wx.toronto.ca · [this report shall not be reproduced except in full without the written authority...

[This report shall not be reproduced except in full without the written authority of the Laboratory.]

24-FEB-17

Lab Work Order #: L1894670

Date Received:AMEC Foster Wheeler - Mississauga

160 TRADERS BLVD., SUITE 110MISSISSAUGA ON L4Z 3K7

ATTN: ALESSANDRO PELLERITOFINAL REV. 316-JUN-17 14:44 (MT)Report Date:

Version:

Certificate of Analysis

ALS CANADA LTD Part of the ALS Group An ALS Limited Company

____________________________________________

Mary-Lynn PiresClient Services Supervisor

ADDRESS: 5730 Coopers Avenue, Unit #26 , Mississauga, ON L4Z 2E9 Canada | Phone: +1 905 507 6910 | Fax: +1 905 507 6927

Client Phone: 905-568-2929

TT163027Job Reference: NOT SUBMITTEDProject P.O. #:

C of C Numbers:Legal Site Desc:

ALS ENVIRONMENTAL ANALYTICAL REPORT

L1894670 CONTD....

2PAGE

Result D.L. Units Extracted AnalyzedSample Details/Parameters

of

TT163027

Qualifier* Batch

* Refer to Referenced Information for Qualifiers (if any) and Methodology.

Version: FINAL REV21

L1894670-1 BH 1-SS1CLIENT on 23-FEB-17 @ 17:30Sampled By:SOILMatrix:

Physical Tests

Cyanides

Saturated Paste Extractables

Metals

Speciated Metals

Organochlorine Pesticides

Conductivity

% Moisture

pH

Cyanide, Weak Acid Diss

SAR

Calcium (Ca)

Magnesium (Mg)

Sodium (Na)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)

Boron (B), Hot Water Ext.

Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Mercury (Hg)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)

Chromium, Hexavalent

Aldrin

gamma-hexachlorocyclohexane

a-chlordane

Chlordane (Total)

g-chlordane

op-DDD

pp-DDD

Total DDD

mS/cm

%

pH units

ug/g

SAR

mg/L

mg/L

mg/L

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

02-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

05-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

0.969

41.3

6.71

<0.050

0.42

127

8.8

18.0

<1.0

1.7

72.2

<0.50

<5.0

0.96

<0.50

8.9

2.7

7.1

11.0

0.0449

<1.0

5.9

<1.0

<0.20

<0.50

<1.0

15.7

24.2

<1.0

<0.020

<0.010

<0.020

<0.028

<0.020

<0.020

<0.020

<0.028

0.0040

0.10

0.10

0.050

0.10

1.0

1.0

1.0

1.0

1.0

1.0

0.50

5.0

0.10

0.50

1.0

1.0

1.0

1.0

0.0050

1.0

1.0

1.0

0.20

0.50

1.0

1.0

5.0

1.0

0.020

0.010

0.020

0.028

0.020

0.020

0.020

0.028

DLM

R3668063

R3666496

R3667405

R3668305

R3668241

R3668241

R3668241

R3668241

R3668227

R3668227

R3668227

R3668227

R3668227

R3668245

R3668227

R3668227

R3668227

R3668227

R3668227

R3666884

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668453

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383


L1894670 CONTD....

3PAGE


of

TT163027

Qualifier* Batch



L1894670-1

L1894670-3

BH 1-SS1

BH 1-SS3

CLIENT on 23-FEB-17 @ 17:30


Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:


Herbicides

Physical Tests

Cyanides


o,p-DDE

pp-DDE

Total DDE

op-DDT

pp-DDT

Total DDT

Dieldrin

Endosulfan I

Endosulfan II

Endosulfan (Total)

Endrin

Heptachlor

Heptachlor Epoxide

Hexachlorobenzene

Hexachlorobutadiene

Hexachloroethane

Methoxychlor

Surrogate: 2-Fluorobiphenyl

Surrogate: d14-Terphenyl

Bromoxynil

2,4-D

Dicamba

Dinoseb

MCPA

Mecoprop

Picloram

2,4,5-T

2,4,5-TP

Surrogate: 2,4-Dichlorophenylacetic Acid

Conductivity

% Moisture

pH


SAR

Calcium (Ca)

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

%

mS/cm

%

pH units

ug/g

SAR

mg/L

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

05-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

<0.020

<0.020

<0.028

<0.020

<0.020

<0.028

<0.020

<0.020

<0.020

<0.028

<0.020

<0.020

<0.020

<0.010

<0.010

<0.010

<0.020

103.1

99.5

<0.080

<0.080

<0.080

<0.080

<0.30

<0.30

<0.080

<0.080

<0.080

91.5

1.10

27.2

7.56

<0.050

0.14

147

0.020

0.020

0.028

0.020

0.020

0.028

0.020

0.020

0.020

0.028

0.020

0.020

0.020

0.010

0.010

0.010

0.020

50-140

50-140

0.080

0.080

0.080

0.080

0.30

0.30

0.080

0.080

0.080

50-150

0.0040

0.10

0.10

0.050

0.10

1.0

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3668198

R3668198

R3668198

R3668198

R3668198

R3668198

R3668198

R3668198

R3668198

R3668198

R3668063

R3666496

R3667405

R3668305

R3668241

R3668241


L1894670 CONTD....

4PAGE


of

TT163027

Qualifier* Batch



L1894670-3

L1894670-5

BH 1-SS3

BH 1-SS5



Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:


Metals

Speciated Metals

Physical Tests

Cyanides


Metals

Magnesium (Mg)

Sodium (Na)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)


Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Mercury (Hg)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)


Conductivity

% Moisture

pH


SAR

Calcium (Ca)

Magnesium (Mg)

Sodium (Na)

Antimony (Sb)

Arsenic (As)

mg/L

mg/L

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

mS/cm

%

pH units

ug/g

SAR

mg/L

mg/L

mg/L

ug/g

ug/g

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

05-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

20.1

6.7

<1.0

<1.0

26.0

<0.50

<5.0

0.40

<0.50

5.9

1.7

3.3

1.3

<0.0050

2.1

3.4

<1.0

<0.20

<0.50

<1.0

15.1

7.7

<0.20

0.187

17.6

7.94

<0.050

0.25

15.4

2.8

4.0

<1.0

1.1

1.0

1.0

1.0

1.0

1.0

0.50

5.0

0.10

0.50

1.0

1.0

1.0

1.0

0.0050

1.0

1.0

1.0

0.20

0.50

1.0

1.0

5.0

0.20

0.0040

0.10

0.10

0.050

0.10

1.0

1.0

1.0

1.0

1.0

R3668241

R3668241

R3668227

R3668227

R3668227

R3668227

R3668227

R3668245

R3668227

R3668227

R3668227

R3668227

R3668227

R3666884

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668194

R3668063

R3666496

R3667405

R3668305

R3668241

R3668241

R3668241

R3668241

R3668227

R3668227


L1894670 CONTD....

5PAGE


of

TT163027

Qualifier* Batch



L1894670-5

L1894670-11

BH 1-SS5

BH 2-SS1



Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:

Metals

Speciated Metals

Physical Tests

Cyanides


Metals

Barium (Ba)

Beryllium (Be)

Boron (B)


Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Mercury (Hg)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)


Conductivity

% Moisture

pH


SAR

Calcium (Ca)

Magnesium (Mg)

Sodium (Na)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)


Cadmium (Cd)

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

mS/cm

%

pH units

ug/g

SAR

mg/L

mg/L

mg/L

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

05-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

16.7

<0.50

<5.0

<0.10

<0.50

9.1

2.2

5.1

1.8

<0.0050

<1.0

4.1

<1.0

<0.20

<0.50

<1.0

19.9

9.5

<0.20

0.309

14.3

7.60

<0.050

<0.10

20.5

1.6

1.2

<1.0

3.1

55.0

<0.50

5.3

0.42

<0.50

1.0

0.50

5.0

0.10

0.50

1.0

1.0

1.0

1.0

0.0050

1.0

1.0

1.0

0.20

0.50

1.0

1.0

5.0

0.20

0.0040

0.10

0.10

0.050

0.10

1.0

1.0

1.0

1.0

1.0

1.0

0.50

5.0

0.10

0.50

R3668227

R3668227

R3668227

R3668245

R3668227

R3668227

R3668227

R3668227

R3668227

R3666884

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668194

R3668063

R3666496

R3667405

R3668305

R3668241

R3668241

R3668241

R3668241

R3668227

R3668227

R3668227

R3668227

R3668227

R3668245

R3668227


L1894670 CONTD....

6PAGE


of

TT163027

Qualifier* Batch




Metals

Speciated Metals


Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Mercury (Hg)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)


Aldrin


a-chlordane

Chlordane (Total)

g-chlordane

op-DDD

pp-DDD

Total DDD

o,p-DDE

pp-DDE

Total DDE

op-DDT

pp-DDT

Total DDT

Dieldrin

Endosulfan I

Endosulfan II

Endosulfan (Total)

Endrin

Heptachlor

Heptachlor Epoxide

Hexachlorobenzene

Hexachlorobutadiene

Hexachloroethane

Methoxychlor

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

18.5

5.0

18.4

25.8

0.179

<1.0

10.9

<1.0

<0.20

<0.50

<1.0

23.3

58.7

<0.20

<0.020

<0.010

<0.020

<0.028

<0.020

<0.020

<0.020

<0.028

<0.020

<0.020

<0.028

<0.020

<0.020

<0.028

<0.020

<0.020

<0.020

<0.028

<0.020

<0.020

<0.020

<0.010

<0.010

<0.010

<0.020

1.0

1.0

1.0

1.0

0.0050

1.0

1.0

1.0

0.20

0.50

1.0

1.0

5.0

0.20

0.020

0.010

0.020

0.028

0.020

0.020

0.020

0.028

0.020

0.020

0.028

0.020

0.020

0.028

0.020

0.020

0.020

0.028

0.020

0.020

0.020

0.010

0.010

0.010

0.020

R3668227

R3668227

R3668227

R3668227

R3666884

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668194

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383


L1894670 CONTD....

7PAGE


of

TT163027

Qualifier* Batch



L1894670-11

L1894670-12

L1894670-13

BH 2-SS1

BH 2-SS2

BH 2-SS3




Sampled By:

Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:


Herbicides

Physical Tests

Polycyclic Aromatic Hydrocarbons



Bromoxynil

2,4-D

Dicamba

Dinoseb

MCPA

Mecoprop

Picloram

2,4,5-T

2,4,5-TP


% Moisture

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene

Benzo(b)fluoranthene

Benzo(g,h,i)perylene

Benzo(k)fluoranthene

Chrysene

Dibenzo(ah)anthracene

Fluoranthene

Fluorene

Indeno(1,2,3-cd)pyrene

1+2-Methylnaphthalenes

1-Methylnaphthalene

2-Methylnaphthalene

Naphthalene

Phenanthrene

Pyrene


Surrogate: p-Terphenyl d14

%

%

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

%

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

02-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

06-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

102.5

105.1

<0.080

<0.080

<0.080

<0.080

<0.30

<0.30

<0.080

<0.080

<0.080

96.5

22.0

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.042

<0.030

<0.030

<0.050

<0.050

<0.050

94.5

88.9

50-140

50-140

0.080

0.080

0.080

0.080

0.30

0.30

0.080

0.080

0.080

50-150

0.10

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.042

0.030

0.030

0.050

0.050

0.050

50-140

50-140

R3667383

R3667383

R3668198

R3668198

R3668198

R3668198

R3668198

R3668198

R3668198

R3668198

R3668198

R3668198

R3666496

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293


L1894670 CONTD....

8PAGE


of

TT163027

Qualifier* Batch



L1894670-13

L1894670-15

BH 2-SS3

BH 2-SS5



Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:

Physical Tests

Cyanides


Metals

Speciated Metals

Physical Tests

Cyanides

Conductivity

% Moisture

pH


SAR

Calcium (Ca)

Magnesium (Mg)

Sodium (Na)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)


Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Mercury (Hg)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)


Conductivity

% Moisture

pH


mS/cm

%

pH units

ug/g

SAR

mg/L

mg/L

mg/L

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

mS/cm

%

pH units

ug/g

02-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

05-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

05-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

0.268

16.7

7.19

<0.050

0.19

23.8

1.7

3.6

<1.0

1.7

44.0

<0.50

<5.0

0.37

<0.50

13.0

3.9

9.9

8.0

0.0320

<1.0

8.9

<1.0

<0.20

<0.50

<1.0

19.1

27.7

<0.20

0.270

19.0

7.29

<0.050

0.0040

0.10

0.10

0.050

0.10

1.0

1.0

1.0

1.0

1.0

1.0

0.50

5.0

0.10

0.50

1.0

1.0

1.0

1.0

0.0050

1.0

1.0

1.0

0.20

0.50

1.0

1.0

5.0

0.20

0.0040

0.10

0.10

0.050

R3668063

R3666496

R3667405

R3668305

R3668241

R3668241

R3668241

R3668241

R3668227

R3668227

R3668227

R3668227

R3668227

R3668245

R3668227

R3668227

R3668227

R3668227

R3668227

R3666884

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668194

R3668063

R3666496

R3667405

R3668305


L1894670 CONTD....

9PAGE


of

TT163027

Qualifier* Batch



L1894670-15

L1894670-20

BH 2-SS5

BH 3-SS1



Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:


Metals

Speciated Metals

Physical Tests

Cyanides


Metals

SAR

Calcium (Ca)

Magnesium (Mg)

Sodium (Na)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)


Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Mercury (Hg)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)


Conductivity

% Moisture

pH


SAR

Calcium (Ca)

Magnesium (Mg)

Sodium (Na)

SAR

mg/L

mg/L

mg/L

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

mS/cm

%

pH units

ug/g

SAR

mg/L

mg/L

mg/L

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

05-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

0.53

22.9

1.7

9.8

<1.0

1.5

29.0

<0.50

<5.0

0.30

<0.50

10.0

3.2

7.4

5.8

0.0142

<1.0

6.9

<1.0

<0.20

<0.50

<1.0

17.7

20.5

<0.20

0.154

5.90

7.75

<0.050

0.56

16.1

1.3

8.8

0.10

1.0

1.0

1.0

1.0

1.0

1.0

0.50

5.0

0.10

0.50

1.0

1.0

1.0

1.0

0.0050

1.0

1.0

1.0

0.20

0.50

1.0

1.0

5.0

0.20

0.0040

0.10

0.10

0.050

0.10

1.0

1.0

1.0

R3668241

R3668241

R3668241

R3668241

R3668227

R3668227

R3668227

R3668227

R3668227

R3668245

R3668227

R3668227

R3668227

R3668227

R3668227

R3666884

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668194

R3668063

R3666496

R3667405

R3668305

R3668241

R3668241

R3668241

R3668241


L1894670 CONTD....

10PAGE


of

TT163027

Qualifier* Batch




Metals

Speciated Metals

Polychlorinated Biphenyls


Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)


Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Mercury (Hg)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)


Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Total PCBs


Aldrin


a-chlordane

Chlordane (Total)

g-chlordane

op-DDD

pp-DDD

Total DDD

o,p-DDE

pp-DDE

Total DDE

op-DDT

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

02-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

<1.0

2.8

47.4

<0.50

6.0

<0.10

<0.50

15.9

5.8

13.5

10.2

0.0144

<1.0

13.4

<1.0

<0.20

<0.50

<1.0

23.7

38.4

0.32

<0.010

<0.010

<0.010

<0.010

<0.020

94.0

<0.020

<0.010

<0.020

<0.028

<0.020

<0.020

<0.020

<0.028

<0.020

<0.020

<0.028

<0.020

1.0

1.0

1.0

0.50

5.0

0.10

0.50

1.0

1.0

1.0

1.0

0.0050

1.0

1.0

1.0

0.20

0.50

1.0

1.0

5.0

0.20

0.010

0.010

0.010

0.010

0.020

60-140

0.020

0.010

0.020

0.028

0.020

0.020

0.020

0.028

0.020

0.020

0.028

0.020

R3668227

R3668227

R3668227

R3668227

R3668227

R3668245

R3668227

R3668227

R3668227

R3668227

R3668227

R3666884

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668194

R3668264

R3668264

R3668264

R3668264

R3668264

R3668264

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383


L1894670 CONTD....

11PAGE


of

TT163027

Qualifier* Batch



L1894670-20

L1894670-21

BH 3-SS1

BH 3-SS2



Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:


Herbicides

Physical Tests

Volatile Organic Compounds

pp-DDT

Total DDT

Dieldrin

Endosulfan I

Endosulfan II

Endosulfan (Total)

Endrin

Heptachlor

Heptachlor Epoxide

Hexachlorobenzene

Hexachlorobutadiene

Hexachloroethane

Methoxychlor



Bromoxynil

2,4-D

Dicamba

Dinoseb

MCPA

Mecoprop

Picloram

2,4,5-T

2,4,5-TP


% Moisture

Acetone

Benzene

Bromodichloromethane

Bromoform

Bromomethane

Carbon tetrachloride

Chlorobenzene

Dibromochloromethane

Chloroform

1,2-Dibromoethane

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

%

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

<0.020

<0.028

<0.020

<0.020

<0.020

<0.028

<0.020

<0.020

<0.020

<0.010

<0.010

<0.010

<0.020

109.7

133.6

<0.080

<0.080

<0.080

<0.080

<0.30

<0.30

<0.080

<0.080

<0.080

94.6

10.3

<0.50

<0.0068

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

0.020

0.028

0.020

0.020

0.020

0.028

0.020

0.020

0.020

0.010

0.010

0.010

0.020

50-140

50-140

0.080

0.080

0.080

0.080

0.30

0.30

0.080

0.080

0.080

50-150

0.10

0.50

0.0068

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3667383

R3668198

R3668198

R3668198

R3668198

R3668198

R3668198

R3668198

R3668198

R3668198

R3668198

R3666496

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703


L1894670 CONTD....

