haake rheostress 600 - upc · 2017. 10. 2. · haake rheostress 600 normal force rheometry not only...

HAAKE RheoStress 600

The modular High-Tech Rheometer

Analyze • Detect • Measure • ControlTM

RheoStress600_GB.qxd 13.01.2004 15:15 Uhr Seite 3

What counts inRheometry...

VC-Motor

VC Motor, powerful ... dynamic ... and extremely fastThe proven VC motor of the RS300 has been furtherimproved and sets new standards with:

a 4th generation diffusion air bearing

high dynamic response due to digital adaptive control loops and an exemplary low inertia (1.1·10-5 kgm2)

response times of 40 ms for shear rate and strain jumps

a standard maximum torque of 200 mNm

a minimum torque of 0.1µNm, realised with the new MSCplus (Micro Stress Control plus)

The VC motor allows the simulation of extreme rheo-logical processes – a rheologist’s dream comes true!

Software modules

Customize HAAKE RheoWin to your needsHAAKE RheoWin can be adapted to suit individual user requirements via special modules:

snapshot for a quick characterizationof an unknown sample

RheoWizard®; the expert help system for creating new jobs

Barcode control for workflow optimization (GLP)

SAP interface for data exchange

automatic comparisons with reference data / master curves

polymer software HAAKE RheoSoft(WLF, Relaxation time spectra, molecular weight distribution)

Tools for complying with the FDA 21 CFR part 11 requirements

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Data Recording

Recording data right from the startMany visco-elastic samples e.g. polymers react to changesin shear stress with a characteristic time delay. Con-clusions can be drawn from this with regard to themicrostructure of the sample, provided that data is available over a wide range of time. With the 400 Hz sampling rate of the HAAKE RheoStress 600, the firstdata point is measured after 2.5 ms. As a result the time dependent properties of visco-elastic substances

can be characterized continuously.

CD-Mode

True deformation controlThe new Controlled Deformation mode isavailable for rotational (strain-jump) as well as oscillatory measurements. In oscillation the desired deformation is attained at the first oscillation period, without iterations, in contrast to the AutoStrain functionality of classical CS-rheometers. Fast rheologicalprocesses, like chemical reactions, thermallyinduced hardening, gel formation kinetics, etc. can thus be recorded continuously.

HAAKE RheoWin

Measuring, evaluation and data export via Drag-&-DropHAAKE RheoWin is a complete measuring and evaluation software for all measuring modes. It controls the HAAKE RheoStress 600 and handles the measured data either graphically or as a table.Some highlights are:

definition of measuring and evaluation sequences(”Jobs”) using Drag-&-Drop

fully automated measurement and evaluation in one job

broad selection of rheological evaluation methods

freely configurable ASCII data export

automatic intermediate saving of measured data

real multitasking; simultaneous measurements withmultiple rheometers

real 32-bit application for Windows® 95/98/Me andNT/2000/XP

highly configurable user managment system

12 operating languages available

Display/Control Unit

Monitoring data on-line even without a PCThe display/control unit of the HAAKE RheoStress 600 isused for manual operation of the lift and the gap setting. It is also used to set preselected shear rates and to inter-vene in PC-controlled measurements. The colour displaymonitors freely selectable rheological and instrument spe-cific data online. Data can be displayed numerically as wellas graphically. Complex measuring sequences are carriedout ”at the touch of a button”, without using a PC.

The display/control unit is part of the standard delivery ofthe HAAKE RheoStress 600 High Performance and anoption for the HAAKE RheoStress 600.


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Normal Force

Rheometry not only in one directionForces acting perpendicular to the direction offlow play an important role in many rheologicalapplications. With the HAAKE RheoStress 600,the normal force can be used as a set parame-ter as well as a measured variable.

The normal stress differences induced byshearing a visco-elastic sample are measuredby the normal force sensor which is integratedin the air-bearing, where it is shielded againstmechanical and thermal influences. The newMFC (Micro Force Correction) extends themeasurable force range down to 0.01 N.

In the FCL mode (Force-Controlled-Loading)samples are loaded under a pre-set normalforce in order to increase the reproducibility.

With the HAAKE RheoStress 600 you can be sure that only the sample properties aremeasured.

Modularity

Trying out new ideas with the HAAKERheoStress 600... acting flexiblyThe HAAKE RheoStress 600 isdesigned for the creative rheolo-gist, who uses a rheometer for dedicated research. The instrumentsetup can be quickly adapted to suit a wide range of requirementsdue to its modular design.

