flff/00002 - us environmental protection agency · substances contingency plan ... site...

FEDERAL ON-BCENE COORDINATOR'S REPORT

LAKIN STAVE FARM

CAMP CONLEY, MASON COUNT*, WEST VIRGINIA

CERCLA REMOVAL ACTIVITY

August 5, 1987 to August 7, 1987

6ERAREGION IIIEMERGENCYRESPONSEPTEAM .

Bentow H. Wilmoth, OSCUnited states Environmental Protection Agency

.Region IIIWheeling, Heat Virginia

flff/00002

TABLE OF CONTENTS

PACTS SHEET

FOREWORD

I. INTRODUCTIONA. Initial Situation/Nature of the IncidentB. Site Locationc. Efforts to Obtain Cleanup by Potential

Responsible Party

II. ROSTER OF AGENCIES, ORGANIZATIONS AND INDIVIDUALSORGANIZATION OF THE RESPONSE

III. NARRATIVE OF EVENTS

IV. RESOURCES COMMITTEDA. Initial Funding RequestB. Total Cost Summary (Estimated)

V. EFFECTIVENESS OF THE REMOVALA. Activities of Various Agencies

1. Potential Responsible Party2. State and Local Forces3. Federal Agencies and Special Forces4. Contractors

B. Disposal Methods and Quantities RemovedVI. CHRONOLOGY OF EVENTS

VII. PROBLEMS ENCOUNTERED AND RECOMMENDATIONS

VIII. LEGAL ASPECTS

APPENDICES

A. MapsB. Special Bulletin Ac. site Safety ProtocolD. Analytical ResultsE. CorrespondenceF. Background Information/state ReportsG. photographic DocumentationH. POLREPsI. Delivery Order/Procurement RequestsJ. Manifests

REGION III PROJECT NO. 179CERCLA IMMEDIATE REMOVAL ACTION ________________ FACTS SHEET

SITE: Lakin State Farm PCB Capacitors site

SIZE: Less than 1 acre

LOCATION: Camp Conley, Mason County, West Virginia

APPROVAL DATE: August 5, 1987

PROJECT DATES: August 5, 1987 to August 7, 1987

DESCRIPTION: The Lakin State Farm Site wasformerly owned by West VirginiaUniversity and used to grow cropsfor experimental purposes. The sitebecame of concern when the farmmanager reported that certain areasof the corn crop displayed abnormalgrowth patterns. In addition thefarm manager reported several drumsof electrical equipment was stagedon site in an unsecured manner. Anassessment by TAT on June 1, 1987revealed high concentrations of PCB(12,000 ppm) in several capacitorsstored on site and in the soilsurrounding the capacitors. Soilanalysis to determine abnormalgrowth patterns in the corn cropwere inconclusive. On August 5,1987 the osc utilized his Delegationof Authority to obtain $50K inCERCLA monies to mitigate the directcontact threat posed by the PCBS.

HAZARDOUS MATERIALS: Polychlorinated biphenyls (PCBs) incapacitor oil and contaminated soiland grease.

QUANTITIES REMOVED: Nine (9) PCB capacitors, seven (7)drums of contaminated soil andgrease, one drum of contaminated sitematerial.

ON-SCENE COORDINATOR (OSC): Benton Wilmoth, EPA Region III,Wheeling, WV

REMOVAL CONTRACTOR: AMO Pollution Services, Inc.,canonsburg, PA

DISPOSAL LOCATION: Temporary Storage at:AMO Pollution ServicesTSD from August l, 1987 toDecember 14, 1987. ManifestDPAB3320343

Final Disposal at:APTUS, Coffeeville, Kansas,PA Manifest jfPAB-4643041

PROJECT CEILING: $50,000.00

PROJECT COST: $18,255.00

Benton Wilmoth, oscU.S. EPA, Region IIIWheeling, WV

FOREWORD

The OSC, as mandated in the National Oil and HazardousSubstances Contingency Plan (NCP) , is required to provide acoordinated Federal response capability at the scene of a suddendischarge of oil or hazardous substance that poses an imminentand substantial threat to the public health and/or theenvironment. In addition, the provisions of the ComprehensiveEnvironmental Response, Compensation and Liability Act (CERCLA)promote a coordinated Federal, State and local reponse tomitigate situations at hazardous waste sites which pose animminent and substantial hazard to the public health and/or theenvironment.

The direct contact and ingestion threats posed to nearbyresidents by the spillage of hazardous material at the unsecuredsite necessitated an emergency response action to abate thethreats. Thus, the provisions of the NCP and CERCLA wereimplemented by the U. S. Environmental Protection Agency, RegionIII, Wheeling, West Virginia.

The overall success of this response would not have beenpossible were it not for the cooperation received from the WestVirginia Department of Natural Resources - I would like tocommend this agency for its efforts and professional handling ofthis pollution incident.

Betfton'M. WilmothOn Scene CoordinatorU. S. EPA - Region IIIWheeling, West Virginia

ARIOQQ06

INTRODUCTION

A. Initial Situation/Nature of the Incident

The Lakin State Farm site was formerly owned by West VirginiaUniversity and used to grow crops for experimental purposes. Thesite is currently owned by consolidated Natural Gas Coal Companyand is leased to Mr. Bartow Jones for farming practices. Thesite became of concern when the farm manager reported thatcertain areas of the corn crop displayed abnormal growthpatterns. Additionally, the farm manager reported that severaldrums containing electrical equipment was staged on site in anunsecured manner. At the request of West Virginia Department ofNatural Resources (WVDNR) EPA On-Scene Coordinator, BentonWilmoth tasked Roy F Weston's Technical Assistance Team (TAT) toconduct an assessment of the site. TAT's assessment revealedseveral drums of capacitors labeled "PCB containing" to be stagedin an open field on site. The soil around the capacitors was heavilystained with a black oily substance and grease like material; stressedvegetation was evident. Analytical results of the material revealedPCB levels in the 12,000 ppm range.

At the time of the assessment, the corn field mentioned earlier,was not planted and therefore made it impossible to determine areas ofpatchy corn growth. TAT obtained soil samples in the corn field butanalyses did not indicate any abnormal levels of pesticides orherbicides.

Based on the high PCB levels and the unsecured manner in whichthe capacitors were stored, the OSC elected to utilize his Delegation ofAuthority 14-1-A (5/1/85) to remove the capacitors andcontaminated soil and grease.

B. Site Location

The Lakin State Farm site is located at Camp Conley, MasonCounty, West Virginia. The community of Ft. Pleasant, WV islocated approximately three miles south of the site. The areasurrounding the site is rural and consists of several farms.

C. Efforts to Obtain Cleanup by Potential Responsible Party

Attempts by the OSC to contact responsible parties for thecleanup of this site were unsuccessful.

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NARRATIVE OF EVENTS

The Lakin State Farm site was referred to EPA's EmergencyResponse Section by the West Virginia Department of NaturalResources (WVDNR) Hazardous Waste Management Branch. WVDNRrequested that EPA assess the site to try and determine thepossible cause of patchy corn growth and investigate the abandonedelectrical equipment staged on site.

On June 1, 1987 members of the TAT team traveled to the siteto conduct an assessment. TAT was accompanied to the site byWVDNR representatives Pamela Hayes and Ava Zeitz. The Lakin

, state Farm is located off of Route 62 on Airport Drive. TAT'sinvestigation of the area revealed several abandoned drums whichcontained capacitors labeled "PCB containing". The groundsurface surrounding the drums and capacitors was covered with oiland a large pile of grease; stressed vegetation was evident. TATobtained several surface soil grap samples and samples of the oilin the capacitors as well as soil samples of the corn field. Allsamples were sent to an EPA approved lab for analysis of PCB andpesticides.

Analytical results from the TAT assessment revealed PCBcontamination in the soil and capacitor oil as high as 12,000ppm. Based on the high PCB levels, the OSC utilized hisDelegation of Authority 14-1-A (5/1/85) to obtain $50,000 inCERCLA monies to remove the capacitors and contaminated soil.The osc issued a Delivery Order to the ERCS contractor for$35,ooo on August 5, 1987. Removal operations commenced onAugust 6, 1987 and were completed on August 7, 1987. ERCSremoved 9 PCB-contaminated capacitors, 4 drums of contaminatedsoil and grease and 1 drum of site generated trash. Allcontaminated material was transported to AMO Pollution Servicestemporary disposal facility until the waste was approved forfinal disposal.

On December li, 1987, 17 drums of PCB-contaminated waste wastransported to APTUS disposal facility, Coffeeville, Kansas forfinal disposal.

RESOURCES COMMITTED

A. Initial Funding Request

On August 5, 1987 the OSC submitted a Special Bulletin A(see Appendix B of this report) for $50,000 to initiate romovalactivities at the site. The money was used to remove all PCB-contaminated capacitors, excavate all contaminated soil andultimately dispose of the material at an EPA approved disposalfacility. In addition, post excavation samples were taken todetermine the effectiveness of the removal.

B. Total Cost Summary (Estimated)

I.

Prime contractor (ERCS) $ 18,255.00Personnel (includes per diem)Transportation/Disposal

TAT 6,831.00 *

Extramural Subtotal $ 25,086.002. Intramural

EPA $ 600.00

TOTAL PROJECT COST $ 25,690.00 *

PROJECT CEILING S 50,000.00

Rounded to nearest dollar.

W

/ I R I O O O I

EFFECTIVENESS OF THE REMOVAL

A,. Activities of Various Agencies

1. Potential Responsible Party

No potential responsible party was located for this sitedespite repeated attempts by the OSC to contact PRP's.

2. State and Local Forces

The West Virginia Department of Natural Resources, HazardousWaste Division was responsible for conducting initialinvestigations into the site and for referring the site to EPA'sEmergency Response Section. WVDNR accompanied TAT on theinitial site assessment.

3. Federal Agencies and Special Forces

Benton Wilmoth of EPA's Emergency Response Section,Wheeling, WV office served as the On Scene Coordinator for thisproject and was responsible for the overall success of theremoval.

EPA's CERCLA Removal Enforcement Section (CRES) assisted theosc with the responsible party search.

4. Contractors

Roy F Weston's Technical Assistance Team (TAT) wasresponsible for conducting the initial assessment at the site andproviding technical assistance to the OSC which includedreviewing state generated analytical results for possiblehazards, drafting funding documents, POLREPS, site safety andsampling plans.

AMO Pollution Services, Inc., Canonsburg, PA served as theERCS subcontractor for the project and was responsible forsupplying all personnel and equipment to remove and properlydispose of the PCB contaminated materials.

B. Disposal Methods and Quantities Removed

ERCS removed 9 PCB-contaminated capacitors, 4 drums ofcontaminated soil and grease and one drum of site generatedtrash. The capacitors were placed into overpack drums andtransported to AMO's temporary disposal facility.

A R I O O O I 2

The contaminated soil surrounding the drums was removed withhand tools and placed into 17H recovery drums. The drums whichpreviously contained the capacitors were taken to AMO's TSD andcrushed for disposal.

All PCB-contaminated material was taken to APTUS disposalfacility in Coffeevllle, Kansas on December 14, 1987 for finaldisposal. The material was transported under PennsylvaniaManifest Number PAB4643041.

CHRONOLOGY OF EVENTS

June i. 19B7 - Roy F. Weston's Technical Assistance Team (TAT)performed a site assessment at the Lakin StateFarm per OSC direction. TAT obtained soil anddrum samples from on site areas and shipped thosesamples to the contract lab program (CLP) foranalysis.

Aug. s. 1987 - OSC received analytical results from the TATassessment of 6/1/87. PCB levels were found inthe soil and capacitor oil as high as 12000 ppm.

The OSC utilized his Delegation of Authority 14-1-A (4/8/B6) to obtain $50K in CERCLA monies tomitigate the PCB contaminated soil and drums.

osc issued a Delivery Order to the ERCS contractorfor $35K to remove and properly dispose of all PCBcontaminated materials.

OSC contacted WVDNR, Hazardous Waste Division, toinform them of EPA's plans to conduct a removal atthe site.

Aug. 6. 1987 - ERCS subcontractor, AMO Pollution Services, Inc.on site to begin removal activities.osc and TAT on scene to coordinate and monitorremoval activities.

Aug. 7. 1987 - ERCS completed the removal of all PCB contaminatedmaterials. Nine (9) PCB capacitors, Seven (7)drums of soil grease from stained areas and two(2) transformers from a farm building on site.

ERCS obtained post excavation samples to determineeffectiveness of cleanup.

osc signed Hazardous Waste Manifest #PAB3320343for transportation of materials to ERCS temporarystorage disposal facility, Canonsburg, PA.

All personnel demobilized from site.

Dec 14. 1987 - Seventeen (17) drums of PCB contaminated wastetransported to APTUS disposal facility,Coffeeville, Kansas, manifest #PAB4643041, forfinal disposal.

A R 1 0 0 Q I I *

LAKIN STATE FARM SITBCAMP CONLEY/LAKIN, MASON CO., 1W

.t.t < <0 IP 20 3O1 cSNiTmTsi . 7 no nmOMdens /-| h'(j Q (j I

SCALE 1:24000o _______________! MIUIOW 0 lOOO i«« MOO IMP tOOO tOOO TOO f(i\

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LAKIN STATfi FARM SITECAMP CONLHY/LAKIN, MASON CO., IVV

A R I D 0016

LAKIN STATE FARM SITECAMP CONLF.Y/LAKIN, flASON CO., IW

SPECIAL BULLETIN ALakin St. Farms PCB Capacitors SiteCamp Conley/Mason County, West Virginia

TO: Regional Response CenterU.S. EPA Region III

DATE: August 5, 1987

FROM: Benton M. WilmothOn-Scene Coordinator (3HH22)

THRU: Stephen R. Wassersug, DirectorHazardous Waste Management Division (3HWOO)

THRU: Thomas Voltaggio, ChiefSuperfund Branch (3HW20)

THRU: Thomas I. Massey, ChiefEmergency Response Section (3HW22)

I. INTRODUCTION

A preliminary assessment performed by the US EPA TechnicalAssistance Team (TAT) carried out in accordance with the NationalContingency Plan, has identified an immediate and significantrisk of harm to human health and the environment posed by thepresence on this site of capacitors containing Polychlorinated

j Biphenyls (PCB) in concentrations up to 12,000 parts per million(PPM). The PCB was found to be leaking from four drumscontaining eight (8) capacitors on the site, The spilled PCB and8 capacitors were unsecured and accessed by the public.

Section 104 of CERCLA calls for the Initiation ofimmediate removal where there is a threat of a release of ahazardous substance which may present an imminent and substantialdanger to public health or welfare.

The Delegation of Authority 14-1-A (4/8/86) authorizes theOSC to approve CERCLA removals with a total cost of less than$50,000. The osc, therefore, approved the use of CERCLA funds atthis site to mitigate the threat to human health and theenvironment by securing and removing the hazardous PCB oil toproper storage and disposal.

II. BACKGROUND

The Lakin State Farms PCB capacitors site is located inCamp Conley/Pt. Pleasant, Mason County, West Virgina. The spilloccurred on the former grounds of the Lakin State Farm, anexperimental farm, previously run by the University of westVirginia to study farming practices. The property is now ownedby Consolidated Natural Gas Coal Co. and is leased to BartowJones for fanning practices.

A R I O O O I 8

SPECIAL BULLETIN ALakin State Farms PCB Capacitors Site (cont.)

The site was referred to EPA On-Scene Coordinator BentonWilmoth from WV DNR Hazardous Waste Division, Pam Hayes. Thesite had a total of 4 drums containing 8 capacitors labeled "PCBcontaining" which were sampled by TAT. Sample analysis wasarranged through EPA's Contract Lab Program. Analysis revealedthe presence of PCB as Aroclor 1242 in excess of 12,000 ppm inthe capacitors.

III. THREAT

PCB is a designated hazardous substance under Section 311(B) of the Clean Water Act, and as such is included as ahazardous substance under CERCLA (Section 101[14]).

PCB has been demonstrated to cause cancer in animals andis a suspected human carcinogen, PCB bioaccumulates in human andanimal tissue in concentrations greater than exposure levels.PCB can cause liver damage, skin pigmentation, and chloracne.PCB can cross the placenta to the fetus and can increase thelevels of certain enzymes found in the liver, lungs, and skin,which in turn can increase the toxicological hazards of otherchemicals,

The drums containing the PCB capacitors leaked an unknownamount of their contents onto the ground surface at the site.The farm area is cared for daily by the farm manager. Thepotential for human exposure is high since the site is unfencedand access is unrestricted.

IV. SCOPE OF WORK

The scope of work proposed for implementation with theemergency $50,000.00 appropriation includes the following: 1)overpacking of the drums containing PCB capacitors; 2) removalof a small portion of stained soil; 3) removal of the overpackedPCB contaminated material to a licensed Temporary StorageFacility; 4) final disposal of the PCB waste.

The authorized budget was as follows:

ERCS $35,000.00EPA $1,500.00TAT $6,000.00EPA HQ. (15%) $7,500.00

TOTAL $50,000.00

f l f t i o o o i g

SPECIAL BULLETIN ALakin State Farm Site (cont.)

VI. OSC ACTION

On August 5, 1987 the OSC issued Delivery Order No.7445-03-002 to ERCS in the amount of $30,000.00 to Initiateremoval actions aimed at mitigating the threat to human healthand the environment.

At this time, no Potential Responsible Parties (PRP)have been identified. As a result, the OSC has initiated thisCERCLA removal.

Because the conditions of the Lakin state Farms PCB sitemeet the conditions of Section 300.65 of the National ContingencyPlan for an immediate removal, the OSC has approved thisimmediate removal action.

Benton M. Wilmoth, oscUS EPA, Region IIIWheeling, WV

AR100020

">, HESTON SPER DIVISIONHAZARDOUS WASTE SITE INVESTIGATION AND EMERGENCY RESPONSE

HEALTH AND SAFETY PLAN

.- --_,_ ,.. --„,,,,_________ REGIONDate of Inspection: fr///fl7 Time: '" TDD No.jOriginal Safety Plan: Yes i>-tto Modification No.___

Site Name: / /c/A|_57j4raLSite Address: street No. /ty/K;W fUrrf fl\n?c$T

County _____________________state MIS' Zip Code,

site Contact: $ fyt*l .TAy.S , t/t/!0/l//€lphone fe -f j.Directions to Site fon uhes/trnj R.T 2. •5au7l> B Pr-

Map Attached: Yea |X^ No TIf Remote Location: Latitude_______Longitude_SITE HISTORY: ffffbit.T£ AaMfae. ra <?*>**> ((to? Attt^Ly

•j flesTititf duMfi tn /'MfleK.rt 6»tc<r 1967-10. SIT& 4/io4<ir\AM.c, »F TRAM 1 fa* M epJ, . _________________________

INCIDENT DESCRIPTION

TYPE: A) Spill ___ Air Release __ Fire ___ HW Site iXotherB) Assessment iX " sampling ^XEmergency Response ___

Clean-up/Renoval ___ other (specify)

C) Urban/Residential ___ Commercial ___ IndustrialRural fX " Remote ___

PHYSICAL DESCRIPTION

Size of sita;jfrVtejC. &/Icars. Terrain; /tf///;f ////S Weather//t/M

containers Involved in the Release or Incident

Drums No. T , Tanks__ No.^___Truck__ License No.__ Tanker__ Box__

Railroad car__ Tank No.__ Box No.__Spill__source^________________ Approximate Volume

Other

MATERIALS INVOLVED:

Name TLV IDLH Overexposure Synptoms) 3 fhjfts. /,0 L *

SPECIAL HAZARDS;

ANTICIPATED LEVEL OF PROTECTION (circle one) : A B (Cj D

WHY! & M4TPfiM. feint £>OAUsJlu SolL •

FIRST AID INSTRUCTIONS FOR KNOWN CONTAMINANTS;suss

PERSONNEL EXPOSURE HAZARDS; (H-high, M-moderate, L-low, U-unknowii)

Inhalation ^ Skin contact *^Inge3tion__ Radioactive_Biological__ Fire__ Explosion__ Unknown ^ ^

PERSONNEL PHYSICAL SAFETY HAZARDS:

Heat t ^ cold__ Noise__ Underground Utilities__Overhead Utilities__ Heavy Equipment__ Slip, Trip, Fall_Sharp Objects < ~ Pressurized Airlines__ cyclinders__Ladders__ scaffolds__ Unguarded Openings-Wall, Floor__

/"Liquids in Open Containers),Liquids in Open Containers/, Ponds, Lagoons_

00022

DOCUMENTATION Performed byi/jEfe MAfrl^.

