cereals & grains

Analytical Instruments Sales & Service: +43 1 877 54 55-0 [email protected] 1

Analytical Instruments

CEREALS & GRAINS

05/2012

AUSTRIA BULGARIA CROATIA CZECH REPUBLIC HUNGARY POLAND ROMANIA SERBIA SLOVAKIA SLOVENIA


2 [email protected] Sales & Service: +43 1 877 54 55-0

Your NOACK Contact

AUSTRIA NOACK & CO AG Auhofstraße 190 1130 Wien, Österreich Tel.: +43 1 877 54 55 - 0 Fax: +43 1 876 54 43 E-mail: [email protected]

POLAND NOACK Polen sp. z.o.o. Ul. Królowej Marysieńki 50 02-954 Warszawa, Polska Tel.: +48 22 853 45 80 Fax: +48 22 853 77 26

HUNGARY NOACK Magyarorszag Kft. Budaörsi ut 131/B Fsz.1 1118 Budapest, Hungary Tel.: +361 246 65 27 Fax: +361 246 69 30

CZECH REPUBLIC NOACK CR, spol. s.r.o. Pacajevova 934/32 149 00 Praha 4 Czech Republic Vídeňská 122 Brno, 619 00 Czech Republic Tel.: +42 05 334 39 721 Tel.: +42 02 679 13 415 Fax.:+42 02 729 10 092

CROATIA NOACK d.o.o. Vodovodna 20 A 10000 Zagreb, Croatia Tel.: +385 1 369 20 10 Fax: +385 1 369 20 11

BULGARIA NOACK BULGARIA LTD Str.Tintyava 13 A 1113 Sofia, Bulgaria Tel.: +359 2 971 22 81 Fax: +359 2 971 38 62

ROMANIA S.C. NOACK Romania S.R.L. Str. Ion Urdăreanu, nr.34, et.5, Sector 5 050688 Bucuresti, Romania Tel.: +40 21 317 66 70 Fax: +40 21 316 66 58

SLOVAKIA NOACK Slovakia s.r.o. Radiova 38 82104 Bratislava 2, Slovakia Tel.: +42 12 434 116 31 Fax: +42 12 434 116 32

SERBIA NOACK & CO South East d.o.o. Stevana Musica 17, App. 17, Fl.5 21000 Novi Sad, Serbia Tel.: +381 21 533 220 Fax: +381 21 533 230

Sales & Service: +43 1 877 54 55-0 [email protected]

CONTENT Analysis of CEREALS & GRAINS

Cereals, Grain, Flour, Dried Fruits, Feed & Forage

NIR-Online – Process control and optimization 4

NIR-Online – Flour Production 8

NIR-Online - Feed 11

AgriQuant A1, B1 12

AgriQuant B1 for Soy Raw Material 14

AgriQuant for Forage 17

AgriQuant B1 for Pig Feed 19

AgriQuant B1 for Cattle Feed 21

FoodQuant B2, B3, B4, B5 23

FoodQuant B3 for Flour 25

AgriCheck™ & AgriCheck Plus 27

MultiCheck™ - Versatile NIR Analyzer 29

OmegAnalyzer G™ - Whole Grain & Oilseed Analyzer 31

humimeter FS4 – Grain moisture meter 33

Please note, that not all products listed in this brochure are distributed by NOACK in all countries. Please consult with your local NOACK contact person.


4 [email protected] Sales & Service: +43 1 877 54 55

NIR-Online – Process control and optimization

Planning, consulting, installation – all under one roof

The perfect solution for controlling, optimizing and documenting

Perfect planning and process integration

Good advice – from the start and whenever it’s needed

Fast and secure installation without downtime



The system: powerful, innovative Technology which optimises production processes Smooth running processes need systems, which can always be relied on. From planning through to realization, you can trust on NIR-Online and be rewarded with maximum return and innovative quality assurance. Whether you analyze foodstuffs, animal feed, chemicals or pharmaceuticals – the same high standards apply to each branch of industry. There is no room for compromise on quality and cost. Whoever invests in optimizing processes must be sure of enjoying consistent, reliable high product quality in return; all this with calculable costs and no extended downtime. The NIR-Online system can be integrated smoothly in all current ERP and process control software, works well through all interfaces and offers maximum process transparency and documentation. The system adjusts the quality to fall in line with new processes and process changes. You will always be able to meet the ever higher demands being presented by the market. Place your trust in a system, which will always be there for you – in all phases of production.

What counts: security, efficiency Your investment in consistent, high product quality The NIR-Online system accompanies processes in their entirety; it reliably controls the raw materials to be processed, monitors production process and subsequently checks the end product. Secure a decisive advantage in your market – reduce costs, avoid downtime, increase product quality, and in doing so, cement long term customer relationships.




A system which excludes errors from the start With the NIR-Online system, you can define and optimize mixing ratios in your laboratory, meaning

you can create the best possible products for your customers. You can conduct small scale experiments on later large scale production goods. Your laboratory can test liquids and pastes, as well as solid and viscous materials with NIR-Online. The system removes quality fluctuation from production processes, enabling constant process monitoring and real-time control. Automatic documentation and the inclusion of measured data in the current process control system guarantee 100% traceability. Manual sampling is rendered unnecessary, product and consumption optimization are ensured and complaints are prevented. The many advantages of the NIR-Online System are plain to see.

