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  • PIERO M. ARMENANTENJIT

    Cake Filtration

  • PIERO M. ARMENANTENJIT

    Cake Filtration Cake filtration consists of passing a solid

    suspension (slurry) through a porous mediumor septum (e.g., a woven wire). The solids inthe slurry are retained on the surface of themedium where they build up, forming anincreasing thicker cake.

    As more slurry is filtered the solids retained onthe medium provide most of filtering action. Incake filtration the cake is the real filteringelement.

  • PIERO M. ARMENANTENJIT

    Cake Filtration (continued) As time goes by the thickness of the cake

    increases, as more solids are filtered. Thisresults in a corresponding increase of thepressure resistance across the cake.

    If the cake is incompressible (i.e., it does notchange its volume as pressure builds up) thepressure resistance increases proportionallyto the cake thickness.

    However, since most cakes are compressiblethe pressure across the cake typicallyincreases even faster than the cake build-up.

  • PIERO M. ARMENANTENJIT

    Cake Filtration (continued) The cake is removed intermittently during

    batch filtration processes. This is done bytaking the filter off line and manually orautomatically collecting the cake.

    The cake is removed continuously incontinuous processes, for example byscraping the cake with blades, as in rotatingfilters.

    Cake washing and drying operations can alsobe incorporated in the operation of mostfilters.

  • PIERO M. ARMENANTENJIT

    Examples of Cake-Forming Filters Filter presses Belt filters Vacuum filters:

    - Rotary vacuum belt filters

    - Rotary vacuum precoat filters

    - Vacuum disk filters

  • PIERO M. ARMENANTENJIT

    Example of a Filter Press

    After Metcalf and Eddy, Wastewater Engineering, 1991, p. 869

  • PIERO M. ARMENANTENJIT

    Cross Section of a Filter Press

    After Freeman, Standard Handbook of Hazardous Waste Treatment andDisposal, 1989, p. 7.9

  • PIERO M. ARMENANTENJIT

    Example of a Belt Filter

    After Freeman, Standard Handbook of Hazardous Waste Treatment andDisposal, 1989, p. 7.10

  • PIERO M. ARMENANTENJIT

    Schematic of a Belt Press Filter

    After Vesilind, Treatment and Disposal of Wastewater Sludges, 1979, p.156.

  • PIERO M. ARMENANTENJIT

    Example of a Rotary Vacuum Belt Filter

    After Freeman, Standard Handbook of Hazardous Waste Treatment andDisposal, 1989, p. 7.8

  • PIERO M. ARMENANTENJIT

    Example of a Rotary Vacuum Precoat Filter

    To Vacuum

    Precoat

    CakeDischarge

    Slurry

    Knife

    Filtrate

  • PIERO M. ARMENANTENJIT

    Precoats and Filter Aids A precoat is a layer of fine particulate material

    (e.g., perlite) added on to the filter septumbefore filtration to form a coating cake

    During filtration the filtered solids in the slurrymay clog the filter and reduce the rate offiltration. This happens especially if theresulting cake is very compressible

    In such cases a filter aid made of fine particlesof a hard but porous material (such as perlite)having good filtering properties is added to theslurry to prevent and filtered with the slurrysolids

  • PIERO M. ARMENANTENJIT

    Common Types of Precoats and FilterAids

    Diatomaceous earth (diatomite)A light siliceous material derived primarilyfrom sedimented diatoms (minute planktonicunicellular or colonial algae with silicifiedskeletons). Typical bulk density: 0.32 g/cm3

    PerliteA volcanic glass made of siliceous rock havinga concentric shelly structure. Typical bulkdensity: 0.16 g/cm3

  • PIERO M. ARMENANTENJIT

    Analysis ofCake Filtration

  • PIERO M. ARMENANTENJIT

    Analysis of Suspended SolidsRemoval During Cake Filtration

    As the suspension moves through the filtermedium (septum) the suspended solids arestopped by the filter septum forming a filter cakeon top of the filter septum

    As more solids suspension passes through thefilter the cake builds up providing most of thefiltering action for the incoming suspension

    Equations can be written to describe the removalof the particles in suspension by the filter (i.e.,the formation of the cake) and the pressure dropof the fluid as it passes through the cake

