chapter 7 comparison of wedm of al/sicp and al/al2o3p...

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151 CHAPTER 7 COMPARISON OF WEDM OF Al/SIC P AND Al/AL 2 O 3P COMPOSITES ____________________________________________________________________ 7.1 Scope In this chapter, a comparative study on WEDM of A359/SiC P and A6061/Al 2 O 3P composites is presented. Comparisons between the characteristics of the machined surfaces, material removal rates and dimensional accuracy in WEDM of SiC and alumina reinforced MMCs are presented. Moreover, critical issues such as wire breakages and wire shifting are discussed in detail. In addition, recommendations are made to overcome these problems in machining of these difficult-to-machine materials. Finally, a new strategy for successful machining of these difficult-to-cut materials is proposed. 7.2 Surface Characteristics Over the years, it has been observed that the EDM/WEDM machined surfaces are significantly different than those machined by using any other machining process. These surfaces have no texture or pattern which extends beyond the individual craters. The non-directional surface patterns have proved to be one of the major advantages of EDM over conventional machining in several applications (Huntress et al., 1986). The examples, in particular, are making of the punches and dies, fluid control parts like fuel jets and injectors. A clear characterization of surface topography is essential to predict the quality and functional behaviour of the surfaces such as static and dynamic stiffness, wear resistance, fretting corrosion etc. (Ramarao et al., 1982). In the present section, the surface characteristics of alumina and SiC reinforced composites are compared. The characteristics of surfaces include surface roughness study, surface appearance, surface topography, and qualitative study of recast layer. In addition, an attempt is made to correlate the important surface roughness parameters with the machining process parameters.

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Page 1: CHAPTER 7 COMPARISON OF WEDM OF Al/SICP AND Al/AL2O3P …shodhganga.inflibnet.ac.in/bitstream/10603/27302/15/15_chapter 7.p… · The non-directional surface patterns have proved

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CHAPTER 7

COMPARISON OF WEDM OF Al/SICP AND Al/AL2O3P COMPOSITES

____________________________________________________________________

7.1 Scope

In this chapter, a comparative study on WEDM of A359/SiCP and A6061/Al2O3P

composites is presented. Comparisons between the characteristics of the machined

surfaces, material removal rates and dimensional accuracy in WEDM of SiC and

alumina reinforced MMCs are presented. Moreover, critical issues such as wire

breakages and wire shifting are discussed in detail. In addition, recommendations are

made to overcome these problems in machining of these difficult-to-machine

materials. Finally, a new strategy for successful machining of these difficult-to-cut

materials is proposed.

7.2 Surface Characteristics

Over the years, it has been observed that the EDM/WEDM machined surfaces are

significantly different than those machined by using any other machining process.

These surfaces have no texture or pattern which extends beyond the individual craters.

The non-directional surface patterns have proved to be one of the major advantages of

EDM over conventional machining in several applications (Huntress et al., 1986). The

examples, in particular, are making of the punches and dies, fluid control parts like

fuel jets and injectors. A clear characterization of surface topography is essential to

predict the quality and functional behaviour of the surfaces such as static and dynamic

stiffness, wear resistance, fretting corrosion etc. (Ramarao et al., 1982).

In the present section, the surface characteristics of alumina and SiC reinforced

composites are compared. The characteristics of surfaces include surface roughness

study, surface appearance, surface topography, and qualitative study of recast layer. In

addition, an attempt is made to correlate the important surface roughness parameters

with the machining process parameters.

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7.2.1 Surface Roughness Studies

A practical EDM surface is a random superposition of craters formed by the thermal

effect of successive discharges. Thus, the most common method of representing the

surfaces by Ra or maximum peak-to-valley distance (Rmax) fails to give a true picture

of the surface. Therefore, in the present study, a number of amplitude and one spacing

parameters have been investigated.

The machined specimens of the experiments reported in Chapter 4 and Chapter 5

were used for this purpose. The measurement and analysis of these specimens are

presented in this section.

The amplitude parameters are the most important parameters to characterize surface

topography. They are used to measure the vertical characteristics of the surface

deviations (Gadelmawla et al., 2002). The following surface roughness parameters,

other than the Ra, were investigated:

1. Root mean square roughness (Rq): This parameter is also known as RMS. It

represents the standard deviation of the distribution of the surface heights. This

parameter is more sensitive than the arithmetic average height (Ra) to large

deviation from the mean line. The RMS mean line is the line that divides the

profile so that the sum of squares of the deviations of the profile height form this

line is equal to zero.

2. Ten-point height (Rz): This parameter is more sensitive to occasional high peaks

or low valleys than Ra. The international ISO system defines this parameter as the

difference in height between averages of the five highest peaks and five lowest

valleys along the assessment length of the profile.

3. Maximum height of the profile (Rt or Rmax): This parameter is very sensitive to the

high peaks or deep valleys or scratches. Rmax or Rt is defined as the vertical

distance between the highest peak and the lowest valley along the assessment

length of the profile.

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4. Mean height of peaks (Rp): It is defined as the mean of the maximum height of

peaks obtained for each sampling length of the assessment length.

5. Mean depth of valleys (Rv): It is defined as the mean of the maximum depth of

valleys obtained for each sampling length of the assessment length.

6. Skewness (Rsk): The skewness of a profile is the third central moment of the

profile amplitude probability density function, measured over the assessment

length. It is used to measure the symmetry of the profile about the mean line. This

parameter is sensitive to occasional deep valleys or high peaks. A symmetrical

height distribution, i.e. as many peaks as valleys, has zero skewness. Profiles with

peaks removed or deep scratches have negative skewness. Profiles with valleys

filled in or high peaks have positive skewness. Skewness parameter can be used to

distinguish between two profiles almost same Ra or Rq values but with different

shapes. The value of the skewness depends on whether the bulk of the material of

the sample is above (negative) or below (positive) the mean line.

7. Kurtosis (Rku): Kurtosis coefficient is the fourth central moment of profile

amplitude probability density function, measured over the assessment length. It

describes the sharpness of the probability density of the profile. If Rku < 3 the

distribution curve is said to be platykurtoic and has relatively few high peaks and

low valleys. Rku > 3 the distribution curve is said to be leptokurtoic and has

relatively many high peaks and low valleys.

8. Mean spacing at mean line (Rsm): The spacing parameters measure the horizontal

characteristics of the surface deviations. The parameter Rsm is defined as the mean

spacing between profile peaks and the mean line.

The results of measured values are given in Appendix ‘E’. The results, shown in

Table E-1 to Table E-5, revealed significant differences between the machined

surfaces of A359/SiCp and A6061/Al2O3p MMCs. These distinguishing features

between two different types of MMCs might be attributed to the differences between

the type of ceramic reinforcements and the type of matrix.

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The major difference found was the characteristic of the profile of the machined

surface, i.e. the value of Rsk. This parameter is very sensitive to deep scratches or

high peaks. The values of skewness appear to be uncorrelated to the machining

parameters for both types of composites. However, skewness values of A6061/Al2O3p

and A359/SiCp were found to be significantly different. In general, the skewness of

EDM machined surfaces is positive. A positive value of Rsk indicates that the surface

profile is ‘empty’ of material. Over the years, it has been observed that EDM

machined surfaces are of positive skewness (Mamilas et al., 1987; Petropoulos et al.,

2004).

The skewness values of A6061/Al2O3p composites were found to be positive.

However, it was negative for the machined surfaces of A359/SiCp composites. The

positive skewness of alumina reinforced composites might be attributed to the

significant presence of alumina particles protruding proudly on the machined

surfaces. The negative skewness of the SiC reinforced composites, however, might be

attributed to the complete removal of the SiC particles from the machined surfaces.

These results were further assessed and checked by scanning electron microscopy of

these machined surfaces. These findings agree with the results of Seo et al. (2006) at

short on-times and low current although their work is on conventional EDM. Based

on the gathered experimental data, statistical regression analysis was employed to

study the correlation of the surface roughness parameters with the machining

conditions. The coefficients of correlations are shown on Table 7.1 for these MMCs.