1. Automatic determination of product homogeneity

Values are calculated without calibration by means of real-time measurement of spectral variation. The graph shows the extent of the variation and the reduction from the mixing process through to the end product.

2. Fast fingerprints for quality control Current measured spectra are compared with known spectra in a database, enabling you to determine the ideal end point of a mixing process. The exact conformity with recipe components can be verified at the same time.

3. Quantitative and qualitative regulation Initially, a calibrated spectral analysis of the individual components is carried out. This more complex method ensures that the conformity of quality and quantity of the recipe components. 100% quality is guaranteed.

NIR-Online is the intelligent, efficient and cost-effective solution for all production and processing companies. Control, correct and document – this leads to: optimized production processes. The integration into both planned and existing systems is quickly completed. NIR-Online will improve your production – effectively and for the long term. Reduce costs and opt for precise product quality. For 100% satisfied customers.



X-ONE (NIR) X-FIVE (VIS) X-THREE (NIR/VIS)

Durable A system equipped with automatic referencing and redundant light source. It gives you 2 years of continuous operation – without maintenance! The use of a diode array spectrometer enables you to achieve superior rapidity of measurement with a high level of accuracy, even with fast moving samples.

X-TWO (NIR/CCD) X-FOUR (NIR/VIS/CCD)

Innovative This innovative system can additionally boast a high resolution color camera, which measures even the most fractional differences in color, structure and size. As such, you are able to determine both outward characteristics and chemical properties, which can then be displayed in whatever form you may choose.

SX-SUITE Outstanding The SX-SUITE software lets you monitor processes all the time, whilst also enabling you to control and optimize in real-time; all this, with outstanding user friendliness. Simple integration of measured data and automatic documentation guarantee 100 % traceability; manual sam-pling and gaps in process monitoring are condemned to the past. Effective consumption optimization and process standardization pave the way to your commercial success.

Typical Specifications

Ex protection from explosion class

1/2 G & D T80 °C

Stainless steel housing IP65

Operating pressure: 30bar

Dimensions: 200x220x135mm, 7kg

Optical reference surface Ø 40mSupply: 12V, 2A

Interfaces: Bluetooth™ up to 10m, RS232, RS422 up to 2km

MTBF > 18 000 hrs.

Measurement period ~ 10ms

CCD colour camera / X-TWO / X-FOUR

Software Windows Vista / Windows XP

DA-spectrometer: 350 to 920nm and/or 950 to 1750nm

Vibrations: 0.2G at 0.1 to 150Hz.

Ambient temperature: -10 to 40 °C Relative humidity: <90 %, non-condensing



NIR – ONLINE

Flour Production

Flour production with complete security and transparency

Grain receive

When grains are delivered to a mill the first analysis of the previous sample is done by the laboratory system X-Rot and afterwards by the process analyser of NIR-Online GmbH. Reflections vary according to quality of grains in near infra red (NIR) spectra. Moisture, protein and other ingredients are directly shown as data and graphs by the NIR-Online software SX-Suite. Contamination, foreign grain and even ergot can be identified by using an additional integrated camera. If deviations are noticed the delivery is stopped immediately, if grains are accepted they are stored selectively according to their quality parameters.

Same NIR technique in laboratory and production

Identical calibrations in laboratory and production

Control by NIR and VIS spectra and picture analysis

Segregation according to quality in grain acceptance

Automatic sampling even for storage samples

Mixture before first lead shot

A certain flour type is produced by drawing the necessary charges from the silos, mixed and tempered accordingly with scales. After some hours of holding time the first lead shot is made controlled by a NIR-Online process analyser with colour camera. This ensures a complete control of the grain mixtures.

Controlled draft and mixing from silos

Automatic adjustment of mixture for protein and/or water

Control and dosage of sprinkled water on grains (tempering)

Huge time saving of holding time


NIR – ONLINE

Flour Production

Flour production and milling A NIR-Online process analyser with camera controls the quality of flour during its production. Especially the ash value is an important quality feature for mills. The presetting in software secures the production of the designated flour according to DIN rules. If deviations are noticed the system readjusts via dosing screws. Report function of the software delivers extensive data for tracking production processes.

Implementation of passage control is optional

NIR and VIS spectra deliver maximum accuracy for ash

Speck control with CCD camera

Flour blending according to ash is possible

Documentation according to current GMP rules

Integration of measured data in all control systems Time invariant

Laboratory measurements

A parallel implementation of a NIR-Online device in the laboratory of the mill ensures usage of the same calibration in production and laboratory. The analyser in the lab mainly measures previous samples and average samples but may also be used for new grain types and special customized flours. Final quality control of goods before dispatch is ensured.

Maximum security and quality standards

Complete reports for the mill management (traceability)

Customer may choose stage of automation

Safe-guarding of delivery

Stable flour quality



NIR – ONLINE

Flour Production

Facts about the NIR-Online process analyser:

Dimension (WxLxH) only 200 x 220 x 135mm

Robust stainless steel case IP 65

Multi parameter analysis

Information in milliseconds

Whole grain and flour measurements

Easy sample presentation

Calibrations inclusive

4 cm diameter spot size

W-Lan, profibus, CAN-Bus

Your benefits:

Optimized production processes and gapless quality control Unique and patented combination of NIR-, VIS- und CCD technology Real-time measurement Consistent high product quality Maximum accuracy for ash Process transparency and documentation Real-time monitoring from intake of raw materials (grain) to finished product Speck control with CCD camera, detection of impurities Save costs through defining and optimizing the mixing ratios and recipes Return of investment in a very short time Automatic calibration