  • PIERO M. ARMENANTENJIT

    Important Variables in Cake Filtration Available pressure drop across cake, DP (Pa) Area of filtration, A (m2) Specific resistances of cake, a (m/kg) Specific resistances of medium (septum), Rm (1/m) Fluid superficial velocity, us (m/s) Size of cake particles, Dp (m) Shape factor for particles, fs Type of solids in suspension Cake void fraction, e (void volume/total bed volume) Time, t (s)

  • PIERO M. ARMENANTENJIT

    Important Variables in Cake Filtration Cake thickness, L (m) Concentration of solids in wastewater, Xw (g/L) Residual concentration of solids in filtrate, XF (g/L) Mass fraction of solids in cake, XC (g/g) Cumulative volume of wastewater fed to filter, VW (L) Cumulative volume of filtrate generated, VF (L) Cumulative mass of wet cake, mc (g) Mass of solids in the cake per volume of filtrate, XS (g/L) Density of wastewater, rw (g/L) Density of filtrate, rf (g/L)

  • PIERO M. ARMENANTENJIT

    Approach to Cake Filtration as aBatch Process

    Cake filtration is intrinsically a batch process.Hence, it can be expected that as filtrationproceeds the cake will build up and thepressure drop across the cake will increase.

    Mathematical modeling of batch cake filtrationis based on the determination of the rate offormation of the cake and the calculation ofpressure drop at any given time.

  • PIERO M. ARMENANTENJIT

    Approach to Cake Filtration as aBatch Process (continued)

    Integral quantities (such as the cumulativevolume of filtrate produced during a timeinterval, or the mass of the cake generatedduring the same interval) can be calculated byintegration of the basic instantaneous massbalances. In these equations the pressuredrop is typically a function of time.

    Continuous filtration is often modeled as asuccession of batch processes carried outover infinitesimally small time intervals.

  • PIERO M. ARMENANTENJIT

    Mass Balance Around a FilterFor a filter operating in a batch mode thefollowing diagram can be drawn:

    (Wet) Cake

    WastewaterFiltrate

    VW XW VF XF

    mc X'c

  • PIERO M. ARMENANTENJIT

    Definition of Xs

    Xs is defined as the mass of (dry) solids in thecake per volume of filtrate generated.

    From this definition it is that:

    XX m

    Vsc c

    F

    = =mass of solids in cakevolume of filtrate

    '

  • PIERO M. ARMENANTENJIT

    Relationship Between SolidConcentrations Around a Filter

    Mass balances around the filter give:

    X V X m X Vw W c c F F= +' (solids)

    r rw W c F FV m V= + (overall)

  • PIERO M. ARMENANTENJIT

    Relationship Between SolidConcentrations Around a Filter (cont.d)

    After an explicit expression for VF has beenobtained it can be substituted in the equationdefining Xs to get:

    X XX X

    X Xs cW F F W

    W W c

    = --

    ''

    r rr

    If the densities of the wastewater and the filtrateare the same, then:

    r r rW F= =

    X XX X

    X Xs cF W

    W c

    = --

    rr

    ''

  • PIERO M. ARMENANTENJIT

    Relationship Between SolidConcentrations Around a Filter (cont.d)

    Special case: A common situation is that inwhich all the solids contained in the suspensionare removed by the filter and contribute to theformation of the cake. In other words, the filtratedoes not contain any solids. In such a case it is:

    XF 0

    and the expression for Xs becomes:

    X XX

    X Xs cW

    c W

    = -

    rr

    ''

  • PIERO M. ARMENANTENJIT

    Relationship Between SolidConcentrations Around a Filter (cont.d)

    Note that, in general, Xs is different from XWOnly if:

    r X Xc W'>>

    it would then be that:

    X XX

    X XX

    XX

    Xs cW

    c Wc

    W

    cW= -

    @ @rr

    rr

    ''

    ''

  • PIERO M. ARMENANTENJIT

    Cumulative Mass Balance for theSolids in the Cake

    At a generic time t a cumulative mass balance forthe solids in the cake (i.e., the solids that havecontributed to the formation of the cake in thetime interval 0-t) gives:

    solids accumulated in the cake during time t

    solids removed from suspension during time t

    =

  • PIERO M. ARMENANTENJIT

    Cumulative Mass Balance for theSolids in the Cake

    The previous equation can be rewrittensymbolically, for a generic time t, as:

    ( ) ( )L A X L A X Vs W s F1- + =e r eThe first term represents the mass of solids in thesolid component of the cake at time t; the secondterm is the amount of solids still in suspension inthe water contained in the cake; and the thirdterm is the amount of solids removed from thefiltrate (and now held in the cake).

