Download - TRACE 1300 Series New Presentation
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Moving from TRACE GC Ultra
to………..
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Mov ing from TRACE GC Ultra to ......
• How Thermo TRACE GC Ultra was structurallyconcepted:
• Mainframe - Oven Overview
• Injectors - Detectors Overview
• Detector base body concept Gas
ModulesOverview
Detectors Overview
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DPFC module
Injectors
detectorscassette
Keypad
Electronics
DGFC module
Detectors
Detectorsbasebodies
Mainframe & Oven Overview
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In ject ions Overview
True coldOn-Column
Split/Splitless PTV Packed and
wide-bore
columns
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It allows simple detector
interchangeability
It ensures flexibility without
adding complexity
Base body
Detector
Oven
GC top deck
Detector base body concept
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Detector base body concept
A common base whichprovides the detector
with main heating and
gas feeding
All detectors are
available with both
Digital Gas Flow Control
(DGFC) and conventional
pressure regulators (non-DGFC)
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Mov ing from TRACE GC Ult ra to ............
.....................................
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.........TRACE 1300 Series Modular Concept
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.....TRACE 1300 - 1310 Series Modu lar Concep t
• A main electronic module that includes: main CPU, oven control,
power supply.
- 2 versions: 220V and 120V
• Injector modules include injector body, electronics for injector
temperature and carrier gas control.
• Detector modules include detector cell and electronics for signal
amplifier –digitalization, for temperature and detector gas control.
• TRACE 1300 – TRACE 1310 can accommodate 2 inlet and 2 detector
modules (2 channels) self-recognized
• Additional external devices can be located into dedicated housing.
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TRACE 1300 - 1310 Series Modular i ty Advantages
• Modules can be tested (also
analytically) separately prior testing
the assembled unit
• Modules can be shipped separately
and assembled during the
installation in field
• Modules can be kept in stock for fast
replacement, upgrading, or change
of configuration
• Possibly modules would be replaced
without requiring a field service
engineer
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TRACE 1300 - 1310 Modu lar Concep t
Trace GC 1300: Local built-in ultra-
simplified user interface - two
buttons and four LEDs.
Trace GC 1310: Touch screen
interface provides instant access for
ease of use and local control
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TRACE 1300 - 1310 Series Modu lar Con cep t
Where the parts were on TRACE GC Ul t ra
and
Where they are now on TRACE 1300 Series
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TRACE GC Ultra TRACE 1300 - 1310
• Injector
• DPFC/DCC module
• EPC Board
• Thermoregulator
(I/O Feedback board)
• Power control
• Injector Module
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TRACE GC Ultra TRACE 1300 – 1310
• Detector Module• Detector
• Base body
• DGFC module
• Detector board
• Thermoregulator
(I/O Feedback board)
• EPC board• Power control
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TRACE GC Ultra TRACE 1300 – 1310
• CPU Board
• I/O Feedback board
• Mother board
• Power supply
• Electronic Compartment
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TRACE GC Ultra TRACE 1300 – 1310
• User Interfaces 1300
• User Interfaces 1310
• GC Keypad
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TRACE 1310
Instrument Control
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TRACE 1310
Configuration
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TRACE 1310
Diagnostics
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TRACE 1310
Status
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TRACE 1310
Maintenance
*When Graph Pack adapters will be used,
the column insertion into the Injector and
Detector inlets must be added of 12mm.
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TRACE 1300 - 1310 HW connect iv i ty
• Two RS-232 ports for Autosamplercontrol
• Thermo Fisher bus I2C with 5V
power for additional auxiliarydevices
• GC Control through Ethernet IP address
• Direct connection to PC (reversed RED cable)
• Connection to LAN (standard GREY cable)
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TRACE 1300 - 1310 Ethernet con figurat ion
• MAC address fixed and assigned in the factory
• IP Address -> need to be assigned
• TCP Port -> 2551 (different from the one used on Trace
GC)
• Chrom-Card and Xcalibur accepts TCP Port=2551
• ChromQuest has a different TCP Port -> need to be changed in
TRACE 1300-1310
• Ethernet Configuration details listed within “Diagnostic”
menu
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TRACE 1300 – 1310 Set up
• From the PC, launch the Setup.exe file named TR1300ST (Service
Tool) entering ThermoFisher as password, then, press OK.• This SW load the whole package zip file as it is. Do not change any file
inside.
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TRACE 1300 – 1310 Set up
• Automatically the SCAN will start to check how many systems are present.
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TRACE 1300 – 1310 Set up
• Selecting the instrument on which IP set-up and Firmware updating must
be performed, automatically the two dedicated options will be activated
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TRACE 1300 – 1310 IP Set up
• Selecting IP Set-up a new page will be shown where GC name and IP
address can be modified.
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TRACE 1300 – 1310 F/W update
Selecting F/W update a new page will be shown, click on “Browse
package name” and select where the package with the new firmware
version is present (C: or USB, or..... ) Do not change any file inside.