Device and automatic calibration function are patented

X-Four system with automatic sampler in a mill. Patented combination of NIR / VIS and camera

Easy installation

XML - / batch report, QC Journal

Automatic calibration function

Redundant light source

ATEX certified

Dust protected

Temperature stabilized

No optical fiber


NIR –ONLINE

Feed

FEED – Raw material intake and production control

Unique and patented combination of NIR/VIS and CCD measurements

Real-time quality control from raw material intake to the finished products

Same NIR-technology in laboratory and production

Optimized production process

Ensure reliable high product quality

Maximum process transparency and documentation

Save costs through optimizing mixing ratios and recipes

Automated calibration Products

Raw material Mixed feed Pet food Silage

Grain Fish feed Dog feed Gras

Canola Pig feed Bird feed Hey

Soja Cattle feed Rodent feed Alfa alfa

Sunflowers Poultry feed Cat feed Corn

Corn Horse feed S.A.feed

Properties and Parameter

Ash pH value Fat/Oil NDF

Fibre Amino acids Starch Moisture

Colour Sugar Ethanol Protein

11 [email protected] Sales & Service: +43 1 877 54 55-0



AgriQuant A1, B1

Optimized sampling solutions

Exceptional spectral performance

No scheduled maintenance, low cost of ownership

Powerful software package with InfraQuant and Horizon QI The light source in the AgriQuant has an expected lifetime of 10 years

and the laser has even longer expected lifetime

Substantial amount of starter calibrations through Quantum calibration

program

Spectroscopic Performance (typical, at 25 °Celsius with InAs detector)

Spectral Range 3,700 to 14,885 cm-1

Signal to Noise (60 s, 16 cm-1, at peak response) > 500 000: 1

Frequency Repeatability (@ 7300 cm-1) < 0.006 cm-1

Frequency Accuracy (@ 7300 cm-1) < 0.01 cm-1

Absorbance Reproducibility (toluene) < 0.002 AU

Optical Bench

Beamsplitter Material ZnSe (non-hygroscopic)

Interferometer Mechanism (patent pending) High-throughput double pivot

Michelson, fully jacketed

Source (with electronic stabilization) Quartz Halogen, 10-year expected life

Solid-state Laser Maintenance Free


AgriQuant A1, B1

The AgriQuant is based on the latest FT-NIR technology from ABB Bomem, the world leader in FT-NIR technology. The equipment combines exceptional performance with low cost of ownership.

AgriQuant A1 has been developed for the analysis of heterogeneous samples with special requirements e.g. soil, where there is a high demand for the sensitivity of the detector. Sampling: The sample is analysed on the QIA1020 accessory. The sample is analysed by reflection measurement in 125ml glass jars with lids. The glass jar rotates during analysis providing representative sampling, making sure the sample is constantly mixed and reducing the effects of product heterogeneity. The glass jar has a large opening for easy filling. The lid ensures that the sample is stored under stable conditions and that influence from the surroundings is minimised. After analysis the glass jar can be safely sent to reference analysis or stored. The glass jar can be cleaned and reused many times. Keeping the cost per analysis very low. There is plenty space on the glass jar for barcode labels. The barcode is easily read by a barcode reader connected to the AgriQuant A1 system.

AgriQuant B1 has been developed for the analysis of heterogeneous samples e.g. feed and forage, but many other products can be analysed on the AgriQuant B1.

Sampling: The sample is analysed on the QIA1020 accessory. The sample is analysed by reflection measurement in 125ml glass jars with lids. The glass jar rotates during analysis providing representative sampling, making sure the sample is constantly mixed and reducing the effects of product heterogeneity. The glass jar has a large opening for easy filling. The lid ensures that the sample is stored under stable conditions and that influence from the surroundings is minimised. After analysis the glass jar can be safely sent to reference analysis or stored. The glass jar can be cleaned and reused many times. Keeping the cost per analysis very low. There is plenty space on the glass jar for barcode labels. The barcode is easily read by a barcode reader connected to the AgriQuant B1 system. Workstation The AgriQuant comes with an external computer, which enables the use of a range of add-ons, offering the user maximum flexibility, e.g. touch screen, label printer and barcode reader. The external PC enables rapid upgrade on-site, this reduces any downtime of the equipment to a minimum. The AgriQuant is supplied with a powerful software: InfraQuant 2.5 (easy to use FT-NIR QC software, to collect, present and handle analytical results) and Horizon QI offering a series of strong spectroscopic tools.



AgriQuant B1 for Soy Raw Material




Powerful software package with InfraQuant and Horizon QI


AgriQuant B1 for Soy Raw Material

Production of animal feeds requires precise control over the different raw materials used. NIR analysers have

widely replaced the traditional methods, since they can run a large amount of samples in a short time. The NIR

analyser is to be placed either in the lab or in the production area and can be operated by plant personnel. The

AgriQuant B1 is a versatile FT-NIR analyser that will deliver analysis results for your soy samples in less than one

minute.

Analyser: AgriQuant B1 The AgriQuant B1 is based on the latest generation FT- NIR technology and has the following main features: • Cutting edge spectral performance and best signal to noise ratio on the market • Very easy to operate and maintain • Strong software package with InfraQuant and Horizon QI • Very low maintenance costs. The AgriQuant B1 has no scheduled maintenance and the light source has an expected lifetime of 10 years.

