Subject Index

A

Adhesion process, polyelectrolyte brushespreparation, 192f

Alcohol esterification, 89sAntifouling properties, polyelectrolytebrushes preparation, 185

Arm number determination, 157ATRP kinetics, 30f

B

Bioactive glycopolymersBIEM, SCVCP, 264fbranched glycopolymers via SCVCP,263s

fluorescent glycopolymer hybridnanoparticles, 265

glucosamine-containing polymerbrushes synthesis, 259s

glycocoplymer-grafted nanoparticles,267f

glycocoplymer-grafted nanospheres,266f

glycopolymer brushes, 260fglycopolymer-grafted DVBmicrospheres synthesis, 261s

glycopolymer-grafted polystyrenenanospheres, 259

grafted microspheres, 265fhyperbranched glycopolymer coveredmicrospheres, 264s

hyperbranched glycopolymer-graftedmicrospheres, 263

magnetic glycopolymer hybridnanoparticles, 265

MAMan grafted microspheres, 262fnanoparticle synthesis, 265soverview, 257polymeric microsphere surfacemodification, 261

ungrafted microspheres, 265fBiomolecule immobilization, polymerbrushes, 251s

Block copolymer phase separation analysis,118

Block copolymersBC1 – BC5, 131fBC1 – BC5 characterization, 130tcomponent peaks, 137t

film parameters, 133tfilm preparation, 132nanostructured polymer filmspreparation, 132

XPS studies, 135films, AFM phase images, 134ffilms, high-resolution C1s spectra, 136ffilms, XPS wide-scan, 136fmorphologies, 132toverview, 127phase separation behaviour, 131SAXS diagrams, 132fsynthesis, 118, 128synthesized block copolymers, 129c

Borate, 28synthesis, 29s

Borate block copolymer micelles, 32fBoronic acid, 28synthesis, 29s

Boronium block copolymers, 28synthesis, 29s

Branched glycopolymers via SCVCP, 263sButyl trithiocarbonate end group removal,16, 18

C

CFStar1, 3 arm star PMMA, 93fCFStar2, 5 arm star PMMA, 93fCFStar3, 8-arm star PMMA, 94fCFStar4, 21 arm star PMMA, 94fChain dimension, polyelectrolyte brushespreparation, 186

Characterization, 145CN(CH3)2C-PStn, DSC curves, 23fCN(CH3)2C-PStn, radical-inducedreduction, 20t

Controlled radical polymerization (CRP)polymer primary structure control, 1polymer-inorganic hybrid materials, 163sequence-controlled CRP processes, 6

Core first PMMA star, dilute solutionproperties, 92

Core first PMMA star synthesis, 89Core first star polymers, arms numberquantification, 95

Core-functionalized star polymers,Ru-catalyzed living radicalpolymerization, 66s

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CRP. See controlled radical polymerization(CRP)

CRP system classification,polymer-inorganic hybrid materials, 165

Crystal assembly reaction, polymerbrushes, 251f

D

Diblock copolymers, Mark-Houwink plots,54f

Direct Ru-encapsulation, microgel-corestar polymers, 67s

DSC characterization, PE-b-POEGMAcopolymers, 56

DSC curvesblock copolymers BC1 – BC5, 131fCN(CH3)2C-PStn, 23fCPDB-PnBAn, 21fH-PnBAn, 21fPABTC-PnBAn, 21fPABTC-PStn, 22fPGMA macro initiator, 122fPGMA-b-PS block copolymer, 122f

DSC thermograms, 56f

F

Fabrication, polymer brushes, 242FeCl2, PPh3-Star, 70fFerrocene containing methacrylatemonomers synthesis, 199

Film preparation, block copolymers, 132nanostructured polymer filmspreparation, 132

XPS studies, 135Fluorescent glycopolymer hybridnanoparticles, 265

Fluorine-condensed star polymers, 76Fluorine-condensed star polymers,ruthenium-catalyzed living radicalpolymerization, 76f

Fluorous Molecular Recognition, 77Friction coefficient, polyelectrolyte brushespreparation, 190f

Functionality determination, 87

G

Glucosamine-containing polymer brushessynthesis, 259s

Glycidyl methacrylate-containing resistpolymer synthesis, 119

Glycocoplymer-grafted nanoparticles, 267fGlycocoplymer-grafted nanospheres, 266fGlycopolymer brushes, 260fGlycopolymer-grafted DVB microspheressynthesis, 261s