    Remark: L, e, and VF can all be functions of time.

  • PIERO M. ARMENANTENJIT

    Cumulative Mass Balance for theSolids in the Cake (continued)

    The volume of water contained in the cake (eLA) istypically much smaller than the volume of filtrate,VF, produced during the time interval 0-t.Furthermore, Xs and Xw are of the same order ofmagnitude. Then, one can safely assume that:

    ( )X V X L As F W>> eHence, the cumulative mass balance for thesolids in the cake becomes:

    ( )L A X Vs s F1- @e r

  • PIERO M. ARMENANTENJIT

    Cake Thickness, L, as a Function ofVolume of Liquid Passed Through

    the FilterThe previously derived mass balance equation forthe solids in the cake:

    ( )L A X Vs s F1- =e rcan be rewritten as:

    ( )LX V

    As F

    s

    =-1 e r

    where L, e, and VF can all be functions of time.

  • PIERO M. ARMENANTENJIT

    Shape Factor of Particles in CakeThe particle shape factor, fp, is defined as:

    fp =Surface area of sphere having same volume as particle

    Surface area of particlei.e.,

    fp

    ppp

    p

    p

    sph p

    D

    DVA

    VD A

    sph

    sph

    = =6 62

    3

    where Dsph is the diameter of a sphere having thesame volume as the particle.

  • PIERO M. ARMENANTENJIT

    Relationship Between Dp, Dsph, and fpSince:

    DVAp

    p

    p

    =6

    and:

    fpsph

    p

    pDVA

    = 16

    then:

    D Dp p sph= f

  • PIERO M. ARMENANTENJIT

    Approximate Relationship BetweenDp and Sieve Opening

    The assumption is often made that:

    D Dsph p

    where Dp is the average size of the particleswhose size is between two sieve openings

    D D Dp s s= 1 2and where Ds1 and Ds2 are the sieve openings.Then:

    D D Dp p sph p p= @f f

  • PIERO M. ARMENANTENJIT

    Pressure Drop During Cake Filtration

    Filter Cake L(t)

    Filter Medium

    Filtrate

    Suspension

    DPc(t)

    DPm

  • PIERO M. ARMENANTENJIT

    Pressure Drop During Cake FiltrationAt any time, t, the pressure drop experienced atthat time by a suspension passing through a filtercake supported by a filter medium (or septum) is:

    ( ) ( )D D DP t P t Pc m= +where:DP(t) = total pressure drop across filterDPc(t) = pressure drop due to filter cakeDPm = pressure drop due to filter mediumRemark: during batch filtration the cake can beexpected to build up, and the pressure drop toincrease as time passes.

  • PIERO M. ARMENANTENJIT

    Pressure Drop Across Filter CakeSince the liquid passing through the filter cakemoves in laminar flow (because of the small poresof the cake and the slow fluid velocity) the Blake-Kozeny equation can be used (instead of the moregeneral Ergun equation) to describe thedependence of the pressure drop through thecake with the superficial velocity, us:

    ( )DP L

    Duc

    p pL s=

    -

    150 1 23

    2

    Ree

    e r Blake-Kozeny equation

    where DPc is the pressure drop through the cake,and is, in general, a function of time.

  • PIERO M. ARMENANTENJIT

    Pressure Drop Across Filter CakesSubstituting the expression for Re in the Blake-Kozeny equation gives:

    ( )DP L

    Duc

    ps=

    -

    1501 2

    3 2me

    e

    As before, DPc is typically a function of time, sincethe cake thickness, L, the superficial velocity, us,and the void fraction, e, can all change with time.

  • PIERO M. ARMENANTENJIT

    Pressure Drop Across Filter Cakes(Carman-Kozeny Equation)

    For filter cakes the constant 150 may not beappropriate since the cake particles arecompressible.

    Therefore the Blake-Kozeny equation is oftenrewritten to produce to so-called Carman-Kozenyequation:

    ( )DP k L

    Duc

    ps=

    -

    1

    2

    3 2

    1m ee Carman-Kozeny equation

    where: k1 = proportionality constant.