12PAGE


of

TT163027

Qualifier* Batch





Hydrocarbons

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

Dichlorodifluoromethane

1,1-Dichloroethane

1,2-Dichloroethane

1,1-Dichloroethylene

cis-1,2-Dichloroethylene

trans-1,2-Dichloroethylene

Methylene Chloride

1,2-Dichloropropane

cis-1,3-Dichloropropene

trans-1,3-Dichloropropene

1,3-Dichloropropene (cis & trans)

Ethylbenzene

n-Hexane

Methyl Ethyl Ketone

Methyl Isobutyl Ketone

MTBE

Styrene

1,1,1,2-Tetrachloroethane


Tetrachloroethylene

Toluene

1,1,1-Trichloroethane


Trichloroethylene

Trichlorofluoromethane

Vinyl chloride

o-Xylene

m+p-Xylenes

Xylenes (Total)

Surrogate: 4-Bromofluorobenzene

Surrogate: 1,4-Difluorobenzene

F1 (C6-C10)

F1-BTEX

F2 (C10-C16)

F2-Naphth

F3 (C16-C34)

F3-PAH

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

03-MAR-17

06-MAR-17

03-MAR-17

06-MAR-17

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.20

<0.050

<0.030

<0.030

<0.042

<0.018

<0.050

<0.50

<0.50

<0.050

<0.050

<0.050

<0.050

<0.050

<0.080

<0.050

<0.050

<0.010

<0.050

<0.020

<0.020

<0.030

<0.050

90.0

97.9

<5.0

<5.0

<10

<10

<50

<50

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.20

0.050

0.030

0.030

0.042

0.018

0.050

0.50

0.50

0.050

0.050

0.050

0.050

0.050

0.080

0.050

0.050

0.010

0.050

0.020

0.020

0.030

0.050

50-140

50-140

5.0

5.0

10

10

50

50

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

RRR

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

VOCJ

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3667308

R3667308


L1894670 CONTD....

13PAGE


of

TT163027

Qualifier* Batch



L1894670-21

L1894670-23

BH 3-SS2

BH 3-SS4



Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:

Report Remarks : Volatile test was conducted on sample with headspace. Results may be biased low.Report Remarks : Volatile test was conducted on sample with headspace. Results may be biased low. RRR-Results have been compromised; previouslyextracted before VOC analysis was completed.

Hydrocarbons


Physical Tests

Cyanides


F4 (C34-C50)

Total Hydrocarbons (C6-C50)

Chrom. to baseline at nC50

Surrogate: 2-Bromobenzotrifluoride

Surrogate: 3,4-Dichlorotoluene

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene




Chrysene


Fluoranthene

Fluorene



1-Methylnaphthalene

2-Methylnaphthalene

Naphthalene

Phenanthrene

Pyrene



Conductivity

% Moisture

pH


SAR

Calcium (Ca)

Magnesium (Mg)

ug/g

ug/g

%

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

mS/cm

%

pH units

ug/g

SAR

mg/L

mg/L

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

02-MAR-17

02-MAR-17

03-MAR-17

06-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

06-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

05-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

<50

<72

YES

89.0

93.5

0.108

<0.050

0.204

0.300

0.239

0.325

0.144

0.095

0.273

<0.050

0.654

0.083

0.134

<0.042

<0.030

<0.030

<0.050

0.739

0.573

94.4

92.4

0.228

9.84

7.77

<0.050

1.39

12.8

1.1

50

72

60-140

60-140

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.042

0.030

0.030

0.050

0.050

0.050

50-140

50-140

0.0040

0.10

0.10

0.050

0.10

1.0

1.0

R3667308

R3667308

R3667308

R3666703

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668063

R3666496

R3667405

R3668305

R3668241

R3668241

R3668241


L1894670 CONTD....

14PAGE


of

TT163027

Qualifier* Batch



L1894670-23

L1894670-26

BH 3-SS4

BH 3-SS7



Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:


Metals

Speciated Metals

Physical Tests

Cyanides


Metals

Sodium (Na)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)


Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Mercury (Hg)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)


Conductivity

% Moisture

pH


SAR

Calcium (Ca)

Magnesium (Mg)

Sodium (Na)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

mg/L

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

mS/cm

%

pH units

ug/g

SAR

mg/L

mg/L

mg/L

ug/g

ug/g

ug/g

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

05-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

19.2

<1.0

2.0

36.5

<0.50

<5.0

0.12

<0.50

12.6

4.2

9.2

9.5

0.0158

<1.0

8.9

<1.0

<0.20

<0.50

<1.0

23.5

28.7

<0.20

0.419

19.5

7.74

<0.050

1.51

28.6

3.8

32.5

<1.0

1.3

22.6

1.0

1.0

1.0

1.0

0.50

5.0

0.10

0.50

1.0

1.0

1.0

1.0

0.0050

1.0

1.0

1.0

0.20

0.50

1.0

1.0

5.0

0.20

0.0040

0.10

0.10

0.050

0.10

1.0

1.0

1.0

1.0

1.0

1.0

R3668241

R3668227

R3668227

R3668227

R3668227

R3668227

R3668245

R3668227

R3668227

R3668227

R3668227

R3668227

R3666884

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668194

R3668063

R3666496

R3667405

R3668305

R3668241

R3668241

R3668241

R3668241

R3668227

R3668227

R3668227


L1894670 CONTD....

15PAGE


of

TT163027

Qualifier* Batch



L1894670-26

L1894670-29

BH 3-SS7

BH 1-SS1, SS2, SS3, SS4. SS5, SS6, SS7 (COMPOSITE)



Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:

Metals

Speciated Metals

Sample Preparation

TCLP Extractables

Beryllium (Be)

Boron (B)


Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Mercury (Hg)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)


Initial pH

Final pH

Acenaphthene

Acenaphthylene

Anthracene

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Benzo(a)anthracene

Benzo(a)pyrene




Fluoride (F)

Nitrate and Nitrite as N

Nitrate-N

Nitrite-N

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

pH units

pH units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

02-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

02-MAR-17

02-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

<0.50

<5.0

<0.10

<0.50

8.5

3.0

6.2

2.3

<0.0050

<1.0

5.8

<1.0

<0.20

<0.50

<1.0

17.2

13.2

<0.20

8.83

5.44

<0.0050

<0.0050

<0.0050

<0.00020

<0.00020

<0.00020

<0.00020

<0.0050

<0.0010

<0.0050

<0.0050

<0.10

<10

<4.0

<2.0

<2.0

0.50

5.0

0.10

0.50

1.0

1.0

1.0

1.0

0.0050

1.0

1.0

1.0

0.20

0.50

1.0

1.0

5.0

0.20

0.10

0.10

0.0050

0.0050

0.0050

0.00020

0.00020

0.00020

0.00020

0.0050

0.0010

0.0050

0.0050

0.10

10

4.0

2.0

2.0

R3668227

R3668227

R3668245

R3668227

R3668227

R3668227

R3668227

R3668227

R3666884

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668227

R3668194

R3667245

R3667245

R3668323

R3668323

R3668323

R3668436

R3668436

R3668436

R3668436

R3668323

R3668323

R3668323

R3668323

R3667519

R3668460

R3668460

R3668460

R3668460


L1894670 CONTD....

16PAGE


of

TT163027

Qualifier* Batch



L1894670-29 BH 1-SS1, SS2, SS3, SS4. SS5, SS6, SS7 (COMPOSITE)CLIENT on 23-FEB-17 @ 18:30Sampled By:SOILMatrix:

TCLP Extractables

TCLP Metals

TCLP VOCs



Total PCBs


Arsenic (As)

Barium (Ba)

Boron (B)

Cadmium (Cd)

Chromium (Cr)

Lead (Pb)

Mercury (Hg)

Selenium (Se)

Silver (Ag)

Uranium (U)


1,2-Dichlorobenzene

1,2-Dichloroethane

1,4-Dichlorobenzene

Benzene


Chlorobenzene

Chloroform

Dichloromethane

Methyl Ethyl Ketone

Tetrachloroethylene

Trichloroethylene

Vinyl chloride




Chrysene


Fluoranthene

Fluorene


Naphthalene

Phenanthrene

Pyrene

Quinoline

Surrogate: d10-Acenaphthene

mg/L

%

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

%

%

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

%

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

<0.00040

79.7

<0.050

<0.50

<2.5

<0.0050

<0.050

0.057

<0.00010

<0.025

<0.0050

<0.25

<0.025

0.065

<0.025

<0.025

<0.025

<0.025

<0.025

<0.10

<0.50

<1.0

<0.025

<0.025

<0.050

104.2

103.8

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

95.6

0.00040

40-160

0.050

0.50

2.5

0.0050

0.050

0.050

0.00010

0.025

0.0050

0.25

0.025

0.025

0.025

0.025

0.025

0.025

0.025

0.10

0.50

1.0

0.025

0.025

0.050

70-130

70-130

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

50-150

VTHS

VTHS

VTHS

VTHS

VTHS

VTHS

VTHS

VTHS

VTHS

VTHS

VTHS

VTHS

VTHS

R3668436

R3668436

R3667746

R3667746

R3667746

R3667746

R3667746

R3667746

R3668383

R3667746

R3667746

R3667746

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668323

R3668323

R3668323

R3668323

R3668323

R3668323

R3668323

R3668323

R3668323

R3668323

R3668323


L1894670 CONTD....

17PAGE


of

TT163027

Qualifier* Batch



L1894670-29 BH 1-SS1, SS2, SS3, SS4. SS5, SS6, SS7 (COMPOSITE)CLIENT on 23-FEB-17 @ 18:30Sampled By:SOILMatrix:

Polycyclic Aromatic HydrocarbonsSurrogate: d12-Chrysene

Surrogate: d8-Naphthalene

Surrogate: d10-Phenanthrene

%

%

%

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

97.9

86.9

96.0

50-150

50-150

50-150

R3668323

R3668323

R3668323

B-HWS-R511-WT

CHLORDANE-T-CALC-WT

CN-TCLP-WT

CN-WAD-R511-WT

CR-CR6-IC-WT

DDD-DDE-DDT-CALC-WT

EC-WT

ENDOSULFAN-T-CALC-WT

Reference Information

Boron-HWE-O.Reg 153/04 (July 2011)

Chlordane Total sums

Cyanide for O. Reg 347

Cyanide (WAD)-O.Reg 153/04 (July 2011)

Hexavalent Chromium in Soil

DDD, DDE, DDT sums

Conductivity (EC)

Endosulfan Total sums

L1894670 CONTD....

18PAGE of

TT163027

A dried solid sample is extracted with calcium chloride, the sample undergoes a heating process. After cooling the sample is filtered and analyzed by ICP/OES.

Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011).

Aqueous sample is extracted by liquid/liquid extraction with a solvent mix. After extraction, a number of clean up techniques may be applied, depending on the sample matrix and analyzed by GC/MS.

The sample is extracted with a strong base for 16 hours, and then filtered. The filtrate is then distilled where the cyanide is converted to cyanogen chloride by reacting with chloramine-T, the cyanogen chloride then reacts with a combination of barbituric acid and isonicotinic acid to form a highly colored complex.


This analysis is carried out using procedures adapted from "Test Methods for Evaluating Solid Waste" SW-846, Method 7199, published by the United States Environmental Protection Agency (EPA). The procedure involves analysis for chromium (VI) by ion chromatography using diphenylcarbazide in asulphuric acid solution.



A representative subsample is tumbled with de-ionized (DI) water. The ratio of water to soil is 2:1 v/w. After tumbling the sample is then analyzed by a conductivity meter.



ALS Test Code Test Description

Soil

Soil

Waste

Soil

Soil

Soil

Soil

Soil

DLM

LCS-H

MES

RRR

VOCJ

VTHS

Detection Limit Adjusted due to sample matrix effects (e.g. chemical interference, colour, turbidity).

Lab Control Sample recovery was above ALS DQO. Non-detected sample results are considered reliable. Other results, if reported, have been qualified.Data Quality Objective was marginally exceeded (by < 10% absolute) for < 10% of analytes in a Multi-Element Scan / Multi-Parameter Scan (considered acceptable as per OMOE & CCME).Refer to Report Remarks for issues regarding this analysis

Soil jar was submitted as VOC sample container. VOC results may be biased low, and do not meet federal (CCME) or provincial requirements (for BC, AB-Tier1, MB, ON, SK).Volatile test was conducted on sample with headspace. Results may be biased low.

Sample Parameter Qualifier key listed:

HW EXTR, EPA 6010B

CALCULATION

APHA 4500CN C E

MOE 3015/APHA 4500CN I-WAD

SW846 3060A/7199

CALCULATION

MOEE E3138

CALCULATION

Method Reference**

Description Qualifier

Matrix

Applies to Sample Number(s)Parameter Qualifier

L1894670-1, -11, -20L1894670-1, -11, -20L1894670-1, -11, -20L1894670-21L1894670-21

EndrinEndrinMethoxychlorAcetoneMethyl Ethyl Ketone

LCS-HMESMESMESMES

QC Samples with Qualifiers & Comments:

Laboratory Control SampleMatrix SpikeMatrix SpikeMatrix SpikeMatrix Spike

QC Type Description

Test Method References:


F-TCLP-WT

F1-F4-511-CALC-WT

F1-HS-511-WT

F2-F4-511-WT

HG-200.2-CVAA-WT

HG-TCLP-WT

LEACH-TCLP-WT

MET-200.2-CCMS-WT


Fluoride (F) for O. Reg 347

F1-F4 Hydrocarbon Calculated Parameters

F1-O.Reg 153/04 (July 2011)

F2-F4-O.Reg 153/04 (July 2011)

Mercury in Soil by CVAAS

Mercury (CVAA) for O.Reg 347

Leachate Procedure for Reg 347

Metals in Soil by CRC ICPMS

L1894670 CONTD....

19PAGE of

TT163027

Analytical methods used for analysis of CCME Petroleum Hydrocarbons have been validated and comply with the Reference Method for the CWS PHC.

Hydrocarbon results are expressed on a dry weight basis.

In cases where results for both F4 and F4G are reported, the greater of the two results must be used in any application of the CWS PHC guidelines andthe gravimetric heavy hydrocarbons cannot be added to the C6 to C50 hydrocarbons. In samples where BTEX and F1 were analyzed , F1-BTEX represents a value where the sum of Benzene, Toluene, Ethylbenzene and total Xylenes hasbeen subtracted from F1.

In samples where PAHs, F2 and F3 were analyzed, F2-Naphth represents the result where Naphthalene has been subtracted from F2. F3-PAH represents a result where the sum of Benzo(a)anthracene, Benzo(a)pyrene, Benzo(b)fluoranthene, Benzo(k)fluoranthene, Dibenzo(a,h)anthracene, Fluoranthene, Indeno(1,2,3-cd)pyrene, Phenanthrene, and Pyrene has been subtracted from F3.

Unless otherwise qualified, the following quality control criteria have been met for the F1 hydrocarbon range:1. All extraction and analysis holding times were met.2. Instrument performance showing response factors for C6 and C10 within 30% of the response factor for toluene.3. Linearity of gasoline response within 15% throughout the calibration range.

Unless otherwise qualified, the following quality control criteria have been met for the F2-F4 hydrocarbon ranges:1. All extraction and analysis holding times were met.2. Instrument performance showing C10, C16 and C34 response factors within 10% of their average.3. Instrument performance showing the C50 response factor within 30% of the average of the C10, C16 and C34 response factors.4. Linearity of diesel or motor oil response within 15% throughout the calibration range.

Fraction F1 is determined by extracting a soil or sediment sample as received with methanol, then analyzing by headspace-GC/FID.

Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG must be reported).

Petroleum Hydrocarbons (F2-F4 fractions) are extracted from soil with 1:1 hexane:acetone using a rotary extractor. Extracts are treated with silica gel to remove polar organic interferences. F2, F3, & F4 are analyzed by GC-FID. F4G-sg is analyzed gravimetrically.

Notes: 1. F2 (C10-C16): Sum of all hydrocarbons that elute between nC10 and nC16.2. F3 (C16-C34): Sum of all hydrocarbons that elute between nC16 and nC34.3. F4 (C34-C50): Sum of all hydrocarbons that elute between nC34 and nC50.4. F4G: Gravimetric Heavy Hydrocarbons5. F4G-sg: Gravimetric Heavy Hydrocarbons (F4G) after silica gel treatment.6. Where both F4 (C34-C50) and F4G-sg are reported for a sample, the larger of the two values is used for comparison against the relevant CCME guideline for F4. 7. F4G-sg cannot be added to the C6 to C50 hydrocarbon results to obtain an estimate of total extractable hydrocarbons. 8. This method is validated for use. 9. Data from analysis of validation and quality control samples is available upon request.10. Reported results are expressed as milligrams per dry kilogram, unless otherwise indicated.


Soil samples are digested with nitric and hydrochloric acids, followed by analysis by CVAAS.


Inorganic and Semi-Volatile Organic contaminants are leached from waste samples in strict accordance with US EPA Method 1311, "Toxicity Characteristic Leaching Procedure" (TCLP). Test results are reported in leachate concentration units (normally mg/L).

