-5300CPSF Constant pressure 0.1 – 300 mL/min 10,000 PSI

*At 220 V, entire power range available. At 110 V, maximum pressure decreases above 250 mL/min.


High Flow Dual Piston Pumps | HF 300

Super Critical Fluid Pumps | SFC-24

Up to 300 mL/min and 8,500 PSIDual piston design for precise flow rates and low pulsation3 year warrantyCeramic pistons and ruby/sapphire check valves

Self-flushing pump head3 year warrantyOutlet filterAll aluminum pump heads (for heat transfer)Stainless Steel fluid path (other than pump heads)Integrated cooling system using Peltier thermoelectric modulesIn-line electronic pressure transducer

HF-300 SPECIFICATIONSFlow Accuracy < 5% of set point

(above 5 mL/min, 1,000 PSI)Flow Precision 0.5% RSDPulsation < ± 5.0% from 150 mL/min,

3,000 PSIDimensions (w x h x d)

9" x 14" x 22" (22.8 x 35.8 x 55.9 cm)

Weight 50 lbs (22.7 kg)Input RS-232

SPECIFICATIONSFlow Accuracy ± 5%Pressure Accuracy ± 2% of full scale pressureConstant Pressure Pressure monitoring (via transducer)

with user-selected upper/lower pressure limits

Control Mode User-selectable pressure point set. Pump flow rate auto-adjusts to maintain pressure

Dimensions (h x w x d)

5.8" x 11.1" x 22.1" (14.6 x 28.3 x 53.7 cm)

Weight 36 lbs (16.3 kg)Input RS-232

Chrom Tech Specialty Pumps

The SFC-24 features integrated cooling systems using Peltier thermoelectric modules. The cooling is fully self-contained within the pump cabinet, eliminating the need for external refrigeration units and the associated piping, coolants, and Freon. Peltier technology is 100% solid state.

SFC-24 PUMPPART NO MODEL FLOW RATE MAX PRESSUREP-2024SFC Constant pressure 0.01 – 24 mL/min 10,000 PSI

P-2024SFC-CF Constant flow 0.01 – 24 mL/min 10,000 PSI

REPLACEMENT PARTSPiston Seal Kit*, Aqueous P-2495Check Valve Kit, Inlet & Outlet P-2485Repl Bulkhead Filter Assembly, ea (Inlet or Outlet) 050190Repl Filter Element for Bulkhead Filter, 2/pk P-1172Replacement Piston P-1097*Seal Kits include: Self-flush seal, O-Ring, Primary Seal, and Removal Tool



Chrom Tech Flash Pumps

CHROM TECH FLASH PUMPSPART NO MODEL MAX FLOWRATE PUMP HEAD MATERIAL MAX PRESSURE PUMP OUTLET CONNECTIONP-M1FS-8 M1 Flash 100.0 mL/min SS 250 PSI For 1/8" OD tubing, 3/8-24 coned thread

PB-M1FS-8 Binary M1 Flash 100.0 mL/min SS 250 PSI For 1/8" OD tubing, 3/8-24 coned thread

P-LD100S-8 LD Class 100.0 mL/min SS 1,000 PSI For 1/8" OD tubing, 3/8-24 coned thread

P-LD100B-8 LD Class 100.0 mL/min PEEK 1,000 PSI For 1/8" OD tubing, 3/8-24 coned thread

REPLACEMENT PARTSP-M1FS/PB-M1FS P-LD100S P-LD100B

Piston Seal Kit*, Aqueous P-1199 P-1096 P-1096BPiston Seal Kit*, Organic 880270 P-3009 —Check Valve Kit, Inlet & Outlet 880417 P-1085 P-1086Self-Flush Check Valve Kit — P-1084 P-1084Sapphire Piston 880357 P-1198 P-1198Inlet Filter Assy (Fitting & Element) 06-0110 06-0110 06-0110Repl Inlet Filter Element, 2/pk P-1170 P-1170 P-1170Repl Outlet Filter Element, ea — P-1172 P-1171 (ea)Replacement outlet nut for 1/8" OD tubing, 10/pk 01-0141 01-0141 06-0175Replacement outlet ferrule for 1/8" OD tubing, 10/pk 01-0143 01-0143 06-0182*Seal Kits include: Self-flush seal, O-Ring, Primary Seal, and Removal Tool

SPECIFICATIONSISOCRATIC M1 FLASH BINARY M1 FLASH ISOCRATIC LD CLASS

Flow Accuracy Within 5% of set flow rate, 2 mL/min and above; 80:20 Water/IPA @ 100 PSI Within 2% of set flow rate, 2.0 mL/min and above; 80:20 Water/IPA at 1,00 PSI

Flow Precision 1.0% RSD 0.5% RSDWetted Materials Synthetic Ruby, Sapphire, UHMWPE, PTFE, SS Synthetic Ruby, Sapphire, UHMWPE, PTFE,

Ceramic, (SS or PEEK)Dimensions (h x w x d) 5.5" x 3" x 10.5" (14 x 8 x 27 cm) 6.5" x 10" x 17" (16 x 25 x 43 cm)Weight 3.5 lbs (1.6 kg) 30 lbs (14 kg)Power 100-240 VAC (± 10%), 50-60 Hz 100-240 VAC (± 10%), 50-60 HzControl Micro USB Port with RS-232 communication, Run/Stop Micro USB Port with RS-232 communication,

Voltage Flow Control, Run/Stop

Chrom Tech Flash Pumps

Prime/purge valve Real-time pressure monitoring with upper and lower pressure limitsDrip tray and leak sensorPulse dampenerSelf-flushing pump heads3 year warranty

Simple keypad controls, LED displaySingle pistonElectronic rapid refill mechanismMotor stall detector 3 year warranty

A versatile series of pumps designed specifically for Flash Chromatography Applications


306®Chrom Tech


Chrom Tech/SSI Pump Replacement PartsMAX PUMP FLOW RATES 5 – 6 mL/min 10 – 12 mL/min 10 mL/min 30 – 50 mL/min 40 mL/minFOR LEGACY PUMPS: P-1500,

Q-Grad, Essence, P-2005, P-2500

P-1010(B), P-2010(B), P-1524CP, P-2024(B), Series 2, Series 3,

Constant Pressure, Flash 2000

P-010(S), Series 1

P-1040(B), P-2040(B), P-2100 (B),

P-1100, Series 2, 3, Flash 2000,

Prep 100

P-040(S), Series 1

PUMP HEAD MODEL L HEAD M HEAD MM HEAD H HEAD MH HEADFOR NEXT GENERATION PUMPS: PBD-LST05(S/B),

PB-LST05(S/B), P-LL05(S/B),

P-LST05(S/B), P-LS05(S/B),

P-CP12S

PBD-LST10(S/B), PB-LST10(S/B),

P-LL10(S/B), P-LST10(S/B), P-LS10(S/B), P-LD12(S/B), P-LD36(S/B),

P-CP24S

P-ML10(S/B), P-MX10(S/B),

P-MXT10(S/B), P-MXT10B-MS,

P-M110(S/B)

PBD-LST40(S/B), PB-LST40(S/B),

P-LL40(S/B), P-LST40(S/B), P-LS40(S/B),

P-LD100(S/B), P-PR100(S/B),

P-CP100S, P-0100F(B)

P-ML40(S/B), P-MX40(S/B),

P-MXT40-(S/B), P-M140(S/B)

Piston assembly, ea P-1597 P-1097 P-0101 P-1198 P-1298Standard piston seal kit, ea P-1595 P-1095 P-0103 P-1096 P-1295Standard piston seals, 10/pk P-1591 P-1090 — P-3003 —Biocompatible piston seal kit*, ea P-1595B P-1095B P-0103B P-1096B P-1295BPiston seal kit, Organic, ea P-1599 P-1099 P-0109 P-3009 P-1299Biocompatible Piston Seal Kit, Organic, ea — P-1099B P-0109B — —Check valve SS (inlet & outlet) P-1085-2 P-1085 P-1085-2 P-1085 P-1085-2Check valve PEEK kit (inlet & outlet) P-1086 P-1086 P-1086 P-1086 P-1086Replacement capsules, SS (10/pk) P-1075 P-1075 P-1075 P-1075 P-1075Replacement capsules, PEEK (10/pk) P-1076 P-1076 P-1076 P-1076 P-1076Self flush check valve kit P-1084 P-1084 — P-1084 —Self flush assembly, SS — — P-1082 — P-1081Self flush assembly PEEK — — P-1088 — P-1089Inlet filter assy (fitting & element) 06-0110 06-0110 06-0110 06-0110 06-0110Inlet filter element, 20 µm (2/pk) P-1170 P-1170 P-1170 P-1170 P-1170Outlet filter element, SS (2/pk) P-1175 P-1175 P-1175 P-1172 P-1172Outlet filter elements for PEEK Pumps, ea P-1171 P-1171 P-1171 P-1171 P-1171Prime purge valve rebuild kit, SS P-1177 P-1177 P-1177 P-1177 P-1177Prime purge valve rebuild kit, PEEK P-1178 P-1178 P-1178 P-1178 P-1178Prime purge valve assy, SS, ea 22-0292 22-0292 22-0292 22-0292 22-0292Prime purge valve assy, PEEK, ea 06-0115 06-0115 06-0115 06-0115 06-0115Pulse dampener w/transducer, SS—for models with real time pressure monitoring

P-1061 P-1061 P-1061 P-1061 P-1061

Pulse dampener w/transducer, PEEK— for models with real time pressure monitoring

P-1062 P-1062 P-1062 P-1062 P-1062

Pulse dampener (no transducer), SS — P-1065 P-1065 P-1065 —Pulse dampener (no transducer), PEEK — P-1066 P-1066 P-1066 —Pulse dampener rebuild kit P-1063 P-1063 P-1063 P-1063 P-1063

*Seal kits include: Self flush seal, O-ring, primary seal, removal tool

Standard Seals—Ultra High Molecular Weight PolyethyleneOrganic seals—Graphite-filled PTFE for use with harsh chemicals

TECH TIP | Seal OptionsNEW!