Temperature Control– Liquid temperature control,

Peltier temperature control, electrical temperature control

Special measuring sensors– High Temperature, Pressure,

Electro-Rheology, UV-curing cell

Options– High Shear, Normal Force


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Temp. Temp Heating Cooling min. max. rate rate

(K/min) (K/min)

Thermal fluid cylinder system -40 200 2 1

Thermal fluid cone & plate system -80 350 3 2

Electric heated cylinder system 30 200 8 1*

Electric heated cone & plate system -80 500 15 2*

Peltier controlled cone & system -60 185 40* 40*

*depending on the properties and temperature of the cooling media

RecommendedDescription Type Shear rate (s-1) Shear rate (s-1) viscosity range

Standard High Shear option (mPas)

Double gap cylinder system DG41 0,007 - 11 415 34 245 0,5 - 10 000

Cylinder Ø 40 mm ISO 3219 Z40 DIN 0,001 - 1 931 5 793 5 - 100 000

Cylinder Ø 20 mm ISO 3219 Z20 DIN 0,001 - 1 931 5 793 50 - 1 000 000

Cylinder Ø 10 mm ISO 3219 Z10 DIN 0,001 - 1 931 5 793 500 - 10 000 000

Cylinder Ø 41 mm DIN 53018 Z41 0,002 - 3 500 10 500 10 - 100 000

Cylinder Ø 38 mm DIN 53018 Z38 0,001 - 1 400 4 200 30 - 500 000

Cylinder Ø 31 mm DIN 53018 Z31 0,0005 - 660 1 980 50 - 1 000 000

Profiled cylinder Ø 38 mm DIN 53018 Z38/S 0,001 - 1 500 4500 50 - 100 000

Disposable cylinder Ø 41 mm ISO 3219 Z41DIN/E 0,001 - 1 931 5793 10 - 100 000

Disposable cylinder Ø 25 mm ISO 3219 Z25DIN/E 0,001 - 1 931 5793 50 - 1 000 000

High shear cylinder 25 µm gap HS25 0,1 - 69 200 207 600 5 - 100

High shear cylinder 100 µm gap HS100 0,1 - 15 000 45 000 5 - 100

Double cone Ø 60 mm, 1° angle DC60/1 0,006 - 9 000 27 000 1 - 50 000

Cone Ø 60 mm, 1° angle * C60/1 0,006 - 9 000 27 000 2 - 100 000

Cone Ø 35 mm, 1° angle * C35/1 0,006 - 9 000 27 000 100 - 1 000 000

Cone Ø 20 mm, 1° angle * C20/1 0,006 - 9 000 27 000 1 000 - 1.0 E+08

Plate Ø 60 mm PP60 0,003 - 4 700 14 100 2 - 100 000

Plate Ø 35 mm PP35 0,002 - 2 700 8 100 100 - 1 000 000

Plate Ø 20 mm PP20 0,001 - 1 570 4 710 1 000 - 1.0 E+08

Plate Ø 35 mm serrated PP35/S 0,002 - 2 700 8 100 100 - 1 000 000

Plate Ø 20 mm serrated PP20/S 0,001 - 1 570 4 710 1 000 - 1.0 E+08

* Cones with angles of 0.5° and 2.0° are available as well

Typical sensor systems

Temperature control devices

HAAKE RheoStress 600 HAAKE RheoStress 600High Performance

Max. Min. Max. Min.

Angular resolution (micro rad) – 0.012 – 0.012

Rotational speed CR-mode (min-1) 1500 0.001 1500 (4500*) 0.001

Rotational speed CS-mode (min-1) 1500 1.0E-7 1500 1.0E-7

Torque (Nm) 0.2 5.0E-7 0,2 1.0E-7

Oscillation frequency (Hz) 100 0.0001 100 0.0001

Normal force* (N) 30 0.01 30 0.01

* optionally

HAAKE RheoStress 600 models and specifications


Analyze • Detect • Measure • ControlTMwww.thermo.com/mc

International/GermanyThermo Electron (Karlsruhe) GmbHDieselstr. 476227 KarlsruheTel. +49(0)721 40 [email protected]

BeneluxThermo Electron B.V.Takkebijsters 14817 BL BredaTel. +31(0)76 [email protected]

France Thermo Electron S.A.16 Avenue du Québec - Silic 76591963 Courtaboeuf CedexTel. +33(0)1 60 92 48 [email protected]

United KingdomThermo Electron Emerald Way, StoneStaffordshire ST15 0SRTel. +44(0)1785 [email protected]

USAThermo Electron25 Nimble Hill Rd.Newington, NH 03801Tel. [email protected]

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haake rheostress 600 - upc · 2017. 10. 2. · haake rheostress 600 normal force rheometry not only...

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