Type: Photo IX" Log Book - Recorder ____ Video,PUBLIC IMPACT

Distance to Nearest: ResidenceA?*? /m/jyschool ____ Hospital,*?

Public Building _____ Other Xto8/fTEvacuation; Yes __ Ho L^ Number __ By Whom: ____ENVIRONMENTAL IMPACT:

Nearest Waterway! Q-ttto fi'tfEK. _______ Distance: /• 5"Condition Obaeryed PotentialSurface Water Contamination ____ . ^^Ground Hater Contamination ______ <_Drinlclng Water Contamination iAir ContaminationSoil ContaminationStressed VegetationDead Fish, Other Animals

PERSONNEL INVOLVED! (NAME, AGENCY, PHONE, ON or OFF SITE)

SITE MANAGER!_________

SITE SAFETY COORDINATOR!

Have Read & Understood TheSite Safety Plan (check)

&enToon

TAT Mite.

STATE fyM M*!Y£S 34 8-5"?2.1' Jl , 7VI -m '.' * —--.-... ll II I I" _l

OTHER

EMERGENCY INFORMATION

EMERGENCY PHONE NUMBERS!Location Phone Notified (Y/N)

Fire fT- flffcfidrtiVrlRSt ' ' // ' " ~police "fr. eicfwtsr fris-Tioi X/Ambulance PT- PtcfiwJT '111 */,Hospital

Nearest Phone o£ fa**ik>qc£ bttm.e fflfibx . /oao ' 4r

DIRECTIONS TO HOSPITAL! fliftfagT /feto .72> IT 6 2. /Uiiig/ 7?i(ATTACH MAP) '

ADDITIONAL EMERGENCY PHONE CONTACTS!

CHEMTREC (800) 424-9300TSCA HOTLINE (BOO) 424-9065,(202)554-1404CDC (404) 452-4100 (Day), (404) 329-2888 (Night)BUREAU OF ALCOHOL, TOBACCO & FIREARMS (800) 424-9555, (202) 566-7777NATIONAL RESPONSE CENTER (800) 424-8802WESTON MEDICAL EMERGENCY SERVICE (513) 421-3063

., WESTON 24 HOUR HOTLINE (215) 524-1325, 1926' PESTICIDE INFORMATION SERVICE (800) 845-7633EPA ERT EMERGENCY (201) 321-6660RCRA HOTLINE (800) 424-9346BUR. OF EXPLOSIVES, A.A. RAILWAYS (202) 835-9500

Prepared by; M<£nA€L X^ffZ£l<W_________ Date:__£Reviewed by:____________________ Date:_

Approved by:___________________________ Date:_

SPER HSO Reviewed by:_^_____________ Date:Followup Required:Followup Performed:Comments: ______

ACTIONS TAKEN ON SITE;

Was Entry Made: YES tx"" NO

Equipment Used: (circle/) LEVEL A B (c) D WHY :a. CTIMJJL .(<> tMaD. . Sate. Sm* XSUL*.

' 'SCBA ___ APR ___ Model ____ Cart. /Can. Type

Poly Tyvek__ Saran Tyvek___ Acid suitRain Gear___i Cotton Coveralls - "Gloves: Inner I/ Butyl j^Nitrile___ Viton__ other_Foot Gear: Safety Boots 6x"5uter Boots__ Booties fc.-

Description of Decontamination Oaedt

AIR MONITORING Performed by.Mfe)

Instrument Readings: Radiation Meter____ CGI_

OVA____ HNU . iSflPM " Detector

OtherWind; Speed_0-.5WDirection $E Temp.67 f Rel. Hum. 85" B.P.Summarize Air-Monitoring Data c/t ^ A )i > (Mty? < 7T,

SAMPLING Performed by:,

Sampling Plar. (w°r N)___ If yes attach copy to safety planNo. of Samples: solid 7 Liquid_Z___ Gas___ other___

Laboratory: U/lfc_______________________________ _Has Lab Been Notified^of Potential Hazard Level? Yes___ No_

Analyses; rdb s

W Sampling Comments:,

'.CWlOSITE/SAFETY PROTOCOL

Lakin State Farm PCB Spill siteLakin, Jackson County, West Virginia

GENERAL

This protocol addresses the safety procedures that will be followed byany and all personnel visiting the site or involved In the CERCLAremoval activity at the Lakin State Farm Site. All personnel enteringthe site shall read and sign this safety plan. The protocol willremain in effect until the osc certifies that the activity isterminated. It does not supercede any Federal OSHA or state or localregulations but is in addition to them. In the event of aconflict between this protocol and a regulation, the more stringent of twill be in force.

Since data available at the present time does not allow a completecharacterization of the PCB capacitors on the site, levels ofprotection for personnel will be set in accordance with the hazard ofthe job function and location on-site as indicated on the attacheddiagram.Respiratorv_Protection_Prograrq

All contractor and governmental personnel involved in on-siteactivities shall have a written respiratory protection program andprove that they are physically fit to wear a respirator. Allpersonnel wearing air-purifying respirators on-site are required to befit tested, while those wearing pressure-demand self-containingbreathing apparatus or air-line apparatus, must be properly trainedand experienced in their use. All respiratory protection equipment isto be properly decontaminated at the end of each workday.

Persons having beards or facial hair mustjiot wear a respirator.

Traininq_and_Hedical_Monitorlng_Program

Personnel will have both formal training and on-the-job training,in accordance with OSHA regulations, for those tasks they areassigned to perform on the active site. All unfamiliaractivities will be rehearsed beforehand.

All contractor and governmental personnel who are exposed to hazardouslevels of chemicals shall prove that they are enrolled in a medicalmonitoring program.

ARIOG026

Lakin State Farm PCB Spill SiteLain, Jackson County, West Virginia 1Page 2Generalise fety_Rules_and_Equipinent

a. There will be no eating, drinking or smoking in the Exclusion Areaor hot side of the Contamination Reduction Area.

b. All personnel must pass through the Contamination Reduction Areato enter the Exclusion Area.

c. An emergency eye wash will be on the hot side of the ContaminationReduction Area.

d. As a minimum, an emergency deluge shower/spray can is to belocated on the clean side of the Contamination Reduction Area.

e. At the end of the work, all personnel working in the ExclusionArea shall take a hygenic shower.

f, All supplied breathing air shall be certified as Grade D orbetter.

g. Where practical, all tools/equipment will be spark proof, explosionresistant and/or bonded and grounded.'

h. Fire extinguishers will be on-site for equipment or personnel firesonly.

i. A first-aid kit will be on-scene at all times during operationalhours. An oxygen inhalator respirator will be available. Thelocation of these items on-site will be posted.

j. Persons having beards or faeialjhair must not wear respirators.

k. No work will be performed in the exclusion area during hours ofdarkness as determined by the site safety officer.

Hornlng_Safety_Meetlng

A morning safety meeting will be conducted each day for all sitepersonnel who sign a daily attendance sheet. The safety procedures,evacuation procedures, and escape procedures, as well as the day'splanned operations, should be discussed.

Lakin state Farm PCB Spill SiteLakin, Jackson County, West VirginiaPage 3CONTROL-ATjrHE_ST.TEi

Access to the site will be restricted by a site security officer andbanner guard Installed during the immediate removal phase at this siteand exit from the site shall be through the gate in the ContaminationReduction Area except in a life-threatening emergency.

All persons entering the site shall sign in and out at the OSC commandpost or with the site security officer.DESIGNATIONJ3FJTORK_ARE3S_AT_THE'SITE

The entire site will be divided into three areas: (l) Exclusion Areawhich known to be or have a potential for becoming contaminated:(2) the contamination Reduction Area where decontamination ofpersonnel and equipment exiting the Exclusion Area is performed;(3) the Support Area which is not contaminated.

The_Exclusion_Area (EA)At the Lakin State Farm PCB Site, the Exclusion Area shallinitially include all areas inside the banner guard.The_Contaminatlon_Reduction Area (CRA)At the Lakin State Farm PCB Site,the Contamination ReductionArea will be located immediately outside the Exclusion areaand will be delineated by roped off area.

The_Support_Area (SA)At the Lakin State Farm PCB Site, the Support Area will be thearea outside the Exclusion Area and Contamination Reduction Area.

Changes_in_Desianation_of_Work-Areas

As work progress on-side, the OSC may determine that an areapreviously designed an EA is no longer classified in that manner. Itis not intended, however, to change the designation of the CRA sincethis may involve the movement of the decontamination facilities andadded expense.

SAFETY_PROCEDURES AND LEVELS OP_PROTECTION

Exclusion_Area

1. All personnel shall enter_and_exlt the Exclusion Area through theContamination Reduction Area.

2. Emergency escape routes from the Exclusion Area will beestablished and reviewed as appropriate at each morningsafety meeting.

Lakin State Farm PCB Spill siteLakin, Jackson County, West VirginiaPage 4

SAFETY PROCEDURES AND LEVELS OF PROTECTION (continued)

Exclusion_Area

3. All personnel In the Exclusion Area shall use the protectiveequipment designed for their job function but in no case shallless than LEVEI,__B be used.

4. Personnel performing the following job functions in theExclusion Area will utilize the designed level of protectionequipment.

Contamination_Reduction_Area

1. Personnel and equipment decontamination will be performed inLevel c.

2. All personnel entering the CRA will utilize a minimum ofLevel_c

protection.3, All personnel entering the CRA must decontaminate which will

be performed in Level_c.4. All equipment entering the CRA must be decontaminated prior to

leaving the CRA,Support Area

1. No contaminated equipment or personnel may enter the Support Area.

2. Except in the case of a release of a Toxic vapor, Level_D willbe appropriate for all personnel in the Support Area.

Pr j r.g_fjpntractor

1. Barrel opening, sampling, and overpacklng will be performed inLevei_B. This applies to anyone involved, including equipmentoperators.

DECONTAMINATION PROTOCOL

All equipment and personnel entering the site must be thoroughlydecontaminated prior to leaving the site, since there are variousprotocol and equipment available for this purpose, the osc willdetermine if the proposed decontamination techniques areapplicable, such determinations will be made on a day-to-day basis as on-site operations dictate.

fiR I 00029

Lakin State Farm PCB Spill Site— Lakin, Jackson County, West Virginia

Page 5

EMERGENCY PROCEDURES

In the event of a medical or other emergency, the OSC or his deslgneewill notify the appropriate authority. The following list of phonenumbers will be posted prominently at each telephone on-site:

1. Fire (304) 675-6151 Point Pleasant

2. Ambulance (304) 911 Point Pleasant

3. Police (304) 675-1104 Point Pleasant

4. Federal Government (215) 597-9898

5. EPA Environmental Response Team (201) 321-6649

6. Hospitals (304) 675-3230 Lakin State Hospital

AR100030

4I9.423-U526Telex 298248 OIIMI UHlRCAl

O.H.MitiilnliCorp,16406 U.S. Runic 2*1 E«»i

ANALYTICAL REPORT RO'Bl"551

OHM

CLIENT: USEPA Region III

ATTNiJ

OHM PROJECT NUMBER: 5142E SAMPLE TYPE: Soils

OHM PROJECT MANAGER: J. Copus ANALYSIS PERFORMED:

P'olychlorinaced Biphenyls (PCBa)

DATE COMPLETED: 9-11-87 DATE RECEIVED: B-28-87

report is "PROPRIETARY AND CONFIDEHTIAL" and delivered to, and intendedfor the exclusive we of, the above named alient only. O.H, Materials Corp,assumes no responsibility or liability for the reliance hereon or nee hereofby anyone other than the above named alient,

All of the analyses and data interpretation that form the basis of Ma reportwas prepared under the direct supervision and control of the undersigned ahoia solely responsible for the contents and conclusions therein,

Reviewed and 7(7 / /Approved by i Si/ Stated' ______

Thyrfas E, Gran, Pp,D,, Manager Analytical Services Pate

Aft I 00031A Subsidiary ol Emironrantil Tiiivnem ind Ttctinologiti Corp.

9-23-871

PROJECT S142E

SUMMARY REPORT OF ANALYTICAL SERVICES

I. INTRODUCTION

O.K. Materials Corp. (OHH) Corporate Laboratory received 4soil samples from USEPA Region III, Lakin, West Virginia.These samples were acquired by OHM's technical personnel andtransferred to the laboratory complete wit.h a chain-of-custody record, a copy of which is attached for reference.These samples were analyzed for polychlorinated biphenyls(PCBs).

II, ANALYTICAL METHODOLOGY

Polychlorinated Biphenyls (PCBs) - Solid/Soil

Solid samples were prepared and analyzed according to USEPATest Methods for Evaluating Solid Wastes, Physical/ChemicalMeTHods, SH-B46, 2nd edition, July 19B2; Method 3550, SonFcation Extraction and Method 8080, Organochlorine Pesticidesand PCBs,

III. ANALYTICAL RESULTS

The following tables detail the analytical results forsamples I5142E-658 through 05142E-661.

0 032

9-23-872

PROJECT 5142E

TABLE \ - SEMI-VOLATILE PCBS BY PC ANALYSIS

SAMPLE IDENTIFIER: LFS1OHM SAMPLE NUMBER: 5142E-658

Compound Concentration (mg/Kg)

Aroclor 1016 38.2

Aroclor 1221 BDLAroclor 1232 BDL


Aroclor 1254 . BDLAroclor 1260 BDL


Limit of Detection - 1.0 mg/Kg ppm (parts-per-raillion)BDL • Below Detection Limit

Aft10003o

9-23-873

PROJECT S142E

TABLE 1 - SEMI-VOLATILE PCBS BY GC ANALYSIS (CONTINUED)




Aroclor 1232 BDL


Aroclor 1254 BDL

Aroclor 1260 BDL

Aroclor 1262 ' BDLAroclor 1266 BDL

Limit of Detection - 1.0 mg/Kg ppm (parts-per-million)BDL • Below Detection Limit

.

PROJECT

TABLE 1 - SEMI-VOLATILE PCBS

SAMPLE IDENTIFIER: LFS3OHM SAMPLE NUMBER: 5142E-G60

Compound

Aroclor 1016

Aroclor 1221Aroclor 1232Aroclor 1242

Aroclor 1248Aroclor 12S4Aroclor 1260

Aroclor 1262Aroclor 1268

9-23-874

S142E

BY GC ANALYSIS (CONTINUED)

Concentration (mg/Kg)

BDL

BDL

BDL

BDL

BDL

BDL

BDL

BDL

BDL

Limit of Detection » 1.0 mg/Kg ppm (parts-per-million)BDL - Below Detection Limit

A i;i i 0 C 0 3 5

9-23-875

PROJECT 5142E

TABLE 1 - SEMI-VOLATILE PCBS BY GC ANALYSIS (CONTINUED)



Aroclor 1016 9.0Aroclor 1221 BDLAroclor 1232 BDL

Aroclor 1242 BDL

Aroclor 1248 BDLAroclor 1254 • BDLAroclor 1260 BDL


Limit of Detection - 1.0 mg/Kg ppra (parts-per-million)BDL - Below Detection Limit

9-23-876

PROJECT 5142E

QC SUMMARY

Percent Spike Recoveries: 1094

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ANALYTICAL REPORT\ Tclf\ 2982411 omillRlKCAl

OHM

CLIENT: USEPA Region IIILakin, HV

OHM PROJECT NUMBER! 5142E SAMPLE TYPE: Liquid Conposlte


Incineration Disposal (Sample; LC01)

DATE COMPLETED: 9-18-87 DATE RECEIVED: 8-28-87

This report is "PROPRIETARY AND CONFIDENTIAL" and delivered to, and intendedfor the exclusive use of, the above named alient only. O.H, Materials Corp,assumes no responsibility or liability for the reliance hereon or use hereofby anyone other than the above named client,

All of the analyses and data interpretation that form the basis of this reportwas prepared under the direct supervision and control of the undersigned whois solely responsible for the contents and conclusions therein.

Reviewed and "TApproved by: f_______/ < ___________ .

Thomas E. Gran, Ph,D,, Manager Analytical Services 'Date

A Subsidiary ol Environmental ttidiliwll flu Technologies Corp.

9-24-871

PROJECT S142E


I. INTRODUCTION

O.H. Materials Corp. (OHM) Corporate Laboratory received onesample from USEPA Region III, Lakin, West Virginia. Thissample was acquired by OHM'S technical personnel and trans-ferred to the laboratory complete with a chain-of-custodyrecord, a copy of which is attached for reference. Thiscomposite was analyzed for Incineration disposal parameters.

II. ANALYTICAL METHODOLOGY

o Metals - Samples were prepared according to USEPA TestMethods for Evaluating Solid Wastes, Physical/ChemicalMethods, SW-B46, 2nd edition, July 1982. Samples wereprepared by either Method 3010, 3030, 3050, or 1310 asappropriate for the following metals: antimony, arsenic,barium, beryllium, cadmium, total chromium, copper, iron,lead, manganese, mercury, nickel, selenium, silver,thallium, and zinc, sample analyses for these metalswere performed according to method 6010, InductivelyCoupled Plasma Method (SW-B46 Proposed Sampling andAnalytical Methodologies, 1984).

o Density - Densities were determined by either ASTM MethodD1298-80 for liquids or by Method 213E for solids,Standard Methods for the Examination of Hater and Waste-water 16th edition, 19S5.

o BTU Content-Solids and Liquids - The BTU content of thesamples was determined by either ASTM E711-81, TestMethod for Gross Calorific Value of Refuse Derived Fuel(RDF-3) by Bomb Calorimeter, Section II, Vol. 11.04 or byASTM D240-76, Test Method for Heat of Combustion ofLiquid Hydrocarbon Fuels by Bomb Calorimeter, Section 5,Vol. 05.01.

o Ash Content - The ash content of the samples wasdetermined by either ASTM E830-81, Test Method for Ash inthe Analysis Samples of Refuse-Derived Fuel (RDF-3),Section II, Vol. 11.04, or by ASTM D482-80 Test Methodfor Ash from Petroleum Products, Section 5, Vol. 05.01.

o Sulfur Content - The sulfur content o£ the samples wasdetermined by either ASTM E775-81, Test Methods for TotalSulfur in the Analysis Sample of Refuse-Derived Fuel,Section II, Vol. 11.04, or by ASTM D129-64 (1978), TestMethod for Sulfur in Petroleum Products (General BombMethod), Section 5, Vol. 05.01.

