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i FRESH AND MECHANICAL PROPERTIES OF SELF-COMPACTING CONCRETE USING BRICK AGGREGATE MD. SUMAN MIA DEPARTMENT OF CIVIL ENGINEERING DHAKA UNIVERSITY OF ENGINEERING & TECHNOLOGY, GAZIPUR August 2020

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i

FRESH AND MECHANICAL PROPERTIES OF

SELF-COMPACTING CONCRETE USING BRICK AGGREGATE

MD. SUMAN MIA

DEPARTMENT OF CIVIL ENGINEERING

DHAKA UNIVERSITY OF ENGINEERING & TECHNOLOGY, GAZIPUR

August 2020

ii

FRESH AND MECHANICAL PROPERTIES OF

SELF-COMPACTING CONCRETE USING BRICK AGGREGATE

A Thesis

by

Md. Suman Mia

Submitted to the Department of Civil Engineering

Dhaka University of Engineering & Technology, Gazipur

In Partial Fulfillment of the Requirements for the Degree

of

MASTER OF SCIENCE IN CIVIL ENGINEERING (STRUCTURAL)

DEPARTMENT OF CIVIL ENGINEERING

DHAKA UNIVERSITY OF ENGINEERING & TECHNOLOGY, GAZIPUR

AUGUST, 2020

iii

APPROVAL

This is to certify that the thesis work submitted by Md. Suman Mia, Student Id.

16201039-P, titled β€œFresh and Mechanical Properties of Self-Compacting Concrete

using Brick Aggregate” has been accepted as satisfactory by the Board of Examiners

in partial fulfillment of the requirements for the award of the degree of Master of

Science in Civil Engineering (Structural) on 31 August 2020.

BOARD OF EXAMINERS

----------------------------------------

Dr. Md. Nazrul Islam

Professor

Department of Civil Engineering

DUET, Gazipur, Bangladesh

Chairman

(Supervisor)

----------------------------------------

Dr. Mohammad Nazim Uddin

Professor and Head

Department of Civil Engineering

DUET, Gazipur, Bangladesh

Member

(Ex-Officio)

----------------------------------------

Dr. Md. Abdus Salam

Professor

Department of Civil Engineering

DUET, Gazipur, Bangladesh

Member

----------------------------------------

Dr. Md. Rezaul Karim

Professor

Department of Civil Engineering

DUET, Gazipur, Bangladesh

Member

----------------------------------------

Dr. Md. Tarek Uddin

Professor

Department of Civil & Environmental Engineering

Islamic University of Technology (IUT), Bangladesh

Member

(External)

iv

DECLARATION

This is to certify that the thesis work titled β€œFresh and Mechanical Properties of

Self-Compacting Concrete using Brick Aggregate” has been carried out by me at the

Department of Civil Engineering, Dhaka University of Engineering & Technology,

Gazipur, Bangladesh. The above thesis work or any part of it has not been submitted

anywhere for any award of degree or diploma (except for publication).

Candidate’s Signature

…………………………………..

Md. Suman Mia

v

ACKNOWLEDGMENTS

All praises belong to Almighty Allah, the most merciful, the most beneficent and the

most kind for giving me the opportunity, courage and enough energy to carry out and

complete this research work.

I wish to express my sincere appreciation and gratitude to my supervisor Professor

Dr. Md. Nazrul Islam, Department of Civil Engineering, DUET, Gazipur, for his

guidance, support, valuable advice, encouragement, intellectual discussions, and

patience throughout this work. He has given me excellent guidance to select this

research topic and allowed me ample freedom in my research. It is truly an honor to me

for getting an opportunity to work under his supervision. His valuable advice highly

appreciated me to solve various critical issues including materials and laboratory-

related problems.

I would like to acknowledge Professor Dr. Md. Abdus Salam for his exemplary

guidance, monitoring, and constant encouragement during the laboratory works as well

as the preparation of this thesis. He also shared his valuable time, knowledge, and

experience with me to enhance the quality of my thesis.

I would like to thank Professor Dr. Md. Rezaul Karim for willingness to help along

with patience to pull me through this thesis. His countless proof readings, corrections

and support made this document possible, and will not be forgotten.

Particularly, I am extremely obliged for the financial support provided by the

Department of Civil Engineering, DUET, Gazipur, in performing this research work.

My present study would have never been completed without their financial support.

I would like to thank all officers and staff of the Civil Engineering Department for

finding unique ways to encourage me and assist me through the good as well as difficult

stages of this research work.

I would like to express my gratitude to some individuals who enabled me, gave me

enough strength and support in completing my Master’s study. Finally, I would like to

express my heartfelt gratitude to my parents and all of my family members and relatives

for praying for me in every step of life. Their love, dedication, and faith in me are the

constant sources of my strength.

vi

ABSTRACT

To avoid the complexities of vibration and consolidation, a special type of concrete

named self-compacting concrete (SCC) is used in the construction works. SCC can

spread into place due to its self-weight even in areas of congested reinforcement. In

view of the potential construction materials, SCC made with brick aggregate can be

used to meet the demand of structural facilities.

To investigate the fresh and mechanical properties of SCC, 12.5 mm and 19 mm

downgraded brick chips were used as coarse aggregate in combination with coarse sand

and Portland composite cement. Trial mixes of SCC were prepared with various

aggregate and cement contents with fixed water to binder ratios of 0.35 and 0.40 and

different dosages of superplasticizer. A total of twenty four successful SCC mixes were

selected in this study.

To investigate the filling ability, passing ability, and segregation resistance of the fresh

concrete, slump flow, T50 flow time, V-funnel flow, V-funnel flow at T5minutes, L-box

and J-ring tests were performed. Different correlations were developed among the fresh

properties of SCC with brick aggregate. The tests of mechanical properties were

conducted on hardened SCC at 28 days to determine the compressive strength, modulus

of elasticity and splitting tensile strength. This study also carried out to suggest the

relations among compressive strength, splitting tensile strength and modulus of

elasticity for SCC with brick aggregate.

Test results indicated that slump flow, J-ring flow and T50 flow time satisfied the

acceptance criteria for the selected of coarse aggregates. There was no visible blocking

and segregation in the L-box, V-funnel and J-ring tests. Thus, SCC with brick aggregate

can possess all the requirements of fresh properties. The compressive strength of

hardened SCC with brick aggregate ranged from 20.00 MPa to 29.00 MPa and the

splitting tensile strength was about one tenth of the compressive strength. The modulus

of elasticity for SCC with brick aggregate was found similar to normal brick aggregate

concrete and 23% lower than the normal concrete made with natural aggregates.

Therefore, SCC with brick aggregate may be an alternative source to the engineers for

concrete construction in Bangladesh.

vii

TABLE OF CONTENTS

Title Page No.

APPROVAL III

DECLARATION IV

ACKNOWLEDGMENTS V

ABSTRACT VI

TABLE OF CONTENTS VII

LIST OF TABLES XI

LIST OF FIGURES XII

NOTATIONS XIV

CHAPTER I INTRODUCTION 1

1.1 GENERAL 1

1.2 PROBLEM STATEMENT 2

1.3 OBJECTIVES OF THE RESEARCH 3

1.4 SCOPE OF THE RESEARCH 3

1.5 OUTLINE OF THE THESIS 4

CHAPTER II LITERATURE REVIEW 6

2.1 INTRODUCTION 6

2.2 DEFINITION OF SCC 6

2.3 ADVANTAGES OF SCC 6

2.4 DEVELOPMENT OF SCC 8

2.5 CLASSIFICATION OF SCC 11

2.6 INGREDIENTS OF SCC 13

2.6.1 Aggregates 14

2.6.2 Cement 19

2.6.3 Admixtures 20

2.7 MIX DESIGN 20

2.8 FRESH PROPERTIES 23

2.8.1 Filling Ability 24

2.8.2 Passing Ability 25

2.8.3 Segregation Resistance 25

2.8.4 Correlations between Fresh Properties of SCC 25

2.9 MECHANICAL PROPERTIES 27

viii

2.9.1 Compressive Strength 28

2.9.2 Splitting Tensile Strength 28

2.9.3 Modulus of Elasticity 29

2.10 SUMMARY 30

CHAPTER III MATERIALS AND METHODOLOGY 31

3.1 INTRODUCTION 31

3.2 MATERIALS 32

3.3 TESTING OF THE MATERIALS 32

3.3.1 Tests for Coarse Aggregate 32

3.3.2 Tests for Fine Aggregate 35

3.3.3 Test for Binding Materials 36

3.3.4 Water 37

3.3.5 Superplasticizer 37

3.4 MIX DESIGN OF SCC 38

3.4.1 Trial and Error Method of Mix Proportioning 39

3.4.2 Detailed on Mix Design 39

3.5 PREPARATION OF CONCRETE SPECIMEN 47

3.5.1 Batching of the Materials 47

3.5.2 Mixing of the Concrete 47

3.5.3 Testing of Fresh Properties of SCC 48

3.5.4 Placing of Fresh Concrete 48

3.5.5 Removal of Mold 48

3.5.6 Curing of Concrete 48

3.5.7 Testing of Hardened Concrete 49

3.6 FRESH PROPERTIES OF SCC MIXTURES 49

3.6.1 Slump-Flow and T50 Flow Test 49

3.6.2 J-Ring Test 50

3.6.3 V-funnel Flow and V-funnel Flow at T 5minutes Test 52

3.6.4 L-Box Test 53

3.7 MECHANICAL PROPERTIES OF SCC 55

3.7.1 Compressive Strength 56

3.7.2 Splitting Tensile Strength 56

3.7.3 Modulus of Elasticity of SCC 57

3.8 SUMMARY 58

ix

CHAPTER IV RESULTS AND DISCUSSION 59

4.1 GENERAL 59

4.2 PROPERTIES OF MATERIALS 59

4.2.1 Coarse Aggregate 59

4.2.2 Fine Aggregate 61

4.2.3 Cement 62

4.2.4 Superplasticizer 63

4.3 PHYSICAL OBSERVATION OF FRESH CONCRETE 63

4.4 FRESH PROPERTIES OF SCC WITH BRICK AGGREGATE 65

4.4.1 Filling Ability 66

4.4.1.3 V- Funnel Flow 71

4.4.2 Passing Ability 72

4.4.3 Segregation Resistance 76

4.5 CORRELATION BETWEEN FRESH PROPERTIES

OF SCC WITH BRICK AGGREGATE 77

4.5.1 Correlation between Slump Flow and J-ring Flow of SCC with

Brick Aggregate 77

4.5.2 Correlation between Slump Flow and T50 Flow Time of SCC 78

4.5.3 Correlation between J-ring Flow and T50 Flow Time of SCC 79

4.6 MECHANICAL PROPERTIES OF SCC WITH

BRICK AGGREGATE 80

4.6.1 Compressive Strength 81

4.6.2 Splitting Tensile Strength 86

4.6.3 Modulus of Elasticity 87

4.7 CORRELATION BETWEEN MECHANICAL PROPERTIES 87

4.7.1 Correlation between Compressive Strength and Splitting Tensile

Strength 88

4.7.2 Correlation between Compressive Strength and Modulus of

Elasticity 89

4.8 SUMMARY 91

CHAPTER V CONCLUSIONS AND RECOMMENDATIONS 92

5.1 INTRODUCTION 92

5.2 CONCLUSIONS 92

5.2.1 Fresh Properties of SCC with Brick Aggregate 92

5.2.2 Mechanical Properties of SCC with Brick Aggregate 93

x

5.3 CONTRIBUTION OF THE STUDY 94

5.4 RECOMMENDATIONS FOR FUTURE STUDY 94

REFERENCES 96

APPENDICES 104

APPENDIX-A PHOTOGRAPHS OF THE INGREDIENTS 104

APPENDIX-B ANALYSIS AND RESULTS OF THE PROPERTIES

OF THE AGGREGATES . 110

APPENDIX-C SUMMARY OF THE TEST RESULTS 118

APPENDIX-D STRESS-STRAIN GRAPHS OF CYLINDRICAL

SPECIMENS . 121

xi

LIST OF TABLES

Table No. Table Caption Page No.

Table 2.1 Typical range of SCC mix composition (EFNARC, 2005) 21

Table 2.2 SCC proportioning trial mixture parameters (ACI 237R-07, 2007) 23

Table 2.3 List of test methods for workability properties of SCC

(EFNARC, 2002) 23

Table 2.4 Acceptance criteria for self-compacting concrete

(EFNARC, 2002) 24

Table 2.5 Correlation between Fresh Properties of SCC

(Safiuddin et al., 2011a) 26

Table 2.6 Correlation between the fresh properties of SCC with palm

oil fuel ash (Safiuddin et al., 2011b) 27

Table 3.1 Ingredients of SCC with BA 32

Table 3.2 Proportion of the unsuccessful trial mixes 41

Table 3.3 Identification of specimens 43

Table 3.4 Proportion of the successful SCC mixes with BA 46

Table 3.5 Volumetric calculation of the ingredients of SCC with BA 46

Table 3.6 Cost of the materials for a cubic meter SCC mixes with BA 47

Table 4.1 Properties of coarse and fine aggregates 60

Table 4.2 Test Results of Cement 62

Table 4.3 Compound compositions of portland composite cement 63

Table 4.4 Technical data of superplasticizer 63

Table 4.5 Fresh properties of SCC with brick aggregate 65

Table 4.6 Mechanical properties of SCC with brick aggregate 80

Table 4.7 Correlation between compressive strength and splitting

tensile strength proposed by researchers 89

Table 4.8 Correlation between compressivestrength and modulus

of elasticity proposed by researchers 90

xii

LIST OF FIGURES

Figure No. Figure Caption Page No.

Fig. 2.1 Definition of self-compacting concrete (Ozawa et al., 1992) 7

Fig. 2.2 Advantages of SCC (Ozawa et al., 1992) 8

Fig. 2.3 Method of achieving self compactability (Okamura and Ouchi, 2003) 10

Fig. 2.4 Comparison of proportion of the materials for SCC and

Conventional concrete (Okamura and Ouchi, 2003) 13

Fig. 2.5 Variables involved in establishing the required fresh SCC

properties (ACI 237R-07, 2007) 22

Fig. 3.1 Crushed bricks as coarse aggregate 33

Fig. 3.2 Fine Aggregate (Coarse Sand) 36

Fig. 3.3 Method of deflocculation and water liberation with use

of Superplasticiser (Deeb and Karihaloo, 2013) 37

Fig. 3.4 Superplasticizer Con-Lub SP 38

Fig. 3.5 Some unsuccessful attempts of fresh SCC 42

Fig. 3.6 Standard mixing sequence (Lotfy, 2006) 48

Fig. 3.7 Slump Flow equipment 50

Fig. 3.8 Slump flow test of SCC with brick aggregate 50

Fig. 3.9 J-Ring test apparatus 51

Fig. 3.10 J-Ring test of SCC with brick aggregate 51

Fig. 3.11 V-funnel test apparatus 52

Fig. 3.12 V-funnel and V-funnel at T5 minutes test 53

Fig. 3.13 L-Box flow test apparatus (all units in mm) 54

Fig. 3.14 L-box filled with concrete 54

Fig. 3.15 Concrete passes through L-box 55

Fig. 3.16 Flow of concrete in L-box. 55

Fig. 3.17 Testing of splitting tensile strength 56

Fig. 3.18 Testing of modulus of elasticity 58

Fig. 4.1 Gradation curve of 12.5 mm downgraded coarse aggregate 60

Fig. 4.2 Gradation curve of 19 mm downgraded coarse aggregate 61

Fig. 4.3 Gradation curve of fine aggregate 62

Fig. 4.4 Surface of the fresh concrete with bubbles formation 64

Fig. 4.5 Surface of the fresh concrete without bubbles formation 64

Fig. 4.6 Variation of Slump Flow of SCC with Brick Aggregate 66

Fig. 4.7 Variation of slump flow of SCC (w/c = 0.35) 67

Fig. 4.8 Variation of slump flow of SCC (w/c = 0.40) 68

Fig. 4.9 T50 slump flow time of SCC using brick aggregate 69

xiii

Fig. 4.10 Variation of slump flow and T50 flow time of SCC 70

Fig. 4.11 Time needed for V-funnel flow 71

Fig. 4.12 Relation between slump flow and V-funnel flow time 72

Fig. 4.13 Variation of slump flow and J-ring flow of SCC with BA 73

Fig. 4.14 Blocking index of SCC mixes with BA 74

Fig. 4.15 Height difference in J-Ring Flow Test of SCC with BA 74

Fig. 4.16 Blocking ratio of SCC Mixes with BA 75

Fig. 4.17 Time needed for V-funnel flow at T5minutes 76

Fig. 4.18 Correlation between J-ring flow and slump flow of SCC 78

Fig. 4.19 Correlation between slump flow and T50 flow time of SCC 79

Fig. 4.20 Correlation between J-ring flow and T50 flow time of SCC 79

Fig. 4.21 Compressive Strength of SCC with Brick Aggregate 81

Fig. 4.22 Effect of aggregate size and cement contents on the

compressive strength of SCC at w/c of 0.35 82

Fig. 4.23 Effect of aggregate size and cement contents on the

compressive strength of SCC at w/c of 0.40 83

Fig. 4.24 Variation of 28 days compressive strength of SCC with 12.5 mm CA 84

Fig. 4.25 Variation of 28 days compressive strength of SCC with 19 mm CA 85

Fig. 4.26 Failure plane of concrete specimens 85

Fig. 4.27 Splitting tensile strength of SCC with brick aggregate. 86

Fig. 4.28 Relationship between compressive strength and

splitting tensile strength 87

Fig. 4.29 Correlation between compressive strength and splitting

tensile strength of SCC with brick aggregate 88

Fig. 4.30 Correlation between compressive strength and modulus

of elasticity of SCC with brick aggregate 90

xiv

NOTATIONS

ACI = American Concrete Institute

ASTM = American Society for Testing and Materials

BA = Brick Aggregate

BI = Blocking Index

BR = Blocking Ratio

Ec = Modulus of Elasticity of Concrete

EFNARC = European Federation of National Associations Representing for Concrete

fΚΉc = Compressive Strength of Concrete at 28 days

fr = Modulus of Rupture

fsp = Splitting Tensile Strength

HRWR = High Range Water Reducer

HWRA = High Water Reducing Admixture

kN = kilo Newton

mm = millimeter

MPa = Mega Pascal (N/mm2)

NC = Normal Concrete

NCA = Natural Coarse Aggregate

POFA = Palm Oil Fuel Ash

RCA = Recycled Coarse Aggregate

SCC = Self-Compacting Concrete

SCM = Supplementary Cementitious Materials

sec = Seconds

SP = Superplasticizer

SSD = Saturated Surface Dry

VMA = Viscosity Modifying Admixture

w/c = Water to Cement Ratio

1

CHAPTER 1 CHAPTER I …………………..

. INTRODUCTION

1.1 GENERAL

Self-compacting concrete (SCC) is a new technology in the concrete industry. It has

become popular because of the improvement of the quality of the concrete and the better

working environment. To enhance the expected strength and durability of concrete, it

is required to produce the less porosity, honeycomb and segregation free durable

concrete. Vibration and compaction are needed for proper placement of fresh concrete

to produce the quality concrete. Sometimes it is not possible to produce quality concrete

due to lack of skilled labor and huge energy consumption. It is also difficult to place

the concrete in the congested areas of reinforcement. To overcome these problem SCC

can be used to avoid the complexities of vibration, compaction and placement of

concrete. SCC is a highly flowable concrete. It can spread radially into the place due to

its self-weight only. It can be placed in the area of highly congested reinforcement. SCC

can be compacted and consolidated without vibration.

SCC is a complex system that is usually proportioned with one or more mineral

admixtures and chemical admixtures in addition to the constituent of normal concrete.

SCC typically includes the same materials as conventionally placed concrete; however,

a special high range water reducer (HRWR) and a viscosity modifying admixture

(VMA) may be used. Therefore, the differences between SCC and conventionally

placed concrete are related to workability and to the changes in materials and mixture

proportions required to achieve workability. The workability of SCC is defined in terms

of three properties: filling ability, passing ability, and segregation resistance which are

also known as the fresh properties of SCC. Filling ability describes the ability of

concrete to flow under its own mass and completely fill the formwork. Passing ability

describes the ability of concrete to flow through confined conditions, such as the narrow

openings between reinforcing bars. Although increasing the filling ability typically

increases passing ability, a high level of filling ability does not assure passing ability.

Segregation resistance describes the ability of concrete to remain uniform in

composition during placement. Segregation resistance includes both static and dynamic

stability. Static stability describes segregation resistance when concrete is at rest.

Dynamic stability describes segregation resistance when concrete is not at rest such as

during mixing and placing (Koehler and Fowler, 2007).

2

The idea of self-compacting was initially proposed by Professor Hajime Okamura in

Japan in 1986 at the University of Tokyo and the large Japanese contractors (Okamura

and Ozawa, 1995). SCC was first developed in Japan and an empirical method for mix

design of SCC was recommended by Okamura and Ozawa (1995). The mechanism for

achieving the self-compatibility of fresh concrete was introduced by Okamura and

Ouchi (2003).

SCC can be pumped from the underneath of a form or dropped from the most effectively

with a recommended maximum fall height of 6 feet (ACI 237R-07, 2007). When SCC

is used with the standard execution method, the construction period is unchanged and

the manpower requirement falls by about 10% (Kato et al., 1993).

To completely fill the formwork and equally distribute the fresh concrete in the

structure, consolidation is very important. Sometimes it is not possible to vibrate and

consolidate the fresh concrete due to poor workmanship and lack of equipment. Due to

having self-consolidating property SCC has overcome this problem (Safiuddin et al.,

2014).

1.2 PROBLEM STATEMENT

In Bangladesh, the growth of structural activities is increasing very rapidly. In that

case, the natural stone has a limited source and there is a crisis to meet the present

demands. Crushed bricks are widely used as an alternative source of natural stone

aggregate in this region. Brick aggregates are locally available, and cheaper than stone

aggregate. To enhance the expected mechanical properties, it is essential to confirm the

proper placement and compaction of concrete. In context of Bangladesh skilled labors

are not available and cost of the skilled labors are high. Sometimes it is not possible to

ensure the proper compaction and placement even in the presence of skilled laborers

and equipment. This problem can be minimized by using SCC. In view of the potential

construction materials, SCC with brick aggregate can be introduced to overcome these

problems and it is required to grab the benefit of new construction materials like SCC

with brick aggregate.

Researchers have investigated various properties of SCC with different types of

aggregates. Fresh and mechanical properties of SCC with natural aggregate was studied

by Mohamad et.al (2016). Fresh properties of SCC were investigated with crushed

granite stone incorporating palm oil fuel ash (POFA) Safiuddin et al. (2011a) and fresh

properties of SCC with recycled concrete aggregate were investigated by Safiuddin et

al. (2012a). Microstructure of high strength SCC with POFA was investigated by Salam

3

et al. (2013). Furnace slag, expanded clay and expanded shale were used as coarse

aggregate by Abdurrahman Lotfy (2006) to study the properties of SCC. Khaleel et al.

(2011) used crushed gravel, uncrushed gravel and crushed limestone to investigate the

effect of coarse aggregate on fresh and hardened properties of SCC. Five different types

coarse aggregate such as basalt, marble, dolomite, limestone and sand stone were used

to study the mechanical properties of SCC by Uysal (2012). An attempt were taken by

Roy et al. (2019) to make SCC with locally available brick aggregate incorporating

different w/c ratio. Dey et al. (2016) investigated the effect of recycled brick aggregate

replacement on the rheological and mechanical properties of self-compacting concrete.

However, most of the previous efforts and attempts in the field of SCC were concerned

with different types of coarse aggregates. A very few attempts were taken to study the

SCC using crushed brick as coarse aggregate. Development of SCC with BA is

expected to improve the homogeneity of the concrete, to eliminate the scarcity of skilled

labor and non-uniformity of concrete with the consumption of less energy. Therefore,

it is necessary to develop proper proportions and guidelines of SCC with BA.