Glycopolymer-grafted polystyrenenanospheres, 259

GPC elution curves, MIs, 59fGPC elution traces, 50fGPC elution traces, run 2, 60fGraft copolymerization, PVDF, 223s, 225sGrafted microspheres, bioactiveglycopolymers, 265f

Gyration contraction factor, 85

H

1H NMR characterization, PE-b-POEGMAcopolymers, 55

1H NMR spectra, MI2, 59fHexadecane droplets, polyelectrolytebrushes preparation, 186f

High density polyethylene, 172H-PnBAn, DSC curves, 21fH-PnBAn, radical-induced reduction, 19tHyperbranched glycopolymer coveredmicrospheres, 264s

Hyperbranched glycopolymer-graftedmicrospheres, 263

Hyperbranched/linear polyethylenemacroinitiators, 46t

I

Indium tin oxide (ITO), SI-ATRP, 200Intrinsic viscosity shrink factor, 86Intrinsic viscosity study, PE-b-POEGMAcopolymers, 54

ITO. See indium tin oxide (ITO), SI-ATRPITO-g-PFcMA-b-PMMA, SI-ATRP, 205f

K

KetonesRu-PEG star-catalyzed transferhydrogenation, 72f

transfer hydrogenation, 72, 73f

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L

Lap shear adhesion strengths,polyelectrolyte brushes preparation, 192f

Linear PMMA, Mark-Houwink plot, 94fLinear synthetic polymer chains, 9fLiving radical polymerization, 74Log[η].M vs. elution volume, polymers,83f

M

M1 polymerization, 34fMagnetic glycopolymer hybridnanoparticles, 265

MALDI-TOF MS spectraω-allyl PMMA 3e, 110fω-benzoyl PBA 6, 111fω-benzoyl PMMA 3d, 109fω-benzoyl PNIPAM 8, 112fω-(δ-lacton)-substituted PMMA 4, 110,111f

ω-methylester PMMA 3c, 109fMALLS, SEC, 84MAMan grafted microspheres, bioactiveglycopolymers, 262f

Mark-Houwink plots, 86Mark-Houwink plots, diblock copolymers,54f

Metal encapsulation, 69Metal-bearing star polymers, microgel-corecatalysis, 71f

Methyl methacrylate 3 arm star polymersynthesis, 89

MI, GPC elution curves, 59fMI2, 1H NMR spectra, 59fMicelle behaviors, aqueous solution, 57Micelle size distributions, 57fMicelle solution preparation,PE-b-POEGMA copolymers, 44

Microgel-core catalysis, 70Microgel-core catalysis, metal-bearing starpolymers, 71f

Microgel-core star polymersfluorine-condensed star polymers, 76fluorous molecular recognition, 77ketones, transfer hydrogenation, 72living radical polymerization, 74metal encapsulation, 69microgel-core catalysis, 70overview, 65Ru-bearing microgel-core star polymers,66

sec-alcohols oxidation, 71

tandem catalyst interchange, 69thermoregulated phase-transfer catalysis,73

MMA polymerisation, 90sMMA polymerisation, 3 arm initiator, 90fMonocleavable BA-ss-AB type triblockcopolymer micelles, 297

Mono-cleavable brush-like symmetrictriblock copolymer synthesis, 297f

Monomer conversion, PVDF, 218fMp, various linear calibration standards,82f

Multi detector SEC, 87Multi-cleavable A(ss)n-B type blockcopolymer, 292

Multiple single scan lines, polymerbrushes, 244f

Mussel glue derived enzymesbioconjugates, 281, 281fconjugate IIIb, 282fconjugation strategy, 275NHS-functionalized chain transferreagent synthesis, 276f

overview, 271PNIPAM, 276f, 281fsynthesis, 275tyrosinase, 273f, 278ftyrosinase, circular dichroism spectra,277f

tyrosinase assay, 277ftyrosinase-PNIPAM conjugate, 279

N

Nanoparticle synthesis, bioactiveglycopolymers, 265s

nBA polymerization, 15New monomers, SI-ATRP, 206NHS-functionalized chain transfer reagentsynthesis, 276f

Nitrilotriacetic acid end-functionalizedpolystyrenes (NTA-PS)applications, 308ATRP, 306f, 306tcharacterization, 305DLS data, 311ffluorescence microscope images, 310fgel permeation chromatogram, 307f1H NMR spectra, 308fmesoporous fibres formation, 311micellar aggregates formation, 309overview, 303preparation, 305sSEM images, 309f, 312f

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synthesis, 305TEM images, 309f, 311f, 312f

