ETC-TOXICONJuly 13, 1988
0 2 3
Environmental Testingand Certification Corp.ETC-TOXICON3213 Monterrey BoulevardBaton Rouge, LA 7081~504-925-5012
Mr. Russell D. HartRemedial Project ManagerCES-MI/WI UnitU.S. Environmental Protection AgencyRegion 5230 South Dearborn StreetChicago, Illinois 60604
RE: Request for Information Dated June 22,1988
Dear Mr. Hart:
The residential well samples analyzed for Rollins Field Services were run in accordancewith Statement of Work for Organic Analysis Multi-Media, Multi-Concentration OrganicsGC/MS Techniques 7/85 Revision (SOW 785), Office of Solid Waste and EmergencyResponse, Washington, D.C., August, 1985.
Instrument Detection Limits were calculated as (° n-1) standard deviation of three 20 ug/Lstandards calibrated against a 50 ug/L standard.
A copy of the data subset has been included for your perusal.
If you havej^x^aesnqhslripase feel free to call me at (504) 925-5012.
Since
Michael D. CrouchPresident
MDC/ecc
EPA Region S Records Ctr.
232427
Initial Calibration DataVolatile HSL Compounds
Case No: Region:
Contractor: Tnyionn I nhnrafcories. Inc.
Contract M»68-01-7026
Instrument I O: FJNN2
Calibration Date:. I "2.-Z-- 67
Minimum AT for SPCC is 0.300(O.25 for Bromoform)
Maximum % RSO for CCC is 30%
I Laboratory ID
I Compound ^"20 RF150 «F200 RTCCC-
pRSO I SPCC-
IChloromethane 1/006 I 3.t>ooiBromomethane . 3/3
Chloride 0.3?7IChloroethaneIMethylene Chloride 3l. <?/.?*/(Acetone yT-733 /.T.47/I Carbon Oisulfide 0./7Q1. 1-Oichloro«thene
1.1 -O«ch(oro«thane[Trans-1. 2-OichtofoetheneI Chloroform
1. 2-Oichloroethane 33?|2-Butanone //. 362. 9. OS"/ /,/t.O1.1. 1-Trichloroeihane
(Cartoon Tetrachloride
I Vinyl Acetate /9.Q8/ I /y.S-67I Bromodichlorometharve
. 2-O«chk>ropropane /9.ra/-1. 3-Dichloropfopenel
I Trichloroethene \jo.off I /y.r«/7Dibfomochloromethane Q.TS31.1. 2-Trichloro«thane ?. 3o/
IBenzene
|cis-1.3-0ichtofopfopeoe|2.Chlofoethy«vinytethefI Bromoform
14-Methyf-2-Pentanone 79. 2,^0812-HenanoneI Tetrachloroethene
1. 1. 2. 2-Tetrachloroethar 0.3/2-OMo'sToluene
IChlorobenxene
IStyrene[Total Xyfones
HF -ResponM Factor (cubccript is lh« Amount of ug/L)fiF -Av«r«oe Re*pon«« Factor
-Percent RaUftve Sundird O««Mtion
CCC -Calibration Check Compounds (.JSPCC -System Performance Check Compounds (-.»
Form VI
GC/MS TUNING AND MASS CALIBRATION
Bromofluorobenzene (BFB)
Case No.
Instrument ID
Lab ID
Contractor Toxicon Laboratories. Incnnmran No. 60-01 -O
Date Q/ ~ #-<^ -*y "7 Time.
Data Release Authorized By:
m/e ION ABUNDANCE CRITERIA XRELATIVE ABUNDANCE
50
75
95
96
173
174
175
176
177
15.0 - 40.0% of the base peak
30.0 • 60.0% of the base peak
Base peak. 100% relative abundance
5.0 • 9.0% of the bate peak
Less than 1.0% of the base peak
Greater than 50.0% of the base peak
5.0 - 9.0% of mass 174
Greater than 95.0%. but leu than 101.0% of mats 174
5.0- 9.0% of mass 176
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THJS PERFORMANCE TUNE APPLIES TO THE FOLLOWINGSAMPLES. BLANKS AND STANDARDS.