Table 7.1 Correlation coefficients of quadratic regression models of selected surface

roughness parameters

Roughness

parameters

Correlation coefficient, r

A6061/Al2O3/

10p

A6061/Al2O3/

22p A359/SiC/10p A359/SiC/20p

A359/SiC/

30p

Rz 0.945 0.91 0.85 0.948 0.916

Rq 0.95 0.88 0.92 0.91 0.97

Rp --- 0.90 --- --- 0.87

Rv 0.83 --- 0.92 0.88 0.917

Rsm 0.83 --- 0.90 --- ---

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7.2.2 Surface Topography

The topography of machined surfaces of alumina and SiC reinforced composites has

been studied. Scanning electron microscopy has been employed to assess the results

of roughness measurements. Moreover, attempt was made to study the effect of spark

energy (on-time) on the crater size and surface morphology of these composites. The

effects of volume fraction and type of ceramic have also been studied so as to

investigate into the causes of significant differences between surface characteristics of

these MMCs.

7.2.2.1 Influence of Spark Energy

The influence of spark energy (on-time) on the crater size can be appreciated from

Figure 7.1 and Figure 7.2. The craters appeared to be deeper and larger in case of

longer on-times as compared to short on-times. A comparison between the craters of

alumina reinforced MMCs and the SiC reinforced composites can also be made from

these figures.

The pulse on-time was found to influence the number of ceramic particles present on

the machined surfaces of alumina particle reinforced MMCs. It has been found that at

high level of spark energy more number of particles gets dislodged from the machined

surface. This was found to be attributed to the greater volume of molten metal at

longer on-time or spark energy causing easy deepening of the craters and

comparatively easy removal of the alumina particles from the machined surface.

Scanning electron micrographs of A6061/Al2O3p composites machined at 0.2 and 1

revealed this significant difference between the densities of alumina particles on the

machined surfaces (Figure 7.3).

The number of ceramic particles on the surface machined at low level of pulse on-

time was found to be greater as compared to the number of particles on the surfaces

machined at longer on-times. The height of the protrusions and depths of the craters

determine the roughness of the machined surface of alumina reinforced composites.

The roughness at the short on-time, thus, might be dominated by the height of the

particle protrusions where as the roughness values will be determined by the

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combined effect of the protrusion height as well as the depth of the discharge craters

at longer on-times. This is explained as deeper discharge craters at longer on-times

and greater protrusion heights at short on-times. This characteristic of A6061/Al2O3p

is, thus, found significantly different than the A359/SiCp MMCs. on the machined

surfaces of A359/SiCp composites, the SiC particulates have found to be absent. This

is in agreement with earlier studies (Gatto, 1997; Ramulu, 2001 and Seo et al., 2006).

Figure 7.1 Effect of pulse on-time on the size of crater in A359/SiCp composites

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Figure 7.2 Effect of pulse on-time on the size of crater in A6061/Al2O3p composites

Figure 7.3 Effect of spark energy on machined surfaces of A6061/Al2O3p

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7.2.2.2 Influence of Ceramic Particulates and Volume Fraction

The effect of volume fraction of ceramic particles on the size of craters can be

appreciated from Figure 7.1 and Figure 7.2. The crater size of 10% reinforcement

composites was found to be greatest among the A359/SiCp MMCs. However, the

craters of 20% and 30% SiC reinforced composites do not show any significant

difference. This trend is similar to the cutting speeds in machining of SiC reinforced

MMCs. The cutting speeds in machining of A359/SiC/10p were found to be greatest

as compared to the 20% and 30% composites of this type. The difference in the

cutting speed of A359/SiC/20p and A359/SiC/30p was also not very significant. This

might be attributed to the complete removal of the SiC particles from the machined

surfaces. In addition, the increase of 10% in ceramic particles beyond 20% may not be

influencing the process behaviour.

The machined surfaces of these different MMCs reveal that the mechanism of

material removal was predominantly melting and/or vaporization of the matrix alloy.

However, a number of issues are, believed to be, associated and these include: high

melt viscosity, reinforcement/matrix reactions, and segregation of the reinforcing

particles (Lloyd et al., 1989; Yue et al., 1996). In general, is has been agreed

unanimously that the ceramic particles remain unaffected during EDM/WEDM

machining and they might dislodge after removal of the surrounding matrix (Muller et

al., 2001; Yan et al., 2005). However, in the present study, the machined surfaces of

A359/SiC and A6061/Al2O3 were found to be fundamentally different from each

other.

The effect of ceramic particles on the size of the crater was found to be more

significant on the machined surfaces of alumina reinforced composites. The size of

crater was found to be limited by the surrounding ceramic particles. This might be

attributed to the plasma flushing capacity at the end of the discharge. The expelling

force at the end of the on-time might be influential to overcome the restrictions

implied by the surrounding alumina particles. This might be attributed to the high

density of ceramic particles protruding on these machined surfaces. The crater shown

in Figure 7.2 d) is an evidence of restriction to the expulsion of the molten aluminium

alloy due to the surrounding alumina particles. As shown in Figure 7.2 d), the depth of

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crater appeared to be greatest. This could be attributed to the concentration of the

spark energy on the conductive alloy trapped between the ceramic particles. These

particles might have caused poor transitivity of the discharge channel by virtue of

their electrical insulating properties. Moreover, the electrical resistivity of alumina is

significantly greater than that of the SiC.

The roughness of alumina reinforced composites was found to increase with the

increased percentage of the alumina reinforcements. The increase in the percentage of

SiC reinforcement lead, however, to reduced surface roughness. Moreover, the

ceramic particles were found protruding proudly on the machined surface of alumina

reinforced composites whereas the SiC particles were found to be absent on the

machined surfaces of A359/SiC composites.

Figure 7.4 Comparison between surfaces machined at 0.2 µs on-time A359/SiCp and

A6061/Al2O3p

The machined surfaces of SiC and alumina reinforced MMCs are shown in Figure 7.4

to appreciate the significant difference in the surface topography of these WEDM

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machined composites. The presence of alumina particles on the machined surface of

the alumina reinforced composite is evident in the Figure 7.4. However, the SiC

particles were not found to appear on the machined surfaces of A359/SiCp

composites. These findings agree with the previous studies of other researchers in

which both Al/SiCp (Gatto et al., 1997) and Al/Al2O3p MMCs have been machined

(Yue et al., 1996; Yan et al., 2005) in different separate experimental investigations.

In these studies, the roughness of SiC reinforced aluminium was found to be superior

to the unreinforced alloy, however, in Al/Al2O3p the roughness was found to be

inferior to the unreinforced alloy. Therefore, the protruding particles and effect of

concentration of discharge energy determine the roughness values in Al/Al2O3p.

It is, thus, believed that different ceramic reinforcements (SiC and Al2O3) may behave

differently in WEDM of these materials. Moreover, different matrix materials (A359

and A6061) might also be influential on the machining characteristics of these

composites. Thus, the difference between reinforcement and matrix alloy thought to

modify the machined surfaces of these MMCs. In the available literature, no

researches have been found to address these issues of major differences between

alumina and SiC reinforced aluminium matrix composites. Therefore, in view of

understanding the cause of this diverse kind of surfaces, SEM along with energy

dispersive X-ray analysis (EDX) of few machined surfaces was undertaken. The

results of these analyses are shown in Figure 7.5 and Figure 7.6. These results

revealed the significant presence of silicon and aluminium on the machined surfaces

of A359/SiCp composites, however, the presence of silicon carbide cannot be

confirmed from this analysis. This finding is in agreement with the earlier studies

(Ramulu, 2001; Seo et al., 2006). Moreover, no particles like features were observed

on the machined surfaces of A359/SiCp composites.

The absence of SiC particles on the machined surfaces of A359/SiCp MMCs could be

attributed either to the complete dislodging of the SiC particles from the metallic

molten matrix or to the chemical reaction between silicon and aluminium leading

towards absorption of silicon into aluminium matrix at high temperature environment

of WEDM process. It has been reported in few papers on solidification of Al/SiC that

silicon may dissociate from silicon carbide and get absorbed in the aluminium matrix

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and the percentage of silicon absorption was found to be dependent on the working

temperature (Lloyd et al., 1989, 1994).

