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    Iranian Journal of Chemical EngineeringVol. 7, No. 2 (Spring), 2010, IAChE

    Resea rch note

    Dynamic Simulation of an Industrial Rotary Dryer

    Sh. Shahhosseini ∗ , M.T. Sadeghi, H. R. Golsefatan

    Process Simulation and Control Research Laboratory, School of Chemical Engineering, Iran University of Science and Technology (IUST), Narmak, Tehran, Iran

    AbstractSolid transport phenomena drastically affect rotary drying process. A change in any

    solid movement variable such as particle hold up or input flow rate results in a significant variation of heat and mass transfer rates. Therefore, in this researchdynamic study of these phenomena was conducted both experimentally andtheoretically. Several experiments was performed employing an industrial granuledryer. The dryer length and diameter were 5 and 1 m, respectively. In each experimentone of the solid movement variables was changed and the resulting dynamic change onthe process was measured. The data was used to estimate the parameters of a dynamicdistributed parameter model of the system using dynamic optimization method. Thedata were also employed to evaluate the model. The model predictions for solid hold upand outlet flow rate were compared with those of the experimental data. The averagemodel error for solid hold up and outlet flow rate were 5.6% and 5.4 %, respectively.

    Keywords: Solid transport, Rotary Dryers, Modeling, Nitrocellulose, Simulation

    ∗ Corresponding author: [email protected]

    1- Introduction Nitro cellulose (NC) is used inmanufacturing lacquer, stencil paper, ink,varnished cloth, sealing cover, binder, leatheroil, nail polish and several other materials.The drying process is the last section of the

    NC production line. In this process thetemperature and moisture content of NC

    particles are tightly controlled to ensure the

    high quality of the product. Rotary dryers aresuccessfully used for solid particle drying.The main advantages of rotary dryers aretheir simplicity, flexibility and largecapacity. Compared with fluidized and

    conveyor-belt dryers rotary dryers are themost expensive to construct but have thelowest operating cost [1]. The rotary dryer issuperior to the fluidized dryer for continuoustreatment of solids. In continuous mode the

    products of fluidized dryer are not uniformdue to the rapid mixing of solids leading tonon-uniform residence time of solids in thedryer [2]. Rotary dryers, if equipped for

    particle lifting flights, are suitable forremoving the solvents (mainly water) fromsolid particles. This dryer can be runcontinuously, while rotation rate, inlet airtemperature and flowrate can be used to

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    control solid temperature and moisture.Particular flight design can be used for eachmaterial, resulting in a large portion of air

    born particles. This leads to high mass and

    heat transfer rates between the air and solid particles.Process control is very important to drying

    processes with significant economicalimpacts. This includes tighter temperatureand moisture control of the product to avoidfinancial penalties as well as associatedoperational problems such as dusting. Mostimportantly, a too high temperature of anindustrial dryer may result in fire or even

    explosion. High moisture content of solid particles at the outlet of the dryer has anadverse impact on the quality of those

    products for which NC is an ingredient suchas paint and nail polish. On the other hand,too much drying would result in more brittle

    particles, leading to more dust in the dryerand in turn increase the chance of anexplosion. Since light particles can be blown

    back and accumulate in the dryer, dustingcan cause dryer over-load. When overloaded,the dryer performs badly yielding higheroutput moisture until it recovers and thecycle reoccurs. Traditional feedback controlshave generally proved inadequate in

    providing stable operation under a range of process disturbances such as changes in inletair and product moisture. To tackle thischallenge, implementation of a model-based

    control for such processes can beadvantageous, with the models capturing thecomplex dynamic interactions in the system.Furthermore, advanced control strategies canimprove the drying because of the largetransportation lag in the dryer and significantinteractions between the process variables. In

    a control study reported by Duchesen et al.,five control strategies have been evaluatedusing a dynamic rotary dryer simulator formineral concentrate [3]. Two control

    strategies are based on PI controllers and theothers use neural network models.In spite of the indisputable importance, theidentified model uncertainties introduced byinaccurate determinations of heat and masstransfer coefficients, as well as solidretention times, have significantly restrictedthe implementation of a model-based controlfor rotary dryers. Consequently, it is essentialto develop an improved dynamic model with

    minimized plant-model mismatch for theaccurate prediction of rotary dryingdynamics and the implementation of model-

    based control. There have been severalattempts to develop models for rotary drying.Sharples et al. [4]; Chandra and Singh [5];Kamke and Wilson [6], Brasil and Seckler[7], and more recently Shene et al. [8] usedmathematical models to study steady state

    behavior of the process. Douglas et al. [9] proposed a model to study the dynamics aswell as the steady state behavior of the

    process. This model is a discretized form of adistributed parameter model. To use thismodel for the distributed rotary dryingsystem, the drum was divided into a numberof equal segments. A lumped parametermodel was then used for each of thesesegments. In order to compute retention

    times, the model employed the semi-empirical correlation suggested by Friedmanand Marshall [10].It can be identified in the literature that keyissues in the modeling of rotary drying

    processes are the computation of heat andmass transfer rates, and the determination of