Value in parenthesis is % mas< 174.Value in parenthesis is % mass 176.
SAMPLE ID LAB ID DATE OF ANALYSIS TIME OF ANALYSIS
01 -
i MM. ii •••»
MASS SPECTRUM01/22/8? 8:36:96 + 4:51SAMPLE: 56NG 4-BFB,1-52-1,1.6ULCOHOS.: DESCBF, 1550U,6'SPIMQ,FIHH82,ETC-TOX1COH,LOW WATER
- #90 - #10635
DATA: BF81228?A #97CALI: BF012287A #3
BASE M/Z: 95RIC: 144896.
r 3564S.
174
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Bate ir./z: 95RIC: 144896.
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BROMOCHLORDMETHANf: ISl1,4-DirLUORGBENZtNE IS?D'J-CHLGROBENZfT.Nhl IS3D4-1, ii-BICHLQROi: THANE SS2DB-TOLUENE SS24-BRQMOFLUOROBENZErNJE SS3CHLOROKETHANE" «* * )BROr-IGMETHANEVINYL CHLORIDE < *^CHLOROETHANtLMETHYLENE CHLORIDEACETONECARBON DISULFIDi-I1,1-DICHLOROETHENC (*)1, 3. OICHLOROETHANF. (**)TRANS-1. 2-L'ICHLGROETHENECHLOROFORM (*)1,2-DICHLOROETHANE2-BUTANONE1,1,1-TRICHLOROETHANECARBON TETRACHLORIDEVINYL ACETATEBR OMODICHLOROMETHANE1, 2-DICHLOROPROPANE (*)TRANS-1,3-DICHLOROPROPENETRICHLOROETHYLENEDIBROMOC HLOROMETHANE1,1,2-TRICHLOROETHANEBENZENECIS-1,3-DICHLOROPROPENE2-CHLOROETHYLVINYL ETHERBROMOFORM <**)4-METHYL-2-PENTANONE2-HEXANONE1122-TETRACLETHANE (*«)TETRACHLOROETHYLENETOLUENE (*)CHLOROBENZENE (**)ETHYLBENZENE <*)STYRENETOTAL XYLENES
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> Amount50.50.5O.47.49.48.18.18.19.19.21.14.2019.19.19.20.17.10.19.21.19.19.19.19.19.18.19.20.IS17.17.19.21.19.19.19.19.19.19.19.
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RIC DATA: US812237I #1 SCAMS 19 TO 60901/22/37 17:30:00 CALI: US812287I #3SAMPLE: 20PPB UOA STD.,3-22-1,5.8ML,IS&SSCONDS.: DESCVP,1550U,6'SP1000,FINN92, ETC-TOXICON,LOW WATERRANGE: G 1, 608 LABEL: N 0.- 4.0 QUAN: A 0, 1.8 J 8 BASE: U 20. 3
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0 j 10 2-3UTANUNL".-'I- C115 1.1, 1--T-:1 C120 CARBON TETRACHL.ORIDE.-:;: C125 VINYL. ACETATE/T: C130 HROMODICHLOROPiKTHANErl<: Ci40 ] , 2-DICHLOROFHOPANr: I*)£':• C145 TRANS-1, 3-DICHLQROPRDPEIvif:.'t C15O TRICHLOROETHYLENEZ:7 C155 DIBROMOCHLOROMETHANE2L- C16O 1, 1, 2-TRJCHLOROETHANE2? C165 BENZENE30 C170 CIS-1,3-DICHLOROPROPENE33 C175 2-CHLOROETHYLV1NYL ETHER3rJ C18O BROMOFORM <**>3>; C205 4-METHYL-2-PENTANCME34 C210 2-HEXANONE3? C225 1122-TETRACLETHANE (**)3i-. C220 TETRACHLOROETHYLENE37 C230 TOLUENE (*)3B C235 CHLOROBENZEN&: (**)39 C240 ETHYLBENZENE (•»)-tO C245 STYRENE•V; C250 TOTAL XYLENES
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Area(Hght) Amount67939.385568.306365.33037.363396.278053.28743.9O04.45886.24513.60726.6087.
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