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TRACE 1300 – 1310 F/W update
• On the new page will be shown the TRACE 1300-1310 configuration with
the current F/W version of the modules installed and the package of the
new firmware version. Select Update to start the F/W updating.
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TRACE 1300 – 1310 F/W update
• F/W updating in progress..............
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TRACE 1300 – 1310 F/W update
• At the end of the F/W updating, all the status cell must be OK.
• Click Done to close the program.
TRACE 1300 - 1310
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TRACE 1300 1310
HMI SW update from USB st ick
• HMI SW can be updated through the USB port positioned below the
touch screen
TRACE 1300 - 1310
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TRACE 1300 1310
HMI SW update from USB s t ick
Configuration
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TRACE 1300 – 1310 Series
..............more in depth
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TRACE 1300 – 1310 SSL In jecto r Modu le
• Manifold (Plumbing)
• Removable SSL Injector Body
• 2 Electronic Boards
• 3 Solenoid Valves
(Carrier, Split & Purge)
• 2 Removable Filters (Carrier & Split)
C SS
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TRACE 1300 – 1310 SSL Injecto r Modu le
• Designed to have a cool head and
septum.• Septa is kept below 150°C even
with inlet set to 350°C
• Lower septum bleeding
(siloxanes)
• No septum sticking• Lower air (oxygen) diffusion
• Longer septa lifetime
• The cool head SSL is optimized
for cold needle injection
0
10
20
30
40
50
60
70
80
90
100
100 150 200 250 300 350 400
T (°C)
D e p t h ( m m )
TRACE 1300 1310
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TRACE 1300 –1310 SSL Technical Speci f icat ion
• Temperature range:
• Maximum temperature 400º C with temperature settings resolution of 1º C units
• Temperature stability 1º C
• Heater cartridge 80W 48Va.c.
• Pneumatics:
• Electronic control only
• Constant pressure
• Constant flow
• Flow regulation through calculated pressure
• Pressure or flow programming in three ramps and four plateaus
• Pressure range:
• 0 to 1000 KPa, with a resolution of .015 KPa, and stability of 0.1 KPa along the entire scale
• Flow ranges:
• Column flow from 0.1 to 100 ml/min, with resolution of 0.01 ml/min
• Split flow from 10 to 1250 ml/min He with resolution of 1mL/min
• Septum purge flow from 0 to 50 ml/min with resolution of 1mL/min
• Ambient temperature and pressure compensation
• Gas saver function
• Operating modes:
• Split /Split less
• Surged Split/Surged Split less
• Large Volume Split less
• Back-flush capability (*) NOTE: Standard SSL CANNOT BE con verted to SSL BKF a new mo dule MUST BE requested.
TRACE 1300 1310 PTV I j t M d l
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TRACE 1300 – 1310 PTV In jecto r Modu le
• Manifold (Plumbing)
• Removable PTV top head
• Removal of bottom column
connection for easier cleaning of
internal body
• 2 Electronic Boards
• 3 Solenoid Valves
(Carrier, Split & Purge)
• 2 Removable Filters (Carrier & Split)
• Cooling Fan
TRACE 1300 1310 PTV I j t M d l
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TRACE 1300 – 1310 PTV In jecto r Modu le
• Removal top body plus tubing
for easier cleaning
• Removal of bottom column
connection for easier cleaningof internal body
TRACE 1300 1310 PTV T h i l S if i t i
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TRACE 1300 – 1310 PTV Technical Specif icat ion
• Temperature operating range:
• Maximum temperature 450º C with temperature settings resolution in 1º C units
• Temperature stability 1º C maximum at 250º C for 30 minutes
• Temperature program rate up to 14.5ºC/sec
• Heater assy 120W 48Va.c.
• Capable of sub ambient operation to -50º C with LN2, 0º C with CO2
• Sub-ambient control will be optional and should not add cost to base unit.
• Three different temperature programmable ramps, four plateaus
• Pneumatics:
• Electronic control only
• Constant pressure
• Constant flow (Flow regulation through calculated pressure)
• Pressure or flow programming in three ramps and four plateaus
• Pressure programming: 0 to 1000 KPa, with a resolution of .015 KPa, and stability of 0.1 KPa along the entire scale
• Flow programming: 0.1 to 100 ml/min, with resolution of 0.01 ml/min
• Independent pressure/flow set points during injection
• Ambient pressure compensation.
• Control of split flow in 1mL/min from 10 to 1250 mL/min He• Gas consumption saver
• Purge flow from 0 to 50 ml/min
• Operating modes:
• Split, Splitless, Solvent Split (Large Volume)
• Back-flush capability (*) NOTE: Standard PTV CANNOT BE co nverted to PTV BKF a new m odu le MUST BE requested.