Figure 7.5 EDS analysis of A359/SiC/20p MMC

001001

0.10 1.10 2.10 3.10 4.10 5.10 6.10 7.10 8.10 9.10 10.10

keV

001

0

1500

3000

4500

6000

7500

9000

10500

12000

Cou

nts

OK

a

AlK

aSi

Ka

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Figure 7.6 EDS analysis of A359/SiC/10p MMC

Thus, it was thought that silicon has been dissociated from the silicon carbide at high

temperature conditions in the WEDM process. Further, the dissociated carbon, as it is

not found in the EDS analysis, might have been vaporized at very high temperatures

of WEDM process. However, the presence of carbon and silicon supports presence of

SiC particles on the machined surfaces of A359/SiC/30p MMC. It might be attributed

to the higher volume fraction of SiC particles on these surfaces. Thus, it can be

0.10 1.10 2.10 3.10 4.10 5.10 6.10 7.10 8.10 9.10 10.10

keV

003

0

1500

3000

4500

6000

7500

9000

10500

12000

Cou

nts

OK

a

AlK

aSi

Ka

003003

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concluded that absence of silicon carbide on the machined surfaces of A359/SiCp

composites was attributed to the type of reinforcements. The role of matrix material,

thus, was found to be insignificant since in previous studies on WEDM of

A6061/SiCp (Gatto et al., 1997) and A356/SiCp composites (Muller et al., 2000) also

SiC particles were absent on the machined surfaces. Moreover, in the recent study by

Seo and co-workers (2006), the percentage of Si was found to be significantly greater

than that in the base alloy up to certain depth from the surface. This also agrees with

the findings of EDX of the above machined surfaces.

In the electro-discharge machining of metallic materials, the energy in the spark gap,

thermal conductivity, melting temperature, heat of fusion, coefficient of thermal

expansion, thermal diffusivity of the electrode determine the depth and diameter of

the craters. This, in turn, decides the surface finish of the machined part. It is known

that higher energy in the gap is responsible for poor surface finish due to larger and

deeper craters. However, in the machining of particle reinforced materials, the surface

morphology is different. In the machining of these materials, the presence of ceramic

particles was found to influence the surface finish (Yue et al., 1996; Yan et al., 2005).

The removal of the ceramic particles from the machined surface into the spark gap

was, believed, found to affect the gap conditions. Thus, the ceramic particles and their

properties might influence the surface quality in two different ways. First, if they

remain on the machined surface the surface quality depends on their size, protrusion

and type. Second, if the particles are released along with the molten metal, the gap

conditions and fluidity of the melt will be influenced. These particles, thus, affect the

roughness values in many ways:

• If the particles remain protruding, unaffected, on the machined surface, the

height of the protrusions and corresponding crater depth determine the

roughness value. Moreover, the depth of crater might be greater due to

concentration of the discharge channel caused by poor transitivity owing to

protruding insulating alumina particulates (arcing).

• If these particles are completely dislodged from the surface, the crater depth

and the depth created due to the particle pullout will determine the roughness.

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• The particles are completely dislodged; however, the droplets of molten metal

smear these created cavities. In this case, the roughness values will be further

different.

• If the dislodged particles remain in the spark gap, the discharge power density

will reduce due to dispersion of the discharge channel and the surface finish

will be improved.

• Other alterations such, as melting and/or evaporation and chemical reaction

between Al and Si of SiC or Al and carbon might result into different

character of machined surfaces.

1. 4Al + 3SiC ↔Al4C3 + 3Si

• The influence of the particles on the fluidity of the molten metal also

contributes toward the characteristics of the machined surfaces.

Thus, based on the above discussions and EDX analysis, it has been confirmed that

SiC particulates have been dislodged from the molten alloy. In case of alumina

reinforced composites, however, the number of particles on the machined surfaces

was significantly high.

These particulates (SiC/Al2O3), thus, found to influence the surface finish in different

ways. The A359/SiCp surfaces have found to be similar to the powder-mixed

dielectric surfaces (smooth and even). This might be attributed to the release of most

of the ceramic (SiC) particulates in the spark gap. Thus, spark channel might spread

and widen. This increased diameter of the discharge channel might have reduced the

discharge power density. Thus, due to reduction in the power density, the craters

formed on A359/SiCp composites have been found to be shallow and smooth, Figure

7.1 and Figure 7.2, as compared to alumina reinforced MMCs (Wong et al. 1998;

Tzeng et al 2001). Moreover, increased volume fraction will introduce more number

of SiC particles in the spark gap resulting in smoother surfaces. This phenomenon,

however, was not possible during machining of alumina reinforced MMCs as these

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particles did not found to be dislodged into the spark gap. The significant number of

protruding particles on the machined surfaces of alumina reinforced MMCs is

evidence of no or very less release of alumina particles.

In case of alumina reinforced composites, however, due to the ‘shielding effect’ of the

particles, the spark might be striking on the same spot due to no other path of least

resistance. This could be the reason of grater fluctuations in the cutting speed during

machining of alumina reinforced composites as compared to silicon carbide

reinforced MMCs. Similarly, this continuous arcing might cause deeper craters due to

repeated sparking concentrated on same area. Therefore, the surface roughness of

alumina reinforced MMCs were dependent on the depth of crater as well as the height

of the protruding alumina particles. This is distinguishable from the surfaces of silicon

carbide reinforced composites, where the SiC particles were not found on the

surfaces.

In addition to the effects of dispersion of discharge channel (A359/SiCp) and poor

transitivity and concentration of spark (A6061/Al2O3p), the effects of change in

fluidity of the molten metal might also be significant on the surface quality of these

MMCs.

The fluidity of the molten material might also be very significant on the re-

solidification of the molten material and thus on the surface finish of the machined

composites. The fluidity of molten A359 is comparatively lower than the fluidity of

molten A6061. In addition, significant reduction in the fluidity of A356 and A6061

due to SiC particles was observed (Lloyd et al. 1989). Therefore, grater amount of the

molten A359 might have remained on the machined surface. The decrease in the

fluidity of A359/SiCp MMCs might have been greater, as compared to alumina

reinforced composites, due to the presence of released SiC particulates in the molten

metal. Moreover, the fluidity of the melt would reduce with greater ceramic particles

in the melt. In addition, the large heat of fusion of alumina reinforced MMCs might

also result in the high fluidity of this composites as compared to SiC reinforced

composites (Ravi et al. 2008). Further, as already known (Lloyd et al 1989), the

reduced fluidity with increased SiC volume fractions could also be responsible for

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improved surface roughness of the A359/SiC MMCs with increasing volume fraction

of SiC particulates.

Although, due to the ‘shielding effect’ of the particles, the flow of molten aluminium

was found to be restricted, the fluidity might be still greater as compared to that in

A359/SiC composites as the melt contained very few or no particles. Moreover, the

larger size of alumina particulates might have also contributed to higher fluidity of

this MMC even at greater volume fraction (Rohatgi et al. 1981).

Thus, it can be concluded that the type of ceramic reinforcements has been found

more significant on the surface topography of the WEDM machined surfaces of

aluminium matrix composites.

7.2.2.3 Influence of Properties of Work Materials

The craters, as shown in Figure 7.1 and Figure 7.2, can be grouped in two

morphological groups. The SiC reinforced composite can be considered as group 1

(Figure 7.1) corresponds to high thermal diffusivity as compared to alumina

reinforced composites. Higher thermal diffusivity might have caused rapid

solidification of the molten metal. Therefore, comparatively smooth, shallow craters,

surfaces might have been produced in machining of these materials as compared to

alumina reinforced composites. The machined surfaces of alumina reinforced

composites, however, appear smaller in size and deeper in depth. The low thermal

diffusivity of these materials might have caused comparatively slow re-solidification

process. Further, low heat of fusion of the A359/SiCp MMCs might have caused

greater reduction in its fluidity as compared to the alumina reinforced composites.

Thus, based on the above discussions, following factors have been considered to

influence the surface characteristics of the machined composites.

• Removal of the ceramic particles (dislodged/remaining on the surface)

• Thermo-physical properties

• Type and properties of ceramic particulate reinforcements

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• Size of the ceramic particulate reinforcements

• Volume fraction of the ceramic reinforcements

• Probable chemical reactions between the matrix and reinforcements

• Fluidity of the molten material after the discharge on-time

Based on the EDX analyses the following mechanism/reactions of material removal

during WEDM process could have been happened:

1. Due to high temperature of the WEDM process, the matrix alloy (in both cases

of alumina and SiC reinforced matrix composites) might have melted and/or

evaporated.

2. The alumina reinforcements remain unaffected and may be removed by ‘drop

out’ mechanism of material removal after weakening of bond between matrix

and the reinforcements (the number is very low).