Nitroxide exchange reaction, polymerbrushes, 247s

NMP initiator syntheses, 147Number-average molecular weightdependencies, 61f

O

Octadecyl acrylate (ODA), 167Octadecyl acrylate, ATRP, 168t, 169f, 170f,171f

Octadecyl acrylate, IR spectra, 171fOctadecyl acrylate polymerization, 168sOctadecyl acrylate polymerization, ATRP,169f

2-Octanone, transfer hydrogenation, 74fODA. See octadecyl acrylate (ODA)ODA polymerization, polymer-inorganichybrid materials, octadecyl acrylatepolymerization, 178, 179

OEGMA, ATRP, 47OEGMA, GPC curves, 48fOEGMA conversion vs. kinetic plots, 49fOEGMA conversion vs. polymerizationtime, 49f, 60f

OH-SS-iBuBr double-head initiatorsynthesis, 296f

Oligomers synthesis, 17Organoboron polymersborate, 28boronic acid, 28boronium block copolymers, 28organoboron quinolate blockcopolymers, 33

overview, 27star polymers, 33

Organoboron quinolate block copolymers,33

Organoboron quinolate monomers, RAFTpolymerization, 34s

Ozone pretreatment, PVDF, 223s, 225s

P

PABTC-PStn, DSC curves, 22fPABTC-PStn, radical-induced reduction,20t

PE MI synthesis, PE-b-POEGMAcopolymers, 43, 45

PE-b-POEGMA copolymers. Seepolyethylene-block-poly[oligo(ethylene

glycol) methacrylate] (PE-b-POEGMA)copolymers

PE-b-POEGMA synthesis, 52tPerfluorinated compounds, fluorousrecognition, 77f

PFcMA brushes, electrochemicalproperties of, 204

PGMA macro-initiator, 122fPGMA macro-initiator, GPC traces, 120fPGMA synthesis, 117. See poly(glycidylmethacrylate), ATRP macro initiator(PGMA) synthesis

PGMA-b-PS block copolymer, 122fPGMA-b-PS block copolymer BCP1, 121fPGMA-b-PS block copolymer phaseseparation, 123

PGMA-b-PS block copolymer synthesis,119s

PGMA-b-PS photoresist block copolymers,photolithography, 123s

PGMA-b-PS photoresist films, 123fPGMA-b-PS thin films, 124fPhosphonic acid coupling agent synthesis,SI-ATRP, 199, 200f

Photolithographic patterning, 122Photolithography, PGMA-b-PS photoresistblock copolymers, 123s

Photolithography patterning, 118PM1-b-PEO, 34fPM2-b-PEO, 34fPMMA 3-arm star polymer, 95fPMMA 5-arm star polymer, 95fPMMA 8-arm star polymer, 96fPMMA 21-arm star polymer, 96fPMMA arms, SEC curves, 68fPMMA stars, Mark-Houwink plot, 94fPMMA stars, SEC results, 92tPnBA thermal properties, 20PnBAn oligomers synthesis, 17tPNIPAM-b-PS star polymers, 36fPODA. See poly(octadecyl acrylate)(PODA)

PODA blends, 172Polyelectrolyte brushes preparationadhesion process, 192fantifouling properties, 185chain dimension, 186chemical structures, 185ffriction coefficient, 190fhexadecane droplets, 186flap shear adhesion strengths, 192foverview, 183repeatable adhesion, 191schematic representation, 187fsliding velocity dependence, 189ftribological behavior, 188

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water, 186fwettability, 185

Polyethylene-block-poly[oligo(ethyleneglycol) methacrylate] (PE-b-POEGMA)copolymersDSC characterization, 561H NMR characterization, 55intrinsic viscosity study, 54materials, 43micelle behaviors, aqueous solution, 57micelle solution preparation, 44OEGMA, ATRP, 47overview, 39PE MI synthesis, 43, 45PE-b-POEGMA synthesis, ATRP, 43synthesis, 42s

PolyFcMA brushes, SI-ATRP, 201f, 203f,204f

Poly(glycidyl methacrylate), ATRP, 120tPoly(glycidyl methacrylate), ATRP macroinitiator (PGMA) synthesis, 117