Biocompatible Seal OptionNow offering biocompatible seals which contain a fluoropolymer energizer (vs the Stainless Steel Energizer)



Other Chrom Tech Pump Supplies

The Model LP-21 LO-Pulse� pulse damper is a patented wide dynamic range pulse damper designed for use with single piston reciprocating HPLC pumps. It uses 1/4-28 SSI-type fittings and operates up to 6,000 PSI.The LO-Pulse� pulse damper reduces pulsations by compressing a fluid held within the bottom cavity of the unit. This fluid is isolated from the LC mobile phase by a durable but flexible inert diaphragm. As the HPLC system pressure increases, fluid in the bottom chamber is compressed. When the LC pump piston is retracting, the compressed fluid expands maintaining system pressure and, more importantly, keeps the mobile phase flowing at a constant rate. When the system pressure is at its maximum allowable pressure (6,000 PSI), the volume of mobile phase in the LO-Pulse is only 0.9 mL.

MODEL LP-21 LO-PULSEPART NO DESCRIPTION20-0218 Model LP-21 LO-Pulse

20-0220 PEEK Model LP-21 LO-Pulse

12-0527 Low cost LO-Pulse (without case)

12-0537 Low cost PEEK LO-Pulse (without case)

P-1063 Spare parts kit (includes diaphragm, o-rings, tools)

Model LP-21 LO-Pulse

TECH TIPIdeal to have at least 500 PSI minimum back pressure for optimum efficiency.

The noise level in the detector resulting from pump pulsations can significantly affect precision in qualification and the detection limit of trace components. The LO-Pulse� pulse damper smooths pump pulsations and maintains constant flow in flow sensitive detectors.

6000-054 U-400/U-401MISCELLANEOUS SUPPLIES FOR CHROM TECH PUMPSPART NO DESCRIPTIONREPLACEMENT LOW PRESSURE INLET TUBINGT-10201 1/8" OD FEP Fluoropolymer tubing, 1/16" ID, 10' lengthREPLACEMENT LOW PRESSURE INLET FITTINGS FOR 1/8" OD TUBINGXP-301 1/4-28 Flat-Bottom Delrin Nut & ETFE Ferrule (P-300), eaHIGH PRESSURE OUTLET FITTINGS FOR TUBING ODU-400 10-32, SS Nut, ea 1/16"

U-401X SS Ferrule, 10/pk 1/16"

6000-054 10-32, PEEK Nut, ea 1/16"

6000-051 PEEK Ferrule, 10/pk 1/16"

25-0155 SS Bulkhead, 2 µm outlet filter, ea 1/8"

051018 Filter Closure, ea 1/8"

01-0141 SS Gland Nut, 10/pk 1/8"

01-0143 SS Ferrule, 10/pk 1/8"REPLACEMENT HIGH PRESSURE OUTLET TUBING1531 1/16" OD PEEK tubing, 0.010" ID, 5' length

U-106 1/16" OD SS tubing, 0.010" ID, 5' length

The recommended minimum back pressure is 50 PSI for optimum check valve performance. For pumps with a pulse dampener, we recommend a minimum of 500 PSI back pressure. If your application will not provide adequate back pressure, adding tubing for restriction to the outlet of the pump is recommended.

TECH TIP

Contact Chrom Tech Support Desk for quotes and recommendations—[email protected]

TECH TIP | CUSTOM PUMP OPTIONS:

Custom jacketed

heads

CHROM TECH PUMP

TYPICAL (MOST MODELS)

CUSTOM OPTIONS

Pump outlet 1/16" OD Outlet 1/8" OD outletPump inlet 1/8" OD

Low Pressure1/8" OD

High pressure Material of Pump Head/Tubing

SS or PEEK

Hastelloy C,Titanium

Other Jacketed heads


308®Chrom Tech


L-3320 Autosampler

The L-3320 is a low cost, high-performance HPLC autosampler with features such as high sampling precision, low cross-contamination, high durability and easy maintenance.

High precision injector provides excellent accuracy and sampling linearity Proprietary needle design significantly reduces sample residue contaminationµL pick-up mode achieves zero sample loss

SPECIFICATIONSSample Volume: Standard: 2*48 1.5 mL vials;

Optional; 96-hole panel, 384-hole panelVolume of Sample Loop:

Standard: 50 µL; Optional: 10, 20, 100 µL

Injection Pump: Standard: 250 µL; Optional: 100 µLSampling Mode: Full loop, partial loopfill and µL pick-upRepeatability: Full loop: RSD ≤ 0.3%;

Partial loop: RSD ≤ 0.5%; µL pick-up: RSD ≤ 1.0%

Cross Contamination:

< 0.05%

Max Sampling Volume:

Full loop = loop volume; Partial loop = 1/2 loop volume; μl pick-up = (loop vol.- 3 × needle vol.)/2

Linearity: > 0.999Max Pressure: 6,000 PSISample Tray: 2 – 48 position trays for 2 mL vials

(12 x 32 mm)Optional 96 well plate tray

User Interface: Clarity Software (sold separately) vis RS-232

Weight: 12.6 KgDimensions: (d x w x h)

17.8" x 14.1" x 9.6"

Power Supply: 100 VAC – 240 VAC, 50/60 Hz, 110W max

L-3320 AUTOSAMPLERPART NO DESCRIPTIONLC-L3320 L-3320 AutosamplerREPLACEMENT PARTS1020001533 Auto Injection Valve

1020001545 Syringe, 30 mm, 250 µL, long screw

1020001546 Distribution Valve, PCTFE

2010001462 Sample Needle

1020000170 Sample Rack - 48-position

L-3320 provides excellent sampling linearity.

L-3320 provides excellent accuracy and linearity of sample injection.

Peak 1Peak 2Peak 3

Peak 1

Peak 2Peak 3




Vacuum Degasser

VACUUM DEGASSER SPECIFICATIONSVolume/Channel: 480 µL Flow Rate/Channel: 1.0 mL/min (for 70% gas removed from MeOH)1

Pressure Drop2: 1.37 mm Hg/mL/min Flow Path ID: 0.45" (1.14 mm)

Wetted Pathways: Metal-free, PEEK and PTFE Connections: 1/4-28 flat-bottom ports3

Signal: 5 mVDC/1 mm Hg absolute from 20 – 800 mm Hg (0.100VDC at 20 mm Hg; 4,000 VDC at 800 mm Hg)

Accuracy: ±1.0% of reading ±0.010VDC from 20 – 800 mm Hg

Display: LED indicator lights Dimensions: 2.87" W x 5.00" H x 9.81" D

Power Requirement: 100 to 240 VAC (±10%), 1A, 50 to 60 Hz (±3 Hz), AC adapter included. Four interchangeable plugs are supplied with the AC adapter: North America/Japan, U.K., Continental Europe and Australia

CE Certification: These products have been certified under the following CE testing standards: EN61326-1; EN55011; EN61300-3-2; EN61300-3-3 and ENG61010-1

Patents: Degasser technology protected by U.S. Patents 5,340,384; 6,248,157 and 6,494,938

The Systec HPLC vacuum degassing systems are high-efficiency, in-line modules that remove dissolved gases from the mobile phase. Their unique design assures reliable continuous operation and the highest level of performance available.Flow-through vacuum degassing chamber with a single amorphous perfluorinated copolymer (Systec AF®) degassing membrane, enabling degassing efficiency 50 times that of PTFE.The ZHCR (Zero Hysteresis / Constant Run) vacuum pump employs a patented closed-loop, micro-stepping rpm control strategy permitting the pump to run with continuously variable speed, providing quick pull-down at high rpm, and then sustaining a consistent vacuum level at low rpm.Fluctuations in detector baseline due to changes in vacuum level are eliminated by not having to repeatedly stop and start a single-speed pump. This also greatly reduces wear and noise.The brushless motor enables quiet operation and is appropriate for environments where solvent vapors may be present.

Ultra-high efficiency degassingContinuous monitoring for leaks and errorsQuiet, long-life operationDesigned for HPLC — No solvent compatibility issues

1) Flow rate that will remove 70% of dissolved gas from a single channel of pure methanol.2) Estimated tubing pressure per unit change in flow assuming laminar flow with a viscosity of 1.0 cp3) Fittings are not included with the unit. Accepts 1/4-28 flangeless fittings.

Tubing ConnectionsETFE tubing is an ideal choice for the fluid pathway between the vacuum degasser and the system’s pump. Its low gas permeability will help ensure the mobile phase solvents do not re-gas while in transit.

TECH TIP

XP-201

VACUUM DEGASSER ORDERING INFORMATIONPART NO DESCRIPTIONVD-2101 2 Channel ModelVD-4101 4 Channel ModelRECOMMENDED FITTINGS AND TUBING (NOT INCLUDED WITH UNIT) :XP-201 Flangeless Fitting Delrin®, Black 1/4-28 Flat-Bottom, for 1/16" ODXP-301 Flangeless Fitting Delrin®, Black 1/4-28 Flat-Bottom, for 1/8" OD1516XL EFTE Natural Tubing, 0.020" ID, 1/16" OD, 100' length1528XL EFTE Natural Tubing, 0.030" ID, 1/16" OD, 100' length1530 EFTE Natural Tubing, 0.062" ID, 1/8" OD, 5' length1530XL EFTE Natural Tubing, 0.062" ID, 1/8" OD, 100' length


310®Chrom Tech


SPECIFICATIONSTemp Range: 10 ° above ambient to 100 °C

Recomm. Flow Range: Up to 8 mL/minTemp Set Increments: 0.1 °C increments

Temp Accuracy: ±2 °C over entire range. The setpoint changes slightly depending on composition and mobile phase flow rate

Temp Repeatability: ±1 °CTemp Stability: ±0.2° C

Thermal Safety cutoff: 118 °C, self-resettingStabilizing Time: 30 min to 100 °C for "ready" at 2 mL/min. For analyses requiring high precision,

wait 30 min after the READY light illuminates before beginning an analysisAvg Cooling Time: 30 min to 10 °C above ambient at 2 mL/min from 100 °C (with cover off)Column Capacity: Up to six (6) analytical or GPC columns, Up to three (3) 3/8" x 30 cm columns,

or four (4) 1/4" x 30 cm columnsChamber Material: Anodized, solvent resistant aluminum