Analysis: The sample is analysed by reflection measurements in 125ml glass jars with lid, which are rotating during analysis. By rotating the glass jar the sample is constantly mixed ensuring representative sampling and that effects from product heterogeneity are reduced.

The glass jar has a large opening for easy filling. The lid ensures that the sample is stored under stable conditions

and protected from influence from the surroundings. After analysis the sample is easily stored or send to

reference analysis. If many samples have to be analysed, the size of the glass jar has plenty of space for a

barcode. The barcode is easily read with a barcode reader connected to the AgriQuant B1.

Calibration The AgriQuant B1 is calibrated against certified methods for the different components.

The NIR region contains both combination and overtone information. The most sensitive bands are those derived

from the O-H, N-H and C-H stretch regions. To compensate for path length changes due to scattering effects

from the sample, all spectra were pre-processed using Multiplicative Scatter Correction and mean centring. A

Partial Least Squares (PLS) model was developed based on the analytical and spectral data.

Calibration Performances, Examples Table 1 shows the performance of the calibrations developed for all the components with chemical reference analysis available.

Conclusion The AgriQuant B1 is a strong FT-NIR analyser for soy raw material, supplying results in less than one minute for multiple components. With the AgriQuant B1 you can eliminate individual analysis on each constituent and save on manpower, training and time. The AgriQuant can be placed in the lab or in the factory. The intuitive InfraQuant software guides the plant personnel through the steps of the analysis and the results are displayed with easy to understand color codes. With barcode option it is possible to measure many samples each hour making the AgriQuant B1 an excellent choice for the feed factory or lab.

Property Range % NIR SECV

Unground

NIR SECV

Ground -

Petri dish

Protein 36 – 49 0.70 0.50

Fat 2 – 25 0.63 0.40

Ash 4.2 – 6.8 0.29 0.33

Raw Cell Matter

2.5 – 7.0 0.72 0.67

Moisture 8.50 – 13.0 0.30 0.20

Density 0.57 – 0.74 0.02 0.02

Table1: Performance of the soy raw material calibrations



AgriQuant for Forage






AgriQuant for Forage

Forage - grass and maize silage - is widely used for feeding cows, and it is mandatory to know all the major components and the feeding value of these products. NIR analyzers have replaced most of the traditional methods, since they can run a large amount of samples in a short time, either manually or automated. The analysis time per sample is less than one minute.

Analyser: The FT-NIR AgriQuant The AgriQuant FT-NIR analyser is used for non-destructive analysis of heterogeneous agricultural samples. The pretreated sample is filled into the lidded glass bottle and placed on the accessory. To ensure consistency and analysis of a large amount of the sample, the sample is mixed during analysis. The sample can be kept due to the sealed bottle. The AgriQuant is powered by the latest ABB Bomem FT-NIR technology and measures the entire spectrum of the sample, i.e. in the range 14000-3800 cm-1 (700-2600 nm). It generates a large amount of high-quality spectral data, which makes it possible to precisely determine multiple components.

With no scheduled maintenance for five years, the AgriQuant is practically maintenance-free. It is equipped with parts with a long lifetime. For instance, the laser and NIR source have an expected lifetime of ten years. AgriQuant is operated with the InfraQuant software, which makes it easy for everybody to work with analyses. Two clicks with the mouse is enough to make the analysis. Among the features is a wizard that guides the operator through the program, spectra are displayed right away, and sample information and trends can be reviewed easily.

Calibration The AgriQuant is calibrated against certified methods for the different components. The NIR region contains both combination and overtone information. The most sensitive bands are those derived from the O-H, N-H and C-H stretch regions. Different pre-processing has been used for the different components, typically mean centring and manual base line correction – sometimes 2nd derivative (Savitsky-Golay). A Partial Least Squares (PLS) model was developed based on the analytical and spectral data.

Calibration Performances – Example 60 samples of dried maize and 70 samples of dried grass have been used for the modelling. The material has been ground and put into glass bottles. Table 1 shows the performance of the calibrations developed for all the components with chemical reference analysis available. Repeatability test has been done with a sample of grass measured 5 times.

Conclusion The AgriQuant FT-NIR analyser is designed for analysing forage and feed. The bottled sample is fixed during analysis to see a large amount of the sample, which will lead to reliable and stable results. The results are obtained in less than one minute on multiple components. This eliminates individual analysis on each constituent and saves manpower, training and time. The analysis can be automated using transport belt, bar code reader or radio frequency tagging.

Grass Range % NIR SECV Repeatability

Protein 6-27 0.69 0.07

Fibre 17-38 0.89 0.08

In Vitro 52-84 1.84 0.54

Sugar 0.2-18.3 0.90 0.12

NDF 29-68 1.54 0.12

ADF 21-40 1.12 0.16

pH 4-5.4 0.094 0.022

Lactic Acid 1.2-13.8 0.62 0.072

Acetic Acid 0.9-3.5 0.27 0.078

Ammonium No. 0.06-0.3 0.030 0.003

Maize Range % NIR SECV Repeatability

Protein 6-10 0.37 0.08

Fibre 14-34 0.73 0.07

In Vitro 62-80 1.52 0.48

Starch 1-38 1.28 0.11

NDF 30-64 1.38 0.16

ADF 18-31 0.76 0.15

pH 3.7-4.1 0.072 0.018

Lactic Acid 2.7-7.2 0.43 0.064

Acetic Acid 1-4.4 0.26 0.077

Ammonium No. 0-0.11 0.008 0.003

Table 1: Performance of the dried forage calibrations



AgriQuant B1 for Pig Feed






AgriQuant B1 for Pig Feed

Production of pig feed requires precise control over the different components based on the final

product specifications. NIR analysers have widely replaced the traditional methods, since they can run

a large amount of samples in a short time. The AgriQuant B1 can be placed in the production area and

be operated by plant personnel. The AgriQuant B1 will deliver analysis results for your pig feed

samples in less than one minute.