3. The un-removed alumina particles remain protruding on the machined

surfaces (large number).

4. The significant presence of these alumina particles on the work piece surface

might adversely affect the stability of the process due to unavailability of new

discharge location easily. This, thus, might cause repeated striking of series of

discharges on the same conductive spot (Tzeng et al. 2001; Pecas et al. 2003).

This arcing would produce deeper craters and, thus, worst surface roughness

due to cumulative effect of deeper craters and higher protrusions of particles.

5. The fluidity in alumina reinforced composites, thus, remains almost unaffected

due to negligible particulates in the melt.

6. In case of SiC reinforced MMCs, however, there are few possibilities:

a. The SiC particles might remain unaffected and can be removed by the

‘dropout’ mechanism.

b. These released particles affect the spark gap conditions and improve

the surface finish similar to powder-mixed-EDM due to discharge

channel dispersion, better spark transitivity and stable machining.

c. The fluidity of the melt reduces significantly due to presence of SiC

particles in the melt.

d. The SiC may react with the matrix and form Al4C3 compound at the

very high temperatures of WEDM process. This compound (Al4C3)

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reduces the fluidity of the molten material significantly (Lloyd, 1988).

However, this possibility might be ruled out in case of A359/SiC/10p

and A359/SiC/20p composites since no carbon was found on the

machined surfaces of these composites.

e. The carbon part of SiC reinforcement might be dissociated and then

vaporized at the high temperature environment of WEDM process.

Then only Al alloy and Si particles could be present on the machined

surfaces.

f. The probability of formation of oxide also cannot be ruled out. Oxide

formation would reduce the fluidity of the melt drastically.

g. Larger heat of fusion of A6061 as compared to A359 might have also

contributed to the greater fluidity of the alumina reinforced

composites.

Based on the above discussion and the EDX results, it can be said that the carbon has

been dissociated and the Si may remain in particle form in the aluminium alloy. The

presence of aluminium carbide has been assessed by X- ray diffraction analysis

(XRD). The results revealed no evidence of formation of aluminium carbide (Al4C3).

In addition, all the machined surfaces were found to show the presence of spinel

(MgAl2O4). This could be the cause of avoid of the reaction between aluminium and

carbon to form aluminium carbide (Yaghmaee and Kaptay, 2002; Lee et al., 2000).

The magnesium aluminium oxide layer may cover the silicon carbide and do not

allow any reaction between aluminium and SiC even at such temperature environment

of the WEDM spark gap. The absence of aluminium carbide causes undesirable

influence on the fatigue life, corrosion strength and fluidity of these composites.

However, in the present study, this compound was not found to form even at the high

temperatures of the WEDM process. These findings disagree with the recent findings

of Yue and colleagues on EDM and Electro-chemical discharge machining (ECDM)

of Al/SiC composites (Liu et al. 2010). Besides, the greater content of Si relative to

A359 alloy was found to agree with the findings of Seo et al. (2006). This finding also

suggests partial melting of the SiC reinforcements. The results of XRD analysis are

shown in Figure 7.7 to Figure 7.10. The detailed list of peaks is given in Appendix F.

Finally, it is believed that, the release of SiC and/or Si in the inter-electrode gap as

well as lower fluidity of the A359/SiC composites has contributed toward smooth

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surfaces of A359/SiC composites as compared to alumina reinforced composites. The

alterations in the gap conditions (discharge channel spreading and spark gap

widening) due to ceramic particles have reduced the depth of craters in the SiC

reinforced composites. The worst surface roughness of alumina reinforced composites

have been found to be attributed to the concentrations of sparks, poor transitivity of

the discharge channel and protrusions of ceramic particulates on the machined

surfaces.

Position [°2Theta]

20 30 40 50 60 70 80 90

Counts

0

1000

2000

3000

4000

SiC 10

Figure 7.7 XRD analysis of A359/SiC/10p composite

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Position [°2Theta]

20 30 40 50 60 70 80 90

Counts

0

200

400

600

SiC 20

Figure 7.8 XRD analysis of A359/SiC/20p composite

Position [°2Theta]

20 30 40 50 60 70 80 90

Counts

0

500

1000

SiC 30 WS

Figure 7.9 XRD analysis of A359/SiC/30p composite

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Position [°2Theta]

20 30 40 50 60 70 80 90

Counts

0

500

1000

1500

Alumina 20

Figure 7.10 XRD analysis of A6061/Al2O3/22p composite

7.2.3 Study of Recast Layer

A layer is formed by molten metal which is not flushed away by the dielectric, but

resolidifies on the sample’s machined surface during cooling. The properties of this

recast layer are critical in most of the engineering applications. The, integrity of

machined surfaces has become more and more important for the newly engineered

materials since they are being put to severe service conditions. In this section, the

study on the cross-section of the machined composites is presented.

The machined surfaces of A359/SiCp, and A6061/Al2O3p were investigated for the

presence recast layer, cracks, and any other surface defect. The investigations on the

recast layer were conducted by using scanning electron microscope. It has been found

that on-time and ceramic volume fraction have significant influence on the thickness

of the recast layer. Figure 7.11 show the recast layer on the machined surfaces of

A359/SiCp at different levels of pulse on-time.

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The presence of recast layer was significant on the A359/SiCp composites. Moreover,

the effect of pulse on-time was also found to show significant influence on the

thickness of the recast layer. It has been found that the thickness of recast layer

increases with increased on-time. It is known that the amount of molten metal which

can be flushed away by the dielectric is almost constant (Bozkurt et al., 1996).

Therefore, with increased on-time, since supplied energy is increased, the amount of

molten material also increases. The recast layer thickness, thus, was found to increase

with increased on-time. The thickness of recast layer was also found to be influenced

by the volume fraction of ceramic reinforcements. The thickness was found to

decrease with increased volume fraction of SiC/Si particulates. It might be attributed

to the SiC particulates released in the spark gap producing the powder-mixed WEDM

effect. During machining of high volume SiC reinforced MMCs, greater number of

particulates might be present in gap causing better dispersion of the spark resulting

into thinner recast layers as compared to lower volume of SiC reinforcements (Tzeng

and Chen, 2005; Syed and Kuppan, 2013). The decreased recast layer thickness was

found to increase with the reduced thermal conductivity of the work material of the

molten material. The change in the form of the recast layer, rather, was very

distinguishable in alumina and SiC reinforced composites. Thus, the type of

reinforcements was also found to show prominent influence.

The presence of significant recast layer on the machined surfaces of A6061/Al2O3p is

shown in Figure 7.12. It is evident that the pulse on-time influences the thickness of

the recast layer. The recast layer was found to vary with the volume fraction of the

alumina reinforcements. The prominent presence of alumina particles on the

machined surfaces of the A6061/Al2O3p composites could be the cause of increase in

the recast layer. This could be attributed to greater power density caused by spark

concentration relative to SiC reinforced MMCs.

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Figure 7.11 Recast layer of A359/SiCp MMCs

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Figure 7.12 Recast layer of A6061/Al2O3p composites

It can be observed in Figure 7.11 and Figure 7.12 that recast layer of silicon carbide

reinforced composites are significantly even as compared to the uneven layer of

alumina reinforced MMCs. This has found to be attributed to the presence of

significant number of Al2O3 particles on the machined surfaces of these MMCs. On

the other hand, the recast layer thickness of A359/SiC composites was found to less as

compared to A6061/Al2O3 composites. This was found to be attributed to the released

SiC particulates in the spark gap during machining of Al/SiCp MMCs.

Thus, finally, it can be stated that the thickness of the recast layer depends on the

pulse energy (pulse current & on-time), fluidity of the molten metal (volume fraction

and type of ceramic reinforcements), and properties and volume fraction of ceramic

reinforcements along with matrix properties. In addition, the effect of ceramic

particles (if present in the gap) on the gap conditions is also very influential.

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7.2.4 Surface Appearance and Defects

In this section, discussion on the observed defects on the machined surfaces is

presented. The high energy of the WEDM process induces various defects on the

machined surfaces of the metallic components. These defects include cracks, voids,

black patches, and bump marks in addition to surface softening. These defects have

been considered as the outcome of various process parameters including spark energy

and the electrode specific thermo-physical properties such as thermal and electrical

conductivities, melting temperature, boiling temperature, coefficient of thermal

expansion, heat of fusion and density of the cathode and anode materials. The surface

defects, in machining of MMCs, however, were found to be significantly influenced

by the type, size and volume fraction of the ceramic particulate reinforcements.