Power Requirement: 100-240 VAC (+/- 10%), 50/60 Hz, 120 WDimensions: (h x w x d) External: 6.4" H x 5.1" W x 19.6" D (16.3 x 13 x 50 cm)

Internal: 1.6" H x 2.7" W x 16.2" D (4.1 x 6.9 x 41 cm)Weight: 15 lbs (6.8 kg)Control Front keyboard control, blue LED, 5-digit display

Column Heaters

NEXT GENERATION COLUMN OVEN ORDERING INFORMATIONCATALOG NO DESCRIPTIONH-705 Next Generation Column Oven with updated electronics for higher performance and increased accuracy

H-705 Column OvenUpdated electronics with higher performance and increased accuracyFront keypad control with 5-digit, blue LED displayCompact footprint requires less bench spaceLarge capacity with no need for special blocks or insertsTemperature is maintained over entire length of fluid pathUniversal power supplySelf-resetting thermal safety cutoff at 118° CAnodized, solvent-resistant aluminum column chamber

Temperature changes throughout the day, and even drafts in your laboratory can adversely affect results. The H-705 column oven accurately maintains temperature within ± 0.2°C to provide precise control and repeatable results that increase the accuracy and consistency of your chromatography.All critical elements—columns, injector, and precolumns—are enclosed in the oven chamber. Constant temperature is maintained over the entire length of the fluid path. Mobile phase is used as the transfer medium so temperature is unaffected by flow rate. The mobile phase passes through an innovative preheater plate within the oven chamber before connecting to the column. The tubing mounted within this plate is 0.010" ID x 50 cm long. Maximum delay volume is 25 µL, though the tubing is crimped in a saw-tooth configuration to minimize volume and optimize heat transfer, as a result, delay volume is only 7.5 µL.

The thermal gradient being measured is solvent temperature entering the column versus that exiting the column. Better separation can be expected if this temperature differential is minimized.

H-705 Column Heater with innovative solvent preheater

Standard Preheater Block

Conventional Oven without preheater

Thermal Gradient vs. Set Point Temperature (Based on 25 cm column)

H-705 replaces legacy H-605 column heater.

030 40 50 60 70 80

5101520253035

Set Point Temperature (°C)

Ther

mal

Gra

dien

t (°C

)




Column Heaters

H-105 Column HeaterHeats multiple columnsPreheats the mobile phaseInjection or switching valves in the heated compartmentTemperature stability

The H-105’s microprocessor controlled heating provides stable and accurate temperature control, reproducible retention times, and stable baselines for temperature sensitive detectors. Increasing column temperatures reduces peak tailing due to surface silanol interactions, improves efficiency, reduces backpressure and prevents column contamination.The column, preheater, and installed valves in the heated cavity are easily accessed through an insulated cover held in place on the top of the unit with thumbscrews. Inadvertent solvent leaks are easily detected and directed away from heater electronics by a drain tube in the heated compartment connected to a bulk head fitting on the back of unit.

H-105 COLUMN HEATERPART NO DESCRIPTIONH-105 Column heater, 120 V

H-105-50 Column heater, to fit 50 cm columns, 120 V

H-105-HT Column heater, high temp, up to 150 ° C, 120 V

H-105-SPEC Column heater custom configuredCOLUMN HEATER ACCESSORIESHX-101 Spare heat exchanger

7725I Sample injector with switch built-in

MonoSLEEVE� & MultiSLEEVE� Controllers & HeatersTemperature Range: 5 °C above ambient to 85 °CTube style design: Unsnap for easy column insertion & removalPlug & Play smart heater technology, self calibrating

HOT SLEEVE & CONTROLLERPART NO DESCRIPTIONH-2001C MonoSleeve single column heater controller, includes: MonoSLEEVE Controller,

Power Supply, USB Cable, GUI, and Manual. Hot Sleeve+ sold separatelyH-2004C MutliSleeve 4 column heater controller, includes: MultiSLEEVE Controller, Power

Supply, USB Cable, GUI, and Manual. Hot Sleeve+ sold separately.H-2005CS 5 cm Hot Sleeve+, requires MonoSLEEVE controller — sold separatelyH-2010CS 10 cm Hot Sleeve+, requires MonoSLEEVE controller — sold separatelyH-2015CS 15 cm Hot Sleeve+, requires MonoSLEEVE controller — sold separatelyH-2025CS 25 cm Hot Sleeve Plus, requires MonoSLEEVE controller — sold separately

H-2030CS 30 cm Hot Sleeve Plus, requires MonoSLEEVE controller — sold separately

HX-038-EXP 3.8 µL Preheater, 1/16" OD x .005" ID x 30 cm, designed to work with EXP fitting

TECH TIPWhen heating your column above 40 °C, it’s important to preheat your mobile phase so a temperature gradient does not occur along the column.Add 10 cm to your column length when ordering your Hot Sleeve and the HX-038-EXP preheater will fit inside the heated column jacket.

SPECIFICATIONSTemp range: 5 ° above ambient to 100 °C

5 ° above ambient to 150 °C (H-105-HT)Temp stability: ±0.1 °C (H-105, H-105-50)

Operating voltage: 120 VAC or 240 VACCase:

(w x l x h)20 x 57 x 13 cm (H-105) 20 x 65 x 13 cm (H-105-50) 20 x 76 x 13 cm (H-105-70)

Heated cavity : (w x l x h)

9 x 44 x 7 cm (H-105) 9 x 58 x 7 cm (H-105-50) 8.3 x 71 x 6.5 cm (H-105-70)

HX-038-EXP(sold separately)

MonoSLEEVE� is the next generation of the original HotSLEEVE controller. With it’s new advanced “Plug-and-Play” technology, MonoSLEEVE can accommodate single HotSleeve Plus column sleeves of different sizes without having to recalibrate to each individual sleeve. The MultiSLEEVE controller is used for applications which require multiple heating zones or multiple LC system heating. Used in conjunction with the HotSleeve Plus heaters, it maintains four independent channels simultaneously and accurately while reducing overall equipment costs.

An optional injection or switching valve can be mounted in the heated compartment. Heating the valve provides sample and mobile phase preheating. Multiple columns can be stored in the H-105 and conveniently selected with a switching valve.

EXP Nut—15-20-03930Hand-tight to 8,700 PSIWrench-tight to 20,000 PSI

EXP Ferrule-15-24-03832


312®Chrom Tech


ECOM FIXED WAVELENGTH UV DETECTORSPART NO DESCRIPTIONFIX21000 Fixed Wavelength Single UV Detector, specify wavelength at time of order

FIX22000 Fixed Wavelength Dual UV Detector, specify wavelength at time of orderREPLACEMENT PARTS22590001 Deuterium lamp

ECOM APPATITE F IXED WAVELENGTH DETECTORDE00000X Apatite UV-VIS Fixed Wavelength DetectorREPLACEMENT PARTS254-12-0.5-M 254 nm Interference Filter

7900000X Analytical Cell HPLC

PREPARATIVE CELL PLCC-15* SPECIFICATIONSVolume/Optical Path: (adjustable) 45 µL/0.3 mm;

55 µL/1.4 mm; 70 µL/2.4 mmCell Connecting: tubing with OD = 1/8",

thread 1/4"-28Maximal Flow Rate: 500 mL/min*Supplied with unit


Detectors

Fixed Wavelength DetectorsSPECIFICATIONS

ECOM FIXED WAVELENGTH ECOM APPATITE FIXED WAVELENGTH

Fixed Wavelength: 200 – 600 nm (256 elements on CCD) (Fixed wavelength set in production)

200 – 600 nm (optional up to 800 nm) (Fixed wavelength set in production)

Bandwidth: According to filter usedLight Source: Deuterium discharge lampLinearity: Better than 2%Typ. Spectral Half-Width: 8 nmAccuracy of Adj. λ: ± 1 nmNoise: ± 5·10-5 AU (254 nm, TC 0.75 s)

(with Test Cell)± 5·10-6 AU (with empty cell 254 nm)

Drift at Test Cell: 1 x 103 AU/hr (254 nm after 1 h)Materials: PTFE; fused silica; stainless steel PTFE, fused silica, stainless steel

(depends on flow-cell)Time Constant: 0.5 s; 0.75 s, 1 s or 2 s (T63

0.3s;0.4s;0.6s;1s)Ca. 1 s

Digital Output: 1 V/AU 1 V/AUInterface: RS-232Power Supply: 24 – 36 V DC 100-240 V 50/60 Hz 110VAPower Input: 48 WDimensions: (w x h x d)

5.2" x 6.6" x 15.2" (131 x 167 x 386 mm)

5.9" x 5.5" x 10.6" (150 x 140 x 270 mm)

Weight: 7 lbs 7.5 lbs

Built in lamp with working hours counterEasy replacement of flow cellSophisticated diagnostic software

This fixed wavelength UV detector is suited for preparative and flash chromatography applications.

ECOM FIXED WAVELENGTH

Apatite is a detector with an interference filter. By means of this filter, this unit can be adjusted at one fixed wavelength in range of 200 – 600 nm (optionally up to 800 nm, filter is not included in price). The unit is designed for use in routine analytical chromatography applications.This unit is easy to operate; reference and sample signals are available for detector diagnostics as well as information on lamp working hours. Output signal is available in digital form on the output connector. The unit is supported in Clarity (CT-C50). The detector is equipped with a high standard deuterium lamp in a special socket that enables easy changing. It is possible to change the interference filter at customer’s preferences.

