______
0 0
UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION IX
75 Hawthorne StreetSan Francisco, CA 94105
WASTE MANAGEMENT DIVISIONRCRA ENFORCEMENT OWICE
TSCA COMPLIANCE EVALUATION INSPECTION REPORT
Purpose: TSCA Compliance Evaluation Inspection
Facility: Clean Harbors Los Angeles, LLC5756 Alba StreetLos Angeles, CA 90058
EPA ID Number: CAD 050 806 850
Date of Inspection: August 25, 2011
EPA Representatives: Jennifer DowneyEnforcement Officer(415) [email protected]
Christopher RollinsEnforcement Officer(415)[email protected]
Facifity Representatives: Dave CochranGeneral Manager(323) 277-2521
Joe ChristopherCompliance Manager(310) 835-0775 x 499
Mac HardawayGeneral Manager — Transformer Services(323) 277-2508
Jesus VelaOperations Supervisor
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Edgar MilitarLaboratory Manager
Report Prepared By: Jennifer Downey
Report Date: October 12, 2011
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0
Introduction
On August 25, 2011, U.S. Environmental Protection Agency (“EPA”) representatives conductedan unannounced Toxic Substances Control Act (“TSCA”) Compliance Evaluation Inspection(“CEr’) of Clean Harbors Los Angeles, LLC (“Clean Harbors”), located at 5756 Alba Street, inLos Angeles, California. The purpose of the inspection was to determine Clean Harbors’compliance with the Polychiorinated Biphenyls (“PCBs”) regulations under 40 Code of FederalRegulations (“C.F.R.”) parts 761, and the California Health and Safety Code (“HSC”), Division20, Chapter 6.5; and the California Code of Regulations (“C.C.R.”), Title 22, Division 4.5.
This inspection report summarizes the events that transpired during the inspection, theobservations and findings made by the EPA inspectors, and information received from thefacility subsequent to the inspection.
Facffitv Background
Facility Name Clean Harbors Los Angeles, LLC (“Clean Harbors”)Established EPA originally granted this facility location a TSCAApproval
under the name Oil Process Company in 1991. On February 15,2002, the TSCA PCB Approval for the 5756 Mba Street facilitylocation expired. However, the permit has been administrativelyextended until EPA can complete its review of Clean Harbors’application for permit renewal, which was submitted prior to thepermit expiration date.
Number of Employees 25 EmployeesHours of Operation 6:00 am to 10:30 pm (2 shifts)Filed Notification of This facility location first filed a Notification of PCB WastePCB Waste Activity Form Activity Form on January 24, 1990. Clean Harbors submitted an
additional Notification of PCB Activity Form notifying EPA ofits generator status on July 26, 2007.
Facility Processes Clean Harbors provides environmental and hazardous wastemanagement services in the United States. The facilityspecializes in decontamination, emergency response, disposaland recovery services related to hazardous waste and used oil.This location also stores and consolidates PCBs and PCBEquipment destined for disposal at TSCA regulated facilities.
Waste Streams Used Oil, PCB liquids, PCB Equipment and scrap metal from theprocessing of Non-PCB and PCB equipment.
PCB Facility Status PCB Commercial Storage FacilityLast Inspection EPA Region 9 last conducted a TSCA PCB inspection of the
Clean Harbors facility on July 16, 2009. Violations documentedin the report included failure to properly mark PCBs and PCBitems, failure to include the removal from service dates on PCBcontainers and manifests, and failure to mark all equipment usedfor handling PCBs with the PCB ML label.
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Facility Inspection
On August 25, 2011, EPA representatives arrived at Clean Harbors Los Angeles, Californiafacility at approximately 11:12 am. Two EPA Region 9 inspectors (Ms. Jennifer Downey andMr. Christopher Rollins) were present during the inspection.
During the in-brief, the inspectors presented their credentials. Mr. Rollins then presented andexplained the Notice of Inspection form (Attachment 3a.) and a TSCA Inspection ConfidentialityNotice form (Attachment 3b.) to the Clean Harbors representatives.
Under TSCA, the Notice of Inspection form is required to be signed prior to conducting aninspection and the TSCA Confidentiality Notice form outlines Clean Harbors’ right to claimPCB materials or documents collected during or after the inspection as TSCA ConfidentialBusiness Information (“CBI”). No documents were declared CBI during EPA’s inspection.Both EPA and the facility signed both forms and EPA concluded its in-brief.
EPA inspectors conducted a walk-through of the facility and collected eleven surface wipesamples to evaluate Clean Harbors’ management of PCBs.
The following summarize the areas inspected and the potential violations found near or adjacentto the Truck Loading Dock, Container Storage Warehouse, and On-Site Laboratory.
Area 1: Truck Loading Dock
The inspectors observed sixteen 55-gallon drums containing PCB waste on pallets in the TruckLoading Dock area that were ready to be shipped offsite (see Photo 2). The out of service datewas marked on the top of each drum. In addition, the drums were marked with a PCB ML label,a hazardous waste label (designating the PCB material as a California-only hazardous waste) andan internal tracking label. The hazardous waste labels and internal tracking labels were eachmarked with their own dates, which did not correspond with the out of service date. Theinspectors noted that all of the hazardous waste labels were marked with an accumulation startdate of 8/24/2011 (see Photo 3). According to facility representatives, the hazardous wastelabels had been affixed to the drums the day before when Clean Harbors generated themanifest(s) which will accompany the waste when it is shipped offsite for treatment and disposalat another facility. The inspectors expressed concern that Clean Harbors was not entering the outof service date as the hazardous waste accumulation start date.
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Area 2: Container Stqrage Warehouse
0
Photo 3— Hazardous Waste Label Dated 8/24/2011
Location Waste Type Potential Violation Photo
Warehouse Floor PCB Wipe Sample None N/A
CH0825 1 1SW-1
Entrance PCB Wipe Sample None N/A
CH0825 1 1SW-2
Ramp PCB Wipe Sample None N/A
CH08251 1SW-3
Leaky Transformer PCB Wipe Sample None 4, 5
CH08251 1SW-4
Bay 1 PCB Wipe Sample None N/A
CH08251 1SW-5
Bay 4 PCB Wipe Sample None N/A
CH08251 1SW-6
Bay 2 PCB Wipe Sample None 7
CHO825I1SW-7
Bay 3 PCB Wipe Sample None 8
CH08251 1SW-8
.11kIZARDOUS WASTE‘•‘ “‘
AW Pfl(jpjg UPfOpl 04PQ*L4 Llti 1
• r* •‘
-
Photo 2— Containers in
Page 6 of 10
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The inspectors observed 2 leaking transformers in Clean Harbors’ Container Storage Warehouse.The first transformer, located in Bay 4, had “330 ppm” written on the side of the transformer (seePhotos 4 and 5). EPA collected a PCB wipe sample of the oil on the day of the inspection(Sample CH0825 11 SW-4). However, according to the analytical results, EPA only detectedPCBs at 6.5 g/100 cm2. The action level for PCB wipe samples under TSCA is 10 .tg/l00 cm2.The second leaky transformer was marked as “6 ppm” and was stored in a containment unit inthe non-PCB (<50 ppm) storage area of the warehouse.
The inspectors observed a metal drum (Drum#24612696) in Bay 3 of the Container StorageWarehouse that had “Assume >500” writtenon the drum lid by the generator, but did nothave a PCB ML label affixed (see Photo 6).EPA asked that Clean Harbors provide EPAwith analytical and profile information for thedrum. On October 4, 2011, Clean Harborssent EPA the requested information(Attachment 4), including laboratory resultsshowing no detectable levels of PCBs in thedrum contents.
The inspectors observed 2 big stains on the floor near Clean Harbors’s electrical pump in Bay 2(see Photo 7). EPA collected a PCB wipe sample over one of the stains (Sample CHO82511SW-7). According to the analytical results, EPA only detected PCBs at .06 igIl00 cm2. Theinspectors also observed significant staining and residue in the gutter area of Bay 3 (see Photo 8).EPA collected a PCB wipe sample in the gutter area (Sample CH08251 1SW-8). According tothe analytical results, EPA only detected PCBs at .2 .tgI100 cm2.
Photo 4— Transformer Marked as “330 ppm”
Photo 6— Drum #24612696 Marked “Assume > 500”
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A total of eight surface wipes (CH08251 1SW-1 to CH08251 1SW-8) were collected inside the
Container Storage Warehouse. None of the wipe samples exceeded the threshold for unresthcted
use under TSCA (10 .tg/1O0 cm2).
Area 3: Onsite Laboratory
Location Waste Type Potential Violation Photo
Lab Hood #1 PCB Wipe Sample N/A — Field Blank N/ACH0825 1 1SW-9
Lab Hood #1 PCB Wipe Sample None N/A
CH08251 1SW-10
Lab Hood #2 PCB Wipe Sample None N/A
CH08251 1SW-1 1
The inspectors observed 3 containers in the temporary PCB storage area inside the Laboratory
(see Photos 9 and 10). A white container, partially filled with PCB oil, was not marked with a
PCB ML label as required. The drum also should be labeled as CA-only hazardous waste. Clean
Harbors affixed the appropriate labels prior to the end of the inspection.
- —- -) 7: Wipe Sample Near Pump in Bay 2
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A total of three surface wipes (CH0825 11 SW-9 to CH0825 11 Sw-il) were collected inside theLaboratory. The analytical results of the wipes were non-detect for PCBs.
Record Review
The inspectors requested that Clean Harbors subsequently provide EPA with an inventory ofPCB items on site at the time of the inspection, analytical and profile information for drum24612696, and analytical information and manifest(s) from decontamination of a PCB tankearlier in the year. Clean Harbors provided the requested information on October 4, 2011(Attachment 4).
Photo 9: Laboratory PCB Storage Area
Photo 10: White PCB Container Not Properly Labeled
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Potential Violation of TSCA PCB Requirements
1. Failure to Mark PCBs and PCB Items [40 C.F.R. § 761.40(a)(1)].Requirements:
TSCA requirement 40 C.F.R. § 761.40(a)(1) states each [PCB Containers] in existence onor after July 1, 1978 shall be marked as ifiustrated in Figure 1 in § 76 1.45(a): The markifiustrated in Figure 1 is referred to as ML throughout this subpart.
Findings:During the inspection, EPA observed a container of PCB oil in the laboratory which wasnot properly marked with a PCB ML label as required under TSCA.
Facility Response:Clean Harbors documented its, return to compliance by affixing a PCB ML label to thecontainer prior to the end of the inspection. Clean Harbors also re-trained their TSCA
facility laboratory teams on all waste standards of operation, including waste containerlabeling requirements, subsequent to the inspection.
List of Attachments
1. Inspection Photo Log2. EPA Region 9 Laboratory Analytical Testing Results3. TSCA Inspection Forms
a. Notice of Inspectionb. TSCA Inspection Confidentiality Noticec. Receipt for Samples and Documentsd. Chain of Custody Record
4. Clean Harbors October 4, 2011 Correspondence
Page 10 of 10
oATTACHMENT 1
Photograph Log for EPA’s August 25,2011Clean Harbors Los Angeles TSCA Inspection
All photographs on this log were taken with a Olympus Tough TG-310 digital camera byChristopher Rollins or Jennifer Downey, RCRA Enforcement Office, EPA Region IX. Pleasenote that each photograph number listed below begins with “P82500”.