Analyser: AgriQuant B1 The AgriQuant B1 is based on the latest generation FT- NIR technology and has the following main features: • Cutting edge spectral performance and best signal to noise ratio on the market • Very easy to operate and maintain • Strong software package with InfraQuant and Horizon QI • Very low maintenance costs. The AgriQuant B1 has no scheduled maintenance and the light source

has an expected lifetime of 10 years.

Analysis: The sample is analysed by reflection measurements in a 125ml glass jar with lid, which is rotating during analysis. By rotating the glass jar the sample is constantly mixed, ensuring representative sampling and that effects from product heterogeneity are reduced. The glass jar has a large opening for easy filling. The lid ensures that the sample is stored under stable conditions and protected from influence from the surroundings. After analysis the sample is easily stored or send to reference analysis. If many samples have to be analysed, the size of the glass jar has plenty space for a barcode, which is easily read with a barcode reader connected to the AgriQuant B1

Calibration The AgriQuant B1 is calibrated against certified methods. The NIR region contains both combination

and overtone information. The most sensitive bands are those derived from the O-H, N-H and C-H

stretch regions. In order to compensate for path length changes due to scattering effects from the

sample, all spectra were pre-processed using Multiplicative Scatter Correction and mean centring. A

Partial Least Squares (PLS) model was developed based on the analytical and spectral data.

Calibration Performances Table 1 shows the performance of the calibrations developed for all the components with chemical reference analysis available. Repeatability tests were performed measuring the same sample 10 times. Performance was tested using a set of 18 unknown samples calculating the SEP (Standard Error of Prediction) value.

Conclusion The AgriQuant B1 is a strong FT-NIR analyser for pig feed, supplying results in less than one minute for multiple components. With the AgriQuant B1 you can eliminate individual analysis on each constituent and save on manpower, training and time. The AgriQuant B1 can be placed in the lab or in the factory. The intuitive InfraQuant software guides the plant personnel through the steps of the analysis and the results are displayed with easy to understand color codes. With barcode option it is possible to measure many samples each hour making the AgriQuant B1 an excellent choice for the feed factory or lab.

Property Range % NIR SECV

Ungrinded

Repeata-

bility

SEP

Protein 13 – 21 0.60 0.20 0.60

Fat 2.5 – 8.5 0.39 0.13 0.48

Starch 17 – 45 1.70 0.70 2.2

Sugar 3.5 – 12 0.50 0.20 0.60

Ash 4 –8 0.26 0.14 0.41

Raw Cell Matter 2.5 – 11 0.54 0.28 0.36

Moisture 10.5–14.5 0.20 0.10 0.30

Density 0.53 –0.67 0.02 0.01 0.02

Phosphorus 0.3 – 0.75 0.04 0.02 0.04

Table1: Performance of the pig feed calibrations



AgriQuant B1 for Cattle Feed






AgriQuant B1 for Cattle Feed

Production of cattle feed requires precise control over the different components based on the final product specifications. NIR analysers have widely replaced the traditional methods, since they can run a large amount of samples in a short time. The AgriQuant B1 can be placed directly in the production area and be operated by plant personnel. The AgriQuant B1 will deliver analysis results for your cattle feed samples in less than one minute.

Analyser: AgriQuant B1 The AgriQuant B1 is based on the latest generation FT-NIR technology and has the following main features: • Cutting edge spectral performance and best signal to noise ratio on the market • Very easy to operate and maintain • Strong software package with InfraQuant and Horizon QI • Very low maintenance costs. The AgriQuant B1 has no scheduled maintenance and the light source

has an expected lifetime of 10 years.

Analysis

The sample is analysed by reflection measurements in a 125ml glass jar with lid, which are rotating during analysis. By rotating the glass jar the sample is constantly mixed ensuring representative sampling and that effects from product heterogeneity are reduced. The glass jar has a large opening for easy filling. The lid ensures that the sample is stored under stable conditions and protected from influence from the surroundings. After analysis the sample is easily stored or send to reference analysis. If many samples have to be analysed, the size of the glass jar has plenty of space for a barcode, which is easily read with a barcode reader connected to the AgriQuant B1.

Calibration The AgriQuant B1 is calibrated against certified methods for the different components. The NIR region contains both combination and overtone information. The most sensitive bands are those derived from the O-H, N-H and C-H stretch regions. To compensate for path length changes due to scattering effects from the sample, all spectra were pre-processed using Multiplicative Scatter Correction and mean centring. A Partial Least Squares (PLS) - model was developed based on the analytical and spectral data. Calibration Performances – Example Table 1 shows the performance of the calibrations developed for all the components with chemical reference analysis available.

