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Focused Ion Beam Thomas unthner Generating a FIB FIB- Applications Presentation talk FOCUSED ION BEAM (FIB) Thomas G¨ unthner TU M¨ unchen 19 th January 2009

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Focused IonBeam

ThomasGunthner

Generating aFIB

FIB-Applications

Presentation talk

FOCUSED ION BEAM(FIB)

Thomas Gunthner

TU Munchen

19th January 2009

Focused IonBeam

ThomasGunthner

Generating aFIB

FIB-Applications

Overview

1 Generating a focused ion beamIon sourcesIon optics

2 FIB-ApplicationsScanning ion microscopy (SIM)Focused ion beam lithography

ResistlithographyMicromachining

Focused IonBeam

ThomasGunthner

Generating aFIB

Ion sources

Ion optics

FIB-Applications

Generating a focused ionbeam

Focused IonBeam

ThomasGunthner

Generating aFIB

Ion sources

Ion optics

FIB-Applications

Sample of a FIB-system

Figure: http://www.fzd.de/db/PicOri?pOid=24361, 01/17/2009

Focused IonBeam

ThomasGunthner

Generating aFIB

Ion sources

Ion optics

FIB-Applications

Ion sources

Gas field ion source (GFIS)

Liquid metal ion source (LMIS)

(Plasma ion gun)

Focused IonBeam

ThomasGunthner

Generating aFIB

Ion sources

Ion optics

FIB-Applications

Gas field ion sources (GFIS)

Figure: http://www.smt.zeiss.com/nts, 01/17/2009

Source tip needle-shaped ⇒ E ∼ 1010 Vm

Imaging Gas ionized at tip as electron tunnels into the tip

Ions accelerated to the extractor

Virtual source size δ < A possible

Focused IonBeam

ThomasGunthner

Generating aFIB

Ion sources

Ion optics

FIB-Applications

Liquid metal ion sources (LMIS)

Figure: http://www.freepatentsonline.com, 01/17/2009

Figure: http://www.ehdtg.com/images, 01/17/2009

Atoms form a“Taylor-Cone”(end radius∼ 101nm ⇒very strongelectric field E )

Electric fieldionize atoms

Virtual sourcesize δ ≈ 50nm

Focused IonBeam

ThomasGunthner

Generating aFIB

Ion sources

Ion optics

FIB-Applications

Liquid metal ion sources (LMIS)

Figure: http://www.freepatentsonline.com, 01/17/2009

Figure: http://www.ehdtg.com/images, 01/17/2009

Atoms form a“Taylor-Cone”(end radius∼ 101nm ⇒very strongelectric field E )

Electric fieldionize atoms

Virtual sourcesize δ ≈ 50nm

Focused IonBeam

ThomasGunthner

Generating aFIB

Ion sources

Ion optics

FIB-Applications

Ion optics

Electrostatic lens system:

Condensor lens: parallelize,creates crossover in E× Bmass filter or apertureObjective lens: focus atsample

Aperture: reduces ion beamcurrent, spherical aberration,helps mass separating

E×B mass filter (Wien filter):separates ions after mass andcharge if an alloy is used (onlyLMIS)

Focused IonBeam

ThomasGunthner

Generating aFIB

Ion sources

Ion optics

FIB-Applications

Further features

Deflector plates: Steering ionbeam over sample with eletricfields in x- and y-direction(compare oscilloscope)

Beam blanker: Deflects ionbeam so much that it will notpenetrate the sample

Focused IonBeam

ThomasGunthner

Generating aFIB

FIB-Applications

SIM

FIB lithography

Resistlithography

Micromachining

FIB-Applications

Focused IonBeam

ThomasGunthner

Generating aFIB

FIB-Applications

SIM

FIB lithography

Resistlithography

Micromachining

Scanning ion microscopy (SIM)

SIM is very similar to SEM (see electron microscopy)

Figure: http://www.crystaltexture.com/jpg 01/17/2009

Detected particles: low-energy secondary electrons(< 10eV ), secondary ions and photons

Focused IonBeam

ThomasGunthner

Generating aFIB

FIB-Applications

SIM

FIB lithography

Resistlithography

Micromachining

Properties of SIM

Ion mass � electron mass⇒ λIon � λe− ⇒ almost nodiffraction if an ion beam is used

Figure:http://www.smt.zeiss.com/nts,01/17/2009

⇒ currently best resolution: 0.24nmIon beam modifies sample during observation (sputteredions)