To fill the formwork uniformly and to spread the fresh concrete in the structure without

compaction and vibration, SCC with BA is expected to play an important role in the

construction sectors. Therefore, research on SCC with brick aggregate will be very

interesting.

1.3 OBJECTIVES OF THE RESEARCH

The principal goal of this research was to investigate the properties of self-compacting

concrete made with crushed brick as coarse aggregate. The specific objectives of this

research were:

a. To investigate the fresh properties of self-compacting concrete with brick

aggregate;

b. To evaluate the effect of brick aggregate on the mechanical properties of self-

compacting concrete;

c. To suggest the potential use of brick aggregate for the production of self-

compacting concrete.

1.4 SCOPE OF THE RESEARCH

This research was associated with the investigation of the fresh and mechanical

properties of self-compacting concrete made with crushed brick as coarse aggregate.

To study the feasibility of SCC with brick aggregate, 19 mm downgraded and 12.5 mm

4

downgraded brick chips were used as coarse aggregate which was prepared by crushing

well burnt first class bricks. Locally available coarse sand as fine aggregate and

Portland Composite Cement (BS EN 197-1:2011/CEM II) as binding material were

used in the preparation of concrete. SCC mixes were fixed by various contents of coarse

aggregate (550 kg/m3, 560 kg/m3 570 kg/m3 and 580 kg/m3) and cement contents (450

kg/m3, 470 kg/m3, 500 kg/m3, 530 kg/m3, 550 kg/m3 and 580 kg/m3). These mixes were

prepared following the EFNARC (2002 and 2005) guidelines and laboratory trial to

satisfy the criteria of SCC. A total of twenty-four successful mixes were prepared with

water binder ratios of 0.35 and 0.40. To increase the workability with less water-cement

ratio, high range water reducer (HRWR) was used as superplasticizer (SP). The

gravimetric mixes were prepared using these materials to investigate the fresh and

mechanical properties. Concrete mixes were varied with the aggregate size, aggregate

volume, dosages of HRWR and water content. Several attempts were carried out to fix

the volume of paste and aggregate to justify the following properties of fresh concrete.

Slump flow

T50 slump flow time

V-funnel flow time

V-funnel flow at T5minutes

J-ring flow

J-ring blocking index

Height difference just inside and outside of the bar at J-Ring

L-box blocking ratio.

After confirming the successful trial mixes, mechanical properties of hardened concrete

were tested in the laboratory. To satisfy the structural requirements of SCC with brick

aggregate, the following mechanical properties have been investigated:

Compressive strength at 28 days (fΚΉc)

Splitting tensile Strength (fsp)

Modulus of elasticity (Ec).

1.5 OUTLINE OF THE THESIS

This thesis focused on the fresh and mechanical properties of SCC with brick aggregate.

It is organized into five chapters describing a summary of the content of each chapter.

In the first chapter, a brief introduction is given about SCC, research significance,

objectives, scope and outline of the thesis.

5

Chapter II describes the historical development of SCC from the very beginning with

the continuous improvement over ninety decades. Based on the review of literature it

includes various materials used in the production of SCC and historical background of

mix proportion. In addition, this chapter describes fresh as well as mechanical

properties of SCC with various aggregates that found from literatures.

The detailed research methodology including the collection and preparation technique

of the materials and testing method used in this research are included in Chapter III.

This chapter also explains a detailed research plan, mix proportions and different testing

procedures of the materials. In addition, this chapter describes the preparation, testing

of the fresh properties of SCC, curing and testing standards or procedure of hardened

concrete specimen that was used in this research.

Chapter IV presents and discusses the test results that were obtained from different

experiments. It also gives various fresh and mechanical properties of SCC specimens

made with brick chips. Correlation between fresh and mechanical properties are

illustrated here. After analyzing the test results, the feasibility to the potential use of

SCC with brick aggregate with different condition have been checked.

In the last chapter, the conclusions and recommendations on the fresh and mechanical

properties of SCC with brick aggregate concrete are reported.

6

CHAPTER 2 CHAPTER II

…………………. LITERATURE REVIEW

2.1 INTRODUCTION

In this chapter, the literature relevant to this research are reviewed. A significant amount

of research paper and articles were studied with respect to different aspects to Self-

Compacting Concrete (SCC) such as mixture proportion methods, fresh and mechanical

properties including the history of the development of SCC. The effects of the use of

different aggregates on the fresh and mechanical properties of SCC have been studied

in this chapter. The literature emphasizes that the use of brick aggregate plays an

important role as a potential material for the production of SCC. A short summary of

various papers and articles were studied and reported here.

2.2 DEFINITION OF SCC

Self-compacting concrete (SCC) is known as super workable concrete or self-

compactable concrete. It is a relatively new type of high performance concrete. This

concrete can be placed without vibration equally well even in the heavily reinforced

sections. It has excellent deformability and segregation resistance, which result in the

quality of the hardened concrete. SCC being independent of the workmanship during

placing. SCC can possess the excellent filling ability, passing ability and segregation

resistance which are known as fresh properties. According to the specification and

guideline of EFNARC (2002), a concrete mix can be classified as SCC if it possesses

the required filling ability, passing ability, and segregation resistance. Self-compacting

concrete (SCC) is defined as, a highly flowable concrete that does not segregate and

can spread into place, fills the formwork with heavily congested reinforcement, and

encapsulates the reinforcement without any mechanical vibration (ACI 237R-07,

2007). It is also known as self-consolidating concrete, self-leveling concrete, self-

placing concrete which all are subsets of SCC. The definition of SCC was included by

Ozawa (Ozawa et al., 1992) which is shown in Fig. 2.1

2.3 ADVANTAGES OF SCC

Self-compacting concrete (SCC) is an important discovery in the history of the

construction industry. It is a highly flowable concrete and helps to place the concrete

with minimal disturbance to the matrix of fresh concrete, leading to a well-finished

product. It possesses improved durability compared with normal vibrated concrete.

7

Fig. 2.1: Definition of self-compacting concrete (Ozawa et al., 1992)

Properly proportioned and placed SCC can result in both economic and technological

benefits for the end user. SCC can provide the following benefits:

Reduce labor, labor cost and equipment.

No need for vibration to ensure proper consolidation.

Ensure the flat surfaces of concrete (self-leveling characteristic).

Enable the casting of concrete that develops the desired mechanical properties.

Accelerate construction and shorter construction duration.

Facilitate the filling of concrete in highly reinforced sections and complex

formwork

Increase construction quality. This can ensure better productivity.

Reduce noise on the job site

Reduce the need of vibration for construction

Permit more flexibility for detailing reinforcing bars and avoid the need to

bundle reinforcement

Create smooth surfaces free of honeycombing and signs of bleeding and

discoloration.

However, the advantages of SCC were summarized by Ozawa et al. (1992) and shown

in Fig. 2.2.

8

Fig. 2.2: Advantages of SCC (Ozawa et al., 1992)

SCC often accompanied by some disadvantages. The main disadvantages of SCC are:

Higher material cost

Higher standard quality control is required for its production

Higher lateral pressure on the formwork

Higher pumping resistance.

However, these disadvantages can be reduced through proper management and

improved mix design.

2.4 DEVELOPMENT OF SCC

Nowadays SCC is a classy building material and a part of modern Civil Engineering

technology. Its use is increasing in the strategy of concrete placement on construction

sites. The number of structures that use this concrete is increasing year to year and

growing anticipation of its effectiveness. The affluent use of SCC requires a valuable

understanding of the behavior of this material, which is vastly divergent from traditional

concrete. For this motive, a lot of research has been conducted on this aspect all around

the world for the last 30 years intended for both practitioners and scientists. The

9

problem of the durability of concrete structures was a major topic of interest in Japan

beginning in 1983. This situation is seen as a major problem facing Japanese society.

The gradual reduction of the number of skilled workers in Japan's construction industry

has caused a similar reduction in the quality of construction work. Therefore, the

development of self-compacting concrete is necessary to guarantee durable concrete

structures in the future.

The idea of self-compacting was initially proposed by Professor Hajime Okamura in

Japan in 1986 (Okamura, 1986) at the University of Tokyo and the reputed Japanese

contractors (e.g. Kajima Co., Maeda Co., Taisei Group Co., etc.). The first prototype

was developed in August 1988 (Ozawa et al., 1992) with satisfactory performance in

hardening, shrinkage, heat of hydration and other properties. Within the last couple of

years, the entire world has increased usage of SCC for cast-in-place and particularly for

precast concrete construction. Many agencies worldwide demonstrate interest and are

working towards developing tests, specifications and finally adopting this kind of

concrete. A lot of initial work and investigation have already been done in Japan and

Europe and it is very important to develop the knowledge of understanding and the

usage of SCC in the Bangladesh for the adoption and enhancement of the concrete

products.

SCC was first introduced with the name Consolidation Free Concrete 1986 (Okamura,

1986). The authors also use the term β€˜High-Flowability’ and β€˜Superflowable’ but they

do not clearly indicate the consolidation property. Due to having the ability of filling

the corner of the formwork under its own weight, it refers to self-compacting

concrete (Ozawa et al., 1992).

Ozawa et al. (1989) have used high-performance concrete which exhibits excellent

performances in the fresh and hardened state. To avoid misleading, the same sense of

self-compacting concrete has been used in Europe and America, the authors use Self-

Compacting High-Performance Concrete to refer the concrete which advocates the

capabilities while fresh state (Okamura and Ozawa, 1994).

The SCCs were used under trade names, such as the NVC (Non-vibrated concrete) of

Kajima Co., SQC (Super quality concrete) of Maeda Co. or the Biocrete (Taisei Co.).

Simultaneously with the developments in the SCC area, research and development

continued in mix-design and placing of underwater concrete where new admixtures

were producing SCC mixes with performance matching that of the Japanese SCC

concrete (Ferraris, 1999).

10

The idea of SCC turned into a spread to the sector after the presentation on self-

consolidating concrete by Ozawa et al. (1992). In April 1997, the Japanese Society of

Civil Engineers (JSCE, 2007) formed a studies sub-committee for setting up hints for

the realistic application of SCC. This changed into finally published in English in

August 1999 (Uomoto, 1999). In August 1998, the first workshop on self-consolidating

concrete turned into held in Kochi, Japan which was an important event for the

development of SCC.

In the overdue nineties, interest and use of SCC unfold from Japan to other international

locations, which includes Europe. Sweden becomes the first in the Europe to start the

development of SCC, and in 1993 the CBI organized a seminar in Sweden for

contractors and manufacturers leading to a challenge aimed at reading SCC for housing

(Billberg, 1999). A specification has been produced in 2002 by EFNARC (EFNARC,

2002) aiming to offer a tenet for the design and use of SCC in Europe primarily based

on contemporary research findings. Most of the important European international

locations have advanced or present inside the system of developing tips or

specifications for the usage of SCC.

The mechanism of obtaining self-compatibility and the proportion of the materials for

SCC are found in literatures. Mechanism of achieving self-compactability, mix design

method and testing method were proposed by Okamura and Ouchi (2003). They have

employed the method to achieve the self compactability shown in Fig. 2.3.

Fig. 2.3: Method of achieving self compactability (Okamura and Ouchi, 2003)

11

Since the early development of SCC in Japan, this new class of high-performance

concrete has been employed in several countries in cast-in-place and precast

applications (Okamura and Ozawa, 1994; Ferraris, 1999; JSCE, 2007; Uomoto and

Ozawa, 1999). The following references provide various examples of the early use of

SCC in civil engineering applications (Okamura and Ouchi, 2003; Billberg, 1999;

RELIM, 2000; Skarendahl, 2013).

SCC has recently been used in concrete repair applications in Canada and Switzerland,

including the repair of bridge abutments and pier caps, tunnel sections, parking garages,

and retaining walls, where it ensured adequate filling of restricted areas and provided

high surface quality (Ouchi, 2001; Hayakawa et al. 1995).

However, the research on SCC spreads all over the world. Researchers have carried

out the studies on self-compacting concrete to improve the best quality concrete and

its application is systematically in progress.

2.5 CLASSIFICATION OF SCC

The requirements for SCC in the fresh state depend on the type of application, and

especially on confinement conditions, placing equipment, placing methods and

finishing methods. Based on the application and fresh state, SCC can be classified to

cover these requirements according to EFNARC (2005).

Based on slump flow:

Slump-Flow Class Slump-flow (mm)

SF1 550 to 650

SF2 660 to 750

SF3 760 to 850

The following are typical slump-flow classes for a range of applications:

SF1 (550-650 mm) is appropriate for unreinforced or slightly reinforced concrete

structures that are cast from the top with free displacement from the delivery point. SF2

(660-750 mm) is suitable for many normal applications e.g. walls, columns and SF3

(760-850 mm) is typically produced with a small maximum size of aggregates (less

than 16 mm) and is used for vertical applications in very congested structures.

12

Based on Viscosity:

Viscosity Class T500 (sec) V-funnel time (sec)

VS1/ VF1 ≀ 2 ≀ 8

VS2/ VF2 > 2 9 to 25

Based on passing ability (L-Box):

Passing ability Class Passing ability

PA1 β‰₯ 0.80 with 2 rebars

PA2 β‰₯ 0.80 with 3 rebars

Based on the visual stability properties of slump flow area of concretes, Kandemir et

al. (2010) classified self-compatibility as:

Self-compatibility Visual information notes

Proper SCC

No indication of segregation. Uniform aggregate distribution

throughout, coarse aggregate carried to the perimeter of the

slump flow. No indication of bleed water or mortar halo on the

surface or around the perimeter.

Acceptable SCC Little evidence of mortar halo and bleed water separation. Good

aggregate distribution, although a small ring of mortar is

present at the outer edges of the slump flow.

Marginal SCC Mix exhibits signs of instability and segregation. More

pronounced mortar halo or uneven distribution of aggregate is

expected.

Unacceptable SCC Mix exhibiting poor aggregate distribution, segregation and

excessive bleed water. Coagulation of the coarse aggregate

particles in the center of the slumping area. Separation of

mortar around the perimeter of the slump-flow area.

13

2.6 INGREDIENTS OF SCC

The basic ingredients of SCC are similar to those of normal concrete. Generally, the

aggregates occupy 55–60% of the SCC volume (Nischay et al., 2015) and play a

substantial role in determining the workability, strength, dimensional stability, and

durability of concrete. Sometimes chemical admixture like high range water reducer

(HRWR) and viscosity modifying admixture (VMA) may be used with the constituent

of normal concrete to produce SCC.

SCC design has little difference from conventional concrete. It may have more fine

contents to fill up existing pours in concrete. SCC mixtures typically designed to have

a higher paste volume, lesser coarse aggregate and higher sand to coarse aggregate ratio

compared to traditional concrete. Increased paste volume can be obtained by increasing

the fine contents. But a well-distributed aggregate grading can reduce fines materials

and dosage of admixture. For successful SCC design, the smaller aggregate is better.

Because it spread out easily by own weight and passing through congested

reinforcement. An ideal SCC should contain a well grade of aggregate size (20-25) mm

(Olafusi et al., 2015) and superplasticizers to achieve a target flowing ability passing

ability and segregation resistance.

Conventional concrete with stone chips has a high water-cement (w/c) ratio for proper

placement of fresh concrete into formwork with heavily congested reinforcement. A

higher w/c ratio for increasing the flowability of concrete may compromise the

durability of SCC. But the proper design of SCC with lower w/c ratio in addition with

HRWR and VMA can flow easily through the congested reinforcement and properly

fill the forms without reducing the strength. A comparison of proportioning of the

materials for SCC and conventional concrete is shown in Fig. 2.4 (Okamura and Ouchi,

2003).

Fig. 2.4: Comparison of proportion of the materials for SCC and conventional

concrete (Okamura and Ouchi, 2003)

14

2.6.1 Aggregates

SCC is a new category of high-performance concrete that exhibits low resistance to

flow to ensure high flowability, and a moderate viscosity to maintain a homogeneous

deformation through restricted sections. The common practice to obtain self-

consolidation behavior in SCC is the limitation of the coarse aggregate content,

reduction of the maximum size of aggregates, and the use of superplasticizer (Khayat,

2015). According to the guideline of EFNARC (2002) for SCC coarse aggregate

volume was kept a maximum 50 percent of total aggregate and aggregate size for SCC

is generally limited to 12-20 mm. The particle size distribution and the shape of coarse

aggregate directly influence the flow and passing ability of SCC and its paste demand.

The maximum aggregate size for SCC is generally limited to 16-20 mm (EFNARC,

2005). However aggregate size 40 mm or above used in SCC but consistency of grading

is of vital importance (EFNARC, 2005).

The improvement of the SCC were possessed with the investigation of various types of

coarse aggregate such as Basalt, marble, dolomite, lime stone and Sandstone (Uysal,

2012), Crushed Granite (McBridge, 2003), Furnace slag, expanded clay and expanded

shale (Abdurrahman Lotfy, 2006), Crush gravel, uncrushed gravel and crush limestone

(Khaleel et al., 2011), Light expand clay aggregate (Maghsoudi et al, 2011), Natural

crushed stone (Zhao et al., 2012), Electric Arc Furnace Slag (SantamarΓ­a et al., 2020),

(crushed brick (Roy et al., 2019). Recycled aggregate also were used as coarse

aggregate by Safiuddin et al. (2011), Dey et al. (2016), Panda and Bal, (2013), Ardalan

et al., (2020) for the preparation of SCC. Incorporation of supplementary cementitious

materials (SCMs) like fly ash (Sua-iam and Makul.,2015) metakaolin (Kannan and

Ganesan, 2014), silica fume, limestone filler (Pradhan and Panda, 2017), marble

powder(Uygunoğlu et al., 2014), slag (Sharma and Khan, 2017), and granite powder

(Sadek et al., 2016) are used to make SCC more homogeneous, viscous, and dense.

Uysal (2012) studied the effectiveness of various types of coarse aggregates on fresh

and hardened properties of self-compacting concrete (SCC). Five different coarse

aggregates such as basalt, marble, dolomite, limestone and sandstone were used to

produce SCC containing fly ash. Slump flow, T50 time and V-funnel tests were

conducted on fresh concrete and abrasion, compressive strength, static and dynamic

elastic moduli and ultrasonic pulse velocity tests were performed on hardened concrete.

The compressive strength values of the hardened SCC were noted at 28 days, 56 days

and 90 days. The best performance was measured in SCC mixture prepared with basalt

aggregate while the lowest was noted in SCC mixture prepared with limestone

aggregate.

15

Grdic et al. (2008) studied the properties of SCC with natural aggregates in addition of

various types of additives like fly ash, silica fume, hydraulic lime and a mixture of fly

ash and hydraulic lime. Test results show that the addition of fly ash to the mixture

containing hydraulic lime is quite beneficial, bringing a substantial improvement of the

behavior of concrete. The silica fume imparts in the SCC a similar behavior to the one

of normal concrete and increase of water/cement ratio for the same concrete

workability.

Nischay et al. (2015) studied the fresh and hardened properties of self-compacting

concrete using recycled aggregate. Fine and coarse aggregates used in this study, both

were collected from concrete waste. Concrete mix proportioned with 0%, 25%, 50%,

75% and 100% replacement of fine and coarse aggregates separately. It was observed

that 50% replacements in all batches of the concrete mix have exhibited satisfactory

flow and compressive strength values.

Jishou Yu et. al. (2015) researched the effect of elongated and flaky particles content

on the properties of concrete. A total of elongated and flaky particles 6.8%, 16% and

25.2% were incorporated in this study. The results revealed that workability,

compressive strength, drying shrinkage and impermeability were weakened with the

increasing of elongated and flaky particle content. The workability and maximum

packing density can be achieved when the content of elongated and flaky particles fewer

than 16%.

Mohamad et al. (2016) conducted research on SCC incorporating high volume fly ash

with natural aggregate to investigate the fresh and mechanical properties. In that study

cement was replaced by fly ash and slump flow, J-ring and V-Funnel test were

performed for fresh state and compressive strength and modulus of elasticity were

determined. Results revealed that up to 40% replacement of fly ash exhibits the

optimum result for the workability and mechanical properties test.

Limestone-based natural aggregate and metakaolin, silica fume, zeolite, and viscosity

modifying admixture were used by Mahoutian and Shekarchi (2015). Two different

types of fine aggregates were used to observe the effect of gradation of sand on the

properties of SCC. The results show that sand grading significantly affects the fresh

properties of SCC and limestone can be effectively used as filler in SCC in high volume

content.

Safiuddin et al. (2011a) suggested that recycled concrete aggregate (RCA) can be used

in SCC. In that study natural coarse aggregate (NCA) was replaced by recycled

16

concrete aggregate to study the properties of SCC. Test results have shown that up to

50% substitution of NCA can be used without affecting the key fresh properties of

concrete.

Crushed granite stone as coarse aggregate and Palm oil fuel ash (POFA) were used as

supplementary materials of cement by Safiuddin et al. (2012a). The study reveals that

the presence of POFA improved the stability of the concrete mixture and provides a

lower visual stability index. Also, the segregation index and segregation factor obtained

from sieve and column tests, respectively, decreased with greater POFA content. The

overall findings suggest that the filling ability and passing ability of SCC decreased

whereas its segregation resistance increased with higher POFA content. In another

study, Palm oil fuel ash was used as a partial replacement of normal Portland cement

with crushed granite stone to study the correlation between different high-strength self-

consolidating concrete (SCHSC) by Safiuddin et al. (2012b). The compressive, splitting

tensile and flexural strengths, modulus of elasticity, ultrasonic pulse velocity, and

porosity of various self-consolidating concrete mixes were investigated. The

experimental findings revealed that strong correlations exist between different

hardened properties of high-strength self-consolidating concrete.

Salam et al. (2013) investigated the microstructures of self-compacting high strength

concrete (SCHSC) with crushed granite stone as coarse aggregate. The main focus of

that study was the effect of palm oil fuel ash (POFA) on the microstructure of self-

consolidating high-strength concrete. The scanning electron micrographs (SEMs) of the

concretes revealed that POFA contributes to producing a denser microstructure, which

increases the compressive strength and reduces the permeable porosity of SCHSC.

A study was conducted on the fresh and mechanical properties of SCC with Waste of

Oil Palm Shell (OPS) as the replacement of natural coarse aggregate by Prayuda et al.

(2018). The results of this study indicate that replacement of aggregate using OPS meets

fresh properties criteria and although the compressive strength of OPS concrete mixture

is lower than normal SCC.

A review of the literature was studied by Shahrukh and Shashikant (2018) on the

aggregate flakiness on the compressive strength and workability of concrete. Study

reveals that flaky aggregates beyond certain limit decreases strength and workability.

Hence the strength of concrete greatly depends on internal structure and flakiness of

aggregates. The compressive strength of concrete decreases with increases in

percentage of flaky aggregates because of increases in voids.

17

Andrews (2009) used expanded clay and crushed limestone to investigated the effect of

lightweight aggregate on SCC. This study focuses on the flow rates of lightweight

aggregates and structural lightweight self-consolidating concrete. The flows of SCC

with all lightweight aggregates were found between 5.5 and 9 seconds. The

compressive strengths and weights of SCC and normal concrete are also compared

along with the flow rates. The author has shown that compressive strength of concrete

increase with increasing the unit weight.

Crushed Granite was used to study the effect of the content and gradation of coarse

aggregate on the passing ability of SCC by McBride (2003) The experiment was

conducted with varying aggregate content and gradation to perform passing ability test,

slump flow test, horizontal flow test and stereology test and to develop a relationship

between passing ability, aggregate size and aggregate free distance. The result shows

that passing ability is a linear function of the ratio of maximum aggregate size and

aggregate free distance and also aggregate random spacing.

