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Macromolecules Vol. 2: Synthesis and Ma- terials Hans-Georg Elias, Plenum Pub- lishing Corporation, New York, 1977. 1131 XXlV pages. price: 39.50. This is the second part of the two volume treatise on Macromolecules of H-G. Elias. While the first part covers Structure and Properties, this second one discusses Synthesis and Materials and, specifically, treats principles and classification of polymerization reac- tions, polycondensation, ionic poly- merization, polyinsertion Ziegler- Natta polymerization, enzymatic poly- merization), free radical polymeriza- tion, photopolymerization, copolymer- ization and reactions of macrom ole- cules. Subsequently, the Author dis- cusses the synthesis of the most com- mon and industrially important poly- mers from polyolefins to polyacrylics, polyethers, polyesthers, polyamides, polynucleotides, protein and poly- sacchandes. The discussion is at the advanced undergraduate and beginning graduate level. Only elementary knowledge of organic, inorganic and physical chemis- try is necessary. Mathematical deriva- tions are kept to a minimum, while the chemical aspects of the polymerization is emphasized, The book’s strong point is the in- tegration of the chemistry into the kinetics of polymerization reactions. Unfortunately the treatment of the structure of polymers before that of their synthesis and polymerization kinetics, as followed by the Author, does not permit a complete and more direct coupling between physical chem- istry, kinetics, molecular structure and molecular aggregates in polymers mor- phology). The present book, while covering these aspects less deeply than other textbooks, is more broad in scope and contains more material than many other textbooks now available on this subject. A drawback of the book when used as a classroom text is the lack of problem set? and the tendency not to articulate concepts through problems. The volume will be most useful as a self-study textbook; it contains an ex- cellent set of references where detailed treatment of many concepts may be found. In sum, the volume represents a val- uable addition to the already long list of textbooks in macromolecular science that have appeared in recent years. GUISEPPE PARRAVANO Professor University of Michigan Measurements in Heat Transfer second edition, E. R G. Eckert and R. J. Gold- stein editors) , McG raw -Hill ook Co., New York, 1976. 656 pages. price: 29.95. This book, which is the second edi- tion of the well known book, Measure- ment Techniques n Heat Transfer originally published in 1970 is a re- view of measurement techniques and instrumentation in experimental heat transfer. This reviewer has found the book to be both useful and understand- able with respect to experimental mea- surement techniques. Individual chapters are authored by acknowledged experts in their areas of research and this provides for very in- depth coverage. However, there is some repetition in descriptions of tem- perature scales which is no doubt at- tributable to this multiple authorship. There are more typographical errors in the book than one might expect in second edition. A major change in the second edition is the replacement of the original three-part Chapter 2 on temperature measurement by two sep arate chapters; Chapter 2 which de- scribes platinum resistance thermom- etry, and Chapter 3, which deals with thermocouple measurements. This change does not signiscantly alter the coverage of these topics. The new edi- tion has added an appendix on the International Practical Temperature Scale o f 1968. Chapter 1 deals with estimation of errors in temperature measurement, particularly with regard to thermo- couples. Temperature measurement using platinum resistance thermometry, thermocouples, and optical techniques is considered in Chapters 2 through 5. Chapters 6 and 7 discuss spectroscopic and other techniques for temperature measurement in high temperature gases and plasmas. Transient methods for estimating surface heat flux is the topic of Chapter 8. Experimental applica- tions of the analogy between heat and mass transfer by convection are men- tioned in Chapter 9. Chapter 10 is concerned with measurements o f ther- mal radiation. Measurement techniques for physical properties important for heat transfer are described in Chapters and 12. Chapters 13 and 14 are de- voted to velocity measurements using Iaser-Doppler and cooled film ane- mometry. The extensive reference lists at the end of each chapter are a definite as- AIChE Journal Vol. 23 No 5 age 77 September I 9

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Macromolecules Vol. 2: Synthesis and Ma-

terials Hans-Georg Elias, Plenum Pub-lishing Corporation, N ew Y or k , 1977.