Poly(glycidyl methacrylate-block-styrene)ATRP, 120tblock copolymer phase separationanalysis, 118

block copolymer synthesis, 118glycidyl methacrylate-containing resistpolymer synthesis, 119

overview, 115PGMA synthesis, 117PGMA-b-PS block copolymer phaseseparation, 123

photolithographic patterning, 122photolithography patterning, 118

Polyhedral ogligomeric silsequioxane-corestar polystyrenearm number determination, 157characterization, 145materials, 144NMP initiator syntheses, 147overview, 141POSS-MAMA-SG1, 2, 146POSS-NH3+Cl-, 145POSS-PS star polymer cleavage, 147star polystyrene, 146star PS, DSC studies, 159star PS synthesis, 150

Polymer brushesbiomolecule immobilization, 251scrystal assembly reaction, 251ffabrication, 242multiple single scan lines, 244fnitroxide exchange reaction, 247soverview, 241polyolefin nanocompositesATRP initiator synthesis, 174, 180

2-bromoisobutyrate functional silicacolloids synthesis, 175, 180

ODA, ATRP, 175, 181radical nitroxide exchange reactions, 246schematic representation, 245fstreptavidin, 246fstructuring, 242surface initiated polymerization, 244ssurface nitroxide exchange reaction,248f

synthesis, 242zeolite L crystals, 248, 249s, 252f

Polymer primary structure controloverview, 1sequence-controlled CRP processes, 6sequence-defined polymer synthesis, 3

Polymer synthesis, polymer-inorganichybrid materials, 167

Polymeric microsphere surfacemodification, 261

Polymer-inorganic hybrid materialsATRP, 166CRP, 165CRP system classification, 165high density polyethylene, 172ODA polymerization, octadecyl acrylatepolymerization, 178, 179

overview, 163PODA blends, 172polymer brushes, polyolefinnanocompositesATRP initiator synthesis, 174, 1802-bromoisobutyrate functional silicacolloids synthesis, 175, 180

ODA, ATRP, 175polymer synthesis, 167surface modification, 174

Polymers, log[η].M vs. elution volume, 83fPoly(methyl methacrylate) (PMMA)graftingATRP grafting, 235scharacterization, 233nitrogen adsorption isotherms, 236foverview, 231pore size distributions, 236fSBA-15 initiator immobilization, 233SBA-15 synthesis, 232surface-initiated ATRP, 233weight change patterns, 237f

Poly(methyl methacrylate) star polymerscore first PMMA star, dilute solutionproperties, 92

core first PMMA star synthesis, 89core first star polymers, arms numberquantification, 95

functionality determination, 87

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gyration contraction factor, 85intrinsic viscosity shrink factor, 86MALLS, SEC, 84Mark-Houwink plots, 86methyl methacrylate 3 arm star polymersynthesis, 88

multi detector SEC, 87overview, 811,1,1-tris(methyl-o-isobutyryl bromide)ethane synthesis, 88

Poly(n-butyl acrylate) (PBA)functionalization, 105s

Poly(N-isopropylacrylamide) (PNIPAM),MALDI-TOF MS spectra, 106f

Poly(N-isopropylacrylamide) (PNIPAM)functionalization, 105s

Poly(octadecyl acrylate) (PODA), 167Poly(octadecyl acrylate), 1H-NMR, 172fPoly(octadecyl acrylate), IR spectra, 171fPoly(octadecyl acrylate), SEM, 173fPoly(vinylidene fluoride) (PVDF)functionalization via ATRP, 214s, 215functionalization via click chemistry,220

functionalization via CRP, 213s, 215s,220

functionalization via RAFTpolymerization, 214s, 219

graft copolymerization, 223s, 225smonomer conversion, 218foverview, 211ozone pretreatment, 223s, 225s

POSS-based alkoxyamine, 150fPOSS-MAMA-SG1, 148f, 149f, 152f, 153f,156f, 157f, 158f

POSS-MAMA-SG1, 2, 146POSS-MAMA-SG1 alkoxyamine 2, 151tPOSS-(MAMA-SG1)n, 150fPOSS-NH3+Cl-, 144s, 145POSS-PS star polymer cleavage, 147POSS-(SG1)8, 144sPS star polymer synthesis, 154fPSBA-b-PS self- assembly, 32fPSBBr2-b-PS, 31fPSt thermal properties, 22PSTMS-b-PS, 31fPStn oligomers synthesis, 18tPVDF-g-PDMAEMA copolymer, 217s

R

Radical nitroxide exchange reactions,polymer brushes, 246

Radical-induced reduction

CN(CH3)2C-PStn, 20tH-PnBAn, 19tPABTC-PStn, 20t

RAFT polymerization. See reversibleaddition fragmentation chain transfer(RAFT) polymerization