Focused IonBeam

ThomasGunthner

Generating aFIB

FIB-Applications

SIM

FIB lithography

Resistlithography

Micromachining

Properties of SIM

Ion mass � electron mass⇒ λIon � λe− ⇒ almost nodiffraction if an ion beam is used

Figure:http://www.smt.zeiss.com/nts,01/17/2009

⇒ currently best resolution: 0.24nmIon beam modifies sample during observation (sputteredions)

Focused IonBeam

ThomasGunthner

Generating aFIB

FIB-Applications

SIM

FIB lithography

Resistlithography

Micromachining

Properties of SIM

Secondary electrons much moresensitive to details of surfacestructure in the target than inSEM, sensitive to work functionof surface

Using ion-induced secondaryions and electrons to gain muchinformation of the sample

Chemical surface analysis bymeans of secondary ions

Figure:http://bp1.blogger.com/rWWz5HvJNko/RYVRwwxZ2I/AAAAAAAAABE,01/17/2009

Focused IonBeam

ThomasGunthner

Generating aFIB

FIB-Applications

SIM

FIB lithography

Resistlithography

Micromachining

Properties of SIM

Very strong contrast with ion-induced secondary electronimages in case of crystalline targets

Figure: http://www.crystaltexture.com/jpg, 01/17/2009

Focused IonBeam

ThomasGunthner

Generating aFIB

FIB-Applications

SIM

FIB lithography

Resistlithography

Micromachining

Focused ion beam lithography (FIBL)

FIBL includes:

Resistlithography

Micromachining

Focused IonBeam

ThomasGunthner

Generating aFIB

FIB-Applications

SIM

FIB lithography

Resistlithography

Micromachining

Resistlithography

Works similar as electron beam lithography

Figure: http://www.techbriefs.com/images/stories/techbriefs/2007, 01/17/2009

Focused IonBeam

ThomasGunthner

Generating aFIB

FIB-Applications

SIM

FIB lithography

Resistlithography

Micromachining

Resistlithography

Thickness of resist adjusted to range of ion beam

Avoid doping by using a two layer resist system

No proximity effect (compare e-beam)

Possible resolution: 20− 30nm

Focused IonBeam

ThomasGunthner

Generating aFIB

FIB-Applications

SIM

FIB lithography

Resistlithography

Micromachining

Micromachining

Creating nanometer structures by

sputtering material from a surface

induce deposition on a surface

Applications:

Failure analysis

Lithographic mask repair

Modification and repair of integrated circuits

Focused IonBeam

ThomasGunthner

Generating aFIB

FIB-Applications

SIM

FIB lithography

Resistlithography

Micromachining

Sputtering

Figure: http://www.eaglabs.com/training/tutorials/sims-theory-tutorial, 01/17/2009

Focused IonBeam

ThomasGunthner

Generating aFIB

FIB-Applications

SIM

FIB lithography

Resistlithography

Micromachining

Sputtering

Figure: Walter Schottky Institut, E24

Focused IonBeam

ThomasGunthner

Generating aFIB

FIB-Applications

SIM

FIB lithography

Resistlithography

Micromachining

Deposition

Figure: http://cim.aamu.edu/Activities, 01/17/2009

Deposition induced by ion beam

Focused IonBeam

ThomasGunthner

Generating aFIB

FIB-Applications

SIM

FIB lithography

Resistlithography

Micromachining

Deposition

Figure: Walter Schottky Institut, E24

Focused IonBeam

ThomasGunthner

Generating aFIB

FIB-Applications

SIM

FIB lithography

Resistlithography

Micromachining

Deposition

Focused IonBeam

ThomasGunthner

Generating aFIB

FIB-Applications

Literature

J.Orloff, High-resolution focused ion beams, Rev.Sci.Instrum.64,1105(1993)

M. Hillmann, 3-dimensionale Nanostrukturierung mittels fokussierterIonenstrahllithographie, (2001)

http://www.smt.zeiss.com

http://www.freepatentsonline.com/6531811-0-large.jpg

http://physics.pdx.edu/ esanchez/Research/ChargedBeam

http://www.ehdtg.com/images

http://www.fzd.de/db/PicOri?pOid=24361

http://bp1.blogger.com/rWWz5HvJNko/

http://www.crystaltexture.com/jpg

http://www.techbriefs.com/images/stories/techbriefs/2007

http://cim.aamu.edu/Activities