This method uses a heated strong acid digestion with HNO3 and HCl and is intended to liberate metals that may be environmentally available. Silicate

Waste

Soil

Soil

Soil

Soil

Waste

Waste

Soil

APHA 4110 B-Ion Chromatography

CCME CWS-PHC, Pub #1310, Dec 2001-S

E3398/CCME TIER 1-HS

MOE DECPH-E3398/CCME TIER 1

EPA 200.2/1631E (mod)

SW846 7470A

EPA 1311

EPA 200.2/6020A (mod)


MET-TCLP-WT

METHYLNAPS-CALC-WT

MOISTURE-WT

N2N3-TCLP-WT

PAH-511-WT

PAH-TCLP-WT

PCB-511-WT

PCB-TCLP-WT

PEST-OC-511-WT

PEST-PAHERB-WT

PH-WT

SAR-R511-WT

VOC-1,3-DCP-CALC-WT

VOC-511-HS-WT


O.Reg 347 TCLP Leachable Metals

ABN-Calculated Parameters

% Moisture

Nitrate/Nitrite-N for O. Reg 347

PAH-O.Reg 153/04 (July 2011)

PAH for O. Reg 347

PCB-O.Reg 153/04 (July 2011)

PCBs for O. Reg 347

OC Pesticides-O.Reg 153/04 (July 2011)

Phenoxy Acid Herbicides by GC/MS

pH

SAR-O.Reg 153/04 (July 2011)

Regulation 153 VOCs

VOC-O.Reg 153/04 (July 2011)

L1894670 CONTD....

20PAGE of

TT163027

minerals are not solubilized. Dependent on sample matrix, some metals may be only partially recovered, including Al, Ba, Be, Cr, Sr, Ti, Tl, V, W, and Zr. Volatile forms of sulfur (including sulfide) may not be captured, as they may be lost during sampling, storage, or digestion. Analysis is by Collision/Reaction Cell ICPMS.


A representative sub-sample of soil is fortified with deuterium-labelled surrogates and a mechanical shaking techniqueis used to extract the sample with a mixture of methanol and toluene. The extracts are concentrated and analyzed by GC/MS. Depending on the analytical GC/MS column used benzo(j)fluoranthene may chromatographically co-elute with benzo(b)fluoranthene or benzo(k)fluoranthene.


Samples are leached according to TCLP protocol and then the aqueous leachate is extracted and the resulting extracts are analyzed on GC/MSD. Depending on the analytical GC/MS column used benzo(j)fluoranthene may chromatographically co-elute with benzo(b)fluoranthene or benzo(k)fluoranthene.

An aliquot of a solid sample is extracted with a solvent, extract is cleaned up and analyzed on the GC/MS.


Soil sample is extracted in a solvent, after extraction a number of clean up techniques may be applied, depending on the sample matrix and analyzed byGC/MS.


Soil and sediment samples are dried by mixing with a desiccant prior to extraction with a solvent mixture. The extracts are dried, concentrated and exchanged into a solvent, derivatized and analyzed by GC/MS.

A minimum 10g portion of the sample is extracted with 20mL of 0.01M calcium chloride solution by shaking for at least 30 minutes. The aqueous layer isseparated from the soil and then analyzed using a pH meter and electrode.


A dried, disaggregated solid sample is extracted with deionized water, the aqueous extract is separated from the solid, acidified and then analyzed usinga ICP/OES. The concentrations of Na, Ca and Mg are reported as per CALA requirements for calculated parameters. These individual parameters are not for comparison to any guideline.


Soil and sediment samples are extracted in methanol and analyzed by headspace-GC/MS.

Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011), unless a subset of the Analytical Test Group (ATG) has been requested (the Protocol states that all analytes in an ATG

Waste

Soil

Soil

Waste

Soil

Waste

Soil

Waste

Soil

Soil

Soil

Soil

Soil

Soil

EPA 200.8

SW846 8270

Gravimetric: Oven Dried


SW846 3510/8270

SW846 8270 (PAH)

SW846 3510/8082

SW846 8270

SW846 8270 (511)

SW846 8270

MOEE E3137A

SW846 6010C

SW8260B/SW8270C

SW846 8260 (511)


VOC-TCLP-WT

XYLENES-SUM-CALC-WT


VOC for O. Reg 347

Sum of Xylene Isomer Concentrations

L1894670 CONTD....

21PAGE of

TT163027

must be reported).

A sample of waste is leached in a zero headspace extractor at 30–2 rpm for 18–2.0 hours with the appropriate leaching solution. After tumbling the leachate is analyzed directly by headspace technology, followed by GC/MS using internal standard quantitation.

Total xylenes represents the sum of o-xylene and m&p-xylene.

Waste

Soil

SW846 8260

CALCULATION

** ALS test methods may incorporate modifications from specified reference methods to improve performance.

The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below:

Laboratory Definition Code Laboratory Location

WT ALS ENVIRONMENTAL - WATERLOO, ONTARIO, CANADA

GLOSSARY OF REPORT TERMSSurrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there.mg/kg - milligrams per kilogram based on dry weight of samplemg/kg wwt - milligrams per kilogram based on wet weight of samplemg/kg lwt - milligrams per kilogram based on lipid weight of samplemg/L - unit of concentration based on volume, parts per million.< - Less than.D.L. - The reporting limit.N/A - Result not available. Refer to qualifier code and definition for explanation.

Test results reported relate only to the samples as received by the laboratory.UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION.Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.

Chain of Custody Numbers:


Quality Control ReportPage 1 of

Client:

Contact:

AMEC Foster Wheeler - Mississauga160 TRADERS BLVD., SUITE 110 MISSISSAUGA ON L4Z 3K7ALESSANDRO PELLERITO

Report Date: 16-JUN-17Workorder: L1894670

Test Matrix Reference Result Qualifier Units RPD Limit Analyzed

B-HWS-R511-WT

CN-WAD-R511-WT

CR-CR6-IC-WT

Soil

Soil

Soil

R3668245

R3668305

R3668194

R3668453

Batch

Batch

Batch

Batch

DUP

IRM

LCS

MB

DUP

LCS

MB

MS

CRM

DUP

LCS

MB

CRM

DUP

LCS

MB

WG2488247-4

WG2488247-2

WG2488247-3

WG2488247-1

WG2487563-3

WG2487563-2

WG2487563-1

WG2487563-4

WG2487564-3

WG2487564-4

WG2487564-2

WG2487564-1

WG2488281-4

WG2488281-3

WG2488281-2

WG2488281-1

L1896249-1

HOTB-SAL_SOIL5

L1894670-1

L1894670-1

WT-SQC012

L1893469-1

WT-SQC012

L1896875-14

















0.11

116.0

104.5

<0.10

<0.050

92.1

<0.050

95.8

108.6

<0.20

96.8

<0.20

107.5

<0.20

105.1

<0.20

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

15

N/A

N/A

N/A

30

35

35

35

70-130

70-130

80-120

70-130

70-130

80-120

70-130

80-120

ug/g

%

%

ug/g

ug/g

%

ug/g

%

%

ug/g

%

ug/g

%

ug/g

%

ug/g

0.13

<0.050

<0.20

<0.20

0.1

0.05

0.2

0.2

RPD-NA

RPD-NA

RPD-NA

26


Client:

Contact:




EC-WT

F1-HS-511-WT

F2-F4-511-WT

Soil

Soil

Soil

R3668063

R3666703

R3667308

Batch

Batch

Batch

DUP

LCS

LCS

MB

DUP

LCS

MB

MS

CRM

DUP

LCS

MB

WG2488250-4

WG2489144-1

WG2489144-2

WG2488250-1

WG2487973-4

WG2487973-2

WG2487973-1

WG2487973-7

WG2487547-3

WG2487547-5

WG2487547-2

WG2487547-1

WG2488250-3

WG2487973-3

WG2487973-6

ALS PHC2 IRM

WG2487547-4

Conductivity

Conductivity

Conductivity

Conductivity

F1 (C6-C10)

F1 (C6-C10)

F1 (C6-C10)


F1 (C6-C10)

F2 (C10-C16)

F3 (C16-C34)

F4 (C34-C50)

F2 (C10-C16)

F3 (C16-C34)

F4 (C34-C50)

F2 (C10-C16)

F3 (C16-C34)

F4 (C34-C50)

F2 (C10-C16)

F3 (C16-C34)

F4 (C34-C50)

0.264

101.5

101.3

<0.0040

<5.0

105.8

<5.0

97.1

99.4

90.2

89.2

89.2

<10

<50

<50

105.5

105.5

91.1

<10

<50

<50

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

1.5

N/A

N/A

N/A

N/A

20

30

30

30

30

90-110

90-110

80-120

60-140

70-130

70-130

70-130

80-120

80-120

80-120

mS/cm

%

%

mS/cm

ug/g

%

ug/g

%

%

%

%

%

ug/g

ug/g

ug/g

%

%

%

ug/g

ug/g

ug/g

0.268

<5.0

<10

<50

<50

0.004

5

60-140

10

50

50

RPD-NA

RPD-NA

RPD-NA

RPD-NA

26


Client:

Contact:




F2-F4-511-WT

HG-200.2-CVAA-WT

MET-200.2-CCMS-WT

Soil

Soil

Soil

R3667308

R3666884

R3668227

Batch

Batch

Batch

MB

CRM

DUP

LCS

MB

CRM

DUP

WG2487547-1

WG2488253-2

WG2488253-6

WG2488253-3

WG2488253-1

WG2488253-2

WG2488253-6

WT-CANMET-TILL1

WG2488253-5

WT-CANMET-TILL1

WG2488253-5

F4 (C34-C50)


Mercury (Hg)

Mercury (Hg)

Mercury (Hg)

Mercury (Hg)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)

Antimony (Sb)

Arsenic (As)

<50

87.0

90.7

0.164

104.5

<0.0050

96.8

105.4

101.9

94.2

92.8

102.5

96.3

98.0

90.2

92.9

101.4

87.1

100.5

89.1

98.7

103.0

92.8

0.21

3.22

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

9.0

1.3

40

30

70-130

80-120

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

ug/g

%

%

ug/g

%

mg/kg

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

ug/g

0.179

0.20

3.13

50

60-140

0.005

26


Client:

Contact:




MET-200.2-CCMS-WT Soil

R3668227BatchDUP

LCS

WG2488253-6

WG2488253-4

WG2488253-5Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)

Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)

Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

3.22

54.5

0.33

<5.0

0.287

20.3

4.92

19.0

26.8

0.32

11.9

0.32

0.20

0.079

0.439

23.3

61.7

99.0

99.0

99.7

97.9

100.3

96.8

97.9

94.2

95.8

95.4

98.6

97.0

95.3

96.7

91.8

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

2.9

0.8

4.4

N/A

5.5

9.2

1.1

2.9

3.9

3.6

8.8

11

9.4

3.5

1.7

0.1

5.1

30

40

30

30

30

30

30

30

40

40

30

30

40

30

30

30

30

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

3.13

55.0

0.34

5.3

0.272

18.5

4.97

18.4

25.8

0.33

10.9

0.29

0.18

0.082

0.432

23.3

58.7

RPD-NA

26


Client:

Contact:




MET-200.2-CCMS-WT

MOISTURE-WT

PAH-511-WT

Soil

Soil

Soil

R3668227

R3666496

R3668293

Batch

Batch

Batch

LCS

MB

DUP

LCS

MB

DUP

WG2488253-4

WG2488253-1

WG2487549-3

WG2487549-2

WG2487549-1

WG2487269-4

L1894670-26

WG2487269-3

Uranium (U)

Vanadium (V)

Zinc (Zn)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)

Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)

% Moisture

% Moisture

% Moisture

1-Methylnaphthalene

94.5

101.3

89.3

<0.10

<0.10

<0.50

<0.10

<5.0

<0.020

<0.50

<0.10

<0.50

<0.50

<0.10

<0.50

<0.20

<0.10

<0.050

<0.050

<0.20

<2.0

20.0

100.1

<0.10

<0.030

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

04-MAR-17

2.6

N/A

20

40

80-120

80-120

80-120

90-110

%

%

%

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

%

%

%

ug/g

19.5

<0.030

0.1

0.1

0.5

0.1

5

0.02

0.5

0.1

0.5

0.5

0.1

0.5

0.2

0.1

0.05

0.05

0.2

2

0.1

RPD-NA

26


Client:

Contact:




PAH-511-WT Soil

R3668293BatchDUP

LCS

WG2487269-4

WG2487269-2

WG2487269-32-Methylnaphthalene

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene




Chrysene


Fluoranthene

Fluorene


Naphthalene

Phenanthrene

Pyrene

1-Methylnaphthalene

2-Methylnaphthalene

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene




Chrysene


Fluoranthene

Fluorene


<0.030

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

108.7

107.9

109.0

105.5

115.5

110.1

103.4

112.0

95.4

111.0

113.5

97.5

96.7

108.3

98.8

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

<0.030

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

26


Client:

Contact:




PAH-511-WT Soil

R3668293BatchLCS

MB

MS

WG2487269-2

WG2487269-1

WG2487269-5 WG2487269-3

Naphthalene

Phenanthrene

Pyrene

1-Methylnaphthalene

2-Methylnaphthalene

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene




Chrysene


Fluoranthene

Fluorene


Naphthalene

Phenanthrene

Pyrene



1-Methylnaphthalene

2-Methylnaphthalene

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene



112.0

108.4

98.1

<0.030

<0.030

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

90.4

83.9

108.3

106.9

108.0

101.8

114.1

106.3

101.5

112.2

86.2

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

%

%

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

%

%

%

%

%

%

%

%

%

0.03

0.03

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

50-140

50-140

26


Client:

Contact:




PAH-511-WT

PCB-511-WT

PEST-OC-511-WT

Soil

Soil

Soil

R3668293

R3668264

Batch

Batch

MS

DUP

LCS

MB

MS

WG2487269-5

WG2487269-4

WG2487269-2

WG2487269-1

WG2487269-5

WG2487269-3

WG2487269-3

WG2487269-3


Chrysene


Fluoranthene

Fluorene


Naphthalene

Phenanthrene

Pyrene

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260


Aroclor 1242

Aroclor 1254

Aroclor 1260

113.3

114.7

89.4

98.6

104.9

87.5

111.3

109.4

100.3

<0.010

<0.010

<0.010

<0.010

99.3

83.2

105.8

101.7

<0.010

<0.010

<0.010

<0.010

93.8

100.1

105.0

102.5

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

N/A

N/A

N/A

N/A

40

40

40

40

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

60-140

60-140

60-140

60-140

60-140

60-140

60-140

%

%

%

%

%

%

%

%

%

ug/g

ug/g

ug/g

ug/g

%

%

%

%

ug/g

ug/g

ug/g

ug/g

%

%

%

%

<0.010

<0.010

<0.010

<0.010

0.01

0.01

0.01

0.01

60-140

RPD-NA

RPD-NA

RPD-NA

RPD-NA

26


Client:

Contact:




PEST-OC-511-WT Soil

R3667383BatchDUP

LCS

WG2487703-4

WG2487703-2

WG2487703-3Aldrin

a-chlordane

g-chlordane

op-DDD

pp-DDD

o,p-DDE

pp-DDE

op-DDT

pp-DDT

Dieldrin

Endosulfan I

Endosulfan II

Endrin


Heptachlor

Heptachlor Epoxide

Hexachlorobenzene

Hexachlorobutadiene

Hexachloroethane

Methoxychlor

Aldrin

a-chlordane

g-chlordane

op-DDD

pp-DDD

o,p-DDE

pp-DDE

op-DDT

pp-DDT

Dieldrin

Endosulfan I

Endosulfan II

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.010

<0.020

<0.020

<0.010

<0.010

<0.010

<0.020

117.2

92.1

97.0

91.6

94.9

85.3

88.3

93.7

88.9

89.0

88.2

92.6

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

%

%

%

%

%

%

%

%

%

%

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.010

<0.020

<0.020

<0.010

<0.010

<0.010

<0.020

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

26


Client:

Contact:




PEST-OC-511-WT Soil

R3667383BatchLCS

MB

MS

WG2487703-2

WG2487703-1

WG2487703-5 WG2487703-3

Endrin


Heptachlor

Heptachlor Epoxide

Hexachlorobenzene

Hexachlorobutadiene

Hexachloroethane

Methoxychlor

Aldrin

a-chlordane

g-chlordane

op-DDD

pp-DDD

o,p-DDE

pp-DDE

op-DDT

pp-DDT

Dieldrin

Endosulfan I

Endosulfan II

Endrin


Heptachlor

Heptachlor Epoxide

Hexachlorobenzene

Hexachlorobutadiene

Hexachloroethane

Methoxychlor



Aldrin

a-chlordane

141.0

98.1

128.7

102.4

98.1

99.4

112.5

122.5

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.020

<0.010

<0.020

<0.020

<0.010

<0.010

<0.010

<0.020

98.9

98.0

123.2

92.7

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

%

%

%

%

%

%

%

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

%

%

LCS-H

0.02

0.02

0.02

0.02

0.02

0.02

0.02

0.02

0.02

0.02

0.02

0.02

0.02

0.01

0.02

0.02

0.01

0.01

0.01

0.02

50-140

50-140

26


Client:

Contact:




PEST-OC-511-WT

PEST-PAHERB-WT

Soil

Soil

R3667383

R3668198

Batch

Batch

MS

DUP

LCS

WG2487703-5

WG2487701-4

WG2487701-2

WG2487703-3

WG2487701-3

g-chlordane

op-DDD

pp-DDD

o,p-DDE

pp-DDE

op-DDT

pp-DDT

Dieldrin

Endosulfan I

Endosulfan II

Endrin


Heptachlor

Heptachlor Epoxide

Hexachlorobenzene

Hexachlorobutadiene

Hexachloroethane

Methoxychlor

2,4,5-TP

MCPA

Mecoprop

2,4,5-T

2,4-D

Bromoxynil

Dinoseb

Dicamba

Picloram

2,4,5-TP

MCPA

Mecoprop

95.7

92.0

101.9

83.4

92.0

94.6

102.3

87.7

87.9

93.5

156.0

97.8

132.2

100.6

100.7

98.0

110.9

144.9

<0.080

<0.30

<0.30

<0.080

<0.080

<0.080

<0.080

<0.080

<0.080

117.2

116.4

124.6

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

50

50

50

50

50

50

50

50

50

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

60-140

60-140

60-140

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

%

%

MES

MES

<0.080

<0.30

<0.30

<0.080

<0.080

<0.080

<0.080

<0.080

<0.080

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

26


Client:

Contact:




PEST-PAHERB-WT

PH-WT

Soil

Soil

R3668198

R3667405

Batch

Batch

LCS

MB

MS

DUP

LCS

WG2487701-2

WG2487701-1

WG2487701-5

WG2487560-1

WG2488363-1

WG2487701-3

L1896309-9

Mecoprop

2,4,5-T

2,4-D

Bromoxynil

Dinoseb

Dicamba

Picloram

2,4,5-TP

MCPA

Mecoprop

2,4,5-T

2,4-D

Bromoxynil

Dinoseb

Dicamba

Picloram


2,4,5-TP

MCPA

Mecoprop

2,4,5-T

2,4-D

Bromoxynil

Dinoseb

Dicamba

Picloram

pH

pH

124.6

111.0

115.7

108.4

107.8

110.1

35.8

<0.080

<0.30

<0.30

<0.080

<0.080

<0.080

<0.080

<0.080

<0.080

103.3

123.1

120.8

129.1

114.7

120.4

105.8

118.7

116.2

39.0

7.88

7.01

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

03-MAR-17

03-MAR-17

0.02 0.3

60-140

60-140

60-140

60-140

30-150

60-140

30-150

50-140

50-140

50-140

50-150

50-140

50-140

50-140

50-140

30-150

6.7-7.3

%

%

%

%

%

%

%

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

%

%

%

%

%

%

%

%

%

%

pH units

pH units

7.86

0.08

0.3

0.3

0.08

0.08

0.08

0.08

0.08

0.08

50-150

J

26


Client:

Contact:




SAR-R511-WT

VOC-511-HS-WT

Soil

Soil

R3668241

R3666703

Batch

Batch

DUP

IRM

MB

DUP

WG2488250-4

WG2488250-2

WG2488250-1

WG2487973-4

WG2488250-3

WT SAR1

WG2487973-3

Calcium (Ca)

Sodium (Na)

Magnesium (Mg)

Calcium (Ca)

Sodium (Na)

Magnesium (Mg)

Calcium (Ca)

Sodium (Na)

Magnesium (Mg)





1,1-Dichloroethane


1,2-Dibromoethane

1,2-Dichlorobenzene

1,2-Dichloroethane

1,2-Dichloropropane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

Acetone

Benzene


Bromoform

Bromomethane


Chlorobenzene

27.6

4.2

1.9

98.0

95.5

108.8

<1.0

<1.0

<1.0

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.50

<0.0068

<0.050

<0.050

<0.050

<0.050

<0.050

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

15

15

15

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

30

30

30

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

70-130

70-130

70-130

mg/L

mg/L

mg/L

%

%

%

mg/L

mg/L

mg/L

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

23.8

3.6

1.7

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.50

<0.0068

<0.050

<0.050

<0.050

<0.050

<0.050

1

1

1

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

26


Client:

Contact:




VOC-511-HS-WT Soil

R3666703BatchDUP

LCS

WG2487973-4

WG2487973-2

WG2487973-3Chloroform





Ethylbenzene

n-Hexane

Methylene Chloride

MTBE

m+p-Xylenes

Methyl Ethyl Ketone


o-Xylene

Styrene

Tetrachloroethylene

Toluene



Trichloroethylene


Vinyl chloride





1,1-Dichloroethane


1,2-Dibromoethane

1,2-Dichlorobenzene

1,2-Dichloroethane

1,2-Dichloropropane

1,3-Dichlorobenzene

<0.050

<0.050

<0.030

<0.050

<0.050

<0.018

<0.050

<0.050

<0.050

<0.030

<0.50

<0.50

<0.020

<0.050

<0.050

<0.080

<0.050

<0.030

<0.010

<0.050

<0.020

98.5

113.4

99.6

107.6

103.2

92.8

107.8

102.4

114.0

107.0

97.9

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

60-130

60-130

60-130

60-130

60-130

60-130

70-130

70-130

60-130

70-130

70-130

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

%

%

%

%

%

%

%

%

%

<0.050

<0.050

<0.030

<0.050

<0.050

<0.018

<0.050

<0.050

<0.050

<0.030

<0.50

<0.50

<0.020

<0.050

<0.050

<0.080

<0.050

<0.030

<0.050

<0.050

<0.020

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

26


Client:

Contact:




VOC-511-HS-WT Soil

R3666703BatchLCS

MB

WG2487973-2

WG2487973-1

1,4-Dichlorobenzene

Acetone

Benzene


Bromoform

Bromomethane


Chlorobenzene

Chloroform





Ethylbenzene

n-Hexane

Methylene Chloride

MTBE

m+p-Xylenes

Methyl Ethyl Ketone


o-Xylene

Styrene

Tetrachloroethylene

Toluene



Trichloroethylene


Vinyl chloride





101.5

131.0

106.9

105.7

107.9

102.0

97.1

103.3

106.5

106.3

107.8

110.7

57.3

90.2

100.3

110.3

102.1

95.0

129.9

112.0

93.7

96.3

91.2

94.8

100.4

102.8

99.5

98.7

86.2

<0.050

<0.050

<0.050

<0.050

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

70-130

60-140

70-130

50-140

70-130

50-140

70-130

70-130

70-130

70-130

70-130

60-130

50-140

70-130

70-130

70-130

70-130

70-130

60-140

60-140

70-130

70-130

60-130

70-130

60-130

70-130

60-130

50-140

60-140

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

ug/g

ug/g

ug/g

ug/g

0.05

0.05

0.05

0.05

26


Client:

Contact:




VOC-511-HS-WT Soil

R3666703BatchMBWG2487973-1

1,1-Dichloroethane


1,2-Dibromoethane

1,2-Dichlorobenzene

1,2-Dichloroethane

1,2-Dichloropropane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

Acetone

Benzene


Bromoform

Bromomethane


Chlorobenzene

Chloroform





Ethylbenzene

n-Hexane

Methylene Chloride

MTBE

m+p-Xylenes

Methyl Ethyl Ketone


o-Xylene

Styrene

Tetrachloroethylene

Toluene



<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.50

<0.0068

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.030

<0.050

<0.050

<0.018

<0.050

<0.050

<0.050

<0.030

<0.50

<0.50

<0.020

<0.050

<0.050

<0.080

<0.050

<0.030

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.5

0.0068

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.03

0.05

0.05

0.018

0.05

0.05

0.05

0.03

0.5

0.5

0.02

0.05

0.05

0.08

0.05

0.03

26


Client:

Contact:




VOC-511-HS-WT Soil

R3666703BatchMB

MS

WG2487973-1

WG2487973-5 WG2487973-3

Trichloroethylene


Vinyl chloride







1,1-Dichloroethane


1,2-Dibromoethane

1,2-Dichlorobenzene

1,2-Dichloroethane

1,2-Dichloropropane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

Acetone

Benzene


Bromoform

Bromomethane


Chlorobenzene

Chloroform





Ethylbenzene

n-Hexane

Methylene Chloride

MTBE

<0.010

<0.050

<0.020

103.9

95.7

112.3

127.1

114.3

121.5

117.9

105.5

122.3

115.5

129.2

122.6

110.2

114.0

149.3

121.9

120.7

121.7

113.8

111.2

116.8

121.6

120.8

121.0

125.5

65.4

102.9

115.3

124.8

115.3

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

ug/g

ug/g

ug/g

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

MES

0.01

0.05

0.02

50-140

50-140

26


Client:

Contact:




VOC-511-HS-WT

CN-TCLP-WT

F-TCLP-WT

HG-TCLP-WT

Soil

Waste

Waste

Waste

R3666703

R3667519

R3668460

Batch

Batch

Batch

MS

DUP

LCS

MB

MS

DUP

LCS

MB

MS

WG2487973-5

WG2488553-3

WG2488553-2

WG2488553-1

WG2488553-4

WG2488480-3

WG2488480-2

WG2488480-1

WG2488480-4

WG2487973-3

L1896258-1

L1896258-1

L1896258-1

L1896258-1

m+p-Xylenes

Methyl Ethyl Ketone


o-Xylene

Styrene

Tetrachloroethylene

Toluene



Trichloroethylene


Vinyl chloride





Fluoride (F)

Fluoride (F)

Fluoride (F)

Fluoride (F)

107.7

145.3

125.9

106.5

109.0

103.8

107.6

113.9

114.8

113.5

112.2

97.0

<0.10

95.0

<0.10

89.5

<10

90.4

<10

88.5

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

N/A

N/A

20

30

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

70-130

50-150

70-130

50-150

%

%

%

%

%

%

%

%

%

%

%

%

mg/L

%

mg/L

%

mg/L

%

mg/L

%

MES

<0.10

<10

0.1

10

RPD-NA

RPD-NA

26


Client:

Contact:




HG-TCLP-WT

MET-TCLP-WT

Waste

Waste

R3668383

R3667746

Batch

Batch

DUP

LCS

MB

MS

DUP

LCS

MB

WG2489377-3

WG2489377-2

WG2489377-1

WG2489377-4

WG2488668-4

WG2488668-2

WG2488668-1

L1895710-8

L1895710-8

WG2488668-3

Mercury (Hg)

Mercury (Hg)

Mercury (Hg)

Mercury (Hg)

Silver (Ag)

Arsenic (As)

Boron (B)

Barium (Ba)

Cadmium (Cd)

Chromium (Cr)

Lead (Pb)

Selenium (Se)

Uranium (U)

Silver (Ag)

Arsenic (As)

Boron (B)

Barium (Ba)

Cadmium (Cd)

Chromium (Cr)

Lead (Pb)

Selenium (Se)

Uranium (U)

Silver (Ag)

Arsenic (As)

Boron (B)

Barium (Ba)

<0.00010

103.0

<0.00010

92.3

<0.0050

<0.050

<2.5

<0.50

<0.0050

<0.050

<0.050

<0.025

<0.25

100.5

98.0

89.8

101.1

97.4

94.9

101.1

97.2

105.6

<0.0050

<0.050

<2.5

<0.50

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

50

40

40

40

40

40

40

40

40

40

70-130

50-140

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

mg/L

%

mg/L

%

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

%

%

%

%

%

%

%

%

%

mg/L

mg/L

mg/L

mg/L

<0.00010

<0.0050

<0.050

<2.5

<0.50

<0.0050

<0.050

<0.050

<0.025

<0.25

0.0001

0.005

0.05

2.5

0.5

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

26


Client:

Contact:




MET-TCLP-WT

N2N3-TCLP-WT

PAH-TCLP-WT

Waste

Waste

Waste

R3667746

R3668460

R3668323

Batch

Batch

Batch

MB

MS

DUP

LCS

MB

MS

DUP

WG2488668-1

WG2488668-5

WG2488480-3

WG2488480-2

WG2488480-1

WG2488480-4

WG2489276-5

WG2488668-3

L1896258-1

L1896258-1

WG2489276-3

Cadmium (Cd)

Chromium (Cr)

Lead (Pb)

Selenium (Se)

Uranium (U)

Silver (Ag)

Arsenic (As)

Boron (B)

Barium (Ba)

Cadmium (Cd)

Chromium (Cr)

Lead (Pb)

Selenium (Se)

Uranium (U)

Nitrate-N

Nitrite-N

Nitrate-N

Nitrite-N

Nitrate-N

Nitrite-N

Nitrate-N

Nitrite-N

Acenaphthene

Acenaphthylene

<0.0050

<0.050

<0.050

<0.025

<0.25

112.1

95.2

84.0

100.3

92.9

89.4

89.9

92.3

94.8

<2.0

<2.0

98.4

96.2

<2.0

<2.0

98.5

97.4

<0.0050

<0.0050

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

06-MAR-17

N/A

N/A

N/A

N/A

30

30

50

50

50-150

50-150

50-150

50-150

50-150

50-150

50-150

50-150

50-150

70-130

70-130

50-150

50-150

mg/L

mg/L

mg/L

mg/L

mg/L

%

%

%

%

%

%

%

%

%

mg/L

mg/L

%

%

mg/L

mg/L

%

%

mg/L

mg/L

<2.0

<2.0

<0.0050

<0.0050

0.005

0.05

0.05

0.025

0.25

2

2

RPD-NA

RPD-NA

RPD-NA

RPD-NA

26


Client:

Contact:




PAH-TCLP-WT Waste

R3668323BatchDUP

LCS

WG2489276-5

WG2489276-2

WG2489276-3Anthracene

Benzo(a)anthracene

Benzo(a)pyrene




Chrysene


Fluoranthene

Fluorene


Naphthalene

Phenanthrene

Pyrene

Quinoline

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene




Chrysene


Fluoranthene

Fluorene


Naphthalene

Phenanthrene

Pyrene

Quinoline

<0.0050

<0.0050

<0.0010

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

84.2

85.9

86.4

85.1

87.1

81.0

86.3

85.0

86.3

88.7

87.7

85.1

81.8

79.9

85.4

90.8

120.8

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50-130

50-130

50-130

50-140

60-140

50-140

50-140

50-150

50-140

50-140

50-150

50-150

50-140

50-130

50-130

50-140

50-150

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

<0.0050

<0.0050

<0.0010

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

26


Client:

Contact:




PAH-TCLP-WT Waste

R3668323BatchMB

MS

WG2489276-1

WG2489276-4 WG2489276-3

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene




Chrysene


Fluoranthene

Fluorene


Naphthalene

Phenanthrene

Pyrene

Quinoline



Surrogate: d12-Chrysene


Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene




Chrysene


Fluoranthene

Fluorene

<0.0050

<0.0050

<0.0050

<0.0050

<0.0010

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

90.3

101.0

103.7

100.0

83.9

84.5

85.3

84.3

86.5

79.8

86.1

85.6

84.9

81.3

86.2

83.7

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

50-150

50-150

50-150

50-150

50-150

50-150

50-150

50-150

50-150

50-150

50-150

50-150

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

0.005

0.005

0.005

0.005

0.001

0.005

0.005

0.005

0.005

0.005

0.005

0.005

0.005

0.005

0.005

0.005

0.005

50-150

50-150

50-150

50-150

26


Client:

Contact:




PAH-TCLP-WT

PCB-TCLP-WT

VOC-TCLP-WT

Waste

Waste

Waste

R3668323

R3668436

R3668166

Batch

Batch

Batch

MS

DUP

LCS

MB

MS

DUP

WG2489276-4

WG2489277-5

WG2489277-2

WG2489277-1

WG2489277-4

WG2488272-4

WG2489276-3

WG2489277-3

WG2489277-3

WG2488272-3


Naphthalene

Phenanthrene

Pyrene

Quinoline

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260


Aroclor 1242

Aroclor 1254

Aroclor 1260


1,2-Dichlorobenzene

1,2-Dichloroethane

1,4-Dichlorobenzene

82.1

79.5

84.4

89.3

126.8

<0.00020

<0.00020

<0.00020

<0.00020

76.1

75.4

90.9

93.6

<0.00020

<0.00020

<0.00020

<0.00020

97.2

73.8

85.6

92.8

<0.025

0.921

<0.025

0.068

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

N/A

N/A

N/A

N/A

N/A

1.0

N/A

5.0

50

50

50

50

50

50

50

50

50-150

50-150

50-150

50-150

50-150

65-130

65-130

65-130

65-130

50-150

50-150

50-150

%

%

%

%

%

mg/L

mg/L

mg/L

mg/L

%

%

%

%

mg/L

mg/L

mg/L

mg/L

%

%

%

%

mg/L

mg/L

mg/L

mg/L

<0.00020

<0.00020

<0.00020

<0.00020

<0.025

0.930

<0.025

0.064

0.0002

0.0002

0.0002

0.0002

40-160

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

26


Client:

Contact:




VOC-TCLP-WT Waste

R3668166BatchDUP

LCS

MB

WG2488272-4

WG2488272-1

WG2488272-2

WG2488272-3Benzene


Chlorobenzene

Chloroform

Dichloromethane

Methyl Ethyl Ketone

Tetrachloroethylene

Trichloroethylene

Vinyl chloride


1,2-Dichlorobenzene

1,2-Dichloroethane

1,4-Dichlorobenzene

Benzene


Chlorobenzene

Chloroform

Dichloromethane

Methyl Ethyl Ketone

Tetrachloroethylene

Trichloroethylene

Vinyl chloride


1,2-Dichlorobenzene

1,2-Dichloroethane

1,4-Dichlorobenzene

Benzene


Chlorobenzene

Chloroform

Dichloromethane

Methyl Ethyl Ketone

<0.025

<0.025

<0.025

<0.10

<0.50

<1.0

<0.025

<0.025

<0.050

102.7

99.2

98.2

101.7

104.8

103.4

102.6

103.3

102.6

92.3

102.7

104.5

103.5

<0.025

<0.025

<0.025

<0.025

<0.025

<0.025

<0.025

<0.10

<0.50

<1.0

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

50

50

50

50

50

50

50

50

50

70-130

70-130

70-130

70-130

70-130

60-140

70-130

70-130

70-130

50-150

70-130

70-130

60-130

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

%

%

%

%

%

%

%

%

%

%

%

%

%

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

<0.025

<0.025

<0.025

<0.10

<0.50

<1.0

<0.025

<0.025

<0.050

0.025

0.025

0.025

0.025

0.025

0.025

0.025

0.1

0.5

1

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

26


Client:

Contact:




VOC-TCLP-WT Waste

R3668166BatchMB

MS

WG2488272-2

WG2488272-5 WG2488272-3

Tetrachloroethylene

Trichloroethylene

Vinyl chloride




1,2-Dichlorobenzene

1,2-Dichloroethane

1,4-Dichlorobenzene

Benzene


Chlorobenzene

Chloroform

Dichloromethane

Methyl Ethyl Ketone

Tetrachloroethylene

Trichloroethylene

Vinyl chloride

<0.025

<0.025

<0.050

103.6

107.5

94.0

92.2

103.0

99.96

104.6

99.7

103.4

105.0

102.9

102.7

100.2

103.3

87.3

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

mg/L

mg/L

mg/L

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

0.025

0.025

0.05

70-130

70-130

26

Quality Control Report

Page 26 of


Sample Parameter Qualifier Definitions:


J

LCS-H

MES

RPD-NA

Duplicate results and limits are expressed in terms of absolute difference.