ECOM APPATITE FIXED WAVELENGTH



Detectors

UV/VIS Variable Wavelength Detectors

ECOM VARIABLE WAVELENGTH DETECTORSPART NO DESCRIPTIONUV-2600 Var λ Detector, 190 – 600 nm, analytical

UV-2800 Var λ Detector, 190 – 800 nm, analytical

UV-2800CE Var λ Detector, 190 – 800 nm, CEREPLACEMENT PARTSADA6000X Analytical flow cell, 2.0 mm path length, AC02

ADA4000X Test flow cell TC01

ADA33000 Deuterium lamp

2052B900 Tungsten lamp with cable and connector (for ECOM UV 2800 only)

RIGOL VARIABLE WAVELENGTH DETECTORSL-3500 Var λ Detector, 190 – 800 nm, analytical

L-3500-FC Analytical flow cell, 10 mm path lengthREPLACEMENT PARTSL-3500-D2 Deuterium lamp

L-3500-W Tungsten lamp


SPECIFICATIONSECOM UV2600 & UV2800 RIGOL L-3500

Wavelength Range: UV 2600: 190 – 600 nm UV 2800: 190 – 800 nm

190 – 800 nm

Wavelength Accuracy: ±1 nmSampling Speed: up to 100 HzDrift: 1 x 10-4 AU/hrNoise: ±3 x 10-6 AU at 254 nm,

TC 1s, 10 Hz±0.5×10-5 AU (JJG)±0.35×10-5 AU (ASTM)

Light Source: Deuterium Deuterium, TungstenInterface: ECOMAC or Clarity Software (sold

separately) via RS-232 or EthernetClarity Software (sold separately) via RS-232

Dimensions: (d x w x h) 19.6" x 11" x 5.5" 18.2" x 14.4" x 5.6"Weight: 20 lb 27.8 lbElectrical: 100 – 240 V 50/60 Hz 100 VA 100 - 240 V, 50/60 Hz, 90 W max

Spectral Half-Width: 6 nmReproducibility: ±0.5 nmTime Constant: 20 – 10,000 msDigital Output: 1 V/AUAnalog Output: 1x configurableWetted Materials: Flow cell dependent—fused silica, PTFE, SST, Vespel, PEEKDisplay, Keypad: VFD 140 x 32 pixels, 10 push buttons

Spectral Width: 8 nmWavelength Precision: 0.2 nmLinear Range: >5x10-4 (JJG) >2.5 AU (ASTM)Flow Cell Pressure: 10 MpsFlow Cell Light Path: 10 mmFlow Cell Volume: 12 µLDetection Limit: 5 x 10-9 g/mL

ECOM’S UV 2600/2800 may be used for analytical applications as well as for preparative/flash chromatography, according to the selected cell. It is easy to operate; light intensities for reference and sample channels are available for detector diagnostics as well as information on lamp operating hours. The detector performs automatic wavelength calibration after the lamp has been switched on. High standard deuterium lamp in a special socket enables easy exchange. Output signal is available in both digital and analog form. Detector could be controlled and used together with Clarity or ECOMAC software via RS-232 or Ethernet interface.The flow cell can be easily removed from the front of the unit. Flow cell AC05 is included as component of the detector.

ECOM UV2600 & UV2800

L-3500 is a variable-wavelength UV-Visible light detector, with wavelength range 190-800 nm. Designed & developed by RIGOL’s patented technology, and manufactured through advanced processing, L-3500 owns world-class performance parameters: data rate up to 100 Hz, very low noise & drift level and detection limit. It can be widely used for analysis of compounds with UV absorbance.

RIGOL L-3500


314®Chrom Tech


SPECIFICATIONSECOM FLASH 10 ECOM FLASH 14 SCHAMBECK 4245

Wavelength Range: See ordering information 190 – 900 nmScan: N/A 200 – 800 nm, 5 Hz, step 3 nm Optional online scanTypical Spectral Half-width: F10-400: 8 nm F10-800: 10 nm

F14-400: 8 nm F14-800: 10 nmAccuracy of Adjustment: ±1 nm ± 2 nmLinearity: > 2.0 AUReproducibility: ± 0.5 nmLight Source: Deuterium discharge lamp (and Halogen lamp to 840 nm) Deuterium Lamp, Tungsten LampNoise: ± 5 x 10-5 AU (at 254 nm TC 0.75 s) ± 1 x 10-5 AU (at 240 nm, 1 sec. Rise time)Drift: 1 x 10-3 AU/hr (at 254 nm after 1 h) 2 x 10-4 AU/hWetted Materials: PTFE; fused silica; stainless steel Stainless Steel; PEEKTime Constant (T90): 0.5 s; 0.75 s; 1 s or 2 s (T63 0.3s; 0.4 s; 0.6 s; 1 s)Digital Output for Integrator: 1 V/AU 1 V/AU (in digital form only) 1 V/AU per channelAnalog Outputs: 4 x 1 V: 5; 3; 2; 1; 0.5; 0.25; 0.1; 0.05 AU/V

for integrator w/sensitivity switchingN/A 1 x 1 V (single wavelength)

2 x 1 V (dual wavelength)Interface: RS-232Power Supply: 90-264 V 100 - 250 V (47—63 Hz)Power Input: 100 VADimensions: 5.3" x 6.7" x 16.5" (135 x 170 x 418 mm) 11.0" x 5.1" x 18.2" (280 x 130 x 463 mm) 12.2" x 6.5" x 18.8" (310 x 165 x 478 mm)Weight: 13.2 lb (6.0 kg) 19.8 lb (9.0 kg) 15.4 lb (7.0 kg)

Absorbance measuring on four wavelengths simultaneouslyUp to 250 mV Analog Offset ProgrammableEasy service and diagnostics using display and keypad

10 step programmable wavelength detector with optional dual wavelength and online scanIntegrated peak detector works as a basic fraction collector— Program start/end peak detection level with selectable time delay

Absorbance measuring on four wavelengths simultaneously – or –Continuous 5 Hz spectral scanClarity PDA module extension supported for 3D measurement

Detectors

ECOM FLASH 10 & FLASH 14FLASH 10 MWD FLASH 14 DAD DESCRIPTIONF10-400 F14-400 200 – 400 nm, 4 wavelength, prep flow cell

F10-800 F14-800 190 – 840 nm, 4 wavelength, prep flow cellREPLACEMENT PARTS22590005 22590005 Deuterium lamp with chip

2052B900 2052B900 Halogen lamp (400 – 840 nm range)

3210000X 3210000X-B Preparative flow cell

12L0000X — Analytical flow cell*


UV/VIS Multiple Wavelength & Diode Array Detectors

SCHAMBECK 4245PART NO DESCRIPTION4245 UV/VIS Detector S 4245, 1 Channel

4245-2 UV/VIS Detector S 4245, 2 Channels

4245-2S UV/VIS Detector S 4245, 2 Channels with online scan option stored internally

REPLACEMENT PARTS4010001 Tungsten Lamp for S 4245, preadjusted

4010002 Deuterium Lamp for S 4245, preadjusted

1032009 Flow cell, analytical, SS, 7.9 μl, 10.0mm flow path

10320013 Flow cell, semi-preparative, SS, 2.7 μl, 1.5mm flow path* ECOM Flash detectors are designed for preparative scale chromatography. Analytical flow cells are available with consideration, please contact Chrom Tech technical support to discuss.



Detectors

RI-S2020 Refractive Index Detector

RI-S2020 REFRACTIVE INDEX DETECTORSPART NO DESCRIPTIONS-2020M Refractive Index Detector, Micro

S-2020A Refractive Index Detector, Analytical

S-2020P Refractive Index Detector, Semi-PreparativeREPLACEMENT PARTSRI2000-030 Micro flow cell

RI2000-001 Analytical flow cell

RI2000-031 Semi-Preparative flow cell

RI2000-012 Replacement lamp

RI2000-024 Seal kit

RI2000-006 Purge valve

The Refractive Index Detector S 2020 series provides a consistent enhancement of the already successfully established RID models RI2000 and RI2000-F. The RID S 2020 series offers users 3 times higher sensitivity, (compared to RI2000) stability and reproducibility required for optimal RI detection in HPLC / GPC. By consistently revising the electronic components, it has been possible to significantly improve drift and noiseThe optical system is now better insulated against temperature changes and with programmable temperature settings, ensures a stable baseline and an optimal signal/noise–ratio. The auto zero, purge, polarity, temperature and the frequency for data output are externally controllable by USB or RS232 Port. RID system status - information such as temperature and total voltage can be externally retrieved by RS232 or USB.The Refractive Index Detector S 2020 offers communication interface to acquire data directly with Clarity Chromatography Software without using any external signal interface. The Refractive Index Detector S 2020 includes - micro, - analytical and - semi preparative refractive index detectors.

RI-S2020 SPECIFICATIONSS 2020M S 2020A S 2020P

Detection Method: Deflection Deflection DeflectionRefractive Index Range: 1.00 – 1.75 1.00 – 1.75 1.00 – 1.75Flow Rate: 0.2 – 3.0 mL/min 0.2 – 3.0 mL/min 5 – 50 mL/minFlow Cell Volume: 4 µL 9 µL 13 µLFlow Cell Pressure: 85 PSI 85 PSI 85 PSIDead Volume Into Cell: 6 µL 24 µL 88 µLLinearity Range: 0 – 500 µRIU 0 – 1,000 µRIU 0 – 20,000 µRIUNoise Level: 10 x 10-9 RIU 5 x 109 RIU 10 x 10-8 RIUAutozero Range: Full Range Full Range Full RangeDrift with 1 ml H20/min: < 1 mV/hour < 1 mV/hour < 1 mV/hourPurge Valve: Yes Yes Yes/No (depends on flow)Integrator Output: +/- 1 VoltRecorder Output: +/- 10 mV/ 100 mV/ 1 VoltRecorder Offset: 0 mV/ 10 mV/ 100 mVRecorder Range 8 steps (1:8) – (16:1)Marker: Yes/No



316®Chrom Tech


ZAM 4000 Evaporative Light Scattering Detector

ZAM 4000 EVAPORATIVE L IGHT SCATTERING DETECTORPART NO DESCRIPTIONZAM4000 ZAM 4000 (without Mass flow controller)REPLACEMENT PARTSZAM3000-1 Nebulizer

ZAM3000-2 Nebulizer chamber

ZAM3000-3 drying chamber

ZAM3000-4 Mass flow controller

ZAM3000-5 Main board

The Evaporative Light Scattering Detector ZAM 4000 is an universal detector for HPLC. It is used to analyze components which do not have UV absorption, cannot be separated with an isocratic solvent and must use a gradient elution, which cannot be used with a refractive index detector. Only mobile phases without any buffers should be used.In contrast to other evaporative light scattering detectors all parts of the ZAM 4000 detectors which come in contact with the sample are made of PTFE or glass. By this parts are inert to common solvents and easy to clean. One more advantage of glass parts is the fact that contamination can be located easily. The nebulization takes place in the glass nebulization chamber. From here the aerosol is guided into the evaporation chamber which is made of glass, too. The solvent evaporated and only small sample particles reach the detection chamber. Here this particles pass a beam of bright light. By this the light is scattered in all directions. The scattered light is detected by a photomultiplier in an angel of 120°. The signal is amplified and exported as the detector signal. All parts which get in contact with the sample can be un-mounted and cleaned easily.