01. Sign located at the front of the facility
02. Drums in Truck Loading Dock area
03. Close-up of drum in Truck Loading Dock area
04. Hazardous waste label on drum in Truck Loading Dock area (8/24/11 accumulation startdate)
05. Top of drum showing out of service date in Truck Loading Dock area
06. Drums in Truck Loading Dock area
07. Top of drum showing out of service date in Truck Loading Dock area
08. Clean Harbors Supplemental Drum Label on drum in Truck Loading Dock area
09. Hazardous waste container near entrance to Container Storage Warehouse
10. Drums near front of Container Storage Warehouse
11.. Labels on a drum near the front of Container Storage Warehouse
12. Labels on a drum near the front of Container Storage Warehouse
13. Leaking “330 ppm” transformer
14. Liquid and stains below “330 ppm” leaking transformer
15. Liquid and stains below “6 ppm” leaking transformer
16. “6 ppm” leaking transformer
17. Transformers and containers in TSCA area of Container Storage Warehouse
18. Transformers and containers in TSCA area of Container Storage Warehouse
19. Transformers and containers in TSCA area of Container Storage Warehouse
20. Transformers and containers in TSCA area of Container Storage Warehouse
21. Labels and markings on top of TSCA regulated item in Container Storage Warehouse
0 022. Hazardous waste labels on non-TSCA PCB items in Container Storage Warehouse
23. Labels on container of potentially PCB contaminated debris in Container StorageWarehouse
24. Drum in Bay 3 of Container Storage Warehouse
25. Drum #246 12696 in Bay 3 of Container Storage Warehouse
26 Hazardous waste label on drum m Contamer Storage Warehouse
27 PCB label on small contamer m Container Storage Warehouse
28 PCB pump and equipment in Bay 2
29 EPA wipe sample CHO82511SW-1
30 EPAwipe sample CHO82511SW-2
31. EPA wipe sample CHO82511SW-3
32. Clean Harbors wipe sample next to CH08251 1SW-3
33. EPA wipe sample CH08251 1SW-4
34. Clean Harbors wipe sample next to C11082511SW-4
35. EPA wipe sample CJzIO82511SW-5
36. EPA wipe sample CHO82511SW-6
37. EPA wipe sample CH08251 1SW-7
38. PCB hose and staining on floor in Bay 2
39. EPA wipe sample CHO82511SW-8
40. After EPA wipe sample CH08251 1SW-8
41. Drums in Bay 3 of Container Storage Warehouse
42. Step can filled with potentially PCB contaminated gloves in Laboratory
43. Containers in Laboratory temporary PCB storage area
44. Containers in Laboratory temporary PCB storage area
45. EPA wipe sample CF108251 ISW-1O
46. EPA wipe sample CH0825 11 Sw-lI
1
P8250004
P8250028
$fr .r
P8250010
P8250005
P8250007 P8250008 P8250009
P8250011 P8250012 P8250013 P8250014 P8250015
P8250018 P8250019
P8250021
P8250020
P8250022 P8250023 P8250024 P8250025
P8250027
P8250031
P8250029 P8250030
P8250032--
P8250034P8250033 P8250035
2FNAL 09 22 11 1535
United States Environmental Protection Agency—- -
— Region 9-Laboratory---1337 S. 46th Street Building 201
Richmond, CA 94804
912212011
Subject: Analytical Testing Results -Project RIIRO8
- SDG1238-
From: Brenda Bettencourt, DirectoEPA Region 9 LaboratoryMTS-2
To: Jennifer DowneyRCRA Enforcement OfficeWST-3
Attached are the results from the analysis of samples from the Clean Harbors LosAngeles 2011 TSCA inspection project. These data have been reviewed in accordancewith EPA Region 9 Laboratory policy.
A full documentation package for these data, including raw data and sample custodydocumentation, is on file at the EPA Region 9 Laboratory. If you would like to requestadditional review and/or validation of the data, please contact Eugenia McNaughton at theRegion 9 QualIty Assurance Office.
If you have any questions, please ask for Richard Bauer, the Lab ProjectManager at (510)412-2300.
Analyses Included In this report:
Date:
PCB Aroclors by GC/ECD PCB Aroclors by OC/ECO
SDGID 112388
PCB wipe extraction: Wipes were transferred from the sample vial to soxhiet extraction apparatus. The sample vials weresubsequently rinsed with dichloromethane and the rinsate added to the soxhlet. Sample wipes 1108070-01 through -08were soiled with black stains, and wipes -09 through -11 appeared clean. Samples -04. -06, and -08 contained smalldebris particles.
Surrogate solke comciounds: Tetrachlora.m-xylene and decachiorobiphenyl were added toeaclTwipe sample assurrogate standards. Only decachlorobiphenyl was evaluated for QC flagging. Tetrachloro-m-xylene is used as asecondary surrogate and only evaluated when the presence of decachlorobiphenyl is suspected in the sample itself (aswhen aroclor 1268 is present in the sample).
Reporting units: All results are reported in ugIlOO cm2, based on the assumption that a 100 cm2 area was wiped.
Work Order(s)
1108070
,cc0SZ Unittates Environmental Protection Aenc
Region 9 Laboratory1337 S. 46th Street, Building 201, Richmond, CA 94804
‘L PRO0 Phone:(510) 412-2300 Fax:(510) 412-2302
Project Manager: Jennifer Downey RCRA Enforcement Office SDG: I 1238B
Project Numher: RIIRO8 75 Hawthorne Street Reported: 09/22/11 15:35
Project: Clean Harbors Los Angeles 2011 TSCA San Francisco CA, 94105
Inspection
Date Collected Date ReceivedSample ID Laboratory ID Matrix
CHO8251ISW-l 1108070-01 Wipe 08/25/11 13:16 08/26/11 11:00
CHO825IISW-2 1108070-02 Wipe 08/25/11 13:21 08/26/11 11:00
CH08251 I SW-3 1108070-03 Wipe 08/25/1 1 13:24 08/26/11 1 1:00
CHO825IISW-4 1108070-04 Wipe 08/25/11 13:32 08/26/11 11:00
CHO825IISW-5 1108070-05 Wipe 08/25/11 13:40 08/26/11 11:00
CHO825IISW-6 1108070-06 Wipe 08/25/11 13:44 08/26/11 11:00
CHO82SIISW-7 1108070-07 Wipe 08/25/11 13:53 08/26/11 11:00
CH082511SW8 1108070-08 Wipe 08/25/11 14:00 08/26/11 11:00
CH0825 I 1SW9 1108070-09 Wipe 08/25/11 14:38 08/26/li 11:00
CH082511SW10 1108070-10 Wipe 08/25/11 14:44 08/26/lI 11:00
CHO8251ISW-l1 1108070-11 Wipe 08/25/11 14:51 08/26/11 11:00
IIOBQThflNALO922 111535 Page I of7
Surrogate: Tetrachlaro-m.xylene
Surrogate: Decachiarobiphenyl
Lab ID:
Sample ID:
Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Aroclor 1262
Aroclor 1268
Wipe-Sampled: 08/25/11 13:24
Polychiorinated Biphenyla by EPA Method 8082A0.1 ugIl00cm B1H0152 08/30/Il 09/01/Il 8082A1S0P335
0.2 ‘ “ “ “ 8082A1S0P335
0.1 ‘ 8082A/S0P335
0.1 “ ‘ ‘ 8082A)S0P335
0.1 ‘ 8082AJS0P335
0.1 ‘ “ 8082A/S0P335
0.1 “ 8082A/S0P335
0.1 ‘ “ 8082AiSOP335
0.1 “ ‘ “ 8082A1S0P335
ited States Environmental Protectioncncy V
Region 9 Laboratory13375.46th Street, Building 201, Richmond, CA 94804
Phone:(51 0) 412-2300 Fax:(51 0) 412-2302
Project Manager: Jennifer Downey RCRA Enforcement Office SDG: 112388
Project Number: Ri 1R08 75 Hawthorne Street Reported: 09/22/1115:35
Project: Clean Harbors Los Angeles 2011 TSCA San Francisco CA, 94105inspection V
3ample ResuIts
_____ ______ ______
V Reanalysis / Qualifiers / QuantitationAnalyte Extract Result Comments LImit Units Batch Prepared Analyzed Method
Lab ID: 1108070-01 Wipe - Sampled: 08/25/1113:16
Sample ID: CH082511SW4 Polychiorinated Blphenyls by EPA Method 8082AAroclor 1016 ND U 0.1 ug/I00cm B1H0152 08/30/Il 09/01/Il 8082A/S0P335
Aroclor 1221 ND U 0.2 ‘ 8082A1S0P335
Aroclor 1232 ND U 0.1 0 ‘ 8082A1S0P335
Aroclor 1242 ND U 0.1 ‘ 0 0 0 8082A1S0P335
Aroclor 1248V ND U
V
0.1 0 0 8082A1S0P335
Aroclor 1254 ND U 0.1 0 0 8082A)S0P335
Aroclor 1260 ND 3, Q2, U 0.1 ‘ “ 8082A1S0P335
Aroclor 1262 ND U 0.1 ‘ “ ‘ 8082A1S0P335
Aroclor 1268 ND U 0.1 “ “ 8082AJS0P335
V
Surrogate: Tetrachloro-m-xylene 89 % 88.8-128%
Surrogate: Decachlorobiphenyl 80 % 47.4-136%
Lab ID: 1108070-02 Wipe - Sampled: 08/25/11 13:21
Sample ID: C1108251 ISW-2 Polychlorinated Biphenyls by EPA Method 8082AArocior 1016 ND U 0.1 ugiIOOcm2 BlH0152 08/30/li 09/01/11 8082A1S0P335
NLV0,2VVV V ‘_“ “ 8082A1S0P335
Aroclor 1232 ND U 0.1 “ 0“ 8082A1S0P335
Aroclor 1242 ND U 0.1 “ “ 8082A/S0P335
Aroclor 1248 ND U 0.1 “ 0“ 8082A1S0P335
Aroclor 1254 ND U 0.1 “ “ ‘ 8082AJS0P335
Aroclor 1260 ND 1, Q2, U ‘ “ ‘ 8082A1S0P335
Aroclor 1262 ND U ‘ “ ‘ 8082A1S0P335
Aroclor 1268 ND U ‘ ‘ “ “ 8082A/S0P335