W

9-24-872

PROJECT S142E


o Pesticides and PCB Content - Samples were prepared byMethod 3510, 3540, or 3550 as appropriate; and analyzedaccording to Method 8080 of USEPA Test Methods forEvaluating Solid Hastes, Physical/Chemical Methods,SW-B467 2nd edition. July 1982.

o Chlorine Content - The samples were analyzed for percentchlorine according to American Society for Testing andMaterials, Section 5, Method D80B-81, Chlorine in New andUsed Petroleum Products (Bomb Method).

o Viscosity - Organic liquids were analyzed using aBrookfield viscometer according to ASTM D2983, Volume5.03, 1983.

o Total Solids - Solid samples were analyzed for TotalSolids (TS) according to Standard Methods, 16th edition,Method 290F, Residue, Total, Gravimetric, Dried ati03°C-105°C.

o GC/MS Volatile Organic Analyses and Screens - Volatileanalysis of the samples are performed using methods basedon USEPAs Test Methods for Evaluating Solid Wastes,Physical/Chemical Methods, SW-846, July 1982; MethodB24'0, GC/MS Methods for Volatile Organics.

o GC/MS Semi-Volatile Organic Analyses and Screens - Acidand base neutral extractables are prepared and analyzedusing methods based on USEPAs Test Methods forEvaluating Solid Hastes, Physical/Chemical Methods,SW-846, July 1982" Method 8240, GC/MS Methods for Semi-Volatile Organics.

o Flash Point - Flash points were performed according tothe procedure specified in USEPA Test Methods for Evalu-ating Solid Wastes, Physical/Chemical Methods, SW-B46,2nd edition, July 1982; Method 1010, Pensky-MartinClosed-cup Method.


The following tables detail the analytical results for sampleI5142E-LC01.

O-OM

9-24-873

PROJECT 5142E

TABLE 1 - INCINERATION DISPOSAL ANALYSIS

SAMPLE IDENTIFIER: Liquid CompositeOHM SAMPLE NUMBER: 5142E-LC01

Parameter Result

Color BrownOdor NoneNumber of Phases 1Percent by volume of phases 100%Physical state of phases Liquid

Density 1.0 gm/cm5Flash Point, PM, CC > 95°C

Viscosity, Brookefield ' > 1.5 cpu

0TU Content < 200 BTU/lbAsh Content < .01* by weightchlorine Content < 0.1% by weightSulfur Content < 0.1% by weight

Total Solids 0.21% by weight

Total Suspended Solids < 0.1% by weightTotal Dissolved Solids 0.19% by weight

H tt ; J C u '-J ii

9-24-874

PROJECT S142E

TABLE 2 - VOLATILE ORGANICS


Compound Concentration (mg/L)

Benzene BDLBromomethane BDLBromodichloromethane BDLBromoforn BDLCarbon Tetrachloride BDLChlorobenzene BDLChloroethane BDL2-Chloroethylvinyl ether BDLChloroform BDLChloromethane BDLDibromochloromethane BDL1,2-Dichlorobenzene BDL1,3-Dichlorobenzene BDL1,4-Dichlorobenzene , BDL1,1-Dichloroethane ' BDL1,2-Dichloroethane BDL1,1-Dichloroethene BDLTrans-1,2-Dichloroethene BDL1,2-Dichloropropane BDLCis-1,2-Dichloropropene BDLTrans-1,3-Dichloropropene BDLEthylbenzene BDLMethylene Chloride BDL1,1,2,2-Tetrachloroethane BDLTetrachloroethene BDL1,1,1-Trichloroethane BDL1,1,2-Trichloroethane BDLTrichloroethene BDLTrichlorofluoromethane BDLToluene BDLvinyl Chloride BDLTotal Xylenes BDL

Limit of Detection - 100 mg/L ppm (parts-per-million)BDL • Below Detection Limit

h Fi i 0 G 0 '•; o

PROJECT S142E

TABLE 3 - VOLATILE HSL COMPOUNDS

SAMPLE IDENTIFIER: Liquid CompositeETC SAMPLE NUMBER: 5142E-LC01

mg/L - ppm (fparts-per-million)BDL - Below Detection Limit

9-24-875

Concentration DetectionCompound (mg/L) Limit (mg/L)

Acetone BDL 1,000Acrolein BDL 5,000

Acrylonitrile BDL 5,000

2-Butanone BDL 1,000

Carbon Disulfide BDL 100Ethyl ether BDL 1,000

Ethylene Dibromide BDL 1,000

2-Hexanone BDL 1,000

4-Methyl-2-Pentanone (MIBK) BDL 1,000

Styrene BDL 1,000Tetrahydrofuran BDL 2,000

l,l,2-Trichloro-l,2,2-trifluoroethane BDL 500

Vinyl Acetate BDL 1,000

Aft

9-24-876

PROJECT S142E

TABLE 4 - VOLATILE SCREEN RESULTS


Compound Concentration (mg/L)• ••••••••••••••••••••(•••(•••••••••••••••••••••(••••••••••••••••••••IIH

No chromatographic peaks present with an area greater than 25% ofthe internal standards

9-24-677

PROJECT S142E

TABLE S - BASE/NEUTRAL COMPOUNDS



Acenaphthene BDLAcenaphthylene BDLAnthracene BDLBenzofa(anthracene BDLBenzo(b)fluoranthene BDLBenzo(k)fluoranthene BDLBenzoja)pyrene BDLBenzojg,h,i)perylene BDLBis(2-chloroethyl)ether BDLBis(2-chloroethoxy)methane BDLBis(2-ethylhexyl)phthalate BDLBis(2-chloroisopropyl(ether BDL4-Bromophenyl phenyl ether BDLButyl benzyl phthalate BDL2-Chloronaphthalene BDL4-Chlorophenyl phenyl ether , BHLChrysene BDLDibenzo(a,h)anthracene BDL

) Di-n-butylphthalate BDL1,3-Dichlorobenzene BDL1,4-Dichlorobenzene BDL1,2-Dichlorobenzene BDLDiethylphthalate BDLDimethylphthalate BDL2,4-Dinitrotoluene BDL2,6-Dinitrotoluene BDLDioctylphthalate BDL1,2-Diphenyl hydrazine BDLFluoranthene BDLFluorene BDLHexachlorobenzene BDLHexachlorobutadiene BDLHexachloroethane BDLHexachlorocyclopentadiene BDLIndeno-(l,2,3-cd)pyrene BDLIsophorone BDLNaphthalene BDLNitrobenzene BDLN-Nitrosodi-n-propylamine BDLN-Nitrosodiphenylamine BDLPhenanthrene BDLPyrene BDL1,2,4-Trichlorobenzene BDL

Limit o£ Detection « 100 mg/L ppm (parts-per-million)BDL • Below Detection Limit

9-24-878

PROJECT S142E

TABLE 6 - ACID EXTRACTABLE



4-Chloro-3-Methylphenol BDL2-Chlorophenol BDL2,4-Dichlorophenol BDL

2,4-Dimethylphenol BDL

2,4-Dinitrophenol BDL

2-Methyl-4,6-Dinitrophenol BDL

2-Nitrophenol BDL

4-Nitrophenol ' BDLPentachlorophenol BDLPhenol BDL2,4,6-Trichlorophenol BDL

Limit of Detection • 100 mg/L ppm (parts-per-million)BDL - Below Detection Limit

ftR100047

9-24-879

PROJECT 5142E

TABLE 7 - ADDITIONAL SEMI-VOLATILE HSL COMPOUNDS

SAMPLE IDENTIFIER; Liquid CompositeOHM SAMPLE NUMBER: 5142E-LC01


Aniline BDLBenzyl Alcohol BDL

4-Chloroaniline BDL

Dibenzofuran BDL

2-Methylnaphthalene BDL2-Methylphenol ' BDL4-Methylphenol BDL

2-Nitroaniline ' BDL3-Nitroaniline BDL4-Nitroaniline BDL

2,4,5-Trichlorophenol BDL

Limit of Detection • 100 mg/L ppm (parts-per-million)BDL • Below Detection Limit

9-24-8710

PROJECT S142E

TABLE 8 - SEMI-VOLATILE SCREEN RESULTS




9-24-8711

PROJECT S142E

TABLE 9 - PESTICIDES AND PCBS


Concentration DetectionCompound (mg/L) Limit (mg/L)

Aldrin BDL 0.1BHC-alpha BDL 0.1BHC-beta BDL 0.1BHC-gamma BDL 0.1BHC-delta BDL 0.1Chlordane BDL 1.04,4'-DDD BDL 0.14,4'-DDE BDL 0.14,4'-DDT BDL 0.1Dieldrin BDL 0.1Endosulfan-alpha BDL 0.1Endosulfan-beta BDL 0.1Endosulfan sulfate BDL 0,1Endrin BDL 0.1Endrin aldehyde BDL 0.1Heptachlor BDL 0.1Heptachlor epoxide BDL 0.1Toxaphene BDL 1.0

POLYCHLORINATED BIPHENYLS

Aroclor 1016 BDL 1.0Aroclor 1221 BDL 1.0Aroclor 1232 BDL. 1.0Aroclor 1242 BDL 1.0Aroclor 1248 BDL 1.0Aroclor 1254 22.0 1.0Aroclor 1260 BDL 1.0

mg/L - ppm (parts-per-million)BDL - Below Detection Limit

flRIOOOSO

9-24-8712

PROJECT b!42E

TABLE 10 - TOTAL METALS FOR INCINERATION DISPOSAL


Compound Name

AntimonyArsenic

BariumBerylliumCadmiumChromium (Total)CopperIronLead

ManganeseMercury

Nickel

SeleniumSilver

ThalliumZinc

Concentrationmg/L

2.8BDL

BDL

BDL

BDL

BDL

, BDL

10.6

8.63

BDL

BDL

BDL

BDL

BDL

BDL

BDL

DetectionLimit mg/L

1.01.01.01.01.01.01.01.01.0.1.0

0.2

1.0

1.0

1.0

1.0

1.0

mg/L • ppn (parts-per-million)BDL - Below Detection Limit

f i R I O O O S l

9-24-8713

PROJECT S142E

QC SUMMARY

A. Conventional Analysis:Cyanide- 76.0%Chloride- 113%

B. GC/MS Priority Pollutant Volatile Organics:BFB Tune File: See attachedSurrogate Recoveries:

Blank Spike1,2-Dichloroethane-d. 70.7 107 104Benzene-d. 117 110 104Toluene-d, 117 115 106

113 111 104

Volatile Organics Spike Recoveries: (In Percentages)

Benzene 106 101Bromomethane 103 101Bromodichloromethane 123 ' 111Bromoform 172 146Carbon Tetrachloride 135 125chlorobenzene 116 109Chloroethane 105 1072-Chloroethylvinyl ether 127 115Chloroform 113 113Chloromethane 96.3 99.0Dibromochloromethane 155 1361,2-Dichlorobenzene 113 1041,3-Dichlorobenzene 115 1041,4-Dichlorobenzene 113 1041,1-Dichloroethane ' 122 1171,2-Dichloroethane 103 96.P1,1-Dichloroethene 115 113Trans-1,2-Dichloroethene 103 1021,2-Dichloropropane 122 1091,3-Dichloropropenes 112 105Ethylbenzene 108 101Methylene Chloride 108 1111,1,2,2-Tetrachloroethane 102 88.2Tetrachloroethene 122 1111,1,1-Trichloroethane 112 1051,1,2-Trichloroethane 114 102Tri:hlnroethene 122 116Trichlorufluoromethane 115 115Toluene 106 102Vinyl Chloride 106 107Total Xylenes 118 115

ARI0005_

9-24-8714

PROJECT S142E

QC SUMMARY (CONTINUED)

Volatile Organics Spike Recoveries (in Percentages): ContinuedAdditional CompoundsMethyl ethyl Ketone" 93.8 99.0Carbon Disulfide 105 112Acetone 81.0 78.4Methyl Isobutyl Ketone 109 106Methyl Pentanone 97.9 97.0Styrene 108 105

C. GC/MS Priority Pollutant Semi-volatile Organics:DFTPP Tune File: See attachedPercent Surrogate Recoveries:

Blank

2-Fluorophenol 50.4 66.8Phenol-d, 36.7 46.8Nitrobenzene-d, 71.1 60.22-Fluorobiphenyl 80.0 , 61.62,4,6-Tribromophenol 46.6 103p-Terphenyl-dn 82.3 113

Semi-volatile Spike Recoveries: (In Percentages)

1,4-Dichlorobenzene 92.22-Chlorophenol 95.4Phenol 45.1N-Nitroso-di-n-propylamine 84.11,2,4-Trichlorobenzene 1064-Chloro-3-Methylphenol 67.9Acenaphthene • 1222,4-Dinitrotoluene 103Dlbutylphthalate 76.54-Nitrophenol 27.0Pyrene 92.2

D. Pesticides, Herbicides: Percent Spike RecoveriesLindane 62.0Toxaphene 59.02,4-D 88.02,4,5-TP 81.0a-BHC 79.6b-BHC 86.3g-BHC 73.0Aldrin 52.0Heptachlor 85.0

9-24-8715

PROJECT 5142E


E. Metals: Percent Spike RecoveriesAntimony 88.2Arsenic 97.2Barium 93.3Beryllium 97.5Cadmium 98.9Chromium 97.4Copper 92.9icon 95.6Lead 95.4Manganese 121Mercury 99.5Nickel 96.2Selenium 92.5Silver 101Thallium 98.5Zinc 114

F, PCBs: Aroclor 1254-% Recovery: 68%

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30 - (0% of the base peak

Base peak, 1001 relative abundance

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lets than 11 of the bate peak

174 Greater than 501 of the bate peak . /,) 7fo175

176

177

5 - 91 of BAII 174 tf.f*

Greater than 951, but leti than101% of 174 (fro

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O.H, Militiilt Corp.1MOO U.S. Kiiule 224 EI

ANALYTICAL REPORT4l9.423.352dT('l««! I«()IIMII.II ilia.

CLIENT: USEPA Region IIILakin, HV

OHM PROJECT NUMBER: 5142E SAMPLE TYPE: SoU Composite


Landfill Disposal (Sample: SC01)

DATE COMPLETED: 9-18-87 DATE RECEIVED: 8-28-87

This report is "PROPRIETY AND CONFIDENTIAL" and delivered to, and intendedfor the exclusive use of, the above named alient only, O.H. Materials Corp.assumes no responsibility or liability for the reliance hereon or use hereofby anyone other than the above named alient.

All of the analyses and data interpretation that form the basis of this reportwas prepared under the direct supervision and control of the undersigned whois solely responsible for the contents and conclusions therein.

Reviewed and < ~T~ZjApproved by: _________/ Z- _________

Thomas E. Gran, Ph.D., Manager Analytical Services /Date

A Subsidiary ol Environmental Tieimem

9-24-871

PROJECT 5142


I. INTRODUCTION

O.H, Materials Corp. (OHM) Corporate Laboratory received onesolid composite sample from USEPA Region III, Lakin, WestVirginia, This sample was acquired by OHM'S technicalpersonnel and transferred to the laboratory complete with achain-ol:~custody record, a copy of which is attached forreference. This sample was analyzed for Landfill Disposalparameters,

II. ANALYTICAL METHODOLOGY

o Total PhenolsThe samples were prepared by accurately weighing anapproximate 20 9 aliquot of each sample and then suspendthe solid in 500 ml Lab Grade I water. The pH of thesample solutions were adjusted to pH 4 with 1+9 phos-phoric acid, then 5 mis of 101 copper sulfate solutionwas added to each sample. Samples were mixed for onehour and prepared and analyzed according to EPA TestMethods for Evaluating Solid Hastes, Physical/ChemicalMethods, SW-846, July 1982; Method 9065, Phenolics(Spectrophotometric, Manual 4-AAP with Distillation).

o GC/MS volatile Organic Analyses and ScreensVolatile analysis of the samples was performed usingmethods based on EPA Test Methods for Evaluating SolidWastes, Physical/Chemical Methods, SW-846, July 1962;Method 8240, GC/MS Methods for volatile Organics.

o GC/HS Semi-Volatile Organic Analyses and Screens

Acid and base neutral extractables wnre prepared andanalyzed using methods based on USEPA Test Methods forEvaluating Solid Hastes, Physical/chemical Methods^SW-846, July 19B2, Method 8270, GC/MS Methods forSemi-Volatile Organics. Extractions were performed byeither Method 3540, Soxhlet Extraction or Method 3550,Sonication Extraction.

o Density - Densities of the samples were determinedaccording to Standard Methods for the Examination ofWater and Wastewater, 16th edition, 1985; Method 213E,Specific Gravity.

rt R i Ll U iJ 6 b

9-24-872

PROJECT S142E

SUMMARY REPORT OP ANALYTICAL SERVICES

Total Solids - Samples were analyzed according toStandard Methods for the Examination of Water and waste-water, 16th edition, 1985; Method 209F, Total, Fixed andVolatile Solids in Solid and Semi-solid Samples,PolYchlorinated Biphenyls and Organochlorine Pesticides-Solid camples were analyzed and prepared according toUSEPA Test Methods for Evaluating Solid Hastes, Physical/Chemical Methods, SW-B46, 2nd edition, 19S2; Method 3550,Sonication Extraction or Method 3540, Soxhlet Extractionand Method 8080, Organochlorine Pesticides and PCBs.

Total and Amenable Cyanide - The samples were prepared byaccurately weighing an approximate 20 gm aliquot of eachsample into 500 ml of Lab Gra^" I water. The sampleswere adjusted to pH 12 and sti.red for one hour. Thesamples were then analyzed according to USEPA TestMethods for Evaluating Solid Wastes, SW-846, 2nd edition,July 1982 (Revised April 1984); Method 9010, Total andamenable Cyanide and by Standard Methods for the Exami-nation of Water and Wastewater, 16th edition, 1985?Method 412E Cyanide Selective Electrode Method.

£H - All samples that were water soluble were tested withpH strips to determine if they were corrosive as per EPA-600/4-84-038 (May 1984); Characterization of HazardousWaste Sites, Vol. III.

Sulfides - Sulfide analyses were performed according toEPA 600/4-84-038, Characterization of Hazardous WasteSites-A Methods Manual, Hay 1984; Section 17, G.1.2.Determination of Sulfide in Solid Phase Hazardous WasteDisposal Site Samples.

Paint Filter Test - This test was performed on thesamples in accordance with Method 9095, Paint FilterLiquids Test; USEPA SW-846, 2nd edition, July 1982, TestMethods for Evaluating Solid Wastes, Physical/chemicalMethods.