ZAM 4000 SPECIFICATIONSDetection Method: Highly sensitive photomultiplier tubeNebulizer Material Drying: Glass, easy to clean, resistant to all common solventsChamber Material: Glass, easy to clean, resistant to all common solventsNebulizer Chamber: Glass, easy to clean, resistant to all common solventsMaterial Light Source: White LEDHPLC Mobile Phase Flow Rate: 0.5 – 3.5 mL/minAdditive Gas Controlling: Fixed gas flow (1.9 L/min.)Gas Consumption: ~ 3.7 L/min.Recorder Output: 0 V - +1.2 VDigital Interface: RS-232Digital Input: AutoZero, Start (Gas on / PMT power) (TTL)Temperature Settings: 35°C - 85°C, ambientData Smoothing: Raw, Fast, Slow, MediumPower: 110 V AC / 220 V ACDimensions (w x h x d): 18 x 49 x 50 cmWeight: 24 kg

Detectors



Detectors

ISCO FOXY FRACTION COLLECTOR SPECIFICATIONSDimensions: (w x d x h)

Foxy R1: 12.25" x 13.0" x 14.0"Foxy R2: 12.25" x 21.0" x 14.9

Inputs: Pump counter1, external peak1, inject, tube advance1, analog peak voltage2

Weight: Foxy R1: 16.95 lbs Foxy R2: 23.4 lbs (with drip tray, no rack)

Outputs: Pump pause3, tube change3

Max Flow Rate: 100 mL/minute Tube Changes:

At detected peaks, plus drop counts, time, orexternal pump counts.

Delay Volume: Diverter valve located at drop former. Delay volume compensation only required for length of tubing to the diverter valve.

System Control:

Operator: front-panel control via touchscreen LCD Integrated systems: direct communication with fraction collector via Ethernet (TCP/IP) and RS-232 serial communications.

Peak Detection: Slope and/or level sense, with or without time window

Operating Voltage:

100/117 VAC 50/60 Hz, 234 VAC 50/60 Hz

These cold room compatible fraction collectors can be adapted to a broad spectrum of applications. The units can distribute fractions into 96 well microplates, standard tube sizes, and bottles. For essentially unlimited volumes, funnel racks can direct fluids to any collection vessel or downstream process. Multiple fraction collectors may be "daisy chained" together to increase your fraction capacity—an exclusive feature from Teledyne ISCO.

Foxy R1 & R2 Fraction Collectors

The two-rack Foxy R2 fraction collector uses radio frequency identification to automatically detect collection racks for easy setup.

Foxy R2 Fraction Collector

ISCO Foxy® R1 & R2 Fraction CollectorsSturdy cast aluminum frameEasy to use symbolic touch screen interfaceBuilt-in Ethernet and RS-232 communication capabilitiesFaster tube changesμL delay volume between diverter valve and drop formerFlow rates up to 100mL/minute

1) High on +3.3 to 5 V or contact closure, active low, 30 ms min, 5 VDC max.2) 0 to 1.0 V nominal, –1.2 to +1.2 V usable, –5 to +5 V max.3) Outputs are open collector active low, 30 ms min, 5 VDC max.

ISCO FOXY FRACTION COLLECTORPART NO DESCRIPTIONFC-R1 Foxy R1, Single rack collector (includes one 13 mm rack)

FC-R2 Foxy R2, 2 rack collector, with rack sensing (includes two 13 mm racks)CONNECTION CABLES FOR FOXY R1 AND R2FCC-474 Remote start signal from HP1100/1200 and peak separation

FCC-170 Pump cable connection (any pump)

FCC-171 Detector cable connection (contact closure or TTL I/O)OPTIONAL RACKS FOR FC-R1 AND FC-R2, EA:FCR-155 (144) 12 mm dia. tubes

FCR-150 (144) 13 mm dia. tubes

FCR-154 (60) 1.5 mL microcentrifuge tubes



FCR-158 (72) MiniVials

FCR-156 (36) 28 mm dia. scintillation vials


FCR-157 (36) 50 mL cone-bottom centrifuge tubes, 28 – 29 mm diameter x 150 mm

FCR-159 (2) 96-well microplatesOPTIONAL RACKS FOR FC-R2 ONLY, EA:FCR-161 Preparative rack with (26) Halar funnels for large fractions (requires qty 1)

FCR-162 Preparative rack with (26) Halar funnels for large fractions (requires qty 1) Organic compatible



318®Chrom Tech


DataApex Clarity Chromatography SoftwareEasy to install and useTools for regulated environmentCompetitive pricing and free software updatesDirect control of many vendors chromatography instrumentsModules for specific calculations and methodology

Clarity is an advanced Chromatography Data Station (CDS) with optional software modules for data acquisition, data processing, and instrument control. Its wide range of data acquisition interfaces (A/D converters, LAN, USB, RS-232) allows connection to virtually any chromatograph.Up to four independent chromatography systems can be simultaneously connected.Clarity can be used with any GC or HPLC. Together with optional control modules and extensions it provides laboratories with a complete chromatography data handling system. The Control modules provide integrated control of selected instruments. Extensions provide functions for specific separation techniques such as PDA or GPC Analysis.Clarity comes with extensive free support from DataApex as well as from the growing community of users in the Clarity forum. Clarity is now compatible with Windows® 10.

Clarity is the most comprehensive of our stations. Its features include data acquisition from multiple instruments, direct control of GCs, LCs and autosamplers using Controls; access to advanced analyses through Extensions; and support of 21 CFR Part 11.

Clarity Lite is a simplified version of Clarity that provides data acquisition from one chromatograph* (up to four detectors sharing a common time-base). Clarity Lite can be easily upgraded at a later date.

O�ine

Clarity Offline allows users to evaluate data and prepare methods. This version cannot acquire data but it can share data or even directly access (through LAN) projects of the other two stations. With Clarity Offline uses are able to work with acquired data on additional computers.

DATAAPEX CLARITY CHROMATOGRAPHY SOFTWAREMODEL DESCRIPTION PART NOSTEP 1 : CHOOSE YOUR SOLUTION PACKAGE(S)Clarity Extensible, Single Instrument SW, CFR21/GLP ready CT-C50Clarity Lite Simplified, Single Instrument SW* CT-C40Clarity Offline Offline version for data processing CT-C59STEP 2 : OPTIONAL EXTENSION MODULES (NOT COMPATIBLE WITH CLARITY LITE)Clarity Add-on Single Instrument Add-on CT-C55SST System Suitability Test CT-A22GPC GPC/SEC data processing CT-A28PDA PDA data processing CT-A29EA Elemental Analysis CT-A30CE Capillary Electrophoresis CT-A31NGA Natural Gas Analysis calculation CT-A32STEP 3 : CHOOSE INSTR UMENT CONTROL OPTION(S)AS Control SW module for autosampler control CT-A26GC Control SW module for GC control CT-A23LC Control SW module for LC control (pump, detector, etc.) CT-A24STEP 4 : DATA ACQUISITION, A/D CONVERTERSColibrick External USB, 1 channel CT-U31Colibrick External USB, 2 channels CT-U32Colibrick External USB, 4 channels CT-U34STEP 5 : USB TO RS232 CONVERTERMultiCOM MultiCOM extends the PC USB Port to 6 COM ports CT-MC01

DataApex Clarity

MultiCOM extends the PC by 6 Com ports (RS232). This enables to connect multiple instruments controlled using the RS232 line. Many of the controlled instruments are connected to the PC via serial cables, which need standard 9-pin (male) connector on the computer side. Modern computers usually do not have more than 1 COM port, and notebooks commonly have none. The MultiCOM RS232 to USB converter is connected to the PC via USB port; these are presently common in both desktop PC’s and notebooks.After the installation, the MultiCOM converter will enable the use of six RS232 compliant serial ports ended with standard DB9M connectors. The MultiCOM converter also includes another USB-A connector for the use with any device with low power consumption, for example the Clarity HW key.The power supply for the MultiCOM converter is normally provided via the USB cable from the computer; however external power supply adapter can also be used.

Contact Chrom Tech Support Desk for a quote specific to the instrumentation in your lab—[email protected]

*Requires A/D converter

*Requires an A/D converter for data collection



SPECIFICATIONSMeasurement Simultaneous data acquisition from up to

four chromatographs, up to 32 signals.Data Acquisition

Any detector with voltage output using DataApex A/D converters or selected digital detectors

A/D Converters

External USB

Regulated Environments

A set of tools for meeting GLP/21 CFR Part 11 requirements, including Audit Trails, Electronic Signature, Password protection, User Accounts, etc

Calibration Internal and external standard calculation methods, calibration of groups of peaks and reference peaks for better identification

Integration More than 25 parameters programmable in time, automatic reintegration, direct graphical modification of the baseline

Automation Sequences, Post Run, Batch processing, Event table, command line parameters

Optional Extensions

GPC, PDA, CE, EA, Validation Kit, SST module

Optional Control Modules

Direct Control of selected instruments: GCs, HPLCs, Autosamplers, Valves, Fraction Collectors, Balances, etc.

Data Export ASCII, AIA, dBaseData Import ASCII, AIAMethod of Calibration History

Each chromatogram can be easily displayed under the same conditions as when it was printed, exported or saved

GCsHPLC SystemsHPLC Components – Detectors, Pumps, Column Ovens, Autosamplers, Fraction Collectors, ValvesAmino Acid AnalyzersBalances

CONTROLS AVAILABLE FOR:

TECH TIPCLARITY CONTROLSControls are software modules that provide an interface with chromatography devices such as Gas Chromatographs, HPLC Pumps, Autosamplers or Valves. Direct control means that the device can be controlled from the Clarity environment. Clarity can store various device methods for each type of analysis and then automatically apply them in a sequence. The control options specific for the controlled device are stored in the measured chromatograms. This ensures traceability of measurement conditions.