1108070-03
C1108251 ISW-3
0.1
0.1
0.1
88.8-128%
4 7.4-136%
9! %
82%
ND U
ND U
ND U
ND U
ND U
ND U
ND J,Q2,U
ND U
ND U
11O7O FINAL 9 22 111535 Page 2 of 7
Lab ID: Wipe - Sampled: 08/25/11 13:32
Sample ID: Polychiorlnated Biphenyls by EPA Method 8082AAroclor 1016 ND U 0.1 ug/IOOcma B1H0152 08/30/Il 09/01/Il 8082AJS0P335
Aroclor 1221 ND U 0.2 ‘ “ 8082A1S0P335
Aroclor 1232 ND U 0.1 “ ‘ “ 8082A1S0P335
Aroclor 1242 ND U 0.1 0 8082AJS0P335
Aroclor 1248 ND U 0.1 “ 8082A1S0P335
Aroclor 1254 ND U 0.1 0 0 8082A1S0P335
Aroclor 1260 0.5 ‘ 09/07/Il 8082A/S0P335
Aroclor 1262 ND U 0.1 0 ‘‘ 09101/11 8082A1S0P335
Aroclor 1268 ND U 0.1 0 8082A1S0P335
Surrogate: Tetrachloro-m-xylene
Surrogate: Decachiorobiphenyl
Lab ID: Wipe - Sampled: 08/2511113:40
Sample ID: Polychlorlnated Biphenyls by EPA Method 8082AAroclor 1016 0.1 ug/loocm’ B1H0152 08/30/Il 09/01/Il 8082A1S0P335
Aroclor 1221 0.2 0 0‘ 8082A1S0P335
Aroclor 1232 0.1 0 0 0 0 8082A1S0P335
Aroclor 1242 0.1 0 0 0 8082A1S0P335
Aroclor 1248 0.10 0 0 0 8082A1S0P335
Aroclór 1254 0.1 0 0 8082A/S0P335
Aroclor 1260 0.1 0 0 0 8082A/S0P335
Aroclor 1262 0.1 0 0 0 0 8082A/S0P335
Aroclor 1268 0.1 0 0 0 8082A1S0P335
WIpe-Sampled: 08/25/11 13:44
Polychlorlnated Blphenyls by EPA Method 8082A0.1 ug/IOOcm2 BIHOI52 08/30/Il 09/01/Il 8082A1S0P335
8082A1S0P335
8082A1S0P335
8082A/S0P335
8082A/S0P335
8082A/S0P335
DS3q7, Unitates Environmental Protection Aeic
9 Laboratory% 1337 S. 46th Street, Building 201, Richmond, CA 94804
LPIO Phone:(510)412-2300 Fax:(510)412-2302
Project Manager: Jennifer Downey RCRA Enforcement Office SDG: I 1238B
Project Number: RI 1R08 75 Hawthorne Street Reported: 09/22/1115:35
Project: Clean Harbors Los Angeles 2011 TSCA San Francisco CA, 94105
Inspection
____
ReanalysIs / QualIfIers I QuantltatlonAnalyte
- Extract Result Comments LImIt UnIts Batch Prepared Analyzed Method
Lab ID: 1108070-03 Wipe - Sampled: 08/25/11 13:24
Sample ID: CHO8Z5I1SW3 Polychlorlnated Blphenyls by EPA Method 8082ASurrogate: Tetrachloro-m-xylene 92 % 88.8-128% BJHOI52 08/30/Il 09/01/11
Surrogate: Decachioroblphenyl 84 % 4 7.4-136% 0
1108070-04
CHOS2SI ISW-4
REl 6.5
1108070-05
CH08251 ISW-5
81 %
75 %
88,8-128%
4 7.4-136%
ND U
ND U
ND U
ND U
ND U
ND U
ND JQ2,U
ND U
ND U
Surrogate: Tetrachloro-m-xylene 89 % 88.8-128%
Surrogate: Decachlorobiphenyl 81 % 4 7.4-136%
Lab ID: 1108070-06
Sample ID: CHO8251ISW-6
Aroclor 1016 ND U
Aroclor 1221 ND U 0.2
Aroclor 1232 0.4 0.1 0
Aroclor 1242 ND U 0.1 0
Aroclor 1248 ND U 0.1
Aroclor 1254 ND U 0.1
I 11L070 FINAL 092211 1535 Page 3 of 7
DS?4 ited States Environmental Protection ency
I Region 9 Laboratory%% J 1337 S. 46th Street, Building 201, Richmond, CA 94804
L PRO’ Phone:(51 0) 412-2300 Fax:(51 0) 412-2302
Project Manager: Jennifer Downey RCRA Enforcement Office SLOG: 112388
Project Number: RI 1R08 75 Hawthorne Street Reported: 09/22/11 15:35
Project: Clean Harbors Los Angeles 2011 TSCA San Francisco CA, 94105
Inspection
r Reanalysis I Qualifiers I Quantitatlon
1AtuuI Extract Result Comments Limit Units Batch Prepared Analyzed Method
Lab ID: 1108070.06 Wipe - Sampled: 08125111 13:44
Sample ID: CH08251 ISW-6 Polychiorinated Biphenyle by EPA Method 8082A
Aroclor 1260 ND 3, Q2, U 0.1 ug/l00cm1 BIHOI52 08/30/I I 09/01/Il 8082A/S0P335
Aroclor 1262 ND U 0.1 “ 8082A/S0P335
Aroclor 1268 ND U 0.1 ‘ 8082A/S0P335
Surrogate: Teirachloro-m-xylene 89 % 88.8-128%
Surrogate: Decachlorobiphenyl 87 % 4 7.4-136%
Lab ID: 1108070-07 Wipe-Sampled: 08/25/11 13:53
Sample ID: CHO825IISW-7 Polychiorinated Biphenyls by EPA Method 8082A
Aroclor 1016 ND U 0.1 ug/IOOcm3 BIHOIS2 08/30/Il 09/02/Il 8082A/S0P335
Aroclor 1221 ND U 0.2 ‘ 8082A/S0P335
Aroclor 1232 ND U 0.1 “ “ 8082A/S0P335
Aroclor 1242 ND U 0.1 ‘ 8082A1S0P335
Aroclor 1248 ND U 0.1 8082A/S0P335
Aroclor 1254 ND U 0.1 ‘ 8082A/50P335
Aroclor 1260 0.06 Cl,J,Q2 0.1 8082A/S0P335
Aroclor (262 - -. ND U 0.1 ‘ 8082A/S0P335
Aroclor 1268 ND U 0.1 ‘ 8082A1S0P335
Surrogate: Tetrachloro-m-xylene 90 % 88.8-128%
Surrogate: Decachlorobiphenyl SI % 47.4-136%
Lab ID: 1108070-08 Wipe-Sampled: 08/25/11 14:00
Sample ID: CHOS25IISW4 Polychiorlnated Biphenyls by EPA Method 8082A
Aroclor 1016 ND U 0.1 ug/1D0cm B1H0152 08/30/Il 09/02/I I 8082A1S0P335
Aroclor 1221 ND U 0.2 ‘ ‘ 8082A/S0P335
Aroclor 1232 ND U 0.1 ‘ ‘ 8082A/S0P335
Aroclor 1242 ND U 0.1 ‘ ‘ ‘ 8082A./50P335
Aroclor 1248 ND U 0.1 ‘ 8082A/S0P335
Aroclor 1254 ND U 0.1 “8082A/S0P335
Aroclor 1260 0.2 J,Q2 0.1 “ 8082AJS0P335
Aroclor 1262 ND U 0.1 ‘ “ 8082A1S0P335
Aroclor 1268 ND Ii 0.1 ‘“ 8082A1S0P335
Surrogate: Teirachloro-m-xylene 95 % 88.8-128%
Surrogate: Decachlorobiphenyl 80 % 47.4-136%
Lab ID: 110807049 Wipe - Sampled: 08/25/11 14:38
Sample ID: CHO82S1ISW-9 Polychiorlnated Blphenyls by EPA Method 8082A
Aroclor 1016 ND U 0.1 ug/lOOcm2 B1H0152 08/30/Il 09/02/Il 8082A1S0P335
Aroclor 1221 ND U 0.2 ‘ ‘ ‘ 8082A1S0P335
Aroclor 1232 ND U 0.1 8082A1S0P335
11ClU7ONALO922115S5 Page4of7
Aroclor 1260
Aroclor 1262
Aroclor 1268
Surrogate: Tetrachlora-m-xylene
Surrogate: Decachiorobiphenyl
Lab ID:
Sample ID:
Aroclor 1016
Aroclor 1221
Aroclor 1232
Aroclor 1242
Aroclor 1248
Aroclor 1254
Aroclor 1260
Aroclor 1262
Aroclor 1268
ND U
ND U
ND U
ND U
ND U
ND U
ND U
ND U
ND U
ND U
ND J,Q2,U
ND U
ND U
Wipe - Sampled: 08125/11 14:44
Polychlorinated Biphenyla by EPA Method 8082A0.1 ug/lOOcma B1H0152 08/30/Il 09/02/I I 8082A/S0P335
0.2 ‘ ‘ 8082A/S0P335
0.1 ‘ ‘ “ 8082A1S0P335
0.1 ‘ ‘ 8082A/S0P335
8082A/S0P335
8082A/S0P335
0.1 “ “ 8082A/S0P335
0.1 8082AJS0P335
8082A1S0P335
Wipe - Sampled: 08/25/11 14:5 1
Polychlorinated Biphënyls by EPA Method 8082A0.1 ug/IOOcm’ BlH0152 08/30/Il 09/02/11 8082A/S0P335
0.2 “ 8082A/S0P335
0.1 ‘ ‘ 8082AJS0P335
0.1 “ “ “ 8082A/S0P335
0,1 ‘ ‘ 8082A/S0P335
0.1 ‘ 8082AJS0P335
0.1 ‘ 8082A1S0P335
0.1 ‘ ‘ 8082A/S0P335
0.1 “ “ 8082A/S0P335
Unit.-étates Environmental Protection Ager
Region 9 Laboratory1337 S. 46th Street, Building 201, Richmond, CA 94804
Phone:(510) 412-2300 Fax:(510) 412-2302
Project Manager: Jennifer Downey RCR.A Enforcement Office SDG: 1 1238BProject Number: RI 1R08 75 Hawthorne Street Reported: 09/22/11 15:35
Project: Clean Harbors Los Angeles 2011 TSCA San Francisco CA, 94105Inspection
--
Reanalysis I QualIfiers I Quantitatlol,Analyte Extct Result Comments Limit Units Batch Prepared Analyzed Method
Lab ID: 1108070-09 Wipe-Sampled: 08125/Il 14:38Sample ID: CHO82SIISW4
PolychlorlnatedBlpltenyls by EPA Method 8082AAroclorI242 ND U 0.1 ug/100cm1 B1H0l52 08/30/Il 09/02/Il 8082A/S0P335Aroclor 1248 ND U 0.1 ‘ “ 8082A1S0P335Aroclor 1254 ND U 0.1 8082A/S0P335Aroclor 1260 ND 3, Q2, U 0.1 ‘ ‘ 8082A1S0P335Aroclor 1262 ND U 0.1 ‘ “ “ 8082A1S0P335Aroclor 1268 ND U 0,1 “ 8082AJS0P335
Surrogate: Tetrachloro-m-xylene 92 % 88.8-128%Surrogate: Decachlorobiphenyl 80 % 4 7.4-136%
Aroclor 1248 ND U 0.1
Aroclor 1254 ND U 0,1
Lab ID:
Sample ID:
Aroclor 1016
Aroclor 1221
1108070-10
CH08251 ISW-IO
Aroclor 1232
Aroclor 1242
ND J,Q2,U
ND U
ND U
91 %
81 %
1108070-11
CH08251 ISW-l I
88.8-128%
47.4-136%
Surrogate: Tetrachloro-m-xylene
Surrogate: Decachiorohiphenyl
90% 88.8-128%
83 % 47.4-136%
1 1(070 fl’IAL 0922 11 55Page 5 of 7
ç€D 0%ited States Environmental Protection AgencyRegion9Laboratory
—J 1337 S. 46th Street, Buflding 201, Richmond, CA 94804Phone:(510) 412-2300 Fax:(510) 412-2302Project Manager: Jennifer Downey
RCRA Enforcement Omce SDG: I 1238BProject Number: RI 1R08
75 Hawthorne Street Reported: 09/22/11 15:35Project: Clean Harbors Los Angeles 201 1 TSCA San Francisco CA, 94105Inspection
-
AnalyteResIt
Batch B1H0152 - Soshlet Extraction - PCBs
Blank (B1HOI5Z-BLKI)Aroclor 1016
Qualifiers / Quantit3on Spike Source %REC RPI) RPDComments Limit Level Result Limits Limit
Prepared: 08/30/11 Analyzed: 09101111Polychlorlnated Biphenyls by EPA Method 8082A - QualIty ControlND U 0.1 ug/lOOc
mAroclor 1221
ND U 0.2Aroclor 1232ND U 0.1Aroclor 1242ND U 0.1Aroclor 1248ND U 0.1Aroclor 1254ND U 0.1Aroclorl26OND J,Q2,U 0.1Aroclor 1262ND U 0.1Aroclor 1268ND U 0.!