Roy et al. (2019) have study the self-compacting concrete (SCC) made with locally

available materials. In their studied a fixed mixed proportion was incorporated with

various water cement ratios. Brick aggregate was used as coarse aggregate to prepare

the SCC mixes. The experimental studies were conducted on the fresh and mechanical

properties of SCC. The results revealed that both compressive and tensile strengths

increased with the reduction of w/c ratio and values of both fresh and mechanical

properties have satisfied the ACI specifications. Therefore, researchers suggested the

locally available materials could be used to develop.

Another research with recycled brick aggregate was carried by Dey et al. (2016). Effect

of recycled brick aggregate (RB) replacement on the rheological and mechanical

properties of self-compacting concrete (SCC) were studied by the researchers. In that

study the virgin brick aggregates were replaced at 0%, 25%, 50%, 75%, and 100% with

recycled brick aggregate. The results indicated that the fresh and mechanical properties

of recycled aggregates concrete is almost similar and it is feasible to produce SCC with

recycled coarse aggregate.

Lotfy (2006) have studied the effect of various lightweight aggregates namely, furnace

slag, expanded clay and expanded shale on the properties of lightweight self-

consolidating concrete to evaluate the fresh and hardened properties. Lightweight Self-

Consolidating Concrete mixture were prepared with water/binder ratio of 0.30 to 0.40,

high range water reducing agent (HRWRA) of 0.3 to 1.2% (by total content of binder)

and total binder content of 410 to 550 kg/m3. Slump flow diameter, V-funnel flow time,

18

J-ring flow diameter, J-ring height difference, L-box ratio, filling capacity, bleeding,

fresh air content, initial and final set times, sieve segregation, fresh weight, 28-days air

and 28 days oven dry unit weights and 7 and 28 days compressive strengths were

evaluated in this study. The mixtures were evaluated by conducting the compressive,

flexural, splitting tensile strength, bond strength, drying shrinkage, sorptivity,

absorption, porosity, rapid chloride-ion permeability, hardened air void (%), spacing

factor, corrosion resistance, resistance to elevated temperature, salt scaling, freeze-thaw

resistance and sulphuric acid resistance tests. It was possible to produce lightweight

self-consolidating concrete mixtures that satisfy the EFNARC criteria for self-

consolidating concrete.

Effect of the shape and size of coarse aggregate on the properties of self-compacting

concrete were investigated by Pandurangan et al. (2012). Authors indicates that the

coarse aggregate shape and size affects the concrete strength through a complex

relationship of aggregate-to- cement paste bonding properties. SCC mixes were

prepared with 60 % and 40% replacement of cement with fly ash and 10 mm, 16 mm

and 20 mm coarse aggregates. The results of this study indicates that the flowability

and strength of SCC mixes with 10 mm to 16 mm was better than SCC with 20 mm.

This study also shows that the shape of the aggregate has no influence on the flowability

of SCC mixes.

Zhao et al. (2012) assess the effect of coarse aggregate gradation on the properties of

SCC with natural crushed stone. Total four A/B (coarse aggregate size 5–10 mm coarse

aggregate weight to size 10–20 mm coarse aggregate weight) ratio of 4/6, 5/5, 6/4, 7/3

were used for the preparation of SCC and the fresh and mechanical properties, porosity

and durability properties of SCC was studied. The results show that aggregate with A/B

ratio for 6/4 has a maximum bulk density of aggregate. The change in A/B ratio from

4/6 to 7/3, the initial slump flow, blocking and segregation ratio are decreasing, while

the wet density of fresh SCC is increasing. SCC with A/B ratio for 6/4 had a maximum

mechanical property, least porosity, carbonation depth, chloride ion diffusion

coefficient.

In a study (Felekoglu et al., 2007), five mixtures with different water/cement ratio and

superplasticizer dosage were investigated. Slump flow, V-funnel, L-box were carried

out to determine optimum parameters for the self-compactibility of mixtures.

Compressive strength, modulus of elasticity and splitting tensile strength hardened

concrete were also studied. Results of this study shows that the optimum water/cement

ratio for SCC is in the range of 0.84–1.07 by volume. The ratios above and below this

range may cause blocking or segregation of the mixture. Also it was obtained that

19

higher splitting tensile strength and lower modulus of elasticities from SCC mixtures

when compared with normal vibrated concrete.

Electric Arc Furnace Slag (EAFS) was used by SantamarΓ­a et al., (2020) as coarse

aggregate in the production of high-volume batches of SCC. Mixtures containing EAFS

aggregate in proportions of nearly 50% by volume are prepared for use as pumpable

and self-compacting mixes with consistency classes of S4 and SF2, respectively. The

results yielded compressive strengths of approximately 60 MPa and elastic moduli of

38 GPa after one year.

All normal concreting sands are suitable for SCC. Both crushed or rounded grains of

sand can be used. Siliceous or calcareous sands can be used. The traditional fine

aggregates such as river or mining sand are also used in SCC. The amount of fines less

than 0.125 mm is to be considered as powder and is very important for the rheology of

the SCC (EFNARC, 2002).

2.6.2 Cement

All types of cement conforming are suitable. In the study of SCC made with locally

available materials by Roy et al. (2019) have used CEM-II/B-M type cements and

Kandemir and TΓΌrkel (2010) have used OPC (CEM-I) with mineral admixture for the

preparation of SCC with different aggregates. The selection of the type of cement will

depend on the overall requirements for the concrete (EFNARC, 2005) such as strength,

durability, etc.

C3A content higher than 10% may cause problems of poor workability

retention.

The typical content of cement is 350-450 kg/m3. More than 500 kg/m3

cement can be dangerous and increase the shrinkage. Less than 350 kg/m3

may only be suitable with the inclusion of other fine fillers, such as fly ash,

pozzolan, etc.

Total powder content 160 to 240 liters (400-600 kg) per cubic meter.

SCC generally requires a low water/binder (W/B) ratio (0.30–0.40), high cement

content, and low amount of coarse aggregate (Ozawa et al., 1989). Besides, SCC needs

several ingredients such as supplementary cementing material (SCM), filler materials

mineral filler, pigments, fly ash, silica fume, ground granulated blast furnace slag,

hydraulic lime etc. in addition to the basic constituents of ordinary concrete. SCC can

be prepared with different types additives: fly ash, silica fume, hydraulic lime and a

mixture of fly ash and hydraulic lime Grdic et al, (2008).

20

2.6.3 Admixtures

It must need HRWR to achieve the self-consolidation capacity of concrete (Okamura

and Ozawa, 1995). Two types of chemical admixture such as HWRA and VMA were

engaged by Roy et al. (2019) in their research. Researchers such as Uysal, (2012), Grdic

et al, (2008) have investigated the SCC with various types of HRWR, VMA for various

fresh and mechanical properties. SCC consists of supplementary cementitious

materials, mineral admixtures such as limestone powder, chemical admixtures such as

superplasticizer (SP) and viscosity modifying agents (VMA), and water.

2.7 MIX DESIGN

Mix design is an essential first step for both research programs and practical application

of concrete and such a step must start with the definitions of the applications of SCC.

To ensure a good balance between the fresh properties of SCC such as deformability

and segregation resistance, the proportion of the constituent materials must be carefully

designed. Properties of SCC like rheology, strength, shrinkage and durability are also

affected by the mix design method, the characteristics of raw materials, incorporation

of chemical and mineral admixtures, aggregate packing density, water to cement ratio

(W/C) (Esmaeilkhanian et al., 2014; Han et al., 2014; Siddique et al., 2012 and Wang

et al., 2014)

There are different mix proportioning methods used to develop SCC mixes, they do

share some similarities. In reviewing of the proposed mix design methods, it is difficult

to compare one method to another, because each method has been developed according

to its own particular conditions and environment, and has its own special features and

some inherent limitations. These methods can be categorized into different classes (Shi

et al., 2015) as empirical mix design method, compressive strength method, aggregate

packing method, a method based on the statistical factorial model, and rheology of paste

model.

There are many techniques available in the literature for proportioning Portland cement

concrete. ACI absolute volume method of mix proportioning (ACI Committee, 2002)

is one of the maximum used normal processes by the concrete industry. Due to the

special desires of SCC in its fresh state much challenge to the designer.

Indicative typical ranges of proportions and quantities in order to obtain self-

compatibility are given below (EFNARC, 2002). Further modifications will be

necessary to meet strength and other performance requirements.

21

Water/powder ratio by volume of 0.80 to 1.10;

Total powder content 160 to 240 liters (400-600 kg) per cubic meter.

Coarse aggregate content normally 28 to 35 percent by volume of the mix.

The water-cement ratio is selected based on requirements. Typically water

content does not exceed 200 liters/m3.

The sand content balances the volume of the other constituents.

EFNARC (2005) gives an indication (Table 2.1) of the typical range of constituents in

SCC by weight and by volume. These proportions are in no way restrictive and many

SCC mixes will fall outside this range for one or more constituents.

Table 2.1: Typical range of SCC mix composition (EFNARC, 2005)

Constituent Typical range by mass

(kg/m3)

Typical range by Volume

(liters/m3)

Powder 380-600

Paste 300-380

Water 150-210 150-210

Coarse Aggregate 750-1000 270-360

Fine aggregate (sand) Content balances the volume of the other constituent,

typically 48-55% of total aggregate weight.

Water/Powder ratio by Vol. - 0.85-1.10

An expert system for mix design of high-performance concrete was developed by Zain

et al. (2005). This system was capable of selecting proportions of mixing water, cement,

supplementary cementitious materials, aggregates and superplasticizer, considering the

effects of air content as well as water contributed by superplasticizer and moisture

conditions of aggregates. This system has explanation facilities, can be incrementally

expanded, and has an easy to understand knowledge base.

The required properties of the fresh and hardened SCC should be concentrated on

during mix designing. Figure 2.5 shows the variables that are focused on with the fresh

properties of SCC (ACI 237R-07, 2007). ACI Committee also proposed a mix

proportioning Procedure for natural aggregates.

22

The following is a summary of steps for determining the performance requirements and

proportioning of SCC (EFNARC, 2005).

Step 1: Determine slump flow performance requirements

Step 2: Select coarse aggregate and proportion (ACI 211.1 and 301);

Step 3: Estimate the required cementitious content and water;

Step 4: Calculate paste and mortar volume;

Step 5: Select admixture;

Step 6: Batch trial mixture;

Step 7: Test. When assessing the workability attributes of SCC (stability, filling

ability, and passing ability), the slump flow test, as well as a test to evaluate

stability and passing ability (such as column segregation, J-ring, or L-box),

should be run; and

Step 8: Adjust mixture proportions based on the test results and then rebatch

with further testing until the required properties are achieved.

Fig. 2.5: Variables Involved in establishing the required fresh SCC properties (ACI

237R-07, 2007)

23

The proposed proportions for the ACI SCC mix design proportioning are presented in

Table 2.2.

Table 2.2: SCC proportioning trial mixture parameters (ACI 237R-07, 2007)

Absolute volume of coarse aggregate 28 to 32% (>12.5 mm nominal size)

50% (<12.5 mm nominal size)

Paste fraction (calculated on volume) 34 to 40% (Total mixture volume)

Mortar fraction (calculated on volume) 68-72% (Total mixture volume)

w/cm 0.32 to 0.45

Cement (powder content) 386 to 475 kg/m3

Many references provide various examples of the mix design and proportioning of mix

design of SCC (Li et al., 2012; Maghsoudi et al., 2011).

2.8 FRESH PROPERTIES

Fresh properties of SCC are described in terms of filling ability, passing ability and

segregation resistance, and is characterized by specific testing methods. SCC is highly

flowable, no segregating concrete that can spread into place, fill formwork, and

encapsulate reinforcement without any mechanical consolidation. There is no one test

that can measure all three characteristics at once. Many different test methods have

been developed in attempts to characterize the properties of SCC.

The test methods which characterizes all the relevant aspects of fresh properties

(EFNARC, 2002) are described in detail in Table 2.3.

Table 2.3: List of test methods for workability properties of SCC (EFNARC, 2002)

Sl. No. Test Method Property Measured value

1 Slump-flow by Abrams cone

Filling ability

Total spread

2 T50 cm slump flow Flow Time

3 V-funnel Flow Time

4 Orimet Flow Time

5 J-ring

Passing ability

Step height, Total flow

6 L-box Passing ratio

7 U-box Height difference

8 Fill-box Visual filling

9 V-funnel at T5minutes Segregation

resistance

Flow Time

10 GTM screen stability test Segregation ratio

24

Also Table 2.4. shows the typical acceptance criteria of self-compacting concrete for a

maximum aggregate size up to 20 mm. These requirements are to be fulfilled at the

time of placing (EFNARC, 2002).

Table 2.4: Acceptance criteria for self-compacting concrete (EFNARC, 2002)

Sl.

No.

Method Unit Typical rang of values

Minimum Maximum

1 Slump-flow by Abrams

cone

mm 550 850

2 T50 cm slump flow sec 2 5

3 J-ring mm 0 10

4 V-funnel sec 6 12

5 V-funnel at T5minutes sec 0 +3

6 L-box (h2/h1) 0.8 1.0

7 U-box (h2-h1)

mm

0 30

8 Fill-box % 90 100

9 GTM screen stability

test

% 0 15

10 Orimet sec 0 5

2.8.1 Filling Ability

The filling ability describes the ability of SCC to flow into and fill completely all spaces

within the formwork, under its own weight. The filling ability of SCC is measured with

slump flow, T50 flow time and V-funnel flow time.

SantamarΓ­a et al. (2020) reported the slump flow of SCC made with Electric Arc

Furnace Slag as coarse aggregate was 680 mm-700 mm. Roy et al. (2019) reported the

slump flow of SCC made with brick aggregate was 427 mm-712 mm, T50 flow time

was varied from 2 to 7 seconds and V-funnel flow was 4-15 sec. In another study, Dey

et al. (2016) shows the value of slump flow of SCC was 735 mm-755 mm, also found

the T50 flow time was 1-2.1sec and V-funnel flow time was 6-11.5 sec with replacement

of natural brick aggregate with recycled aggregate. Khayat (2015) reported that an SCC

with a slump flow of 650 mm for the 20 mm size natural CA with 555 kg/m3 of

cementitious materials can be more suitable for casting highly congested structures.

Nischay et al. (2015) also reported that when natural aggregate replaced by the recycled

aggregate, slump flows were 690 mm and 580 mm for 25% and 100% replacement

25

respectively. Safiuddin et al. (2014) revealed that the slump flow high strength SCC

made with crushed granite varied from 605 mm to 720 mm, T50 slump flow time varied

in the range of 2-4.8 sec and V-funnel ranges from 6-13.5 sec. To ensure adequate self-

consolidation capacity, a minimum slump flow of 600 mm is generally recommended

for SCC (Khayat, 2000). Madandoust and Mousavi (2012) measured the T50 flow times

for self-compacting concrete containing a maximum nominal size 12.5 mm limestone

gravel as coarse aggregate within the range of 1.3-7.97 sec. Mohamad et al. (2015)

reported the T50 flow time for SCC with natural aggregate in the range of 1-6 sec.

Safiuddin et al. (2011a) reported that the T50 slump flow time varied in the range of 2.6-

4.5 sec for SCC with recycled aggregate. Felekoglu et al. (2007) reported the slump

flow values with 690 mm and 695 mm but their behavior in fresh state was totally

different having V-funnel times of 3 and 46 sec, respectively with the 15 mm maximum

size coarse aggregate (crushed limestone).

2.8.2 Passing Ability

The passing ability refers to the ease with which concrete can pass among various

obstacles and narrow spacing in the formwork without blockage. J-ring, L-box and

U-box tests are used to measure the filling ability of fresh SCC. Felekoglu et al. (2007)

reported filling abilities with L-box ratio of 0.95 and 0.50. Safiuddin et al. (2011b)

reported the J-ring flow values were in the range of 590–700 mm and the differences

between slump flow and J-ring flow were below 50 mm. Dey et al. (2016) found the

L-box ratio was 0.9-1.00 with recycled brick aggregate. Roy et al. (2019) reported the

values of L-box ratio for SCC with brick aggregate was 0.67-0.98.

2.8.3 Segregation Resistance

Segregation resistance of concrete describes the ability of a material to maintain the

homogeneous distribution of its various constituents during its flow and setting.

V-funnel at T5minutes, GTM screen stability test and column segregation tests are

performed to justify the segregation resistance of SCC. SantamarΓ­a et al. (2020) use the

column segregation test to evaluate segregation in the self-compacting concrete

mixtures and satisfactory results. Also the researchers Roy et al. (2019), Dey et al.

(2016), Khayat (2015), Nischay et al. (2015) and Mohamad et al. (2015) reported that

no visible blocking or segregation in their study.

2.8.4 Correlations between Fresh Properties of SCC

The correlation between the fresh properties of SCC made with various materials were

studied by the researchers (Safiuddin et al. 2011b, Madandoust and Mousavi, 2012).

Recycled coarse aggregate (RCA) was used as partial and full replacements of natural

26

coarse aggregate (NCA) by Safiuddin et al. (2011a) to produce self-consolidating

concrete. SCC mixes were produced substituting 0%, 30%, 50%, 70%, and 100% NCA

with RCA by weigh. Authors have found a strong correlation between the fresh

properties. This study reveals that J-ring flow and slump flow of the SCC mixes are

strongly correlated with a linear relationship. T50 slump flow time and V- funnel flow

time varied with a similar way. Also the segregation index and slump flow of the SCC

mixes were strongly correlated with a linear relationship. The correlation between these

properties are presented in the Table 2.5.

Table 2.5: Correlation between Fresh Properties of SCC (Safiuddin et al., 2011a)

Property Equation and Correlation

J-ring flow (JF) and slump flow (SF) JF = 1.1307 (SF) – 120.26, r = 0.9909

T50 slump flow time (T50) and V- funnel

flow time (Tv)

Tv = 6.6729 (T50) – 12.021, r = 0.9765

Segregation index (SI) and slump flow

(SF)

SI = 0.0288 (SF) – 7.7376, r = 0.9682

Madandoust and Mousavi (2012) found a relationship between T50 and V-funnel time

in their study of fresh and mechanical properties of SCC with metakaolin. The result

of the correlation between V-funnel time (VF) and T50 time (T50)is shown in Equation

(2.1).

VF = 2.691Γ—(T50)1.1575 (2.1)

R2 = 0.925

In another study, Safiuddin et al. (2011b) developed the correlation between the fresh

properties of SCC with Palm oil fuel ash. Correlation between J-ring flow and slump

flow, inverted slump cone flow spread and slump flow, inverted slump cone flow time

and 50-cm slump flow time, V-funnel flow time and 50-cm slump flow time,

segregation index and slump flow and segregation factor and segregation index were

described in their study. These correlations are listed in Table 2.6.

27

Table 2.6: Correlation between the fresh properties of SCC with palm oil fuel ash

(Safiuddin et al., 2011b)

Property Equation and Correlation

J-ring flow (JF) and slump flow (SF) JF = 0.9543 (SF)

RΒ² = 0.9634

Inverted slump cone flow spread and

slump flow

ISCFS = 0.9198 (SF) + 20.974

RΒ² = 0.9743

Inverted slump cone flow time and 50-

cm slump flow time

TISCF = 1.2074 (T50) + 0.5413

RΒ² = 0.9339

V-funnel flow time and 50-cm slump

flow time

TV = 2.7614 (T50) - 0.6247

RΒ² = 0.9265

Segregation index and slump flow SI = 0.0918 (SF) - 48.223

RΒ² = 0.8833

2.9 MECHANICAL PROPERTIES

The performance of concrete is significantly influenced by the quality of concrete. Self-

compacting concrete and traditional concrete of similar compressive strength have

comparable properties and if there are differences, these are usually covered by the safe

assumptions on which the design codes are based. However, SCC composition does

differ from that of traditional concrete; so information on any small differences may be

observed (EN1992-1).

In the design of concrete structures, engineers may refer to a number of concrete

properties, which are not always part of the concrete specification. The most relevant

properties are:

Compressive strength

Tensile strength

Modulus of elasticity

Creep

Shrinkage

Coefficient of thermal expansion

Bond to reinforcement

Shear force capacity in cold joints

Fire resistance

High-quality concrete will ensure that the structural performance of the concrete will

not be affected by the loss or durability due to deterioration and poor construction

28

practices. SCC has an abundant resource for future research on durability and structural

performance. Hardened concrete properties of SCC may be engineered through the

mixture proportion to be similar to, or better than, those of a conventional concrete

mixture. For the same raw material sources and the same specified compressive

strength, the engineering properties of SCC should be similar to those of conventional

concrete. To verify this, the same test methods and procedures employed for

conventional concrete should be used for SCC.

2.9.1 Compressive Strength

Compressive strength is the most valuable property of concrete. Although in many

practical cases other characteristics, such as durability, impermeability and volume

stability, may in fact be more important (Neville, 1997). According to Uysal (2012),

the highest compressive strength values were measured in SCC mixture prepared with

the basalt aggregate while the lowest compressive strength values were noted in SCC

mixture prepared with limestone aggregate at 28 days. The lowest value of static elastic

modulus has been obtained for SCC mixture containing limestone aggregate.

In a study of the effect of recycled brick aggregate on self-compacting concrete (Dey

et al., 2016), authors shows the 28 days compressive strength, tensile strength, and

failure pattern of hardened concrete. The compressive strength of 35 MPa was obtained

when 75% of virgin brick aggregate was replaced by recycled brick aggregate. Tensile

strength and modulus of elasticity result indicated almost similar properties. The results

showed that it is feasible to produce SCC with recycled coarse aggregate.

Another study (Roy et al., 2019) observed that both compressive and tensile strengths

(28 days) increased with the decrease of w/c ratio, and the compressive strength was

about 20-40 MPa and was around ten times of the tensile strength. This study was

conducted with brick aggregate with a fixed mixed proportion varying the w/c ratios

only.

2.9.2 Splitting Tensile Strength

Splitting tensile strength (fsp) is generally expressed as a function of the square root of

compressive strength (fΚΉc) and it is greater than direct tensile strength and lower than

flexural Strength. Splitting tensile strength is used in the design of structural concrete

members to evaluate the shear resistance provided by concrete and to determine the

development length of reinforcement.

Roy et al. (2019) reported the compressive strength of SCC with brick aggregate around

ten times of the splitting tensile strength. The correlation between compressive strength

29

and splitting tensile strength of SCC made was illustrated by Madandoust and Mousavi

(2012). The authors established a strong correlation between these hardened properties.

That study represents that splitting tensile strength development followed the same

pattern as compressive strength in SCC. The correlation of these properties are shown

in Equation (2.2).

fsp = 1.7593Γ—(fΚΉc/10)0.392 (2.2)

where, fsp = Splitting Tensile Strength

fΚΉc = Compressive Strength

2.9.3 Modulus of Elasticity

Generally, the modulus of elasticity is expressed as a function of the square root of

compressive strength. Modulus of elasticity of concrete is related to compressive

strength, aggregate type and content, and unit weight of the concrete. Some

observations have shown that for equal compressive strength, the elastic modulus of

SCC can be as much as 10 to 15% lower than that of conventional concrete of similar

compressive strength due to the required adjustments of mixture proportions to make

SCC (Bennenk, 2002). Other studies have shown the opposite that at an equal

compressive strength, the elastic modulus of SCC coincides well with that of

conventional concrete (Persson, 1999).

The compressive and flexural strengths and modulus of elasticity were measured by

Khaleel et al. (2011). The research reveals that a lower maximum size of coarse

aggregate leads to higher strengths compared to a higher maximum size of coarse

aggregate in SCC mixes. It was noticed that the compressive and flexural strength and

modulus of elasticity of the mixes made with the 10 mm maximum size of coarse

aggregate is higher than the values of the mixes made with the 20 mm maximum size

of coarse aggregate. This is due to the smaller maximum size of coarse aggregate that

has the larger surface area that results in a higher bonding strength in the transition zone

around aggregate particles when concrete is under loading.