  • PIERO M. ARMENANTENJIT

    Superficial Velocity in Cake FiltrationAs before, the superficial (or approach) velocity isdefined as the velocity of the liquid as it flowsthrough a cross section equal to that of the tank(or filter vessel) in the absence of the cake. It isalso equal to the filtrate flow rate, QF, divided bythe total cross-sectional area normal to flow, i.e.:

    uQA

    dVd t As

    F F= = 1

    where:A = cross sectional area or empty filter vessel

    VF = volume of filtrate passed through the cakeduring time t

  • PIERO M. ARMENANTENJIT

    Equation for Pressure Dropin the Cake

    Combining together the equations:

    ( )DP k L

    Duc

    ps=

    -

    1

    2

    3 2

    1m ee uQA

    dVd t As

    F F= = 1

    and: ( )LX V

    As F

    s

    =-1 e r

    the following expression for DPc is found:( )

    ( )DPk

    DX VA

    dVd tc s p

    s F F=-

    -

    1

    2

    3 2 2

    1 11r

    ee e

    m

  • PIERO M. ARMENANTENJIT

    Equation for Pressure Dropin the Cake

    The previous equation can be re-arranged to givethe final equation for the pressure drop in thecake:

    DP X VA

    dVd tc

    s F F= a m 2

    where a = specific cake resistance to filtration, isgiven by:

    ar

    ee

    = -kDs p1

    2 3

    1

    DPC, L, a, and VF can all be functions of time.

  • PIERO M. ARMENANTENJIT

    Equation for Pressure Dropin Filter Medium (Septum)

    The pressure drop across the filter medium(septum) can also be expressed using theCarman-Kozeny equation that can be rewritten as:

    ( )DP k LD

    umm

    m

    m

    pms=

    -

    2

    2

    3 2

    1m

    ee

    where the subscript m refers to the medium andthe superficial velocity is given by:

    uQA

    dVd t As

    F F= = 1

  • PIERO M. ARMENANTENJIT

    Equation for Pressure Drop in FilterMedium (continued)

    The resulting expression of the pressure drop inthe medium is:

    DP RA

    dVd tm m

    F= m 1

    where:

    ( )R k

    LDm

    m

    m

    m

    pm

    =-

    2

    2

    3 2

    1 ee

    with Rm = specific resistance of medium tofiltration

  • PIERO M. ARMENANTENJIT

    Equation for Total Pressure DropDuring Cake Filtration

    Recalling that the total pressure drop in a filter is:( ) ( )D D DP t P t Pc m= +

    it is:

    ( ) ( ) ( )DP t t X V tA

    RA

    dVd t

    s Fm

    F= +

    a m m2

    1

    Since by definition it is: QF(t) = dVF/dt, then:

    ( ) ( )( ) ( )[ ]dVd t

    Q tA P t

    t X V t ARF

    Fs F m

    = =+

    2 Dm a

    This is the main design equation for cake filters.

  • PIERO M. ARMENANTENJIT

    Specific Cake Resistance andCake Compressibility

    From the expression for a:a

    re

    e= -k

    Ds p1

    2 3

    1

    one can incorrectly assume that the pressureacross the cake has no impact on specific cakeresistance. In fact, the void fraction e for mostcakes can be significantly affected by pressure,since the cake is often compressible. Since thepressure drop changes with time the void fractione can also be a function of time, at least inprinciple.

  • PIERO M. ARMENANTENJIT

    Specific Cake Resistance andCake Compressibility

    In practice, it is convenient to carry outexperiments to determine:

    the specific cake resistance under no pressuredifference (no compression). Cake is built upby gravity filtering;

    the effect of pressure difference across thecake on the specific cake resistance. Cake isbuilt up first and then compressed to a knowpressure with a piston provided with a porousbottom. Filtrate is passed trough the cake.

  • PIERO M. ARMENANTENJIT

    Specific Cake Resistance andCake Compressibility

    Piston

    Suspension

    Filtrate

    Cake

    CakeBuildup

    CompressedCake

    Suspension

    Filtrate

    Filtrate

    PP

  • PIERO M. ARMENANTENJIT

    Specific Cake Resistance andCake Compressibility (continued)Possible results of cake compression experiment:

    cake is incompressible. Cake resistance, a isindependent of DP;

    cake is compressible. Cake resistance isexpressed as:

    ( )a a= o sPDwith: ao = empirical constant

    s = coefficient of compressibility (typicalrange for most domestic sludges: 0.4-0.9; lime sludges: 1.05; sand: 0).