Surrogate: Tetrachloro-m.xyiene0.180
“ 0.200 90 88.8-128Surrogate: Decachlorobiphenyl
0.167“ 0.200 84 47.4-136
LCS (BIHOIS2-BSI)Aroclor 1016
0.8920.1 ug/lOOc 1.00 89 88.6-139 200m
Aroclor12600.847
0.1 1.00 85 86.5-139 200Surrogate: Tezrachloro-m-xylene0.175
“ 0.200 88 88.8-128Surrogate: IJecach/orobiphenyl
0.1670.200 84 4 7.4-136
11(8070 FINAL 09 22 111535
Page 6 of 7
0United States Environmental Protection Agen
Region 9 Laboratory
1337 S. 46th Street, Building 201, Richmond, CA 94804 —
Phone:(510) 412-2300 Fax:(510) 412-2302
Project Manager: Jennifer DowneyRCRA Enforcement Office SDG: I 1238B
Project Number: RI 1R0875 Hawthorne Street Reported: 09/22/11 15:35
Project: Clean Harbors Los Angeles 2011 TSCA San Francisco CA, 94105
Inspection
Qualifiers and Comments
Q2 The laboratory control standard associated with this sample did not meet recovery criteria for this analyte (see LCS
results for this batch in QC summary).
3 The reported result for this analyte should be considered an estimated value.
CI The reported concentration for this analyte is below the quantitation limit.
U Not Detected
NR Not Reported
RE 1, RE2, etc: Result is from a sample re-analysis.
4 4
—
p
4
..
;.
p
11 (O 10 rAL )9 22 111535
Page 7 of 7
( ‘pited States Environmental Protection AL )vWashington, D.C. 20460
Toxic Substances Control Act
NOTICE OF INSPECTION
The public reporting burden for this collection of information is estimated to average 5 minutes per response. This estimate includes time
for reviewing Instruct1ns. searching existing data sources, gathering and mairtialning the needed data, and completing and reviewing the
collection of information. Send comments regarding the burden estimate or any other aspect of this collection of information to the Chief,
Information Policy Branch (PM-223), US Environmental Protection Agency, 401 M Street, SW, Washington, DC 20480, and to the Office of
information and Regulatory Affairs, Office of Management and Budget. Washington, 0020503, marked ATrENTION: Desk Officer for EPA
inspec Sign tUr— -
-- Recipient Signepire
——----—--/ C’
Name U J N4ni /.-Q_’_•n(_
-
fill.- / Date lgned lit). Date Signed
-.,v. ---:r ‘‘2S \\ t71 /-A
Form Approved0MB No. 2070-0007Approval Expires 10-31-92
1. investIgation identificatIon 2. TIme 3. Firm Name
372/P;r(,.33 [oauYse.No.
W12 U,-trs Ls
4. Inspector Address . nrm Address
J5k S’zoo’- 75 .57S( ,tb’
4’‘S 5j A 9O)5’
N51-3
REASON FOR INSPECTION
Under the authority of Section 11 of the Toxic Substances Control Act:
‘jj For the purpose of inspecting (Including taking samples, photographs, statements, and other inspection activities) an
establishment, facility, or other premises in which chemical substances or mixtures or articles containing same are manufactured,
processed or stored, or held before or after their distribution in commerce (including records, tiles, papers, processes, controls, and
facilltlâ) and any conveyance being used to transport chemical substances, mixtures, or articles containing same in connection
with their distribution in commerce (including records, files, papers, processes, controls, and facilities) bearing on whether the
requirements of the Act applicable to the chemical substances, mbctures, or articles within or associated with such premises or
‘- conveyance have been complied with.
C] in addition, this inspection extends to (Check appropdate blocks):
L] A. Financial data C] D. Personnel data
C] B. Sales data [] E. Research data
C] C. Pricing data
The nature and extent of inspection of such data specified in A through E above is as follows:
C.rtmc.uonI certify that the statements I have made on this form and all attachments thereto are true accurate, and comDlete, I acknowledge that anyknowinalv false or misleadina statement may k I.hkI. by fin, or imprisonment or boh under annlhjihla law.
EPA 7740-3 Rev (8-91) Regional Office
WASH INcTON, 2UbU
a’TOXIC SUBSTANCES CONTROL ACT ()
T A INSPECTION CONFIDENTIALITY NOTICE
0MB No 2U70-0007Approval expires 10-31-92
1. INVESTIGATION IDENTIFICATION 2. FIRM NAME
DATE INSPECTOR NO. No.
. ‘‘ - _
.‘. L - f.?[)s
3. INSPECTOR NAME 4.IF)RM.DRESSW, •
%i1 ( $ - r.- ‘l
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TO AiERT A CONFIDENTIAL BUSINESS INFöRMAOM CLAIM
It is possible that EPA will receive public requests for release of the, ., 2, Th in? rrnatlDr, is not, end has not been, reasonably obtainable
information obtained during Inspection of the facility above. Such - withoul your company’s consent by other persons (other than
requests will be handled by EPA In accordance with provjsion* Of the governmental bodies) by use of legitimate means (other than
Freedom of Information Act (FOIA), S USC 552 EPA regulationS dIscovery based on sholng’of special need In a judicial or
issued thereunder 40 CFR Pert 2 and the Toxic Substances Control qasudlcsel proceeding)
Act (TSCA) Section 14 EPA is required to make Inspection data
available in response to FOIA request unless the Administrator of te 3, ‘‘ The informatIon ‘15 no; publicly available elsewhere.
Agency determines that the data contain Information entItled to conil- ,.• . .
dential treatment or may be withheld from release under othet excep- , : Disclosure of the InformatIOn would caUse substantial
tions of FOIA harm to your company’s competitive position
Any or all the information collected by EPA durhStr1aêC,Ie31 m At the completion of the InspectIon, you edil be given a receipt for all
be claimed confidential if it relates to trade secret, orcomrsati. documept, sampIes and other materIals collected At that time you
financial matters that you consider to be confIdential bUsines, nfbfr’2 . may make aIaIfnI that sOme’ or all of the Information I. confidential
mation. If you assert a CBI cOim, EPA will disclose the lnformatlQfl ‘ : ,buliies$ Information. .‘ ‘ ‘
only to the extent, and by means of the procedures set forth Imq -. ‘ ‘ ‘ ‘ .
regulations (cited above) governing EPA a treatmeflt of confI*I If you are not authorized by your cseflpany to essert a CBl claim this
business information. Among other things the regulations rqufreiha1 ,notige will be sent by cerlf led mail, along whit the receipt for docu
EPA notify you In advance of publicly discIoIng any lnfotat1lQW meqts samples, end other matrIaJi to tp Chiet Executive Officer of
you have claimed as confidential busineet intORn$l IOUr flrr WIthin 2 days of this date TI*’Phl** SegutIve Officer must
retu?n a stitemsflt specltylrig ary iqfbñflpWQflr Which should receive
A confidential business information (CSI) claim mdi’ be asserted aIas, -. confidential treafrner,t
time You may assert a CBl claim prior to during or after th’ -
mation is collected. The declaration form was developed by the
to assist you In asserting CBI claim. If it Is more coflvenlan* ferØ., , toi
assert a CBI claim ‘on yourown stationery or by marking the lndlylduI
documents or samples “TSA. confidential businesS lnformat)on,’ It Is
not necessary for you to use this-form. The iflipeajar will b g(
answer any questions you may have ragarØIrt)e Apency’S ,CRprocedures. ‘ ‘
- “ ,
While you may claim any collected Information or sample as coñfiden
tial busineSs information, such claims are unlikely to be upheld if they
are challenged unless the iiformation meets the following criteria:
1. Your company has taken measures to protect the confi
dentiality of the Information, and it intends to contiñu8 ‘
to take such measures.
The etUtemqflt trOth the Chief Executiw Officer should be addressed
,•r- .‘ ‘
.4
• ‘. -
and mailed by registered, returni-ecelpt requested mail within 7 calen
dar days of receIpt of this Notice. Claims may be made any time
after the inspection, but ins action data will not be entered into the
speciql security system for TSCA confidentIal business information
until an officIal confidentiality claim is made. The date will b handled
under the agency’s routine security system unless and until a claim Is
made. - .•,
TO BE COMPLETED BY FACILITY OFFICIAL Nr he’Ii onion ibe p isesä.iUWwho is authorized to maki
. -- -
•r,,’ .bdfleat - identielity claims for the a copy of this Notice and other
- ‘ ‘
‘ ‘ I - , erleis will bq sent to the company’s chief executive osticer. If
I have received and reed the notice pony official whe shOtild also receive this Information
SIGNATURE
‘— 4
NAME ‘1TrLE.
- ‘ ‘ ‘‘ ‘, “
:“.‘ •;
..— ‘‘— — — —
TITLE ‘- DATE SIGNED ‘ ADDRESS - ‘ -.
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EPA Form 77404 (12-82) REGIONAL OFFICE
flUS ENVIRONMENTAL PROTECTION AGENCY
WASHINGTON, DC 20460
TOXIC SUBSTANCES CONTROL ACT
RECEIPT FOR SAMPLES AND DOCUMENTS
1. INVESTIGATION IDENTIFICATION 2. COMPANY NAME
DATE I INSPECTION NO. I DAILY SEQ. NO. C \e r- o oc o3 Pr is &LCI25/\\ IF1SV I
3 INSPECTOR ADDRESS uSE, 9 4. COMPANY ADDRESS
‘75 -- 54r€c-k 75(, Poe S4nath
Scir Fr4fc.sco) L Q) CA
For internal EPA use. Copres of this form may be provided to receipient as acknowledgement of the documents and samples of chemical substances and/or
mixtures described below collected in connection with the administration and enforcement of the Toxic Substances Contrdl Act.