Elastic modulus of common aggregate is greater than that of the absolute volume of the

paste of SCC is greater than that of ordinary concrete, one might expect that the elastic

modulus of SCC would be smaller than that of ordinary concrete with a comparable

compressive strength (Bonen and Shah, 2005).

30

2.10 SUMMARY

Definition of SCC, advantages and disadvantages of SCC, historical development of its

wide range application all over the world, classification based on requirements and

properties, mechanism of achieving self-compactibility, materials, mix proportion and

the attempts to improve the quality of SCC are illustrated in this chapter. In addition,

this chapter describes fresh as well as mechanical properties of SCC with various types

of aggregate from the literatures. Based on the discussion on the SCC from the

literature, it was found that SCC can be a best alternate to the engineers and construction

sectors in context of Bangladesh. It can be produce the SCC with lower labor cost and

without the necessities of skilled labors and equipment. To avoid the complexities of

vibration and placement of concrete in the congested areas of structures, SCC can be

used to produce quality concrete. In past, investigation of the SCC was conducted using

various types of CA but a very few attempts were taken to study the SCC using crushed

brick as coarse aggregate. In this study, brick aggregate was used as the substitute of

natural aggregate to introduce SCC with brick aggregate as a new construction material

and grab the benefit of this new building material. It is expected that, SCC with BA,

reduce non-uniformity of concrete and play an important role in the construction

sectors. That’s why this study intended to investigate the fresh and mechanical

properties of self-compacting concrete with brick aggregate.

31

CHAPTER 3 CHAPTER III …… …..

. MATERIALS AND METHODOLOGY

3.1 INTRODUCTION

This chapter includes different types of experimental data required to determine the

properties of the ingredients of concrete, processes of manufacturing of concrete and

tests to determine the properties of fresh and hardened properties of SCC with brick

aggregate. To launch this experimental work, concrete was prepared with locally

available 19 mm and 12.5 mm downgraded coarse aggregate made from locally

available crushed bricks, available coarse sand, Portland composite cement and high

range water reducer (HRWR). Under the experimental investigation, the physical

properties of materials were evaluated. This research program includes the following

methodology step by steps:

Selection and collection of the materials

Preparation of the materials

Testing the physical and chemical properties of materials

Mix design and proportioning the materials for trial mixes

Preparation of trial mixes

Testing the fresh properties of SCC

Slump flow

T50 slump flow time

V-funnel flow time

V-funnel flow at T5minutes

J-ring flow

J-ring blocking index

Height difference at J-Ring

L-box blocking ratio.

Preparation of the cylindrical specimen (Ø 100 mm Γ— 200 mm)

Testing the mechanical properties of hardened SCC

Compressive Strength (fΚΉc)

Splitting Tensile Strength (fsp)

Modulus of Elasticity (Ec).

Analysis of test results and conclusion

In this research program all the testing methods were followed according to standard

specification and guidelines.

32

3.2 MATERIALS

In this research, locally available first class well burnt brick were used to prepare the

coarse aggregate. Locally available coarse sand as fine aggregate, Portland cement as

binding material, potable water and high range water reducer (HRWR) were used as

concrete making materials. All of these materials were collected from locally available

sources and their properties were investigated in the laboratory to set the parametric

criteria for SCC. The materials used in this study are listed in Table 3.1.

Table 3.1: Ingredients of SCC with BA

Coarse Aggregate 19 mm downgraded

12.5 mm downgraded

Fine Aggregate Locally available coarse sand (Sylhet sand)

Binder Portland Composite Cement

(BS EN 197-1:2011/CEM II/B-M)

Water Potable water

Admixture Superplasticizer (SP), ASTM C494 Type: F and G

3.3 TESTING OF THE MATERIALS

3.3.1 Tests for Coarse Aggregate

Although aggregates are most commonly known to be inert filler in concrete, the

different properties of aggregate have a large impact on the strength, durability,

workability, and economy of concrete. The aggregate most of which retains on the 4.75

mm sieve and contains only that much of fine material as is permitted by the

specifications are termed coarse aggregate (Gambhir, 2006). In general, the aggregates

having a size larger than 4.75 mm is coarse aggregate. The graded coarse aggregate is

described by its nominal maximum size or downgraded size, i,e., 37.5 mm, 25 mm, 19

mm and 12.5 mm. For example, nominal maximum size aggregate 12.5 mm means an

aggregate most of which passes through 12.5 mm sieve. In this study locally available

brick chips of sizes 19 mm and 12.5 mm downgraded have been used as coarse

aggregate. The coarse aggregates used in this study are prepared by crushing first

class burnt clay bricks. The photograph of the coarse aggregate (CA) is

illustrated in Fig. 3.1.

33

Fig. 3.1: Crushed bricks as coarse aggregate

Burnt clay bricks were collected from locally available sources and were crushed

manually and then sieved for grading. If all the particles of an aggregate are of uniform

size, the compacted mass will contain more voids, whereas an aggregate comprising

particles of various sizes will give a mass containing lesser voids. The particle size

distribution of a mass of aggregate should be such that the smaller particles fill the voids

between the larger particles. The proper grading of an aggregate produces dense

concrete. It is, therefore, essential that the coarse and fine aggregate be well-graded to

produce quality concrete. The sieve analysis is conducted to determine the particle size

distribution and fineness modulus of coarse aggregate called gradation. The fineness

modulus (FM) is a numerical index of fineness, giving some idea of the mean size of

the particle present in the entire body of the aggregate. The standard test method ASTM

C136 (2019) was followed for grading of coarse aggregate. The sieve analysis was

performed through standard sieve sizes of 37.5, 19.0, 9.5, 4.75, 2.36, 1.18, 0.60, 0.30,

and 0.15 mm by a mechanical sieve shaker for 15 minutes. The calculation related to

fineness modulus of fine aggregate has been included in the Appendix B and the value

of FM of coarse aggregate are listed in Table 4. 1 and the gradation curve of coarse

aggregates are shown in Fig. 4.1 of Chapter IV.

The absorption capacity of coarse aggregate was determined according to standard test

method ASTM C127 (2015). The value of the absorption capacity of the coarse

aggregates has been listed in the Table 4.1 in Chapter IV. The calculation related to this

test has been included in the Appendix. The calculation of absorption capacity is shown

in Equation (3.1).

12.5 mm downgraded CA 19 mm downgraded CA

34

Percentage of absorption = (B-A)/A*100 (3.1)

Where,

A = weight of oven-dry test sample in air

B = weight of saturated surface dry test sample in air

The unit weight of coarse aggregates is necessary to use for many methods of

selecting proportions for the concrete mixture. They may also be used for

determining the mass/volume relationship of aggregates. This test method

conforms to the standard specification of ASTM C 29 (2017). The unit weight

of various sizes of coarse aggregates has been given in the Table 4.1

in Chapter IV. The calculation has been given in the Appendix. The calculation of

unit weight shown in Equation (3.2).

M = (G-T)/V (3.2)

where

M = Dry rodded bulk density

T = Mass of the measure

G = Mass of the aggregate plus measure

V = Volume of the measure

Aggregates generally contain pores, both permeable and impermeable, for which

specific gravity has to be carefully defined. With this specific gravity of each

constituent known, its weight can be converted into solid volume and this is also

required in calculating the compacting factor in connection with the workability

measurements. This test method conforms to the standard specification of ASTM

C 127 (2015). The value of the specific gravity of the coarse aggregate has been

listed in the Table 4.1 in Chapter IV. The calculation related to this test has been

included in the Appendix. The calculation of the bulk specific gravity shown in

Equation (3.3).

Bulk specific gravity (SSD basis) = B/(B-C) (3.3)

Where,

B = weight of saturated surface dry test sample in air

C = weight of saturated test sample in water.

35

The flakiness index of an aggregate sample is found by separating the flaky

particles and expressing their mass as a percent of the mass of the sample. This

test is applicable to the materials passing a 63 mm sieve and retained on a 6.3

mm sieve. Aggregates are classified as flaky when they have a thickness of less

than 60% of their mean size.

Elongation index of an aggregate sample is found by separating the elongated

particles and expressing their mass as a percent of the mass of the sample. This

test is applicable to the materials passing a 50 mm sieve and retained on a 6.3

mm sieve. Aggregates are classified as elongated when they have a length

(greatest dimension) of more than 1.8 of their mean sieve size. These test

methods conformed to the standard (ASTM D 4791, 2010).

All the properties (FM, unit weight, specific gravity, water absorption,

elongation and flakiness index) of 19 mm and 12.5 mm downgraded coarse

aggregates used in the laboratory experiment are shown in Table 4.1 (Chapter

IV).

3.3.2 Tests for Fine Aggregate

Locally available fine aggregate (coarse sand) was used in this study. The photograph

of the fine aggregate is illustrated in Fig. 3.2. The standard test method ASTM C136

(2019) was followed for sieve analysis of fine aggregate. Standard sieve sizes of #4, #8,

#16, #30, #50, and #100 were used to analyze the fineness modulus (FM) of sand.

Absorption capacity and specific gravity of fine aggregate were determined according

to the standard test method as prescribed by ASTM C128 (2015). Unit weight values

of fine aggregates are necessary for selecting proportions for the concrete mixture. They

may also be used for determining the mass/ volume relationship of aggregate. This test

method conforms to the standard specification of ASTM C 29 (2017). The calculation

related to these properties (FM, unit weight, specific gravity and water absorption) has

been included in the Appendix.

All the properties (FM, unit weight, specific gravity and water absorption) of fine

aggregate used in the laboratory experiment are shown in Table 4.1 and the gradation

curve of fine aggregate is shown in Fig. 4.2 in Chapter IV.

36

Fig. 3.2: Fine aggregate (Coarse Sand)

3.3.3 Test for Binding Materials

In this study Portland Composite Cement (BS EN 197-1:2011/CEM II/B-M) was used

as binding materials. Usually, the grain size of the cement particles is within 7 ~ 200

ΞΌm (0.007 ~ 0.2 mm) (Building Materials in Civil Engineering, 2011). Cement paste to

a standard condition of wetness, called 'normal consistency' to regulates the water

content. The normal consistency of a cement paste is defined as that consistency which

will permit a Vicat's plunger having 10 mm diameter and 50 mm length to penetrate to

a depth of 10 mm from the top of the mold. Initial setting time is regarded as the time

elapsed between the moments that the water is added to the cement, to the time that the

paste starts losing its plasticity. The final setting time is the time elapsed between the

moment that the water is added to the cement and the time when the paste has

completely lost his plasticity and has attained sufficient firmness to resist certain

definite pressure. The setting time of cement indicates how long the cement will remain

workable when used in a concrete mix. Normal consistency and setting times were

determined by using the Vicat apparatus and test methods conform to the standard

requirements of ASTM specifications C187 (ASTM C187, 2016) and C191 (ASTM

C191, 2019) respectively. The strength of cement is usually determined from the test

on mortar made with cement. The compressive of the cement mortar was measured and

test methods conform to the ASTM standard requirements of specification C109

(ASTM C109, 2020). The properties of cement used for this experiment ensured

satisfactory properties according to ASTM C150 (2020) as a binding material for

concrete. The composition of cement and the test results of the cement used in this study

have been listed in the Table 4.2 and Table 4.3 of Chapter IV respectively.

37

3.3.4 Water

Water is an important ingredient of concrete as it actively participates in the chemical

reaction with cement. Since it helps to form the strength-giving cement gel (C-S-H),

the quantity and quality of water are required to be looked into very carefully. Water

used in mixing concrete shall be clean and free from injurious amounts of oils, alkalis,

salts, organic materials or other substances that may be deleterious to concrete. In this

study potable water from the tap was used in the mixture of concrete.

3.3.5 Superplasticizer

In SCC two types of chemical admixtures are used to increase the workability of fresh

concrete with lower water-cement ratio. These are known as superplasticisers or as high

range water-reducer (HRWR) and viscosity modifying agents (VMA) or as anti-

washout admixtures. Superplasticizer (SP) controls the flow properties of SCC, allows

the reduction of the water-cement ratio maintaining workability to reach the desired

strength and durability. SP enhances the flowability of SCC by its liquefying and

dispersing actions (Hu and Larrard, 1996; Yen et al., 1999). Superplasticiser

deflocculates the cement particles and frees the trapped water by its dispersing action

and hence enhances the flowability of SCC as illustrated in Fig. 3.3. However, a high

amount of SP could cause segregation and bleeding.

Fig. 3.3: Method of deflocculation and water liberation with use of Superplasticiser

(Deeb and Karihaloo, 2013)

In this research locally available superplasticizer Con-Lub SP was used in the

preparation of SCC with brick aggregate. It is a ready-to-use liquid superplasticizer that

extremely improves the high range water reducing performance and complies with the

requirements of the following standards: ASTM C 494 (2019), Type F & G. Con-Lub

SP Polycarboxylate Superplasticizer for high water reduction has been primarily

developed for applications in the ready-mixed and precast concrete industries where the

38

highest durability and performance are required. Technical Specification of this

superplasticizer has complied with the requirements of the following standards (ASTM

C494, 2019). Some technical information of Con-Lub SP is included in Table 4.4 of

Chapter IV. The physical appearance of Con-Lub SP is yellowish. The photograph of

SP used in this study is illustrated in Fig. 3.4.

The optimum dosages of Con-Lub SP to meet specific requirements should

always be determined by trials using the materials and conditions that will be

experienced in use.

Fig. 3.4: Superplasticizer Con-Lub SP

3.4 MIX DESIGN OF SCC

To ensure a good balance between the fresh properties of SCC such as deformability

and segregation resistance, the proportion of the constituent materials must be carefully

designed. Mix design is an essential first step for both research programs and the

practical application of concrete. There are different mix proportioning methods used

to develop SCC mixes. Each method has been developed according to its particular

conditions and environment and has its special features and some inherent limitations.

These methods can be categorized into different classes (Shi et al., 2015) such as the

empirical mix design method, compressive strength method, aggregate packing

method, the method based on the statistical factorial model, trial and error method and

39

rheology of paste model. In this study, the trial and error method of mix proportion was

adopted for proportioning SCC.

3.4.1 Trial and Error Method of Mix Proportioning

Based on the relationship between the w/c ratio and compressive strength, the design

of the mix can be made by selecting the water-cement ratio to suit the requirement of

workability, strength and durability. With this water-cement ratio, trial batches are

prepared with different aggregates and cement ratios. From this, it is possible to

determine the optimum proportion and amount of the aggregate that will produce a

workable mix with a minimum of the paste content for determining the fine aggregate.

With judgment and experience, one may arrive at the proportions of fine and coarse

aggregate.

Having a fixed water-cement ratio, aggregate cement ratio and the amount of fine

aggregate in the total aggregate content, the freshly mixed concrete needs to test the

fresh properties to satisfy the criteria of standard SCC mix. Then cylindrical specimens

of concrete can be prepared from each successful mix in the laboratory following the

standard procedure. After the required period of curing the specimens can be tested for

its compressive strength. The mix can be slightly adjusted, if necessary, by changing

the w/c ratio or the aggregate cement ratio to suit the actual requirement of the job. In

the trial and error method, due consideration has to be given for the moisture content

of the aggregates.

3.4.2 Detailed on Mix Design

In this research, concrete making materials were proportioned based on the trial mixes.

The component materials of SCC trial mixes were proportioned according to the

guideline of EFNARC (2002) with slight modification in the laboratory. Through the

laboratory trial and testing the fresh properties of SCC with brick aggregate, the content

of ingredients and dosages of SP were fixed. Some initiatives were failed due to

segregation of concrete, blockage and less passing and filling ability. The time of

mixing of the concrete in the mixer machine and the application of the SP dosages into

the fresh concrete has some influence on the properties of SCC. In some cases, the

physical appearance of the fresh concrete may predict the segregation free flowable

concrete. After applying the laboratory trial and based on the knowledge from literature,

mix proportion of SCC with brick aggregate were fixed for this research.

40

The initial guideline for the proportion of the ingredients according to EFNARC (2002)

are:

Coarse aggregate content (by volume of mix) = 28-35 %

Water powder ratio (by volume) = 0.8-1.1

Total powder content (kg/m3) = 400-600

Sand content (volume) > 40 % of the mortar

Sand < 50% of paste volume

Sand by weight of total aggregate > 50%

Free water (litter/m3) < 200

Paste (% of the volume of the mix) > 40

The following is a summary of steps for determining the performance requirements and

proportioning of SCC (EFNARC, 2005).

Step 1: Determine slump flow performance requirements

Step 2: Select coarse aggregate and proportion (ACI 211.1 and 301);

Step 3: Estimate the required cementitious content and water;

Step 4: Calculate paste and mortar volume;

Step 5: Select admixture;

Step 6: Batch trial mixture;

Step 7: Test. When assessing the workability attributes of SCC (stability, filling

ability, and passing ability), the slump flow test, as well as a test to evaluate

stability and passing ability (such as column segregation, J-ring, or L-box),

should be run; and

Step 8: Adjust mixture proportions based on the test results and then rebatch

with further testing until the required properties are achieved

In this study, materials were proportioned for trial mixes following the guideline of

EFNARC (2002, 2005). Initially the weight cement, water, coarse aggregate were

determined for the fresh concrete. Sand content was calculated considering the volume

of paste and mortar and weight of the fresh concrete about 2150 -2300 kg/m3 to prepare

trial mix for 1m3 fresh concrete.

41

Table 3.2: Proportion of the unsuccessful trial mixes

Coarse

Aggregate

(kg/m3)

Fine

Aggregate

(kg/m3)

Cement

(kg/m3)

Water

(kg/m3)

Water-

cement

ratio

SP

Dosages

(% of

Cement)

Comments

700 800 600 180 0.30 1.6 Unsuccessful

660 890 600 180 0.30 1.6 Unsuccessful

600 940 600 180 0.30 1.6 Unsuccessful

550 980 580 175 0.30 1.6 Unsuccessful

550 890 580 203 0.35 1.2 Unsuccessful

560 980 500 175 0.35 1.2 Unsuccessful

570 944 530 186 0.35 1.2 Unsuccessful

580 970 550 193 0.35 1.2 Unsuccessful

550 890 580 203 0.35 1.3 Unsuccessful

560 980 500 175 0.35 1.3 Unsuccessful

570 944 530 186 0.35 1.3 Unsuccessful

580 970 550 193 0.35 1.3 Unsuccessful

560 980 400 175 0.35 1.6 Unsuccessful

560 980 400 175 0.40 1.6 Unsuccessful

Table 3.2 presents the mix proportion of trial mixes that were performed in the

laboratory with changing the size of aggregates, fine aggregates and SP dosages. These

initiatives were failed due to segregation of concrete, blockage and less passing and

filling ability as shown in Fig. 3.5. Locally available fine aggregate was also

incorporated in this study for trial but due to having very small particle size, it was not

possible to use these materials. Smaller particles have a larger surface area and it

demands more water and SP dosages. Due to having the limitation of the use of SP

dosages this fine aggregate was discarded from this study.

Applying many laboratory trials and based on the knowledge from literature, four basic

successful trial mixes of SCC were fixed with various contents of aggregates. In this

research, 12.5 mm and 19 mm downgraded brick chips were used as coarse aggregate

with coarse sand as fine aggregate and Portland composite cement at fixed water binder

ratios at 0.35 and 0.40. Mixes were prepared using varying the content of

superplasticizer (SP) to satisfy the fresh properties of SCC. All the aggregates were

considered in saturated surface dry conditions. In some cases, a little modification of

the water content was applied due to the variation of aggregate moisture content on its

surface. A total of twenty-four successful mixes were prepared in the laboratory for

SCC with brick aggregate. The details of the identification of successful mix

42

proportions for a cubic meter SCC with BA are listed in Table 3.3 and with the SP

dosages of successful trial mixes are listed in Table 3.4. Volumetric calculation of the

ingredients of SCC with BA are shown in Table 3.5

Fig. 3.5: Some unsuccessful attempts of fresh SCC

For easy identification of the cylindrical specimen of each trial mix, some identity mark

was provided for successful concrete mix at this stage and the details of specimens

identification are given in Table 3.3

43

Table 3.3: Identification of specimens

Case

No. Notation Description

Case -1 C450A12W35

Mix category A, Cement Content = 450 kg/m3 , CA

Content = 560 kg/m3, Aggregate size = 12.5 mm

downgraded, w/c ratio = 0.35

Case -2 C470A12W35

Mix category A, Cement Content = 470 kg/m3 , CA

Content = 560 kg/m3, Aggregate size = 12.5 mm

downgraded, w/c ratio = 0.35

Case -3 C500A12W35

Mix category A, Cement Content = 500 kg/m3 , CA

Content = 560 kg/m3, Aggregate size = 12.5 mm

downgraded, w/c ratio = 0.35

Case -4 C530B12W35

Mix category B, Cement Content = 530 kg/m3 , CA

Content = 570 kg/m3, Aggregate size = 12.5 mm

downgraded, w/c ratio = 0.35

Case -5 C550C12W35

Mix category C, Cement Content = 550 kg/m3 , CA

Content = 580 kg/m3, Aggregate size = 12.5 mm

downgraded, w/c ratio = 0.35

Case -6 C580D12W35

Mix category D, Cement Content = 580 kg/m3 , CA

Content = 550 kg/m3, Aggregate size = 12.5 mm

downgraded, w/c ratio = 0.35

Case -7 C450A19W35

Mix category A, Cement Content = 450 kg/m3 , CA

Content = 560 kg/m3, Aggregate size = 19 mm

downgraded, w/c ratio = 0.35

Case -8 C470A19W35

Mix category A, Cement Content = 470 kg/m3 , CA

Content = 560 kg/m3, Aggregate size = 19 mm

downgraded, w/c ratio = 0.35

Case -9 C500A19W35

Mix category A, Cement Content = 500 kg/m3 , CA

Content = 560 kg/m3, Aggregate size = 19 mm

downgraded, w/c ratio = 0.35

Case -10 C530B19W35

Mix category B, Cement Content = 530 kg/m3 , CA

Content = 570 kg/m3, Aggregate size = 19 mm

downgraded, w/c ratio = 0.35

Case -11 C550C19W35

Mix category C, Cement Content = 550 kg/m3 , CA

Content = 580 kg/m3, Aggregate size = 19 mm

downgraded, w/c ratio = 0.35

44

Case -12 C580D19W35

Mix category D, Cement Content = 580 kg/m3 , CA

Content = 550 kg/m3, Aggregate size = 19 mm

downgraded, w/c ratio = 0.35

Case -13 C450A12W40

Mix category A, Cement Content = 450 kg/m3 , CA

Content = 560 kg/m3, Aggregate size = 12.5 mm

downgraded, w/c ratio = 0.40

Case -14 C470A12W40

Mix category A, Cement Content = 470 kg/m3 , CA

Content = 560 kg/m3, Aggregate size = 12.5 mm

downgraded, w/c ratio = 0.40

Case -15 C500A12W40

Mix category A, Cement Content = 500 kg/m3 , CA

Content = 560 kg/m3, Aggregate size = 12.5 mm

downgraded, w/c ratio = 0.40

Case -16 C530B12W40

Mix category B, Cement Content = 530 kg/m3 , CA

Content = 570 kg/m3, Aggregate size = 12.5 mm

downgraded, w/c ratio = 0.40

Case -17 C550C12W40

Mix category C, Cement Content = 550 kg/m3 , CA

Content = 580 kg/m3, Aggregate size = 12.5 mm

downgraded, w/c ratio = 0.40

Case -18 C580D12W40

Mix category D, Cement Content = 580 kg/m3 , CA

Content = 550 kg/m3, Aggregate size = 12.5 mm

downgraded, w/c ratio = 0.40

Case -19 C450A19W40

Mix category A, Cement Content = 450 kg/m3 , CA

Content = 560 kg/m3, Aggregate size = 19 mm

downgraded, w/c ratio = 0.40

Case -20 C470A19W40

Mix category A, Cement Content = 470 kg/m3 , CA

Content = 560 kg/m3, Aggregate size = 19 mm

downgraded, w/c ratio = 0.40

Case -21 C500A19W40

Mix category A, Cement Content = 500 kg/m3 , CA

Content = 560 kg/m3, Aggregate size = 19 mm

downgraded, w/c ratio = 0.40

Case -22 C530B19W40

Mix category B, Cement Content = 530 kg/m3 , CA

Content = 570 kg/m3, Aggregate size = 19 mm

downgraded, w/c ratio = 0.40

Case -23 C550C19W40

Mix category C, Cement Content = 550 kg/m3 , CA

Content = 580 kg/m3, Aggregate size = 19 mm

downgraded, w/c ratio = 0.40

45

A specimen with the abovementioned designation is identified as follows:

C450 A 12 W35

Case -24 C580D19W40

Mix category D, Cement Content = 580 kg/m3 , CA

Content = 550 kg/m3, Aggregate size = 19 mm

downgraded, w/c ratio = 0.40

A = Coarse aggregate content 560 kg/m3

B = Coarse aggregate content 570 kg/m3

C = Coarse aggregate content 580 kg/m3

D = Coarse aggregate content 550 kg/m3

W12 = 12.5 mm downgraded coarse aggregate

W19 = 19 mm downgraded coarse aggregate

35 = w/c ratio is 0.35

40 = w/c ratio is 0.40

C450 = Cement content 450 kg/m3

C470 = Cement content 470 kg/m3

C500 = Cement content 500 kg/m3

C530 = Cement content 530 kg/m3

C550 = Cement content 550 kg/m3

C580 = Cement content 580 kg/m3

46

Table 3.4: Proportion of the successful SCC mixes with BA

Specimen ID

Coarse

Aggregate

Type

w/b

ratio

Cement

(kg)

Coarse

Aggregate

(kg)

Fine

Aggregate

(kg)

Water

(kg)

HRWR

%

C450A12W35 12.5 mm

0.35

450 560 980 157.5 1.5

C470A12W35 12.5 mm 470 560 980 164.5 1.4

C500A12W35 12.5 mm 500 560 980 175 1.6

C530B12W35 12.5mm 530 570 944 186 1.4

C550C12W35 12.5mm 550 580 970 193 1.4

C580D12W35 12.5mm 580 550 890 203 1.6

C450A19W35 19 mm 450 560 980 157.5 1.4

C470A19W35 19 mm 470 560 980 164.5 1.4

C500A19W35 19mm 500 560 980 175 1.6

C530B19W35 19 mm 530 570 944 186 1.5

C550C19W35 19 mm 550 580 970 193 1.4

C580D19W35 19 mm 580 550 890 203 1.6

C450A12W40 12.5 mm

0.4

450 560 980 180 1.4

C470A12W40 12.5 mm 470 560 980 188 1.4

C500A12W40 12.5 mm 500 560 980 200 1.4

C530B12W40 12.5mm 530 570 944 212 1.4

C550C12W40 12.5mm 550 580 970 220 1.4

C580D12W40 12.5 mm 580 550 890 232 1.4

C450A19W40 19 mm 450 560 980 180 1.4

C470A19W40 19 mm 470 560 980 188 1.4

C500A19W40 19mm 500 560 980 200 1.4

C530B19W40 19 mm 530 570 944 212 1.4

C550C19W40 19 mm 550 580 970 220 1.4

C580D19W40 19 mm 580 550 890 232 1.4

Table 3.5: Volumetric calculation of the ingredients of SCC with BA

Specimen

Category

Volume (m3/m3) Percentage of Ingredients

Volume of

FA in

Mortar

CA Cement FA Water Paste Mortar wf /wc %

A 0.27 0.16 0.37 0.18 0.34 0.72 0.64 0.52

B 0.27 0.17 0.35 0.19 0.36 0.72 0.62 0.50

C 0.28 0.17 0.36 0.19 0.36 0.72 0.62 0.50

D 0.26 0.18 0.35 0.20 0.38 0.74 0.63 0.48

47

Cost of the materials for concrete is also an important factor in the proportioning of

materials for concrete. Table 3.6 presents the cost of the materials for a cubic meter

SCC mixes with BA.

Table 3.6: Cost of the materials for a cubic meter SCC mixes with BA

Materials

Unit

Unit

price

Volume of the materials

for the mix category (m3)

Cost of the materials for a

cubic meter SCC mix (taka)

A B C D A B C D

BA m3 3200 0.27 0.27 0.28 0.26 864 864 896 832

Cement m3 12000 0.16 0.17 0.17 0.18 1920 2040 2040 2160

Sand m3 1600 0.37 0.35 0.36 0.35 592 560 576 560

SP litter 160 8 7.42 7.7 9.28 1280 1187 1232 1485

Total Cost: 4656 4651 4744 5037

3.5 PREPARATION OF CONCRETE SPECIMEN

To conduct a feasibility study of the production of SCC with brick aggregate, trial mixes

were used for casting concrete with crushed brick as coarse aggregate, fine aggregate,

cement, water and high range water reducer. All concrete mixtures were prepared

following various stages of the casting of the test specimens are explained in the

following sections.

3.5.1 Batching of the Materials

Proper and accurate measurement of all the materials were used in the production of

concrete. It is essential to ensure uniformity of proportions and aggregate grading in

successive batches. In this study, gravimetric batching was used for measuring the

materials.

3.5.2 Mixing of the Concrete

The objective of mixing is to coat the surface of all aggregate particles with cement

paste and to blend all the ingredients of the concrete into a uniform mass. In this study,

concrete mixing was done by tilting type mixer machine. The speed of the mixer

machine was about 15 to 20 revolutions per minute. Only the aggregates were mixed

for half minutes in the mixer machine. Then water was added and mixed for five

minutes with 75% of the mixing water, then cementitious materials were added and

mixed for an additional minute. Finally, the remaining water and HRWRA were added

to the mixture and mixed for another 15 minutes. When the HRWR was mixed with the

48

concrete, huge bubbles were formed to deflocculate the cement particle to impart the

fluidity of fresh concrete. Mixing was continued up to diminishing of the bubble from

the surface of the concrete. The total mixing time was about 22-25 minutes. The similar

mixing sequence was followed by Lotfy (2006) and is illustrated in Figure 3.6.

Fig. 3.6: Standard mixing sequence (Lotfy, 2006)

3.5.3 Testing of Fresh Properties of SCC

To ensure the fresh properties of SCC, the flowability, passing ability, filling ability

and segregation resistance of fresh concrete were confirmed just after mixing by slump

flow method, T50 time, V-funnel, V-funnel at T5 minutes, L-box and J-ring tests. Unit

weight tests of fresh concrete also were conducted in the laboratory.

3.5.4 Placing of Fresh Concrete

The methods used in placing concrete in its final position have an important effect on

its homogeneity, density and behavior in service. In this study, concrete was poured

into the cylindrical mold of size Ø100 mm Γ— 200 mm to perform the mechanical

properties (compressive strength, tensile strength and modulus of elasticity) of

hardened concrete.

3.5.5 Removal of Mold

The hardened cylindrical concrete specimens were brought out removing the mold after

48 hours of their casting. Then leveling of the specimens on their surface by permanent

marker pen were done so that they can be separated without any confusion. Much care

was taken while removing the mold so that the specimens do not affect adversely.

3.5.6 Curing of Concrete

The physical properties of concrete depend largely on the extent of hydration of cement

and the resultant microstructure of the hydrated cement. Hydration of cement is

activated in the presence of water. For this reason, the curing of concrete is obviously

required. In this study, the submerged water curing method was used for the curing of

49

concrete. Test specimens were immersed under normal water in the curing tank for 28

days.

3.5.7 Testing of Hardened Concrete

The cylindrical concrete specimens were tested to calculate the compressive strength,

splitting tensile strength and modulus of elasticity. The interpretation of these test

results gives the output of this research.

3.6 FRESH PROPERTIES OF SCC MIXTURES

To satisfy the criteria of SCC, flowability, passing ability, filling ability and segregation

resistance of fresh concrete were confirmed by slump flow method, T50 time, V-funnel,

V-funnel at T5 minutes, L-box and J-ring tests conducted as per EFNARC Guideline

(EFNARC, 2005). The fresh unit weight was tested according to ASTM C 138 (2001)

.

3.6.1 Slump-Flow and T50 Flow Test

The slump flow is used to assess the horizontal free flow of SCC in the absence of

obstructions. This test is performed similarly to the conventional slump test using the

Guideline of EFNARC (2005). The mean spread of the resulting concrete patty is

measured horizontally instead of measuring the slumping distance vertically. Slump-

flow test is used to determine flow ability of self-compacting concrete. The equipment

consists of one slump cone and one flow table shown in Fig. 3.7. A concentric diameter

of 500 mm is marked on the table. The slump cone is filled with concrete while pressing

the slump cone to the table. Next, the slump cone is lifted vertically and measurement

was taken as the diameter of concrete. Simultaneously, stopwatch was started to record

the time taken for the concrete to reach the 500 mm spread circle. This is the T50 time

in sec. Also the final spread diameter of the concrete was measured in two perpendicular

directions. The average of the two measured diameters is known as slump flow in mm.

It was taken in concern that, there was no mortar or cement paste without coarse

aggregate at the edge of the pool of concrete. Fig. 3.8 shows the slump flow

measurement of this research.

50

Fig. 3.7: Slump Flow equipment

Figure 3.2: Slump Flow test apparatus

Fig. 3.8: Slump flow test of SCC with brick aggregate

3.6.2 J-Ring Test

The J-Ring test itself has been developed at the University of Paisley, Scotland. The

test is used to determine the passing ability of the concrete. The equipment consists of

an open steel ring, drilled vertically with holes to accept threaded sections of

reinforcement bar. These sections of bar can be of different diameters and spaced at

different intervals. The diameter of the ring of vertical bars is 12 in (300 mm), and the

height of 4 in (100 mm) shown in Fig. 3.9. The J-Ring can be used in conjunction with

the slump flow test. After the test, the difference in height between the concrete inside

and that just outside the J-Ring is measured. This is an indication of passing ability, or

the degree to which the passage of concrete through the bars is restricted. The J-Ring

is placed centrally on the base-plate with the slump-cone. The cone is filled without

tamping and lifted vertically to allow the concrete to flow out freely. The final diameter

of the concrete in two perpendicular directions is measured. The average of the two

measured diameters is known as J-Ring flow in mm. The difference in height between

the concrete just inside the bars and that just outside the bars is also measured. The

51

average of the difference in height at four locations in mm is the measure of J-ring test.

This test method covers the standard Guideline of EFNARC (2002) for SCC. Fig. 3.10

shows the J-ring flow measurement of this research.

Fig. 3.9: J-Ring test apparatus

Fig. 3.10: J-Ring test of SCC with brick aggregate

52

3.6.3 V-funnel Flow and V-funnel Flow at T 5minutes Test

V-funnel test is used to determine the flowability of SCC. The equipment consists of a

V-shaped funnel as shown in Fig. 3.11 and Fig. 3.12. The V-funnel is filled to its upper

level with concrete. Within 10 seconds after filling, the trap door allowed the concrete

to flow out under gravity. Time was measured with stopwatch when the trap door is

opened, and time recorded up to the discharge to complete. This time is taken to the

time when light is seen from above through the funnel. This is known as the V-funnel

flow time in sce. The whole test has to be performed within 5 minutes.

Without cleaning the surface of the funnel, apparatus was refilled with new concrete

and left for 5 minutes to settle and then allow the concrete to flow out under gravity.

Time was measured with stopwatch when the trap door is opened, and time recorded

up to the discharge to complete. This time is taken to the time when light is seen from

above through the funnel. This is known as the V-funnel at T5minutes flow time in sce. If

the concrete shows segregation, then the flow time will increase significantly. V-funnel

at T5minutes flow time gives the measurement of segregation resistance. This test method

covers the standard Guideline of EFNARC (2002) for SCC.

Fig. 3.11:V-funnel test apparatus

53

Fig. 3.12: V-funnel and V-funnel at T5 minutes test

3.6.4 L-Box Test

The test assesses the flow of the concrete, and also the extent to which it is subject to

blocking by reinforcement. The details of the L-shaped box are shown in Fig. 3.13. The

apparatus consists of a rectangular-section box in the shape of an β€˜L’, with a vertical

and horizontal section, separated by a moveable gate, in front of which vertical lengths

of reinforcement bar are fitted. The gap between reinforcement bars is 1.5 in (35 mm),

but can be changed to other gap sizes. The vertical section is filled with concrete, then

the gate lifted to let the concrete flow into the horizontal section. When the flow has

stopped, the height of the concrete at the end of the horizontal section is expressed as a

proportion of that remaining in the vertical section (H2/H1). Acceptable values of the

so-called blocking ratio H2/H1 can be 0.80 – 1.00. It indicates the slope of the concrete

when at rest. This is an indication passing ability, or the degree to which the passage of

concrete through the bars is restricted. This test method covers the standard Guideline

of EFNARC (2002) for SCC. The testing procedure of L-box are illustrated in Fig. 3.14,

Fig. 3.15 and Fig. 3.16

54

Fig. 3.13: L-Box flow test apparatus (all units in mm)

Fig. 3.14: L-box filled with concrete

55

Fig. 3.15: Concrete passes through L-box

Fig. 3.16: Flow of concrete in L-box.

3.7 MECHANICAL PROPERTIES OF SCC

The cylindrical specimens of size Ø 100 mm Γ— 200 mm were prepared from each

successful mix of SCC with brick aggregate to test the compressive strength, tensile

strength and modulus of elasticity of hardened concrete. After demolding, cylindrical

specimens were subjected to curing for 28 days. After the specified curing period was

over, the concrete cylinders were subjected to these tests according to standard

procedure.

56

3.7.1 Compressive Strength

Concrete cylindrical specimens of size 100 mm diameter and 200 mm height were

casted using trial mixes for SCC with brick aggregate. Compressive strength test was

performed by Universal Testing Machine (UTM) following the ASTM C39 (2002)

specifications. The compression load was applied and increased gradually until the

specimens failed and the maximum or ultimate load carried by the specimen was

recorded. The compressive strength was calculated based on the ultimate load and the

cross-sectional area of the cylinder, and averaged from the results of three specimens.

3.7.2 Splitting Tensile Strength

Splitting tensile test was carried out as per ASTM C496 (2004). After the specified

curing period concrete cylinders of size 100 mm diameter and 200 mm height were

subjected to splitting tensile test using universal testing machine. Tests were carried out

on triplicate specimens and the average splitting tensile strength values were recorded

on three specimens for each replacement. Fig. 3.17 shows the testing of splitting tensile

strength of SCC.

Fig. 3.17: Testing of splitting tensile strength

The splitting tensile strength was determined according to the following Equation (3.4).

fsp = 2𝑃/πœ‹LD (3.4)

Where,

fsp = splitting tensile strength

𝑃 = maximum applied load indicated by the testing machine

𝐿 = average specimen length

𝐷 = specimen diameter

57

3.7.3 Modulus of Elasticity of SCC

The stress-strain curve of concrete is nonlinear. Its modulus of elasticity is given by the

slope of the stress strain curve. The modulus of elasticity (Ec) increases with increase

of compressive strength of concrete. The modulus of elasticity (Ec) of concrete depends

on the following factors:

(a) Age of concrete

(b) Properties of aggregates and cement

(c) Rate of loading

(d) Type and size of specimen

According to ASTM C 469-02 (2002) Ec is computed on the basis of compressive

strength. This standard specification states that the modulus of elasticity is applicable

with the customary working stress range of 0 to 40% of the ultimate concrete strength.

Under this study, cylindrical specimens made with brick aggregate were tested for

modulus of elasticity at 28 days. The specimens were tested using a compressometer as

shown in Fig. 3.18. The specimens were tested to 40% of the ultimate concrete strength

and the modulus was calculated from the following Equation (3.5):

Ec =S2βˆ’π‘†1

Ξ΅2βˆ’0.000050 (3.5)

Where

Ec = Modulus of elasticity of concrete (psi)

S2 = Stress corresponding to 40% of the ultimate load of the

concrete (psi)

S1 = Stress corresponding to a longitudinal strain of Ξ΅1 at 50

millionths (psi)

Ξ΅2 = Longitudinal strain produced by S2

58

Fig. 3.18: Testing of modulus of elasticity

3.8 SUMMARY

This chapter has explained the preparation of materials and experimental procedures,

methodology and detailed experimental investigations that were used for this research.

The required materials used for preparation of SCC using brick aggregate have also

been mentioned. Besides this the methods, instruments and machine used for testing

the fresh and mechanical properties of concrete are given with some photographs. The

preparation and testing of SCC with BA are described with appropriate testing

standards. Relevant testing information are included in Appendix.

59

CHAPTER 4 CHAPTER IV

………… … RESULTS AND DISCUSSION

4.1 GENERAL

This chapter emphasizes the properties of self-compacting concrete made with brick

aggregate. To justify the workability of fresh SCC in terms of passing ability, filling

ability and segregation resistance properties, slump flow, T50 cm flow time, V-funnel

flow time, V-funnel flow at T5 minutes and L-box tests were conducted in this research.

Compressive strength, modulus of elasticity and splitting tensile strength test were

performed for hardened concrete. Test results are discussed separately in this chapter.

This chapter also describes the material properties and mixture proportions for the

ingredients of SCC.

4.2 PROPERTIES OF MATERIALS

In this study, 19 mm and 12.5 mm downgraded coarse aggregate made from locally

available crushed bricks were used with available coarse sand (Sylhet Sand), Portland

composite cement and Con-Lub SP as high range water reducer to produce mixes of

SCC. The physical and chemical properties of the materials are described in the

following sections.

4.2.1 Coarse Aggregate

Coarse aggregates were prepared by crushing the locally available first class clay bricks.

The physical properties of coarse aggregates were confirmed by standard test

specifications that have been elaborated in the previous chapter and properties observed

for these coarse aggregate are summarized in Table 4.1.

From Table 4.1, it is observed that fineness modulus, specific gravity (OD), water

absorption, unit weight, elongation and flakiness index of brick aggregate were 6.79,

1.73, 19.7%, 917 kg/m3, 10.9 and 12.06 respectively for 19 mm downgraded coarse

aggregate. Also the values of these properties for 12.5 mm downgraded were 6.56, 1.73,

19.8%, 923 kg/m3, 10.8 and 11.6 respectively.

60

Table 4.1: Properties of coarse and fine aggregates

Properties

Coarse Aggregate Fine

Aggregate

(Coarse

Sand) (19 mm

Downgrade)

(12.5 mm

Downgrade)

Fineness Modulus 6.79 6.56 2.81

Unit weight (OD) (kg/m3) 917 923 1512

Water absorption (%) 19.7 19.8 1.0

Field Moisture (%) 7.41 7.42 0.35

Specific Gravity (Oven dry) 1.73 1.73 2.61

(SSD) 2.07 2.07 2.63

Elongation Index 10.9 10.8 -

Flakiness Index 12.6 11.6 -

Rashid et al. (2012) found fineness modulus, specific gravity, water absorption and unit

weight of brick aggregate as 7.17, 2.03, 16.0% and 903 kg/m3 respectively and fineness

modulus, specific gravity, water absorption of fine aggregate as 1.62, 2.65 and 2.04%

respectively. The value of the properties of aggregates mentioned in the Table 4.1 are

very similar to these researchers.

Fig. 4.1: Gradation curve of 12.5 mm downgraded coarse aggregate

0

20

40

60

80

100

1 10 100

12.5 mm Downgraded CA ASTM Lower Limit ASTM Upper Limit

Sieve size (mm)

%

Fin

er

61

Fig. 4.2: Gradation curve of 19 mm downgraded coarse aggregate

Fig. 4. 1 and Fig. 4.2 illustrate the gradation curves of brick aggregates. The grading

of these aggregates falls within the range of the upper and lower limits of the ASTM

C33 (2018) standards and as such, meet the gradation requirements. However, the

coarse aggregates were slightly out of the boundary for the 19 mm sieve size for both

gradation curve. This is the evidence of well grading occurring between the upper and

lower limits with a decrease in the percentage of the aggregates passing through the

respective sieve sizes. Additionally, there is no indication of gap grading in the

respective sieve sizes.

4.2.2 Fine Aggregate

Fine aggregate used in this study was collected from local sources named as Sylhet sand.

The physical properties of fine aggregates were confirmed by standard test

specifications that have been elaborated in the previous chapter and properties observed

for these fine aggregates are summarized in Table 4.1.

The properties of the fine aggregate used in this study designated as fineness modulus,

unit weight, water absorption and specific gravity were 2.81, 1512 kg/m3, 1.0% and

2.61 respectively. Rashid et al. (2012) found fineness modulus, specific gravity, water

absorption of fine aggregate as 1.62, 2.65 and 2.04% respectively. The value of the

properties of aggregates mentioned in the Table 4.1 are very similar to these

researchers.

0

20

40

60

80

100

1 10 100

19 mm Downgraded CA ASTM Lower Limit ASTM Upper Limit

Sieve size (mm)

% F

iner

62

Fig. 4.3 represents the gradation curve for fine aggregate used in this study with the

sample size within the range of the specification of ASTM C33 (2018). The fineness

modulus of fine aggregate should be within the range of 2.3 to 3.1 for continuous

grading. The fine aggregate that was used in this study have a fineness modulus of

2. 81 which is the evidence of well grading occurring for this aggregate.

Fig. 4.3: Gradation curve of fine aggregate

4.2.3 Cement

In this study, locally available Portland composite cement was used. The physical

properties of cement were confirmed by standard test specifications that has been

elaborated in the previous chapter and properties and compound compositions

(mentioned by manufacturer) observed for this materials are summarized and presented

in Table 4.2 and Table 4.3 respectively.

Table 4.2: Test Results of Cement

Name and Type of Cement Portland Composite Cement

BS EN 197-1:2011/CEM II(B-M)

Normal Consistency (%) 28

Initial Setting Time 104 Minutes

Final Setting Time 4 hours 30 minutes

Compressive Strength (MPa) 19.40 (3 days) 20.30 (7 days) 23.8 (28 days)

0

20

40

60

80

100

0.1 1 10

Fine Aggregate ASTM Lower Limit ASTM Upper Limit

Sieve size (mm)

% F

iner

63

Table 4.3: Compound compositions of portland composite cement

Compounds Percentage by Mass CEM II (B-M) Standard

Clinker 70-79 65-79

Gypsum 0-5 0-5

Slag, Fly ash & Limestone 21-30 21-35

4.2.4 Superplasticizer

Con-Lub SP is a high range water reducer, accelerating super plasticizer and an

extremely powerful de-flocculating agent. This superplasticizer was used in the mixes

of SCC to achieve the fresh properties of SCC. Technical data provided by

manufacturer are listed in Table 4.4.

Table 4.4: Technical data of Superplasticizer

Type of superplasticizer ASTM C494; Type F and G

Appearance Light Yellow Liquid

Specific Gravity at 20Β° C 1.07Β±0.01

pH value 7Β±1

Alkali Content (%) No affecting Alkali

Chloride Content (%), expressed as a

percentage of mass of total admixture

zero

Dosages by weight of cement 0.6-1.6%

4.3 PHYSICAL OBSERVATION OF FRESH CONCRETE

At the time of mixing, the physical state of the fresh concrete was observed. It was

found that huge bubbles formed on the concrete at the time of mixing which is shown

in Fig. 4.5. It was also observed that fresh SCC with the bubbles on the surface

possesses segregation and bleeding in the concrete. With increasing the mixing time,

these bubbles got diminished gradually. As a results, there was no bleeding and

segregation in the fresh concrete as shown in Fig. 4.6. When water was added to the

ingredients of concrete, the cement particle entraps water with air. Due to the addition

of SP, it starts to deflocculate the cement particle and frees the water and air to impart

the fluidity of fresh concrete. When all the cement particles get deflocculated by the

64

dispersing action of SP and entrap water and air gets free, then the fresh concrete shows

the good quality of flowability and stability.