  • PIERO M. ARMENANTENJIT

    Specific Cake ResistanceTypical values of the specific cake resistance, a,are in the following ranges:

    1013-1015 m/kg for raw sludges; 1011-1012 m/kg for well conditioned sludges.

  • PIERO M. ARMENANTENJIT

    Typical Specific Cake Resistancewith Chemical Conditioning

    0 0.5 1 1.5 2 2.5

    Chemical Conditioner (%)

    1E+010

    1E+011

    1E+012

    1E+013

    1E+014

    Spe

    cific

    Cak

    e R

    esis

    tanc

    e, a

    (m/k

    g)

    After Vesilind, Treatment and Disposal of Wastewater Sludges, 1979, p.156.

  • PIERO M. ARMENANTENJIT

    Compressibility of Sludges as Measuredby the Specific Resistance Test

    1 10 100

    Vacuum Pressure (kPa)

    1E+010

    1E+011

    1E+012

    Spe

    cific

    Cak

    e R

    esis

    tanc

    e, a

    (m/k

    g)

    After Vesilind, Treatment and Disposal of Wastewater Sludges, 1979, p.156.

  • PIERO M. ARMENANTENJIT

    Batch Filtration OperationsBatch cake filtration is typically carried out underone of the following conditions:

    Constant filtrate flow rate. Since the pressuredrop across the filter increases as a result ofcake buildup this condition implies that theupstream pressure must be increased withtime.

    Constant pressure drop across the filter. Thiscondition implies that the filtrate flow ratedeclines as the cake builds up.

    Variable flow rate and variable pressure drop.

  • PIERO M. ARMENANTENJIT

    Batch Cake Filtration atConstant Filtrate Flow Rate

    In some cases cake filtration is carried out usinga positive displacement pump. This results in aconstant flow rate process. Then:

    QF = constantRecalling the design equation for cake filters it is:

    ( )( ) ( )[ ]

    dVd t

    QA P t

    t X V t ARF

    Fs F m

    = =+

    2 Dm a

    Important: although QF = dVF/dt is a constant, VF(the total filtrate at time t) is not. In fact, it is:

    dV Qdt V Q tF F F= =

  • PIERO M. ARMENANTENJIT

    Batch Cake Filtration atConstant Filtrate Flow Rate (cont' d)

    Assuming that the cake is not compressible (i.e.,a is independent of DP) the pressure buildupwhile operating at constant filtrate flow rate (i.e.,constant QF) is given by:

    ( ) ( )[ ]DP t X V t ARA

    Qs F m F=+m a

    2

    i.e., recalling that VF = QFt:

    ( )DP t X QA

    tR Q

    As F m F= +ma m

    2

    2 ( )for constantQF =

  • PIERO M. ARMENANTENJIT

    Applications of Batch Cake Filtrationat Constant Filtrate Flow Rate

    Batch cake filtration at constant filtrate flowrate is used primarily in sludge dewatering;

    The type of filters that utilizes filtration methodis the filter press;

    Positive displacement pumps are used to forcethe suspension through the filter;

    Gauge pressures up to 225 psi (15 atm) areused.

  • PIERO M. ARMENANTENJIT

    Batch Cake Filtration at Constant DPIf the pressure across the filter is constant thegeneral filtration equation:

    ( ) ( )( ) ( )[ ]dVd t

    Q tA P t

    t X V t ARF

    Fs F m

    = =+

    2 Dm a

    becomes:

    ( ) ( )[ ]dVd t

    Q tA P

    X V t ARF

    Fs F m

    = =+

    2 Dm a

    Note that the coefficient a is constant (but notnecessarily equal to ao) even if the cake iscompressible, since DP = constant.