RECEIPT OF DOCUMENT(S) AND/OR SAMPLE(S) DESCRIBED IS HEREBY ACKNOWLEDGED:
NO.DESCRIPTION
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DUPICATE OR SPLIT SAMPLES: REQUESTED AND PROVIDED E1 NOT REQUESTED El g€€6* riar Y&
INSPECTOR SIGNATURE CLAIMANT SIGNATURE
NAMENAME
J?YWr 1:k)cdk) (- I&’1L CoC_4PrNTITLE DATE SIGNED TITLE DATE SIGNED
Ev. Sc. r4 5 3)2 / v,ZA f1A4L- 1/
‘REPA
FPA FORM 7740-1 (REVISED JULY 1996) rr’.v,juo v iJr.o OBSOLTh *Js GPO: 1998-444-861/90159 ir.,ijrCOPY
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Clean Harbors5657 Alba StreetLos Angeles, CA 90058
323.277.2500800282.0058www.cleanharbors.com
October 4, 2011
VIA EMAIL (Delivery notification requested)
Mr. Christopher RollinsU.S. EPA, Region IXWST-375 Hawthorne StreetSan Francisco, CA 94105
RE: Clean Harbors Los Angeles, LLC — TSCA Inspection August 25, 2011
Dear Mr. Rollins:
This letter is to update you in regards to the facility inspection conducted at Clean Harbors Los
Angeles, LLC on August 25, 2011. Based upon your observations and inspection fmdings, we
conducted some additional due diligence on the matters you raised during the post-inspection
briefing and would like to share our findings with you, for the record:
1. During the facility inspection, it was observed that Drumil 24612696 had the speculative
statement “Assume >500” written on the drum lid, by the generator. We have contacted
the generator in order to determine the PCB source of contamination as it is our usual
practice to learn as much about the waste characterization and source before we manage
PCB waste at our TSCA- permitted facilities. While we are awaiting confirmation from
the TSCA waste generator, Clean Harbors Los Angeles, LLC decided to sample and
analyze the contents of the 55-gallon drum to determine the chemical concentration of
PCB in this container, utilizing USEPA approved laboratory analytical methods. The
sample was sent to Advanced Technology Laboratories, an independent, NELAP and
California-certified laboratory, for PCB analysis. The results of the analysis indicate
there were no delectable PCBs. A copy of the Advanced Technologies Laboratory report
is enclosed for verification purposes.
2. During the facility inspection, the contents of a laboratory waste accumulation drum was
questioned. Although we believe that the laboratory waste accumulation drum was in
compliance with applicable RCRA and TSCA requirements, we have decided to re-train
our TSCA facility laboratory teams on all Clean Harbors Laboratory Waste Standards of
Operation (SOPs), to include waste container labeling requirements and waste
classification under applicable State and Federal Rules and regulations.
“People and Technology Creating a Better Environment”
0arbor®
3. During the facility inspection, you collected 10 wipe samples from floor areas that werediscolored or stained to determine if these areas were impacted by PCB spills. We alsocollected 2 additional split samples from each area you sampled, and sent one set of oursplit sampled to a California approved and certified laboratory for analysis in accord withthe TSCA requirements. The results of analysis indicates all samples tested below theTSCA surface contamination standard (<10 g/100cm2) with the highest sample resultbeing 2.2 .tgIl 00cm2. A copy of our laboratory report is also enclosed.
During the meeting, you requested four items from us. The site map was provided in themeeting and the remaining items are included in the email. These items include, the inventoryfor Bays 1 thru 6 as of 8/25/Il; profile and analytical for drum 24612696 (profile LASCE-0174);and the decontamination procedures, manifests and analytical for the February 2011 tankcontamination.
In summary, we believe that we have faithfully responded to your concerns. We have alsoprovided additional technical and analytical information, specific your inspection observations,which should assist you as you complete your inspection report.
Please do not hesitate to contact me if you have any further questions concerning thiscorrespondence and especially the analytical data enclosed with this correspondence. I can bereached at (323) 277-2521 or via email at cochrand(icleanharbors.com.
Sincerely,
Dave CochranFacility Manager
oClean Harbors TSCA Cleanup for Non-TSCA Tank
2/17/li — tote with 40 gallons oil of 242 ppm oil was mistakenly pumped into tank V-b.Tank V-b normally has oil <50 ppm.
2/22/11 — after reviewing lab analyticals, it was discovered that TSCA oil had beenpumped into tank V-I 0. The tank, piping, pump and hoses used for pumping the totewere all closed off at this time as they were deemed TSCA contaminated. Even thoughanalytical results showed that the oil in v-rn was 5.7 ppm, the 10,000 gallons in the tankwere considered TSCA because of contact with the oil mentioned above. We began touse a pump with other hoses to continue pumping <50 oil into a separate tank. Thatprocessing could continue. No oil had been removed from tank V-10 between 2/17 and2/22/il.
2/23/li — arrangements were being made to properly dispose of the contaminated oil aswell as decon the tank, piping, pump, and hoses. There was no spill of TSCA oil, sodecon procedures were being applied to those things that had touch ed the oil.
2/24/il — The 10,000 gallons were pumped into 2 isotainers to be shipped via rail toClean Harbors PPM in Coffeyville, KS. 5,800 gallons were put into one isotainer and theother 4,200 gallons were put into. Once tank V-iO was emptied, it was time for thedecontamination process of the tank, pump, hoses, and piping. As per federal regulationsin CFR 761.79, 2000 gallons of a cleaning solvent with <50 ppm PCB was used to deconthe tank and other equipment. Because the tank has a capacity of 20,000 gaLlons, 2000gallons of mineral oil with <50 ppm PCB were used for decontamination. The cleaningsolvent was flushed into the tank through the pump, piping and hoses that were used topump the original 242 ppm PCB oil into tank V-I 0. The cleaning solvent was put in thetank from the top to ensure it cleaned the walls of the tank. This process was done threetimes with this solvent to insure the tank was cleaned. After each cleaning/flushing, asample was taken of the solvent to check the PCB content. The results of the firstcleaning was 4.2 ppm. The solvent after the second cleaning was 4.8 ppm. The thirdcleaning took place after the second result was confirmed. The third sample was takenand then analyzed in the evening by the lab.
2/2 5/1 1 — Upon arrival on the next day, the sample results for the last cleaning was readywith a reading of 5.3 ppm. We reviewed that all the piping, hoses and pump had been partof the tank cieanout for all three flushings and that it was ready to be returned to service.The tank, piping, pump and hoses were all deemed as non-porous. The isotainerscontaining the now TSCA oil wcre shipped to the railcar. At the Clean HarborsCoffeyville facility, the oil will be put through a dechloration process to remove all PCBsfrom the oil. After everything was reviewed to make sure the cleaning process had beendone properly, the tank and equipment were returned to normal service.
•0 o
arbor
__
ENVIRONMENTAL SERVICES, INC. TSCA Tank Rinse Log
A. TankID V-10
B. Tank Capacity 20000 gallons
C. Date Rinsed 2/24/2011
D. Type of Rinsate Used mineral oil <50 ppm PCB
E. Rinsate Volume 2025 gallons
(3 rinses x 0.1 x Tank Capacity)
F. Rinse System GPM 45 gal/minute
G. Minimum Rinse Time Req’d 45 minutes
(Rinse Vol Req’dJ Rinse System GPM)
H. Actual Rinse Time
Start Time 7:15AM
Stop Time 8:00AM
Elapsed Time 45 mm.
I. Rinse Performed By JV (initials)
J. Rinsate Analytical Results
[ample ID: V-b-i Sample ID: Sample ID:
Test Result: 4.2 PP Test Result: ppm Test Result: ppm
K. Tank Interior InspectedReleased By TV (initials)
0
or
__
EN VIRONMENTAL SERVICES, INC. TSCA Tank Rinse Log
A. TankID V-b
B. Tank Capacity 20000 gallons
C. Date Rinsed 2/24/2011
D. Type of Rinsate Used mineral oil <50 ppm PCB
E. Rinsate Volume 2025 gallons(3 rinses x 0.1 x Tank Capacity)
F. Rinse System GPM 45 gal/minute
G. Minimum Rinse Time Req’d 45 minutes(Rinse Vol Req’dJ Rinse System GPM)
H. Actual Rinse Time
Start Time 10:10AM
Stop Time 10:55AM
Elapsed Time 45 mm.
I. Rinse Performed By JV (initials)
J. Rinsate Analytical Results
Sample ID: V-10-2 Sample ID: Sample ID:
Test Result: 4.8 ppm Test Result: ppm Test Result: ppm
K. Tank Interior InspectedReleased By JV (initials)
flarbor
__
ENV:ROHMENTAI. SffiVtCES INC. TSCA. Tank Rinse Log
A. Tank ID V-b
B. Tank Capacity 20000 gallons
C. Date Rinsed 2/24/2011
D. Type of Rinsate Used mineral oil <50 ppm PCB
E. Rinsate Volume 2025 galLons
(3 rinses x 0.1 x Tank Capacity)
F. Rinse System GPM 45 gal/minute
G. Minimum Rinse Time Req’d 45 minutes
(Rinse Vol Req ‘ dJ Rinse System GPM)
H. Actual Rinse Time
Start Time 1:20PM
Stop Time 2:05PM
Elapsed Time 45 mm.
I. Rinse Performed By JV
J. Rinsate Analytical Results
Sample ID: V-10-3 Sample ID: Sample ID:
Test Result: ppm Test Result: ppm Test Result: ppm
K. Tank Interior InspectedReleased By TV (initials)
0
CLEAN HARBORS LOS ANGELESg LLC TSCADECONTAMINATION OF TANK V-1O
What Happened
A tote containing 40 gallons of oil that contained 242 ppm PCBwas pumped by personnel into tank V-10 on 2/17/11. This tanknormally contains oil <50 ppm PCB. This occurred due toemployee error.The problem was identified on 2/22/11 when the supervisorbrought it to management’s attention. At this time the facilityceased pumping into tank V-i 0 and closed it down by shuttingdown the valves. The pump, piping and hose used to pump theTSCA oil were shut down as well. From the time of the incident on2/17/11 until the problem was discovered and the tank shut downon 2/22/11, only oil <50 ppm had been added to tank V-W.Nothing was removed from the tank during this same time period.At the time the tank was shut down, there was 8,100 gallons of oilinside. Due to the TSCA contact rule, all 8,100 gallons wereconsidered TSCA regulated.The EPA and California DTSC were notified on 2/22/11 of theincident.
Decontamination
The 8,100 gallons of contaminated oil were pumped through thesame pump and piping and hose into portable railcar containers forproper offsite disposal.It was determined that the tank decontamination must take placeaccording to 40 CFR 761.79 (c)( 1) as the tank is a PCB container.Tank V-i 0 needed to be rinsed three times with a predeterminedsolvent. Mineral oil < 50 ppm PCB was to be used.