Flash Point - Flash points were performed at 60°Caccording to the procedure specified in USEPA TestMethods for Evaluating Solid wastes, Physical/cHeiicalMethods, SW-846, 2nd edition, July 1982; Method 1020, 'Seta-flash closed-cup Method.

9-24-873

PROJECT S142E


RCRA Parameterso Metals - Samples were prepared and analyzed according to

USEPA Test Methods for Evaluating Solid Hastes, Physical/Chemical Methods, SW-B46, 2nd edition, July 1982. Sampleswere prepared by either Method 3010, 3030, 3050, or 1310as appropriate for the following metals; arsenic, barium,cadmium, chromium, lead, mercury, selenium, and silver.Sample analyses fgr these metals were performed accordingto method 6010, Inductively Coupled Plasma Method (SW-846Proposed Sampling and Analytical Methodologies, 1984).

o Pesticides - Solid sample leachates were analyzed forpesticides according to Standard Methods for the Examina-tion of Water and Wastewater, 16th edition, 1965; Method509A.

o Herbicides - Solid sample leachates were analyzed forpesticides according to Standard Methods for theExamination of Water and Wastewater, 16th edition, 1985;Method 509B.


The following tables detail the results of the variousanalyses performed on Sample I5142E-SC01.

A \\ i u u u 6 b

9-24-674

PROJECT S142E

TABLE 1 - LANDFILL DISPOSAL ANALYSIS

SAMPLE IDENTIFIER: Solid CompositeOHM SAMPLE NUMBER: 5142E-SC01

Parameter Result

Color BrownOdor Strong, SolventFlash Point, SF, CC > 90°CDensity 1.23 gm/cm3

pH Test 6.5 pH units

Total Sulfide < 10 mg/KgTotal Cyanide < 1.0 mg/Kg

Amenable Cyanide , < 1.0 mg/KgTotal Phenols 0.750 mg/Kg

Paint Filter Test , Pass

Total Solids 90.9% by weight

Total Organic Carbons 78,000 mg/Kg

i U i.;

9-24-875

PROJECT S142E

TABLE 2 - VOLATILE ORGAMxCS



Benzene BDLBromomethane BDLBromodichloromethane BDLBromoform BDLCarbon Tetrachloride BDLChlorobenzene BDLChloroethane BDL2-Chloroethylvinyl ether BDLChloroform BDLChloromethane BDLDibromochloromethane BDL1,3-Dichlorobenzene . BDL1,2-Dichlorobenzene BDL1,4-Dichlorobenzene BDL1,1-Dichloroethane ' BDL1,2-Dichloroethane BDL1,1-Dichloroethene BDLTrans-1,2-Dichloroethene BDL1,2-Dichloropropane BDLTotal Dichloropropenes BDLEthylbunzene BDLMethylene Chloride BDL1,1,2,2-Tetrachloroethane BDLTetrachloroethene BDL1,1,1-Trichloroethane BDL1,1,2-Trichloroethane BDLTrichloroethene BDLToluene BDLVinyl Chloride BDL

Limit of Detection • 100 mg/Kg ppm (parts-per-million)BDL • Below Detection Limit

i U 0 0 6 7

9-24-876

PROJECT S142E

TABLE 3 - VOLATILE HSL COMPOUNDS


Concentration DetectionCompound (mg/Kg) Limit (mg/Kg)

Acetone ., BDL 1,000Acrolein BDL 5,000Acrylonitrile BDL 5,0002-Butanone BDL 1,000

Carbon Disulfide BDL 100

Ethyl ether BDL . 1,000Ethylene Dibromide BDL 1,0002-Hexanone BDL 1,000

4-Methyl-2-Pentanone (MIBK) BDL 1,000

Styrene BDL 1,000

Tetrahydrofuran BDL 2,000

l,l,2-Trichloro-l,2,2-trifluoroethane BDL 500

Vinyl Acetate BDL 1,000

mg/Kg • ppm (parts-per-million)BDL - Below Detection Limit

9-24-877

PROJECT S142B

TABLE 4 - VOLATILE SCREEN




flfilO(J069

9-24-878

PROJECT 5142ETABLE 5 -BASE/NEUTRAL' COMPOUNDS


Compound . Concentration (mg/kg)Acenaphthene BDLAcenaphthylene BDLAnthracene BDLBenzo(a)anthracene BDLBenzo(b)fluoranthene BDLBenzo(k)fluoranthene BDLBenzo(a)pyrene BDLBenzo(g,h, Uperylene BDLBis(2-chloroethyl)ether BDLBls(2-chloroethoxy)methane BDLBis(2-ethylhexyl)phthalate BDLBis(2-chloroisopropyl)ether BDL4-Bromophenyl phenyl ether BDLButyl benzyl phthalate BDL2-Chloronaphthalene BDL4-Chlorophwnyl phenyl ether .BDLChrysene BDLDibenzo(a,h)anthracene BDLDi-n-butylphthalate ' BDL1,3-Dichlorobenzene BDL

) 1,4-Dichlorobenzene BDL1,2-Dichlorobenzene BDLDiethylphthalate BDLDimethylphthalate BDL2,4-Dinitrotoluene BDL2,6-Dinitrotoluene BDLDioctylphthalate BDL1,2-Diphenyl hydrazine BDLFluoranthene BDLFluorene BDLHexachlorobenzene BDLHexachlorobutadiene BDLHexachloroethane BDLHexachlorocyclopentadiene BDLIndeno-(l,2,3-cd)pyrene BDLIsophorone BDLNaphthalene BDLNitrobenzene BDLN-Nitrosodi-n-propylamine BDLN-Nitrosodiphenylaraine BDLPhenanthrene BDLPyrene BDL1,2,4-Trichlorobenzene BDLLimit of Detection - 100 mg/kg ppm (parts-per-million)BDL • Below Detection Limit

^100070

9-24-879

PROJECT S142E

TABLE 6 - ACID EXTRACTABLE



4-Chloro-3-Methylphenol BDL

2-Chlorophenol ' BDL

2,4-Dichlorophenol BDL2,4-Dimethylphenol BDL2,4~Dinitrophenol BDL2-Methyl~4,6-Dinitrophenol BDL

2-Nitrophenol BDL

4-Nitrophenol ' BDL

,_1 Pentachlorophenol BDL

Phenol BDL2,4,6-Trichlorophenol BDL

Limit of Detection • 100 mg/Kg ppra (parts-per-raillion)BDL • Below Detection Limit

Aft 100071

9-24-8710

PROJECT 5142E

TABLE 7 - ADDITIONAL SEMI-VOLATILE HSL COMPOUNDS



Aniline BDL

Benzyl Alcohol BDL

4-chloroaniline BDLDibenzofuran BDL2-Methylnaphthalene BDL2-Methylphenol BDL4-Methylphenol ' BDL

2-Nitroaniline , BDL3-Nitroaniline BDL4-Nitroaniline BDL2,4,5-Trichlorophenol BDL

Limit of Detection • 100 mg/Kg ppra (parts-per-million)BDL • Below Detection Limit

riftlOGU72'

9-24-8711

PROJECT 5142E

TABLE 8 - SEMI-VOLATILE SCREEN RESULTS

SAMPLE IDENTIFIER: Solid CompositeOHM SAMPLE NUMBER; 5142E-SC01

Compound Concentration (mg/Kg)• •••••••liWHWHBHII«PIBHP««««BWBWWP>'"*''B'IIB""ll"*B"I>*'l"<*BI — *' —***B** —****"

No chronatographic peaks present with an area greater than 25% ofthe internal standards

V

flfllOOQ73

9-24-8712

PROJECT S142E

TABLE 9 - PESTICIDES AND PCBS

SAMPLE IDENTIFIER:OHM SAMPLE NUMBER:

Concentration DetectionCompound Name mg/Kg Limit mg/Kg

Aldrin BDL 0.1BHC-alpha BDL 0.1BHC-beta BDL 0.1BHC-gamma BDL 0.1BHC-delta BDL 0.1Chlordane BDL 1.04,4'-ODD BDL 0.14,4'-DDE BDL 0.14,4'-DDT BDL 0.1Dieldrin BDL 0.1Endosulfan-alpha BDL 0.1Endosulfan-beta BDL 0.1Endosulfan Sulfate BDL 0.1Endrin 'BDL 0.1Endrin Aldehyde BDL 0.1Heptachlor BDL 0.1Heptachlor Epoxide BDL 0.1Toxaphene BDL 1.0

POLYCHLORINATED BIPHENYLS

Aroclor 1016 BDL 1.0Aroclor 1221 BDL 1.0Aroclor 1232 BDL 1,0Aroclor 1242 125 1.0Aroclor 1248 BDL 1.0Aroclor 1254 BDL 1.0Aroclor 1260 BDL 1.0

mg/Kg • ppm (parts-per-million)BDL • Below Detection Limit

9-24-8713

PROJECT S142E

TABLE 10 - RCRA PARAMETERS

SAMPLE IDENTIFIER: EP Toxicity Leachate; Solid CompositeOHM SAMPLE NUMBER: 5142E-SC01

Concentration DetectionCompound (mg/L) Limit (mg/L)• m H • m mmm m m m m mmmmm m m m H • m m m mmmmmmM* m mm mmmm m m mmmmmmmmm m •••••• ••••)••• i

RCRA Metals

Arsenic BDL 0.1Barium BDL 0,1Cadmium BDL 0.1Chromium BDL 0.1Lead BDL 0.1Mercury BDL 0.05Selenium BDL 0.1Silver BDL 0.1

Pesticides

Lindane BDL 0.001Endrin BDL 0.001Methoxychlor BDL 0,01Toxaphene BDL 0,01

Herbicides

2,4-D BDL 0,012,4,5-TP BDL 0,01

__ . pp (parts-per-_illion)BDL • Below Detection~Limit

9-24-8714

PROJECT 5142E

QC SUMMARY

A. Conventionals analysis:Cyanide-76.0%Chloride-113%

B. GC/MS Priority Pollutant Volatile Organics:BFB Tune File: See attachedSurrogate Recoveries:

Blank1,2-Dichloroethane-d. 106 107 104Benzene-d, Ill 110 104Toluene-d, 116 115 106BFB 108 111 104

Volatile Organics Spike Recoveries: (In Percentages)Benzene 106 101Bromomethane , 103 101Bromodichloromethane 123 111Bromoform 172 146Carbon Tetrachloride 135 125Chlorobenzene 116 109Chloroethane 105 1072-Chloroethylviayl ether 127 115Chloroform 113 113Chloromethane 86.3 99.0Dibromochloromethane 155 1361,2-Dichlorobenzene 113 1041,3-Dichlorobenzene 115 1041,4-Dichlorobenzene 113 1041,1-Dichloroethane 122 1171,2-Dichloroethane 103 96.81,1-Dichloroethene 115 113Trans-1,2-Dichloroethene 103 1021,2-Dichloropropane 122 1091,3-Dichloropropenes 112 105Ethylbenzene 108 101Methylene Chloride 108 1111,1,2,2-Tetrachloroethane 102 88.2Tetrachloroethene 122 1111,1,1-Trichloroethane 112 1051,1,2-Trichloroethane 114 102Trichloroethene 122 116Trichlorofluororaethane 115 115Toluene 106 102 ,Vinyl Chloride 106 107Total Xylenes 118 115

A f t i U U U / 6

9-24-8715

PROJECT 51426


Volatile Organics Spike Recoveries (in Percentages): Continued

Additional CompoundsMethyl ethyl Ketone 93.8 99.0Carbon Disulfide 105 112Acetone 81.0 78.4Methyl Isobutyl Ketone 109 106Methyl Pentanone 97.9 97.0Styrene 108 105

C. GC/MS Priority Pollutant Semi-volatile Organics:DFTPP Tune File: See attachedPercent Surrogate Recoveries:

Blank2-Fluorophenol 89.2 111Phenol-d. 88.2 119Nitrobenzene-d, ' 84.0 1182-Fluorobiphei. A 102 12S2,4,6-Tribromophenol 92.2 > 119

D, Pesticides, Herbicides: Percent Spike Recoveries

Lindane 62.0Toxaphene 59.02,4-D 88.02,4,5-TP 81.0a-BHC 79.6b-BHC 86.3g-BHC 73.0Aldrin . 52.0Heptachlor 85.0E. Metals: Percent Spike Recovecies

Arsenic 101 94.5Barium 96.4 98.5Cadmium 108 106Chromium 104 103Lead 101 99.6Mercury 99.5 97.6Selenium 101 98.8Silver 101 100F. PCBs Percent Recovery: Aroclor 1254; 165%

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36 0 00 0.00 0, Minima Min Inten: 0.282 tt 0 haxima

Man '/. RA 7. RIC Inten. Mass Y. RA X. RIC Inten.

36.00' S 094 0. IB IB 104.00 S 0.31 006 6.37.00? S 9. 66 1.B9 166. 105.00 S 0.57 0. 11 11.36 00? S B. 79 1.72 169. 106.00 S 0.47 0.09 939. 00'' S 2. 91 0. 57 56 109, 00 S 021 0. 01 4.43. 00'1 S 1.37 0. B5 64 11100 S 0,88 0.17 17.44. 00° S S 54 0 44 43 112.00 S 0 BB 0.17 17.45.00"' S 1. 5fc 030 30. 113.00 S 0.47 009 9.47. OC" S 1 93 0.36 37 114.00 S 0 05 0,01 1.46 00" S 0 fcS 0 12 12. 115 00 S 0.36 0.07 7.«9. 00"' S 5.4: 1.06 104 11700 S 0.05 0.01 1.50,00? S £=1.71 5. BO 571 116.00 S 0.52 0.10 10.51. 00"' 5 6. 35 1.64 161 119.00 S 0. 42 0.06 B.52 00? 5 0. 45 0 OB 6 120. 00 S 0. 47 0. 09 9.54.00'' S 0 31 0.06 6. 125.00 S 0.36 0.07 7.56.00? S l.&fc 0.30 30. 126.00 S 0.16 0-03 357.00? S 5.93 1.16 114. 128.00 S 0.47 009 9.58.00? S 1.51 0.29 29, 129.00 S 0 16 0.03 3.60,00? S 0.99 0.19 19 130.00 's 0.26 0,05 5'1.00? £ 4.47 0. 87 86, 132.00 S 0.21 0.04 4.-2.00' 5 A. 53 0.86 B7. 136 00 S 0,16 0,03 3.63.00"' S 4.11 0. BO 79. 141.00 S 0.31 0.06 6.6500? S 0.31 0.06 6. 14300 S 0.62 0.12 12.66 00"' £ 9 31 1.82 179 148.00 S 0.21 0 04 4.-9.00 S S 72 1..90 167. 149.00 S 0.31 0. 06 670 00 S 0 52 0.10 10. 150.00 S 05: 0.10 107200 S 099 0.19 19. 151.00 S 0.26' 0/05 573.00 5 3. BO 0.74 73 152.00 S 0.16 0.03 3.74.00 S 1524 2.96, 293 153.00 S 0.05 0.01 1,75.00 S 5349 10.45 1026 159.00 S 0,10 0.02 2.7600 5 364 0.71 70. 161.00 S 0.05 0.01 1.77,00 S 0 94 0.16 IB. 170.00 S 0.21 0,04 4.78.00' S 0.52 0.10 10 173,00 S 0.5? 0,10 10.79.00 S 3.12 0.61 60. 174,00 S 74.51 14,55 1432,80,00 S 1.30 0.25 25. 175.00 S 4.16 0. 61 80.Bl.OO S 3.07 0,60 59. 176.00 S 73. 7B 14.41 1418.82.00 S 1,61 0,32 31, 177,.00 S 4 16 0.81 BO.63,00 S 0,36 0.07 7, 178.00 S 0.10 0.02 2,84 00 S 0,42 0,08 B 183,00 S 0.05 0,01 1.85.00 S 0,57 0,11 11, 186,00 S 0.10 0,02 2.86,00 S 0.57 0,11 11, 191,00 S 0.52 0,10 10,87,00 S 5,20 1.02 100, 207.00 B 0,26 0.05 5.BB, 00 S 4 53 0,88 87, 210,00 B 0.05 0,01 1.91,00 S 0. BE 0,17 17, 223.00 S 0.05 0,01 ),3. 00 S 2, 03 0, 40 39. 262, 00 S 0, 47 0, 09 9,

TO, 00 S 3.07 0,60 59, 281,00 S 0.16 0.03 3,94,00 S 9,42 1.84 1B1, 282.00 B 0.10 0.02 2.95.00 S 100, 00 19, 53 1922,96 00 S 6. 24 1. 22 120,96 00 S 0.05 0,01 1. ,1,; , ;,. • ; , , ,101.00 S 0.36 0.07 7. "" '^-"JCfU

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m/z Int. m/z Int. . tn/z Int. m/z Int. m/z Int.

39.00 6.23 78.00 3.15 128.95 21.28 198.95 6.79 256.00 6.7244.00 .04 79.00 3.76 129.95 1.66 203.95 2.81 258.00 3.0448.90 .57 79.90 2.35 134.95 1.39 204.95 5.15 273.00 1.6850.00 15.17 81.00 4.03 140.90 2.22 205.95 21.07 274.00 3.7751.00 56,14 92.95 5.34148.00 2.25206.95 2.68275.00 23.3152.00 2.55 97.95 4.04 156.00 1.94 216.95 6.81 276.00 2.6655.90 1.79 98.95 3.37 167.00 4.14 220.95 5.88 277.00 1.6157.00 4.05 100.85 1.75 167.90 1.71 222.95 1.57 296.00 6.1557.90 .93 106.95 12.54 178.90 3.11 224.05 11.93 323.05 2.3162. "0 2.10107.95 1.88180.00 2.13225.05 3.32365.00 2.4164M) .96 109.95 30.20 185.00 1.20 226.95 5.18 423.05 3.9668.90 65.64 110.95 4.38 186.00 11.41 244.05 10.21 441.05 11.5774.00 4,95 116,95 9.75 187.10 3.39 245.05 1.43 442.05 76.9475.00 8,19 122.95 1.34 192.00 .96 246.05 2.10 443.05 13.6776.00 2,70126.95 43.21195.95 3.3 255,.00 .49.34 444.05 1.4177.00 44.86127.95 3.29197.95 100. ftri I UU ij 0_"

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RUN NUMBER jj)_____ QC REPORT NO.________ ANALYST,

me oca: EN

•/c516B

6970127197

J.99275

365

441

442

443

Ion Abundance Criteria30-60% of Bass 196

less than 2% of MSB 69Bass 69 relative abundanceless than 2% of uss 6940-60% of »asc 196less than 1% of uss 196base peak, 100% relative abundance5-9% of BBSS 19610-30% of Base 196greater than 1% of BBSS 196less than Bass 443

greater than 40% of BBSS 19617-23% of BBSS 442

1 Relative Abundance

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a PvtonQinn Ccnlcr lor Eilonsion Morgantown, Wosi VirginiaC UAICIlorulI and Conlinuing Education 26506Service

West VirginiaUniversity July 7, 1986

HEMOHANDUH

To: Dr. A. L. BarrAssociate Director, HVAFES

From: Charles B. Sperow, J,Extension Specialist

Subject: Corn Injury/At Chemicals at Former Ohio Valley -Experiment Farm

1, Corn Injury

The corn In question was examined and I JM MM onthe corn plants or on weeds In the field which. »uii*i t •<),h«rblold« Injury. Corn plants in the severely affected areasand throughout n<uch of the field showed Btfcn«*lUB .d«fioi«noysymptoms, Soil wiplts were ttker which should Indicate whethermagnesium deficiency resulted from low soil magnesium or lowavailability due to excessively acid soil,

Except for suspected low pH, corn production practicesappeared good. Tom Rouah, resident Manager, reported thefollowing:

Pioneer 3179Planted a3-26 Hay, 36" rona1501 N as anhydrous ammonia3001 10-20-20 broadcast110* 10-20-20 In planter5 1/2f/aore Furadan 15Q1 _al Eradloane per acre incorporatedAtrezire ?rd slmazlne (no rate stated) pre-emergence

Stand counts taken on 3 July showed populations of 25.6and 22.6 thousand plants per acre In tht "normal" and affectedareas, respectively. "Normal" plants were at growth stageV10/V11 which would predict a planting date of 19-26 May whichcorrelated with stated planting date.

rl U i U (.• ij _ Du'uo by inu won Vi'g>nni univuiidy CODOUM^O riiuri'jion Soivico nrc iiv.iii.iDiti to W pv'aons niinout ia<jmn 10 MCII coioi

101 nfliicn.ii oi.r>n (xnanocsp

Cooperative Extension Service aXf.iS.,lonWest Virginia University

MEMORANDUM

To: Dr. A. L. BarrAssociate Director, WVAFES

Date: July 9, 1986

From: Charles B. Sperow I _Extension Specialist-agronomy

Subject: Follow-up of Corn Injury/Ag Chemicals Memorandum of 7July

1. Soil Test Results

SampleNo, pH P ' K Ca Mg

"Affected" 1 3.-,9 110 304 210 233 4.0 143 256 90 185 ' J..» 106 256 120 1*

"Normal" 2 M 154 416 740 564 4.4 97 212 400 966 4.4 94 316 450 2?oi-. f 7"

>Jft2. (a) In^vtry initanc*. the u*pl*-tren th»

"affaaud" site was l pel,ia.l <«vd.,i|«gaa«ip) than that from the"normal" site.