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    solid retention times. The reported worksalso show that there are two main difficultiesin computing heat and mass transfer rates ofrotary dryers. First, the contact surface area

    between the solid and the gas is not constant.This area depends on several variables suchas solid hold-up, solid distribution, thestickiness of the particles and the hinderednature of the falling particle curtain. A modelthat considers all the variables affecting thecontact surface area is extremelycomplicated. Such a model has not beenreported in the literature. Second,computations of mass and heat transfer

    coefficients are not sufficiently accurate.They are commonly calculated usingempirical equations whose parameters areestimated by employing a set of experimentaldata obtained under a specific set ofoperating conditions. When the operatingconditions change, these equations may notestimate the coefficients accurately. Hence,there is a need for an adaptive model that canestimate these parameters on-line.Shahhosseini et al. have developed a modelfor a rotary sugar dryer that employs on-lineexperimental data to adapt itself to anyoperating conditions [11].Solid particle distribution in the drum affectsthe amount of contact surface between thesolid and the gas. Solid particle retentiontime influences the time the particles can stayin contact with the gas to transfer heat and

    mass. Any heat and mass transfer model for asolid particle dryer must be able toreasonably predict solid flowrate and solidhold-up. There have been several reports inthe literature regarding the modeling aspectsof solid transport in dryers. If the model isdeveloped for model-based control, it must

    be simple and yet represent the dynamics ofthe system accurately.Several researchers have attempted todevelop mechanistic solid transport models,

    Matchett and Baker [12], Sherritt et al. [13],Sherritt et al. [14] and Wang et al. [15].However, the reported models are not fullymechanistic and still employ some empiricalcorrelations. Earner [16] found these modelswere more complicated than the Friedmanand Marshall model and did achievesatisfactory accuracy. Shahhosseini et al.modified the Friedman and Marshall solidtransport model by adding one more

    parameter to it, resulting in more flexibilityand accuracy of the model predictions [17].The main objective of this study was toobtain a simple and yet accurate model for anindustrial rotary dryer. This model wasneeded for inferential and model basedcontrol of the dryer. Such a model has beenreported for a pilot sugar rotary drying

    process by Shahhosseini et al. [17]. Sincesolid material and particle size in theindustrial NC dryer are different from thoseof sugar dryers, the parameters in solidtransport equations of the process modelwere to be estimated employing the industrialexperimental data dryer. In this work, severalexperiments were conducted to collect thedata necessary to estimate solid transportmodel parameters and to evaluate the model.The model predictions and the experimental

    data were compared in order to evaluate themodel.

    2- Mathematical modelThe model used in this work, for theindustrial dryer was similar to that reported

    by Shahhosseini et al. [11]. Since the aim of

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    this work was a comparative study on thesolid transport aspect of the model, only solidtransport equations are presented here. Moredetailed aspects of the model are given in this

    reference [11]. The following equation showsthe dependency of solid hold up and flowrateon the time and space.

    z F

    t H s s

    ∂ ∂

    ∂ ∂ = (1)

    Where, H s is the solid hold-up of the dryer(kg) and F s is the solid outlet from the dryer(kg/s). One way to solve such a partial

    differential equation is to use the method oflines, in which the dryer is divided into nsections as shown in Fig. 1.In this way Equation 1 is discretized and can

    be written as follows.

    1 s( i )

    s( i ) s( i )dH

    F F fo r i 1 ,.. .,ndt

    −= − = (2)

    Where, H s(i) is the solid hold-up in the ithsection of the dryer (kg), and F s(i) is the solid

    outlet from the ith section of the dryer (kg/s).The following retention-time equationsinitially proposed by Friedman and Marshalland modified by Shahhosseini are also

    incorporated into the solid model [8 & 10].