9 0
The items that needed decontamination here were the tank, the
pump, and the piping. The hose was deemed to be made of porous
material. We delegated the hose to be PCB and put it with other
PCB equipment.Approximately 2,025 gallons were used to decontaminate the tank.
This satisfies the requirement that the volume of the rinsate solvent
must be at least 10% of the volume of the container. The solvent
was pumped from another tank through the contaminated piping
and the contaminated pump. The solvent was put into the tank V
10 to rinse the walls. After the rinsing, a sample of the rinsate
solvent was obtained to determine the current PCB level of the
solvent. The PCB content of the solvent after the first rinse was 4.2
PPM. The solvent was removed from the tank. The tank was rinsed
likewise a second time. Again, a sample was taken for analysis.
The PPM level showed to be 4.8 ppmPCB for this solvent. This
was done again a third time with the solvent. The result was 5.3
ppm for the third rinsing.The tank, the piping, and the pump were considered decontaminate
at this time.The rinsate solvent was added to the railcar containers to bedisposed of. Additional oil <50 ppm PCB was added to the lastrailcar container to make sure it was full.
Disposal
The material was put in these portable containers for rail. Theywere shipped to a railcar from the Clean Harbors Los Angelesfacility and loaded on the railcar. The railcar was then shipped tothe Clean Harbors PPM facility in Coffeyville, KS for disposal.
5696A
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RE
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August 29, 2011
Edgar MilitarV ELAP No.: 1838
Clean Harbors Environmental Services, inc. NELAP No.: 021 07CA
5756 Alba St. CSDLAC No.: 10196
Los Angeles, CA 90058-1946 ORELAP No.: CA300003
TEL: (323) 277-2501
FAX: (323) 277-2523 WorkorderNo.: 119573
RE:
Attention: Edgar MilitarV
Enclosed are the results for sample(s) received on August 26, 2011 by Advanced TechnologyLaboratories . The sample(s) are tested for the parameters as indicated in the enclosed chain ofcustody in accordance with the applicable laboratory certifications.
Thank you for the opportunity to service the needs of your company.
Please feel fiee to call me at (562W89-4045 if I can he of further assistance lO your company.
Sincerely,
Eddie F. ,ddguez
Laborat’ory Director
The cover lefler and the case narradve are an integra’ part of this analytical report and cannot be reproduced in part orin its entirety without written permission from the client and Advanced Technology Laboratories.
V Advwtcrd Technology 1 o 5- ——--—
3275 Walnut A’enue Sgno1 Hill, CA 90755 Tel: 562 989-4045 Fax: 562 989-4040
0Advanced TechnoIov Laboratories — Date: 29-Aug-il
CLIENT: Clean Harbors Environmental Services, Inc.
Project: CASE NARRATIVELab Order: 119573
Analytical Comments for EPA 8082
Sample 1] 9573-OO1A, surrogate recovery biased low possibly due to matrix interferences.
Id Page 1 of 4
:2.c lfr(rlUUl JJj? t::’i W1755 Tel: 562. 989.1945 1u.x: 562.989.404t’j
2of5
o 0ANALYTICAL RESULTS
Advanced Technology Laboratories Print Date: 29-Aug-Il
CLIENT: Clean Harbors Environmental Services, Inc. Client Sample ID: 24612696
Lab Order: 119573Collection Date: 8/26/2011 10:45:00 AM
Project:Matrii: SOLID
LabID: I19573-OQIA
Analyses Result PQL Qual Units OF Date Analyzed
PCBS BY GC/ECDEPA 355DB EPA 8082
RuniD: GC4_l 10827A DC Batch: 75167 PrepDate: 8/27/2011 Analyst: HL
Aroclor 1016 ND 50 pg/Kg 1 8/27/2011 07:45 PM
Aroclor 1221 ND 99 pg/Kg 1 8/27/2011 07:45 PM
Aroclor 1232 ND 50 pg/Kg 1 8/27/2011 07:45 PM
Aroclorl242 ND 50 pg/Kg 1 8/2712011 07:45 PM
Aroclor 1248 ND 50 pg/Kg 1 8/27/2011 07:45 PM
Arodor 1254 ND 50 pg/Kg 1 8/27/201/ 07:45 PM
Aroc/or 1260 ND 50 pg/Kg 1 8/2712011 07:45 PM
Aroclsr 1262 ND 50 pg/Kg 1 8/27/2011 0745 PM
Aroclor 1268 ND 50 pg/Kg 1 8/27/2011 07:45 PM
Surr: Decachlorobiphenyl 13.6 39-122 5 %REC 1 8/27/2011 07:45 PM
Suer: Telrachloro-m-xylene 67.6 - 45-111 %REC 1 8/27/2011 0745 PM
Qualifiers: Analyte detected in the associated Method Blank B Value above quantilotion range
It Ho/ding times for preporatiun or analysis exceeded Nt) Not Detected at the Reporting Limit
S Spike/Surrogate outside of I/torts duo to matrix interference Results are wet unless otherwise spent//mi
DO Surrogate Diluted Out
.td,tnceri irrchnoTh”,
LaIxnl/toriLw3275 1i’rh:ni tvvtnet, &:I il/il ct i’,’55 ll: 562. ‘MP.It.VS rccs-: 56...9894(14u1
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2230
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ighL
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ND
16
Ara
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ND
16
Aro
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1232
ND
/6
Aro
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1242
ND
16
Aro
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1248
ND
16
Aro
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1254
ND
16
Aro
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1260
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16
Ars
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1262
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16
Aro
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1268
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16
Suer
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17.9
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4511
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Run
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Clie
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atch
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7516
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Ana
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1Se
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2230
421
Ana
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SPK
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Hig
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147.
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6.7
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1616
6.7
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119
Surr
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Surr
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15.7
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ID:
1195
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8082
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/Kg
Pre
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ate:
8127
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1R
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atch
ID:
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Ana
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8/27
/201
1S
eqN
o:22
3042
2
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Res
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SP
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SP
KR
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aI%
RE
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Hig
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PDR
efV
at%
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Lim
ItD
ual
Qua
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ers:
Aro
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1016
159.
630
1616
6.7
095
.849
115
Aro
clor
1260
172.
620
1616
6.7
010
445
133
Suer
:D
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heny
l15
.906
10.6
795
.439
122
BA
naly
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epar
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Not
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the
Rep
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Spik
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outs
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Order:
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Project:
TestC
ode:
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Sam
pleID
:119581001A
MS
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pType:
MS
TestC
ode:8082_S
Units:
pg/Kg
PrepD
ate:8/2712011
RunN
o:136130
Client
ID:
ZZ
ZZ
ZZ
Batch
ID:
75167T
eatNo:
EPA
8082E
PA3550B
Analysis
Date:
8/27/2011S
eqNo:
2230422
Arialyte
Result
PQL
SPKvattie
SP
KR
eIVaI
%R
EC
Low
Um
itH
ighUm
itR
PD
RefV
aI%
RPD
RPD
Lim1I
Quat
Surr;T
elrachluro-m-xytene
16.47616.67
98.845
111
Sam
pletD
:119981-O
OIA
MSD
Sam
pType:
MSI3
TestC
ode:8082_S
Units:
pg/Kg
Prep
Dale:
8/27/2011R
uriNo:
135130
Client
ID:
ZZ
ZZ
ZZ
Batch
ID:
75167T
estNo:
EP
A8082
EPA
358/lBA
nalysisD
ate:8127I2011
SeqNo:
2230423
Anatyte
Result
PaL
SP
kvaltte
SP
KR
eIVaI
%R
EC
Lew
Um
itH
ighLim
ilR
PD
ReIV
aI%
RPD
RPD
Lim
itQ
ual
Aroclor
1016159.614
16166.7
095.8
48115
159.60.0100
20
Aroclor
1260172.206
16166.7
0103
48133
172.60.238
20
Sure:D
ecachlorabiphenyt15.995
16.6795.9
39122
020
Sure:T
etrachlaro-m-uylene
16,74416.67
10049
III0
0
QualifrereB
Aealyte
detectedin
theassociated
Method
Blank
EV
alueabove
quantilatranrange
HH
oldingtim
esfar
prepaeatloeor
unalrsisexceeded
Nt)
Not
Detected
at theR
eportingL
imit
RR
PDoutside
acceptedrecovery
limits
SSpikelSurrogate
outside0f
limits
dueto
matrix
interfereece
DO
SurrogateD
ilutedO
utC
alculationsare
basedon
rawvalues
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fleanHarij’MSTE MATERIAL PROFILE SHEO--‘-w-- lean Harbors_Profile No. lasce-O 174
_______________
A. GENERAL INFORMATIONGENERATOR EPA ID #IREGISTRATION S CA0006908BIB GENERATOR NAME: Southern California Edison
GENERATOR CODE (Assigned by Clean Harbors) 1NV0267,4 CITY Monrovia STATE/PROVINCE CA ZIP/POSTAL CODE 91016ADDRESS 1218 South Fifth Ave Waste and Water Division 2n
PHONE: (626) 3024187CUSTOMER CODE (Acognad by Clean Harbors) SOUIGO9 CUSTOMER NAME: Southern California Edison CompanyADDRESS PG Box 800 CITY Rosemead STATE/PROVINCE CA ZIP/POSTAL COOS 91770
B. WASTE DESCRIPTIONWASTE DESCRIPTION: Debits/Soil, Unknown PCB level. Assumed >SOOppmPROCESS GENERATING WASTE: Spill Cleanup
IS THIS WASTE CONTAINED IN SMALL PACKAGING CONTAINED WITHIN A LARGER SHIPPING CONTAINER? No
C. PHYSICAL PROPERTIES Id 25C or TiE)
PHYSICAL STATE NUMBER OF PHASES/LAYERS VISCOSITY (It liquId preserrl) COLORSOLID WITHOUT FREE LIQUID 1 2 3 TOP 0.00 1 . 100 (e.g. Waler)POWDER
MIDDLE 0,00 101- 500 (e.g. Molar 0/)MONOLITHIC SOLID % BY VOLUME (Appfox.(UQUID WITH NO SOLIDS BOTTOM 0.00 501 - 10.000 (eg. Molasses)LIQUID/SOLID MIXTURE
0 10,000% FREE LIQUID ODOR% SETTLED SOLID
e NONE BOILING POINT ‘F (‘C) MELTING POINT’F (‘C) I TOTAL ORGANIC% TOTAL SUSPENDED SOLID— CARBON0095 (e35(SLUDGE MILD
n 140 (=60) I = 1%95- 100 (35-38)GAS/AEROSOL STRONG140.200(00-93) I 1-9%101-129)38-54)
._.DescrIbe:.‘ = 200 (93) I 0 10%.