In the present study, the cracks, voids, pock marks and black patches were observed

on the machined surfaces. Moreover, particle pull-outs were observed in all types of

MMCs. Cracks were found to be induced due to high thermal stresses induced on the

machined surfaces due to rapid cooling of the molten metal. The cracks could also be

generated due to high electrical forces applied during the machining process. The

appearance of cracks, however, was significant on the machined surfaces of

A359/SiCp composites only. The machined surfaces of alumina reinforced composites

were found to be free from cracks. This finding agrees with some of the earlier studies

by various researchers (Brahmankar et al., 2000). The differentiating feature of the

machined surfaces of different MMCs might be attributed to the different types of

matrix materials. Since the matrix of SiC reinforced MMCs is a cast aluminium alloy,

the inherent defects in the cast material might be responsible for the occurrences of

cracks on the surface of A359/SiC MMCs. The observed cracks on the surfaces of

A359/SiCp are shown in Figure 7.13.

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Figure 7.13 a) Particle pullout, b) Cracks on machined surfaces of A359/SiCp

composites

Figure 7.14 Cracks on machined surfaces of A359/SiC/30p composites resembling

thermal spalling mechanism

The cracks observed on the machined surfaces of A359/SiC/30p could be attributed to

the thermal spalling mechanism of material removal, which is generally dominant

material removal mechanism in EDM machining of ceramic materials. The major

reason of this mechanical mode of material removal is very high melting temperature

of ceramic materials as well as poor performance of these materials in tension.

Although, the presence of electrically conductive aluminium alloy in the A359/SiC

composites determines the material removal mechanism in the present study, the

possibility of spalling cannot be completely ruled out in MMCs with higher volume

fraction of ceramic reinforcements such as in case of A359/SiC/30p. Recent

investigations in machining of Al/SiC composites using EDM and ECDM has also

claimed thermal spalling as the major material removal mechanism (Liu et al., 2010).

The type of cracks shown in Figure 7.14 has been observed on the machined surfaces

of A359/SiC/30p MMCs.

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In addition, voids, chimney, pock marks, re-solidified globules, and black patches

were observed on the machined surfaces of Al/Al2O3p. The black patches, attributed to

abnormal arcing, were, however, observed only on the machined surfaces of alumina

reinforced composites. This might be due to high arcing tendency during machining

of this material. Similar black patches were reported in the earlier studies on

WEDM/EDM machining of alumina reinforced aluminium matrix composites and

cemented carbides (Gadalla et al., 1992; Brahmankar et al., 2000; Mahdavinejad et

al., 2005).

The observed black patches are as shown in Figure 7.15. These patches have found to

be attributed to abnormal arcing. It was found, during machining, that arcing was very

frequent in machining of the alumina reinforced composites only. This difference in

the frequency of arcing might also be the cause for the lower cutting speed in

machining of the alumina reinforced composites.

Arcing is not desirable in WEDM since it could lead the process towards wire

breakage and also damage the machined surface. Arcing is determined by the

magnitude of the ignition delay time and it is either due to poor transitivity of

discharge channel or excessive debris in the gap and continuous repeated discharge at

the same spot or location. Low or almost zero ignition delay might result due to

highly contaminated spark gap and ease in initiation of discharge. The spark gap

contamination is determined by the volume of the molten metal in the previous pulse

and also the flushing efficiency of the process. However, the reason of arcing might

be unavailability of sufficient conductive path on the surface (due to protruding

alumina particles) as well as excessive debris, due to concentration of spark, in the

gap to assist easy ignition. Thus, the black patches appeared on the alumina reinforced

composites are attributed concentration of spark energy repeatedly on the same spot

or discharge location. In addition, it is also found to be attributed the low flushing

efficiency at relatively small gap size of the process in machining of this material.

This phenomenon of burning due to arcing was, however, not found on the machined

surfaces of SiC reinforced composites. This could be attributed to the relatively stable

machining conditions due to widening of the spark gap and dispersion of the

discharge channel caused by the presence of SiC/Si particulates in the inter-electrode

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gap. The burning marks are the evidence of abnormal arcing during machining these

materials. The EDS analysis further confirm this by the presence of carbon in the

vicinity of the black spots on the machined surfaces. It is interesting to note that these

black spots are located almost surrounding the alumina particles. This fact also

support the phenomenon of arcing caused by the discharge concentration due to poor

transitivity of the discharge channel caused by the shielding effect produced by

surrounding alumina particles.

Figure 7.15 Black patches on the machined surface of Al/Al2O3/10p

7.3 Cutting Rate The cutting rates were found to be significantly high in machining of A359/SiCp

composites as compared to the A6061/Al2O3p composites. This difference in the

cutting rates of these MMCs have found to be attributed to the thermo-physical

properties of the ceramic reinforcements (especially electrical resistivity), composites

materials, the matrix materials along with the gap alterations due to the presence of

different ceramic particulates in the MMCs.

The machining efficiency of the WEDM process depends mainly on the stability of

the process. The stability, generally, is attributed to the spark gap distance, effective

removal of debris from the gap and presence of debris in the gap to facilitate the

ignition at a larger spark gap (Wong et al., 1998). However, the role of debris is very

complicated. The absence of debris can result in arcing owing to the lack of a precise

feeding mechanism (or cause servo hunting). This happens in the initial stages of

ignition. On the other hand too much debris is, generally, believed to be the dominant

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cause of spark concentration (arcing) that leads to unstable machining (Luo et al.,

1997 and Mohri et al., 1991).

A stable machining process, however, demands evenly dispersed discharge locations

that depend mainly upon debris concentration and distribution. Therefore, gap debris

have been reported to have most significant effect on the discharge transitivity, gap

size, breakdown strength and deionization (Luo et al., 1997; Tzeng et al., 2001).

Based on the above discussion and knowledge, the following factors are, believed to

be, influential for significantly different cutting rates during machining of these

composites:

• The alumina particles were found to be unaffected during the process. These

insulating particles were found protruding on the machined surfaces. Thus, the

initiation of ignition might be difficult due to poor electrical conductivity of

alumina compared to SiC. Therefore, the transitivity and even dispersion of

the discharge channel could also be adversely affected. Thus, spark

concentrations, arcing and unstable process behaviour was obvious as

discussed above. The black patches shown in Figure 7.15 supports the

concentration of sparks adjacent to the alumina particles.

• Due to high protrusions of the alumina particles on the machined surfaces, the

flow of the molten matrix might have been impeded. This can also be seen

from Figure 7.2. This inefficient flushing might result into excessive

conductive molten material in the spark gap. During this type of gap

contamination, abnormal arcing may take place due to reduced or even no

ignition delay time. The control system of the WEDM machine may retract the

wire electrode back, in such situations, to avoid wire breakages by reducing

the supply current.

• The two conditions discussed above were observed frequently during

machining of the alumina reinforced composites. The process was not stable

during machining this type of material and the electrode retraction was

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frequently observed on the machine tool monitor. If the indicator shown

positive value, the gap is too large and the speed increases. Moreover, if it

shows a negative value, the gap is too short and the control action reduces the

wire forwards speed or retract the wire away from the work piece.

• Severe fluctuations in such gap status were observed during machining of

alumina reinforced composites especially at low pulse on-time (0.2 µs). This

could be attributed to the lack of debris in the gap to initiate the ignition and

insufficient energy to break down the dielectric strength. The servo might be,

therefore, hunting for the discharge location and also accompanied by spark

concentration when the spark is initiated.

• However, these fluctuations were not observed during machining of the SiC

reinforced composites. The process was found to be stable during the total

cutting length of these materials. The stability of SiC reinforced composites

have found to be attributed to the complete release of the SiC and/or Si

particles from the machined surface. These particles once released, could

remain in the gap to assist initiation of the next spark at a relatively large spark

gap. This is well supported by experimental studies on powder mixed EDM

process (Wong et al., 1998; Schumacher et al., 2004; Tzeng et al., 2001).

Moreover, earlier studies by Gatto (1997); Ramulu (2001) and Seo et al.

(2006) also reported similar results although the powder mixed effect was not

been discussed.

• The stability during machining of SiC reinforced MMCs was found to be

attributed to the increased gap size, effective removal of the debris, and thus

better transitivity of the discharge. Moreover, with the increased number of

SiC and/or Si particles released in the gap might cause greater stability of the

process.