Conclusion The AgriQuant B1 is a strong FT-NIR analyzer for cattle feed, supplying results in less than one minute for multiple components. With the AgriQuant B1 you can eliminate individual analysis on each constituent and save on manpower, training and time. The AgriQuant B1 can be placed in the lab or in the factory. The intuitive InfraQuant software guides the plant personnel through the steps of the analysis and the results are displayed with easy to understand color codes. With barcode option it is possible to measure many samples each hour making the AgriQuant B1 an excellent choice for the feed factory or lab.

Grass Range % NIR SECV Ungrinded

Corr. Coefficient

Protein 14 – 38 0.80 0.99

Fat 2 – 10 0.45 0.89

Starch 6 – 35 1.60 0.95

Sugar 3 – 10 0.70 0.80

Ash 5.5 – 10.5 0.70 0.74

Raw Cell Matter 6 – 16 1.18 0.80

Moisture 9 – 15 0.40 0.90

Density 0.5 – 0.64 0.01 0.77

Salt 0.6 – 1.2 0.07 0.80

Phosphorus 0.5 – 0.95 0.03 0.93

Table 1: Performance of the cattle feed calibrations



FoodQuant B2, B3, B4, B5




Powerful software package with InfraQuant and Horizon QI The light source in the FoodQuant has an expected lifetime of 10 years


Substantial amount of starter calibrations through Quantum calibration

program

Spectroscopic Performance (typical, at 25 °Celsius with InAs detector)

Spectral Range 3,700 to 14,885 cm-1

Signal to Noise (60 s, 16 cm-1, at peak response) > 500 000: 1

Frequency Repeatability (@ 7300 cm-1) < 0.006 cm-1

Frequency Accuracy (@ 7300 cm-1) < 0.01 cm-1

Absorbance Reproducibility (toluene) < 0.002 AU

Optical Bench

Beamsplitter Material ZnSe (non-hygroscopic)

Interferometer Mechanism (patent pending) High-throughput double pivot

Michelson, fully jacketed

Source (with electronic stabilization) Quartz Halogen, 10-year expected life

Solid-state Laser Maintenance Free


FoodQuant B2, B3, B4, B5

The FoodQuant is based on the latest FT-NIR technology from ABB Bomem, the world leader in FT-NIR technology. The equipment combines exceptional performance with low cost of ownership. FoodQuant B2 has been developed for the analysis of homogeneous samples, e.g. powders and food additives, but many other types of products can be analysed using the FoodQuant B2. Sampling: The sample is analysed by reflection measurements in petri dishes on the QIA1025

sampling accessory. The petri dishes used for the analysis can be made of either glass, plastic or Teflon depending on local requirements. Teflon is especially suitable for production sites where glass and plastic are not allowed on site. After analysis the glass and Teflon petri dishes can be cleaned and reused many times. Keeping the cost per analysis very low.

FoodQuant B3 has been developed for analysis of heterogeneous products, e.g. flours, but many other types of products can be analyzed on the FoodQuant B3. Sampling: The sample is analysed by reflection measurements in petri dishes on the QIA1026

sampling accessory. The petri dishes can be made of either glass, plastic or Teflon depending on local requirements. The sample is spinning during analysis. This ensures representative sampling, that the analyser is seeing a large part of the sample and that effects from product heterogeneity is reduced. After analysis the glass and Teflon petri dishes can be cleaned and reused many times

The FoodQuant B4 has been developed for analysis of heterogeneous products, e.g. pastes, but many other types of products can be analysed using the FoodQuant B4. Sampling: The sample is analysed by reflection measurements in petri cups on the QIA1028 sampling

accessory. The petri cup is made of Teflon. This means that the petri cup can be brought into the production area, e.g. directly to the churn. The sample is spinning during analysis. This ensures representative sampling, that the analyser is seeing a large part of the sample and that effects from product heterogeneity is reduced. After analysis the Teflon petri cup can be cleaned and reused many times. Keeping the cost per analysis very low.

FoodQuant B5 has been developed for analysis of liquid samples, e.g. sugar solutions, soya etc, but many other samples can be analysed using the FoodQuant B5. Sampling: The sample is analysed by transmission measurements in inexpensive vials on the

QIA1075 Universal Vial Sampler. The Universal Vial Sampler has space for 5mm, 8mm and 12mm vials (outer diameter). The vial with the sample is placed in the heated vial holder before analysis. This ensures representative sampling, that the sample is analysed at the right temperature and that effects from temperature fluctuations are reduced. After analysis the vials are disposed off

Workstation The FoodQuant B2 comes with an external computer, which enables the use of a range of add-ons, offering the user maximum flexibility, e.g. touch screen, label printer and barcode reader. The external PC enables rapid upgrade on-site, this reduces any downtime of the equipment to a minimum. The FoodQuant is supplied with a powerful software: InfraQuant 2.5 (easy to use FT-NIR QC software, to collect, present and handle analytical results) and Horizon QI offering a series of strong spectroscopic tools.



FoodQuant B3 for Flour




Powerful software package with InfraQuant and Horizon QI The light source in the FoodQuant has an expected lifetime of 10 years



FoodQuant B3 for Flour

Many parameters are of interest for the production of flour in order to have production within specifications and to obtain an end product with the desired performance. FoodQuant B3 will provide a fast and accurate result for these parameters, e.g. moisture, protein, gluten and many more. The FoodQuant B3 is perfectly suited to replace traditional laboratory methods which are cumbersome, expensive and require trained personnel. The results are obtained on the FoodQuant B3 in less than a minute, enabling tighter process control and faster reaction in production.