0= 130 )v54)I
FLASH POINT ‘F (‘C) pH SPECIFIC GRAVITY ASH BTUILB )MJ/kg)n 731=23) n 2 0 0.8 (e.g. Gasoline) 02,000(01.6)
‘i 001 =2073- 190 (23-38) 2.1- 6.9 0.81.O (e.g. Ethanol) s’ 2.000-5,000 (4.6-11.6)0.1- 1.0 Ueknown —
101 -140 (38-60) 7 (Non/ret) 1.0 (e.g. Waler) 5,000-10,000111 6-232)II. 5.0141 -200 (50-93) 7.1— 12.4 1.0-12 (e.g. Antifreeze) = 10.000)’23.2I5.1 -20.00 200 (=83) 0= 12.5 “, n 1.2 (e.g. Methylena Chlonde) Actual:
I). COMPOSITION (List the complete compositIon Dl the waste. Include any Inert uomponenTe and/ar debris. Ranges (or Individual components are actreptable. If a trade nasa isused, please supply an MOOS Please do not use abbreviations.)
CHEMICAL MIN MAX UOMASPHALT 0.0000000 — 100.0000000 %CABLE, MASONRY - - - 0.0000000 — 100.0000000 %CARDBOARD
. 0.0000000 — 100.0000000 %CERAMIC 0.0000000 — 100.0000000 %CITRUS BASED SOLVENTS - - 0.0000000 — 20.0000000 %DEBRIS 0.0000000 — 100.0000000 %DIESEL 0.0000000 — 5.0000000 %DRANIED EQUIPMENT LAST CONT. PCB 0.0000000 — 100.0000000 %GLASS 0.0000000 — 100.0000000 %METAL PARTS, PIPES 0.0000000 — 100.0000000 %
DOES THIS WASTE CONTAIN ANY HEAVY GAUGE METAL DEBRIS DR OTHER LARGE OBJECTS (EX - METAL PLATE OR PIPING =1/4’ THICK OR ‘12 YES NOLONG. METAL REINFORCED HOSE =12 LONG. METAL WIRE 012 LONG, METAL VALVES, PIPE FITTINGS. CONCRETE REINFORCING BAR ORPIECES OF CONCRETE u3V
It yes, describe, includIng drmenoionm
DOES THIS WASTE CONTAIN ANY METALS IN POWDERED OR OTHER FiNELY DIViDED FORM’ YES ,s’ NODOES THIS WASTE CONTAIN OR HAS IT CONTACTED ANY OF THE FOLLOWING: ANIMAL WASTES. HUMAN BLOOD. BLOOD PRODUCTS. BODY YES s’ NOFLUIDS, MICROBIOLOGICAL WASTE. PATHOLOGICAL WASTE, HUMAN OR ANIMAL DERIVED SERUMS OR PROTEINS OR ANY OTHERPOTENTIALLY INFECTIOUS MATERIAL?
I acknowledge that this waste material in nerther infectious sea does II contain any eaganlem known To Sea threat Ira human haellTr This crelilicehon isbased ott try knowledge a/the reeler/al. Soled I/re answer below Oral apples
The waste wan never enpnued To potenleliy electrons material.YES NO
Chemical disintedion or some other form eT olenhizahon has been applied To lire waste. YES NOI ACKNOWLEDGE THAT THIS PROFILE MEETS THE CLEAN HARBORS BATTERY PACKAGING REQUIREMENTS. YES NOI ACKNOWLEDGE THAT MY FRIABLE ASSESTOS WASTE IS DOUBLE BAGGED AND WETTED YES NOSPECIFY THE SOURCE CODE ASSOCIATED WITH THE WASTE. G15 SPECIFY THE FORM CODE ASSOCIATED WITH THE WASTE. W002
Repeal Prlntvd On-Thursday. August29 2011 lWINWEBlProt9ehWaste PraEte.rdl Page 1 014
NOCs
C!!a!r.$kL niors Profile No. lasce-0174 1DE. CONSTITUENTS
Are these vaNes bened on testing or knowledge? : Knsndedge Testing
It based on kttoteledge. please desmUe In detat. the rationale applied tn identity and charaderlze the waste matetial. Pleesa Include referenca Is Matenal Safety Data Sheets (MSOS)
when applicable. inclade the chemical or trade-came represented by the MSOS, and or deleted paocess Ce operatIng pemcedrjres which generate the waste.
[pee eentaeleetsd heart. 1.1>500 ppm peelH
Please indicate which constituents below apply. Concentrations must be entered when applicable to assist In accurate review and expedited approvat
of your waste profile. Please note thet the total regulated metals and other constituents sections require answers.
RCRA REGULATED METALS REGULATORY TCLP TOTAl. UDM NOT APPLICABLE
LEVEL (mall) mglt
0504 ARSENIC 0.5
Dcc EARILIM - -100.0
0050 CADMIUM 1.0
0007 CHROMIUM 5.0
DSO - LE 5.0ret
DOSS MERCURY 0.2 -
OStO SELENIUM 1.0
0511 SILVER 5.21
VOLATILE COMPOUNDS OTHER CONSTITUENTS MAX UOM NOT
0510 eENZENE 0.5APPLICABLE
0010 CARSON TETRACHLORIOE 0.5 BROMINE
D02t CNLOR005NZENE 100.0 CHLORINE .0
DS22 CHLOROFORM e.S FLUORINE‘5,
D020 1,2-DICHLOROETHANE 0.5 IODINE‘.0
D029 11-DICHLORDETHYLENE 0.7 SULFUR5,’ -
0035 MSTNYL ETNYL I4STDNE 200 S POTASStUMit - - - -
0030 TETRACHLOROEThYLENE 07 SODIUMit
0040 TRICHLDRDETHYLENE 0.5 AMMONIAit.
D043 VINYL CHLORIDE 0.2 CYAtdIOE AMENABLE ‘v’ - -
SEMI-VOLATILE CDMPOUNDSCYANIDE REACTIVE - -
—
5,
D523 o-CRESOL 200.0 CYANIDE TDTAL
D024 m-CRESOL 200.0 SULFIDE REACTIVE 5,,
0025 p-CRESDL 200.0 Pce.
DO2E CRESOL (TOTAL) 2000
0027 I4DICHLOR000NZENE 7.5‘ NONE NONE
0030 2,4.DGdITROTOLUEPIE 0i3CI000PPM n5OPPM
0032 HCHLOROFE 013OP ‘ v=SOPPM
D033 NEXACNLDRDBUTADIENE 05 WASTE REGULATO BY TSCA 40
0034 HEXACNLOROEFNANE 3.0CFR 701?
DO3E NITRDEENZENE — 3M . YES NO
0037 PENTACNLOROPHENOL 100.0
D038 PYRIDINE 5.0 -
D041 24,5-TRICHLOROPNENOL 400.0
D0d2 2,4,S-TRICHLOROPHENDL 2.0
PESTICIDES AND HERBICIDES
0012 ENDRIN 0.02
0013 UNDANS 04 -
D014 METHOXYCHLOR 10.0
0010 TOXAPHENE 0.5
0015 2.4-0 10.0
D017 2.4,5-TP)SILVSX) 1,0
0020 CHLORDAO4E 0.03
D031 NSPTACHLOR (AND ITS EPOXIDS) 0.000
ADDtTIONAL HAZARDSDOES THIS WASTE NAVE ANY UNDISCLOSED HAZARDS OR PRIOR INCIDENTS ASSOCIATED wtm IT. WHICH COULD AFFECT THE WAY IT SHOULD ES HANDLED?
YES :f NO (Ityes, captain)
CHOOSE ALL THAT APPLY
OSA REGULATEO SUBSTANCE EXPLOSIVE FUMING “ OSHA RSGULATEO CARCINOGENS
POLYMERtZABLE RAOIOACTIVE REACTIVE MATERIAL NONE OF THE ABOVE
Report Printed On: Thursday, Aegasl 20.2011Pege 2 of 4IWINWESIPreOIs\Weste PrsFde,nS
ricanHarbor Clean Harbors Profile No. lasce-0174
NO IS THIS WASTE PROHIBITED FROM LAND DISPOSAL WITHOUT FURTHER TREATMENT PER 40 CFR PART 268?
LOR CATEGORY: Not subject to LOftVARIANCE INFO:
YES ‘‘ NO ISTHISAUNIVERSALWASIE?
YES NO IS THE GENERATOR OF THE WASTE CLASSIFiED AS CONDITIONALLY EXEMPT SMALL QUANTiTY GENERATOR (CESQG)?
YES NO IS This MATERIAL GOING TO BE MANAGED AS A RCRA EXEMPT COMMERCIAL PRODUCT. WHICH IS FUEL (40 CFR 261.2 (CX2XII))?
YES ‘ NO DOES TREATMENT OF THIS WASTE GENERATE A FOOd OR PSi B SLUDGE?
YES NO IS THIS WASTE STREAM SUBJECT TO THE INORGANIC METAL BEARING WASTE PROHIBITION FOUND AT 40 CFR 268.3(C)?
YES ‘e NO DOES TI-RS WASTE CONTAIN VOC’S IN CONCENTRATIONS acr5Q PPM?
YES NO DOES THE WASTE CONTAIN GREATER THAN 20% OF ORGANIC CONSTITUENTS WITH A VAPOR PRESSURE cm .3KPA (.044 PSIA)?
YES T NO DOES THIS WASTE CONTAIN AN ORGANIC CONSTITUENT WHICH IN ITS PURE FORM HAS A VAPOR PRESSUREc 77 KPA (11 .2 PSIA)?
YES NO IS THIS CERCLA REGULATED (SUPERFUND ) WASTE?
YES ‘ NO IS THE WASTE SUBJECT TO ONE OF THE FOLLOWING NESHAP RULES?
Hazardous Orgasire NESHAP (HON) oslo (subpart 0) Pharmacosticels production (subpart GOD)
YES NO IF THIS IS A US EPA HAZARDOUS WASTE. DOES THIS WASTE STREAM CONTAIN BENZENE?
YES NO Doss the waste stream corns horn a facility wily one of the SIC codes listed Under benzene NESHAP or Is this waste regulated under the berlzeneNESHAP sates because the orIgInal source of tho waste shorn a eberolcal monnafactesring, wke by-product rsra,neay. or petroleum rethnecy prreccos7
YES NO Is the gereefstln source of the waste stream a taNdy arty Total Annual Beozene (TAB) trio Mg!year?
What 5 the TAB quantity too your tacdlty? I I Megagram(year (1 Mg = 2,200 Ibo)
The basis for this determination is: Knowledge of the Waste Or Test Data KnowledBe Testing
Describe tine knowledge: - “10. DOTITDG iNFORMATION
DOTITOG PROPER SHIPPING NAME:
UN3432, POLYCHLORINATED BIPHENYLS, SOLID, 9, PG (II
H. TRANSPORTATION REQUIREMENTSESTIMATED SHIPMENT FREQUENCY ONETIME WEEKLY MONTHLY QUARTERLY YEARLY OTHER
CONTAINERIZED BULK LIQUID BULK SOUD1.15 CONTAINERSISHIPMENT
STORAGE CAPACITYGALLONSISHIPMENT: 0Mb, -O Max GAL. SHIPMENT UOM: TON YARD
CONTAINER TYPE: TONSfYARDS/SHIPMENT: 0 Mm - 0 MaxCUBiC YARD BOX s.’ PALLET
TOTE TANK DRUMOTHER.
