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EOBT: from past to future
Ludwig Josef Balk
Faculty of Electrical, Information and Media Engineering University of Wuppertal,
42119 Wuppertal, Germany
It is now fifty years ago that both electron beams and laser sources became commercially available to enable inspection techniques for all kinds of applications, but in special for the characterization and the testing of electronics devices. This happened more or less simultaneously with the beginning of integration of electronic components. While at the early times a simple imaging was done only, in the mid 60ies first work was carried out using all kinds of interaction products due to the impact of optical and electron beams to determine device features and their malfunctioning. Those interaction products could well be particles or photons as well as properties like electrical current and voltage. Although these kinds of testing techniques became more and more important, it took more than twenty year that a special conference on this topic was born: the 1st European Conference on Electron and Optical Beam Testing of Electronic devices (EOBT), which was organized in the year 1987 in Grenoble by Bernard Courtois and Eckhard Wolfgang. From then on this conference continued till 1995 as an independent meeting that had attracted several hundreds of scientists and engineers. However, as quite often in research, if a new field becomes mature, the size of a conference reduces, which gave rise to the decision of merging the EOBT with ESREF due to their strong overlap in the field of failure analysis. There EOBT remained an important topic, sometimes as a special session or in other years merged with failure analysis in general.
Over the years it had turned out that simple systems cannot always fulfill the tasks needed, due to the reduced sizes of structures and the demand on extreme spatial resolution as well as due to the more and more complicated vertical structure of devices, making it necessary to either prepare devices destructively or to go for sources with high vertical penetration such as for instance ion beams. And last not least so-‐called hybrid systems came into being enabling the simultaneous measurement of various device properties.
The presentation will give a review of some of the important advantages presented in all of the EOBT conferences, without being complete, and it will try to give a view into what may be the needs for future developments.
General remarks concerning failure analysis and device diagnostics
If one wants to carry out a local analysis of properties of any kind of a sample, one has to carry out an experiment dedicated to the property in question and one has to couple this necessarily with a clear local definition. Whereas direct imaging techniques allow in-‐
in-‐situ and fast studies of materials, such as optical or electron microscopes, they do not easily allow a detailed analysis of the data achieved. This is the main advantage of all kinds of scanning systems, in which a focused source is utilized to excite the specimen under test locally and where all sorts of interaction
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products may be used to create the information desired
Fig.1: Overview of interaction mechanisms
The local correlation can be achieved by scanning the location of the impact point of the excitation source, the spatial resolution by modifying source parameters, in special source diameter and penetration depth.
Fig.2: [1] shows all possible interactions in case of a light source for the case of a semiconductor sample.
If one uses a time dependent, in special pulsed, beam the temporal behavior of the arising products and by this temporal device properties can be analysed, too.
Out of all kinds of possible scanning sources electron and optical beams gained the highest importance, mainly due to the easiness for scanning and due to a very mature instrumentation.
Scanning electron microscope (SEM) and laser scanning microscope (LSM)
The scanning electron microscope (SEM) was invented by KNOLL 1935 [2] following the invention of the electron microscope by RUSKA 1933 and the scanning transmission electron microscope by VON ARDENNE 1938 [3].
Fig.3: Knoll’s electron beam scanner
Although further development was carried out till the beginning of second world war, it took a long time till an SEM became a commercial product. Essentially it was OATLEY [4], who finally was able to persuade Cambridge Instrument Company to go into production with their “Stereoscan”, the prototype of it was delivered to Dupont Chemical Corporation in the U.S.A. in 1964, two years later followed up by the Japanese company JEOL.
Fig 4: Cambridge Stereoscan (jpl.nasa.gov)
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Most important for the further use in electronics was the improvement in spatial resolution due to the invention of the cold field emission gun by CREWE in the mid 60ies, which was followed up by the first commercial FE-‐SEM, later denominated “critical dimension (CD)”-‐SEM, by Hitachi in 1972.
Fig.5: Hitachi, 1972, FE-‐SEM HFS-‐2
In case of laser scanning microscopy (LSM) at first the laser had to be invented. This happened to be in 1960 by MAIMAN for red light following up the original invention (for microwaves) by TOWNES, who died this year in the age of 99.
Fig.6: Nobel Prize winner Charles Townes
Again it took a while for the LSM to come into being due to the invention by BARTELL and RITZ, of the Department of Chemistry at the University of Michigan, in the year 1975. And finally in 1982 the first commercial LSM was produced by Carl Zeiss. In the following 3dimensional imaging became possible by the
introduction of confocal operation allowing lateral and vertical resolution down to 20nm (Fraunhofer-‐Institut für Solare Energiesysteme ISE), again a huge gap between 1957, the year when it was originally patented by MINSKY.