Based on the above discussions, it appears that the SiC particles alter the gap status

favourably as compare to the alterations made by the alumina particles. It is possible

because the SiC particles have been easily removed in WEDM gap. The machined

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surfaces also support this easy removal of SiC particles as compared to the removal of

Al2O3 particles.

Therefore, finally, it can be concluded that the abnormal gap status and arcing is the

main cause of low cutting rates in machining of alumina reinforced composites. The

larger size of alumina particles might also be responsible for this significant

difference in the surface morphology as well as cutting rate.

7.4 Kerf Width

Although the difference is not very significant, as compared to the kerf width of SiC

reinforced composites kerf were found to be on lower side in alumina reinforced

composites. This could be attributed to the material properties, stability of wire

electrode, and wear of wire electrode. In addition, the discharge gap widening caused

by the presence of SiC/Si particles released in the spark gap has also been found to

influence the gap width. Thus, effects of material properties on kerf width might be

reduced by the widening of the spark gap. Although, the kerf width was expected to

be greater in case of A359/SiCp composites due to gap widening, the difference was

found to be very small. This could be attributed to reduced lateral gap at greater

cutting rates as observed in these composites compared to alumina reinforced MMCs.

7.5 Wire Electrode Breakages

The technologies of WEDM have grown rapidly in last two decades owing to the

requirement in various manufacturing fields. However, a few problems involved in

WEDM are still far from solved. Among them, wire breaking during machining

process is one of the serious problems in the application of WEDM. The occurrence

of wire rupture would result in a great increase of machining time, a decrease of

machining accuracy, and the deterioration of the machined surface.

If gap voltage is the feedback for the servo system to decide on the gap status and

consequently on the forward feed speed of the wire electrode, then it may fail in

conditions when the wire comes across non-conducting ceramic particles. This is

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explained like this: even at small actual gap width, the gap voltage sensor may not fed

back the real status of the gap when the gap is contaminated by a number of non-

conducting particles and therefore the system may fed the wire very rapidly after a

feedback signal of larger gap. This rapid forward speed of wire may cause the wire

electrode to collide with the work material (ceramic particles). This blind forward

feed of the wire electrode is termed as ‘blind feeding’. The collision of the blindly fed

wire electrode into the cluster of ceramic particles might lead to wire breakage.

If the spark gets a conductive aluminium alloy, instead of spark, an arc can be formed.

This arc, however, would lead to damaging effects on the electrode. In both these

cases, the wire breaks. This kind of behaviour was observed during machining of

alumina reinforced composites at low level of energy, i.e. at 0.2 μs on-time. The gap

was very much fluctuating and the cutting speed was not stable during machining of

alumina reinforced MMCs. This unstable wire forward feed is attributed to the

presence of non-conductive particles in the wire path, since the electrical resistivity of

alumina particulates is significantly higher as compared to that of SiC particulates.

Thus, although the servo voltage setting is selected as of that for steel or aluminium,

the chances of wire breakages are very high as the wire electrode is subjected to

greater heat due to spark concentration and arc leaving more molten aluminium in the

gap. The increase in the upper and lower flushing pressure during machining of

alumina reinforced MMCs could be the reason of this excessive gap contamination

causing abnormal arcing. Further, the colour of spark was also significantly abnormal

and deteriorated during machining of these MMCs. Therefore, one of the options is to

increase the value of servo voltage for machining of ceramic reinforced composites.

However, this will result in lower cutting speed and low productivity. Figure 7.16

shows the surface and end of the broken wire electrode. The broken part reveals a

fluid like nature of the wire surface due to excessive energy supplied to the wire

electrode due to abnormal arcing. Moreover, the EDS analysis reveals presence of

aluminium on the surface of the wire electrode. It supports the possibility of arcing

and even bridging of the electrode gap by the molten aluminium alloy caused by

concentration of spark energy at the same spot due to poor discharge transitivity

associated with the presence of insulating alumina particulates on the work surface.

The wire breakages, therefore, have been found to occur more frequently during

machining of alumina reinforced MMCs. Thus, it can be concluded that wire

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breakages, mainly, occur due to abnormal arcing and the role of mechanical failure

due to blind feeding was found to be insignificant. Therefore, to avoid wire breakages

in machining of ceramic reinforced metal matrix composites, abnormal arcing should

be avoided by maintaining proper feedback about the gap status as well as by proper

flushing of the gap.

Figure 7.16 Micrograph of broken wire electrode

Figure 7.17 EDS analysis of the broken wire electrode

0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00

keV

009

0

100

200

300

400

500

600

700

800

900

1000

Cou

nts

CK

aO

Ka

AlK

aCuL

lC

uLa

CuK

a

CuK

b

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7.6 Wire Electrode Shifting

Wire shifting is one of the major issues associated in machining of ceramic reinforced

composites. It affects the integrity of the machined surfaces adversely. The presence

of non-conducting ceramic particles such as silicon carbide or aluminium oxide was

considered as the major cause of wire shifting. Wire shifting leaves a bump mark on

the machined surfaces. This mark is undesirable and need to be addressed by

employing post processing. Wire shifting, therefore, has been identified as big

problem as breaking of wire electrodes during machining.

If the servo voltage is kept at high values and off-times are increased to avoid wire

breakages, the productivity is adversely affected due to long ignition delay time and

reduced pulse frequency. Longer ignition delay period leads not only to low

machining rate but also adversely affects wire electrode equilibrium. Over the years, it

has been accepted that wire electrode slackness takes place at low pulse frequency

and wire vibration is a problem at higher pulse frequency. The off-time contributes

toward the wire equilibrium and consequently wire shifting since it increases the

ignition delay time, reduces the pulse frequency and consequently increases the wire

slackness (Altpeter et al., 2004; Giandomenico et al., 2008). This unbalance of wire

electrode further leads to streaks and band marks on the work piece surface.

Wire shift, generally take place when the wire do not get any conductive path. In this

case, the wire search for conductive path and may get it before the front gap is too

short to form arc or collide with the insulating ceramic particles. Thus, the wire

follows a new path of least resistance. Moreover, this new path can only be found and

achieved if ignition is possible by break down of the insulated gap. In general, it has

been observed that the gap width must be smaller to allow the wire to find a new

conductive path (Yue et al., 1996; Altpeter et al., 2004; Giandomenico et al., 2008).

Moreover, the wire may also be able to find a new path if the open circuit or no-load

voltage is high enough to breakdown the dielectric strength. However, in machining

of particulate reinforced MMCs, the presence of ceramic particulates (SiC/Al2O3)

might also assist the ignition of new spark. Therefore, the shifting may require greater

ignition or open circuit voltage to overcome the insulating properties. In the present

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study also all wire shifting have taken place when the open voltage was set at high

value (100V and 120V) during the screening experiments.

Previous studies in machining of steel or other monolithic materials have reported the

phenomenon of wire shifting. The authors of these studies claimed that wire shift is

attributed it to the presence of non-conducting ingredients in the machined material

(Klocke et al., 2005). In the present study, the work piece materials are aluminium

matrix composites reinforced with SiCp or Al2O3p. The reinforcements of these

MMCs are electrically insulators. It is known that WEDM/EDM process can machine

only electrically conductive materials and insulators cannot be machined by WEDM.

Thus, it is believed that the concentration and focus of the supplied spark energy

remains on the conductive matrix material only.

The presence of the ceramic particles in the small machining gap may alter the status

of the inter-electrode gap. The alteration of the inter-electrode gap can be of different

types. Clustering of ceramic particles, in the spark gap, might increase the dielectric

strength of the spark gap. However, if they don’t form a significantly large cluster,

these particles might also assist ignition even at larger gap width.

This study has revealed the important fact that the number of occurrences of wire

shifting is significantly more during machining of SiCp MMCs as compared to

alumina reinforced composites. This is attributed to the release of SiC/Si particulates

in the inter-electrode gap. However, during machining of alumina reinforced MMCs,

the lateral ignition (wire shifting) was not found to be assisted due to the absence of

released alumina particles in the spark gap. Therefore, arcing and wire breakages were

found to be more frequent during machining of A6061/Al2O3p composites.