Fig. 4.4: Surface of the fresh concrete with bubbles formation

Fig. 4.5: Surface of the fresh concrete without bubbles formation

65

4.4 FRESH PROPERTIES OF SCC WITH BRICK AGGREGATE

To investigate the filling ability, passing ability, and segregation resistance of the fresh

concrete, slump flow, T50 flow time, V-funnel flow, V-funnel flow at T5 minutes,

L-box and J-ring tests were performed. These results are shown in Table 4.5 and

discussed below.

Table 4.5: Fresh properties of SCC with brick aggregate

Specimen ID

Filling ability Passing ability Segregation

Resistance

SF1

(mm)

T502

(s)

Tv3

(s)

JF4

(mm)

BI5

(mm)

JF6

(mm) BR7

Tv58

(s) +

C450A12W35 590 4.5 7.5 565 25 10 0.89 +2.9

C470A12W35 610 4.3 7 580 30 9 0.93 +2.3

C500A12W35 640 3.85 7.5 605 35 8 0.95 +2.5

C530B12W35 630 3.6 6.5 615 15 3 0.98 +2.7

C550C12W35 620 3.56 6.3 595 25 4 0.99 +2.5

C580D12W35 660 4 8.1 620 40 4.5 1.00 +3

C450A19W35 580 4.8 6.8 560 20 8 0.96 +2.9

C470A19W35 605 4.6 6.8 580 25 8 0.95 +3.2

C500A19W35 610 4.5 6.6 580 30 7 0.98 +3.5

C530B19W35 615 4.3 6.5 570 45 9 0.98 +3.5

C550C19W35 610 4 6.5 555 55 9 0.88 +3.5

C580D19W35 620 4.5 6.4 585 35 6 0.98 +2

C450A12W40 610 4 7 585 25 9 0.88 +3.9

C470A12W40 620 3.8 6.5 595 25 6 0.90 +3.6

C500A12W40 650 3.4 6 610 40 5 0.95 +2.4

C530B12W40 640 3.6 5.8 600 40 8 0.95 +2.3

C550C12W40 640 3.56 5.8 610 30 9 0.90 +2.5

C580D12W40 670 3 6.5 650 20 3 0.98 +2.5

C450A19W40 595 4.2 6.1 570 25 10 0.94 +2.3

C470A19W40 620 3.9 6.2 597 23 9 0.92 +2.8

C500A19W40 640 4.1 6.5 600 40 6 0.90 +3.0

C530B19W40 640 4.3 6.2 610 30 9 0.90 +3.0

C550C19W40 630 3.9 6 590 40 10 0.88 +3.1

C580D19W40 650 3.8 7.5 610 40 7 0.95 +2.5 1slump flow, 2T50 slump flow time, 3V-funnel flow time, 4 J-ring flow, 5 J-ring blocking

index, 6 Height difference just inside and outside of the bar, 7 L-box blocking ratio, 8V-

funnel at T5minutes

66

4.4.1 Filling Ability

Filling ability of SCC with BA has confirmed by slump flow, T50 flow time and

V-funnel flow test in the laboratory for this research.

4.4.1.1 Slump Flow

Slump flow is a filling ability test of fresh SCC. The range of the slump flow varies

from 550 mm to 850 mm (EFNARC, 2005). The results of the slump flow of SCC with

brick aggregate are shown in Table 4.5 and the graphical presentation of these results

with various concrete mixes are shown in Fig. 4.6

Fig. 4.6: Variation of Slump Flow of SCC with Brick Aggregate

From Fig. 4.6 it is observed that maximum slump flow of 670 mm was found with 12.5

mm size CA with a w/c ratio 0.40 and the minimum value of slump flow was 580 mm

with 19 mm size CA with w/c ratio 0.35. It is also observed that the slump flow of the

concrete mixes prepared with w/c ratio of 0.40 exhibits better results in term of slump

flow than the concrete mixes prepared with w/c of 0.35. In case of higher w/c ratio,

excess amount of water increases the fluidity of concrete mixes and hence the higher

slump flow. All the SCC mixes have satisfied the required criteria of filling ability

according to standard guideline of EFNARC (2005). SantamarΓ­a et al. (2020) reported

the slump flow 680 mm-700 mm for the SCC made using Electric Arc Furnace Slag as

550

570

590

610

630

650

670

690

C45

0A

12

W35

C47

0A

12

W35

C50

0A

12

W35

C53

0B

12

W3

5

C55

0C

12

W3

5

C58

0D

12

W35

C45

0A

19

W35

C47

0A

19

W35

C50

0A

19

W35

C53

0B

19

W3

5

C55

0C

19

W3

5

C58

0D

19

W35

C45

0A

12

W40

C47

0A

12

W40

C50

0A

12

W40

C53

0B

12

W4

0

C55

0C

12

W4

0

C58

0D

12

W40

C45

0A

19

W40

C47

0A

19

W40

C50

0A

19

W40

C53

0B

19

W4

0

C55

0C

19

W4

0

C58

0D

19

W40

Slu

mp

Flo

w (

mm

)

Concrete Mixes

Minimum Value

67

coarse aggregate. Roy et al. (2019) reported the slump flow of SCC made with brick

aggregate is 427 mm-712 mm. In another study of SCC with replacement of natural

brick aggregate with recycled one by Roy et al. (2016), the value of slump flows was

reported 735 mm-755 mm. Khayat (2015) reported that an SCC with a slump flow of

650 mm for the 20 mm size natural CA with 555 kg/m3 of cementitious materials can

be more suitable for casting highly congested structures. Nischay et al. (2015) also

reported that when natural aggregate replaced by the recycled aggregate, slump flows

were 690 mm and 580mm for 25% and 100% replacement respectively. Safiuddin et

al. (2014) revealed that the slump flow SCC made with crushed granite varied from

605 mm to 720 mm. To ensure adequate self-consolidation capacity, a minimum slump

flow of 600 mm is generally recommended for SCC (Khayat, 2000). Therefore, from

the above discussion it can be concluded that SCC mixes with brick aggregate shows

good passing ability. This extends the tendency of flowability revealed as a highly

flowable SCC.

Fig. 4.7 presents the variation of slump of SCC with 12.5 mm and 19 mm CA at w/c

ratio of 0.35. Slump flow series with 12.5 mm CA (660 mm, 640 mm, 630 mm and 620

mm) and 19 mm CA (620 mm, 610 mm, 615 mm and 610 mm) were found for the CA

contents of 550 kg/m3, 560 kg/m3, 570 kg/m3 and 580 kg/m3 respectively. It is found

that the higher slump flow value with 12.5 mm CA compared to 19 mm CA. Also the

slump flow value of SCC with BA decreases with increasing the CA content.

Fig. 4.7: Variation of slump flow of SCC (w/c = 0.35)

600

620

640

660

680

540 550 560 570 580 590

Slu

mp F

low

(m

m)

CA Content (kg/m3)

12.5 mm CA with w/c = 0.35

19 mm CA with w/c = 0.35

68

Fig. 4.8 presents the variation of slump of SCC with 12.5 mm and 19 mm CA at w/c

ratio of 0.40. Slump flow series with 12.5 mm CA (670 mm, 650 mm, 640 mm and 640

mm) and 19 mm CA (650 mm, 640 mm, 640 mm and 630 mm) were found for the CA

contents of 550 kg/m3, 560 kg/m3, 570 kg/m3 and 580 kg/m3 respectively. It is found

the similar result of SCC mixes with w/c of 0.35 that lower sizes CA possesses higher

slump flow value and it is decreases with increasing the CA content. A very good filling

ability was attained with 12.5 mm CA over the 19 mm size CA in all cases. Similar

results were reported by Olowofoyeku et al. (2019), Kasim et al. (2017) and

Pandurangan et al. 2012) that the lower size of coarse aggregate yielded better slump

flow properties than higher size of aggregates. This may be attributed that the particle

size distribution and the shape of coarse aggregate directly influence the flow and

passing ability of SCC and its paste demand. Smaller size aggregate cause less blocking

and the greater flow because of reduced internal friction.

Fig. 4.8: Variation of slump flow of SCC (w/c = 0.40)

In case of all concrete mixes, the slump flow decreased with the increase of CA content.

Lower content of CA possessed a very good slump flow. It may be attributed that with

increasing the CA content, amount of aggregate increased for the concrete mix and the

internal friction among the aggregate particles increased which results the blocking in

the concrete flow and lower the slump flow.

From the above discussion, it can be concluded that smaller size CA and lower content

of CA can hold a very good filling ability in terms of slump flow. All mixes have

620

640

660

680

540 550 560 570 580 590

Slu

mp F

low

(m

m)

CA Content (kg/m3)

12.5 mm CA with w/c = 0.40

19 mm CA with w/c = 0.40

69

satisfied the provision specified for slump flow of SCC. Therefore, all mixtures

possessed adequate slump with consistency.

4.4.1.2 T50 Flow Time

T50 flow time is also a measure of filling ability. The standard range of the time required

to flow 50 cm is 2-5 sec according to EFNARC (2005). This parameter indicates that

the concrete mixes possess moderate viscosity. Fig. 4.9 shows the T50 slump flow for

all concrete mixes.

Fig. 4.9: T50 slump flow time of SCC using brick aggregate

Fig. 4.9 shows the he values of T50 slump flow time for this study were found 3-4.8 sec.

Test results indicated that all concrete mixes fulfilled the requirements of flow time

according to the standard parameter (EFNARC, 2005). It is observed that trial mixes

with 19 mm CA took greater time to flow than 12.5 mm CA at all w/c ratios. The

maximum T50 flow time was recorded as 4.8 sec when 19 mm CA (C450A1935) were

mixed with a w/c ratio of 0.35. Roy et al. (2019) reported the T50 flow time of SCC with

BA was varied from 2 to 7 seconds. Dey et al. (2016) also found the T50 flow time of

SCC with recycled aggregate replaced with BA is 1-2.1 sec. Madandoust and Mousavi

(2012) measured the T50 flow times for self-compacting concrete containing a

2

2.5

3

3.5

4

4.5

5

5.5

C45

0A

12

W35

C47

0A

12

W35

C50

0A

12

W35

C53

0B

12

W3

5

C55

0C

12

W3

5

C58

0D

12

W35

C45

0A

19

W35

C47

0A

19

W35

C50

0A

19

W35

C53

0B

19

W3

5

C55

0C

19

W3

5

C58

0D

19

W35

C45

0A

12

W40

C47

0A

12

W40

C50

0A

12

W40

C53

0B

12

W4

0

C55

0C

12

W4

0

C58

0D

12

W40

C45

0A

19

W40

C47

0A

19

W40

C50

0A

19

W40

C53

0B

19

W4

0

C55

0C

19

W4

0

C58

0D

19

W40

T5

0 F

low

tim

e (s

ec)

Concrete Mixes

Maximum

value Minimum

value

70

maximum nominal size 12.5 mm limestone gravel as coarse aggregate within the range

of 1.3-7.97 sec. Mohamad et al. (2015) reported the T50 flow time for SCC with natural

aggregate in the range of 1-6 sec. Safiuddin et al. (2011b) reported that the T50 slump

flow time varied in the range of 2.6-4.5 sec for SCC with recycled aggregate.

Fig. 4.10 presents the variation of slump flow and T50 flow time of the SCC mix made

with brick aggregate. It is observed that T50 time was maximum in the case of the SCC

having low slump flow value.

Fig. 4.10: Variation of slump flow and T50 flow time of SCC

From this research, minimum slump flow values were found with 19 mm size CA and

a w/c ratio of 0.35 and simultaneously the T50 flow time for this mix was maximum.

On the other hand, maximum slump flow values were found with 12.5 mm size CA and

a w/c ratio of 0.40, and simultaneously the T50 flow time for this mix was minimum.

This may be attribute that the larger size CA contains higher irregular shaped aggregates

and causes the resistance to flow of SCC mixes compared to smaller sizes CA. This

variation takes place due to the angularity and elongation of 19 mm CA over the

aggregate size of 12.5 mm. However, SCC with brick aggregate possesses a moderate

viscosity with respect to T50 flow time. However, it can be concluded that T50 flow time

is inversely proportional to slump flow value for any SCC mix.

2.5

3

3.5

4

4.5

5

550

600

650

700

C45

0A

12

W35

C47

0A

12

W35

C50

0A

12

W35

C53

0B

12

W3

5

C55

0C

12

W3

5

C58

0D

12

W35

C45

0A

19

W35

C47

0A

19

W35

C50

0A

19

W35

C53

0B

19

W3

5

C55

0C

19

W3

5

C58

0D

19

W35

C45

0A

12

W40

C47

0A

12

W40

C50

0A

12

W40

C53

0B

12

W4

0

C55

0C

12

W4

0

C58

0D

12

W40

C45

0A

19

W40

C47

0A

19

W40

C50

0A

19

W40

C53

0B

19

W4

0

C55

0C

19

W4

0

C58

0D

19

W40

T5

0F

low

Tim

e (s

ec)

Slu

mp f

low

(m

m)

Concrete Mixes

Slump Flow T50 Flow Time

71

4.4.1.3 V- Funnel Flow

Results of V-funnel flow tests of different concrete mixes are presented in Table 4.5.

V-funnel flow test is used to measure the filling ability of self-compacting concrete. In

this test, time is measured to pass the fresh concrete through the V-funnel. The standard

value of the time for V-funnel flow time is 6 to 12 sec according to EFNARC (2002).

Results obtained from these test exhibited the satisfactory parameter for these values.

Graphical presentation of the time needed for V-funnel flow tests are shown in Fig.

4.11.

Fig. 4.11: Time needed for V-funnel flow

Maximum and minimum value of V-funnel time were recorded as 8.1 sec and 5.8 sec

which represent good passing ability. From graph it is observed that there was no

specific condition to characterize the V-funnel time. Roy et al. (2019) reported the V-

funnel flow was 4-15 sec. In another study, Dey et al. (2016) shows the value of

V-funnel flow time was 6-11.5 sec with replacement of natural brick aggregate with

recycled aggregate.

0

1

2

3

4

5

6

7

8

9

C450A

12W

35

C4

70A

12

W3

5

C500A

12W

35

C530B

12W

35

C550C

12W

35

C5

80D

12

W3

5

C450A

19W

35

C470A

19W

35

C500A

19W

35

C5

30B

19W

35

C550C

19W

35

C580D

19W

35

C450A

12W

40

C4

70A

12

W4

0

C500A

12W

40

C530B

12W

40

C550C

12W

40

C5

80D

12

W4

0

C450A

19W

40

C470A

19W

40

C500A

19W

40

C5

30B

19W

40

C550C

19W

40

C580D

19W

40

Tim

e (s

ec)

Concrete Mixes

V-funnel Flow Time

72

The relation between the slump flow and time for V-funnel flow is presented in Fig.

4.12. It is observed that there is no specific relation between V-funnel flow time and

slump flow of SCC with. In some cases, V-funnel flow time depends on the aggregate

sizes and water cement ratios. In case of higher w/c ratio, required V-funnel time is

lowered compared to others. To reiterate, the filling ability in terms of V-funnel flow

time depends on the size and volume fraction of the coarse aggregate. This is because

the resistance to flow through V-funnel due to irregular shaped aggregates is overcome

by paste volume in SCC mixes (Pandurangan et al., 2012).

Fig. 4.12: Relation between slump flow and V-funnel flow time

4.4.2 Passing Ability

Passing ability of SCC with BA has confirmed by J-Ring flow and L-Box test in the

laboratory for this research.

4.4.2.1 J-Ring Flow Test

J-Ring flow of the different SCC mixes are presented in Table 4.5. Fig 4.13 presents

the J-ring flow of fresh SCC with the variation slump flow of concrete mixes. The figure

reveals that the J-ring flow of SCC with BA follows the similar trend of slump flow.

4.5

5

5.5

6

6.5

7

7.5

8

8.5

500

550

600

650

700

C4

50

A12

W35

C4

70

A12

W35

C5

00

A12

W35

C5

30

B12

W3

5

C5

50

C12

W3

5

C5

80

D12

W35

C4

50

A19

W35

C4

70

A19

W35

C5

00

A19

W35

C5

30

B19

W3

5

C5

50

C19

W3

5

C5

80

D19

W35

C4

50

A12

W40

C4

70

A12

W40

C5

00

A12

W40

C5

30

B12

W4

0

C5

50

C12

W4

0

C5

80

D12

W40

C4

50

A19

W40

C4

70

A19

W40

C5

00

A19

W40

C5

30

B19

W4

0

C5

50

C19

W4

0

C5

80

D19

W40

V-F

unnel

Tim

e (s

ec.)

Slu

mp F

low

(m

m)

Concrete Mixes

Slump flow V-Funnel Flow Time

73

Maximum J-ring flow (650 mm) was found with concrete mix C580D1W240 at which

water-cement ratio is 0.40 with 12.5 mm coarse aggregate and the minimum (555 mm)

was at w/c ratio of 0.35 with 19.5 mm coarse aggregate for the concrete mix

(C550C19W35). In the case of concrete mix (C550C19W35), the content of CA is high

compared to others and w/c ratio is 0.35. This may be attributed that higher CA content

with lower w/c ratio possessed a decrease in J-ring flow due to internal friction among

the aggregates particles. Due to having a higher value of elongation and flakiness of 19

mm size CA over 12.5 mm CA, the larger size aggregate may directly influence the

flow of particle through J-ring. Safiuddin et al. (2011b) reported the J-ring flow values

were in the range of 590–700 mm and the differences between slump flow and J-ring

flow were below 50 mm.

Fig. 4.13: Variation of slump flow and J-ring flow of SCC with BA

Fig 4.14 presents the blocking index of freshly mixed SCC. The blocking index (BI) is

the difference between slump flow and J-ring flow of fresh concrete which is a measure

of passing ability. A lower value of blocking index indicates a good passing ability.

From Fig. 4.14 it is observed that the highest and lowest value of the blocking index

were 55 mm and 15 mm. Except the mix (C550C19W35) with 19 mm CA with w/c of

0.35, all mixes have met the standard requirement of blocking index (BI ≀ 50 mm)

according to EFNARC (2002). A higher value of the blocking index was achieved with

the combination of larger size CA and lower water-cement ratio.

500

550

600

650

700

C450A

12W

35

C4

70A

12

W3

5

C500A

12W

35

C530B

12W

35

C550C

12W

35

C5

80D

12

W3

5

C450A

19W

35

C470A

19W

35

C500A

19W

35

C530B

19W

35

C550C

19W

35

C580D

19W

35

C450A

12W

40

C470A

12W

40

C500A

12W

40

C530B

12W

40

C550C

12W

40

C580D

12W

40

C450A

19W

40

C470A

19W

40

C500A

19W

40

C530B

19W

40

C550C

19W

40

C580D

19W

40

Flo

w (

mm

)

Concrete Mixes

Slump Flow J-ring flow

74

Fig. 4.14: Blocking index of SCC mixes with BA

Fig 4.15 shows the height difference of concrete in J-ring. Records of the tests of this

study revealed that the maximum height difference of the concrete just inside and

outside the J-ring was maximum 10 mm.

Fig. 4.15: Height Difference in J-Ring Flow Test of SCC with BA

The value of this height difference fulfilled the requirements (Height difference ≀ 10

mm) of SCC specified by EFNARC (2002). It is also found that the height difference

0

10

20

30

40

50

60

C450A

12W

35

C4

70

A1

2W

35

C5

00

A1

2W

35

C5

30

B1

2W

35

C5

50

C1

2W

35

C5

80

D1

2W

35

C4

50

A1

9W

35

C4

70

A1

9W

35

C5

00

A1

9W

35

C5

30

B1

9W

35

C5

50

C1

9W

35

C5

80

D1

9W

35

C4

50

A1

2W

40

C4

70

A1

2W

40

C5

00

A1

2W

40

C5

30

B1

2W

40

C5

50

C1

2W

40

C5

80

D1

2W

40

C4

50

A1

9W

40

C4

70

A1

9W

40

C5

00

A1

9W

40

C530B

19W

40

C5

50

C1

9W

40

C5

80

D1

9W

40

Blo

ckin

g I

nd

ex (

mm

)

Concrete Mixes

Maximum Range

0

2

4

6

8

10

12

C45

0A

12

W35

C47

0A

12

W35

C50

0A

12

W35

C53

0B

12

W3

5

C55

0C

12

W3

5

C58

0D

12

W35

C45

0A

19

W35

C47

0A

19

W35

C50

0A

19

W35

C53

0B

19

W3

5

C55

0C

19

W3

5

C58

0D

19

W35

C45

0A

12

W40

C47

0A

12

W40

C50

0A

12

W40

C53

0B

12

W4

0

C55

0C

12

W4

0

C58

0D

12

W40

C45

0A

19

W40

C47

0A

19

W40

C50

0A

19

W40

C53

0B

19

W4

0

C55

0C

19

W4

0

C58

0D

19

W40

Hei

gh

t D

iffe

ren

ce in

J-r

ing (

mm

)

Concrete Mixes

Maximum value

75

in J-ring increases with the size of aggregate. Due to having lower elongation and

flakiness of smaller sizes aggregate, it shows good passing ability compared with larger

size aggregate.

4.4.2.2 L-Box Test

L-box test is a measure of filling ability of freshly mixed SCC. It is expressed in terms

of the value of H2/H1 known as Blocking Ratio (BR). Fig 4.16 represent the BR of

different concrete.

Fig. 4.16: Blocking ratio of SCC Mixes with BA

It is observed from Fig. 4.16 that the BR for all mixes of SCC with brick aggregate

have satisfied the required value. The value of the BR is limited to 0.80-1.0 according

to EFNARC (2002). The value of the BR of the concrete mixes had greater than 0.88

which indicates good passing ability of fresh concrete. Felekoglu et al. (2007) reported

filling abilities with L-box ratio of 0.95 and 0.50 with crushed lime stone. Dey et al.

(2016) found the L-box ratio was 0.9-1.00 with recycled brick aggregate. Roy et al.

(2019) reported the values of L-box ratio for SCC with brick aggregate was 0.67-0.98.

No segregation or blocking of aggregates was observed. All mixtures had excellent

passing ability with less tendency of segregation which indicates good flow ability of

SCC in the presence of congested reinforcement.

0.80

0.85

0.90

0.95

1.00

1.05

C450A

12W

35

C470A

12W

35

C500A

12W

35

C530B

12W

35

C550C

12W

35

C580D

12W

35

C450A

19W

35

C470A

19W

35

C500A

19W

35

C530B

19W

35

C550C

19W

35

C580D

19W

35

C450A

12W

40

C470A

12W

40

C500A

12W

40

C530B

12W

40

C550C

12W

40

C580D

12W

40

C450A

19W

40

C470A

19W

40

C500A

19W

40

C530B

19W

40

C550C

19W

40

C580D

19W

40

Blo

ckin

g R

atio

Concrete Mixes

Maximum Range Minimum Range

76

4.4.3 Segregation Resistance

Segregation resistance of SCC with BA has been measured in terms of V-funnel flow

at T5minutes for this research.

4.4.3.1 V-Funnel Flow at T5minutes

V-funnel flow at T5minutes is the measure of the segregation resistance. This property can

explain the internal or external bleeding of water, accumulation of aggregates or paste

at the top surface and aggregate on the bottom surface of the concrete (Bonen and Shah,

2005). To measure the segregation resistance for SCC, V-funnel at T5minutes test was

performed in the laboratory for this research. Table 4.5 also represents the time required

for V-funnel at T5minutes. This parameter is the measure of the segregation resistance.

The optimum range of the time for V-funnel at T5minutes is 0 to +3 with the time needed

for V-funnel. Results obtained from these test exhibited the satisfactory parameter for

these values. Graphical presentation of the time needed for V-funnel and V-funnel at

T5minutes tests are shown in Fig. 4.17.

