characterization of aegle marmelos fiber reinforced composites

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    Characterization of Aegle

    Marmelos Fiber Reinforced

    Composite

    Dr. M. Naga Phani Sastry,

    Smt. K. Devaki Deviand

    Din Bandhu

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    A composite material is a combination of a binding resin (matrix) with

    small filaments of solid material (reinforced material).

    Green composite or bio-composite is a composite material which consists

    of one or more phase(s) of natral or biological origin. As reinforcement! it

    incldes bio wastes li"e lea#es of cocont shell! waste wood powder! waste

    paper! or e#en b$-prodcts of food crops! or fibers from plant or

    #egetables sch as cotton! flax! hemp! %te! cane! banana and the li"e.

    &e to en#ironmental contamination! the need for green composite arises.

    'n this paper! the bar" of Aegle Marmelos is ta"en as natral fiber for

    examining tensile strength and flexral strength. canning lectron

    Microscope (M) anal$sis is also accomplished to "now the bonding

    between the reinforcement and the matrix.

    '*+R,&C+',*

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    +o prepare the composite materials for different fiber #olme fractions

    and fiber lengths with bar"s of Aegle Marmelos as reinforcement.

    +o e#alate the #arios mechanical properties li"e tensile strength (+)

    and flexral strength (F) for these de#eloped composite specimens.

    +o #alidate the experimental reslts sing regression anal$sis.

    +o anal$ze the microstrctre of composites sing M anal$sis.

    ,/C+'0

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    Materials sed for the preparation of test specimens

    Epoxy resin

    Hardener

    Aege Marmeos !Bivam" #i$er

    Mouds

    MA+R'A1

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    +he following steps were in#ol#ed in the preparation of test specimens2

    #i$er extra%tion &rom the $arks o& Aege Marmeos.

    Moud preparation $y appying moud reeasing agent.

    #i$er %utting as per the moud spe%i&i%ations

    Homogeneous mixing o& epoxy and hardener in a proportionate manner.

    Pa%ement o& &i$ers into the moud in a desired orientation.

    Pouring the homogeneous mixture o& epoxy and hardener so'y into moud.

    (emova o& ex%essive epoxy and hardener soution.

    )uring &or proper hardening.

    )utting o& spe%imens as per AS*M standards.

    +3 '*0,10& '* 3C'M* 3R3ARA+',*

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    'n order to "now the performance of the composites prepared in the

    present wor"! the following tests and anal$sis are condcted2

    *ensie test

    #exura test

    SEM anaysis

    efore performing these tests! the specimens are ct as per the A+M

    standards.

    ++ A*& A*A14' 3RF,RM&

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    As per A+M standards! the following dimensions are emplo$ed for tensile

    tests and flexral tests2

    &imensions of specimen for tensile test

    &imensions of specimen for flexral test

    &'M*',* ,F 3C'M*

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    +M for tensile and flexral tests

    5'3M*+ & F,R ++ A*& A*A14'

    M anal$sis apparats

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    +he following steps were in#ol#ed in the preparation of test specimens2

    (a) traight ,rientation (b) Cris Cross ,rientation

    (c) lant ,rientation

    pecimens in #arios orientation for tensile tests

    3C'M* 3R3AR& F,R +*'1 ++

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    +he following steps were in#ol#ed in the preparation of test specimens2

    (a) traight ,rientation (b) Cris Cross ,rientation

    (c) lant ,rientation

    pecimens in #arios orientation for flexral tests

    3C'M* 3R3AR& F,R F16RA1 ++

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    +ensile strength of three different orientations are compared as follows2

    C,M3AR',* ,F +*'1 +R*G+7

    Weight

    of fiber

    Straight

    orientation

    Criss-cross

    orientation

    Slant

    orientation

    5 29.71 9.44 6.69

    10 32.64 13.32 12.52

    15 35.87 15.83 8.65

    20 39.93 18.31 14.35

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    +ensile strength of three different orientations are compared as follows2

    C,M3AR',* ,F F16RA1 +R*G+7

    Weight

    of fiber

    Straight

    orientation

    Criss-cross

    orientation

    Slant

    orientation

    5 63.35 19.91 63.85

    10 83.77 21.22 66.35

    15 95.18 29.54 71.66

    20 101.86 48.37 80.36

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    0alidation of the experimental reslts is carried ot sing regression anal$sis. 'n

    this wor"! one factor anal$sis has been carried ot with a single factor! weight of

    the fiber (w). Regression e8ations are modelled with the experimental reslts to

    identif$ the relation between the inpt parameter 9w: and the responses! tensile

    strength and flexral strength! gi#en in the following e8ations2

    traight orientation2

    +s;.?>>@ B.D@EA B.B;;EA= ------------------ (;)

    Fs;.; @.D>BEA B.;>?EA= ------------------ (=)

    Criss-cross orientation2

    +s=

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    C,M3AR',* ,F 63R'M*+A1 A*& 3R&'C+& 0A1

    Straight Tensile strength (MPa) Flexural Strength (MPa)

    Wt of fiber

    (g)

    Exp Pred %

    dev

    Exp Pred %

    dev

    5 29.71 29.736 -0.08 63.35 63.56 -0.33

    10 32.64 32.56 0.243 83.77 83.13 0.766

    15 35.87 35.945 -0.22 95.18 95.82 -0.67

    20 39.93 39.903 0.066 101.8

    6

    101.6 0.21

    Criss-cross

    Wt of fiber

    (g)

    5 9.44 9.507 -0.71 19.91 20.085 -0.88

    10 13.32 13.119 1.51 21.22 20.695 2.474

    15 15.83 16.031 -1.27 29.54 30.065 -1.77

    20 18.31 18.243 0.365 48.37 48.195 0.361

    Slant

    Wt of fiber

    (g)

    5 6.69 6.667 0.343 63.85 63.879 -0.04

    10 10.87 10.939 -0.63 66.35 66.263 0.131

    15 16.42 16.351 0.42 71.66 71.747 -0.12

    20 22.88 22.903 -0.1 80.36 80.331 0.036

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    'n the present wor"! the interfacial bonding between the matrix and reinforcement

    composites are carried ot. +he cr$ogenicall$ cooled and fractred specimen

    srfaces are gold coated and the fractred srface is photographed sing canning

    lectron Microscope (M). +he following figre depicts the microstrctres of

    ntreated fiber nder M2

    Fig. >2 ntreated Aegle Marmelos fiber =BB6 magnification(traight! lant

    and Criss-cross orientations)

    M A*A14'

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    Composites of epox$ dispersed with @! ;B! ;@ and =B wtI Aegle Marmelos

    fiber! ha#e been sccessfll$ prepared.

    #alation of mechanical properties (tensile and flexral strengths) and

    M anal$sis has been performed for #arios orientations.

    't was fond that the tensile strength of the composites in straight

    orientation increases with the weight of the fiber within the experimental

    range.

    +he flexral strength of straight and criss-cross orientations increases with

    an increase in weight of the fibers.

    From the M anal$sis diagrams! it is e#ident that the fiber pllot within

    the specimen is de to the lesser bonding between the reinforcement and

    the matrix material.

    R1+ A*& C,*C1',*

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    +7A*J 4,K