In the present study, based on the observations during machining process, the first

type of alteration of the spark gap is, believed to be, influencing the occurrences of

wire shifting. Significant change in the wire forward feed rate was observed and noted

during screening experiments of both types of composites. The change in the wire

forward feed rate was a negative change, i.e. the wire forward feed was found to be

reduced significantly for a fraction of moment. The location of wire, in the work

material, at time of reduction in the cutting rate was noted carefully. These machined

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samples were then carefully observed and also assessed by using Scanning electron

microscopy (SEM) for further investigations. Figure 7.18 show bump or band mark

on the machined surfaces. Figure 7.19 show the results of EDS analysis of these band

marks.

Figure 7.18 Band marks on a) A359/SiC/30p and b) A6061/Al2O3/22p composite

a)

b)

Figure 7.19 EDS of Band marks on a) A359/SiCp and b) A6061/Al2O3p composite

0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00

keV

001

0

100

200

300

400

500

600

700

800

900

1000

Cou

nts

CK

aO

Ka

AlK

aSi

Ka

0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00

keV

001

0

800

1600

2400

3200

4000

4800

5600

6400

7200

8000

Cou

nts

CK

aO

Ka

MgK

aA

lKa

CuL

lC

uLa

CuK

a

CuK

b

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Based on the observations made during machining experiments, and the study of

machined surfaces, these band marks have found to be attributed to the presence of

insulating ceramic particles in the machined composites. Finally, the following

sequences are thought to have taken place during machining of these samples.

• A cluster of ceramic particles might have come across the forward travelling

wire electrode during machining. This clustering could be due to high energy

in the discharge channel.

• The spark might not ignite when the wire electrode come across these

electrically insulating particles.

• The feedback system might send a misleading signal about the status of the

gap due to the insulating particles in the gap. The control action could then be

to reduce the forward feed speed of the wire electrode. However, although, the

lateral gap width is not small enough, at higher open circuit voltage the wire

may shift laterally by breaking the strength of the spark gap.

• The wire electrode now searches for conductive path of least resistance. At

this point of time, if the lateral gap width is low enough to overcome the

dielectric strength of the lateral gap, the wire may shift laterally due to

sparking laterally instead of front sparking.

• In other case, if the wire forward speed is increased due to the difference in the

actual gap voltage and the set value of the gap voltage, i.e. Aj, the forward

moving wire might collide with the work piece. This could be termed as ‘blind

feeding’ of the wire electrode. This collision, however, could be avoided if the

lateral gap is small enough to overcome its dielectric strength. In addition, the

presence of debris (SiC/Si) might also assist the lateral ignition.

• Increase in wire forward feed speed was found to take place in alumina

reinforced MMCs prior to wire breakages due to significantly higher electrical

resistivity of alumina particulates as compared to SiC particles. Thus, in SiC

reinforced MMCs, these released SiC and/or Si particles could assist the spark

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to initiate by formation of a bridge of relatively conductive path. Therefore,

the wire forwards feed was found to be reduced drastically prior to the wire

shifting.

The above sequences of actions taking places in the gap were also observed during

machining of these materials at certain level of process parameters. Based on these

observations the following parameters are found to be significant on the occurrences

of wire shifting.

• Pulse off-time

• Pulse on-time

• Open circuit voltage

• Wire tension

• Volume fraction and type of ceramic reinforcements

Thus, it can be, thus, concluded that pulse off time, servo voltage, on time and open

circuit voltage might be very influential on the phenomenon of wire shifting (Altpeter

and Perez, 2004; Schumacher et al., 2004). In addition, wire mechanical tension

contributes towards the wire vibration and wire slackness. Therefore, by counteracting

the wire slackness and vibrations, higher wire mechanical tension may help reducing

wire shifting.

7.7 Recommendations for strategy to machine MMCs

Based on the experiments, observations and literature survey, it has been found that

two major problems, wire breaking and shifting, arise during machining of ceramic

reinforced aluminium matrix composites. Therefore, it is necessary to develop entirely

separate machining strategy to machine these materials. The results show that the

pulse frequency may vary significantly during machining of MMCs. These significant

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variations might be attributed to the presence of entirely dissimilar phases of these

materials (metal and ceramic), and the significant difference in the thermo-physical

properties of the reinforcements and the metallic matrices. It is believed that the

presence of non-conducting ceramic particles, excessive molten material or almost no

debris in the spark gap lead to either wire shifting or to breakages of wire electrode.

The conservative machining setting to avoid wire breakages include longer off-time,

high servo voltage, greater wire speed, low wire tension and low pulse on-time.

However, at these machining settings the productivity and dimensional accuracy of

the machined components is lost. In addition, the integrity of the machined surface is

adversely affected due to shifting of the electrode wire at low wire tension, high open

voltage, short pulse on-time and longer off-time.

Based on the observations of the machining process, it has been found that ignition

delay time might be affected due to the presence of ceramic particles in the machined

materials. It was observed, during experiments, that the sparking frequency was too

low or rather negligible during machining at conservative machining settings such as

longer off-time, low on-time, and low wire tension. It is believed to be attributed to

the excessive time required to initiate the spark at some point of time and place during

the forward cutting motion of the wire electrode. As discussed earlier in the section of

wire shifting, these locations were noted and SEM investigations of such locations on

the machined surfaces were conducted. The SEM and EDX analysis of these specific

locations of the machined surfaces revealed that the presence of cluster of silicon

carbide was found to be excessive in A359/SiC composites. Similarly, the alumina

particles were found to be significant near the wire shift mark in the A6061/Al2O3

composites.

Therefore, the observed reductions (almost zero) in the cutting speed, the wire shift

mark at the location of the reduced wire forward speed and the presence of clustered

ceramic particles are, believed to be, interrelated and interdependent. The reduction in

the wire cutting speed is believed to be attributed to the changed gap status. The

ignition delay might be attributed to the presence of insulating ceramic particles in the

spark gap. Thus, based on the experimental setting during wire shift in the screening

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experiments, of the following conditions are believed to promote the shifting of wire

electrode:

1. Low Wire tension: at lower wire mechanical tension, the wire can shift toward

the lateral surfaces to find new path of least resistance for ignition. Thus, low

wire tensions assist the shifting of wire electrode.

2. Longer Pulse off-time: At longer off-times, the spark gap might be completely

flushed during the off-time. This might increase the spark gap dielectric

strength causing increase in the ignition delay time of the next spark. In

addition, wire electrode slackness is probable at low pulse frequency.

3. Higher Open circuit voltage: at higher open voltage, the spark can easily jump

on the side wall surfaces on the work material. Thus, even at wider spark gap,

the wire shifting is possible at greater open voltages. This is possible due to

small lateral gap width as compared to front gap width at significantly

moderate cutting speeds.

4. Longer Pulse on-time: at longer on-times, the removed molten material is

larger, thus, the possibility of longer ignition delay is reduced. Therefore, at

longer on-times, the wire shifting was, generally, not noted.

5. Greater volume fraction of ceramic particles: the frequency of occurrences of

wire shifting was found to be more in machining of MMCs with higher

volume fractions of ceramic reinforcements. It could be due to the ineffective

removal of these particles as well as their clustering in the gap or on the

machined surfaces during machining. Thus, the volume fraction of ceramic

reinforcements assists the increased ignition delay time and therefore the

shifting of wire. However, the electrical resistivity of the ceramic particulates

might have also caused the different gap status in these MMCs.

Similarly, the above mentioned factors also contribute toward the breakages of wire

electrode.

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1. High wire tension: it might cause breakages of the wire electrode due to high

tensile load at even higher temperature during machining. Further, at increased

ignition delay time, the wire may not shift and collide with the work material

(ceramic cluster) because of high mechanical wire tension. Thus, the greater

wire tension assists the wire breakages.

2. Longer pulse off-time: it may avoid the wire breakages by increasing the

ignition delay and consequently the reducing the pulse frequency. Thus, the

longer off-times assist to reduce wire breakages.

3. High open voltage: at high open voltage, the wire may find path along the side

wall as well as may also break the dielectric strength during machining. Thus,

the ignition delay could be reduced. In addition, the wire breakages could also

be reduced due to easier ignition at comparatively wider gap width. However,

at excessively high open voltage abnormal arcing or even bridging of the spark

gap by the molten metal and ceramic particles might cause severe wire

breakages. Thus, the open voltage little more than that employed for the

aluminium alloy should be used for aluminium MMCs.