  • PIERO M. ARMENANTENJIT

    Batch Cake Filtration atConstant DP (continued)

    Since DP = constant, the previous equation can beintegrated by separating variables:

    ( )m a X V ARA P

    dV d ts F m F

    Vt

    F '' '

    +

    = 2

    00D

    Integration of this equation yields:

    ( ) ( )ma mXA P

    V tR

    A PV t ts F

    mF2 2

    2

    D D+ = ( )for constantDP =

  • PIERO M. ARMENANTENJIT

    Batch Cake Filtration atConstant DP (continued)

    The previous equation can be rewritten as:

    ( ) ( )h gV t V t tF F2 + =where DP is constant, and the parameters h and gare given by the equations:

    h ma= XA P

    s

    2 2 D and gm= RA P

    m

    D

  • PIERO M. ARMENANTENJIT

    Batch Cake Filtration at Constant DP:Determination of Filtration Parameters

    The determination of h and g from batchexperiments conducted at constant DP can bemade by rearranging the equation:

    ( ) ( )ma mXA P

    V tR

    A PV t ts F

    mF2 2

    2

    D D+ =

    as: ( ) ( )t

    V tX

    A PV t

    RA PF

    sF

    m= +ma m2 2 D D

    with: slope and intercept= = = =hma g mXA P

    RA P

    s m

    2 2 D Dand t/VF = y-coordinate and VF = x-coordinate

  • PIERO M. ARMENANTENJIT

    Determination of the Specific Cake ResistanceThrough Batch Filtration Experiments atConstant DP: Buchner Funnel Apparatus

    Buchner Filter

    Vacuum Gauge

    Graduated Cylinder

    To Vacuum

  • PIERO M. ARMENANTENJIT

    Determination of the Specific Cake ResistanceThrough Batch Filtration Experiments at

    Constant DP: Filter Leaf Apparatus

    VacuumGauge

    GraduatedCylinder

    To Vacuum

    FilterLeaf

  • PIERO M. ARMENANTENJIT

    Example of ExperimentalDetermination of Filtration Constants

    0 0.001 0.002 0.003 0.004 0.005 0.006

    Cumulative Filtrate Volume, VF (m3)

    0

    5,000

    10,000

    15,000

    20,000

    25,000

    t/VF

    (s/m

    3 )

    ExperimentalRegression

    Intercept = 6840.95 s/m3

    Slope = 2.85378E+006 s/m6

  • PIERO M. ARMENANTENJIT

    Batch Cake Filtration at Constant DP:Approximate Equations

    If the resistance of the filter medium, Rm, is verysmall in comparison to the cake resistance, a, thebatch filtration equation can be rewritten as:

    ( )t XA P

    V ts s@ma2 2

    2

    D ( )V t A P

    Xt

    tF

    F

    @ =22 D

    ma hi.e.:

    ( )Q t dVd t

    A PX t tF

    F

    F

    = @ =12

    2 12

    12 Dma h

    Note that QF(t) 0 for t .

  • PIERO M. ARMENANTENJIT

    Batch Cake Filtration at Constant DP:Plot of Approximate Expression

    for VF(t)

    Time, t

    Cum

    ulat

    ive

    Filtr

    ate

    Vol

    ume,

    VF

  • PIERO M. ARMENANTENJIT

    Applications of Batch Cake Filtrationat Constant DP

    Batch cake filtration at constant DP is usedprimarily in sludge dewatering;

    The types of filters using this filtration methodinclude:

    - Filter presses

    - Belt filter presses

  • PIERO M. ARMENANTENJIT

    Continuous Cake Filtration atConstant DP: Rotary Vacuum Filters

  • PIERO M. ARMENANTENJIT

    Continuous Cake Filtration atConstant DP: Rotary Vacuum Filter

    CakeDewatering

    CakeDischarge

    Suspension

    Solids

    Cake

    Blade

    CakeFormation

    q

  • PIERO M. ARMENANTENJIT

    Continuous Cake Filtration atConstant DP: Rotary Vacuum Filters

    In continuous filtration operations, such asthose involving vacuum rotary filters, eachfilter element undergoes a batch cakefiltration, followed by a cake dewatering phase,and a cake discharge phase with each rotation.

    The filter cake is formed under a constant DPdriving force generated by a vacuum.

    The filter cake is formed only during the timeperiod when the filter surface is immersed inthe suspension.