Fig.7: Confocal LSM (taken form malone.bioquant.uni-heidelberg.de)
Integration of electronic circuits
Although the first patent for an integrated device by JACOBI (Wikipedia) originates from 1949, it lasted till several authors came along with the first realization at the end of the 50ies, one of them, KILBY, was awarded the 2000 Nobel Prize.
Fig.8: First Integrated Circuit Invented by Jack Kilby, 1958, Texas Instruments
Pretty soon the scale of integration went on in a fantastic manner, as one can see in comparison of Fig.10.
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Fig 9: Kilby, Dallas News 12 September 2014
This tremendous increase in device density on a chip was later on described by MOORE, well known as Moore’s Law.
Fig.10: Moore’s Law (2015 Pete Carey, San Jose Mercury News
Obviously this dependence is associated with a decrease of node size, too.
Fig:11: Node size (Helen Wills Neuroscience Institute1, Berkeley, 2013
Aside from this an even higher complexity arose with the invention of devices with more than just electrical and electronical functionality, the so-‐called micro-‐electro-‐mechanical systems (MEMS), and later on with the increase of device density by three-‐dimensional packaging. Both gave rise to the need to characterize local thermal and mechanical properties, too.
Fig.12: Artist’s view of 3D-‐integration
Interaction mechanisms important for determination of electronical properties
As already mentioned, electron or optical beam impact causes multiple interaction products that can be used for device characterization. Although some of them are identical for the two different beam sources, a larger variety is given for a primary electron beam. Out of these the probably most important ones are secondary electrons, induced current, and luminescence.
Secondary electrons firstly allow precise metrological evaluation and secondly via the so-‐called voltage contrast (VC) a local potential distribution of the device. Electron beam induced current (EBIC) is a powerful mode for determining locations of electrically active areas, such as pn-‐junctions. Cathodoluminescence (CL) can be used to analyze optoelectronic properties in devices made from or with direct band gap material.
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The years before the EOBT conference came into being
Confining the review of these years to research using electron beams (though the situation for laser based experiments was quite similar), one has to mention that from 1965 onwards many researchers were involved in understanding the new SEM based modes and in optimizing the information gained from them. And it is important to mention that in these days research, both in university and in industry, was very thorough and detailed.
VC was first detected by SMITH [5] in 1955, however, more detailed information was reported by Everhart [6] in 1959, WELLS in 1968 [7], and LUKIANOFF in 1972 [8]. The further implementation of so-‐called beam blankers or choppers allowed to link the investigation of local device properties with temporal analysis to enable local determination of switching behavior of a device under test. Here important work was carried out by PLOWS and NIXON in 1969 [9] and GOPINATH in 1974 [10].
EBIC was deeply studied by DONOLATO [11], LEAMY [12], VAN OPDORP [13], and last not least by David B HOLT [14], who died last year at the age of 86, who published many papers on this topic. His last publication, a book co-‐authored with BG Yacobi entitled “Extended Defects in Semiconductors electronic properties, device effects and structures” was published in 2014.
CL was originally discussed by WITTRY in 1965 [15], followed up by PANKOVE in 1968 [16] and BALK in 1973 [17]. Here a lot of work was involved in introducing spectral analysis of the emitted light as well as its temporal behavior for characterization of minority carrier properties.
Later in the early 80ies MOUROU utilized the electro-‐optic effects (Pockels and Kerr effects) for temporal sampling of high frequency devices with picosecond resolution [18].
The beginning of EOBT
As there were great activities in the field of local analysis of electronic devices, many conferences had incorporated this topic into their program. Quite often these were physics conferences like IITRI Scanning Electron Microscopy, IXCOM, or the Oxford Conference of Semiconducting Materials. The IEEE International Electron Device Meeting (IEDM) included sessions accordingly. Most important were two conferences with respect to beam testing:
the IEEE International Reliability Physics Symposium (IRPS), already existing since 1952, and the International Symposium for Testing and Failure Analysis (ISTFA) since 1974.
However, there was no suitable conference existing in Europe dedicated to this topic in spite of its great importance in these days. In this respect it was a more than needed event that in the year 1986 two researchers in this field decided to organize an according meeting. These were Eckhard WOLFGANG from Siemens AG in Munich and Bernard COURTOIS from TIMA-‐CMP in Grenoble, who finally created in a very successful manner the “1st European Conference on Electron and Optical Beam Testing” (EOBT) which took place 9–11 December 1987 in Grenoble.