Analyser: FoodQuant B3 The FoodQuant B3 is based on the latest generation FT-NIR technology and has the following main features:

• Cutting edge spectral performance and best signal to noise ratio on the market • Very easy to operate and maintain • Strong software package with InfraQuant and Horizon QI • Very low maintenance costs. The FoodQuant B3 has no scheduled maintenance and the light

source has an expected lifetime of 10 years The sample is analysed by reflection measurement in petri dishes, which can be made of either glass, plastic or Teflon depending on local requirements. Teflon is especially suited for production sites where glass and plastic is not allowed on-site.

Analysis: The sample to be analysed is loaded into a petri dish, which is then placed on the analyser. The analysis is initiated in the software and the result is obtained in less than a minute. The petri dish is spinning during the analysis, ensuring that the FoodQuant B3 is seeing a large part of the sample and reducing effects from product heterogeneity. This is especially important for very heterogenic product like flour.

Calibration and calibration performances

Calibration work has been preformed on various types of flours, including treated soft, treated hard, untreated soft, untreated hard, cake flour, noodle flour and general purpose. Below the performance obtained on the FoodQuant B3 can be found.

Conclusion The FoodQuant B3 is a powerful tool for fast analysis of many parameters in flours, e.g. moisture, protein and gluten. The FoodQuant B3 can be placed in the laboratory on in the production area. The intuitive InfraQuant software guides the operator through the steps of the analysis and the results are displayed with easy to understand colour codes. Q-Interline have starter calibrations available for different types of flour, which will enable a faster start-up for the FoodQuant B3 in your laboratory or production.

Property Interval secv

Moisture 9.8 - 14.0 0.19

Protein 8.0 - 14.0 0.25

Ash 0.3 - 0.8 0.03

Gluten 24 – 40 0.55

Water Absorption 52-68 0.8

Granulation 96.8 - 99.8 0.3

Speck Count 4.5 - 50.75 0.3

Lightness (L) 89 - 94 0.4

Falling Number 350 - 450 15

pH 3.9 - 6.6 0.09



AgriCheck™ - Analyzer for whole grain & corn

AgriCheck Plus - Analyzer for whole grain, powders and liquids

AgriCheck™ - a compact NIR Analyzer for whole grain and seeds

AgriCheck Plus - a compact NIR Analyzer

for whole grain, seeds, powders and liquids


AgriCheck™ - Analyzer for whole grain & corn

AgriCheck Plus - Analyzer for whole grain, powders and liquids

AgriCheck™ is a cost effective solution for grain and seed analysis. While not as versatile as the MultiCheck, it offers the same accuracy and performance in a compact package.

Typical Applications

Whole grain and seed analysis including: corn, soy, rice, wheat, barley, etc.,… Universal calibrations are available for protein, moisture, fat, starch, fiber, gluten, sedimentation…. With optional top mounted reflectance mode (AgriCheck Plus): flour, tea, coffee, spices, powders, pastes, liquids, … Our calibration services can develop calibrations for almost any significant component or property for your particular product.

Key Features

Fixed pathlength cell is capable of measuring a wide range of grains by utilizing the Bruins dynamic range extender technology

Patented sample feed insures accurate measurements

Dynamic Range Extender extends sample coverage with fixed pathlength

Optional reflectance mode for bakery products and powders

~40 second analysis time with 10 subsamples

Fully transferable calibrations between instruments

Options

Reflectance – The optional top mounted reflectance port allows for measurement of fine powders such as flour, tea, coffee, spices, and other powders.

Grain density – This optional accessory integrates with the instrument to automatically provide grain density which is incorporated into the report

Temperature – Measures the temperature of the grain which is incorporated into the report

Technical Specifications

Wavelength range: 730 nm – 1.100 nm in transmission mode 1.100 nm – 2.500 nm in reflectance mode

Light source: Halogen Detector: Silicon Sampling device: Whole grain flow cell Operation: Touch screen, optional keyboard and mouse Increment: 0,5 nm Interface: 2 USB, 1 Ethernet, 1 serial, 1 parallel System dimensions: 450 B x 450 H x 400 mm Weight: 22 kg Algorithm: use of PLS - Model ("Partial Least Squares")



MultiCheckTM

Versatile NIR Analyzer Two in One

MultiCheckTM is the most versatile instrument to measure in transmission and

reflection of cereals, whole grain, feed & forage, flour and powders


MultiCheckTM

Versatile NIR Analyzer Two in One

MultiCheck™ is the flagship of Bruins Instruments NIR Analyzer’s. The MultiCheck™ is the most versatile instrument in the NIR Analyzer line and is capable of performing measurements in both transmission (wheat, barley, corn, rice, soy, oil seed and more) and reflectance for easy and precise measurements of fine powders such as flour, meal, mixed seed, coffee, tea, or any homogenous substance.

Typical Applications MultiCheck™ is a computer controlled double beam NIR-Spectrophotometer, pre-calibrated for the determination of whole grains and seeds including: corn, soy, rice, wheat, barley, oil seeds, etc.... Universal calibrations are available for protein, moisture, fat, starch, fiber, gluten, sedimentation,…. In reflectance mode: feed & forage, flour, mixed seed, tea, coffee, spices, pastes, powders… Our calibration services can develop calibrations for almost any significant component or property for your particular product.