The Instrument window is the control center of the whole process of data acquisition and evaluation.

The Chromatogram window displays the chromatogram and results. Users can easily review/edit acquired chromatograms visually in the graph or through Integration table. The Result tables (Results, Summary, Column Performance, etc.) can be easily customized to display the data you want exactly the way you want to see it.

Instrument Window

Chromatogram Window

Monitoring of the signal from detectors

Sequence Tab

Settings of directly controlled equipment

Single Analysis

Method setup Integration parameters

Information Table

Chromatogram review and

modify already measured chro-

matogram

Calibration use sample

as calibration standard

(calibrate or recalibrate)

Print custom-ized reports

from the analysis

Method setup calibrated calculations

DataApex Clarity


320®Chrom Tech


Pickering Post Column Reactors

Works with ALL HPLC Systems Yes YesComponents specifically designed for Post-Column Derivatization Yes No

Pump Technology Syringe ReciprocatingPiston Wash Automatic AutomaticProgrammable System Flush Yes NoColumn Oven Yes NoTemperature Gradient Column Oven Yes No

Automatic Column Oven Cool Down (10 min) Yes No

Electronic Valves Yes NoCheck Valves No YesFlow Restrictors No YesQuick Change Reactor Cartridges Yes NoAll Fluidics on Front Panel Yes NoInert Flow Path Standard CustomLCD Display Graphical TextFull 32 bit PC Control Windows Software Included No

Program Storage Unlimited NoNetwork Enables Yes NoRemote Diagnostics Yes YesReduced Bench Space Yes NoIntegrated Reagent Tray Yes NoIntegrated Spill Tray Yes NoIntegrated Lab Gas Manifold Yes YesReduce Maintenance Costs Yes NoReduce Reagent Usage/Costs Yes No

FEATURES PINNACLE VECTOR

Aminoglycoside Antibiotics Amino Acids Bromate Biogenic Amines Carbamate Pesticides

Chromium VI Formaldehyde Glyphosate Herbicide

Guanidinos

Hexosamines Mycotoxins

Paralytic Shellfish Toxins

Paraquat & Diquat

Polyphoshates/Phosphonates Polyether Antibiotics

Sulfa Drugs

Transition/Rare Earth Metals Trichothecene Mycotoxins

Vitamins B1, B6

APPLICATIONS PINNACLE VECTOR

SPECIFICATIONSPINNACLE PCX VECTOR PCX

Dimensions: (h x w x d)

21.25" x 10.5" x 18.25" (54 x 26.7 x 46.4 cm)

17" x 8.75" x 16" (43 x 21.6 x 41.2 cm)

Weight: 60 lbs (27.2 Kg) – Duplex 25.3 lbs (11.5 Kg)Electrical: 100-120V, 50/50 Hz, 1.7A, 200 W or 200-240V, 50/60 Hz, 0.8A, 200 WMains Voltage: ± 10 % of nominalREAGENT PUMPSFlow Range: 50 μL to 1500 μL/min 0.05 – 2.00 mL/minMax Pressure: 500 PSI 2,000 PSIFlow Accuracy: 3%Flow Precision: 0.5% RSDREACTORTemperature: 41 °F (5 °C) above ambient to 266 °F (130 °C)Dwell Volumes: 0.1 – 3 mLSafety: Thermal safety switch limits temperature to 302 °F to prevent damagePressure: Reaction coil withstands up to 600 PSI (42 bar) inlet pressure at 266 °FCOLUMN HEATER (PINNACLE PCX ONLY)Column 6 or 8 mm OD x 50 – 250 mm in

length (column and guard) N/A

Temperature: holds within ±1 °C above ambient to 75 °C

N/A

The Pinnacle PCX Sigma Series is part of the complete integrated system of instruments, chemicals, columns, methods and support for post-column derivatization. Each component is specifically designed to optimize the sensitivity and selectivity of post-column analysis.

The Vector PCX provides the selectivity and sensitivity required for most standard post-column applications while being reliable and easy to use. Designed as a step-up from the previous model PCX5200, the Vector PCX has several improvements and innovations, featuring:

Inert pumpsPEEK liquid manifoldsIntegrated gas manifoldEasy access and monitoring of fluidicsSimple control interface (no computer required)Reduced bench space profile

The electronic syringe pump provides true pulse-free flow for superior sensitivity and consistencyThe pump cylinder and head is made from a single piece of inert ceramic for durability and non-reactivityElectronic valves eliminate troublesome check valves and allow automated pump flushingInert flow path extends system life and reduces maintenanceColumn oven temperature gradient programming improves separation and run times—Pinnacle PCX is the only post-column system with this feature

Pickering Post Column Derivatization


3218 0 0 . 8 2 2 . 5 2 4 2 | 9 5 2 . 4 3 1 . 6 0 0 0 | w w w. c h r o m t e c h . c o mAuthorizedDistributor

PICKERING POST-COLUMN REACTORS

APPLICATIONREAGENT

PUMPREACTOR VOLUME VOLTAGE PART NO

PINNACLE PCXAmino Acids (OPA Detection), Aminoglycoside Antibiotics, Biogenic Amines, Polyamines, Paraquat/Diquat

Single 0.15 mL 120 V 1153-1011240 V 1153-1012

Amino Acids (TRIONE® Ninhydrin detection), Ochratoxin A, Formaldehyde, Bromate

Single 0.5 mL 120 V 1153-1021240 V 1153-1022

Mycotoxins including Aflatoxins & Fumonisins

Single Knitted 1.4 mL

120 V 1153-1031240 V 1153-1032

Cholesterol Single Knitted2.8 mL

120 V 1153-1041240 V 1153-1042

Carbamate Pesticide, Glyphosate Herbicide, Streptomycin, (OPA detection)

Dual 0.5 mL 120 V 1153-1051240 V 1153-1052

Paralytic Shellfish Toxins Dual Knitted1.0 mL

120 V 1153-1061240 V 1153-1062

Trichothecene Mycotoxins Dual Knitted1.2 & 1.6 mL

120 V 1153-1071240 V 1153-1072

Polyether Antibiotics Dual Knitted1.4 mL

120 V 1153-1081240 V 1153-1082

Voglibose Analysis Single Knitted3.5 mL

120 V 1153-1101240 V 1153-1102

Chromium VI, includes Dead-head Pressure Transducer


120 V 1153-1103240 V 1153-1104

Alprostadil Analysis, includes Dead-head Pressure Transducer


120 V 1153-1105240 V 1153-1106

Pinnacle Dead-head upgrade kit for Pinnacle pressure transducer, recommended when applications call for highly corrosive reagents

1552-0040

VECTOR PCX

Carbamate Pesticides, Glyphosate Herbicide, Streptomycin, (OPA detection)

Dual 0.5 mL 120 V 1154-4051 240 V 1154-4052

Streptomycin Dual 0.5 mL 120 V 1154-4001 240 V 1154-4002

Paralytic Shellfish Toxins Dual Knitted 1.0 mL

120 V 1154-4061240 V 1154-4062

Trichothecene Mycotoxins Dual Knitted1.2 mL and

1.6 mL

120 V 1154-4071240 V 1154-4072

Polyether Antibiotics Inert PEEK Dual

Knitted 1.4 mL

120 V 1154-4081240 V 1154-4082

Voglibose Analysis Single Knitted 3.5 mL

120 V 1154-4101240 V 1154-4102

Amino Acids (OPA detection), Aminoglycoside Antibiotics, Biogenic Amines

Single 0.15 mL 120 V 1154-4011

240 V 1154-4012

Amino Acids (TRIONE® Ninhydrin detection), Ochratoxin A, Formaldehyde, Bromate

Single 0.5 mL 120 V 1154-4021

240 V 1154-4022

Aflatoxins Analysis Single Knitted 1.4 mL

120 V 1154-4031240 V 1154-4032

Since Vector PCX does not have a column oven it is important to use an HPLC column oven to ensure stable column temperature and prevent retention time drifts and separation problems.

NEXT GENERATION COLUMN OVENPART NO DESCRIPTIONH-705 Next Generation Column Oven

Next Generation Column Oven (sold separately)

SafeguardsPost-column Reagent BackflowVector PCX: A pressure switch installed between LC (eluent) pump and sample injector turns off power to reagent pumps and reactor when the pump pressure drops to 425 PSI, ensuring reagent will not flow upstream and damage the column. The Vector PCX will not restart automatically.Pinnacle PCX: In-line check valve: Prevents reagent back flow into the column when HPLC pressure drops.

Post-column System Over-pressureA relief valve pre-calibrated to open at 485 PSI prevents rupture of the post-column reactor tubing in the event of downstream blockage, and reduces the possibility that all or part of the reagent flow will be diverted to the column.

Detector Noise, PrecipitationBack-pressure regulator applies 7 bar (100 PSI) to the detector noise and precipitation due to solvent outgassing or boiling adjustable (2 – 10 bar).

TECH TIPPINNACLE DEAD-HEAD PRESSURE TRANSDUCERSome post-column applications call for highly corrosive reagents, which will damage the Pinnacle pressure transducer. We now have a dead-head kit available for the Pinnacle pressure transducer. This will allow you to record the reagent pressure without passing corrosive reagent through the pressure transducer. A dead-head upgrade kit is available or you can purchase a brand new Pinnacle pre-plumbed with the dead-headed pressure transducer.