The EOBT was planned as a biannual meeting and attracted a few hundreds of participants. It took place as an independent conference following the Grenoble event in 1989 in Duisburg, Germany, in 1991 in Como, Italy, in 1993 in Zurich, Switzerland, and finally in 1995 in Wuppertal, Germany.
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Fig.13: First EOBT cover
It has to be mentioned that WOLFGANG remained member of the steering committee from the very beginning till today.
Fig.14: Eckhard Wolfgang 2006 at ESREF in Wuppertal
Although the EOBT steering committee had decided in 1995 to continue with the conference, due to the decreasing number of participants it was discussed 1996 to go for a joint venture with a related conference. The only reasonable choice in this respect was the European Symposium on Reliability of Electron Devices, Failure Physics and Failure Analysis (ESREF) which was founded in 1990 and which had a strong overlap with EOBT. Therefore it was decided in Enschede, Netherlands, during the 1996 ESREF, to merge EOBT with ESREF, and consequently it became a separate topic “session C” from 1997 onwards till nowadays, although there remained an additional overlap with the topic of failure analysis of session D.
Fig.15: 5th EOBT: Bernard Courtois, Erich Hödl (rector of Wuppertal University), Ursula Kraus (Lady Mayoress of Wuppertal), Ludwig Josef Balk, Eckhard Wolfgang (from left to right)
The years 1987 – 1995
One main topic in 1987 was the development of testing by means of VC as underlined by a still important overview by LUKIANOFF [19]. Typical topics were development of electron energy spectrometers for quantitative measurements, see the work by DINNIS [20], and the early stages of linking electron beam test systems with CAD data bases.
Fig.16: Spectrometer simulation, DINNIS
Fig.17: Electron beam test system linked with a CAD database, KOMATSU et al. [21]
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A second major topic was OBIC of integrated circuits, as reported by WILSON [22].
Fig.18: OBIC image of dislocations in a silicon bipolar transistor due to red light impact [22]
The influence of the color of the exciting laser was discussed by ZIEGLER and FEUERBAUM [1]
Table 1: taken from [1]
Fig.19: Influence of laser color on OBIC results [1]
The years after the first EOBT were strongly involved in improvement of existing techniques as well as in the introduction of new methods rather than in applications or case studies. In this manner RAO reported on design and implementation of a high performance e-‐beam tester, fig.17 being a photograph of the system [23].
Fig.20: E-‐beam-‐tester from Intel
At these days still a lot of own design of the electron beam column was necessary, too.
Fig.21: Electron beam column [23]
Fig.22 demonstrates the temporal resolution as well as the application for logic state mapping [23]
Fig.22: Temporal sensitivity of e-‐beam-‐tester
A comprehensive discussion of the different operation modes of VC was given by REINERS [24] in 1989.
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Although e-‐beam testing became mature, still laser beam applications were developed such as the laser beam assisted logic state analysis.
Fig.23: Automatic test equipment for laser beam testing (FOUILLAT 1991) [25]
As an important technique for ultra-‐high frequency applications the method of electro-‐optic probing was introduced by WHITAKER. Fig. 20 gives a good description of the system and demonstrates the extreme temporal sensitivity [26].
In parallel to this, attempts were undertaken to achieve picosecond-‐resolution with e-‐beam systems as well either by improved beam blankers or by use of laser stimulated electron emission (see Fig. 25)..
Approaching the end of a “stand alone”-‐EOBT conference, papers on applications of e-‐beam testing gained importance, and, whereas at the beginning only IC applications were discussed, the new applications were more versatile, such as the investigation of solar cells by MIL’SHTEIN [28].
a) Schematic of e-‐o-‐sampling system
b) Exciting and probing beams
c) Temporal response of GaAs switch
Fig.24: Electro-‐optic sampling of integrated circuits [26]
Fig.25: E-‐beam testing with laser induced photoemission (FIXL, 1993) [27]
Fig.26: Potential drop over solar cells for different illumination conditions [28]
Finally, the 1995 conference was the onset of techniques using scanning probe microscopy,
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in special scanning force microscopy (SFM), in order to achieve highest spatial resolution, as demonstrated by two examples.
SPRENGEPIEL reported on measurements on passivated submicron IC by electro-‐force probing [29].