1131 XXlV pages. price: 39 .50 .

This is the second part of the twovolume treatise on Macromolecules ofH-G. Elias. While the first part coversStructure and Properties, this secondone discusses Synthesis and Materialsand, specifically, treats principles and

classification of polymerization reac-tions, polycondensation, ionic poly-merization, polyinsertion Ziegler-Natta polymerization, enzymatic poly-merization), free radical polymeriza-tion, photopolymerization, copolymer-ization an d reactions of macrom ole-cules. Subsequently, the Author dis-cusses the synthesis of the most com-mon and industrially important poly-mers from polyolefins to polyacrylics,polyethers, polyesthers, polyamides,polynucleotides, protein and poly-

sacchandes.The discussion is at the advancedundergraduate a nd beginning graduatelevel. Only elementary knowledge oforganic, inorganic and physical chemis-try is necessary. Mathematical deriva-tions are kept to a minimum, while thechemical aspects of the polymerizationis emphasized,

The book’s strong point is the in-tegration of the chemistry into thekinetics of polymerization reactions.Unfortunately the treatment of thestructure of polymers before that of

their synthesis and polymerizationkinetics, as followed by the Author,does not permit a complete and moredirect coupling between physical chem-istry, kinetics, molecular structure andmolecular aggre gates in polymers mo r-

phology). The present book, whilecovering these aspects less deeply thanother textbooks, is more broad in scopeand contains more material than manyother textbooks now available on thissubject. A draw back of th e book whenused as a classroom text is the lack ofproblem set? and the tendency not toarticulate concepts through problems.The volume will be most useful as a

self-study textbook; it contains an ex-cellent set of references where detailedtreatment of m any concepts may befound.

In sum , the volume represents a val-uable addition to the already long listof textbooks in macromolecular sciencethat ha ve a ppeare d in recent years.

GUISEPPEPARRAVANO

ProfessorUniversity of Michigan

Measurements in Heat Transfer second

edition, E. R G. Ecker t and R. J. Gold-

stein editors), McGraw-Hil l ook Co.,

New York, 1976. 656 pages. price:

2 9 . 9 5 .

This book, which is the second edi-tion of the well known book, Measure-ment Techniques n Heat Transferoriginally published in 1970 is a re-view of measurement techniques andinstrumentation in experimental heattransfer. This reviewer has found thebook to be both useful and understand-able with respect to experimental mea-

surement techniques.Individual chapters are authored by

acknowledged experts in their areas ofresearch a nd this provides for very in-depth coverage. However, there is

some repetition in descriptions of tem-

perature scales which is no doubt at-tr ibutable to this multiple authorship.The re are more typog raphical errors inthe book than one might expect insecond edition. A major change in thesecond edition is the replacement of

the original three-part Chapter 2 ont emperatu re measurement by two s e parate chapters; Chapter 2 which de-

scribes platinum resistance thermom-

etry, and Chapter 3, which deals withthermocouple measurements. Thischange does not signiscantly alter thecoverage of these topics. The new edi-t ion has added an appendix on theInternational Practical TemperatureScale of 1968.

Chapter 1 deals with estimation of

errors in temperature measurement,particularly with regard to thermo-couples. Temperature measurementusing platinum resistance thermometry,thermocouples, and optical techniquesis considered in Chapters 2 through 5.Chapters 6 and 7 discuss spectroscopicand other techniques for temperaturemeasurem ent in high temperature gasesand plasmas. Transient methods forestimating surface hea t flux is the topicof Chapter 8. Experimental applica-tions of the analogy between heat andmass transfer by convection are men-tioned in Chapter 9. Chapter 10 isconcerned with measurements of ther-mal radiation. Measurement techniquesfor physical properties important forheat transfer are described in Chapters

and 12. Chapters 13 and 14 are de-voted to velocity measurements usingIaser-Doppler and cooled film ane-mometry.

The extensive reference l is ts at theend of each chapter are a definite as-

AIChE Journal Vol. 23 No 5)age 77 September I9