Repeatable adhesion, polyelectrolytebrushes preparation, 191

Reversible addition fragmentation chaintransfer (RAFT) polymerizationanalyses, 15butyl trithiocarbonate end groupremoval, 16, 18

materials, 14nBA polymerization, 15oligomers synthesis, 17overview, 13PnBA thermal properties, 20PSt thermal properties, 22styrene polymerization, 16

Ru-bearing microgel-core star polymers,66

Ru-catalyzed living radical polymerizationcore-functionalized star polymers, 66smicrogel-core star polymers, 67s

RuCpCl-star-catalyzed living radical(co)polymerization, 75t

Run 2, GPC elution traces, 60fRun 5 sample, 6 1H NMR spectra, 55fRu-PEG star-catalyzed transferhydrogenation, ketones, 72f

Ru-star polymers, SEC curves, 68f

S

Schematic representationpolyelectrolyte brushes preparation, 187fpolymer brushes, 245f

Sec-alcohol oxidation, 71, 71fSequence-controlled CRP processes, 6Sequence-controlled polymers, 2, 7fSequence-defined oligomers synthesis, 4fSequence-defined polymer, 2Sequence-defined polymer synthesis, 3Sheddable A-ss-B type biodegradableblock copolymer micelles, 295

SI-ATRP. See surface initiated atomtransfer radical polymerization(SI-ATRP)

SiO2, PODA polymer brushes, 177fSiO2-PODA, TGA, 176fSliding velocity dependence,polyelectrolyte brushes preparation, 189f

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Star polymer-catalyzed living radicalpolymerization, 74f

Star polymers, 33schematic representation, 83fSEC traces, 155fsynthesis, 35ssynthesis, ATRP, 91f

Star polystyrene, 146, 160fStar PS, DSC studies, 159Star PS synthesis, 150Stimuli-responsive degradable blockcopolymer micelles, 290f

Streptavidin, 246fStructuring, polymer brushes, 242Styrene polymerization, 16, 156f, 157fSurface initiated atom transfer radicalpolymerization (SI-ATRP)electrochemical characterization, 202ferrocene containing methacrylatemonomers synthesis, 199

ITO, 200ITO-g-PFcMA-b-PMMA, 205fnew monomers, 206overview, 197phosphonic acid coupling agentssynthesis, 199, 200f

polyFcMA brushes, 201f, 203f, 204fvinylic ProDOT monomers synthesis,206f

Surface initiated polymerization, 244sSurface modification, polymer-inorganichybrid materials, 174

Surface nitroxide exchange reaction,polymer brushes, 248f

T

Tandem catalyst interchange, 69Tellurium-metal transmetallation reaction,ω-end functionalized polymers, 101

Thermoregulated phase-transfer catalysis,73, 74f

Thiol-responsive degradable blockcopolymer micellesaqueous micellization, 289fcell viability, 298development strategies, 290monocleavable BA-ss-AB type triblockcopolymer micelles, 297

mono-cleavable brush-like symmetrictriblock copolymer synthesis, 297f

multi-cleavable A(ss)n-B type blockcopolymer, 292

OEOMA, 293tOH-SS-iBuBr double-head initiatorsynthesis, 296f

overview, 287sheddable A-ss-B type biodegradableblock copolymer micelles, 295

ssABP, 292f, 294f, 296f, 298f, 299fstimuli-responsive degradable blockcopolymer micelles, 290f

Tribological behavior, polyelectrolytebrushes preparation, 188

Triple-detector GPC, 51f1,1,1-Tris(methyl-o-isobutyryl bromide)ethane synthesis, 88

Tyrosinase, 273f, 278f

V

Vinylic ProDOT monomers synthesis,SI-ATRP, 206f

W

ω-alkynylated PNIPAM 9, 112ω-allyl PMMA 3e, 110, 110fω-benzoyl PBA 6, 110, 111fω-benzoyl PMMA 3d, 108, 109fω-benzoyl PNIPAM 8, 112, 112fω-carboxylic acid PMMA 3b, 108ω-deuterated PMMA 3a synthesis, 108ω-(δ-lacton)-substituted PMMA 4, 110,111f

ω-end functionalized polymersMALDI-TOF MS spectra, 103foverview, 99synthesis, 101s, 102t, 104tellurium-metal transmetallationreaction, 101

ω-end functionalized polymers synthesis,108

Wettability, polyelectrolyte brushespreparation, 185

ω-methylester PMMA 3c, 108, 109f

Z

Zeolite L crystals, 248, 249s, 252f

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