Fig.27: Principle of SFM-‐testing
MERTIN optimized the method of electro-‐optic sampling by the introduction of near-‐field detection by means of a fiber as used in scanning near-‐field optical microscopy (SNOM) [30)
Fig.28: Comparison of SFM result with sampling oscilloscope [29]
a) Pockels-‐cell experiment
b) Indirect and direct (back side) probing
c) SNOM fiber detection for high spatial resolution
Fig.29: Electro-‐optical system with SNOM fiber detection [30]
Summarizing this period is best by referring to the preface of the 1995 meeting: “if we look back at the years that have elapsed since the first EOBT, the changes are clearly apparent. In the first place, electron beam testing has developed to become a standard procedure for design verification and failure analysis…..Optical techniques have also developed further, but no commercial equipment for them is available…..scanning probe techniques, such as the electric force microscope, have developed very well.” This indicates the relative high importance of e-‐beam testing at that time.
ESREF Session C – since 1997
With the merger of EOBT into the ESREF conference automatically the total number of contributions dedicated to this topic reduced significantly. Moreover, due to the fact that many techniques had become quite mature the number of papers with new scientific content shrank as well, and case studies and applications made a much stronger
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contribution than in earlier days. Nevertheless there still is a good amount of interesting developments given.
With respect to new scanning probe techniques the analysis of quantum devices by MONTELIUS (1998) has to be mentioned as an example for one-‐dimensional electron transport [31].
Fig.30: Local measurement of electrical behavior of single electron device for different temperatures [31]
In 2009 TIEDEMANN reported on Finite Element Analyses assisted Scanning Joule Expansion Microscopy on Interconnects in order to understand the thermo-‐mechanical stress in devices[32].
Fig31: a)temperature distribution, b) vertical and c) lateral displacement, d)modulus of total displacement vector [32].
This research followed up local thermal measurements in devices by means of scanning thermal microscopy, as already reported by FIEGE in 1998 [33].
Measurement of mechanical properties was also reported by DILHAIRE (1999) by means of goniometric probing of thermally induced waves, a technique being applied later by the same author on electronic devices [34].
Fig.32: Non-‐invasive probing of thermo-‐ mechanical features of MOS transistor: a) 40 seconds, b )10 minutes, and c) 45 minutes after excitation [34]
Finally GRAUBY showed (2005) that this technique is applicable to non-‐invasive analysis of devices [35].
Fig.33: a) optical image, b) magnitude and c) phase shift of normal surface displacement [35] of ESD protection circuit
Aside of this optical method, other techniques of optical beam testing still remained, and for other applications rather than for devices of extremely high integration, they gained new importance. DE WOLF introduced in 1997 the use of micro-‐Raman spectroscopy for the
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analysis of conduction lines [36]. Laser beam backside probing of CMOS circuits was reported by KASAPI in 1999. Due to short laser, pulse waveforms of about 10GHz could be analyzed stroboscopic [37].
Last not least POGANY demonstrated in 2002 the ability of electric field mapping in InGaP HEMTs and GaAs Terahertz emitters by means of backside infrared OBIC [38].
Fig.34: a) band diagram of gate region, b) cross section, c) OBIC scan in mesa area: OBIC of InGaP-‐HEMT [38]
On the other hand the minute structures of todays integrated devices often do not allow either a non destructive analysis or techniques on bulk material at all, as the interaction volume of an electron beam would be by far too large. This is why the “old fashioned” transmission electron microscope gained its importance back in failure analysis (see for instance ENGELMANN, 2000). Quite often the TEM (or STEM) analysis is accompanied with a FIB (focused ion beam) system for optimum specimen preparation, as in the example of 980nm SL SQW InGaAs/AlGaAS pump laser diode (VANZI; 2000) [40].
Fig.35: Analysis of InGaAs/AlGaAs pump laser a) expected hottest area, b) enlarged view of overstressed facet [40]
But coming to an end of this capture, two opposite effects can be noted. New methods based on optical probes gain further importance, and on the other hand the old SEM still remains an important and reliable tool, as shown by two examples. Using a laser SQUID microscope NIKAWA (2011) could visualize defects in an Vdd line [41].
a) basic concept
b) schematic of system
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c) localization of open defect Fig.36: SQUID measurement of conduction line [41]
And, combining 3D simulation with SEM images allows high quality topography without the disturbing influence of the electric and magnetic fields being present (CIAPPA, 2014) [42]..