DRUM SIZE -
I. SPECIAL REQUESTc000MENTS OR 000UESTS
GENERATOR’S CERSFICAI105I reilly that I am anthorlast tin eercule thu doocnent as an outllotlrod agent. thereby mIsty Octal Intoinnation eubeniord In this art attached doosments Is canectto the best at my knowledge. I atlascodIfy that any samples subtnttled are ropresenlatlvs Ut the actual waste. It Clean Harbors dIscovers e doorspenoy dunn0 Ike appmcel pmcne, Generator grants Clean Harbors the authority to amendthe pmfle, as Clear darters deems necessary. ID teneca lye discrepancy.
AUTHORIZED SIGNATURE
____________________
ThIS waste pmgle has beer submlond using Clear Harbors ele000ntu elonetare system.
40 cyn Sec 204.12 required notice:Au reqvhnd by Fedeeh Resource Coese’aatre.r erd neawaray tart regrilatione laced br4tl CFR Pact 204.12101 met ad rqctvslret State hazardous weste tnasdeawns. sakes Is hereby presIded that dl ClaacHflrtOve tanirltes Oar cray to Used IC treat slam. .rd toe dIspose at fire hazesdous resale duscrtbnd en this walE petite have the ep000peiale prenrits and the capacity to macsee Ores. waste..
Places note this par.rua must be eubnrdled for ro evehauao It these Ire, borer a strange In era aaua goolcealleg pruersa or wires Store hens bOon slreigeo th lire dnwnactr nornposeren 0 phytcd drarautorotco Ofthe Inatecat.
NAME (PRINT) TITLE DATE
F. REGULATORY STATUS
YES ‘p’, NO USEPA HAZARDOUS WASTE?
YES NO DO ANY STATE WASTE CODES APPLY?
1261TUbas Waste Code [0u1s0021
YES ‘ NO DO ANY CANADIAN PROVINCIAL WASTE CODES APPLY?
YES
-i
Report Pnrnted On : Thursday, August25 2011 NIIINWEB)ProIEe\Weate Prattle nil Page 3 of 4
jgnIiar&Sj EiDarbors Profile No. lasce-0174 C)Addendum
0. COMPOSITION
CHEMICAL
MEl — MAX UOM
PAPER
0.00000 — 100.000 %
00 0000
PCBS
0.05000 — 100.000 %
00 0000
PIPE
0.00000 — 100.000 %
00 0000
PLASTIC.
0.00000 — 100.000 V.
00 0000
SOIL0.00000 — 100.000 %00 0000
W0000.00000 — 100.000 %00 0000
Report Printed On Thursday, August 25.2011 AuIIdwEOIPmme\wasra PsoIIIesdI Page 4 of 4
0 0.
Advanced Technoloay Laboratories Date: 29-Aug-il
CLIENT: Clean Harbors Environmental Services, Inc.
Project: CASE NARRATIVELab Order: 119573
Analytical Comments for EPA 8082
Sample II 9573-OOIA, surrogate recovery biased low possibly due to matrix interferences.
Page 1 of 4tdt’a,wcd icvi’imfogi
3275 H’,,’nur 4 n-flue. Signal 1111!. CA 90755 ‘Tel: 562. 989.4045 Fax: .S62.989 4040
2 of 5
ANALYTICAL RESULTSPrint Date: 29-Aug-li
PrepDate: 8/27/2011 Analyst: HL
1 8/27/2011 07:45 PM
1 8/27/2011 07:45 PM
1 8/2712011 07:45 PM
1 8/27/2011 07:45 PM
1 8/27/2011 07:45 PM
1 8/27/2011 07:46 PM
1 8/27/2011 07:45 PM
1 8127/2011 07:45 PM
1 8/2712011 07:45 PM
1 8/2712011 07:45 PM
1 8/27/2011 07:45 PM
5275 Walnut ‘henna, Signal Hill. C4 9//755 Tel: 562. 989.4045 Fax: 562.9ç9.41140
0
Advanced Technology Laboratories
0
CLIENT: Clean Harbors Environmental Services, Inc. Client Samp)e ID: 24612696
Lab Order: 119573Collection Date: 8/26/2011 10:45:00 AM
Project:,
Matrix: SOLID
Lab ID: 1I9573-OOIA
Analyses Result PQL Qual Units DF Date Analyzed
PCBS BY GC1ECI2
RufliD: GC4110827A
EPA 35506 EPA 8082
QC Batch: 75167
Aroctor 1016 ND 50 hg/Kg
Aroctor 1221 ND 99 pg/Kg
Aroclor 1232 ND 50 pg/Kg
Aroclor 1242 ND 50 pglKg
Aroclor 1248 ND 50 pg/Kg
Aroctor 1254 ND 50 pg/Kg
Aroclor 1260 ND 50 pg/Kg
Nec/or 1262 ND 50 pg/Kg
Aroclor 1268 ND 50 pg/Kg
Surr: Decachlorobiphenyl 13.6 39-122 S %REC
Surr Tetrachloro-m-xytene 67.6 45-111 %REC
Qualifiers: B Analyte detected in the associated Method Blank
It Holding times for preparation or analysis exceeded
S Spike/Surrogate outside of limits due to matrix interference
DO Surrogate Diluted Out
.tdvinwcdrerhnolagj
E Va/se above quantitation range
NI) Not Detected at the Reporting Limit
Results are wet unless otherwise specified
3 of 5
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W-4
546
546
CM#6
8606
66dw
ptra
n-0’
POLO
12PP
M;
See
dram
2439
4009
2475
3079
0807
2323
‘DW
-412
0012
00CM
#669
8889
dmpt
rae-
0’PO
LE8P
PM; S
eedr
um24
3940
0924
7530
8008
0723
23‘D
W4
679
679
CM#6
8685
86dm
ptra
n-0’
POLE
16PP
M;S
eedr
am24
3940
0624
7530
8108
0723
23‘D
W-4
405
405
CM68
8068
611
dmpt
ran-
0’PO
LE#P
PM;
See
dram
2439
4009
2475
3085
DBOT
2323
‘018
-460
160
1CM
#868
6068
dmpt
ran-
0’PO
LE8P
PM;
See
dram
2439
4009
2475
3086
D#O
T23
23‘0
184
337
337
CM#8
6968
66dm
ptra
e-0’
POLE
138P
M;
See
dram
2439
4009
2475
3087
DBS
T23
23‘D
W4
637
637
CM#9
8011
086
dmpt
run-
0’PO
LL8P
PM;
See
dram
2439
4909
2475
3088
DBOT
2323
‘OW
468
9#8
9CM
#660
6666
dmpt
ran-
0’PO
LE7P
PM;
See
dram
2439
4090
2480
1919
CHTR
1616
tWA
2787
2787
CM#6
6080
66D
WPT
RAN
-PO
LESS
OPP
M;S
eedr
am24
8887
4024
8019
21CH
TR16
16‘D
WA
2736
2736
CM#6
9666
66O
WPT
RAN
-PO
LE22
1PPM
;See
dram
2488
8740
2486
4781
CHTR
99
‘DW
-452
352
3CM
#866
8668
L#SC
E-00
3PO
LE62
PPM
;Se
edr
am24
7626
4924
8824
46C
HT#
68
DW
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928
0CM
6601
1660
6LA
SCE-
003
POLE
#OPP
M;S
eedr
am24
7626
4924
8966
55CH
TR7
7‘D
W-4
740
740
CM#8
6669
66LA
SCE-
003
TRA
NSF
OR
MER
eSO
n499
PFM
PCBS
(74
PPM
);Se
edr
um24
7626
4924
6887
40C
#TR
3030
‘0W
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9826
08CM
#868
6866
DW
PTRA
N-
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82PP
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SCA
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Do
not
ship
oat
ofco
antr
y24
7530
8906
0T23
23‘0
W-S
703
703
CM60
0866
66dm
ptra
n-0’
POLE
12PP
M;
See
dram
2439
4009
2475
3090
D6O
T23
23.0
W-s
-79
479
4CM
#666
6666
dmpt
ran-
0’PO
LE6P
PM;
See
drum
2439
4009
2475
3091
DBOT
2320
‘0W
-S67
5#7
5CM
6110
6680
8dm
ptra
n-0’
POLE
138P
M;
See
dram
2439
4009
2475
3092
D8O
T23
23.0
W-s
#82
#82
CM#6
6666
66dm
ptru
n-G
’PO
LE8P
FM;
See
drum
2439
4006
2476
2649
CHTR
2222
OW
-S21
321
3CM
8/4/
2011
LASC
E-00
3PO
LE94
PPM
;C
onta
ins
TSCA
PCBs
,D
ono
tsh
ipoa
tof
U.S
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APC
BS,
DO
NO
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IPO
UT
OF
COU
NTR
YEV
ALU
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FOR
PRO
CESS
ON
RE
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,OtJ
TB
OU
NO
TO
COFF
EYV
ILLE
ONLY
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ruct
with
this
cast
2480
5816
CHTR
1616
.0W
-s74
074
0CM
#688
1163
6LA
SCE-
003
TRA
NSF
OR
MER
nSO
c499
PPM
PCRS
(56
PPM
);Se
edr
um24
7626
4524
7389
0808
0024
24‘D
W-#
150
150
CM#6
6688
86LA
SCE-
G17
BUSH
ING
44PP
M;
See
dram
2472
1440
2473
9909
0800
2424
‘OW
-S15
0-
150
CM#6
6691
186
LASC
E-O
lTBU
SHIN
G17
PPM
;Se
edr
um24
7214
4024
7389
1506
0024
24‘D
W-6
150
150
CM#6
8683
811
LASC
E-01
7BU
SHIN
G3S
PPM
;See
dram
2472
1440
2473
8911
0600
2424
018-
615
015
0CM
9686
6666
LASC
E-G
17BU
SHIN
G37
PPM
;Se
edr
am24
7214
4024
7530
7709
0123
23‘D
W-#
670
870
CM#0
6666
06dm
ptru
n-0’
POLE
SPPM
;Se
edr
am24
3940
0924
7530
9309
0723
23‘O
W-6
440
440
CM#8
8666
116
dmpt
run-
9’PO
LESP
PM;
See
dram
2439
4009
2480
5647
CHTR
1616
.0W
-s22
022
0CM
#899
8886
OW
PTR
AN
-pol
eSS
PPM
;Se
edr
um24
6BB
740
2481
4144
0807
1515
‘OW
-S-
1206
1206
CM
#061
1801
16dm
ptra
ntoi
pale
28pp
m;S
eedr
um24
3940
0B24
8141
45OB
OT15
15‘O
W-S
1718
1718
CM#0
6686
116
dmpt
ran-
0ipa
le4l
ppm
;Se
edc
am24
3940
0924
8968
18CH
OR
77
‘OW
-S31
31CM
6116
9666
0LA
SCE-
G16
BUSH
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B6P
PM;S
eedr
am24
8966
1424
8968
19CH
OR
77
‘OW
-S31
31CM
1866
8668
LASC
8-G
1BBU
SHIN
G81
PPM
;Se
edr
um24
8968
1424
6968
29CH
DR
77
‘018
-631
31CM
6888
8888
LASC
E-G
1RBU
SHIN
G6G
PPM
;Se
edr
um24
9968
14