    0 8 0 5

    at ( i ) ( i ) . .

    s( i ) s p

    ( F ) R L

    tan( )R D D F

    α β γ

    δ

    ⎡ ⎤+⎢ ⎥= +⎢ ⎥⎣ ⎦

    (3)

    Where: F a is the air flowrate (kg/s) Rt is the retention time (s)δ is the drum slope to horizontal(degrees)

    R s is rotation speed of the drum (rpm) D is the dryer diameter (m) D p is weight average particle size (m)α, β , and γ are parameters which should

    be estimated using experimental dataThe model parameters ( α, β , and γ) wereestimated using experimental data and anoptimization routine written in this study.

    s( i ) s( i ) t( i ) H F R for i 1 ,.. .,n= = (4)

    Figure 1. The divisions of the dryer applied to discretize the partial differential equations.

    air input

    output

    solid in ut

    air output

    i-1i i+1

    F s(i-1)F s(i)

    F s(i+1)

    Fa(i+1)

    F a(i-1)Fa(i)

    1

    n

    solid

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    A mass balance equation is also presented inorder to demonstrate the importance of thesolid transport equations to calculate heatand mass transfer rates. Solid water content

    mass balance for the ith segment is given by:

    1 1

    w ( i )

    s( i ) s( i ) w( i ) s( i ) w( i ) r( i ) w( i )

    s( i )

    dM

    dt dH

    ( F M F M ) d M dt

    H

    for i 1 ,...,n

    − −

    =

    − − −

    =

    (5)

    Where, M w(i) is solid moisture content anddr(i) is drying rate in the ith segment of thedryer. This equation indicates that solid flowrate and hold up of the ith segment, whichare calculated from equations 2 and 4,respectively, can be used to compute solidwater content of the ith segment. Since thedynamic model is supposed to be used foron-line model-based control of the process,drying rate was computed using the on-linedata of inlet and outlet air humilities andflow-rates applying the following equation:

    ininaout out ar W F W F d )()( −= (6)

    Applying equation (6) needs to assume thatdrying rate remains constant over a short

    sampling period. The drying rate in eachsegment of the dryer d r(i) can be computed ifthe distribution of the solid water content inthe dryer is known. Alternatively, it can be

    calculated by dividing the drying rate,obtained from equation (6), to the number ofthe segments (n) as shown below.

    nd

    d r ir =)( (7)

    3- Experimental methodsThe experiments were designed in order toobtain appropriate data for the estimation ofthe model parameters ( α , β and γ) and to

    investigate the effects of air flowrate,rotation speed and solid flowrate on the solidretention time in the dryer. The experimentswere conducted employing an industrialdryer. The dryer length and diameter were 5and 1 m respectively. There were 11 flightsmounted on the inside of the drum. Aconveyer belt was used to feed particles tothe dryer in a constant rate. The dryer wasequipped to appropriate instruments to keepthe rotation speed and inlet air flowrate andtemperature at their desired values. Table 1shows the conditions of the threeexperiments performed in this study.

    Table 1. The conditions of experiments 1 to 3.

    Number of the experiment 1 2 3

    The specific test

    A pulse in solid inlet from

    5.3 to 7 kg/min for 20minutes

    A step in solid inlet from5.3 to 2.75 kg/min

    A step in air flow rate from2500 to 1500 m 3/hr

    Air flow rate (m 3/hr) 2500 2500 2500

    Inlet solid flowrate (kg/min) 5.3 5.3 2.75

    Rotation speed (rpm) 1.1 1.1 0.75

    Inlet NC moisture content 31% 31% 31%

    Outlet NC moisture content 19.9% 16.7% 18.4%

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    4- Results and discussionsThe steady state and one set of dynamic datawere employed to estimate the parameters ofthe model ( α, β and γ). The estimated values

    were 16.302, 1.012 and .785 for α, β and γ,respectively. The model was then used to

    predict solid holdup and output flowrate,while estimated parameter values wereinserted into the model equations. Anotherset of experimental data was then comparedwith the model predictions, produced in thesame conditions. Figures 2 to 5 indicate someof the comparisons between mode

    predictions and the data. On the whole, the

    model predicted solid hold up and outlet flowrate with average errors of 5.6% and 5.4 %respectively.Fig. 2 shows the response of the process interms of solid output flow rate to a pulseinput in terms of solid inlet from 5.3 to 7kg/min, which took 20 minutes. The pulsestarted 175 minutes after the onset of the

    experiment. The experimental data in thisfigure indicate that solid output begins to risearound 25 minutes after the solid input wasstepped up, which means there is a death

    time in the response of the output flow rate tothe input flow rate. The simulation results ofthis figure show the model can predict thedeath time. The model is able to predict thedeath time since it is a distributed parametermodel so that the sum of the retention times,calculated for all of the segments of thedryer, are equal to the death time that is

    predicted by the model. However, the predicted death time is much shorter (around

    10 minutes). Similar behavior can beobserved when the pulse is finished at 195minutes. The figure indicates that the model

    prediction profile and the experimental datafollow very close trends. Therefore, themodel has been able to predict the processresponse reasonably well.