Fig.37: 3D simulation of field influence a) isolines of electric field and mesh structure, b) trajectories of electrons [42]
Future aspects
As already mentioned the number of contributions with innovative contents has decreased, and more and more case studies are being reported lately. This is, however, not really a must, as one can see by comparison with other conferences. The recent ISTFA symposia, as an example, contained a lot of new approaches, especially in connexion with the needs for 3D integrated devices. And, some of these papers are authored by European groups, such as the work on “3D void imaging in through silicon vias by X-‐ray nanotomography in a SEM” by LALOUM from ST Microelectronics [43]., Here it may be necessary to motivate researchers, in special
those from Europe, to participate at “ESREF-‐session C”. A further issue it to move to other excitation sources rather than electrons or light, in order to achieve very high penetration depths for the analysis of devices without the need for decapsulation. This may be important for assessment of high power devices, as a sample preparation may change the device behavior significantly. In this respect X rays are one option, another one can be the use of ions in the MeV energy regime. And last not least, as physical failure analysis becomes more complicated, it may be necessary to join it more intensively with computer assisted methods.
References
[1] E. Ziegler and H.P. Feuerbaum, ME 7 (1987), 309-‐316
[2] M. Knoll, Z. Tech. Phys. 11 (1935), 467-‐475
[3] M. von Ardenne, Z. Phys. 109 (1938), 553-‐572
[4] see for instance: C.W. Oatley, JAP 53 No 2 (1982), R1
[5] K.C.A. Smith.and C.W. Oatley, Brit. J. Appl. Phys. 6 (1955), 391-‐399
[6] T. E. Everhart et al., J. Elec. Cont. 7 (1959), 97-‐111
[7] O.G. Wells and C.G. Bremer, J.Phys. E: Sci. Instr. 1 (1968), 902-‐906
[8] G.V. Lukianoff and T.R. Touw, IITRI/SEM (1975), 465-‐571
[9] G.S. Plows and W.C. Nixon, J.Phys. E: Sci. Instr. 1 (1968), 595-‐600
[10] A. Gopinath and M.S. Hill, IITRI/SEM (1973), 197-‐204
[11] C. Donolato, Optik 52 (1978), 19-‐36
[12] H.J. Leamy, JAP 53 No 6 (1982), R51-‐R80
[13] C. van Opdorp, Philips Res. Rept. 32 (1977)
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[14] D.B. Holt, see for instance: DB Holt et al. “Quantitative Scanning Electron Microscopy”, Academic Press, London, New York, San Francisco (1974)
[15] D.B. Wittry and D.F. Kyser, JAP 36 No 4 (1965), 353-‐358
[16] J.I. Pankove, JAP 39 No 12 (1968), 5368-‐5371
[17] see for instance: LJ. Balk and E. Kubalek, IITRI/SEM (1977), 739-‐776
]18] J.A. Valdmanis et al., APL 41 (1990), 211
[19] G.V. Lukianoff, ME 7 (1987), 115-‐129
[20] A.R. Dinnis, ME 7 (1987), 139-‐146
[21] F. Komatsu et al., ME 7 (1987), 267-‐274
[22] T. Wilson, ME 7 (1987), 297-‐307
[23] V.R.M. Rao and P. Winer, ME 12 (1990), 295-‐302
[24] W. Reiners, ME 12 (1990), 325-‐340
[25] P. Fouillat et al., ME 16 (1992), 287-‐294
[26] J.F. Whitaker et al., ME 12 (1990), 369-‐397
[27] A.J. Fixl and K.A. Jenkins, ME 24 (1994), 81-‐88
[28] S. Mil’shtein, ME 31 (1996), 3-‐12
[29] J. Sprengepiel et al., ME 31 (1996), 181-‐186
[30] W. Mertin, ME 31 (1996), 365-‐376
[31] L. Montelius et al., MR 38 (1998) 943-‐950
[32] A.-‐K. Tiedemann et al., MR 49 (2009), 1165-‐1168
[33] G.B.M. Fiege et al., MR 38 (1998), 957-‐962
[34] S. Dihaire et al., MR 39 (1999), 981-‐985
[35] S. Grauby et al., MR 45 (2005), 1482-‐1489
[36] I. de Wolf et al., MR 37 (1997), 1591-‐1594
[37] S. Kasapi et al., MR 39 (1999), 957-‐961
[38] D. Pogany et al., MR 42 (2002), 1673-‐1677
[39] H.J. Engelmann et al., MR 40 (2000), 1747-‐1751^
[40] M. Vanzi et al., MR 40 (2000), 1753-‐1757
[41] K. Nikawa et al., MR 51 (2011), 1624-‐1631
[42] M. Ciappa et al., MR (2014)
[43] D. Laloum et al., ISTFA Proceedings (2013)
Abbreviations:
IITRI/SEM: IITRI Scanning Electron Microscope Symposium, Chicago, U.S.A.
ME: Microelectronics Engineering
MR: Microelectronics Reliability