Lab Control Sample recovery was above ALS DQO. Non-detected sample results are considered reliable. Other results, if reported, have been qualified.Data Quality Objective was marginally exceeded (by < 10% absolute) for < 10% of analytes in a Multi-Element Scan / Multi-Parameter Scan (considered acceptable as per OMOE & CCME).Relative Percent Difference Not Available due to result(s) being less than detection limit.

Limit ALS Control Limit (Data Quality Objectives)DUP DuplicateRPD Relative Percent DifferenceN/A Not AvailableLCS Laboratory Control SampleSRM Standard Reference MaterialMS Matrix SpikeMSD Matrix Spike DuplicateADE Average Desorption EfficiencyMB Method BlankIRM Internal Reference MaterialCRM Certified Reference MaterialCCV Continuing Calibration VerificationCVS Calibration Verification StandardLCSD Laboratory Control Sample Duplicate

Legend:

The ALS Quality Control Report is provided to ALS clients upon request. ALS includes comprehensive QC checks with every analysis to ensure our high standards of quality are met. Each QC result has a known or expected target value, which is compared against pre-determined data quality objectives to provide confidence in the accuracy of associated test results.

Please note that this report may contain QC results from anonymous Sample Duplicates and Matrix Spikes that do not originate from this Work Order.

Hold Time Exceedances:

All test results reported with this submission were conducted within ALS recommended hold times.

ALS recommended hold times may vary by province. They are assigned to meet known provincial and/or federal government requirements. In the absence of regulatory hold times, ALS establishes recommendations based on guidelines published by the US EPA, APHA Standard Methods, or Environment Canada (where available). For more information, please contact ALS.

Client:

Contact:


26

Printed on 3/3/2017 2:37:41 PM

ALS Sample ID: L1894670-21Client Sample ID: BH3-SS2

2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0

Time - Minutes

0

50

100

150

200

250

300

350

400

450

500

Response - M

illiVolts


28-FEB-17


Date Received:AMEC Foster Wheeler - Mississauga

160 TRADERS BLVD., SUITE 110MISSISSAUGA ON L4Z 3K7

ATTN: ALESSANDRO PELLERITOFINAL REV. 216-JUN-17 14:43 (MT)Report Date:

Version:



____________________________________________

Mary-Lynn PiresClient Services Supervisor

ADDRESS: 95 West Beaver Creek Road, Unit 1, Richmond Hill, ON L4B 1H2 Canada | Phone: +1 905 881 9887 | Fax: +1 905 881 8062


ADDITIONAL 01-MAR-17 14:17Comments:


C of C Numbers:Legal Site Desc:


L1895710 CONTD....

2PAGE


of

TT163027

Qualifier* Batch



L1895710-1 BH 4 SS1CLIENT on 24-FEB-17Sampled By:SOILMatrix:

Physical Tests

Volatile Organic Compounds% Moisture

Acetone

Benzene


Bromoform

Bromomethane


Chlorobenzene


Chloroform

1,2-Dibromoethane

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


1,1-Dichloroethane

1,2-Dichloroethane




Methylene Chloride

1,2-Dichloropropane




Ethylbenzene

n-Hexane

Methyl Ethyl Ketone


MTBE

Styrene



Tetrachloroethylene

Toluene



Trichloroethylene


Vinyl chloride

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

15.6

<0.50

<0.0068

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.030

<0.030

<0.042

<0.018

<0.050

<0.50

<0.50

<0.050

<0.050

<0.050

<0.050

<0.050

<0.080

<0.050

<0.050

<0.010

<0.050

<0.020

0.10

0.50

0.0068

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.030

0.030

0.042

0.018

0.050

0.50

0.50

0.050

0.050

0.050

0.050

0.050

0.080

0.050

0.050

0.010

0.050

0.020

R3666488

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703


L1895710 CONTD....

3PAGE


of

TT163027

Qualifier* Batch



L1895710-1

L1895710-2

BH 4 SS1

BH 4 SS2

CLIENT on 24-FEB-17

CLIENT on 24-FEB-17

Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:


Hydrocarbons

Physical Tests

Cyanides


Metals

o-Xylene

m+p-Xylenes

Xylenes (Total)



F1 (C6-C10)

F1-BTEX

F2 (C10-C16)

F3 (C16-C34)

F4 (C34-C50)





Conductivity

% Moisture

pH


SAR

Calcium (Ca)

Magnesium (Mg)

Sodium (Na)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)


Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Mercury (Hg)

ug/g

ug/g

ug/g

%

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

mS/cm

%

pH units

ug/g

SAR

mg/L

mg/L

mg/L

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

07-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

07-MAR-17

02-MAR-17

05-MAR-17

03-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

07-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

<0.020

<0.030

<0.050

91.6

102.8

<5.0

<5.0

<10

<50

<50

<72

YES

88.6

88.8

0.140

32.9

7.55

<0.050

<0.10

28.4

<1.0

1.7

<1.0

1.7

37.1

<0.50

<5.0

0.18

<0.50

10.3

3.3

9.0

11.4

0.0278

0.020

0.030

0.050

50-140

50-140

5.0

5.0

10

50

50

72

60-140

60-140

0.0040

0.10

0.10

0.050

0.10

1.0

1.0

1.0

1.0

1.0

1.0

0.50

5.0

0.10

0.50

1.0

1.0

1.0

1.0

0.0050

SAR:M

R3666703

R3666703

R3666703

R3666703

R3666703

R3667308

R3667308

R3667308

R3667308

R3667308

R3666703

R3669057

R3666488

R3668064

R3668305

R3669663

R3669663

R3669663

R3669663

R3668768

R3668768

R3668768

R3668768

R3668768

R3669705

R3668768

R3668768

R3668768

R3668768

R3668768

R3668376


L1895710 CONTD....

4PAGE


of

TT163027

Qualifier* Batch



L1895710-2

L1895710-3

L1895710-4

BH 4 SS2

BH 4 SS3

BH 4 SS4

CLIENT on 24-FEB-17

CLIENT on 24-FEB-17

CLIENT on 24-FEB-17

Sampled By:

Sampled By:

Sampled By:

SOIL

SOIL

SOIL

Matrix:

Matrix:

Matrix:

Metals

Speciated Metals

Physical Tests


Physical Tests

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)


% Moisture

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene




Chrysene


Fluoranthene

Fluorene



1-Methylnaphthalene

2-Methylnaphthalene

Naphthalene

Phenanthrene

Pyrene



Conductivity

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

mS/cm

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

02-MAR-17

02-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

03-MAR-17

02-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

06-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

07-MAR-17

<1.0

6.9

<1.0

<0.20

<0.50

<1.0

18.6

26.4

0.33

13.4

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.042

<0.030

<0.030

<0.050

<0.050

<0.050

100.1

93.5

0.171

1.0

1.0

1.0

0.20

0.50

1.0

1.0

5.0

0.20

0.10

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.042

0.030

0.030

0.050

0.050

0.050

50-140

50-140

0.0040

R3668768

R3668768

R3668768

R3668768

R3668768

R3668768

R3668768

R3668768

R3668194

R3666488

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3669057


L1895710 CONTD....

5PAGE


of

TT163027

Qualifier* Batch



L1895710-4

L1895710-6

BH 4 SS4

BH 4 SS7

CLIENT on 24-FEB-17

CLIENT on 24-FEB-17

Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:

Physical Tests

Cyanides


Metals

Speciated Metals

Physical Tests

Cyanides


% Moisture

pH


SAR

Calcium (Ca)

Magnesium (Mg)

Sodium (Na)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)


Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Mercury (Hg)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)


Conductivity

% Moisture

pH


%

pH units

ug/g

SAR

mg/L

mg/L

mg/L

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

mS/cm

%

pH units

ug/g

02-MAR-17

02-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

07-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

05-MAR-17

03-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

07-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

03-MAR-17

07-MAR-17

02-MAR-17

05-MAR-17

03-MAR-17

14.0

7.41

<0.050

0.49

22.6

1.0

8.7

<1.0

1.8

45.2

<0.50

<5.0

<0.10

<0.50

4.9

1.6

3.3

2.1

<0.0050

<1.0

3.2

<1.0

<0.20

<0.50

<1.0

11.9

9.3

<0.20

0.305

7.23

7.72

<0.050

0.10

0.10

0.050

0.10

1.0

1.0

1.0

1.0

1.0

1.0

0.50

5.0

0.10

0.50

1.0

1.0

1.0

1.0

0.0050

1.0

1.0

1.0

0.20

0.50

1.0

1.0

5.0

0.20

0.0040

0.10

0.10

0.050

R3666488

R3668064

R3668305

R3669663

R3669663

R3669663

R3669663

R3668768

R3668768

R3668768

R3668768

R3668768

R3669705

R3668768

R3668768

R3668768

R3668768

R3668768

R3668376

R3668768

R3668768

R3668768

R3668768

R3668768

R3668768

R3668768

R3668768

R3668194

R3669057

R3666488

R3668064

R3668305


L1895710 CONTD....

6PAGE


of

TT163027

Qualifier* Batch



L1895710-6

L1895710-8

BH 4 SS7

BH 4 SS9

CLIENT on 24-FEB-17

CLIENT on 24-FEB-17

Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:


Metals

Speciated Metals

Sample Preparation

TCLP Extractables

SAR

Calcium (Ca)

Magnesium (Mg)

Sodium (Na)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)


Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Mercury (Hg)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)


Initial pH

Final pH

Acenaphthene

Acenaphthylene

Anthracene

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Benzo(a)anthracene

SAR

mg/L

mg/L

mg/L

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

pH units

pH units

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

07-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

02-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

06-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

07-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

03-MAR-17

02-MAR-17

02-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

0.87

30.8

2.1

18.5

<1.0

1.3

31.0

<0.50

<5.0

<0.10

<0.50

8.8

2.7

5.9

4.3

0.0084

<1.0

5.6

<1.0

<0.20

<0.50

<1.0

15.8

17.0

<0.20

9.32

5.83

<0.0050

<0.0050

<0.0050

<0.00020

<0.00020

<0.00020

<0.00020

<0.0050

0.10

1.0

1.0

1.0

1.0

1.0

1.0

0.50

5.0

0.10

0.50

1.0

1.0

1.0

1.0

0.0050

1.0

1.0

1.0

0.20

0.50

1.0

1.0

5.0

0.20

0.10

0.10

0.0050

0.0050

0.0050

0.00020

0.00020

0.00020

0.00020

0.0050

R3669663

R3669663

R3669663

R3669663

R3668768

R3668768

R3668768

R3668768

R3668768

R3669705

R3668768

R3668768

R3668768

R3668768

R3668768

R3668376

R3668768

R3668768

R3668768

R3668768

R3668768

R3668768

R3668768

R3668768

R3668194

R3667245

R3667245

R3668323

R3668323

R3668323

R3668436

R3668436

R3668436

R3668436

R3668323


L1895710 CONTD....

7PAGE


of

TT163027

Qualifier* Batch




TCLP Extractables

TCLP Metals

TCLP VOCs



Benzo(a)pyrene




Fluoride (F)

Nitrate and Nitrite as N

Nitrate-N

Nitrite-N

Total PCBs


Arsenic (As)

Barium (Ba)

Boron (B)

Cadmium (Cd)

Chromium (Cr)

Lead (Pb)

Mercury (Hg)

Selenium (Se)

Silver (Ag)

Uranium (U)


1,2-Dichlorobenzene

1,2-Dichloroethane

1,4-Dichlorobenzene

Benzene


Chlorobenzene

Chloroform

Dichloromethane

Methyl Ethyl Ketone

Tetrachloroethylene

Trichloroethylene

Vinyl chloride




Chrysene


mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

%

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

%

%

mg/L

mg/L

mg/L

06-MAR-17

06-MAR-17

06-MAR-17

07-MAR-17

07-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

07-MAR-17

07-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

<0.0010

<0.0050

<0.0050

<0.10

<10

<4.0

<2.0

<2.0

<0.00040

79.1

<0.050

<0.50

<2.5

<0.0050

<0.050

<0.050

<0.00010

<0.025

<0.0050

<0.25

<0.025

<0.025

<0.025

<0.025

<0.025

<0.025

<0.025

<0.10

<0.50

<1.0

<0.025

<0.025

<0.050

104.4

105.4

<0.0050

<0.0050

<0.0050

0.0010

0.0050

0.0050

0.10

10

4.0

2.0

2.0

0.00040

40-160

0.050

0.50

2.5

0.0050

0.050

0.050

0.00010

0.025

0.0050

0.25

0.025

0.025

0.025

0.025

0.025

0.025

0.025

0.10

0.50

1.0

0.025

0.025

0.050

70-130

70-130

0.0050

0.0050

0.0050

R3668323

R3668323

R3668323

R3667519

R3668460

R3668460

R3668460

R3668460

R3668436

R3668436

R3667746

R3667746

R3667746

R3667746

R3667746

R3667746

R3668383

R3667746

R3667746

R3667746

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668166

R3668323

R3668323

R3668323


L1895710 CONTD....

8PAGE


of

TT163027

Qualifier* Batch



L1895710-8

L1895710-9

L1895710-10

BH 4 SS9

BH 5 SS1

BH 5 SS2

CLIENT on 24-FEB-17

CLIENT on 24-FEB-17

CLIENT on 24-FEB-17

Sampled By:

Sampled By:

Sampled By:

SOIL

SOIL

SOIL

Matrix:

Matrix:

Matrix:


Physical Tests


Physical Tests

Cyanides


Metals

Fluoranthene

Fluorene


Naphthalene

Phenanthrene

Pyrene

Quinoline





% Moisture

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Total PCBs


Conductivity

% Moisture

pH


SAR

Calcium (Ca)

Magnesium (Mg)

Sodium (Na)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

%

%

%

%

%

ug/g

ug/g

ug/g

ug/g

ug/g

%

mS/cm

%

pH units

ug/g

SAR

mg/L

mg/L

mg/L

ug/g

ug/g

ug/g

ug/g

ug/g

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

02-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

02-MAR-17

02-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

02-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

07-MAR-17

02-MAR-17

05-MAR-17

03-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

93.8

96.6

81.5

94.1

10.7

<0.020

<0.020

<0.020

0.023

<0.040

91.4

0.115

8.53

7.57

<0.050

<0.10

18.2

<1.0

1.2

<1.0

1.4

21.6

<0.50

<5.0

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

0.0050

50-150

50-150

50-150

50-150

0.10

0.020

0.020

0.020

0.020

0.040

60-140

0.0040

0.10

0.10

0.050

0.10

1.0

1.0

1.0

1.0

1.0

1.0

0.50

5.0

DLM

DLM

DLM

DLM

DLM

SAR:M

R3668323

R3668323

R3668323

R3668323

R3668323

R3668323

R3668323

R3668323

R3668323

R3668323

R3668323

R3666488

R3668264

R3668264

R3668264

R3668264

R3668264

R3668264

R3669057

R3666488

R3668064

R3668305

R3669663

R3669663

R3669663

R3669663

R3668768

R3668768

R3668768

R3668768

R3668768


L1895710 CONTD....

9PAGE


of

TT163027

Qualifier* Batch




Metals

Speciated Metals



Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Mercury (Hg)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)


Acetone

Benzene


Bromoform

Bromomethane


Chlorobenzene


Chloroform

1,2-Dibromoethane

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene


1,1-Dichloroethane

1,2-Dichloroethane




Methylene Chloride

1,2-Dichloropropane



ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

07-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

07-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

0.23

<0.50

8.0

3.1

9.1

5.7

0.0133

<1.0

5.9

<1.0

<0.20

<0.50

<1.0

15.8

18.4

<0.20

<0.50

<0.0068

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.030

<0.030

0.10

0.50

1.0

1.0

1.0

1.0

0.0050

1.0

1.0

1.0

0.20

0.50

1.0

1.0

5.0

0.20

0.50

0.0068

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.050

0.030

0.030

R3669705

R3668768

R3668768

R3668768

R3668768

R3668768

R3668376

R3668768

R3668768

R3668768

R3668768

R3668768

R3668768

R3668768

R3668768

R3668194

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703


L1895710 CONTD....

10PAGE


of

TT163027

Qualifier* Batch





Hydrocarbons



Ethylbenzene

n-Hexane

Methyl Ethyl Ketone


MTBE

Styrene



Tetrachloroethylene

Toluene



Trichloroethylene


Vinyl chloride

o-Xylene

m+p-Xylenes

Xylenes (Total)



F1 (C6-C10)

F1-BTEX

F2 (C10-C16)

F2-Naphth

F3 (C16-C34)

F3-PAH

F4 (C34-C50)





Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene



ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

03-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

<0.042

<0.018

<0.050

<0.50

<0.50

<0.050

<0.050

<0.050

<0.050

<0.050

<0.080

<0.050

<0.050

<0.010

<0.050

<0.020

<0.020

<0.030

<0.050

85.7

96.0

<5.0

<5.0

<10

<10

<50

<50

<50

<72

YES

80.8

85.1

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

0.042

0.018

0.050

0.50

0.50

0.050

0.050

0.050

0.050

0.050

0.080

0.050

0.050

0.010

0.050

0.020

0.020

0.030

0.050

50-140

50-140

5.0

5.0

10

10

50

50

50

72

60-140

60-140

0.050

0.050

0.050

0.050

0.050

0.050

0.050

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3666703

R3667308

R3667308

R3667308

R3667308

R3667308

R3666703

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293


L1895710 CONTD....