  • PIERO M. ARMENANTENJIT

    Continuous Cake Filtration atConstant DP: Cycle Time

    The immersion period in each cycle (i.e., for eachfull rotation of the filter drum) is given by:

    t f t fk c k= = = =2

    22p

    wqp

    pw

    qw

    where: tc = cycle time (time for one full rotation)fk = fraction of cycle time available for cake

    formation = fraction submergence of drumsurface

    q = angle comprising the sector immersed insuspension (rad)

    w = rotational (angular) velocity (rad/s)

  • PIERO M. ARMENANTENJIT

    Continuous Cake Filtration atConstant DP: Filtration EquationDuring the time period t = fk tc the filter cake in arotary filter is formed just as in a batch operation.The (batch) filtration equation for part of thecontinuous process is:

    ( ) ( )ma mXA P

    V tR

    A PV t t f ts F

    mF k c2 2

    2

    D D+ = =

    since DP is constant.

  • PIERO M. ARMENANTENJIT

    Continuous Cake Filtration atConstant DP: Filtrate Generated

    During a CycleThe previous quadratic expression is an equationin VF that can be solved for VF and rearranged togive:

    ( )V t AX

    R Rf t X P

    Fs

    m mk c s= - + +

    a

    am

    2 2 D

  • PIERO M. ARMENANTENJIT

    Continuous Cake Filtration atConstant DP: Filtrate Flux

    The previous equation can be rearranged to give:

    Filtrate flux = =

    = = - + +

    QA

    VAt X

    Rt

    Rt

    f X Pt

    F

    F

    c s

    m

    c

    m

    c

    k s

    c

    1 222a

    am

    D

    which predicts the filtrate flux, i.e., the amount offiltrate VF produced per unit filter area during acycle (or full rotation) lasting a time interval tc.QF = average filtrate flow rate during the interval tc

  • PIERO M. ARMENANTENJIT

    Continuous Cake Filtration atConstant DP: Filter Loading

    This equation can be rewritten to give the amountof filter solids loading, Gk, produced during thesame cycle:

    G V XAt

    Rt

    Rt

    f X Ptk

    F s

    c

    m

    c

    m

    c

    k s

    c

    = = - + +

    1 222a

    am

    D

    where:

    Gk = filter solids loading (kg/m2 s) = amount ofsolids filtered per unit filter area over a timeinterval tc.

  • PIERO M. ARMENANTENJIT

    Continuous Cake Filtration atConstant DP: Continuous Operation

    Since a continuous process is nothing more thana sequence of cycles, each one lasting tc, then:

    Filtrate flux = = - + +

    QA X

    Rt

    Rt

    f X Pt

    F

    s

    m

    c

    m

    c

    k s

    c

    1 222a

    am

    D

    The equation:

    G V XAt

    Rt

    Rt

    f X Ptk

    F s

    c

    m

    c

    m

    c

    k s

    c

    = = - + +

    1 222a

    am

    D

    can be used to describe the continuous operationof a rotary (vacuum) filter.

  • PIERO M. ARMENANTENJIT

    Continuous Cake Filtration atConstant DP: Rotational VelocityIf the angular velocity is expressed in rpm, i.e.:

    N = 602wp

    then the cycle time and the rotational (angular)velocities (in rad/s or rpm) are related by:

    tNc

    = =2 60pw

    where: w = rotational (angular) velocity in rad/stc = cycle time (to complete a rotation) in secondsN = rotational (angular) velocity in rpm (rotations

    per minute).

  • PIERO M. ARMENANTENJIT

    Continuous Cake Filtration atConstant DP: Continuous Filtrate Flux

    The continuous filtrate flux can be convenientlyexpressed in terms of the agitation velocity:

    ( )Filtrate flux = = - + +

    QA X

    R R f X PFs

    m m k s12 2

    2 2

    2aw

    pw

    pw a

    mpD

    ( )Filtrate flux = = - + +

    QA X

    R N R N f N X PFs

    m m k s160 60

    260

    2 2

    2aa

    mD

    where: tc = cycle time (to complete a rotation), in sN = rotational (angular) velocity in rpm (rotations

    per minute).

  • PIERO M. ARMENANTENJIT

    Continuous Cake Filtration atConstant DP: Simplified EquationsIf the resistance of the filter medium, Rm, is verysmall then the equations for continuous filtrationcan be simplified and rewritten as:

    Filtrate flux = = @QA

    VAt

    f PX t

    F F

    c

    k

    s c

    2 Dma

    G V XAt

    f X Ptk

    F s

    c

    k s

    c

    = @ 2 Dma

    These equations are especially useful tounderstand the relationships between the variousvariables affecting a continuous filtration process.