(b) Available iwgnasiuo and pH arc cxtreuwly lows, For corn the ptl should be at least pH 6.2 and

available magnesium should be greater than 100,

(c) %»»• *mly»o confirm th« Mrli«r di«|nosisat.

cc: Or, Barton BakerDr, Steve BlizzardGeorge SticklerTom Roust)Carl Cook

CBS/drw

Wcsl Virginia Univorsily. U.S. Qop«nnranl ol Aonculliiro, nnd Wcsl Virginia Counllos Coopornllng

Eciml OpfwnunilxMIIirmnVm) Xciiod'lltlllMiiM D

Cooperative Extension ServiceWest Virginia University courthouse Annex

Point Pleasant, WV 25550July 9, 1986

Mr. Albert T, Kouah, Jr.Acting Farm ManagerLakin State FarmLakin, WV 25250

Dear Tom,i

I received the letter you sent to George Stickler, Farm Director,yesterday July 8,:,nnd would like to comet a few statements containedin the correspondence concerning the corn problem at the old ExperimentalStation.

Our preliminary or auapacted problem was related to the soil, Thiswe suggested a'sample be sent to the Wait Virginia DipartnenC of Agriculturelabs in Charleston for analysis, The corn was dying In an unusual patternthat would and did raise a question of underground water problems.

We did point out the dump Biti in a daprtnlon on the hill abova thtproblea area, but did not indicate that pesticides had been disposed therewhen the station was closed down,

We found a few (Chr«* or four) 55 gallon dru|S setting In the fieldapproximately 30 faac fron the dump ai|| that contained •Ustilcal aqul.raentand an unknown liquid. i.'.Some drums were open and I think acme had tops intact.I do not recall finding any smaller containers at the site.

We found a variety of chemicals and unknown materials in the buildingsaround the shop area. These art now beingTemovid.

We did not determine that runoff from the dump was causing the problem,only a possibility.

We talked about acveral possibilities, but did not dttirnine the exactcauia,-

As a follow up, we had our Extension Specialist-Agronomy, Charlie Sperow,visit the uite to help determine possible causes. I am sure he will be Intouch with you,

Sincerely,

Carl 11. CookExtension Agent

George SticklerCharlie Sperow

Wcsl Virginm univtirjily. U S Dupiuimeni ol Agriculluru, iinil West Virginia Counlins Coopuinlmg

Injured corn plants may partially recover. Previousexperience haa shown that aa the season progreaaea and pHdepression from nitrogen fertilizer becomes leaa pronouncedplant roots will take up sufficient magnesium to resume nearnormal growth. If the situation la due to an absolute lack ofmagnesium and not to pH recovery will be alight or none,

The areas in the field showing injury, on casual examination(especially when viewed from the tobacco barn area), appeared tofollow drainage patterns, However, the patterns followed naturallandforaa other than water courses. On the very aandy aoilaalight and subtle changes in pH, magnesium, organic matter,texture and/or water holding capacity can exert draaatioinfluence on plant growth. It »ay b« that_thi.p(i_q)ttaDgeo_»rB tooBBilOo..b«..deta.qiedJ>y our jp.il tutil*~

2. On-alte Ag Chemicals

a, The old office building, farm shop, machine storageand fertilizer barn wore Inspected for the presence of farmchemicals. The tobacco barn waa Inspected except for theupatairs storage room and the conditioning room. There waa noelectricity in the building and these two dark rooms could notbe inspected. No chemicals were found in the parts examined.

b, Materials found In the office, shop and machine shedwere placed in plastic garbage oana. In addition to farochemicals, aome aoap and unlabelled jara with unidentifiedcontents from the office building were also placed In theplaatio oana, A summary of materials removed follows:

Description Amount

Gallons Pounds

Amidea

Thiooarbonatea 2.5

i'.'\ •• <f i.-.1.''"''.', Eptan, EradloaneVernan, Knoxweed

Phenoxya and benzoles,1- . 9 K *•'"*Eateron 245 ~W* '

Seaone luli'mn /,'r- i;ck\°iv \ <>.t",:Banvel n-mfU'oty -y,h"Air\\i/td ben-talc

Hitfilea 0.7

Bromoxynll Cl\tarJ'n\\<;f'arn\

J-l i i i U '-• i.) ij (j

V

Methanearaonate 0.5

Ansal

Miscellaneous 1.1 2.5

Mon 2139, Karail,Off-Shoot, Clobber, , ,,,iv i-mr"''/ ' ''.' '-Dikar, Solan M^wwWW

Pressurized Cylinder*

Trizone ?

Unidentified

Granular 2 x 50 Ib.druma, 1 intact, 1 disintegrated

Office Building Tobacco Chemicals

20 Jars, 1 qt. or less of varioustobacco sucker control chemicals

(In the machine storage building, there were 11 emptycontainers in various states of decomposition.)

Total obwioals: 6.6 gal of liquids9 pounds of pwdtri and oryatali

'May be hazardous because of pressure and ruaty condition.

o. Three of the four garbage cana were transported to theHorticulture Farm at Morgantown. The fourth can could not beloaded and was left In the machine ahed at Point Pleasant.

d. The dump area back of the tobacco barn was examined,The alte waa mostly covered and was overgrown with vegetation,It was impossible to determine what was contained in the dumpsite.

e. Adjacent to the dump alte there were fpur 55 galloi<l Nn*t WP»M«<I to b« tranaforaer* ,, Adjacent to the barrels waa an

iiaui [iliuiit iJMl^flTTwnfr'hf unidentified natter, Thla could behazardous material. It's source is not known.

f, There was a 55 gallon barrel in the machine shed whichcontained no identification. It was in too fragile condition toattempt to move. Subsequent conversation with Clint Hlokmanindicated that it may contain waste oil.

i' i :

3. V. Va, Farm Conmlaalon actions

a. A soil sample waa taken from the crop area between thefarm shop and the fertilizer barn for pesticide residueanalysis,

b, A water sample waa taken at the old brick residence.The source of thla water was the irrigation well, The waterwill be tested for possible ground water contamination bypesticide.

1, It la not expected that any pesticide reaidues will be foundin the water sample. The soil sample will probably showreaidues of the pesticides recently applied but none other. Thekind and amount of pesticides found present no potential soilpollution or ground water hazard,

5. Vet to be done:

a. Diipoae of naterial* brought fron Point Pleasant.Steve Blizzard 'should be able to handle this,

b, Bring the rMalnins can from Point Pleasant and dlapea*of it properly.

o, Identify contents of the 55 galloa drua at feintPleaeaat and take appropriate action.

d, Peternin* if druia oontalalai trwafonier parta weredlapoaed of by HTO and take

00: Dr. Barton BakerDr. Steve BlizzardGeorge SticklerTon RouahCarl Cook

tTATEOFWCtTVIRQINIADEPARTMENT OF NATURAL RESOURCES

CHAIU.HTON JWOS

ARCHA,MQORI>,JR, Division of Waste Management RONALD R. POTESTAa«iri»r 1260 Greenbrler Street DirKi«

Charleston, West Virginia 25311 MICHAHA,ROTOSOoputy Director

Mr. Ben Wilmoth November 5, 1986U.S. EPA303 Methodist Bldg.Wheeling, WV 26003 Re: Lakin State Farm

Dear Ben:Enclosed are the results of our soil analyses at Lakin State Farm.

The detection limits on some of these parameters Is.high. Apparentlythe samples were "dirty" and this is the best the lab can do. 1 am toldthat the "u" designation means that the substance may have detected but

) not quantified. As a result, I propose that more sampling be done.Hopefully some samples in the clump area may be taken, I have asked thata complete history be worked up on the site as well as information onthe Irrigation well. 1 mentioned in my letter to Agriculture that EPAWFO was sent a copy of the results.

Very £ru)y vours,

Pamela D. HayesSection LeaderSite Investigation

and ResponseDivision of Waste Management

RDM/milEnclosures

t . cc Ron Potesta

;'•; i U U 0 3

WV DEPARTMENT OR NATURAL RESOURCESDIVISION OF WATER RESOURCES

~ GUTHRIE CENTER LABORATORY' 4000 Bronda Lane, Charleston, WV 26312

(304) 34Q.4057

ORGANICS ANALYSIS DATA SHEET

Branch Submitting Sample: ____UA-4 A* 0 a31_y ^ A j T <s_____Program for Which Samples are to be Analyzed: __Inspector Taking Sample: _____i'Ansi« oDate Sample Was Taken: ______•*-Z7-K£Date Sample Received: i______'s-l.^ ••*£_Sample Matrix: _________sen.____Sample Containers & Amounts: i «Ph of Sample BtXolUwtW: ____S,'{.Field Sample Ph Adjustment and Preservation: _Type of Analysis Requested: ____n^Sample Parameters Requested: ______Field Sample Identification Number: o.

Laboratory Comments: _____________

Sample Analysis Reported to:: L-UC..(Q~ It) iJ Ti VvY A^ - NdDate Sample Was Reported: /O - I — Q gi

Data Release Authorized by:,

RECEIVEDOCT 319M

l if "iiuniPlvnlon »r Hnlt Wa

Laboratory Chief

QCLForml.Q**• l>86


VOLATILE COMPOUNDS

CASNumber

67-64-1107-02-8107-13-171-43-275-27-475-25-274-83-978-93-375-15-056-23-5108-90-775-00-3110-75-867-66-374-87-3124-48-194-50-1

541-73-1106-46-775-34-3107-06-274-35-4156-60-578-87-5

COMPOUNDNAME

AcetoneAcroleinAcrylonitrileBenzeneBromodichloromethaneBromoformBromomethane2 • ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChloroethane2 • Chloroethyl vinyl etherChloroformChloromethaneDlbromochloromethane1,2- Dichlorobenzene1, 3- Dichlorobenzene1,4- Dichlorcbenzene1 , 1 - Dichloroethane1,2- Dichloroethane1, 1 • Dichloroethenetrans- 1,2- Dichloroethene1, 2- Dichloropropane

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GCL Form 1.21-86


VOLATILE COMPOUNDS

CASNumber

10061-02-5

10061-02-6

100-41-4591-78-6

75-09-2108-10-1

79-34-5

127-18-4108-88-371-55-679-00-579-10-6100-42-5108-05-475-01-495-47-6108-38-3106-42-3

COMPOUNDNAME

cls-1,3- Dichloropropenetrans- 1, 3 • DichloropropeneEthylbenzene2 • HexanoneMethylene chloride4 • Methyl • 2- pentanone1, 1,2, 2 • TetrachloroethaneTetrachloroetheneToluene1, 1, 1 • Trichloroethane1, 1,2- TrichloroethaneTrlchloroetneneStyreneVinyl acetateVinyl chlorideo-Xylenem-Xylenep-Xylene

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1 CU

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(CM

GCL Form 1,31-86

ORQANICS ANALYSIS DATA SHEET

SEMIVOLATILE COMPOUNDS

CASNumber

83-32-9208-96-862-53-3120-12-792-87-556-55-3205-99-2207-08-9191-24-250-32-865-85-0100-51-6

111-91-1

111-44-439638-32-9

117-81-7101-55-385-68-7

106-47-859-50-791-58-795-57-8

7005-72-3218-01-9

COMPOUNDNAME

AcenaphtheneAcenaphthyleneAnilineAnthraceneBenzldineBenzo (a) anthraceneBenzo (b) fluorantheneBenzo (k) fluorantheneBenzo (ghi) peryleneBenzo (a) pyreneBenzole acidBenzyl alcoholBis ( • 2- chloroethoxy) methaneBis ( • 2- chloroeihyl) etherBis ( • 2- chloroisopropyl) etherBis ( • 2- ethylhexyl) phthalate4 • Bromophenyl phenyl ether>4HNMfiJMiPii A: 'v'' ""• , • -•• 'v- --''1' ''-"4-Chloroaniline4 • Chloro -3- methylphenol2 • Chloronaphthalene2 • Chlorophenol4- Chlorophenyl phenyl etherChrysene

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1-86



CASNumber

53-70-3132-64-995-50-1541-73-1106-46-791-94-1

120-83-284-66-2105-67-9131-11-384-74-2534-52-151-28-5121-14-2606.20.2117-84-0206-44-086-73-7118-74-187-68-377-47-467-72-1193-39-578-59-1

COMPOUNDNAME

Dibenzo (a, hi anthraceneDibenzofuran1, 2 - Dichlorobenzene1, 3- Dlchlorobenzena1, 4 • Dichlorobenzene3, 3' • Dichlorobenzidine2,4 • DichlorophenolDiethyl phthalate2, 4-DimethylphenolDimethyl phthalateDi-n-butyl phthalate4, 6 • Dinitro • 2 • methylphenol2, 4 • Dinitrophenol2, 4 • Dinltrotoluene2, 6-DinitrotolueneDl-n-octyl phthalateFluorantheneFluoreneHexachlorobenzeneHexachlorobutadieneHexachlorocyclopentadieneHexachloroethaneIndeno (1,2, 3-cd)pyreneIsophorone

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GCLForm1'7 ..„„;•' 1-86



CASNumber

91-57-695-48-7106-44-591-20-388-74-4

99-09-2100-01.6

98-95-3

88-75-5

100-02-762-75-9621-64-786-30-6

87-86-585-01-8

108-95-2

129-00-0

120-82-195-95-488-06-2

COMPOUNDNAME

2 • Methylnaphthalene2 • Methylphenol4 • MethylphenolNaphthalene2-Nitroanillne3 • Nitroaniline4- NitroanilineNitrobenzene2-Nitrophenol4 • NitrophenolN-NitrosodimethylamineN-Nitrosodi-n-propylamlneN-Nitrosodiphenylamine (1)PentachlorophenolPhenanthrenePhenolPyrene1,2, 4-Trichlorobenzene2, 4, 5 • Trichlorophenol2, 4, 6 • Trichlorophenol

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GCL Form 1,8


PESTICIDES AND PCB'S

CASNumber

309-00-2

319-84-6319-85-7

57-74-972-54-872-55-950-29-3

819-86-860-57-1959-98-9

33213-65-9

' 1031-07-8

72-20-87421-93-453494-70-5

58-89-976-44-8

1024-57-372-43-5

12574-11-211104-28-211141-16-563469-21-912672-29-611097-69-111096-82-5

8001-35-2

COMPOUNDNAME

Al.drinAlpha -BHCBeta • BHCChlordane4, 4' • ODD4, 4' • DDE4, 4' • DOTDelta • BHCDieldrinEndosulfan IEndosulfanllEndosulfan SulfateEndrinEndrin AldehydeEndrin KetoneGamma-BHC (lindane)HeptachlorHeptachlor EpoxideMethoxychlorPCB- 1016PCS- 1221PCB -1232PCB • 1242PCB • 1248PCB -1254PCB -1260Toxaphene

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•3.-5UGCL Form 1.10

l'iiU-U'JU 1-86


DATA REPORTING QUALIFIERS

One or more of the following specific data qualifiers were used in reporting results,

U • Indicates the parameter was analyzed for but was not detected, The detection limit (Note1,) for the parameter was reported followed by a U leg., 10U),

J • Indicates the presence of a parameter which met the identification criteria but was presentat a concentration less than the detection limit.

E- Indicates an estimated concentration for a tentatively identified compound where a 1:1response to an internal standard was assumed,

C- Indicates trie identification of a parameter was confired by GC/MS, This qualifier wasapplied only to parameters which were not analyzed by a GC/MS method,

B • Indicates the parameter was present In the method blank as well as the sample, The reportedresult should be viewed with caution and should be considered to be of questionable value,

X • Indicates the parameter was identified and/or quantitated after the designated holding timespecified in the methodology, The reported result was for Informational purposes only,

Note 1: The laboratory has established minimum target values for each parameter, These valuesreflect the lower limits the laboratory expects to achieve on routine samples and for which thereis a high level of confidence in the results, These are not necessarily the method or instrumentdetection limits, The actual detection limits used with the U qualifier will be dependent on theparticular sample and the concentration/dilution actions required to perform the analysis withinthe working range of the instrument(s), The detection limits for a sample will be the minimumtarget values or some multiple of the minimum target values,

Note 2: The reported results are not corrected for recoveries.

Note 3: All soil sample results are reported on a dry weight basis,

GCL Form 1,4Rev, 4-86,

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3 3:x n3 s

WV DEPARTMENT OF NATURAL RESOURCESDIVISION OF WATER RESOURCESGUTHRIE CENTER LABORATORY

4900 Brenda Lane, Charleston, WV 25312(304) 348-4057


Branch Submitting Sample; ___n/>j<ygpaus uiftCT^______Program for Which Samples are to be Analyzed: ___iInspector Taking Sample: _____PnHf<.n t) nDate Sample Was Taken: _____t-i7-*ilDate Sample Received:______y. 1% -KCSample Matrix: _________S.QI i_____Sample Containers & Amounts: \ x ft e. .Ph of Sample ol Collection: ____'j.lField Sample Ph Adjustment and Preservation: __________Type of Analysis Requested: ____AU f r t i < - t i i v rt^uSample Parameters Requested:Field Sample Identification Number: pt LAICIU M7«Tg

Laboratory Comments: ____________________

Sample Analysis Reported to: LuCJO. \aJTl\/tY£)c>-~jia'2a-yaQ.li4Date Sample Was Reported: 10 — / — Ql/>__________________________

Data Release Authorized by: __________Laboratory Chief

RECEIVEDQCT 31986

tuil Mnnnft wilt uri'srs'

QCLForm 1.0;;M ! 1-66



One or more of the following specific data qualifiers were used in reporting results.