Pickering Post Column Derivatization

See Next Generation Column Oven (pg 310)


322®Chrom Tech


AMINO ACID ANALYSIS KITSPART NO DESCRIPTION0352-0061 30-MINUTE HIGH EFFICIENCY COLLAGEN HYDROLYSATE KIT:1154110T 30-Minute Sodium Cation-exchange Column 4.6 x 110 mm &

1700-0070 amino acid test mixture1700-3102 Cation-exchange GARD™ assy: Holder w/2 replaceable GARD™Na220 Sodium Diluent, pH 2.20, 4 x 250 mLNa315 Sodium Eluent, pH 3.15, 4 x 950 mLNa425 Sodium Eluent, pH 4.25Na640 Sodium Eluent, pH 6.40RG011 Sodium Column Regenerant, 950 mLT100C TRIONE® Ninhydrin Reagent, 4 x 950 mL (4-month shelf life)012506C Sodium Calibration Standard, for collagen hydrolysate,

0.25 µmole/mL, 5 mL0352-0062 KIT IDENTICAL TO 0352-0061 WITH T200 REPLACING T100C:T200 TRIONE® Two-part Ninhydrin Reagent, prepares 4 x 900 mL0352-0063 KIT IDENTICAL TO 0352-0061 WITH ITEMS BELOW REPLACING T100C:OD104 OPA Diluent, 4 x 950 mLO120 o-Phthalaldehyde, 5 g3700-2000 Thiofluor™, 10 g (2 ea per kit)0352-0057 30-MINUTE HIGH EFFICIENCY PROTEIN HYDROLYSATE KIT:1154110T 30-Minute Sodium Cation-exchange Column 4.6 x 110 mm

& 1700-0070 amino acid test mixture1700-3102 Cation-exchange GARD™ assy: Holder w/ 2 replaceable GARD™Na220 Sodium Diluent, pH 2.20, 4 x 250 mLNa315 Sodium Eluent, pH 3.15, 4 x 950 mLNa425 Sodium Eluent, pH 4.25Na640 Sodium Eluent, pH 6.40RG011 Sodium Column Regenerant, 950 mLT100C TRIONE® Ninhydrin Reagent, 4 x 950 mL (4-month shelf life)012506H Sodium Calibration Standard, for protein hydrolysate,

0.25 µmole/mL, 5 mL0352-0058 KIT IDENTICAL TO 0352-0057 WITH T200 REPLACING T100C:T200 TRIONE® Two-part Ninhydrin Reagent, prepares 4 x 900 mL0352-0059 KIT IDENTICAL TO 0352-0057 WITH ITEMS BELOW REPLACING T100C:OD104 OPA Diluent, 4 x 950 mLO120 o-Phthalaldehyde, 5 g3700-2000 Thiofluor™, 10 g (2 ea per kit)0352-0020 30-MINUTE HIGH EFFICIENCY OXIDIZED FEED HYDROLYSATE

KIT:1154110T 30-Minute Sodium Cation-exchange Column 4.6 x 110 mm

& 1700-0070 amino acid test mixture1700-3102 Cation-exchange GARD™ assy: Holder w/ 2 replaceable GARD™Na220 Sodium Diluent, pH 2.20, 4 x 250 mLNa270 Sodium Eluent, pH 2.70, 4 x 950 mLNa425 Sodium Eluent, pH 4.25Na640 Sodium Eluent, pH 6.40RG011 Sodium Column Regenerant, 950 mLT100C TRIONE® Ninhydrin Reagent, 4 x 950 mL (4-month shelf life)1700-0155 Sodium Calibration Standard, for oxidized feed hydrolysate,

0.25 µmole/mL, 5 mL0352-0021 KIT IDENTICAL TO 0352-0020 WITH T200 REPLACING T100C:T200 TRIONE® Two-part Ninhydrin Reagent, prepares 4 x 900 mL

AMINO ACID ANALYSIS KITS (CONTINUED)PART NO DESCRIPTION0352-0022 KIT IDENTICAL TO 0352-0020 WITH ITEMS BELOW REPLACING T100C:

OD104 OPA Diluent, 4 x 950 mL

O120 o-Phthalaldehyde, 5 g

3700-2000 Thiofluor™, 10 g (2 ea per kit)

AT30SH STANDARD 60-MINUNTE PROTEIN HYDROLYSATE KIT:

1193250 Sodium Ion-exchange Column, 3.0 x 250 mm (with test mixture 1700-0070)

1700-3102 Cation-exchange GARD™ assy: Holder w/ 2 replaceable GARD™

Na328 Sodium Eluent, pH 3.28, 4 x 950 mL


T100C TRIONE® Ninhydrin Reagent, 4 x 950 mL (3-month shelf life)

RG011 Sodium Column Regenerant, 950 mL

Na220 Sodium Diluent, pH 2.20, 4 x 250 mL

012506H Sodium Calibration Standard, for protein hydrolysate, 0.25 µmole/mL, 5 mL

0352-0030 KIT IDENTICAL TO AT30SH WITH T200 REPLACING T100C:

T200 TRIONE® Two-part Ninhydrin Reagent, prepares 4 x 900 mL

AO30SH KIT IDENTICAL TO AT30SH WITH ITEMS BELOW REPLACING T100C:

OD104 OPA Diluent, 4 x950 mL



1154150T Sodium Ion-exchange Column, 4.0 x 150 mm (w/test mixture 1700-0070)







012506H Sodium Calibration Standard, for protein hydrolysate, 0.25 µmole/mL, 5 mL

0352-0031 KIT IDENTICAL TO AT31FH WITH T200 REPLACING T100C:

T200 TRIONE® Two-part Ninhydrin Reagent, prepares 4 x 900 mL

AO31FH KIT IDENTICAL TO AT31FH WITH ITEMS BELOW REPLACING T100C:

OD104 OPA Diluent, 4 x950 mL



AT32FC H IGH-EFFICIENCY 55-MINUTE COLLAGEN HYDROLYSATE KIT:

1154150T Sodium Ion-exchange Column, 4.0 x 150 mm (with test mixture 1700-0070)


AT31FH HIGH-EFFICIENCY 55-MINUTE PROTEIN HYDROYSIS KIT:




AT31FH HIGH-EFFICIENCY 55-MINUTE PROTEIN HYDROYSIS KIT (CONT.) :



012506C Sodium Calibration Standard, for collagen hydrolysate 0.25 µmole/mL, Proline and Hydroxyproline, 1.25 µmole/mL, 5 mL

Pickering Analysis Kits


3238 0 0 . 8 2 2 . 5 2 4 2 | 9 5 2 . 4 3 1 . 6 0 0 0 | w w w. c h r o m t e c h . c o mAuthorizedDistributor

AMINO ACID ANALYSIS KITS (CONTINUED)PART NO DESCRIPTION0352-0032 KIT IDENTICAL TO AT32FC WITH T200 REPLACING T100C:T200 TRIONE® Two-part Ninhydrin Reagent, prepares 4 x 900 mL

AO32FC KIT IDENTICAL TO AT32FC WITH ITEMS BELOW REPLACING T100C:OD104 OPA Diluent, 4 x 950 mL



0352-0018 60-MINUTE OXIDIZED FEED HYDROLYSATE KIT:1154150T Sodium Ion-exchange Column, 4.0 x 150 mm

(with test mixture 1700-0070)1700-3102 Cation-exchange GARD™ assy: Holder w/ 2 replaceable GARD™






1700-0155 Sodium Calibration Standard, for oxidized feed hydrolysate, 0.25 µmole/mL, 5 mL

0352-0017 KIT IDENTICAL TO 0352-0018 WITH T200 REPLACING T100C:T200 TRIONE® Two-part Ninhydrin Reagent, prepares 4 x 900 mL

0352-0019 KIT IDENTICAL TO 0352-0018 WITH ITEMS BELOW REPLACING T100C:OD104 OPA Diluent, 4 x 950 mL


3700-2000 Thiofluor™, 10 g, (2 ea per kit)

0352-0006 70-MINUTE PHYSIOLOGIC FLUID/NATIVE SAMPLE KIT:0354675T Lithium Ion-exchange Column, 4.6 x 75 mm (with test mixture

1700-0070)1700-3102 Cation-exchange GARD™ assy:Holder w/ 2 replaceable GARD™

1700-1125 Lithium Eluent, pH 2.80, 4 x 950 mL

Li220 Lithium Diluent, pH 2.20, 4 x 250 mL



RG003 Lithium Column Regenerant, 950 mL

1700-0170 Lithium Calibration Standard, without Norleucine and AGPA, 0.25 µmole/mL, 5 mL

SP100 SERAPREP™, 250 mL

UP100 URIPREP™, 250 mL


0352-0007 KIT IDENTICAL TO 0352-0006 WITH T200 REPLACING T100C:T200 TRIONE® Two-part Ninhydrin Reagent, prepares 4 x 900 mL







AT33SP STANDARD 185-MIN. PHYSIOLOGIC FLUID/NATIVE SAMPLE KIT:

0393250 Lithium Ion-exchange Column, 3.0 x 250 mm (with test mixture 1700-0070)

AMINO ACID ANALYSIS KITS (CONTINUED)PART NO DESCRIPTIONAT33SP STANDARD 185-MIN. PHYSIOLOGIC FLUID/NATIVE SAMPLE KIT (CONT.):1700-3102 Cation-exchange GARD™ assembly:

Holder w/ 2 replaceable GARD™sLi275 Lithium Eluent, pH 2.75, 4 x 950 mLLi750 Lithium Eluent, pH 7.50, 4 x 950 mLT100C TRIONE® Ninhydrin Reagent, 4 x 950 mL (3-month shelf life)RG003 Lithium Column Regenerant, 950 mLLi220 Lithium Diluent, pH 2.36, 4 x 250 mL011006P Lithium Calibration Standard, with norleucine, 0.25 µmole/mL, 5 mLSP100 SERAPREP™, 250 mLUP100 URIPREP™, 250 mL0352-0033 KIT IDENTICAL TO AT33SP WITH T200 REPLACING T100C:T200 TRIONE® Two-part Ninhydrin Reagent, prepares 4 x 900 mL

(12-month shelf life)AO33SP KIT IDENTICAL TO AT33SP WITH ITEMS BELOW REPLACING

T100C:OD104 OPA Diluent, 4 x 950 mLO120 o-Phthalaldehyde, 5 g3700-2000 Thiofluor™, 10 g (2 ea per kit)0352-0015 HIGH-EFFICIENCY 120-MIN. PHYSIOLOGIC FLUID/NATIVE SAMPLE KIT:0354100T Lithium Ion-exchange Column, 4.0 x 100 mm

(with test mixture 1700-0070)1700-3102 Cation-exchange GARD™ assembly:

Holder w/ 2 replaceable GARD™sLi275 Lithium Eluent, pH 2.75, 4 x 950 mLLi750 Lithium Eluent, pH 7.50, 4 x 950 mLT100C TRIONE® Ninhydrin Reagent, 4 x 950 mL (3-month shelf life)RG003 Lithium Column Regenerant, 950 mLLi220 Lithium Diluent, pH 2.36, 4 x 250 mL011006P Lithium Calibration Standard, with norleucine, 0.25 µmole/mL, 5 mLSP100 SERAPREP™, 250 mLUP100 URIPREP™, 250 mL0352-0011 KIT IDENTICAL TO 0352-0015 WITH T200 REPLACING T100C:T200 TRIONE® Two-part Ninhydrin Reagent, prepares 4 x 900 mL0352-0012 KIT IDENTICAL TO 0352-0015 WITH ITEMS BELOW REPLACING T100C:OD104 OPA Diluent, 4 x 950 mLO120 o-Phthalaldehyde, 5 g3700-2000 Thiofluor™, 10 g ( 2 ea per kit)0352-0013 TEMPERATURE GRADIENT PHYSIOLOGIC FLUID/NATIVE SAM-

PLE KIT:0354100T Lithium Ion-exchange Column, 4.0 x 100 mm

(with test mixture 1700-0070)1700-3102 Cation-exchange GARD™ assembly: Holder w/ 2 replaceable

GARD™1700-1125 Lithium Eluent, pH 2.80, 4 x 950 mLLi220 Lithium Diluent, pH 2.20, 4 x 250 mLLi365 Lithium Diluent, pH 3.65, 4 x 950 mLLi375 Lithium Diluent, pH 3.75, 4 x 950 mLRG003 Lithium Column Regenerant, 950 mL1700-0170 Lithium Calibration Standard, without Norleucine and AGPA,

0.25 µmole/mL, 5 mLSP100 SERAPREP™, 250 mLUP100 URIPREP™, 250 mLT100C TRIONE® Ninhydrin Reagent, 4 x 950 mL (3-month shelf life)



324®Chrom Tech


AMINO ACID ANALYSIS KITS (CONTINUED)PART NO DESCRIPTION0352-0014 KIT IDENTICAL TO 0352-0013 WITH T200 REPLACING T100C:T200 TRIONE® Two-part Ninhydrin Reagent, prepares 4 x 900 mL





PESTICIDE & HERBICIDE ANALYSIS KITSPART NO DESCRIPTION0352-0002 CARBAMATE PESTICIDES ANALYSIS KIT, 23+ COMPOUNDS0840250 Carbamate Column, expanded resolution, 4.0 × 250 mm (with

Carbamate Test Mixture 1700-0063)18ECG001 Guard Cartridge Holder with 3 guard cartridges

CB130 Carbamate Hydrolysis Reagent, 4 × 950 mL

CB910 Carbamate OPA Diluent, 4 × 950 mL



1700-0132 ChlorAC™ Buffer, 250 mL

0352-0003 CARBAMATE PESTICIDES ANALYSIS KIT, FOR EPA METHOD 531.1 :

18ECG001 Guard Cartridge Holder with 3 guard cartridges



O120 o-Phthalaldehyde, 5



0352-0009 CARBAMATE PESTICIDES ANALYSIS KIT, FOR EPA METHOD 531.2 :


CB130.2 Carbamate Hydrolysis Reagent, 4 × 950 mL





0352-0004 CARBAMATE PESTICIDES ANALYSIS KIT, FOR AOAC METHOD 985.23:

1846150 Analytical Column, rapid analysis/QC, 4.6 × 150 mm (with Carbamate Test Mixture 1700-0063)




0352-0040 BIOGENIC AMINES/POLYAMINES ANALYSIS KIT:O120 o-Phthalaldehyde, 5 g



PESTICIDE & HERBICIDE ANALYSIS KITS (CONTINUED)PART NO DESCRIPTION0352-0010 GLYPHOSATE HERBICIDE ANALYSIS KIT, FOR EPA METHOD

547, AOAC METHOD 991.08:1954150 Cation-exchange Column, K+ form, 4.0 × 150 mm (with

Glyphosate Test Mixture 1700-0080)1700-3102 Cation-exchange GARD™ assy: Holder w/ 2 replaceable GARD™

K200 Glyphosate Potassium Phosphate Eluent, 4 × 950 mL

RG019 Glyphosate Column Regenerant, 950 mL

GA104 Glyphosate OPA Diluent, 4 × 950 mL

GA116 Glyphosate Hypochlorite Diluent, 4 × 950 mL



1700-0140 RESTORE™, 250 mL

9410917 ALKION™ Cation-exchange Column, K+ form, 4.0 × 150 mm

9493020 ALKION™ Guard Column, K form, 3.0 × 20 mm

1100-0200 Flow Restrictor, 300 PSI, 10 cm

K563 Potassium Phosphate Eluent, pH 5.63, 4 × 950 mL

K600 Potassium Phosphate Eluent, pH 6.00, 4 × 950 mL

K130 Potassium Column Regenerant, 950 mL

OD104 OPA Diluent, 4 × 950 mL



0352-0041 AMINOGLYCOSIDE ANTIBIOTICS ANALYSIS KIT:9410917 ALKION™ Cation-exchange Column, K form, 4.0 × 150 mm

9493020 ALKION™ Guard Column, K form, 3.0 × 20 mm


1700-1101 Potassium Phosphate Eluent, KO1, 4 × 950 mL

1700-1102 Potassium Hydroxide Eluent, KO2, 4 × 950 mL

1700-1103 Potassium Chloride Eluent, KO3, 4 × 950 mL




0352-0042 PARAQUAT/DIQUAT IN WATER ANALYSIS KIT:9410917 ALKION™ Cation-exchange Column, K form, 4.0 × 150 mm

9493020 ALKION™ Guard Column, K+ form, 3.0 × 20 mm


1700-1101 Potassium Phosphate Eluent, KO1, 4 × 950 mL

1700-1102 Potassium Hydroxide Eluent, KO2, 4 × 950 mL

1700-1103 Potassium Chloride Eluent, KO3, 4 × 950 mL

0352-0053 MULTI-RESIDUE MYCOTOXIN KIT :1612124 MYCOTOX™ Reversed-phase Column, 4.6 × 250 mm

18ECG001 Guard Cartridge Holder with 3 cartridges



1700-1108 Sodium Phosphate Eluent, pH 3.3


0352-0050 AFLATOXIN ANALYSIS KIT:1612124 MYCOTOX™ Reversed-phase Column, 4.6 × 250 mm


0352-0051 POLYETHER ANTIBIOTICS KIT:2381750 Polyether Column, 4.6 × 250 mm


3700-2200 Vanillin, 30 g



Modular Design

SENSIVATE POST-COLUMN REACTORCHOOSE: 1. PCR SYSTEM 2. REACTOR BLOCK 1 (HEATED) 3. OPTIONAL REACTOR BLOCK 2 (AMBIENT)

PCR0 = Post Column Reactor Unit R015 = 0.15 mL Reactor R015 = 0.15 mL ReactorPCR1 = Single Reagent Post Column System (1 pump) R050 = 0.50 mL Reactor R050 = 0.50 mL ReactorPCR2 = Dual Reagent Post Column System (2 pumps) R140 = 1.40 mL Reactor R140 = 1.40 mL Reactor

For custom reactor size: RXXX = XXX mL Reactor Vol

For custom reactor size: RXXX = XXX mL Reactor Vol

POPULAR SENSIVATE CONFIGURATIONSPART NO 1. PCR SYSTEM 2. REACTOR BLOCK 1 (HEATED) 3. OPTIONAL REACTOR BLOCK 2 (AMBIENT)PCR0-R050 PCR0 – Post Column Reactor Unit R050 – 0.50 mL Reactor N/A

PCR1-R015 PCR1 – Single Reagent Post Column System R015 – 0.15 mL Reactor N/A




PCR2-R050-R015 PCR2 – Dual Reagent Post Column System R050 – 0.50 mL Reactor R015 – 0.15 mL Reactor

PCR2-R140-R140 PCR2 – Dual Reagent Post Column System R140 – 1.40 mL Reactor R140 – 1.40 mL Reactor

PCR2-R200 PCR2 – Dual Reagent Post Column System R200 – 2.0 mL Reactor N/A

The Sensivate’s modular design means you can configure your own system. To configure your part number, choose one option from columns 1 and 2. If second reactor is required, choose option from column 3.

ACCESSORIESPART NO DESCRIPTION160808 Sparging Option Assembly, Includes 2 multi-valve bottle caps, 1 pressure regulator, mounting hardware, tubing, fittings. Bottles not included.

160819 Pressure Control Switch

Sensivate Post-Column ReactorDisposable reactor cartridgesAll PEEK fluid pathAll connections accessible from front panel—ease of maintenanceUpper/lower pressure and temperature limits, and system shutdown relayReactor designed to reduce band broadening—not just a coil

Continuous loop, fully sealedMulti-directional path for effective mixingInteractive front keypad control with digital display and ready light

- Temperature set point - Temperature display

PUMP SPECIFICATIONSFlow rates: 0.01 – 2.50 mL/min Pressure: 0 – 2,000 PSI (138 bar)Flow Accuracy:

± 3% from set point

Flow Precision:

< 0.5% RSD

Materials: All PEEK fluid path, including pump heads

Dimensions (h x w x d):

11.8" x 10.5" x 17" (30 x 27 x 43 cm)

Weight: 54 lbs (14 kg)Electrical 120/230 VAC, 50/60 HzInput: RS-232

REACTOR SPECIFICATIONSTemp. Operating Range:

10 – 150 °C above ambient

Temp. Accuracy:

± 2 °C over entire range (outlet fluid temperature vs set point)

Temp. Repeatability:

± 1 °C

Safety Cutoff Temp.:

160 °C

Stabilizing Time:

60 minutes to 150 °C for "Ready" indication

Input: RS-232

Automatic piston wash (significantly improves seal life)Back Pressure Coil for proper Pulse Dampener operation (approx. 1,000 PSI @ 1.0 mL/min)Interactive front keypad with digital read-out:

- Flow rate set points - Pressure readout - Set upper/lower pressure limit


hplc instrumentation - chrom tech, inc.hplc instrumentation 296 chrom tech ® replaces dual piston,...

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