    0 50 100 150 200 250 300 350 4005

    5.2

    5.4

    5.6

    5.8

    6

    6.2

    6.4

    6.6

    6.8

    7

    o u

    t p u

    t f l o w

    r a

    t e ( k g

    / m i n )

    time (min)

    when pulse started

    modelexp

    Figure 2 . The comparison between solid output data of experiment 1 and the model predictions .

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    The reason is that Fig. 3 shows the responseof the process in terms of solid output flowrate to a step change in solid inlet from 5.3 to7 kg/min, which occurred 175 minutes after

    the experiment was started. This figuredisplays that solid output flow rate hasstarted to respond to the step down around 25minutes later. This indicates that the modelhas been able to predict the death time aswell. This figure implies high accuracy of themodel, since the model prediction profilestays very close to the experimental data.Fig. 4 depicts model predictions andexperimental data in terms of dryer holdup

    during experiment 2. In this experiment solidinlet rate was dropped down from 5.3 to 7kg/min 180 minutes after the experiment wasstarted. Since a reduction in the solid inletdoes not immediately lower solid outlet, asshown in Fig. 3, solid holdup decreases rightafter the decrease in the solid input rate. Theholdup gradually decreases till it reaches anew level. The figure also indicates a goodagreement between the model predictionsand the experimental data.Figure 5 displays the model predictions and

    the experimental data of experiment 3 interms of solid outlet. In this experiment airflow rate was dropped down from 2500 m 3/hrto 1500 m 3/hr 275 minutes after the start of

    the experiment. Since air flow affects themovement of air born particles, a change inits rate almost immediately causes a variationin solid outlet. In this research the dryerworked in counter current mode where theair flow blows back the air born solid

    particle. Therefore, a decrease in air flow ratemeans less blowing air, leading to atemporary increase in the solid outlet due tothe sudden reduction of air resistance against

    solid movement. The figure also indicatesthat the model could predict this

    phenomenon. The reason for the modelability to predict this phenomenon isconceivable by observing equation 3. Thisequation implies a reduction in the air flowrate (Fa) causes a decrease in solid retentiontime, leading to an increase in solid flow rate.However, according to equation (3), thesevariations happen immediately, while theexperimental data display rather gradualchanges.

    0 50 100 150 200 250 300 350 4002.5

    3

    3.5

    4

    4.5

    5

    5.5

    fsin = 5.3 kg/min

    step down time

    fsin = 2.75 kg/min

    o u t p u

    t f l o w r a

    t e ( k g

    / m i n )

    time (min)

    model

    exp

    Figure 3. The comparison between solid output data of experiment 2 and the model predictions .

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    0 50 100 150 200 250 300 350 4000

    50

    100

    150

    200

    250

    300

    350

    400

    fsin = 5.3 kg/min

    fsin=2.75 kg/min

    H o

    l d u p

    ( k g )

    time (min)

    model

    exp

    solid inlet

    Figure 4. Comparison between solid hold up data of experiment 2 and the model predictions .

    0 100 200 300 400 500 6000

    0.5

    1

    1.5

    2

    2.5

    3

    3.5

    fa = 2500( m 3 /hr )

    fa = 1500( m 3 /hr )

    o u

    t p u

    t f l o w

    r a

    t e ( k g

    / m i n )

    time (min)

    model

    exp

    air flow rate

    Figure 5. Comparison between solid output data of experiment 3 and the model predictions.

    5- ConclusionA mathematical model that computes heatand mass transfer rates from on-lineexperimental data was developed for anindustrial granule dryer. This model employsmodified Friedman and Marshal Equation.Solid transport equations of the model wereevaluated against the experimental data.

    Visualized and quantitative comparisons between model predictions and theexperimental data indicated that the modelcould reasonably represent the solid transport

    phenomena. The average model error forsolid holdup and outlet flow rate were 5.6%and 5.4 %, respectively. Therefore, it can beconcluded that the model is sufficiently

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    accurate to be used for the optimization andmodel-based control of industrial rotarydryers.

    6- NomenclatureD dryer diameter, mD p weight average particle size, mdr drying rate, kg/sFa air flowrate, kg/sFs solid outlet from the dryer, kg/sFs(i) solid outlet from the ith section of

    the dryer, kg/sH s solid hold-up of the dryer, kgH s(i) solid hold-up in ith section of the

    dryer, kgL(i) length of the ith segment, mMw solid water content, kg/kgR t retention time, sR s rotation speed of the drum, rpmt time, sw air humidity, kg/kgz dryer length, mα , β, γ parameters which should be

    estimated using experimental dataδ drum slope to horizontal, degrees

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