U • Indicates the parameter was analyzed for but was not detected, The detection limit (Note1.) lor the parameter was reported followed by a U (eg,, 10U).

J • Indicates the presence of a parameter which met the identification criteria but was presentat a concentration less than the detection limit,

E- Indicates an estimated concentration for a tentatively identified compound where a 1:1response to an internal standard was assumed.

C- Indicates the identification of a parameter was confired by GC/MS, This qualifier wasapplied only to parameters which were not analyzed by a GC/MS method.

B • Indicates the parameter was present In the method blank as well as the sample. The reportedresult should be viewed with caution and should be considered to be of questionable value,

X • Indicates the parameter was identified and/or quantltated after the designated holding timespecified in the methodology, The reported result was for informational purposes only.

Note 1: The laboratory has established minimum target values for each parameter, These valuesreflect the lower limits the laboratory expects to achieve on routine samples and for which thereis a high level of confidence in the results, These are hot necessarily the method or instrumentdetection limits, The actual detection limits used with the U qualifier will be dependent on theparticular sample and the concentration/dilution actions required to perform the analysis withinthe working range of the instrument(s). The detection limits for a sample will be the minimumtarget values or some multiple of the minimum target values,

Note 2: The reported results are not corrected for recoveries,


GCL Form 1.4Rev. 4-86.

I u - I U i.



GASNumber

309-00-2319-84-6319-85-757-74-972-54-872-55-950-29-3

819-86-860-57-1959-98-9

33213-65-91031-07-872-20-8

7421-93-453494-70-5

58-89-976-44-8

1024-57-372-43-5

12574-11-211104-28-211141-16-553469-21-912672-29-611097-69-11 1096-82-5

8001-35-2

COMPOUNDNAME

AldrinAlpha- BHCBeta • BHCChlordane4, 4' • ODD4, 4' • DDE4, 4' • DOTDelta -BMCDialdrinEndosulfan 1Endosulfan IIEndosulfan SulfateEndrinEndrin AldehydeEndrin KetoneGamma-BHC (lindane)HeptachlorHeptachlor EpoxideMethoxychlorPCB • 1016PCB- 1221PCB -1232PCB -1242PCB • 1248PCB -1254PCB • 1260Toxaphene

ug/Kg.••us/I

I.Sf U

liSwI.«U3.5 UI.T/W

!*<• iI-5&l.«uC6-%l.tflA

i.fcuAUHI.SWU'U

l. WI.XMI,«U

3SUJStf.;..

^M

JS4-';?SM3SIA

1SU35 W•liu

GCL Form 1.10M . l l I'86



CASNumber

91-57-6

95-48-7

106-44-5' 91-20-3

88-74-499-09-2100-01-698-95-3

88-75-5

100-02-762-75-9621-64-786-30-687-86-585-01-8108-95-2129-00-0120-82-195-95-488-06-2

COMPOUNDNAME

2 • Methylnaphthalene ^2 • Methylphenol4 • MethylphenolNaphthalene2- Nitroaniline3- Nitroaniline4- NitroanilineNitrobenzene2 • Nitrophenol4- NitrophenolN-NitrosodimethylamineN-Nltrosodi-n-propylamineN-Nitrosodiphenylamine (1)PentachlorophenolPhenanthrenePhenolPyrene1, 2, 4 • Trichlorobenzene2, 4, 5 • Trichlorophenol2, 4, 6- Trichlorophenol

ug/Kg.*>g/fc-

•'.'So M3S(m3SCU

310-1

KOCH

l«00-l

IfiC&U

3 SOU

700 M

me -.700U

isou,3SCH

1 !jOQ W

3 SOU

•a'iOH

3^aM3SCM

1.SPH

3SCU

(1) • Cannot be separated from diphenylamine.

GCL Form 1,8li86



CASNumber

53-70-3

132-64-995-50-1541-73-1106-46-7

91-94-1

120-82-284-66-2105-67-9131-11-384-74-2534-52-151-28-5121-14-2606-20-2117-84-0206-44-086-73-7118-74-187-68-377-47-467-72-1193-39-578-59-1

COMPOUNDNAME

Dibenzo (a, h) anthraceneDibenzofuran1,2- Dichlorobenzene1,3- Dichlorobenzene1,4- Dichlorobenzene3, 3' • Dichlorobenzidlne2,4 • DichlorophenolDiethyl phthalate2, 4 • DimethylphenolDimethyl phthalateDi-n-butyl phthalate4, 6 • Dinitro • 2 • methylphenol2, 4 • Dinitrophenol2, 4 • Dinitrotoluene2,6- DinitrotolueneDi-n-octyl phthalateFluorantheneFluoreneHexachlorobenzeneHexachlorobutadieneHexachlorocyc I opentadieneHexachloroethanelndeno(1,2, 3-cd) pyreneIsophorone

ug/Kg,uy/L

1 tfOOU

350 14

•JSouiSOM

350W

3SCH

isou.IftOGW

T SOU

3S6M

35GH

.TSOU

TSC.I

3SOM

TSOU

MOaT;OUI%OCU

3.50 W.

GCL Form 1,71-00



CASNumber

83-32-9208-96-8

62-53-3

120-12-792-87-556-55-3205-99-2207-08-9191-24-250-32-865-85-0100-51-6111-91-1

111-44-439638-32-9

117-81-7101-55-385-68-7106-47-859-50-7

91-58-795-57-8

7005-72-3218-01-9

COMPOUNDNAME

AcenaphtheneAcenaphthyleneAnilineAnthraceneBenzidineBenzo (a) anthraceneBenzo (b) fluorantheneBenzo (k) fluorantheneBenzo (ghi) peryleneBenzo (a) pyreneBenzole acidBenzyl alcoholBis ( • 2- chloroethoxy) methaneBis ( • 2- chloroethyl) etherBis ( • 2- chloroisopropyl) etherBis ( • 2- ethylhexyl) phthalate4 • Bromophenyl phenyl etherHH0M i4-Chloroaniiine4 -Chloro -3- methylphenol2 • Chloronaphthalene2 • Chlorophenol4- Chlorophenyl phenyl etherChrysene

ug/Kg.-_9it--

•; o u.isauIVOCU

•JSOU

3SCM•3S.OU

T.scuitfooa700 L\

3S0U3SOM

3SO-I

TSOy

•.',. DU35CM

2SOU

3 SOU

350M

•iSOU,

3SOU3 SO ^-V

GCL- Form 1.6•. • . , : ,,- 1-86'•• n , v C' I o 0


VOLATILE COMPOUNDS

CASNumber

10061-02-5

10061-02-6

100-41-4591-78-6

75-09-2

108-10-1

79-34-5127-18-4108-88-371-55-679-00-579-10-6100-42-5108-05-475-01-495-47-6108-38-3

106-42-3

COMPOUNDNAME

cis-1, 3- Dichloropropenetrans- 1,3- DichloropropeneEthylbenzene2 • HexanoneMethylene chloride4 • Methyl • 2- pentanone1, 1,2, 2 • TetrachloroethaneTetrachloroetheneToluene1,1,1- Trichloroethane1, 1, 2 • TrichloroethaneTrichloroetheneStyreneVinyl acetateVinyl chlorideo-Xylenem-Xylenep-Xylene

ug/Kg,-n.it-

II WII W

M

l i e u

I I M

IIU\IUI I UnuII U

II W

II UHWII U

GCL Form 1,31-86


VOLATILE COMPOUNDS

CASNumber

67-64-1107-02-8107-13-171-43-275-27-475-25-274-83-978-93-375-15-056-23-5108-90-775-00-3

110-75-867-66-3

74-87-3124-48-194-50-1541-73-1106-46-775-34-3107-06-274-35-4156-60-578-87-5

COMPOUNDNAME

AcetoneAcroleinAcrylonitrileBenzeneBromodichloromethaneBromoformBromomethane2-ButanoneCarbon dlsul'WeCarbon tetrachlorldeChlorobenzeneChloroethane2 • Chloroethyl vinyl etherChloroformChloromethaneDibromochloromethane1, 2- Dichlorobenzene1,3- Dichlorobenzene1,4- Dichlorobenzene1, 1 • Dichloroethane1, 2 • Dichloroethane1 , 1 - Dichloroethenetrans- 1,2- Dichloroethene1, 2 • Dlchloropropane

ug/Kg,-«*<fc-

II UII -AII Ul l u

IIU.

I I UII W

IIU

noUIIU

IIU

IIU

IIU

l l uI I U

55 14

IIUI I U

GCL Form 1.21-86

rln I U'J i UU

WV DEPARTMENT OF NATURAL RESOURCESDIVISION OF WATER RESOURCE-5QUTHRIE CENTER LABORATORY

4900 Brenda Lane, Charleston, WV 25312|304| 348.4037


Branch Submitting Sample: n A-?-ft rc o Q 1 r> tj/\vrg________Program for Which Samples are to be Analyzed: c. s ft f 11\Inspector Taking Sample: _____I'misiA ft HA/SSDate Sample Was Taken: ______K -fl-^c_________Date Sample Received: ______K- ?•»•<<.Sample Matrix: __________jjc <«.Sample Containers & Amounts: ___I xPh of Sample H Collection: ____S.'iField Sample, Ph Adjustment and Preservation: ___________________Typn of Analysis Requested: ____AII I'tio^n-r <>ovL-rn ~TSample Parameters Requested: ____________________Field Sample Identification Number:

, Laboratory Comments:

Sample Analysis Reported to: L U f.10. l£> fJ 11 l/-tYQ S " rTQ "2.&Y(l&Us)Date Sample Was Reported: ID- I— &V_____________________

Data Release Authorized by: mLaboratory Chief

RECEIVEDOCT 31966

GCL Form Ifl.; , : j _ j j_ C;



One or more of the following specific data qualifiers were used in reporting results,

U • Indicates the parameter was analyzed for but was not detected, The detection limit (Note1,) for the parameter was reported followed by a U (eg,, 10U),


E- Indicates an estimated concentration for a tentatively identified compound where a 1:1response to an internal standard was assumed,

C- Indicates the identification of a parameter was confired by GC/MS, This qualifier wasapplied only to parameters which were not analyzed by a GC/MS method.

B • I ndicates the parameter was present in the method blank as well as the sample, The reportedresult should be viewed with caution and should be considered to be of questionable value,

X • Indicates the parameter was identified and/or quantitated after the designated holding timespecified in the methodology, The reported result was for Informational purposes only.

Note 1: The laboratory has established minimum target values for each parameter, These valuesreflect the lower limits the laboratory expects to achieve on routine samples and for which thereis a high level of confidence in the results, These are not necessarily the method or instrumentdetection limits, The actual detection limits used with the U qualifier will be dependent on theparticular sample and the concentration/dilution actions required to perform the analysis withinthe working range of the instrument(s), The detection limits for a sample will be the minimumtarget values or some multiple of the minimum target values,



GCL Form 1.4Rev. 4-86,

u u i

QRGANICS ANALYSIS DATA SHEET


CASNumber

309-00-2

319-84-6319-85-757-74-972-54-872-55-950-29-3

819-86-8

60-57-1959-98-9

33213-65-91031-07-872-20-8

7421-93-453494-70-5

58-89-9

76-44-81024-57-372-43-5

12574-11-211104-28-211141-16-563469-21-912672-29-611097-69-111096-82-5

8001-35-2

COMPOUNDNAME

AldrinAlpha- BHCBeta- BHCChlordane4, 4'- ODD4, 4' -DDE4, 41 • DOTDelta -BMCDieldrinEndosulfan 1Endosulfan IIEndowlfanSulfateEndrinEndrin AldehydeEndrin KetoneGamma-BHC (lindane)HeptachlorHeptachlor EpoxideMethoxychlorPCB -1016PCS- 1221PCB -1232.PCB -1242PCB -1248PCB -1254PCB -1260Toxaphene

ug/Kg,-u*4r

I.V W

i.sruI.5TU37W

l.*tl,'

(5 1

— LH—I.»U

—— LH ——i.fcUuuUWI.VUI.VU

l.ifU'I.VH

l.'ifM

T7 vA37 M37 U

4?u17 U.

37W3),iA•J7U•37 VA

1-86

ORGANICS ANALYSIS DATASHEET


CASNumber

91-57-6

95-48-7

106-44-5

' 91-20-3

88-74-499-09-2100-01-6

98-95-3

88-75-5

100-02-762-75-9621-64-786-30-687-86-585-01-8108-95-2129-00-0

120-82-1

95-95-4

88-06-2

COMPOUNDNAME

2 • Methylnaphthalene2 • Methylphenol4- MethylphenolNaphthalene2- Nitr'wniline3- Nitroaniline4- NitroanilineNitrobenzene2- Nitrophenol4- NitrophenolN-NitrosodlmethylamineN-N itrosodi-n-propylamineN-Nitrosodlphenylamine (1)PentachlorophenolPhenanthrenePhenolPyrene1,2, 4 • Trichlorobenzene2, 4, 5 • Trichlorophenol2, 4, 6 • Trichlorophenol

ug/Kg,-«9/U

}?OU

370U

370U

370

U'OOW, '

l%00>4

I'KiJoW37CU.

7'JOM

I&OCU

7^0M

^>OU

3?OU

I^OO-(

370W

•370W

3?OW

T7CW

"\Vft-.

T/OU

• Cannot be separated from dlphenylamine,

GCL Form 1,8

ORGANICS ANALYSIS DATASHEET


CASNumber

53-70-3

132-64-995-50-1541-73-1106-46-791-94-1

120-83-284-66-2105-67-9131-11-384-74-2534-52-151-28-5121-14-2606-20-2117-84-0206-44-086-73-7118-74-187-68-3

77-47-4

67-72-1193-39-578-59-1

COMPOUNDNAME

Dibenzo (a, h) anthraceneDibenzofuran1,2- Dichlorobenzene1,3- Dichlorobenzene1,4- Dichlorobenzene3, 3' • Dichlorobenzidine2,4 • DichlorophenolDiethyl phthalate2, 4 • Dimethylphenol 'Dimethyl phthalateDi-n-butyl phthalate4, 6 • Dinitro • 2 • methylphenol2, 4 • Dinitrophenol2, 4 • Dinitrotoluene2,6- DinitrotolueneDi-n-octyl phthalateFluorantheneFluoreneHexachlorobenzeneHexachlorobutadieneHexachlorocyclopentadieneHexachloroethaneIndeno (1,2, 3-cd) pyreneIsophorone

ug/Kg,•UJ/L-

I fOCU

37C lA

170U

J70H

37CU

37CU

370U

1*00 vA

370 -t

370U

}70U

370M

370U

^OU

37dU

3toU

J?CU

KCOU

370M

GCL Form 1,7



CASNumber

83-32-9208-96-862-53-3120-12-792-87-556-55-3

205-99-2207-08-9191-24-250-32-865-85-0100-51-6111-91-1111-44-4

39638-32-9

117-81-7101-55-385-68-7106-47-859:50-791-58-795-57-8

7005-72-3218-01-9

COMPOUNDNAME

AcenaphtheneAcenaphthyleneAnilineAnthraceneBenzidlneBenzo (a) anthraceneBenzo (b) fluorantheneBenzo (k) fluorantheneBenzo (ghi) peryleneBenzo (a) pyreneBenzole acidBenzyl alcoholBis ( • 2- chloroethoxy) methaneBis ( • 2- chloroethyl) etherBis ( • 2- chloroisopropyl) etherBis ( • 2- ethylhexyl) phthalate4 • Bromophenyl phenyl ether

••••••04-Chloroaniline4 • Chloro -3- methylphenol2 • Chloronaphthalene2 • Chlorophenol4- Chlorophenyl phenyl etherChrysene

ug/Kg,-«*<U

3 >0 w370 U

I r<fl 0 U

370 M

370U,

170 IA

370U

ItfOO W

730 U

17011

.170•nou.370W

3?0\.\

.370U

jmmg'170U

370 -<

370U

.170U

170U

170 U

GCL- Form 1,6 , . j


VOLATILE COMPOUNDS LAB SAMPLE ffGCL. Z^l-S

1 CASNumber

10061-02-5

10061-02-6

100-41-4591-78-675-09-2108-10-179-34-5127-18-4108-88-371-55-679-00-579-10-6100-42-5108-05-475-01-495-47-6108-38-3106-42-3

COMPOUNDNAME

cis-1, 3 • Dichloropropenetrans- 1, 3 • DichloropropeneEthylbenzene2 • HexanoneMethylene chloride4 • Methyl • 2- pentanone1, 1, 2, 2 • TetrachloroethaneTetrachloroetneneToluene1, 1, 1 • Trichloroethane1, 1,2- TrichloroethaneTrlchloroetheneStyreneVinyl acetateVinyl chlorideo-Xylenem-Xylenep-Xylene

ug/Kg,-«3Ar

\l UU UIIU

MOW

\l wIIUII UIIU

IIU

im

uuIIUII UMU

GCL Form 1.31-86

" • '•• •-• . i o


VOLATILE COMPOUNDS

CASNumber

67-64-1107-02-8107-13-171-43-275-27-475-25-274-83-978-93-375-15-056-23-5108-90-775-00-3

1 10-75-867-66-374-87-3124-48-194-50-1541-73-1106-46-775-34-3107-06-274-35-4156-60-578-87-5

COMPOUNDNAME

AcetoneAcroleinAcrylonltrileBenzeneBromodichloromethaneBromoformBromomethane2 • ButanoneCarbon disulfldeCarbon tetrachlorideChlorobenzeneChloroethane2 -Chloroethyl vinyl etherChloroformChloromethaneDlbromochloromethane1, 2 • Dichlorobenzene1,3- Dichlorobenzene1,4- Dichlorobenzene1, 1 • Dichloroethane1,2- Dichloroethane1, 1 • Dichloroethenetrans- 1,2- Dichloroethene1,2- Dichloropropane

ug/Kg.•*STt-

II U

M UII UIIU

IIU

IIU

IIU

IIU

MOW

IIU

IIU

II U

IIU

II U

II U

55 UIIU

IIU.

GCL Form 1.2

WV DEPARTMENT OF NATURAL RESOURCESDIVISION OF WATER RESOURCESCUTHRIE CENTER LABORATORY

il.OO Brenda Lane, Charleston, WV 25312


Branch Submitting Sample: __Program lor Which Samples are to be. ilyzed: _Inspector Taking Sample: ______PftMgiDate Sample Was TaKen: _______•« • ? ? -fstDate Sample Received: ______Sample Matrix: _________Sample Containers & Amounts: ____i y iPh ol Sample nffi-tferaon: ______S , oField Sample Ph Adjustment and Preservation: _Type of Analysis Requested: ____mi fSample Parameters Requested: _______Field Sample Identification Number: IJM

Laboratory Comments: __________

Sample Analysis Reported toDate Sample Was Reported:

; LU c. ICL /A/1] |A?.r<o -

Data Release Authorized by: PiyUi-fiaA/e1 /, r\hrf\j>.V\Laboratory Chief

RECEIVEDOCT 3I986

GCL Form 1,0, i • i i u '••> 1-88



One or more of the following specific data qualifiers were used In reporting results,

U • Indicates the parameter was analyzed for but was not detected, The detection limit (Note1.) for the parameter was reported followed by a U (eg,, IOU),

J • Indicates the presence of a parameter which met the identification criteria but was presentat a concentration less than the detection limit.