4. Low pulse on-time: at longer on-times, the energy in the gap is greater.

Therefore, the wire breakages could be severe at these high values. Thus, low

on-times generally avoid wire breakages. However, in MMCs, the wire may

feed blindly in to the ceramic particles and collide at too low on-time. During

machining of the alumina reinforced MMCs, the concentration of the spark

energy due to poor discharge transitivity was found to assist the wire

breakages even at low on-times.

5. Lower volume fraction of ceramic particles: this will not alter the gap status

significantly. The wire breakages as well as wire shifting can be avoided with

the machining settings near to the settings recommended by the machine

manufacturer.

Although wire shifting and breakage found to pose limitations in machining of these

MMCs, they cannot be easily avoided by selecting a set of machining parameters due

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to random behaviour of the WEDM process as well as the random nature of the

ceramic particles in the work piece. Therefore, it is believed that a new machining

strategy is necessary to machine these materials. This strategy should take care of the

gap status and take corrective action during the machining process.

The major parameter identified to measure for determining the gap status is ignition

delay time. Based on the on-line measurement of the ignition delay time the status of

the gap could be interpreted and then corrective actions can be taken to avoid either

wire breakages or the wire shifting. The proposed machining setting, adjustable

parameters, for controlling the gap are open voltage, wire tension, pulse off-time,

pulse on-time, servo voltage, flushing pressure and wire speed. According to the

symptoms reflected in the variations of machining conditions during the wire shifting

and rupture process, based on the results obtained in this study and the experiences in

WEDM, a scheme is proposed to prevent wire breakages as well as wire shifting in

machining of ceramic particulate reinforced aluminium matrix composites. Figure

7.20 illustrates the flow chart of the scheme.

To apply this strategy, the ignition delay period is to be measured accurately and fed

back if the measured ignition delay time (td) is too short than the reference ignition

delay time frequency (Td) or less than the lower limit of the ignition delay time (TDL),

the discharge parameters at the "microseconds" order should be adjusted immediately

to decrease of discharging energy and pulse on-time to reduce the pulse frequency. In

addition, the off-time and wire mechanical tension should be reduced to avoid wire

breakages. Further, the flushing pressure and wire speed should be increased to

prevent wire breakages. The pulse on-time and short pulse time should be reduced

when the measured ignition delay is too small than the reference delay time. The

range of ignition delay time should be determined by doing extensive experimental

measurements of the delay time in machining of these composite materials.

If the ignition delay time is very long as compared to the reference delay time or

greater than the higher limit of the reference ignition delay time (TDH) to be

determined by experimental measurement of the ignition delay, a bad gap condition,

i.e. presence of nonconductive particles in the gap is encountered. In this case, wire

breakages due to “blind feeding” are possible. Moreover, wire shifting is also

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probable due to lateral sparking. If this state of process lasted for a relatively long

period of time, the open circuit voltage, flushing pressure, wire tension, wire speed

and short pulse time should be increased to avoid lateral shifting of the wire electrode.

In addition, parameters such as servo voltage, water conductivity and maximum no

load feed rate which have long time response on the process should be adjusted at

once to cope with the such bad gap condition. In both cases, the ignition delay time

should be kept within a certain range so that high metal removal rate can be achieved.

The present strategy can be further developed by doing extensive experiments and

collections of data related to peak current, ignition delay time, gap voltage and

machining frequency.

In addition, the application of the powder mixed dielectric also show promise in

machining of these MMCs. Appropriate powder and mixture may lead to successfully

avoid wire breakages as well as wire shifting in machining of such materials. A study

will need to correlate the ignition delay and powder mixture so as to improve the

process stability and performance.

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Figure 7.20 Flow chart of proposed strategy for machining of ceramic reinforced

MMCs.

START

INITIALIZATION

DATA INPUT

INCREASED: Flushing pressure, Pulse off-time, wire speed

DECREASED: Pulse on-time, Wire tension

IF td ≤ TDL

IF td ≥ TDH

YES

NO

INCREASED: Open circuit voltage, flushing pressure, pulse on-time, short pulse time, wire

tension and wire speed

DECREASED: Pulse off-time

YES

NO

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7.8 Conclusions

In this chapter, comparison on machinability of two different aluminium matrix

composites is reported. In addition, discussions on vital observations during

machining of these composites are presented. The critical issues such as wire

breakages and wire electrode shifting are discussed at length. A comparative study on

the machined surfaces of these composites is also presented. Finally, a machining

strategy, based on ignition delay time, is also proposed as one step towards

developing machining technology for ceramic reinforced metal matrix composites.

Based on this study, the following conclusions may be drawn:

• The WEDM performance of A359/SiCp and A6061/Al2O3p MMCs were found

to be significantly different. Although, melting and/or evaporation of

aluminium alloy matrix were found as the major material removal mechanism

in these MMCs, thermal spalling could be the reason of material removal in

A359/SiC/30p composite.

• Cutting rate and surface finish were found to be better in machining of

A359/SiCp as compared to WEDM of A6061/Al2O3p composites. This was

found to be attributed to the better stability of the process during machining of

SiC reinforced composites. The observed stability in machining of this type of

MMCs could be due to gap widening, discharge channel spreading and

relatively better transitivity of discharge channel as compared to alumina

reinforced composites.

• The skewness parameters of machined surfaces of A359/SiCp and

A6061/Al2O3p have found to be significantly different exhibiting the release

and/or partial melting of SiC and protrusions of unaffected alumina

particulates.

• In A359/SiCp MMCs the surface roughness was found to reduce with

increased volume fraction of SiC particles. However, surface roughness was

found to increase with increased volume fraction of the alumina particles in

A6061/Al2O3p composites. The combined effect of deeper craters caused by

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spark concentration and the height of the particulate protrusions was found to

increase the roughness of A6061/Al2O3p composites with increased ceramic

volume fraction.

• Significant presence of recast layer was found on the machined surfaces of

both types of MMCs. Thickness of recast layer was found to be attributed to

pulse on-time and volume fraction of ceramic reinforcements. Moreover, the

recast layer was found to be very even in A359/SiCp composites as compared

to the uneven recast layers found in A6061/Al2O3p MMCs.

• Defects such as pock marks, cracks, voids and black patches were found on

the WEDM machined surfaces of these MMCs. However, A359/SiCp MMCs

were found free from the black patches and cracks were not found on the

machined surfaces of A6061/Al2O3p composites. This was found to be

attributed to the stable machining conditions during machining of SiC

reinforced MMCs. On the other hand, the concentration of spark energy due to

poor discharge transitivity caused severe arcing resulting in black patches was

found in case of alumina reinforced MMCs.

• Wire breakages were found to pose limitations on the cutting speed in

machining of these composites. The wire breakages were found to be severe

during machining of A6061/Al2O3p composites as compare to A359/SiCp

MMCs. The wire breakages were found to be attributed to the abnormal arcing

caused by the presence of insulating ceramic reinforcements on the work

surfaces (alumina). These particles have been found to resist the discharge

channel to form causing concentration of spark at the same spots. The

significant difference between the thermal and electrical properties of

aluminium matrix and the ceramic reinforcements was found to be responsible

for the frequent wire breakages during machining of these materials.

• Wire shifting was found to deteriorate the machined surfaces of both types of

composites. The number of occurrences of wire shifting was found to be more

in machining of A359/SiC/30p composites. The presence of ceramic particles

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in the inter-electrode gap and/or machined surface was found to be responsible

for the shifting of the wire electrode.

• On-time, off-time, open voltage, wire speed, and wire tension were found to

influence the phenomenon of wire breakages and wire shifting. It was also

attributed to the volume fraction, size, and type of ceramic reinforcements and

thermo-physical properties of these composites.

• To successfully machine these MMCs a new strategy is proposed. Ignition

delay time is proposed as the measure of the status of the inter-electrode gap.

• Wire breakages could be reduced by reducing the on-time, open voltage, wire

tension and by increasing flushing pressure, and wire speed.

• Wire shifting was found to be avoided by increasing the on-time, wire tension,

and flushing pressure. Moreover, it can be avoided by reducing the open

voltage and wire speed.

• The range of variations of these process parameters would, however, be

determined on the basis of ignition delay time. Therefore, to determine the

range of ignition delay time, to avoid wire breakages as well as wire shifting,

extensive experimentation and measurements of ignition delays during

machining these materials is necessary.