Key Features

Variable pathlength from 8 to 30 mm to accommodate a variety of grain and seed

Reflectance mode for feed & forage, pet food, bakery products and powders


Subsamples improve the measurement of inhomogeneous samples

Fully transferable calibrations between instruments

Options Grain density – This optional accessory integrates with the instrument to automatically provide grain density which is incorporated into the report Temperature – Measures the temperature of the grain which is incorporated into the report

Technical Specifications

Wavelength range: 730 nm - 1.100 nm in transmission mode 1.100 nm - 2.500 nm in reflectance mode Light source: Halogen Sampling presentation: Automatic feed with multiple sub-sample

measurements Operation: Touch screen System Dimensions: 590 L x 470 H x 400 W mm Weight: 40 kg



OmegAnalyzer G™

Whole Grain & Oilseed Analyzer

OmegAnalyzer G™ is the workhorse of Bruins Instruments NIR-Grainanalyzer’s


OmegAnalyzer G™ Whole Grain & Oilseed Analyzer OmegAnalyzer G™ is the workhorse of Bruins Instruments NIR-Grainanalyzer’s. The “G” is a versatile instrument for grain analysis and is capable of handling grain and seed such as wheat, barley, corn, rice, soy, rapeseed and more. This instrument offers USA NTEP certification and a host of upgrade options and accessories.

Typical Applications

Whole grain and seed analysis including: corn, soy, rice, wheat, barley, oils seeds, etc. Universal calibrations are available for protein, moisture, fat, starch, fibre, gluten, sedimentation…. Optional Micro Cell measures flour, powders and small amounts of grain

Our calibration services can develop calibrations for almost any significant component or property for your particular product.

Key Features

NTEP certified*

Variable pathlength from 8 to 30 mm to accommodate a variety of grain and seed


Fully transferable calibrations between Instruments

Options

Grain density – This optional accessory integrates with the instrument to automatically provide grain density which is incorporated into the report.

Macro Cell – For measuring flours, powders, and small amounts of grain by transmission available in path lengths from 3 – 30 mm.

Temperature – Measures the temperature of grain which is incorporated into the report.

Specifications

0,5 nm scan increment

Dimensions: 580 L X 400 H X 470 W mm

Sample Presentation: automatic feed with multiple sub-sample measurements

Wavelength range: 730 - 1.100 nm transmission

Weight: 40 kg

* The OmegAnalyzer G™ meets or exceeds the accuracy and performance requirements for Grain Analyzer’s as detailed in NIST handbook 44. A Certificate of Conformance, Number 09-058, was issued under the National Type Evaluation Program (NTEP) of the National Conference on Weights and Measures, certifying this model for commercial use on the following grains: (see NCWM website for details)

http://www.ncwm.net/ntep/index.cfm?fuseaction=detail&ID=3442



humimeter FS4

Grain moisture meter

Whole grain moisture meter for use in

farming, trade, seed growing, research, laboratories, food and animal feed industry

Your benefits:

Very fast and accurate due to 300 g whole grain measurement

For all product types and finished products

Reduces your drying costs

Protects against mould and resulting damages


humimeter FS4

Grain moisture meter FS4 with datalog:

Online function for data transfer

Integrated memory with printer connection

Very easy to operate

Menus are in German, English, Italian and French

A portable measuring instrument series for measuring using innovative sensor technology

Only an exactly moisture measurement of grain and special fruits allows fair payment for producers, traders and end customers. The quality check by grain and special fruits is very important. To prevent machine problems and to be sure that you don´t buy water to a high product price. With humimeter FS4 grain moisture meter you get the measurement within seconds. Switch on the measuring instrument, fill it with grain and read off the moisture content from the LCD. It is possible to store the measured value on the device. The measured data can be transfer to PC or mobile printer. Stored data are transferred to other programs using the integrated online function. More than 50 000 customer-specific solutions have been designed and produced for industry and university institutions.

Technical data:

Maize, rye, triticale, wheat, spelt, barley, oats, rape, pumpkin seeds, peas, soybeans, beetle beans, horse beans, sunflower seeds, rice, raw coffee, poppy seeds, calibration curve and customer calibrations.

Measuring range 0 to 50% depending on the material

Resolution 0.1%

Hectoliter compensated

Sample temperature measurment

Temperature can be set to°C or °F as required

Automatic temperature compensation

Measurement within seconds without prior treatment of samples

Hold function, manual saving of results, datalog for 10.000 logs with measuring point report

Supplier´s data and batch number can be recorded

Customer calibrations function for special fruits, granulate etc.

Robust stainless housing

With digital scale, case, measuring cup, PC interface, PCsoftware, USB Adapter and batteries

Optional: printer, ISO measuring device check

Device Calibration

accuracy

Measuring

range

Species Sample Interface

FS1 0,1 % 5 – 30 % 12 100 ml

FS2 0,6 % 5 – 40 % 14 300 g

FS4 0,4 % 0 – 50 % 32 300 g Yes



NOTES


NOTES

Fotos used in this brochure by courtesy of our suppliers NIR-Online, Q-Interline, Bruins Instruments and Schaller GmbH



AUSTRIA BULGARIA CROATIA CZECH REPUBLIC HUNGARY POLAND ROMANIA SERBIA SlOVAKIA SLOVENIA

CONTACT:

NOACK & CO AG

Auhofstraße 190

A-1130 Vienna, Austria

Tel.: +43 1 877 54 55

Fax: +43 1 876 54 43

E-mail: [email protected]

www.noackgroup.com

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