E • Indicates an estimated concentration for a tentatively identified compound where a 1:1response to an internal standard was assumed.

C- Indicates the Identification of a parameter was conflred by GC/MS. This qualifier wasapplied only to parameters which were not analyzed by a GC/MS method,

B • Indicates the parameter was present in the method blank as well as the sample, The reportedresult should be viewed with caution and should be considered to be of questionable value.

X • Indicates the parameter was identified and/or quantltated after the designated holding timespecified In the methodology, The reported result was for informational purposes only.

Note 1: The laboratory has established minimum target values for each parameter, These valuesreflect the lower limits the laboratory expects to achieve on routine samples and for which thereis a high level of confidence in the results, These are not necessarily the method or instrumentdetection limits, The actual detection limits used with the U qualifier will be dependent on theparticular sample and the concentration/dilution actions required to perform the analysis withinthe working range of the Instrument(s), The detection limits for a sample will be the minimumtarget values or some multiple of the minimum target values,



GCL Form 1,4Rev, 4-86,



GASNumber

309-00-2319-84-6319-85-757-74-972-54-872-55-950-29-3

819-86-860-57-1959-98-9

33213-65-91031-07-872-20-8

7421-93-453494-70-5

58-89-976-44-8

1024-57-372-43-5

12574-11-211104-28-211141-16-563469-21-912872-29-611097-69-111096-82-58001-35-2

COMPOUNDNAME

AldrinAlpha- BHCBeta • BHCChlordane4, 4' -ODD4, 4' • DDE4, 4' • DOTDelta- BHCDieldrinEndosulfan IEndosulfan 1 1Endosulfan SulfateEndrinEndrin AldehydeEndrin KetoneGamma-BHC (lindane)HeptachlorHeptachlor EpoxideMethoxychlorPCB -1016PCS- 1221PCB -1232PCB -1242PCB -1248PCB • 1254PCB • 1260Toxaphene

ug/Kg,-usrtr-

I.71AI.7UI.7IA31 M

1.7 LA

?1

———— LM ————.7UIt,7U

.7U

.?U

.7U

.7U

.7U

•?M

_*• 3j|

3<4iT34 U

a^M.11 MVI U

GCL Form 1.10,,.... ..'-• • ; •• 1-86



CASNumber

91-57-6

95-48-7106-44-5

1 91-20-3

88-74-499-09-2100-01-698-95-3

88-75-5100-02-762-75-9621-64-786-30-687-86-585-01-8108-95-2129-00-0120-82-195-95-488-06-2

COMPOUNDNAME

2 • Methylnaphthalene2 • Methylphenol4- MethylphenolNaphthalene2- Nitroaniline3- Nitroaniline4- NitroanilineNitrobenzene2 • Nitrophenol '4- NitrophenolN-NitrosodlmethylamineN-Nltrosodi-n-propylamineN-Nitrosodiphenylamine (1)PentachlorophenolPhenanthrenePhenolPyrene1, 2, 4 • Trlchlorobenzene2, 4, 5- Trichlorophenol2, 4, 6 • Trichlorophenol

ug/Kg,•ajft.

?M 0 u.

3MOU

310U

31Cm

I700W

170014

I700U.

3HOU

70C-U

I700W

700 U

3MOU

310 M

noon310W

3HOU

T10V<

IMGU

•?klOM

"3 IOU

(1) • Cannot be separated from dlphenylamine,

GCL Form 1,8



CASNumber

53-70-3

132-64-995-50-1541-73-1106-46-791-94-1120-83-284-66-2105-67-9131-11-384-74-2534-52-151-28-5121-14-2606-20-2117-84-0206-44-086-73-7118-74-187-68-377-47-467-72-1193-39-578-59-1

COMPOUNDNAME

Dibenzo (a, h) anthraceneDibenzofuran1, 2 • Dichlorobenzene1, 3- Dichlorobenzena1,4- Dichlorobenzene3, 3' • Dichlorobenzidine2,4 • DlchlorophenolDiethyl phthalate2, 4 • DimethylphenolDimethyl phthalateDi-n-butyl phthalate4, 6 • Dinitro • 2 • methylphenol2, 4 • Dinitrophenol2, 4 • Dinitrotoluene2, 6 • DinitrotolueneDi-n-octyl phthalateFluorantheneFluoreneHexachlorobenzeneHexachlorobutadieneHexachlorocyclopentadieneHexachloroethanelndeno(1,2, 3-cd) pyreneIsophorone

ug/Kg,-«9/L

1 100^

.IOU

31 OU

31 OM310M

310U

3iouI ? a o M

TtOM

310U

110-1

mow^ltc^llflM

SI CV

1HC.U

310U

1 7 _0 U

.IOU

GCL Form 1.7

OHGANICS ANALYSIS DATA SHEET


CASNumber

83-32-9208-96-862-53-3120-12-792-87-556-55-3

205-99-2207-08-9191-24-250-32-8

. 65-85-0100-51-6111-91-1111-44-4

39638-32-9

117-81-7101-55-385-68-7106-47-859-50-791-58-795-57-8

7005-72-3218-01-9

COMPOUNDNAME

AcenaphtheneAcenaphthyleneAnilineAnthraceneBenzidlneBenzo (a) anthraceneBenzo (b) fluorantheneBenzo (k) fluorantheneBenzo (ghi) peryleneBenzo (a) pyreneBenzole acidBenzyl alcoholBis ( • 2- chloroethoxy) methaneBls(-2-chloroethyl)etherBis ( • 2- chlorolsopropyl) etherBis ( • 2- ethylhexyl) phthalate4- Bromophenyl phenyl ether

•••MM*4-Chloroanlllne4 • Chloro -3- methylphenol2 • Chloronaphthalene2 • Chlorophenol4- Chlorophenyl phenyl etherChrysene

ug/Kg.-MJ/fc-

"31O H

-101A

I700W

31014

110U

310U

11CU

notfw70 OU

TtO U

3MO «A

310M

1MOU

•»-if5LI

TIC U

•MV1'10 U

,?1CU

>|OU

HUMT10M '

3i i? u.

GCL- Form 1,6


VOLATILE COMPOUNDS

CASNumber

10061-02-510061-02-6100-41-4591-78-675-09-2108-10-179-34-5127-18-4108-88-371-55-679-00-579-10-6100-42-5108-05-475-01-495-47-6108-38-3106-42-3

COMPOUNDNAME

cls-1,3- Dichloropropenetrans- 1, 3- DichloropropeneEthylbenz-jne2 • HexanoneMethylene chloride4 • Methyl • 2- pentanone1, 1,2, 2 • TetrachloroethaneTetrachloroetheneToluene '1, 1, 1 • Trichloroethane1,1,2- TrichloroethaneTrichloroetheneStyreneVinyl acetateVinyl chlorideo-Xylenem-Xylenep-Xylene

ug/Kg,>"uy/L

\OU

IOU

\ou

I OOU

IOU

IOUIOU

IOIA

IOU

IOU

iouIOUIOUIOU

GCL Form 1.31-86


VOLATILE COMPOUNDS

CASNumber

67-64-1107-02-8107-13-171-43-275-27-475-25-274-83-978-93-375-15-056-23-5108-90-775-00-3110-75-867-66-374-87-3124-48-194-50-1

541-73-1106-46-775-34-3

107-06-274-35-4156-60-578-87-5

COMPOUNDNAME

AcetoneAcroleinAcrylonitrlleBenzeneBromodichloromethaneBromoformBromomethane2 • ButanoneCarbon dlsulfldeCarbon tetrachlorideChlorobenzeneChloroethane2 • Chloroethyl vinyl etherChloroformChloromethaneDibromochloromethane1,2- Dichlorobenzene1,3- Dichlorobenzene1,4- Dichlorobenzene1,1- Dichloroethane1,2- Dichloroethane1, 1 • Dichloroethenetram- 1,2- Dichloroethene1,2-Dlchloropropane

ug/Kg,-U9/W

1 O W

IOU

IOU

IOU

ICU

IOU

lou

IOU

IOOU

(OUIOU,

IOUIOU

IOU

.IOU

.souI O WlOu,

GCL Form 1,2

WV DEPARTMENT OF NATURAL RESOURCESDIVISION OF WATER RESOURCESQUTHRIE CENTER LABORATORY

~ 4900 Bronda Lane, Charleston, WV 2531 21304} 348.4Q67


Branch Submitting Sample: _ ___ n/v?flgpou 'j UA.VII; _____Program for Which Samples am to be Analyzed: ___ c.sii t\.nInspector Taking Sample: ______i*,uricifl .")Date Sample Was Taken: _______.-77 • fr(,Date Sample Received: _______R-.fr-Sample Matrix: __________s&i >.Sample Containers & Amounts: ___i x ft e +Ph of Sample .w-GfltteMkin: _____S,CField Sample Ph Ad|ustment and Pmservatlon: ______________Type of Analysis Requested: ____.-VL pmeeiiv Pr HUTAMTSample Parameters Requested: _____________________Field Sample Identification Number: os ^ft<iM .JTATS rnt\

} Laboratory Comments: ____-rm i^nt^f c<>H-.»:^cn n m.t.TtlLt TVC. CP

Sample Analysis Reported to: l-Uf I CL Ifi^Tt (/e.foG - T^A 2 t.i/a&t,Lt lw<Date Sample Was Reported: 0~ I -#£ ________________________

Data Release AuthorUed Iby: KjjfJl Wj 17 rjJLaboratory Chief

RECEIVEDQCT 31.68

GCL Form 1,0 ' '1.86

.. ORGANICS ANALYSIS DATA SHEET


One or more of the following specific data qualifiers were used in reponing results,

U • Indicates the parameter was analyzed for but was not detected, The detection limit (Note1.) for the parameter was reported followed by a U (eg,, 10U),


E • Indicates an estimated concentration for a tentatively identified compound where a 1:1response to an internal standard was assumed,

C- Indicates the identification of a parameter was confired by GC/MS, This qualifier wasapplied only to parameters which were not analyzed by a GC/MS method,

B • Indicates the parameter was present In the method blank as well as the sample, The reportedresult should be viewed with caution and should be considered to be of questionable value.

X • Indicates the parameter was identified and/or quantltated after the designated holding timespecified in the methodology, The reported result was for informational purposes only,

Note 1: The laboratory has established minimum target values for each parameter, These valuesreflect the lower limits the laboratory expects to achieve on routine san,~ies and for which thereis a high level of confidence in the results, These are not necessarily Me method or instrumentdetection limits, The actual detection limits used with the U qualifier will be dependent on theparticular sample and the concentration/dilution actions required to perfurm the analysis withinthe working range of the instrument(s), The detection limits for a sample will be the minimumtarget values or some multiple of the minimum target values,


Note 3; All soil sample results are reported on a dry weight basis.

GCL Form 1.4Rev, 4-86,



CASNumber

309-00-2

319-84-6319-85-757-74-972-54-872-55-950-29-3

819-86-8

60-57-1959-98-9

33213-65-91031-07-8

72-20-87421-93-453494-70-5

58-89-976-44-8

1024-57-372-43-5

12574-11-211104-28-211141-16-563469-21-912672-29-611097-69-111096-82-58001-35-2

COMPOUNDNAME

AldrinAlpha- BHCBeta- BHCChlordane4, 4' -ODD4, 4' -DDE4, 4' -DOTDelta • BHCDleldrinEndosulfan 1Endosulfan II •EndowlfanSulfateEndrinEndrin AldehydeEndrin KetoneGamma-BHC (lindane)HeptachlorHeptachlor EpoxideMethoxychlorPCB -1016

PCB- 1221PCB-1232PCD- 1242PCB -1248PCB -1254PCB -1260Toxaphene

ug/Kg,~u«rt-

l.«U

UMl.tfU3S<4UuU&

li-f'Mtl.ttU•ftt-M'-WI.^U

I.KU

I.^M

I. U

I.VU

i.tr'UI.YU

l.fru3.5U

3£U

———— ———3|UJS11A

3SU

3JSU

TSU

?S U.GCL Form 1,10



CASNumber

91-57-695-48-7106-44-5

' 91-20-388-74-499-09-2100-01-698-95-388-75-5100-02-762-75-9621-64-786-30-687-86-585-01-8

108-95-2129-00-0120-82-195-95-488-06-2

COMPOUNDNAME

2 • Methylnaphthalene2 • Methylphenol4 • MethylphenolNaphthalene2- Nitroaniline3- Nitroaniline4 • NitroanilineNitrobenzene2- Nitrophenol4 • NitrophenolN-NitrosodimethylamineN-Nitrosodi-n-propylamineN-Nitrosodiphenylamine (1)PentachlorophenolPhenanthrenePhenolPyrene1, 2, 4 • Trichlorobenzene2, 4, 5 - Trichlorophenol2, 4, 6 • Trichlorophenol

ug/Kg,..-n -

"MJr^

•jsou1SOU

3SOU

3 SOUItfOOM

I«OOU

itfoou350 U700M

lo-OOM

700 H

3SOU

.T.50U

l^flfl M

3.50 U

"3SO U

3..CM3SOU

\SO -I

•^c,OU

(1) • Cannot be separated from dlphenylamine,

GCL Form 1,81-86



CASNumber

53-70-3132-64-995-50-1541-73-1106-46-791-94-1120-83-284-66-2105-67-9131-11-384-74-2534-52-151-28-5121-14-2606-20-2117-84-0206-44-086-73-7118-74-187-68-377-47-467-72-1193-39-578-69-1

COMPOUNDNAME

Dibenzo (a, h) anthraceneDibenzofuran1,2- Dichlorobenzene1, 3 • Dlchlorobenzena1, 4 • Dichlorobenzene3, 3' • Dichlorobenzidine2,4 • DichlorophenolDiethvl phthalate2, 4 • DlmethylphenolDimethyl phthalateDi-n-butyl phthalate4, 6 • Dinitro • 2 • methylphenol2, 4 • Dlnitrophenol2, 4 • Dinitrotoluene2, 6 • DinitrotolueneDi-n-octyl phthalateFluorantheneFluoreneHexachlorobenzeneHexachlorobutadleneHexachlorocyclopemadieneHexachloroethaneIndeno (1, 2, 3-cd) pyreneIsophorone

ug/Kg,otg/t-

| VOOUISO U

3504^50U

350M

3SOM

3 50 U

is1 sou

3SOU

TSOU

"5SOU

3SC,v\-

3S<?U

T50U

•J50U1 3 SOU

VSOU

1VCCLI

VSCt\

GCL Form 1.7



CASNumber

83-32-9208-96-862-53-3120-12-792-87-556-55-3205-99-2207-08-9191-24-250-32-865-85-0100-51-6111-91-1111-44-4

39638-32-9

117-81-7101-55-385-60-7.106-47-859-50-791-58-795-57-8

7005-72-3218-01-9

COMPOUNDNAME

AcenaphtheneAcenaphthyleneAnilineAnthraceneBenzidlneBenzo (a) anthraceneBenzo (b) fluorantheneBenzo (k) fluorantheneBenzo (ghl) perylene 'Benzo (a| pyreneBenzole acidBenzyl alcoholBis ( • 2- chloroethoxy) methaneBis(-2-chloroefhyl)etherBis ( • 2- chlorolsopropyl) etherBis(-2-ethylhexyl) phthalate' 4 • Bromophenyl phenyl ether(WWHW Wff W Wi m

4-Chloroanillne4 • Chloro -3- methylphenol2 • Chloronaphthalene2 • Chlorophenol4- Chlorophenyl phenyl etherChrysene

ug/Kg,-*sft?

.TJQu

.1SOMi <<C 0 U

150H

-Sou330U

3 SOU,

1 -iiOO U

700U

3. SOU

3SO U

?50.\

TSOv.1

350LI

3 SOU

'-.•rS'S'tfu'•350 u.3S6H3 SOW

3SOUT?OW

ISO -V

GCL-Form 1,61-86


VOLATILE COMPOUNDS

CASNumber

10061-02-510061-02-6

100-41-4591-78-6

75-09-2108-10-179-34-5127-18-4108-88-371-55-679-00-579-10-6100-42-5108-05-475-01-495-47-6108-38-3106-42-3

COMPOUNDNAME

cis-1, 3- Dichloropropenetrans -1,3- DichloropropeneEthylbenzene2 • HexanoneMethylene chloride4 • Methyl • 2- pentanone1, 1,2, 2 • TetrachloroethaneTetrachloroetheneToluene1, 1, 1 • Trichloroethane1, 1, 2 • TrichloroethaneTrichloroetheneStyreneVinyl acetateVinyl chlorideo-Xylenem-Xylenep-Xylene

ug/Kg,rW*t-

|l U

1 1 U

u u

MOU

\ 1 U

I I U

IIM

lluIIU

I I U

II U

II U

uuI I U

GCL Form 1.3


VOLATILE COMPOUNDS

CASNumber

67-64-1107-02-8107-13-171-43-275-27-475-25-274-83-978-93-375-15-056-23-5108-90-775-00-3110-75-867-66-374-87-3124-48-194-50-1

541-73-1106-46-775-34-3107-06-274-35-4156-60-578-87-5

COMPOUNDNAME

AcetoneAcroleinAcrylonitrileBenzeneBromodlchloromethaneBromoformBromomethane2 • ButanoneCarbon disulfideCarbon tetrachlorideChlorobenzeneChloroethane2 • Chloroethyl vinyl etherChloroformChloromcthaneDlbromochloromethane1,2- Dichlorobenzene1, 3 • Dichlorobenzene1,4- Dichlorobenzene1, 1 • Dichloroethane1, 2 • Dichloroethane1, 1 • Dichloroethenetrans- 1,2- Dichloroethene1,2-Dlchloropropane

ug/Kg,• UQ/l-

11 L\

II U

IIU

IIU

IIU

M U

II U

IIUIIOU

ll U

II UII UII UI I Ml l Uss ul l UII U

GCL Form 1,21-86

POLREP #1 - Lakin State FarmsLakin, Mason Co., WV

"*t CERCLA Site Assessment

ATTENTION: Tom Massey and Tim Fields

I. Situation (6/1/87)A. Site referred to EPA through WVDNR on 8/26/86 in

response to public concern that pesticides/hazardous wastesallegedly buried on the site could be possible cause for patchyinjury to corn plants in adjacent field.

B. TAT review of data concluded that previous diagnosisby WV Dept. of Agriculture had proven that corn plant injury wasdue to magnesium deficiency and low soil ph. However, TAT notedthat there was mention of several drums of electrical equipmenton site. Therefore, TAT recommended that an assessment beperformed to evaluate the possibility that PCB containingcapacitors or transformers were involved.