TRACE 1300 1310 I j t M d l
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TRACE 1300 – 1310 In jecto r Modu les
SSL Body PTV Head
TRACE 1300 1310 FID D t t M d l
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TRACE 1300 – 1310 FID Detecto r Modu le
• Manifold (Plumbing)
• Detector body
• 2 Electronic Boards
• 3 Solenoide Valves
(Air, Hydrogen & Make up)
TRACE 1300 1310 D t t S if i t i
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TRACE 1300 – 1310 Detecto r Specif ic at ions
• FID Techn ical Specif ic ations
• Maximum operating temperature, 450º C
• Flameout detection and warning
• Automatic flame re-ignition with shutdown of gases upon failure (3
times)• MDA: <2 pg carbon/sec as propane
• Linear dynamic range 10^7
• Acquisition rate up to 300 Hz
TRACE 1300 1310 Detecto r Specif ic at ions
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TRACE 1300 – 1310 Detecto r Specif ic at ions
• TCD Techn ical Specif icat ions
• Maximum operating temperature, 400º C, filament ambient to 450º C
• Operating modes: constant mean temperature
• Filament protection in case of carrier gas failure
• Compatible with Fe/Ni or W/Re filaments• MDA: 600 pg ethane/ml He carrier
• Linear dynamic range >= 10^6
TRACE 1300 1310 Detecto r Specif ic at ions
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TRACE 1300 – 1310 Detecto r Specif ic at ions
• NPD Technical Specif icat ions
• Compatibility with DET’s TID-2, Agilent’s BLOSand other DET TID types.
• MDL: Nitrogen: 0.05 pg N/s or better;
Phosphorus: 0.02 pg P/s or better.
• Dynamic and Linear Range: Dynamic range of response: 10E6; Linear
range: 10E4 or better.
• Selectivity: N/C = 50,000 to 1 gN/gC or better; P/C = 200,000 to 1 gP/gC
or better.
• Data acquisition rate: Up to 300Hz to be compatible with fast and
ultrafast GC.
• Maximum Operating Temperature: Up to 450°C.
• Heating Current setting: 1.00 to 3.50 A (or different range according to
the source requirements) in 0.01 steps.
• Source protection in case of gas failure
TRACE 1300 1310 Detecto r Specif ic at ions
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TRACE 1300 – 1310 Detecto r Specif ic at ions
• ECD Techn ical Specif icat ions
• Maximum operating temperature: 400º C
• Cell volume <= 150 µl
• Acquisition rate up to 100 Hz
• Operating mode: constant current, pulse modulated• MDA <= 5 fg Lindane
• Linear dynamic range: >10^4 Ar/CH4 make-up
• Equipped with removable collector electrode for local maintenance
TRACE 1300 1310 Pneumatic Net
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TRACE 1300 – 1310 Pneumatic Net
TRACE 1300 1310 Gas Net Assembly
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TRACE 1300 – 1310 Gas Net Assembly
TRACE 1300 1310 Gas Net Location
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TRACE 1300 – 1310 Gas Net Location
TRACE 1300 – 1310 Components lo cat ion
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TRACE 1300 1310 Components locat ion
Hermes back view
toroidal
transform
electronic box
gases inlet
fan motor
H2
sensor
(optional)
Hot air
outlet duct
main switch
detector
moduleinjector
module
oven
door
insulation
material
TRACE 1300 – 1310 Oven heating
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TRACE 1300 – 1310 Oven heating
• The tension rate changes from 230V to 120V but not the baffle.
• The serial or parallel heaters wiring is driven by the electronic box,
according to the tension rate. heating element
RTD
back viewfront view
TRACE 1300 – 1310 Module “Electronics”
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Backplane
TRACE 1300 – 1310 Module Electronics
CONTROL AREA
Connections for:
2 x injector
2 x detectors
1 x PT100
1 x door switch
1 x stepper (flaps)
1 x H2 sensor
3 x 24V auxiliary
POWER AREA
Connections for:
1 x main line
1 x 500VA pri.
1 x 500VA sec.
1 x heater
1 x fan (oven)
TRACE 1300 – 1310 Module “Electronics”
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Electronic compartment
Oven & Power
Main CPU
External Interface
Power switching
Breaker
Fan Handles
TRACE 1300 – 1310 Module Electronics
TRACE 1300 – 1310 Series Auto samplers
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TRACE 1300 – 1310 Series Auto samplers
In ject ion posi t ion Inlet maintenance posit ion
TRACE 1300 – 1310 Series Auto samplers
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In let Maintenance pos it ionInject ion posi t ion
TRACE 1300 1310 Series Auto samplers
TRACE 1300 – 1310 Series Auto samplers
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TRACE 1300 1310 Series Auto samplers
TRACE 1300 – 1310 Series Auto samplers
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TRACE 1300 1310 Series Auto samplers
TRACE 1300 - 1310 Series & ISQ
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TRACE 1300 1310 Series & ISQ
TRACE 1310 & ISQ must look like a single instrument
when coupled
TRACE 1300 – 1310 Series