Fig. 4.17: Time needed for V-funnel flow at T5minutes

0

2

4

6

8

10

12

C4

50

A1

2W

35

C470A

12W

35

C5

00

A1

2W

35

C5

30

B1

2W

35

C5

50

C1

2W

35

C580D

12W

35

C4

50

A1

9W

35

C4

70

A1

9W

35

C5

00

A1

9W

35

C530B

19W

35

C5

50

C1

9W

35

C5

80

D1

9W

35

C4

50

A1

2W

40

C470A

12W

40

C5

00

A1

2W

40

C5

30

B1

2W

40

C5

50

C1

2W

40

C580D

12W

40

C4

50

A1

9W

40

C4

70

A1

9W

40

C5

00

A1

9W

40

C530B

19W

40

C5

50

C1

9W

40

C5

80

D1

9W

40

Tim

e (s

ec)

Concrete Mixes

V-funnel Flow Time V-funnel Flow at T 5minutes

77

Fig. 4.17. shows the time needed for V-funnel flow at T5minutes test for SCC with BA. It

is observed that all the concrete mixes except C470A19W35, C500A19W35,

C530B19W35, C500C1935, C450A12W40 and C470A12W40 have satisfied the

criteria of segregation resistance It is one of the major attributes of SCC with BA. It

was observed that there was no blocking or segregation for any mixture and thus

exhibited excellent segregation resistance. SantamarΓ­a et al. (2020) use the column

segregation test to evaluate segregation in the self-compacting concrete mixtures and

satisfactory results. Also the researchers Roy et al. (2019), Dey et al. (2016), Khayat

(2015), Nischay et al. (2015), Mohamad et al. (2015) reported that no visible blocking

or segregation in their study.

4.5 CORRELATION BETWEEN FRESH PROPERTIES OF SCC WITH

BRICK AGGREGATE

The results of the fresh properties of SCC with brick aggregate for various mixes are

discussed in this chapter. All the SCC mixes possessed good fresh properties. The

detailed description of these test results have been present in the previous sections. This

section, mainly focuses the correlations between different fresh properties of SCC made

with brick aggregate.

4.5.1 Correlation between Slump Flow and J-ring Flow of SCC with Brick

Aggregate

The correlation between slump flow (SF) and the J-ring flow (JF) of fresh concrete

made with brick aggregate is shown in Fig. 4.18. It is observed that J-ring flow of SCC

with brick aggregate is linearly proportional to slump flow. The coefficient of

correlation between them is 0.8196 and the correlation exists between the slump flow

and the J-ring flow of fresh SCC is expressed as,

JF = 0.9494(SF), RΒ² = 0.8196 (4.1)

Safiuddin et al. (2011b) correlated the slump flow and the J-ring flow of SCC with

POFA and have found a strong correlation between them and the relation is expressed

as,

JF = 0.9543 (SF), RΒ² = 0.9634 (4.2)

78

In another study (Safiuddin et al., 2011a) authors have derived the correlation between

slump flow and the J-ring flow of SCC made with recycle aggregates and found a strong

correlation of these properties and mathematically expressed as,

JF = 1.1307 (SF) – 120.6, r = 0.9909 (4.3)

In this study, the expression indicates a good correlation between slump flow and

J-ring flow of fresh SCC with brick aggregate.

Fig. 4.18: Correlation between J-ring flow and slump flow of SCC

4.5.2 Correlation between Slump Flow and T50 Flow Time of SCC

The slump flow of fresh SCC with brick aggregate also correlated with T50 flow time.

The correlation between slump flow and the T50 flow time of fresh concrete made with

brick aggregate is shown in Fig. 4.19. It is observed that T50 flow time decreases with

increasing the slump flow and possesses a good passing ability and filling ability. The

coefficient of correlation between them is 0.5416 and the correlation exists between the

slump flow and T50 flow time of fresh SCC is express as,

TF = -0.0143(SF) + 12.921 (4.4)

RΒ² = 0.5416

JF = 0.9494(SF)

RΒ² = 0.8196

540

560

580

600

620

640

660

560 580 600 620 640 660 680

J-R

ing F

low

(m

m)

Slump Flow (mm)

79

Fig. 4.19: Correlation between slump flow and T50 flow time of SCC

4.5.3 Correlation between J-ring Flow and T50 Flow Time of SCC

The J-ring flow of fresh SCC with brick aggregate is also correlated with T50 flow time.

The correlation between J-ring flow and the T50 flow time of fresh concrete made with

brick aggregate is shown in Fig. 4.20. It is observed that T50 flow time decreases with

increasing the J-ring flow and possesses a good passing ability and filling ability. The

coefficient of correlation between them is 0.5594 and the correlation exists between the

slump flow and T50 flow time of fresh SCC which is expressed as,

TF = -0.0148(JF) + 12.773 (4.5)

RΒ² = 0.5594

Fig. 4.20: Correlation between J-ring flow and T50 flow time of SCC

TF = -0.0143(SF) + 12.921

RΒ² = 0.5416

2.75

3.25

3.75

4.25

4.75

5.25

560 580 600 620 640 660 680

T5

0F

low

Tim

e (s

ec)

Slump Flow (mm)

TF = -0.0148(JF) + 12.773

RΒ² = 0.5594

2.5

3

3.5

4

4.5

5

540 560 580 600 620 640 660

T5

0F

low

Tim

e (s

ec)

J-ring Flow (mm)

80

4.6 MECHANICAL PROPERTIES OF SCC WITH BRICK AGGREGATE

Mechanical properties are the most dominating factors and significant parameters for

SCC. These properties may be affected by many factors such as w/c ratios, aggregate

contents, shape and sizes of CA, properties of aggregates etc. In this study, mechanical

properties of SCC made with crushed brick as coarse aggregates were determined by

compressive strength, modulus of elasticity, and splitting tensile strength tests of

hardened concrete. The mechanical behavior of SCC with brick aggregate observed in

this study are presented in Table 4.8.

Table 4.6: Mechanical Properties of SCC with Brick Aggregate

Specimen ID

Compressive

Strength, f'c

(MPa)

Splitting

Tensile

Strength, fsp

(MPa)

Modulus of

Elasticity, Ec

(GPa)

C450A12W35 21.10 2.08 16.75

C470A12W35 24.41 2.48 18.02

C500A12W35 28.20 2.81 19.05

C530B12W35 27.81 2.73 23.91

C550C12W35 26.33 2.47 21.75

C580D12W35 29.81 2.89 16.94

C450A19W35 20.72 2.12 16.64

C470A19W35 22.67 2.29 17.33

C500A19W35 24.54 2.41 20.75

C530B19W35 23.08 2.21 15.09

C550C19W35 24.04 2.33 19.44

C580D19W35 25.65 2.59 19.76

C450A12W40 20.05 2.1 16.30

C470A12W40 21.94 2.23 17.11

C500A12W40 23.23 2.42 15.11

C530B12W40 24.07 2.45 16.72

C550C12W40 20.10 2.46 16.22

C580D12W40 24.06 2.46 18.33

C450A19W40 20.24 2.07 16.37

C470A19W40 21.13 2.11 16.75

C500A19W40 21.65 1.98 16.25

C530B19W40 22.55 2.25 15.92

C550C19W40 20.05 2.02 15.57

C580D19W40 23.67 2.64 15.38

81

4.6.1 Compressive Strength

Compressive strength is the key performance indicator for the structural use of concrete.

In this study compressive strength of hardened concrete was tested only for 28 days.

Compressive strength behavior of SCC with brick aggregate are presented in Table 4.6.

Fig. 4.21 shows the variation of compressive strength of SCC with brick aggregate. It

is found that the compressive strength of SCC ranges from 29.81 MPa to 20.05 MPa.

According to BNBC (1993), minimum strength of concrete required for earthquake

resistant structure is 20 MPa but it can be relaxed up to 17 MPa for using in a building

structure up to 4 story. In this research, SCC with brick aggregate have satisfied the

required strength along with the all fresh properties. Research on SCC with BA was

conducted by Roy et al. (2019). Authors reported the compressive strength of 20 MPa

to 40 MPa for the SCC with brick aggregate for the w/c ratios of 0.50 and 0.35

respectively. In an another study, Dey et al. (2016) reported the compressive strength

of 25 MPa to 35 MPa for a w/c ratio of 0.40 of the SCC mixes with virgin and recycled

brick aggregates.

Fig. 4.21: Compressive strength of SCC with brick aggregate

4.6.1.1 Effect of Aggregate Size and Cement Contents on Compressive Strength

of SCC

Fig. 4.22 presents the compressive strength of SCC with brick aggregates for the

concrete mixes prepared with 12.5 mm and 19 mm CA with w/c ratios of 0.35. In case

of 12.5 mm CA, compressive strengths were found 21.10 MPa, 24.41 MPa, 28.20 MPa,

0.00

10.00

20.00

30.00

40.00

12.5 mm CA with

w/c = 0.35

19 mm CA with

w/c = 0.35

12.5 mm CA with

w/c = 0.40

19 mm CA with

w/c = 0.40

Com

pre

ssiv

e S

tren

gth

(M

Pa)

Cement Content (kg/m3)

450 470 500 530 550 580

82

27.81 MPa, 26.33 MPa and 29.81 MPa with cement content 450 kg/m3, 470 kg/m3, 500

kg/m3, 530 kg/m3, 550 kg/m3 and 580 kg/m3 respectively. In case of 19 mm CA,

compressive strengths were found 20.72 MPa, 22.67 MPa, 24.54 MPa, 23.08 MPa,

24.04 MPa and 25.65 MPa with cement content 450 kg/m3, 470 kg/m3, 500 kg/m3, 530

kg/m3, 550 kg/m3 and 580 kg/m3 respectively. It is found that maximum compressive

strength was 29.81 MPa with 12.5 mm downgraded CA and minimum compressive

strength of 20.72 MPa with 19 mm downgraded CA. The results of this study show that

compressive strength of SCC with BA increase with the increment of cement content.

However, the compressive strength increases with decreasing the size of coarse

aggregate and increasing the cement contents. This is due to the higher cement content

with smaller size of coarse aggregate that has the larger surface area which results

higher bonding strength around the aggregate particles (Pandurangan et al., 2012;

Uddin et al., 2017).

Fig. 4.22: Effect of aggregate size and cement contents on the compressive strength

of SCC at w/c of 0.35

Fig. 4.22also presents the compressive strengths 21.10 MPa, 24.41 MPa and 28.20 MPa

were found with CA content 560 kg/m3 and 27.81 MPa, 26.33 MPa and 29.81 MPa

were found with CA content 570 kg/m3, 580 kg/m3 and 550 kg/m3 respectively for 12.5

mm CA. In case of 19 mm CA, compressive strengths were found 20.72 MPa, 22.67

MPa and 24.54 MPa with CA content 560 kg/m3 and 23.08 MPa, 24.04 MPa and 25.65

MPa were found with CA content 570 kg/m3, 580 kg/m3 and 550 kg/m3 respectively.

15.00

20.00

25.00

30.00

35.00

440 470 500 530 560 590

Com

pre

ssiv

e S

tren

gth

(M

Pa)

Cement Content (kg/m3)

12.5 mm CA 19 mm CA

83

It is also observed that the compressive strength of SCC with brick aggregate decreased

with higher CA content. It may be attributed that, homogeneity of concrete decreased

with increasing the aggregate content and possessed a lower compressive strength.

Fig. 4.23 indicates the variation of compressive strength of SCC with brick aggregate

at w/c ratio of 0.40. The compressive strengths were found 20.05 MPa, 21.94 MPa,

23.23 MPa, 24.07 MPa, 20.05 MPa and 23.67 MPa with cement content 450 kg/m3,

470 kg/m3, 500 kg/m3, 530 kg/m3, 550 kg/m3 and 580 kg/m3 respectively for 12.5 mm

CA. In case of 19 mm CA, compressive strengths were found 20.24 MPa, 21.13 MPa,

21.65 MPa, 22.55 MPa, 20.05 MPa and 23.65 MPa with cement content 450 kg/m3,

470 kg/m3, 500 kg/m3, 530 kg/m3, 550 kg/m3 and 580 kg/m3 respectively. The

characteristics of the strength were found similar to the strength with w/c ratio of 0.35.

However, it is also found that the compressive strength of SCC with brick aggregate

decreased with larger size coarse aggregate.

Fig. 4.23: Effect of aggregate size and cement contents on the compressive strength

of SCC at w/c of 0.40

15.00

20.00

25.00

30.00

440 470 500 530 560 590

Com

pre

ssiv

e S

tren

gth

(M

Pa)

Cement Content (kg/m3)

12.5 mm CA 19 mm CA

84

4.6.1.2 Variation of Compressive Strength of SCC with Water Cement Ratio

and Cement Contents

The compressive strength of self- compacting concrete is also affected by water cement

ratios. The variation of the compressive strength of SCC with w/c ratio and aggregate

content are again shown in Fig. 4.24 and Fig. 4.25.

Fig. 4.24: Variation of 28 days compressive strength of SCC with 12.5 mm CA

Fig. 4.24 indicates the variation of compressive strength of SCC found in the testing of

hardened concrete made with 12.5 mm downgraded brick aggregate at w/c ratios of

0.35 and 0.40. The figure reveals that the compressive strength decreases with

increasing the water-cement ratio. The strength of concrete is a function of its porosity.

The high w/c ratio increases the consistency and fluidity of the concrete mix. During

the setting and hardening of concrete, the amount of water decreases in the hydration

process. However, air pores are formed due to excess water that reduce mechanical

strength. Air pores break the continuity of the uniformity of concrete structure.

Adding more water (increased w/c ratio), the cement paste becomes dilute and creates

more water filled pore spaces between the grains thus larger pores are formed to cover

the spatial gap (the water) between them which interface with the development of

strength. Fig 4.25 also exhibits the similar results with 19 mm downgraded coarse

aggregate.

15.00

20.00

25.00

30.00

35.00

440 470 500 530 560 590

Com

pre

ssiv

e S

tren

gth

(M

Pa)

Cement Content (kg/m3)

12.5 mm CA with w/c = 0.35 12.5 mm CA with w/c = 0.40

85

Fig. 4.25: Variation of 28 days compressive strength of SCC with 19 mm CA

In addition, the failure plane of the cylindrical specimen was observed and shown in

Fig. 4.26. The failure plane exhibits the combined failure of concrete (internal mortar-

aggregate failure) which gives a confidence to use SCC with brick aggregate in the

concrete construction. Thus, all the mixtures had satisfactory compressive strength at

28 days.

Fig. 4.26: Failure plane of concrete specimens

15.00

20.00

25.00

30.00

440 470 500 530 560 590

Co

mp

ress

ive

Str

ength

(M

Pa)

Cement Content (kg/m3)

19 mm CA with w/c = 0.35 19 mm CA with w/c = 0.40

86

4.6.2 Splitting Tensile Strength

Splitting tensile strength (fsp) is generally expressed as a function of the square root of

compressive strength (fΚΉc) and it is greater than direct tensile strength and lower than

flexural Strength. Splitting tensile strength is used in the design of structural concrete

members to evaluate the shear resistance provided by concrete and to determine the

development length of reinforcement.

Fig. 4.27: Splitting tensile strength of SCC with brick aggregate

From the results of splitting tensile strength, the following are observed as shown in

Fig. 4.27. The maximum and minimum splitting tensile strength were 2.89 MPa and

1.98 MPa.

Fig. 4.28 shows the splitting tensile strength of SCC made with brick aggregate at 28

days as a function of compressive strength. It can be seen that the splitting tensile

strength of hardened SCC with brick aggregate is linearly proportional to the

compressive strength of concrete. Analysis of test results show that the compressive

strength and splitting tensile strength are related. An increase in one generally reflected

in an increase in the other and the compressive strength was around ten times of the

splitting tensile strength. A similar result of splitting tensile strength for SCC with brick

aggregate was also reported by Roy et al. (2019).

0.00

10.00

20.00

30.00

40.00

C450A

12W

35

C470A

12W

35

C500A

12W

35

C530B

12W

35

C550C

12W

35

C580D

12W

35

C450A

19W

35

C470A

19W

35

C500A

19W

35

C530B

19W

35

C550C

19W

35

C580D

19W

35

C450A

12W

40

C470A

12W

40

C500A

12W

40

C530B

12W

40

C550C

12W

40

C580D

12W

40

C450A

19W

40

C470A

19W

40

C500A

19W

40

C530B

19W

40

C550C

19W

40

C580D

19W

40

Co

mp

ress

ive

and

Sp

liti

ng T

ensi

le S

tren

gth

(M

Pa)

Concrete Mixes

Compressive Strength Splitting Tensile Strength

87

Fig. 4.28: Relationship between compressive strength and splitting tensile strength

4.6.3 Modulus of Elasticity

Generally, the modulus of elasticity is expressed as a function of the square root of

compressive strength. The values of elastic modulus results are included in Table 4.6

and the sample graphs of the stress strain diagram of hardened concrete are included in

Appendix D.

Different codes have prescribed some empirical relations to determine the modulus of

elasticity of concrete. These relationships are shown in Table 4.8. The modulus of

elasticity of normal concrete is between 18.25 to 22.76 GPa. From the Table 4.8, it is

observed that the maximum and minimum values of modulus of elasticity were 23.91

GPa and 15.09 GPa. Due to having the lower compressive capacity of brick aggregate

concrete, the value of modulus of elasticity of SCC with brick aggregate was slightly

lower than the normal concrete.

4.7 CORRELATION BETWEEN MECHANICAL PROPERTIES

The correlations are developed by the variation of compressive strength, which stands

for different mix proportion, aggregate size and water cement ratios with the splitting

tensile strength and modulus of elasticity. The results are presented in figures and

discussed categorically. The results include the correlation between compressive

strength with the splitting tensile strength and modulus of elasticity of SCC with brick

aggregate.

fsp = 0.10f'cRΒ² = 0.7343

1.5

2

2.5

3

3.5

18.00 21.00 24.00 27.00 30.00

Sp

liti

ng

Ten

sile

Str

eng

th,

f sp

(MP

a)

Compressive Strength f'c (MPa)

88

4.7.1 Correlation between Compressive Strength and Splitting Tensile Strength

Experimental values of splitting tensile strength of SCC with brick aggregate are plotted

and shown in Fig. 4.29. The relation illustrates the splitting tensile strength

corresponding the square root of compressive strength for 28 days. From this figure it

is seen that, splitting tensile strength increases with the square root of compressive

strength. The analysis of the test values indicates the following relations [Eq. (4.7)]

with a determination coefficient of 0.65.

fsp = 0.50 βˆšπ‘“π‘β€² (4.7)

in which both units of fsp and fΚΉc are in MPa

Fig. 4.29: Correlation between compressive strength and splitting tensile strength of

SCC with brick aggregate

The expressions of the correlation suggested by many researchers for the prediction of

the splitting tensile strength of concrete are shown in Table 4.7. It can be found that the

results of the present study is similar to the SCC made with BA by Roy et al. (2019).

A study on the BA was conducted by Uddin et al. (2017) and suggested the relation

between compressive strength and splitting tensile strength. The authors find the

correlation coefficient between these are 0.72, 0.68, 0.75 and 0.53 with various sizes

CA. The equation proposed by this authors are presented in Table 4.7. The relation

suggested by JSCE (2002) indicates that the result of this study overestimate the

splitting tensile strength about 13 % compared to normal concrete. However, the

relation as suggested by this study represents 10.7% and 15.25% lower splitting tensile

strength compared to normal concrete according to ACI 318-11 (2011) and ACI 363R

fsp = 0.50√f'c

RΒ² = 0.65

1.50

1.75

2.00

2.25

2.50

2.75

3.00

4.00 4.50 5.00 5.50 6.00

Spli

ting T

ensi

le S

tren

gth

, f s

p(M

Pa)

(√f'c ) MPa

89

( 1992); and 23% lower splitting tensile strength compared to Jaber et al.(2018) for

SCC with natural aggregate and 5.6% and 27.5 % lower compared with Uddin et al.,

(2017) and Mansur et al. (1999) for SCC with normal concrete with brick aggregate

respectively.

Table 4.7: Correlation between compressive strength and splitting tensile strength

proposed by researchers

Type of concrete Suggested

expressions

Units Reference

Normal Concrete fsp = 0.44βˆšπ‘“π‘

β€²

fsp = 0.56βˆšπ‘“π‘β€²

fsp = 0.59βˆšπ‘“π‘β€²

MPa

MPa

MPa

JSCE (2002)

ACI 318-11 (2011)

ACI 363R ( 1992)

SCC with Natural

Aggregate fsp = 0.65βˆšπ‘“π‘

β€²

MPa Jaber et al.(2018)

Normal Concrete

with BA fsp = 0.45 βˆšπ‘“π‘

β€²

fsp = 0.53 βˆšπ‘“π‘β€²

fsp = 0.69 βˆšπ‘“π‘β€²

fsp = 5.7 βˆšπ‘“π‘β€²

MPa

MPa

MPa

psi

Noaman et al. (2018)

Uddin et al. (2017)

Mansur et al. (1999)

Akhtaruzzaman and A.

Hasnat (1983)

SCC with BA fsp = 0.10 𝑓𝑐′

fsp = 0.50 βˆšπ‘“π‘β€²

-

MPa

Roy et al. (2019)

Present Study

4.7.2 Correlation between Compressive Strength and Modulus of Elasticity

Experimental values of modulus of elasticity were plotted Fig. 4.30. The relation

between modulus of elasticity and the corresponding square root of compressive

strength for 28 days is shown in Equation (4.8). It is seen that the modulus of elasticity

increase with the increases of compressive strength as expected.

Es = 3640 βˆšπ‘“π‘β€² (4.8)

in where both Es and fΚΉc are in MPa

The expressions suggested by researchers for the prediction modulus of elasticity

concrete are shown in Table 4.8. The expression presented by this study indicates that

the modulus of elasticity of SCC with brick aggregate is 15.1%, 12.25% and 13.2%

higher than that of Noaman et al. (2018), Uddin et al. (2017) and Mia et al. (2015). On

the other hand, Mansur et. al. [1999] reported approximately 10% and BNBC (2006)

indicates 2.93 % lower the initial tangent modulus for SCC with normal brick aggregate

concrete. The modulus of elasticity of SCC with brick aggregate were found about 23%

90

lower than the natural aggregate concrete that predicted by following the specifications

of BNBC (2006), JSCE (2002) and ACI 318-11 (2011)

Fig. 4.30: Correlation between compressive strength and modulus of elasticity of

SCC with brick aggregate

Table 4.8: Correlation between compressive strength and modulus of elasticity

proposed by researchers

Type of

concrete

Suggested

expressions

Units Reference

Normal

Concrete

Ec = 4700βˆšπ‘“π‘β€²

Ec = 4700βˆšπ‘“π‘β€²

Ec = 4730βˆšπ‘“π‘β€²

MPa

MPa

MPa

BNBC (2006)

JSCE (2002)

ACI 318-11 (2011)

Normal

Concrete

with BA

Ec =3087βˆšπ‘“π‘β€²

Ec =3194βˆšπ‘“π‘β€²

Ec =3750βˆšπ‘“π‘β€²

Ec =3215βˆšπ‘“π‘β€²

Ec = 4050 βˆšπ‘“π‘β€²

Ec = 37500 βˆšπ‘“π‘β€²

Ec = 40000 βˆšπ‘“π‘β€²

MPa

MPa

MPa

MPa

MPa

psi

psi

Noaman et al. (2018)

Uddin et al. (2017)

BNBC (2006)

Mia et al. (2015)

Mansur et al. (1999)

Rashid et al. (2008)

Akhtaruzzaman and Hasnat(1983)

SCC

with BA

Ec = 3640 βˆšπ‘“π‘β€² MPa Present Study

EC = 3,640 √f'c

10,000

15,000

20,000

25,000

4.00 4.50 5.00 5.50 6.00

Mo

du

lus

of

Ela

stic

ity,

EC

(MP

a)

√f'c (MPa)

91

4.8 SUMMARY

This chapter summarized all the experimental test results including different physical

and chemical properties of materials. In addition to that, fresh properties of SCC mixes

with brick aggregate are described and the correlation between these properties have

been demonstrated. The mechanical properties (compressive strength, splitting tensile

strength and modulus of elasticity) and their correlations are described and compared

with the normal concrete made with brick aggregate. Comparative study with previous

research findings also has been carried out.