IX. Actions TakenA. TAT reviews site file and recommends site assessment

be performed.B. osc tasks TAT with site assessment and coordination

: with WVDNR.c. TAT performs site assessment including Level "C"

entry, drum sampling, soil sampling, photo and log bookdocumentation, and mapping of site.

D. TAT collected 4 drum samples, 8 soil samples, andcontacted EPA-CRL (Colleen Walling) to arrange for 14 day turnaround.III. Future Plans

A. osc/TAT awaits analytical data to schedule removal ofPCB capacitors.

B. TAT to ship samples on 6/8/87 for CLP analysis.

Benton Wilmoth, OSCUS EPA - Region IIIWheeling, West Virginia

POLREP #2 - Lakin State Farm PCB siteNear Lakin/Pt. Pleasant, Mason Co., WV

ATTENTION: Tom Massey and Tim Fields

I. Situation (1400 hours - 8/7/87)A. OSC/TAT received analysis data indicating PCB

concentrations in excess of 1,200 ppm in capacitor oil. The datafollows 6/1/87 TAT assessment per OSC request.

B. Following data QA/QC by TAT, OSC activates emergencyremoval action using S50K authority to mitigate the immediatethreat to human health and the environment.

C. Estimated Costs to Date (COB 8/7/87):costs to Date Ceiling

EPA $ .5K $1.5KEPA HQ (15%) 1.1K 7.5KTAT 1.8K 6.OKERCS 5.OK 35.OK

Totals $ 8.4K $50.OK

D. Weather: Sunny and hot, 90 degrees with high relativehumidity.

E. Personnel on scene: EPA - 1TAT - 2ERCS - 4

II. Actions Taken

A. OSC Issues delivery order #7445-03-002 to ERCS for $35Kfor removal actions on 8/5/87 at 1300 hours.

B. ERCS subcontractor, AMO Pollution Services ofCanonsburg, PA, mobilized to site 8/6/87 to begin removalactivities.

c. osc contacted WVDNR, Hazardous Waste Division, to informthem of mobilization and removal actions.

D. OSC on scene 8/6/87 to coordinate removal activities.

E. TAT on scene 8/6/87 to perform contractor monitoring,site safety support, and administrative support to osc.

F. ERCS completes removal activites as of 1330 hours on8/7/87 Including 9 PCB capacitors, 4 drums which capacitors weredumped, 7 drums of soil and grease from stained area and one drumof contaminated site material. ERCS was removed two smalltransformers from nearby barn on site suspect of PCBcontamination.

G. ERCS performed post cleanup soil sampling per the OSCrequest from previously contaminated area.

H. OSC signed PA Waste Transport Manifest #PAB3320343, at1100 hours on 8/7/87 for transportation of material to ERCS TSDfacility in canonsburg, PA.

I. EPA, TAT and ERCS demoblized from site 1400 hours 8/7/87upon completion of cleanup activities.

III. Future Plans

A. osc awaits results of post cleanup sampling to determinethe effectiveness of removal and if further rmeoval actions arewarranted.

B. ERCS to sample removal material for final disposalcharacterization.

c. osc awaits results from ERCS disposal analysis for finaldisposal of materials.

D. TAT to begin draft of osc Report pending ERCS samplinganalysis.

E. osc to provide additional information to EPA CERCLAEnforcement. '

yWWUAIMBentbn M'. Wilmoth, oscU.S. EPA Region IIIWheeling, WV

.flKIN STflTE FRHM, PCB SITELfiKIN/ PT. PLEflSflNTr MflSQN CO. , WV

; TOM MflSSEY flND TIM r7 1 ELDS

aP-ClhiL BULLETIN- PROJECT BrflTUS.

I. aiTUflTION (ISOO HOURS, SEPT I, 1987)

ft. _ PCB CflPfClTQRS, 4 DRUMS WHIC.H CRPHCJTORS WtiRE DUhPEO, 7DRUMS DP SOIL rtND SREflbE PRUM STfilNED HRER_ RNO 1 DRUM OFClJNTOl'UNrtTED SITE MflTERIflL WtiRfcl RtiMUV&D TO ftl'IO POLLUTION TSiD_rfl_ILITY (CHNQNBBcRG, PM UN 6/7/37.

B. POSTCLEflNUP SflflPLINS WflS PERFORMED TO DETERMINE WHETHERFURTHER flCTIQN IS NECESSfiRY.

C. USC fiWfUTS DISPOSflL flPPrtQVfiL FOR ftEMOVED WrtSTE MrtTKRlflLS,DISPOSHL RNflLYSIS RESULTS.

D. PSC flrifilTS RESULTS OF POSTCLEflNUP SAMPLING RESULTS.

£. OSC CftHNOT DETERMINE ft FINHL SI'IE CLOriUKE UflTE flT THIS 'TIMEDUE TO Thti flFOKEMENTIONED FflCTORS.

--.'1. FUTURE PLflNB

A. 0-HJ REPORT DRflFT TO BE STflRTED, COMPLETION OF WHICH ISDEPENDENT UN QFF1CIRL SITE CLOSURE HS DETERMINED BY THE QSC.

iX/k*l,wCvU (.v. vv\.&CV\BENTON WILMQTH, OSCEPfi REOION HI,.

MS, WV

,-.. Lakin State Farm PCB siteNear Lakin/Pt. Pleasant, Mason Co., WV

ATTENTION: TOM MASSEY AND TIM FIELDS

SPECIAL BULLETIN - PROJECT STATUS

I. Situation (1200 hours, 10/01/87)A. 9 PCB capacitors, 4 drums which capacitors were dumped,

7 drums of soil and grease frum stained area and 1 drum ofcontaminated site material were removed to AMO Pollution TSDfacility (Canonsburg, PA) on 8/7/87.

B. Post-cleanup sampling was performed to determine whetherfurther action is necessary.

c. osc awaits results of post-cleanup sampling results.

D. osc cannot determine a final site closure date at thistime due to the aforementioned factors.

II. Future Plans

A. osc report draft to be started,'completion of which isdependent on official site closure as determined by the OSC.

Be'nton Wilmo'th, oscus EPA - Region IIIWheeling, WV

Lakin State Farm PCB SiteNear Lakln/Pt. Pleasant, Mason Co., WVATTN: Mike Zlckler and Tim Fields

cc: Steve Jarvela

SPECIAL BULLETIN - PROJECT STATUS

I. Situation (1200 hrs., 11/01/87)A. 9 PCB capacitors, 4 drums which capacitors were dumped,

7 drums of soil and grease from stained area and 1 drum ofcontaminated site material were removed to AMO Pollution TSDfacility (canonsburg, PA) on 8/7/87.

B. Post-cleanup sampling was performed to determine whetherfurther action Is necessary.

C. osc awaits results of post-cleanup sampling results.D. osc cannot determine a final site closure date at this

time due to the aforementioned factors.

II. Future PlansA. osc report draft to be started, completion of which is

dependent on official site closure as determined by the OSC.

Benton Wilmoth, OSCUS EPA - Region IIIWheeling, WV

POLREP #3 AND FINAL - LAKIN STATE FARM SITECAMP CONLEY, MASON COUNTY, WV

ATTENTION: BOB CARON, STEVE JARVELA AND TIM FIELDS

I. SITUATION (1/29/88 1700 HRS)

A. OSC RECEIVED CONFIRMATION THIS DATE THAT SEVENTEEN (17) DRUMSOF PCB CONTAMINATED CAPACITORS, SOIL AND DRUMS WERE SHIPPED FROMAMO POLLUTION SERVICES, INC. TEMPORARY STORAGE DISPOSAL FACILITYTO THE APTUS DISPOSAL FACILITY IN COFFEEVILLE, KANSAS ON DECEMBER14, 1987 FOR FINAL DISPOSAL. DRUMS WERE SHIPPED UNDER MANIFESTDPAB4643Q41.

B. ESTIMATED COSTS TO DATE:AGENCY COSTSEPA 600.00ERCS 18,255.00TAT 6,830.00TOTAL 25,685.00

C. THE OSC ANTICIPATES NO ADDITIONAL EPA INVOLVEMENT WITH THISSITE AND IS REQUESTING THAT AH, REMAINING FUNDS BE DEOBLIGATEDFROM THIS PROJECT. LAKIN STATE FARM SITE DELIVERY ORDER NUMBER7445-03-002; CONTRACT #68-01-7445; DCN# E72A95; APPROPRIATION#6820X83.45; ACCOUNT I7QFA3.VWE2A.

II. ACTIONS TAKEN

A. SEVENTEEN DRUMS OF PCB CONTAMINATED WASTE DELIVERED TO APTUS,COFFEEVILLE, KANSAS FOR FINAL DISPOSAL ON DECEMBER 14, 1987.

III. FUTURE PLANS

'A.'.. OSC REPORT TO BE COMPLETED UPON RECEIPT OF FINAL MANIFEST ANDFINAL PROJECT COST INVOICE.

B-NTON M. HILMOTH, SENIOR OSCU.S. EPA, REGION IIIWHEELING, WEST VIRGINIA

DELIVERY ORDER FOR EMERGENCY RESPONSE CLEANUP SERVICES

ll/ui tlolimr order it issued stilijact to nil turns ami conditions ol Ilia contract itlanlilied in Slack 2.11. DATE OF ORDER 2. CONTRACT NIJMOEH 3. ORDER NUMBER

4. TIME OF INITIAL ORDER III Initial orderwas*{Specify time tonal

i. DELIVERY ORDER CEILING AMOUNT lOMjalcil Ainaiinl/$, DQD,

0. ACCOUNTING AND APPROPRIATION DATABAM Apiiioiiniiliun Number Poeumiml Cunliol No, Account Niiinliur Olij-CI ClansDPM

7». ISSUED TO: CONTRACTOR INmt, Mlrtss, ami IIP Coital On ISSUED DY: ORDERING OFFICE /Name, Adittess. andllPCodal

7.. PROURAM MANAGER IName »nd Phone Number! 8b. EPA REGION/USCG DISTRICT Be. ZONE

7c. RESPONSE MANAGER INtma ami Phone Number)

Dolt £8d. ON-SCENE COORDINATOR INami and Pinna Number/

9, RESPONSE LOCATION (Site Name and/or Address mil ZIP Cotlel, Sfufr.. rrt« ft8

10. CONTRACTOR REQUIRED ON SITE IDele end TimalDAM

11. REQUIRED WORK COMPLETION DATE

12. STATEMENT OF WORKThe Conir.cior shall furnish the necessary personnel, mmorlnls, sotvicos, tncHiiios, and olherwlsa ilo all thingsnncossary lor or Incidonl lo the padormiincii ol Ilia work sni lonh bolow:

j ?***»*

13, ORDERING OFFICERNAME/TITL SIGNATURE DATE

.PAFm1MO.ni1l.a3) ORDERINGOPFICER/OSC . ,5,OTo ,,,-.«,«W1,4

let utt & Httunrntnl aHiti c/irV/________________________________Pagef, /Sna* * US .nvMoflfTMnlll Prelection Aairt«y,r [3V

oEPAWiihington, DC 20400ProcurementRequest/Order

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i, Uftieot nvqun

QR-04-374 Tilfphom NumoirZ«IM7-98JI

S. Dm Hum RtqwK)ASAP

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jllvtf To IProjtct Mfntyffl 3.A4KM4141 CbMUwt St., thilt., PA 1910

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ll.TiliphoniNumtnr

12.FlninclilDili

b. Sirvlclng Finance Olllci Numbir NOTE: Item 12|d) Oocumenl Type — Controcl ° "C,Purchase Order•"P"

.FMOUu .....,,,,..,.... DocuimntControl Number Account NumlHr

[HI W MailOtJIOtlClisi

Amount In)Cent

33.000

13. SugotilBd Somce //v«m». A <t»iu, HP CtxU, Hmi/Camtal H. Amount gl monoycommand n:

D OriginalD IncreaseQ Decrease

15. For Smill PuichiMi Only: Contracting Ollico II luiho.Hut loexcood me tmouni ihonn in .lock 12|h| By 10% or1100, whlchivor n lo».

Qr« PNO16, Approvals

a. Branch/Olllco Dale d, Properly Management Ollloer/Deslgnee

vialon/OHIceSttpbn

DateX"'

c, Funds lined In Block 12 end Block 16 W inyl .re..<"available and reserved, /Signature el Cenit)/ing.0ttic/i

'Date t. Other tSptcilfl Date

17. Dale ol Order 18. Order Number 19, Contract Number lit inyl 20. Discount Terms

21. FOB Point 22, Delivery to FOB Point by On or litlort IDalel 23, Person Taking Order/Quote and Phone No,

<4, Contractor INimt, xtdrtss, ZIP Cods/ 2S, Type ol OrderD a, Purchase

Reference your quote ISaa block 231

Ple«elurnl>niheaboveoniheterm9ipec!l!odgn!>g|hsldosolihltordtrsndonthe attached sheets, II any, Including deliver/ as Indicated.

P b, Delivery provisions on the reverse are deleted. The delivery order Issubject to the terms and conditions ol the contract. ISaa Black IS/

c, Donl QvVrllien Q (Miming28. Schedule

himNumber

IdSupplln of S«nricti Quinlitv

Or«rmEitlmlltdUnit PIIM

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Amount111

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sra ii! __'LOUTIOli Ctmtji Ukla .

Cityi KHM2UUI V?

DOJVUI OUni 7445-01-002

Total I27, United Slim ol Ammlc* 28, Typed Name and Title ol Contracting Officer

"vl!on-1900.B|Rev.».aa)Ptevious6.liloniireobsolete, ' COPYB-pnOPERTYMANAGEMENTOFFKC\

PENNSYLVANIA DEPARTMENT OF ENVIRONMENTAL RESOURCESBUIIIU ol Wlilt Minigimenl

p,0, loHjOM P-mippren*,_„_.- H-rrHburj, PA 171.0 OM' "» »•»«•»

_*.8M.5l:REV.tV17 Pl«e« pdnlor type, |Form designed Ic-f'uM on elite (la-PlKh) lyi>emllif,| ________liftiti l-AI UNIFORM HAZARDOUS

WASTE MANIFEST1. UtnflfllOf I UD KPrt IU no.p.A.p.o.3.a.9.6.v.2.3. *"' le noi mt*n4 ey F«H»( ten

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Dlacr.KMnovla M'd DUT rfrn* with Buadn tkdth. l/32A9BaIfti QENERATOR'8 CERTIFICATION: I hi'ifiy dtcim ih.i mq coniinn ul tmi cootionmint m fully *n<4 *CCLH-I»IV iivicnbtii .ttovi by P'OfJ*' iriipptng nimi ,mj KIcuiiilim. p«M_, miriiil, im) IIIHIH/, *M in m ill nipicii m piopir condition loi innipori or mgnrriy icpwfltna to ipplicibii miirnitionii inu nonnnil guvunmitH nuuUiiani,

ll i _m i iiim quimiiv giniiiiut. I iiiiiiy m<i I imi * piogiHrn 111 Hliit* if '»'iut« in* vuiunn «nu lumciir «*"« «»n»Mi«J w INI o_i)i_« i D^« Uiiirmmm 10 Dt i«onu(nii,'iiiipticiici.it in_ inn i fiivt iiiiciid im pdcii.iliii m*ihuu gl iininmit, noiig*, 01 ilnpoiii cuirinilf iviiliWi in ini winch mimmuii ih« pni.ni -nil luiuit mini 10 hwmin hi»linind m« iiwuunmini, QR, il I im a imiil \\,tnMi gin-iimi, I hiv» m.u. 4 uouti linn illuii to mmnnui my tvnif gin.iiiiiun inJ i*nci itii IHIII w«iii m«n.«iiniini miihJg mil niv»liDii 10 nil ind inn i cm itloio,

17, TcwiPintti 1 Artna»i«i<i»mnl 03

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D. 1 DH ixafilnlin TTuutoxMT flll«I/v <500 • 310 UM..524 UM.

C,4.mot C-p-ottan - 130 llw.>Q. Melry Omiei« Daemon CnOimtxi «l na \») l nrtom nutiiteli MVXKI by iMe mn-lin uiotpi * ncnJ In torn 11,

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Copy 5 - TSD Facility; Mall to Generator

PENNSYLVANIA DEPARTMENT OF ENVIRONMENTAL RESOURCESBureau ot Waste Management

P, 0, Box 2063Hauiiburg, PA 17120

PtMM print or type, (Form dettgned loi im on illi I12.pltchl typemttH.I__ Fern Approvid. OriH He. 8000.041)4. E»plrei 7.31.68 _

JNIFORM HAZARDOUSWASTE MANIFEST

I.Qenerelof'sUSEPAID^No.'tv 2, Ptge 1ol •

kiltmuWofi In IM ih«Hd wenli cwl lequlied by Federal Hw

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A,'_«te Mertten

~ra—— ——— ,u»..i ._* .I-*-.. TOV.i.:; .. - .i, TnnljKrttl 1 Compwiy NllTN 0, US EPA ID Number

AM Mutton J*vx._»._r.-c. \i C,1. mi Trim.'10;."PA-AH""""

7. Trmiponir i Compiny Nimi ' 9, US EPA I. Niimbf rL

9, Diilgniud Facility Nimi mlif III Addmi 10, U9 EPA ID Numtw..'State Tim.lDlA WilSWI.Vlwi-'. frf'" PA-AM ' l-.-vti^'iiitiitl '""vrF. tj-npon'ii'i FtxM i •'" r"'g. aiite FedtiY'e IP">"!'* Ndi' Raqulrad'1

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Hei.Code PtiyikllSlal ^ _m1tjf , H", Code Phyifcal SineK, Hendttg Cod« l« Wattle Uited Above

16. GENERATOR'S CERTIFICA\ON: ln.r.Sji>.tlii«lliiMliitiinl.niioMliiltonlij»m.»lnlultilnrtKlur«lilr«wlti»lltw.fr|xof)llltlip(i»iJnimiinitmcl.iiil,w,(Mtkul. muhrl ind liln'id, ind in In ill mpKti In Pfopir comliiion lot irinipou by htghwiy iccotdlng to ippllciui mliinilicnil ind nitionil goviinm.nl figulmoni.Unlut I im i. imill quintity gtn«ll« vdrahfi txtn »impltd by ilnuti or iigulilion liom int duty lo miki I null mlnlmluilon piiMlcillon undtl S«1ion 3001 [til ol RCRA, I iliotirtily inn I nivi • piogdm In plKi lo iidu<l'*9Iumi ind lORlciiy ol null ginitiltd lo mi dtgiH I hivi dtlnmintdJo In icwomicilly pnclicibli ind I hni Mliclid Ihi melhod ofUMiminl. ilotigi. ot dtip«Ml «ufnnlly niiliWi lob* wnicnminimim Ihi pnt.nl ind lutwl- inrin toJiwmin hnnirfTld Ihi invironm.nl.

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20, Ftctty Owrm M Opmtor, pxttncrton ol recoil ol huMdow tnetiiWi covimt py tt* nwvtwl IIHQI H notid In hwn It,

IPA Form 6700,22 I3-B4I••••• • -••••_';_CpPY3--T5DFAaiini MAILJP GENERATOR

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