  • PIERO M. ARMENANTENJIT

    Continuous Cake Filtration atConstant DP: Simplified Equations

    If the resistance of the filter medium, Rm, is verysmall the equations for continuous filtration can beexpressed as a function of the rotational velocity as:

    Filtrate flux = = @ @QA

    VAt

    f PX

    F F

    c

    k

    s

    D wpma

    @ 260

    f P NX

    k

    s

    Dma

    where: tc = cycle time (to complete a rotation) in sN = rotational (angular) velocity in rpm (rotations

    per minute).

  • PIERO M. ARMENANTENJIT

    Applications of Continuous CakeFiltration at Constant DP

    Continuous cake filtration at constant DP is themost widely used method of sludgedewatering;

    The types of filters using this filtration methodinclude:

    - Rotary vacuum belt filter

    - Rotary vacuum precoat filters

    - Rotary vacuum drum filters

    - Rotary vacuum disc filters

  • PIERO M. ARMENANTENJIT

    Comparison of Different Types of FiltersRotary

    Drum BeltFilters

    Belt FilterPresses

    FilterPresses

    GranularDeep-Bed

    Filters

    Size 1-70 m2 1-2 m beltwidth

    0.02-16 m3 0.2-10 m2

    Solids inFeed (%)

    2-5 2-8 -- --

    Solids inCake (%)

    15-20 15-25 28-40

    SolidsLoading

    10 kg/m2 h 190-270kg/m h

    -- 0.12-0.5m3/m2 min

    After Freeman, Standard Handbook of Hazardous Waste Treatment andDisposal, 1989, p. 7.12

  • PIERO M. ARMENANTENJIT

    Design Information for PressureCake Filters

    Cycle time: of the order of hours

    Solids loading: 0.2-2 lb/fth

    Solids in cake: up to 50%

    Remark: although solids loading in pressurefilters (e.g., filter presses) is typically smaller thanthat of vacuum filters the percentage of solids inthe cake is typically higher. This is the result ofthe higher pressure that can be used in theoperation of pressure filters (as opposed to amaximum of 1 atm in vacuum filters).

  • PIERO M. ARMENANTENJIT

    Design Information for Rotary Vacuum FiltersDiameter: up to 5 mLength: up to 6 mVacuum levels: typically 20 in. Hg (68 kPa)Submergence: 15-25% of drum area

    PrimarySludges

    Waste-activatedsludges

    Solids loading 20-60 kg/m2h(4-12 lb/ft2h)

    5-20 kg/m2h(1-4 lb/ft2h)

    Solids in cake 25-40%(typically 20-25%)

    10-15%

    After Sundstrom and Klei, Wastewater Treatment, 1979, p. 234.

  • PIERO M. ARMENANTENJIT

    Operation of Rotary Vacuum Filters Solids loading increases with increasing drum

    submergence, drum rotational speed, pressuredifference across cake, solids concentration infeed.

    Percentage of solids in cake decreases withincreasing drum submergence, and drumrotational speed.

    Rotary vacuum filters can be used to dewatersludges from activated sludge plants(biological sludges), chemical sludges, andsludges from precipitation operations.

  • PIERO M. ARMENANTENJIT

    Additional Information and Exampleson Cake Filtration

    Additional information and examples on can be found inthe following references:

    Sundstrom, D. W. and Klei, H. E., 1979, WastewaterTreatment, Prentice Hall, Englewood Cliffs, NJ, p.229-234.

    Geankoplis, C. J., Transport Processes and UnitOperations, 3rd Edition, 1993, Allyn and Bacon,Boston, pp. 800-815.

    Freeman, H. M. (ed.), 1989, Standard Handbook ofHazardous Waste Treatment and Disposal, McGraw-Hill, New York, pp. 7.3-7.19.

  • PIERO M. ARMENANTENJIT

    Additional Information and Exampleson Cake Filtration

    Haas, C. N. and Vamos, R. J., 1995, Hazardous andIndustrial Waste Treatment, Prentice Hall, EnglewoodCliffs, NJ, pp. 75-78.

    Wentz, C. W., 1995, Hazardous Waste Management,Second Edition, McGraw-Hill, New York. pp. 196-200.

    Vesilind, P. A., 1979, Treatment and Disposal ofWastewater Sludges, Ann Arbor Science, Ann Arbor,MI, pp. 140-161.

  • PIERO M. ARMENANTENJIT