It is observed that the properties of SCC related to workability requirements for

successful placement of concrete exhibits excellent deformation ability and proper

stability to flow under its own weight without segregation and blockage. Also the

properties of the hardened concrete exhibit satisfactory performance in the laboratory

results. Therefore, SCC can be used as a new construction material with locally

available brick aggregate as coarse aggregate.

92

CHAPTER 5 CHAPTER V …...…

C CONCLUSIONS AND RECOMMENDATIONS

5.1 INTRODUCTION

This thesis work has examined the fresh and mechanical properties of self-compacting

concrete with crushed brick as coarse aggregate. The overall findings reveal that SCC

has met all the requirements as a new construction material in the laboratory with

locally available brick aggregate. The main factors controlling the fresh and mechanical

properties of SCC have been investigated. This chapter provides overall conclusions of

the research findings, contributions of the present study and proposes several

recommendations for future study.

5.2 CONCLUSIONS

The research work concentrated on fresh and mechanical properties of self-compacting

concrete with crushed brick as coarse aggregate. From the test results and analysis, the

following conclusions can be drawn.

5.2.1 Fresh Properties of SCC with Brick Aggregate

(i) The SCC mixes with brick aggregate were developed successfully based

on the trial mixes using different w/c ratios, aggregate contents, and

superplasticizer for both 12.5 mm and 19 mm downgraded brick

aggregates.

(ii) Slump flow and J-ring flow increased with increasing w/c ratio and

decreased with increasing aggregate content.

(iii) Slump flow, J-ring flow and T50 flow time indicated better results for

12.5 mm downgraded brick aggregate over 19 mm downgraded brick

aggregate in all cases.

(iv) Results of the Slump flow, T50 flow time and V-funnel flow time were

found to be satisfactory according to EFNARC and indicated good

filling ability of SCC with brick aggregate.

(v) J-ring flow and L-box test results indicates that SCC mixes with BA

possessed good passing ability. Thus, SCC with brick aggregate can be

used in the congested area of the reinforcement.

(vi) L-box test on the SCC mixtures with brick aggregate indicated that the

mixtures possessed good passing ability. The values of blocking ratio

for all mixes indicates very good passing ability. Thus SCC with brick

93

aggregate can be used where the flow of concrete needed through the

congested reinforcement.

(vii) There was no visible blocking and segregation in the L-box, J-ring and

V-funnel at T5 minutes tests.

(viii) There are good correlations observed between slump flow, J-ring flow

and T50 flow time.

(ix) All parameters of the fresh properties of SCC with brick aggregate

indicate very good passing ability and filling ability according to

standard guideline of EFNARC.

From above discussion it may be concluded that brick aggregate can be an alternate

source of coarse aggregate for the production of SCC to meet the present demand of

construction facilities.

5.2.2 Mechanical Properties of SCC with Brick Aggregate

(i) Compressive strength of SCC with brick aggregate increased with lower

sizes of coarse aggregate.

(ii) Higher water cement ratio possessed lower compressive strength of

hardened SCC.

(iii) Compressive strength of SCC with brick aggregate decreased with higher

aggregate content.

(iv) The maximum and minimum compressive strength of hardened SCC with

brick aggregate have satisfied the required strength according to BNBC

for earthquake resistant structure.

(v) Splitting tensile strength of hardened SCC with brick aggregate is directly

proportional to the compressive strength of hardened concrete.

(vi) Compressive strength and splitting tensile strength are related, and

compressive strength was about ten times of the splitting tensile strength

for SCC with brick aggregate. Eq. 4.7 can be used to determine the

splitting tensile strength of SCC with brick aggregate.

(vii) Modulus of elasticity for SCC with brick aggregate is proportional to the

compressive strength of hardened concrete.

(viii) It was found that the values of modulus of elasticity for SCC with brick

aggregate were about 2.93% lower than that of BNBC (2006) for normal

brick aggregate concrete and 23% lower than that of ACI Code (2011)

expression. Eq. 4.8 may be used to predict the modulus of elasticity of

SCC with brick aggregate.

94

Therefore, the properties of the hardened state of SCC with brick aggregate gives a

confidence to use SCC with brick aggregate in the concrete construction in Bangladesh.

5.3 CONTRIBUTION OF THE STUDY

The present study has contributed to the present state of knowledge of the fresh and

mechanical properties of SCC with brick aggregate. The main contributions of this

research are as follows:

(i) Demonstration of the successful production of SCC with brick

aggregate as a new construction material.

(ii) An approach for the proportioning of SCC mixes with brick aggregate

to find the necessary fresh properties.

(iii) Determination of mechanical properties of hardened SCC with brick

aggregate which will be helpful for the structural use of concrete.

(iv) Investigation and explanation of the fresh and mechanical properties

which can be used to predict the behavior of SCC with brick aggregate.

(v) Enhancement of new research area and idea about the properties of

SCC with brick aggregate.

5.4 RECOMMENDATIONS FOR FUTURE STUDY

From the results obtained and the knowledge gained about SCC with brick aggregate,

the following aspects that were not investigated in the present study can be

recommended for future works:

1) It would be recommended to have more trial mixes with water/powder

ratios in the range of 0.45 to 0.50, both for 12.5 mm and 19 mm

downgraded sizes of aggregate without a viscosity modifying agent.

2) There are needed more trial mixes with various coarse and fine

aggregates contents for a fixed cement content in case of water cement

ratios of 0.35, 0.40, 0.45 and 0.50 for both 12.5 mm and 19 mm

downgraded brick aggregates.

3) It would be interesting to use different superplasticizers with different

dosages.

4) Different additives can be used in the preparation of SCC with brick

aggregates to increase the paste volume in concrete.

5) Supplementary cementitious materials can be added as a partial

replacement of cement and the behavior of SCC can be observed.

6) Recycling brick aggregates can be used as partial replacement of virgin

brick aggregates in the preparation of SCC.

95

7) Microstructures of the SCC with brick aggregate can be analyzed based

on their scanning electron micrographs (SEMs).

8) High strength SCC with brick aggregate can be produced with changing

the proportion of the materials.

9) Flexural strength and Poisson’s ratio of SCC brick aggregate can be

determined for the hardened concrete.

10) It would be advisable to evaluate the durability properties (water

absorption, porosity, sulfate and chloride resistance) of SCC with brick

aggregates

11) It would be interesting to establish design charts of the mix design

method for proportioning SCC mixes with brick aggregate.

12) The role of composition parameters (coarse aggregate volume, paste to

solids and water to binder ratios of SCC mixes with different ratios of

fibers on the properties of SCC with brick aggregate can be studied.

13) The cement, fly ash, HRWR, and air entrainment could be changed in

different mixes to compare all of the results.

96

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104

APPENDICES

APPENDIX-A

PHOTOGRAPHS OF THE INGREDIENTS

Fig. A1: Coarse Aggregate

Fig. A2: Fine Aggregate and Admixture

Fig. A3: Mixing Machine

12.5 mm CA 19 mm CA

105

Fig. A4: Slump Flow

Fig. A4: J-ring Flow and V-funnel Flow

106

Fig. A5: L-box Test

Fig. A6: Hardened Concrete

107

Fig. A7: Surface of the Hardened Concrete

Fig. A8: Splitting Tensile Strength

108

Fig. A10: Failure Surface of the Hardened Concrete after Splitting Tensile Strength

Test

109

Fig. A11: Compressive Strength and modulus of Elasticity Test

Fig. A10: Failure Surface of the Hardened Concrete after Compressive Strength Test

110

APPENDIX-B

ANALYSIS AND RESULTS OF THE PROPERTIES OF THE AGGREGATES

Table B1: FM test of 12.5 mm Downgraded Coarse Aggregate

Sieve

Size

Weight

Retained

(gm)

Percent

Retained

Cumulative

Percent

Retained

% Finer FM

3" 0.00 0.00 0.00 100.00

6.56

1.5" 0.00 0.00 0.00 100.00

3/4" 218.00 4.36 4.36 95.64

3/8" 2370.00 47.40 51.76 48.24

#4 2386.00 47.72 99.48 0.52

#8 26.00 0.52 100.00 0.00

#16 0.00 0.00 100.00 0.00

#30 0.00 0.00 100.00 0.00

#50 0.00 0.00 100.00 0.00

#100 0.00 0.00 100.00 0.00

Pan 0.00 - - -

Sum 5000.00 - 655.60

-

Table B2: ASTM Limits for12.5 mm Downgraded Coarse Aggregate

Sieve Size

(mm)

Percent Finer

12.5 mm Downgraded

CA

ASTM Lower

Limit

ASTM Upper

Limit

76 100 100 100

37.5 100 100 100

20 96 100 100

9.5 48 40 70

4.75 1 0 15

2.36 0 0 5

111

Table B3: Water Absorption Test of Coarse Aggregate (12.5 mm downgrade)

Sample

Identification

Mark

Weight in Oven dry

Condition

Weight in SSD

condition

Water Absorption

Capacity

(gm) (gm) (%)

CA-12.5 4173 5000 19.8

Table B4: Field Moisture Test of Coarse Aggregate (12.5 mm downgrade)

Sample

Identification

Mark

Weight in Oven dry

Condition

Weight in Field

condition

Water Absorption

Capacity

(kg) (kg) (%)

CA-12.5 18.62 20.00 7.42

Table B5: Unit Weight Test of Coarse Aggregate (12.5 mm downgrade)

Sample

Identification

Mark

Weight of Mold +

Coarse aggregates

Weight of

Mold

Volume of

Mold

Unit weight

(kg/m3)

(kg) (kg) (m3) (%)

CA-12.5 8.27 6.75 0.001647 923

Table B6: Specific Gravity Test of Coarse Aggregate (12.5 mm downgrade)

Oven dry

weight

Saturated

surface dry

weight in air

Weight of

aggregate in

water

Bulk

specific

gravity

(Dry)

Bulk

specific

gravity

(SSD) (gm) (gm) (gm)

5000 5985 3096 1.73 2.07

112

Table B7: Report on the Tests of Elongation Index (12.5 mm)

BS Test Sieve

Size, Passing

BS Test Sieve

Size,

Retaining

Weight

Retained

Percentage

Retained

Weight of

Elongated

Particles

Weighted

Elongation

Index

mm mm gm % gm %

50.0 37.5 0.0 0.0 0.0 0.0

37.5 28.0 0.0 0.0 0.0 0.0

28.0 20.0 268.0 5.6 0.0 0.0

20.0 14.0 1584.0 33.2 100.0 2.0

14.0 10.0 1958.0 41.0 327.0 6.6

10.0 6.3 967.0 20.2 145.0 2.9

Total Weight = 4777.0 100.0 572.0 11.6

Table B8: Report on the Tests of Flakiness Index (12.5 mm)

BS Test Sieve

Size, Passing

BS Test Sieve

Size, Retaining

Weight

Retained

Percentage

Retained

Weight of

Flaki

Particles

Weighted

Flakiness

Index

mm mm gm % gm %

50.0 37.5 0.0 0.0 0.0 0.0

37.5 28.0 0.0 0.0 0.0 0.0

28.0 20.0 268.0 5.6 43.0 0.9

20.0 14.0 1584.0 33.2 185.0 3.8

14.0 10.0 1958.0 41.0 222.0 4.5

10.0 6.3 967.0 20.2 81.0 1.6

Total Weight = 4777.0 100.0 531.0 10.8

113

Table B10: Gradation of Coarse Aggregate (19 mm downgraded)

Sieve Size Weight

Retained (gm)

Percent

Retained

Cumulative

Percent

Retained

% Finer FM

3" 0.00 0.00 0.00 100.00

6.79

1.5" 0.00 0.00 0.00 100.00

3/4" 545.00 10.90 10.90 89.10

3/8" 2897.00 57.94 68.84 31.16

#4 1517.00 30.34 99.18 0.82

#8 26.00 0.52 99.70 0.30

#16 15.00 0.30 100.00 0.00

#30 0.00 0.00 100.00 0.00

#50 0.00 0.00 100.00 0.00

#100 0.00 0.00 100.00 0.00

Pan 0.00 - - -

Sum 5000.00 - 678.62 -

Table B11: ASTM Upper and Lower Limit for CA

Sieve

Size

(mm)

Percent Finer

19 mm Downgraded

CA

ASTM Lower

Limit

ASTM Upper

Limit

76 100 100 100

37.5 100 100 100

19 89 90 100

9.5 31 20 55

4.75 1 0 10

2.36 0 0 5

Table B12:Water Absorption Test of Coarse Aggregate (19 mm downgrade)

Sample

Identification

Mark

Weight in Oven dry

Condition

Weight in SSD

condition

Water Absorption

Capacity

(gm) (gm) (%)

CA-19 4177 5000 19.7

114

Table B13: Field Moisture Test of Coarse Aggregate (19 mm downgrade)

Sample

Identification

Mark

Weight in Oven dry

Condition

Weight in Field

condition

Water Absorption

Capacity

(kg) (kg) (%)

CA-19 18.62 20.00 7.41

Table B14: Unit Weight Test of Coarse Aggregate (19 mm downgrade)

Sample

Identification

Mark

Weight of Mold +

Coarse aggregates

Weight of

Mold

Volume of

Mold

Unit weight

(kg/m3)

(kg) (kg) (m3) (%)

CA-19 8.26 6.75 0.001647 917

Table B15: Specific Gravity Test of Coarse Aggregate (19 mm downgrade)

Oven dry

weight

Saturated

surface dry

weight in air

Weight of

aggregate in

water Bulk specific

gravity (Dry)

Bulk specific

gravity (SSD)

(gm) (gm) (gm)

5000 5985 3096 1.73 2.07

115

Table B16: Report on the Tests of Elongation Index (19 mm)

BS Test Sieve

Size, Passing

BS Test Sieve

Size,

Retaining

Weight

Retained

Percentage

Retained

Weight of

Elongated

Particles

Weighted

Elongation

Index

mm mm gm % gm %

50.0 37.5 0.0 0.0 0.0 0.0

37.5 28.0 0.0 0.0 0.0 0.0

28.0 20.0 1040.0 21.1 34.0 0.7

20.0 14.0 2465.0 50.0 298.0 6.0

14.0 10.0 1157.0 23.5 215.0 4.4

10.0 6.3 269.0 5.5 74.0 1.5

Total Weight = 4931.0 100.0 621.0 12.6

Table B17: Report on the Tests of Flakiness Index (19 mm)

BS Test Sieve

Size, Passing

BS Test Sieve

Size, Retaining

Weight

Retained

Percentage

Retained

Weight of

Flaky

Particles

Weighted

Flakiness

Index

mm mm gm % gm %

50.0 37.5 0.0 0.0 0.0 0.0

37.5 28.0 0.0 0.0 0.0 0.0

28.0 20.0 1040.0 21.1 158.0 3.2

20.0 14.0 2465.0 50.0 204.0 4.1

14.0 10.0 1157.0 23.5 149.0 3.0

10.0 6.3 269.0 5.5 28.0 0.6

Total Weight = 4931.0 100.0 539.0 10.9

116

Table B18: Sieve Analysis of Fine Aggregate

Sieve No. Weight

Retained (gm)

Percent

Retained

Cumulative

Percent

Retained

FM

4 0.0 0.00 0.00

2.81

8 25.0 5.00 5.00

16 84.0 16.80 21.80

30 220.0 44.00 65.80

50 116.0 23.20 89.00

100 50.0 10.00 99.00

Pan 5.0 - -

Total 500.0 - 280.60

Table B 19: ASTM upper and lower limit for FA

Sieve Size (mm) Percent Finer

Fine Aggregate ASTM Lower Limit ASTM Upper Limit

4.75 100 95 100

2.36 95.00 80 100

1.18 78.20 50 85

0.6 34.20 25 60

0.3 11.00 5 30

0.15 1.00 0 10

Table B20: Field Moisture Test of Coarse Sand

Sample

Identification

Mark

Weight in Oven dry

Condition

Weight in Field

condition

Water Absorption

Capacity

(kg) (kg) (%)

FA 19.93 20.00 0.35

Table B21: Water Absorption Test of Coarse Sand

Sample

Identification

Mark

Weight in Oven dry

Condition

Weight in SSD

condition

Water Absorption

Capacity

(gm) (gm) (%)

FA 495 500 1.0

117

Table B22: Unit Weight Test of Coarse Sand

Sample

Identification

Mark

Weight of Mold +

Fine aggregates

Weight of

Mold

Volume of

Mold

Unit weight

(kg/m3)

(kg) (kg) (m3) (%)

FA 9.24 6.75 0.001647 1512

Table B23: Specific Gravity Test of Coarse Sand

Oven dry

weight

Saturated

surface dry

weight in

air

Weight of

flask +

water

Weight of

flask +

water +

sample

Apparent

specific

gravity

Bulk

specific

gravity

(Dry)

Bulk

specific

gravity

(SSD) (gm) (gm) (gm) (gm)

99 100 369 431 2.68 2.61 2.63

Table B24: Compressive Strength of Brick

Sample

No.

Average Cross

Sectional Area Crushing Load

Crushing

Strength

Average Crushing

Strength of

Individual Brick

(mm2) (kN) (MPa) (MPa)

1A 13572 102 7.5 7.2

1B 13225 90 6.8

2A 13216 126 9.5 8.8

2B 12882 104 8.1

3A 12544 100 8.0 8.0

3B 12432 101 8.1

4A 12426 118 9.5

9.6

4B 11752 113 9.6

118

APPENDIX-C

SUMMARY OF THE TEST RESULTS

Table C1: Mix Proportion of SCC with BA

Specimen ID

Coarse

Aggregate

Type

w/b

ratio

Cement

(kg)

Coarse

Aggregate

(kg)

Fine

Aggregate

(kg)

Water

(kg)

HRWR

%

C450A12W35 12.5 mm

0.35

450 560 980 157.5 1.5

C470A12W35 12.5 mm 470 560 980 164.5 1.4

C500A12W35 12.5 mm 500 560 980 175 1.6

C530B12W35 12.5mm 530 570 944 186 1.4

C550C12W35 12.5mm 550 580 970 193 1.4

C580D12W35 12.5mm 580 550 890 203 1.6

C450A19W35 19 mm 450 560 980 157.5 1.4

C470A19W35 19 mm 470 560 980 164.5 1.4

C500A19W35 19mm 500 560 980 175 1.6

C530B19W35 19 mm 530 570 944 186 1.5

C550C19W35 19 mm 550 580 970 193 1.4

C580D19W35 19 mm 580 550 890 203 1.6

C450A12W40 12.5 mm

0.4

450 560 980 180 1.4

C470A12W40 12.5 mm 470 560 980 188 1.4

C500A12W40 12.5 mm 500 560 980 200 1.4

C530B12W40 12.5mm 530 570 944 212 1.4

C550C12W40 12.5mm 550 580 970 220 1.4

C580D12W40 12.5 mm 580 550 890 232 1.4

C450A19W40 19 mm 450 560 980 180 1.4

C470A19W40 19 mm 470 560 980 188 1.4

C500A19W40 19mm 500 560 980 200 1.4

C530B19W40 19 mm 530 570 944 212 1.4

C550C19W40 19 mm 550 580 970 220 1.4

C580D19W40 19 mm 580 550 890 232 1.4

119

Table C2: Fresh Properties of SCC with BA

Specimen ID

Filling ability Passing ability Segregation

Resistance

SF1

(mm)

T502

(s)

Tv3

(s)

JF4

(mm)

BI5

(mm)

JF6

(mm) BR7

Tv58

(s) +

C450A12W35 590 4.5 7.5 565 25 10 0.89 +2.9

C470A12W35 610 4.3 7 580 30 9 0.93 +2.3

C500A12W35 640 3.85 7.5 605 35 8 0.95 +2.5

C530B12W35 630 3.6 6.5 615 15 3 0.98 +2.7

C550C12W35 620 3.56 6.3 595 25 4 0.99 +2.5

C580D12W35 660 4 8.1 620 40 4.5 1.00 +3

C450A19W35 580 4.8 6.8 560 20 8 0.96 +2.9

C470A19W35 605 4.6 6.8 580 25 8 0.95 +3.2

C500A19W35 610 4.5 6.6 580 30 7 0.98 +3.5

C530B19W35 615 4.3 6.5 570 45 9 0.98 +3.5

C550C19W35 610 4 6.5 555 55 9 0.88 +3.5

C580D19W35 620 4.5 6.4 585 35 6 0.98 +2

C450A12W40 610 4 7 585 25 9 0.88 +3.9

C470A12W40 620 3.8 6.5 595 25 6 0.90 +3.6

C500A12W40 650 3.4 6 610 40 5 0.95 +2.4

C530B12W40 640 3.6 5.8 600 40 8 0.95 +2.3

C550C12W40 640 3.56 5.8 610 30 9 0.90 +2.5

C580D12W40 670 3 6.5 650 20 3 0.98 +2.5

C450A19W40 595 4.2 6.1 570 25 10 0.94 +2.3

C470A19W40 620 3.9 6.2 597 23 9 0.92 +2.8

C500A19W40 640 4.1 6.5 600 40 6 0.90 +3.0

C530B19W40 640 4.3 6.2 610 30 9 0.90 +3.0

C550C19W40 630 3.9 6 590 40 10 0.88 +3.1

C580D19W40 650 3.8 7.5 610 40 7 0.95 +2.5

120

Table C3: Mechanical Properties of Hardened SCC with brick aggregate

Specimen ID

Compressive

Strength, f'c

(MPa)

Splitting

Tensile

Strength, fsp

(MPa)

Modulus of

Elasticity, Ec

(GPa)

C450A12W35 21.10 2.08 16.75

C470A12W35 24.41 2.48 18.02

C500A12W35 28.20 2.81 19.05

C530B12W35 27.81 2.73 23.91

C550C12W35 26.33 2.47 21.75

C580D12W35 29.81 2.89 16.94

C450A19W35 20.72 2.12 16.64

C470A19W35 22.67 2.29 17.33

C500A19W35 24.54 2.41 20.75

C530B19W35 23.08 2.21 15.09

C550C19W35 24.04 2.33 19.44

C580D19W35 25.65 2.59 19.76

C450A12W40 20.05 2.1 16.30

C470A12W40 21.94 2.23 17.11

C500A12W40 23.23 2.42 15.11

C530B12W40 24.07 2.45 16.72

C550C12W40 20.10 2.46 16.22

C580D12W40 24.06 2.46 18.33

C450A19W40 20.24 2.07 16.37

C470A19W40 21.13 2.11 16.75

C500A19W40 21.65 1.98 16.25

C530B19W40 22.55 2.25 15.92

C550C19W40 20.05 2.02 15.57

C580D19W40 23.67 2.64 15.38

121

APPENDIX-D

STRESS-STRAIN GRAPHS OF CYLINDRICAL SPECIMENS

Fig. D1: Typical Stress-Strain Diagram of SCC with BA

Fig. D1: Typical Stress-Strain Diagram of SCC with BA

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

0.000000 0.000500 0.001000 0.001500 0.002000

Str

ess

(psi

)

Strain

0

500

1000

1500

2000

2500

3000

0.000000 0.000500 0.001000

Str

ess

(psi

)

Strain

122

Fig. D1: Typical Stress-Strain Diagram of SCC with BA

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

0.000000 0.000500 0.001000 0.001500 0.002000 0.002500 0.003000

Str

ess

(psi

)

Strain