11PAGE


of

TT163027

Qualifier* Batch



L1895710-10

L1895710-11

BH 5 SS2

BH 5 SS3

CLIENT on 24-FEB-17

CLIENT on 24-FEB-17

Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:


Physical Tests

Cyanides


Metals


Chrysene


Fluoranthene

Fluorene



1-Methylnaphthalene

2-Methylnaphthalene

Naphthalene

Phenanthrene

Pyrene



Conductivity

% Moisture

pH


SAR

Calcium (Ca)

Magnesium (Mg)

Sodium (Na)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)


Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Mercury (Hg)

Molybdenum (Mo)

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

mS/cm

%

pH units

ug/g

SAR

mg/L

mg/L

mg/L

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

01-MAR-17

02-MAR-17

02-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

07-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

07-MAR-17

02-MAR-17

05-MAR-17

03-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

07-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.042

<0.030

<0.030

<0.050

<0.050

<0.050

93.2

87.3

0.112

8.06

7.64

<0.050

0.36

15.1

1.2

5.4

<1.0

1.2

18.5

<0.50

<5.0

0.22

<0.50

7.5

2.9

5.9

5.8

0.0090

<1.0

0.050

0.050

0.050

0.050

0.050

0.050

0.042

0.030

0.030

0.050

0.050

0.050

50-140

50-140

0.0040

0.10

0.10

0.050

0.10

1.0

1.0

1.0

1.0

1.0

1.0

0.50

5.0

0.10

0.50

1.0

1.0

1.0

1.0

0.0050

1.0

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3668293

R3669057

R3666488

R3668064

R3668305

R3669663

R3669663

R3669663

R3669663

R3668768

R3668768

R3668768

R3668768

R3668768

R3669705

R3668768

R3668768

R3668768

R3668768

R3668768

R3668376

R3668768


L1895710 CONTD....

12PAGE


of

TT163027

Qualifier* Batch



L1895710-11

L1895710-12

BH 5 SS3

BH 5 SS4

CLIENT on 24-FEB-17

CLIENT on 24-FEB-17

Sampled By:

Sampled By:

SOIL

SOIL

Matrix:

Matrix:

Metals

Speciated Metals

Physical Tests

Cyanides


Metals

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)


Conductivity

% Moisture

pH


SAR

Calcium (Ca)

Magnesium (Mg)

Sodium (Na)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)


Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Mercury (Hg)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

mS/cm

%

pH units

ug/g

SAR

mg/L

mg/L

mg/L

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

07-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

05-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

03-MAR-17

07-MAR-17

02-MAR-17

05-MAR-17

03-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

07-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

5.5

<1.0

<0.20

<0.50

<1.0

14.9

19.4

<0.20

0.117

9.62

7.92

<0.050

0.81

13.8

1.1

11.6

<1.0

1.1

14.0

<0.50

<5.0

0.13

<0.50

5.7

2.5

3.7

1.9

<0.0050

<1.0

4.5

<1.0

<0.20

<0.50

<1.0

1.0

1.0

0.20

0.50

1.0

1.0

5.0

0.20

0.0040

0.10

0.10

0.050

0.10

1.0

1.0

1.0

1.0

1.0

1.0

0.50

5.0

0.10

0.50

1.0

1.0

1.0

1.0

0.0050

1.0

1.0

1.0

0.20

0.50

1.0

R3668768

R3668768

R3668768

R3668768

R3668768

R3668768

R3668768

R3668194

R3669057

R3666488

R3668064

R3668305

R3669663

R3669663

R3669663

R3669663

R3668768

R3668768

R3668768

R3668768

R3668768

R3669705

R3668768

R3668768

R3668768

R3668768

R3668768

R3668376

R3668768

R3668768

R3668768

R3668768

R3668768

R3668768


L1895710 CONTD....

13PAGE


of

TT163027

Qualifier* Batch




Metals

Speciated Metals

Vanadium (V)

Zinc (Zn)


ug/g

ug/g

ug/g

05-MAR-17

05-MAR-17

02-MAR-17

06-MAR-17

06-MAR-17

03-MAR-17

11.0

9.7

<0.20

1.0

5.0

0.20

R3668768

R3668768

R3668194

B-HWS-R511-WT

CN-TCLP-WT

CN-WAD-R511-WT

CR-CR6-IC-WT

EC-WT

F-TCLP-WT

F1-F4-511-CALC-WT


Boron-HWE-O.Reg 153/04 (July 2011)

Cyanide for O. Reg 347

Cyanide (WAD)-O.Reg 153/04 (July 2011)

Hexavalent Chromium in Soil

Conductivity (EC)

Fluoride (F) for O. Reg 347

F1-F4 Hydrocarbon Calculated Parameters

L1895710 CONTD....

14PAGE of

TT163027

A dried solid sample is extracted with calcium chloride, the sample undergoes a heating process. After cooling the sample is filtered and analyzed by ICP/OES.


The sample is extracted with a strong base for 16 hours, and then filtered. The filtrate is then distilled where the cyanide is converted to cyanogen chloride by reacting with chloramine-T, the cyanogen chloride then reacts with a combination of barbituric acid and isonicotinic acid to form a highly colored complex.


This analysis is carried out using procedures adapted from "Test Methods for Evaluating Solid Waste" SW-846, Method 7199, published by the United States Environmental Protection Agency (EPA). The procedure involves analysis for chromium (VI) by ion chromatography using diphenylcarbazide in asulphuric acid solution.


A representative subsample is tumbled with de-ionized (DI) water. The ratio of water to soil is 2:1 v/w. After tumbling the sample is then analyzed by a conductivity meter.


Analytical methods used for analysis of CCME Petroleum Hydrocarbons have been validated and comply with the Reference Method for the CWS PHC.

Hydrocarbon results are expressed on a dry weight basis.

In cases where results for both F4 and F4G are reported, the greater of the two results must be used in any application of the CWS PHC guidelines andthe gravimetric heavy hydrocarbons cannot be added to the C6 to C50 hydrocarbons. In samples where BTEX and F1 were analyzed , F1-BTEX represents a value where the sum of Benzene, Toluene, Ethylbenzene and total Xylenes hasbeen subtracted from F1.

In samples where PAHs, F2 and F3 were analyzed, F2-Naphth represents the result where Naphthalene has been subtracted from F2. F3-PAH represents a result where the sum of Benzo(a)anthracene, Benzo(a)pyrene, Benzo(b)fluoranthene, Benzo(k)fluoranthene, Dibenzo(a,h)anthracene, Fluoranthene, Indeno(1,2,3-cd)pyrene, Phenanthrene, and Pyrene has been subtracted from F3.

Unless otherwise qualified, the following quality control criteria have been met for the F1 hydrocarbon range:1. All extraction and analysis holding times were met.2. Instrument performance showing response factors for C6 and C10 within 30% of the response factor for toluene.

ALS Test Code Test Description

Soil

Waste

Soil

Soil

Soil

Waste

Soil

DLM

MES

SAR:M


Data Quality Objective was marginally exceeded (by < 10% absolute) for < 10% of analytes in a Multi-Element Scan / Multi-Parameter Scan (considered acceptable as per OMOE & CCME).Reported SAR represents a maximum value. Actual SAR may be lower if both Ca and Mg were detectable.

Sample Parameter Qualifier key listed:

HW EXTR, EPA 6010B

APHA 4500CN C E

MOE 3015/APHA 4500CN I-WAD

SW846 3060A/7199

MOEE E3138


CCME CWS-PHC, Pub #1310, Dec 2001-S

Method Reference**


Matrix

Applies to Sample Number(s)Parameter Qualifier

L1895710-1, -10L1895710-1, -10

AcetoneMethyl Ethyl Ketone

MESMES

QC Samples with Qualifiers & Comments:

Matrix SpikeMatrix Spike

QC Type Description

Test Method References:


F1-HS-511-WT

F2-F4-511-WT

HG-200.2-CVAA-WT

HG-TCLP-WT

LEACH-TCLP-WT

MET-200.2-CCMS-WT

MET-TCLP-WT

METHYLNAPS-CALC-WT

MOISTURE-WT

N2N3-TCLP-WT

PAH-511-WT


F1-O.Reg 153/04 (July 2011)

F2-F4-O.Reg 153/04 (July 2011)

Mercury in Soil by CVAAS

Mercury (CVAA) for O.Reg 347

Leachate Procedure for Reg 347

Metals in Soil by CRC ICPMS

O.Reg 347 TCLP Leachable Metals

ABN-Calculated Parameters

% Moisture

Nitrate/Nitrite-N for O. Reg 347

PAH-O.Reg 153/04 (July 2011)

L1895710 CONTD....

15PAGE of

TT163027

3. Linearity of gasoline response within 15% throughout the calibration range.

Unless otherwise qualified, the following quality control criteria have been met for the F2-F4 hydrocarbon ranges:1. All extraction and analysis holding times were met.2. Instrument performance showing C10, C16 and C34 response factors within 10% of their average.3. Instrument performance showing the C50 response factor within 30% of the average of the C10, C16 and C34 response factors.4. Linearity of diesel or motor oil response within 15% throughout the calibration range.

Fraction F1 is determined by extracting a soil or sediment sample as received with methanol, then analyzing by headspace-GC/FID.


Petroleum Hydrocarbons (F2-F4 fractions) are extracted from soil with 1:1 hexane:acetone using a rotary extractor. Extracts are treated with silica gel to remove polar organic interferences. F2, F3, & F4 are analyzed by GC-FID. F4G-sg is analyzed gravimetrically.

Notes: 1. F2 (C10-C16): Sum of all hydrocarbons that elute between nC10 and nC16.2. F3 (C16-C34): Sum of all hydrocarbons that elute between nC16 and nC34.3. F4 (C34-C50): Sum of all hydrocarbons that elute between nC34 and nC50.4. F4G: Gravimetric Heavy Hydrocarbons5. F4G-sg: Gravimetric Heavy Hydrocarbons (F4G) after silica gel treatment.6. Where both F4 (C34-C50) and F4G-sg are reported for a sample, the larger of the two values is used for comparison against the relevant CCME guideline for F4. 7. F4G-sg cannot be added to the C6 to C50 hydrocarbon results to obtain an estimate of total extractable hydrocarbons. 8. This method is validated for use. 9. Data from analysis of validation and quality control samples is available upon request.10. Reported results are expressed as milligrams per dry kilogram, unless otherwise indicated.


Soil samples are digested with nitric and hydrochloric acids, followed by analysis by CVAAS.


Inorganic and Semi-Volatile Organic contaminants are leached from waste samples in strict accordance with US EPA Method 1311, "Toxicity Characteristic Leaching Procedure" (TCLP). Test results are reported in leachate concentration units (normally mg/L).

This method uses a heated strong acid digestion with HNO3 and HCl and is intended to liberate metals that may be environmentally available. Silicate minerals are not solubilized. Dependent on sample matrix, some metals may be only partially recovered, including Al, Ba, Be, Cr, Sr, Ti, Tl, V, W, and Zr. Volatile forms of sulfur (including sulfide) may not be captured, as they may be lost during sampling, storage, or digestion. Analysis is by Collision/Reaction Cell ICPMS.


A representative sub-sample of soil is fortified with deuterium-labelled surrogates and a mechanical shaking techniqueis used to extract the sample with a mixture of methanol and toluene. The extracts are concentrated and analyzed by GC/MS. Depending on the analytical GC/MS column used

Soil

Soil

Soil

Waste

Waste

Soil

Waste

Soil

Soil

Waste

Soil

E3398/CCME TIER 1-HS

MOE DECPH-E3398/CCME TIER 1

EPA 200.2/1631E (mod)

SW846 7470A

EPA 1311

EPA 200.2/6020A (mod)

EPA 200.8

SW846 8270

Gravimetric: Oven Dried


SW846 3510/8270


PAH-TCLP-WT

PCB-511-WT

PCB-TCLP-WT

PH-WT

SAR-R511-WT

VOC-1,3-DCP-CALC-WT

VOC-511-HS-WT

VOC-TCLP-WT

XYLENES-SUM-CALC-WT


PAH for O. Reg 347

PCB-O.Reg 153/04 (July 2011)

PCBs for O. Reg 347

pH

SAR-O.Reg 153/04 (July 2011)

Regulation 153 VOCs

VOC-O.Reg 153/04 (July 2011)

VOC for O. Reg 347


L1895710 CONTD....

16PAGE of

TT163027

benzo(j)fluoranthene may chromatographically co-elute with benzo(b)fluoranthene or benzo(k)fluoranthene.


Samples are leached according to TCLP protocol and then the aqueous leachate is extracted and the resulting extracts are analyzed on GC/MSD. Depending on the analytical GC/MS column used benzo(j)fluoranthene may chromatographically co-elute with benzo(b)fluoranthene or benzo(k)fluoranthene.

An aliquot of a solid sample is extracted with a solvent, extract is cleaned up and analyzed on the GC/MS.


A minimum 10g portion of the sample is extracted with 20mL of 0.01M calcium chloride solution by shaking for at least 30 minutes. The aqueous layer isseparated from the soil and then analyzed using a pH meter and electrode.


A dried, disaggregated solid sample is extracted with deionized water, the aqueous extract is separated from the solid, acidified and then analyzed usinga ICP/OES. The concentrations of Na, Ca and Mg are reported as per CALA requirements for calculated parameters. These individual parameters are not for comparison to any guideline.


Soil and sediment samples are extracted in methanol and analyzed by headspace-GC/MS.


A sample of waste is leached in a zero headspace extractor at 30–2 rpm for 18–2.0 hours with the appropriate leaching solution. After tumbling the leachate is analyzed directly by headspace technology, followed by GC/MS using internal standard quantitation.


Waste

Soil

Waste

Soil

Soil

Soil

Soil

Waste

Soil

SW846 8270 (PAH)

SW846 3510/8082

SW846 8270

MOEE E3137A

SW846 6010C

SW8260B/SW8270C

SW846 8260 (511)

SW846 8260

CALCULATION

** ALS test methods may incorporate modifications from specified reference methods to improve performance.







L1895710 CONTD....

17PAGE of

TT163027

GLOSSARY OF REPORT TERMSSurrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there.mg/kg - milligrams per kilogram based on dry weight of samplemg/kg wwt - milligrams per kilogram based on wet weight of samplemg/kg lwt - milligrams per kilogram based on lipid weight of samplemg/L - unit of concentration based on volume, parts per million.< - Less than.D.L. - The reporting limit.N/A - Result not available. Refer to qualifier code and definition for explanation.




Client:

Contact:




B-HWS-R511-WT

CN-WAD-R511-WT

CR-CR6-IC-WT

EC-WT

F1-HS-511-WT

Soil

Soil

Soil

Soil

Soil

R3669705

R3668305

R3668194

R3669057

Batch

Batch

Batch

Batch

DUP

IRM

LCS

MB

DUP

LCS

MB

MS

CRM

DUP

LCS

MB

DUP

LCS

MB

WG2489875-4

WG2489875-2

WG2489875-3

WG2489875-1

WG2487563-3

WG2487563-2

WG2487563-1

WG2487563-4

WG2487564-3

WG2487564-4

WG2487564-2

WG2487564-1

WG2489876-4

WG2490110-1

WG2489876-1

L1895710-2

HOTB-SAL_SOIL5

L1894670-1

L1894670-1

WT-SQC012

L1893469-1

WG2489876-3













Conductivity

Conductivity

Conductivity

0.18

77.3

116.1

<0.10

<0.050

92.1

<0.050

95.8

108.6

<0.20

96.8

<0.20

0.385

99.6

<0.0040

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

3.9

N/A

N/A

0.0

30

35

35

20

70-130

70-130

80-120

70-130

70-130

80-120

90-110

ug/g

%

%

ug/g

ug/g

%

ug/g

%

%

ug/g

%

ug/g

mS/cm

%

mS/cm

0.18

<0.050

<0.20

0.385

0.1

0.05

0.2

0.004

RPD-NA

RPD-NA

22


Client:

Contact:




F1-HS-511-WT

F2-F4-511-WT

HG-200.2-CVAA-WT

Soil

Soil

Soil

R3666703

R3667308

R3668376

Batch

Batch

Batch

DUP

LCS

MB

MS

CRM

DUP

LCS

MB

CRM

DUP

LCS

MB

WG2487973-4

WG2487973-2

WG2487973-1

WG2487973-7

WG2487547-3

WG2487547-5

WG2487547-2

WG2487547-1

WG2489266-2

WG2489266-6

WG2489266-3

WG2489266-1

WG2487973-3

WG2487973-6

ALS PHC2 IRM

WG2487547-4

WT-CANMET-TILL1

WG2489266-5

F1 (C6-C10)

F1 (C6-C10)

F1 (C6-C10)


F1 (C6-C10)

F2 (C10-C16)

F3 (C16-C34)

F4 (C34-C50)

F2 (C10-C16)

F3 (C16-C34)

F4 (C34-C50)

F2 (C10-C16)

F3 (C16-C34)

F4 (C34-C50)

F2 (C10-C16)

F3 (C16-C34)

F4 (C34-C50)


Mercury (Hg)

Mercury (Hg)

Mercury (Hg)

<5.0

105.8

<5.0

97.1

99.4

90.2

89.2

89.2

<10

<50

<50

105.5

105.5

91.1

<10

<50

<50

87.0

98.5

0.218

103.0

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

N/A

N/A

N/A

N/A

5.0

30

30

30

30

40

80-120

60-140

70-130

70-130

70-130

80-120

80-120

80-120

70-130

80-120

ug/g

%

ug/g

%

%

%

%

%

ug/g

ug/g

ug/g

%

%

%

ug/g

ug/g

ug/g

%

%

ug/g

%

<5.0

<10

<50

<50

0.208

5

60-140

10

50

50

60-140

RPD-NA

RPD-NA

RPD-NA

RPD-NA

22


Client:

Contact:




HG-200.2-CVAA-WT

MET-200.2-CCMS-WT

Soil

Soil

R3668376

R3668768

Batch

Batch

MB

CRM

DUP

WG2489266-1

WG2489266-2

WG2489266-6

WT-CANMET-TILL1

WG2489266-5

Mercury (Hg)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)

Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Molybdenum (Mo)

<0.0050

97.8

108.8

110.1

93.7

97.4

104.0

100.4

97.4

86.6

93.9

101.5

84.3

101.2

93.8

98.6

106.2

97.2

0.28

3.17

73.4

0.56

6.4

0.152

19.9

7.46

15.5

32.5

0.47

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

1.9

3.1

0.9

1.1

0.0

3.3

0.9

0.8

4.3

4.5

1.2

30

30

40

30

30

30

30

30

30

40

40

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

mg/kg

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

0.27

3.08

72.8

0.56

6.4

0.147

19.7

7.40

14.9

31.1

0.48

0.005

22


Client:

Contact:




MET-200.2-CCMS-WT Soil

R3668768BatchDUP

LCS

MB

WG2489266-6

WG2489266-4

WG2489266-1

WG2489266-5Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)

Cadmium (Cd)

Chromium (Cr)

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)

Antimony (Sb)

Arsenic (As)

Barium (Ba)

Beryllium (Be)

Boron (B)

Cadmium (Cd)

Chromium (Cr)

14.2

0.32

0.67

0.119

0.423

29.5

54.2

103.7

101.5

99.5

94.1

93.3

95.8

97.3

96.8

94.7

93.6

98.6

96.0

96.7

101.3

93.9

95.7

99.4

91.4

<0.10

<0.10

<0.50

<0.10

<5.0

<0.020

<0.50

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

0.8

13

2.9

3.8

6.2

0.2

0.5

30

30

40

30

30

30

30

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

14.3

0.28

0.65

0.115

0.398

29.5

54.4

0.1

0.1

0.5

0.1

5

0.02

0.5

22


Client:

Contact:




MET-200.2-CCMS-WT

MOISTURE-WT

PAH-511-WT

Soil

Soil

Soil

R3668768

R3666488

R3668293

Batch

Batch

Batch

MB

DUP

LCS

MB

DUP

WG2489266-1

WG2487550-3

WG2487550-2

WG2487550-1

WG2487269-4

L1895710-11

WG2487269-3

Cobalt (Co)

Copper (Cu)

Lead (Pb)

Molybdenum (Mo)

Nickel (Ni)

Selenium (Se)

Silver (Ag)

Thallium (Tl)

Uranium (U)

Vanadium (V)

Zinc (Zn)

% Moisture

% Moisture

% Moisture

1-Methylnaphthalene

2-Methylnaphthalene

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene




Chrysene


<0.10

<0.50

<0.50

<0.10

<0.50

<0.20

<0.10

<0.050

<0.050

<0.20

<2.0

8.25

100.1

<0.10

<0.030

<0.030

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

02-MAR-17

02-MAR-17

02-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

2.4

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

20

40

40

40

40

40

40

40

40

40

40

40

40

90-110

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

%

%

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

8.06

<0.030

<0.030

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

0.1

0.5

0.5

0.1

0.5

0.2

0.1

0.05

0.05

0.2

2

0.1

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

22


Client:

Contact:




PAH-511-WT Soil

R3668293BatchDUP

LCS

MB

WG2487269-4

WG2487269-2

WG2487269-1

WG2487269-3Fluoranthene

Fluorene


Naphthalene

Phenanthrene

Pyrene

1-Methylnaphthalene

2-Methylnaphthalene

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene




Chrysene


Fluoranthene

Fluorene


Naphthalene

Phenanthrene

Pyrene

1-Methylnaphthalene

2-Methylnaphthalene

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene


<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

108.7

107.9

109.0

105.5

115.5

110.1

103.4

112.0

95.4

111.0

113.5

97.5

96.7

108.3

98.8

112.0

108.4

98.1

<0.030

<0.030

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

N/A

N/A

N/A

N/A

N/A

N/A

40

40

40

40

40

40

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

0.03

0.03

0.05

0.05

0.05

0.05

0.05

0.05

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

22


Client:

Contact:




PAH-511-WT

PCB-511-WT

Soil

Soil

R3668293BatchMB

MS

WG2487269-1

WG2487269-5 WG2487269-3



Chrysene


Fluoranthene

Fluorene


Naphthalene

Phenanthrene

Pyrene



1-Methylnaphthalene

2-Methylnaphthalene

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene




Chrysene


Fluoranthene

Fluorene


Naphthalene

Phenanthrene

Pyrene

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

90.4

83.9

108.3

106.9

108.0

101.8

114.1

106.3

101.5

112.2

86.2

113.3

114.7

89.4

98.6

104.9

87.5

111.3

109.4

100.3

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

04-MAR-17

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

50-140

50-140

22


Client:

Contact:




PCB-511-WT

PH-WT

SAR-R511-WT

Soil

Soil

Soil

R3668264

R3668064

R3669663

Batch

Batch

Batch

DUP

LCS

MB

MS

DUP

LCS

DUP

IRM

WG2487269-4

WG2487269-2

WG2487269-1

WG2487269-5

WG2487635-1

WG2489142-1

WG2489876-4

WG2489876-2

WG2487269-3

WG2487269-3

L1895710-2

WG2489876-3

WT SAR1

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260


Aroclor 1242

Aroclor 1254

Aroclor 1260

pH

pH

Calcium (Ca)

Sodium (Na)

Magnesium (Mg)

Calcium (Ca)

Sodium (Na)

Magnesium (Mg)

<0.010

<0.010

<0.010

<0.010

99.3

83.2

105.8

101.7

<0.010

<0.010

<0.010

<0.010

93.8

100.1

105.0

102.5

7.49

7.01

3.3

75.1

1.7

97.2

78.9

88.9

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

05-MAR-17

05-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

07-MAR-17

N/A

N/A

N/A

N/A

0.06

2.2

12

0.7

40

40

40

40

0.3

30

30

2

60-140

60-140

60-140

60-140

60-140

60-140

60-140

6.7-7.3

70-130

70-130

70-130

ug/g

ug/g

ug/g

ug/g

%

%

%

%

ug/g

ug/g

ug/g

ug/g

%

%

%

%

pH units

pH units

mg/L

mg/L

mg/L

%

%

%

<0.010

<0.010

<0.010

<0.010

7.55

3.3

66.7

2.4

0.01

0.01

0.01

0.01

60-140

RPD-NA

RPD-NA

RPD-NA

RPD-NA

J

J

22


Client:

Contact:




SAR-R511-WT

VOC-511-HS-WT

Soil

Soil

R3669663

R3666703

Batch

Batch

MB

DUP

WG2489876-1

WG2487973-4 WG2487973-3

Calcium (Ca)

Sodium (Na)

Magnesium (Mg)





1,1-Dichloroethane


1,2-Dibromoethane

1,2-Dichlorobenzene

1,2-Dichloroethane

1,2-Dichloropropane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

Acetone

Benzene


Bromoform

Bromomethane


Chlorobenzene

Chloroform





Ethylbenzene

n-Hexane

Methylene Chloride

<1.0

<1.0

<1.0

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.50

<0.0068

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.030

<0.050

<0.050

<0.018

<0.050

<0.050

07-MAR-17

07-MAR-17

07-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

40

mg/L

mg/L

mg/L

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.50

<0.0068

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.030

<0.050

<0.050

<0.018

<0.050

<0.050

1

1

1

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

22


Client:

Contact:




VOC-511-HS-WT Soil

R3666703BatchDUP

LCS

WG2487973-4

WG2487973-2

WG2487973-3MTBE

m+p-Xylenes

Methyl Ethyl Ketone


o-Xylene

Styrene

Tetrachloroethylene

Toluene



Trichloroethylene


Vinyl chloride





1,1-Dichloroethane


1,2-Dibromoethane

1,2-Dichlorobenzene

1,2-Dichloroethane

1,2-Dichloropropane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

Acetone

Benzene


Bromoform

Bromomethane


Chlorobenzene

<0.050

<0.030

<0.50

<0.50

<0.020

<0.050

<0.050

<0.080

<0.050

<0.030

<0.010

<0.050

<0.020

98.5

113.4

99.6

107.6

103.2

92.8

107.8

102.4

114.0

107.0

97.9

101.5

131.0

106.9

105.7

107.9

102.0

97.1

103.3

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

40

40

40

40

40

40

40

40

40

40

40

40

40

60-130

60-130

60-130

60-130

60-130

60-130

70-130

70-130

60-130

70-130

70-130

70-130

60-140

70-130

50-140

70-130

50-140

70-130

70-130

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

<0.050

<0.030

<0.50

<0.50

<0.020

<0.050

<0.050

<0.080

<0.050

<0.030

<0.050

<0.050

<0.020

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

22


Client:

Contact:




VOC-511-HS-WT Soil

R3666703BatchLCS

MB

WG2487973-2

WG2487973-1

Chloroform





Ethylbenzene

n-Hexane

Methylene Chloride

MTBE

m+p-Xylenes

Methyl Ethyl Ketone


o-Xylene

Styrene

Tetrachloroethylene

Toluene



Trichloroethylene


Vinyl chloride





1,1-Dichloroethane


1,2-Dibromoethane

1,2-Dichlorobenzene

1,2-Dichloroethane

1,2-Dichloropropane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

106.5

106.3

107.8

110.7

57.3

90.2

100.3

110.3

102.1

95.0

129.9

112.0

93.7

96.3

91.2

94.8

100.4

102.8

99.5

98.7

86.2

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

70-130

70-130

70-130

60-130

50-140

70-130

70-130

70-130

70-130

70-130

60-140

60-140

70-130

70-130

60-130

70-130

60-130

70-130

60-130

50-140

60-140

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.05

22


Client:

Contact:




VOC-511-HS-WT Soil

R3666703BatchMB

MS

WG2487973-1

WG2487973-5 WG2487973-3

Acetone

Benzene


Bromoform

Bromomethane


Chlorobenzene

Chloroform





Ethylbenzene

n-Hexane

Methylene Chloride

MTBE

m+p-Xylenes

Methyl Ethyl Ketone


o-Xylene

Styrene

Tetrachloroethylene

Toluene



Trichloroethylene


Vinyl chloride






<0.50

<0.0068

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.030

<0.050

<0.050

<0.018

<0.050

<0.050

<0.050

<0.030

<0.50

<0.50

<0.020

<0.050

<0.050

<0.080

<0.050

<0.030

<0.010

<0.050

<0.020

103.9

95.7

112.3

127.1

114.3

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

50-140

50-140

50-140

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

ug/g

%

%

%

%

%

0.5

0.0068

0.05

0.05

0.05

0.05

0.05

0.05

0.05

0.03

0.05

0.05

0.018

0.05

0.05

0.05

0.03

0.5

0.5

0.02

0.05

0.05

0.08

0.05

0.03

0.01

0.05

0.02

50-140

50-140

22


Client:

Contact:




VOC-511-HS-WT Soil

R3666703BatchMSWG2487973-5 WG2487973-3


1,1-Dichloroethane


1,2-Dibromoethane

1,2-Dichlorobenzene

1,2-Dichloroethane

1,2-Dichloropropane

1,3-Dichlorobenzene

1,4-Dichlorobenzene

Acetone

Benzene


Bromoform

Bromomethane


Chlorobenzene

Chloroform





Ethylbenzene

n-Hexane

Methylene Chloride

MTBE

m+p-Xylenes

Methyl Ethyl Ketone


o-Xylene

Styrene

Tetrachloroethylene

Toluene


121.5

117.9

105.5

122.3

115.5

129.2

122.6

110.2

114.0

149.3

121.9

120.7

121.7

113.8

111.2

116.8

121.6

120.8

121.0

125.5

65.4

102.9

115.3

124.8

115.3

107.7

145.3

125.9

106.5

109.0

103.8

107.6

113.9

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

MES

MES

22


Client:

Contact:




VOC-511-HS-WT

CN-TCLP-WT

F-TCLP-WT

HG-TCLP-WT

MET-TCLP-WT

Soil

Waste

Waste

Waste

Waste

R3666703

R3667519

R3668460

R3668383

Batch

Batch

Batch

Batch

MS

DUP

LCS

MB

MS

DUP

LCS

MB

MS

DUP

LCS

MB

MS

WG2487973-5

WG2488553-3

WG2488553-2

WG2488553-1

WG2488553-4

WG2488480-3

WG2488480-2

WG2488480-1

WG2488480-4

WG2489377-3

WG2489377-2

WG2489377-1

WG2489377-4

WG2487973-3

L1896258-1

L1896258-1

L1896258-1

L1896258-1

L1895710-8

L1895710-8


Trichloroethylene


Vinyl chloride





Fluoride (F)

Fluoride (F)

Fluoride (F)

Fluoride (F)

Mercury (Hg)

Mercury (Hg)

Mercury (Hg)

Mercury (Hg)

114.8

113.5

112.2

97.0

<0.10

95.0

<0.10

89.5

<10

90.4

<10

88.5

<0.00010

103.0

<0.00010

92.3

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

N/A

N/A

N/A

20

30

50

50-140

50-140

50-140

50-140

70-130

50-150

70-130

50-150

70-130

50-140

%

%

%

%

mg/L

%

mg/L

%

mg/L

%

mg/L

%

mg/L

%

mg/L

%

<0.10

<10

<0.00010

0.1

10

0.0001

RPD-NA

RPD-NA

RPD-NA

22


Client:

Contact:




MET-TCLP-WT Waste

R3667746BatchDUP

LCS

MB

MS

WG2488668-4

WG2488668-2

WG2488668-1

WG2488668-5

WG2488668-3

WG2488668-3

Silver (Ag)

Arsenic (As)

Boron (B)

Barium (Ba)

Cadmium (Cd)

Chromium (Cr)

Lead (Pb)

Selenium (Se)

Uranium (U)

Silver (Ag)

Arsenic (As)

Boron (B)

Barium (Ba)

Cadmium (Cd)

Chromium (Cr)

Lead (Pb)

Selenium (Se)

Uranium (U)

Silver (Ag)

Arsenic (As)

Boron (B)

Barium (Ba)

Cadmium (Cd)

Chromium (Cr)

Lead (Pb)

Selenium (Se)

Uranium (U)

Silver (Ag)

Arsenic (As)

Boron (B)

Barium (Ba)

<0.0050

<0.050

<2.5

<0.50

<0.0050

<0.050

<0.050

<0.025

<0.25

100.5

98.0

89.8

101.1

97.4

94.9

101.1

97.2

105.6

<0.0050

<0.050

<2.5

<0.50

<0.0050

<0.050

<0.050

<0.025

<0.25

112.1

95.2

84.0

100.3

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

40

40

40

40

40

40

40

40

40

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

50-150

50-150

50-150

50-150

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

%

%

%

%

%

%

%

%

%

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

%

%

%

%

<0.0050

<0.050

<2.5

<0.50

<0.0050

<0.050

<0.050

<0.025

<0.25

0.005

0.05

2.5

0.5

0.005

0.05

0.05

0.025

0.25

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

22


Client:

Contact:




MET-TCLP-WT

N2N3-TCLP-WT

PAH-TCLP-WT

Waste

Waste

Waste

R3667746

R3668460

R3668323

Batch

Batch

Batch

MS

DUP

LCS

MB

MS

DUP

WG2488668-5

WG2488480-3

WG2488480-2

WG2488480-1

WG2488480-4

WG2489276-5

WG2488668-3

L1896258-1

L1896258-1

WG2489276-3

Cadmium (Cd)

Chromium (Cr)

Lead (Pb)

Selenium (Se)

Uranium (U)

Nitrate-N

Nitrite-N

Nitrate-N

Nitrite-N

Nitrate-N

Nitrite-N

Nitrate-N

Nitrite-N

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene




Chrysene


Fluoranthene

Fluorene

92.9

89.4

89.9

92.3

94.8

<2.0

<2.0

98.4

96.2

<2.0

<2.0

98.5

97.4

<0.0050

<0.0050

<0.0050

<0.0050

<0.0010

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

03-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

30

30

50

50

50

50

50

50

50

50

50

50

50

50

50-150

50-150

50-150

50-150

50-150

70-130

70-130

50-150

50-150

%

%

%

%

%

mg/L

mg/L

%

%

mg/L

mg/L

%

%

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

<2.0

<2.0

<0.0050

<0.0050

<0.0050

<0.0050

<0.0010

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

2

2

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

22


Client:

Contact:




PAH-TCLP-WT Waste

R3668323BatchDUP

LCS

MB

WG2489276-5

WG2489276-2

WG2489276-1

WG2489276-3Indeno(1,2,3-cd)pyrene

Naphthalene

Phenanthrene

Pyrene

Quinoline

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene




Chrysene


Fluoranthene

Fluorene


Naphthalene

Phenanthrene

Pyrene

Quinoline

Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene




Chrysene


<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

84.2

85.9

86.4

85.1

87.1

81.0

86.3

85.0

86.3

88.7

87.7

85.1

81.8

79.9

85.4

90.8

120.8

<0.0050

<0.0050

<0.0050

<0.0050

<0.0010

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

N/A

N/A

N/A

N/A

N/A

50

50

50

50

50

50-130

50-130

50-130

50-140

60-140

50-140

50-140

50-150

50-140

50-140

50-150

50-150

50-140

50-130

50-130

50-140

50-150

mg/L

mg/L

mg/L

mg/L

mg/L

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

0.005

0.005

0.005

0.005

0.001

0.005

0.005

0.005

0.005

0.005

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

22


Client:

Contact:




PAH-TCLP-WT

PCB-TCLP-WT

Waste

Waste

R3668323

R3668436

Batch

Batch

MB

MS

DUP

WG2489276-1

WG2489276-4

WG2489277-5

WG2489276-3

WG2489277-3

Fluoranthene

Fluorene


Naphthalene

Phenanthrene

Pyrene

Quinoline





Acenaphthene

Acenaphthylene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene




Chrysene


Fluoranthene

Fluorene


Naphthalene

Phenanthrene

Pyrene

Quinoline

Aroclor 1242

Aroclor 1248

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

<0.0050

90.3

101.0

103.7

100.0

83.9

84.5

85.3

84.3

86.5

79.8

86.1

85.6

84.9

81.3

86.2

83.7

82.1

79.5

84.4

89.3

126.8

<0.00020

<0.00020

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

N/A

N/A

50

50

50-150

50-150

50-150

50-150

50-150

50-150

50-150

50-150

50-150

50-150

50-150

50-150

50-150

50-150

50-150

50-150

50-150

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

mg/L

mg/L

<0.00020

<0.00020

0.005

0.005

0.005

0.005

0.005

0.005

0.005

50-150

50-150

50-150

50-150

RPD-NA

RPD-NA

22


Client:

Contact:




PCB-TCLP-WT

VOC-TCLP-WT

Waste

Waste

R3668436

R3668166

Batch

Batch

DUP

LCS

MB

MS

DUP

LCS

WG2489277-5

WG2489277-2

WG2489277-1

WG2489277-4

WG2488272-4

WG2488272-1

WG2489277-3

WG2489277-3

WG2488272-3

Aroclor 1254

Aroclor 1260

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260


Aroclor 1242

Aroclor 1254

Aroclor 1260


1,2-Dichlorobenzene

1,2-Dichloroethane

1,4-Dichlorobenzene

Benzene


Chlorobenzene

Chloroform

Dichloromethane

Methyl Ethyl Ketone

Tetrachloroethylene

Trichloroethylene

Vinyl chloride

<0.00020

<0.00020

76.1

75.4

90.9

93.6

<0.00020

<0.00020

<0.00020

<0.00020

97.2

73.8

85.6

92.8

<0.025

0.921

<0.025

0.068

<0.025

<0.025

<0.025

<0.10

<0.50

<1.0

<0.025

<0.025

<0.050

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

N/A

N/A

N/A

1.0

N/A

5.0

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

65-130

65-130

65-130

65-130

50-150

50-150

50-150

mg/L

mg/L

%

%

%

%

mg/L

mg/L

mg/L

mg/L

%

%

%

%

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

<0.00020

<0.00020

<0.025

0.930

<0.025

0.064

<0.025

<0.025

<0.025

<0.10

<0.50

<1.0

<0.025

<0.025

<0.050

0.0002

0.0002

0.0002

0.0002

40-160

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

22


Client:

Contact:




VOC-TCLP-WT Waste

R3668166BatchLCS

MB

MS

WG2488272-1

WG2488272-2

WG2488272-5 WG2488272-3


1,2-Dichlorobenzene

1,2-Dichloroethane

1,4-Dichlorobenzene

Benzene


Chlorobenzene

Chloroform

Dichloromethane

Methyl Ethyl Ketone

Tetrachloroethylene

Trichloroethylene

Vinyl chloride


1,2-Dichlorobenzene

1,2-Dichloroethane

1,4-Dichlorobenzene

Benzene


Chlorobenzene

Chloroform

Dichloromethane

Methyl Ethyl Ketone

Tetrachloroethylene

Trichloroethylene

Vinyl chloride




1,2-Dichlorobenzene

1,2-Dichloroethane

1,4-Dichlorobenzene

102.7

99.2

98.2

101.7

104.8

103.4

102.6

103.3

102.6

92.3

102.7

104.5

103.5

<0.025

<0.025

<0.025

<0.025

<0.025

<0.025

<0.025

<0.10

<0.50

<1.0

<0.025

<0.025

<0.050

103.6

107.5

94.0

92.2

103.0

99.96

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

70-130

70-130

70-130

70-130

70-130

60-140

70-130

70-130

70-130

50-150

70-130

70-130

60-130

50-140

50-140

50-140

50-140

%

%

%

%

%

%

%

%

%

%

%

%

%

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

%

%

%

%

%

%

0.025

0.025

0.025

0.025

0.025

0.025

0.025

0.1

0.5

1

0.025

0.025

0.05

70-130

70-130

22


Client:

Contact:




VOC-TCLP-WT Waste

R3668166BatchMSWG2488272-5 WG2488272-3

Benzene


Chlorobenzene

Chloroform

Dichloromethane

Methyl Ethyl Ketone

Tetrachloroethylene

Trichloroethylene

Vinyl chloride

104.6

99.7

103.4

105.0

102.9

102.7

100.2

103.3

87.3

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

06-MAR-17

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

%

%

%

%

%

%

%

%

%

22


Page 22 of




J

MES

RPD-NA


Data Quality Objective was marginally exceeded (by < 10% absolute) for < 10% of analytes in a Multi-Element Scan / Multi-Parameter Scan (considered acceptable as per OMOE & CCME).Relative Percent Difference Not Available due to result(s) being less than detection limit.


Legend:






Client:

Contact:


22

Printed on 3/3/2017 6:08:21 PM

ALS Sample ID: L1895710-1Client Sample ID: BH4 SS1

2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0

Time - Minutes

0

50

100

150

200

250

300

350

400

450

500

Response - M

illiVolts

Printed on 3/6/2017 11:38:12 AM

ALS Sample ID: L1895710-10Client Sample ID: BH5 SS2

2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0

Time - Minutes

0

50

100

150

200

250

300

350

400

450

500

Response - M

illiVolts

APPENDIX F

Tables:

Soil Chemical Analyses

Table 1 - Soil Chemical AnalysesVolatile Organic Compounds

Sample Location BH3 BH4 BH5Sample ID BH3-SS2 BH4 SS1 BH5 SS2

Soil Type Clayey Silt Fill Topsoil and SandySilt/Silty Sand Fill Silty Sand Fill

Sample Depth (mbgs) 0.8-1.4 0-0.6 0.7-1.3Field Vapour Reading 0/0 0/0 0/0Sampling Date 23-Feb-2017 24-Feb-2017 24-Feb-2017Analyzed Date 3-Mar-2017 3-Mar-2017 3-Mar-2017Laboratory ID L1894670-21 L1895710-1 L1895710-10Certificate of Analysis No. L1894670 L1895710 L1895710

Table 1 Table 2 Table 3 Table 9SCS SCS SCS SCS

Acetone 0.5 0.5 28 28 0.5 <0.50 <0.50 <0.50Benzene 0.0068 0.02 0.17 0.17 0.02 <0.0068 <0.0068 <0.0068Bromodichloromethane 0.05 0.05 1.9 13 0.05 <0.050 <0.050 <0.050Bromoform 0.05 0.05 0.26 0.26 0.05 <0.050 <0.050 <0.050Bromomethane 0.05 0.05 0.05 0.05 0.05 <0.050 <0.050 <0.050Carbon tetrachloride 0.05 0.05 0.12 0.12 0.05 <0.050 <0.050 <0.050Chlorobenzene 0.05 0.05 2.7 2.7 0.05 <0.050 <0.050 <0.050Dibromochloromethane 0.05 0.05 2.9 9.4 0.05 <0.050 <0.050 <0.050Chloroform 0.05 0.05 0.17 0.17 0.05 <0.050 <0.050 <0.0501,2-Dibromoethane 0.05 0.05 0.05 0.05 0.05 <0.050 <0.050 <0.0501,2-Dichlorobenzene 0.05 0.05 1.7 4.3 0.05 <0.050 <0.050 <0.0501,3-Dichlorobenzene 0.05 0.05 6 6 0.05 <0.050 <0.050 <0.0501,4-Dichlorobenzene 0.05 0.05 0.097 0.097 0.05 <0.050 <0.050 <0.050Dichlorodifluoromethane 0.05 0.05 25 25 0.05 <0.050 <0.050 <0.0501,1-Dichloroethane 0.05 0.05 0.6 11 0.05 <0.050 <0.050 <0.0501,2-Dichloroethane 0.05 0.05 0.05 0.05 0.05 <0.050 <0.050 <0.0501,1-Dichloroethylene 0.05 0.05 0.05 0.05 0.05 <0.050 <0.050 <0.050cis-1,2-Dichloroethylene 0.05 0.05 2.5 30 0.05 <0.050 <0.050 <0.050trans-1,2-Dichloroethylene 0.05 0.05 0.75 0.75 0.05 <0.050 <0.050 <0.050Methylene Chloride 0.2 0.05 0.96 0.96 0.05 <0.20 <0.050 <0.0501,2-Dichloropropane 0.05 0.05 0.085 0.085 0.05 <0.050 <0.050 <0.050cis-1,3-Dichloropropene 0.03 NV NV NV NV <0.030 <0.030 <0.030trans-1,3-Dichloropropene 0.03 NV NV NV NV <0.030 <0.030 <0.0301,3-Dichloropropene (cis & trans) 0.042 0.05 0.081 0.083 0.05 <0.042 <0.042 <0.042Ethylbenzene 0.018 0.05 1.6 15 0.05 <0.018 <0.018 <0.018n-Hexane 0.05 0.05 34 34 0.05 <0.050 <0.050 <0.050Methyl Ethyl Ketone 0.5 0.5 44 44 0.5 <0.50 <0.50 <0.50Methyl Isobutyl Ketone 0.5 0.5 4.3 4.3 0.5 <0.50 <0.50 <0.50MTBE 0.05 0.05 1.4 1.4 0.05 <0.050 <0.050 <0.050Styrene 0.05 0.05 2.2 2.2 0.05 <0.050 <0.050 <0.0501,1,1,2-Tetrachloroethane 0.05 0.05 0.05 0.05 0.05 <0.050 <0.050 <0.0501,1,2,2-Tetrachloroethane 0.05 0.05 0.05 0.05 0.05 <0.050 <0.050 <0.050Tetrachloroethylene 0.05 0.05 2.3 2.3 0.05 <0.050 <0.050 <0.050Toluene 0.08 0.2 6 6 0.2 <0.080 <0.080 <0.0801,1,1-Trichloroethane 0.05 0.05 3.4 3.4 0.05 <0.050 <0.050 <0.0501,1,2-Trichloroethane 0.05 0.05 0.05 0.05 0.05 <0.050 <0.050 <0.050Trichloroethylene 0.01 0.05 0.52 0.52 0.05 <0.010 <0.010 <0.010Trichlorofluoromethane 0.05 0.25 5.8 5.8 0.25 <0.050 <0.050 <0.050Vinyl chloride 0.02 0.02 0.022 0.022 0.02 <0.020 <0.020 <0.020o-Xylene 0.02 NV NV NV NV <0.020 <0.020 <0.020m+p-Xylenes 0.03 NV NV NV NV <0.030 <0.030 <0.030Xylenes (Total) 0.05 0.05 25 25 0.05 <0.050 <0.050 <0.050

RDL

Notes: Ontario Regulation 153/04, as amended, Table 1 Full Depth Background Site Condition Standards (SCS) forresidential/parkland/institutional/industrial/commercial/community property use (Table 1 SCS), Table 2 Full Depth Generic SCS in a potablegroundwater condition for residential/parkland/institutional property use (Table 2 SCS), Table 3 (non-potable groundwater) SCS for residential/parkland/ institutional property use (Table 3 SCS), and Table 9 (non-potable groundwater) SCS for all type of property use (Table 9 SCS), andmedium/fine textured soils . All values reported in µg/g (ppm) dry weight basis, unless otherwise noted. Table 1 SCS exceedances indicated inSHADING. Table 2 SCS exceedances indicated in THICK FRAME. Table 3 SCS exceedances indicated in BOLD. Table 9 SCS exceedancesindicated in UNDERLINE. "RDL" means reportable detection limit. "<" indicates not detected above the RDL as shown. "ppm" means parts permillion. Field vapour readings shown in ppm unless otherwise noted. Field vapour readings shown as combustible organic vapour (COV) / totalorganic vapour (TOV). "NV" means no value. "NA" means not applicable.

TT163027 Page 1 of 1

Table 2 - Soil Chemical AnalysesPetroleum Hydrocarbons

Sample Location BH3 BH4 BH5Sample ID BH3-SS2 BH4 SS1 BH5 SS2

Soil Type Clayey Silt FillSandy

Silt/Silty Sandfill

Silty Sand Fill

Sample Depth (mbgs) 0.8-1.4 0-0.6 0.7-1.3Field Vapour Reading 0/0 0/0 0/0Sampling Date 23-Feb-2017 24-Feb-2017 24-Feb-2017

Analyzed Date 3 and 5-Mar-2017 3 and 6-Mar-2017

3 and 6-Mar-2017

Laboratory ID L1894670-21 L1895710-1 L1895710-10Certificate of Analysis No. L1894670 L1895710 L1895710


PHC F1 (C6-C10 less BTEX) 5.0 25 65 65 25 <5.0 <5.0 <5.0PHC F2 (>C10-C16) 10 10 150 150 10 <10 <10 <10PHC F3 (>C16-C34) 50 240 1300 1300 240 <50 <50 <50PHC F4 (>C34)* 50 120 5600 5600 120 <50 <50 <50

RDL

Notes: Ontario Regulation 153/04, as amended, Table 1 Full Depth Background Site Condition Standards (SCS) forresidential/parkland/institutional/industrial/commercial/community property use (Table 1 SCS), Table 2 Full Depth Generic SCS in a potablegroundwater condition for residential/parkland/institutional property use (Table 2 SCS), Table 3 (non-potable groundwater) SCS forresidential/ parkland/ institutional property use (Table 3 SCS), and Table 9 (non-potable groundwater) SCS for all type of property use (Table9 SCS), and medium/fine textured soils . All values reported in µg/g (ppm) dry weight basis, unless otherwise noted. Table 1 SCSexceedances indicated in SHADING. Table 2 SCS exceedances indicated in THICK FRAME. Table 3 SCS exceedances indicated in BOLD.Table 9 SCS exceedances indicated in UNDERLINE. "RDL" means reportable detection limit. "<" indicates not detected above the RDL asshown. "ppm" means parts per million. Field vapour readings shown in ppm unless otherwise noted. Field vapour readings shown ascombustible organic vapour (COV) / total organic vapour (TOV). "NV" means no value. "NA" means not applicable. "F" means fraction. * IfF4 analysis by GC/FID did not reach baseline, F4 gravimetric analysis was conducted. Higher of two F4 values shown. "-" means notanalyzed.


Table 3 - Soil Chemical AnalysesPolycyclic Aromatic Hydrocarbons

Sample Location BH2 BH3 BH4 BH5Sample ID BH2-SS2 BH3-SS2 BH4 SS3 BH5 SS2

Soil Type Clayey Silt Fill Clayey Silt FillSandy

Silt/Silty Sandfill

Silty Sand Fill

Sample Depth (mbgs) 0.8-1.4 0.8-1.4 1.5-2.1 0.8-1.4Field Vapour Reading 0/0 0/0 0/0 0/0Sampling Date 23-Feb-2017 23-Feb-2017 24-Feb-2017 24-Feb-2017Analyzed Date 4-Mar-2017 4-Mar-2017 7-Mar-2017 7-Mar-2017Laboratory ID L1894670-12 L1894670-21 L1895710-3 L1895710-10Certificate of Analysis No. L1894670 L1894670 L1895710 L1895710


Acenaphthene 0.050 0.072 29 58 0.072 <0.050 0.108 <0.050 <0.050Acenaphthylene 0.050 0.093 0.17 0.17 0.093 <0.050 <0.050 <0.050 <0.050Anthracene 0.050 0.16 0.74 0.74 0.22 <0.050 0.204 <0.050 <0.050Benzo(a)anthracene 0.050 0.36 0.63 0.63 0.36 <0.050 0.3 <0.050 <0.050Benzo(a)pyrene 0.050 0.3 0.3 0.3 0.3 <0.050 0.239 <0.050 <0.050Benzo(b)fluoranthene 0.050 0.47 0.78 0.78 0.47 <0.050 0.325 <0.050 <0.050Benzo(g,h,i)perylene 0.050 0.68 7.8 7.8 0.68 <0.050 0.144 <0.050 <0.050Benzo(k)fluoranthene 0.050 0.48 0.78 0.78 0.48 <0.050 0.095 <0.050 <0.050Chrysene 0.050 2.8 7.8 7.8 2.8 <0.050 0.273 <0.050 <0.050Dibenz(a,h)anthracene 0.050 0.1 0.1 0.1 0.1 <0.050 <0.050 <0.050 <0.050Fluoranthene 0.050 0.56 0.69 0.69 0.69 <0.050 0.654 <0.050 <0.050Fluorene 0.050 0.12 69 69 0.19 <0.050 0.083 <0.050 <0.050Indeno(1,2,3-cd)pyrene 0.050 0.23 0.48 0.48 0.23 <0.050 0.134 <0.050 <0.050Methylnaphthalene, 2-(1-) 0.042 0.59 3.4 3.4 0.59 <0.042 <0.042 <0.042 <0.0421-Methylnaphthalene 0.030 0.59 3.4 3.4 0.59 <0.030 <0.030 <0.030 <0.0302-Methylnaphthalene 0.030 0.59 3.4 3.4 0.59 <0.030 <0.030 <0.030 <0.030Naphthalene 0.050 0.09 0.75 0.75 0.09 <0.050 <0.050 <0.050 <0.050Phenanthrene 0.050 0.69 7.8 7.8 0.69 <0.050 0.739 <0.050 <0.050Pyrene 0.050 1 78 78 1 <0.050 0.573 <0.050 <0.050

RDL

Notes: Ontario Regulation 153/04, as amended, Table 1 Full Depth Background Site Condition Standards (SCS) forresidential/parkland/institutional/industrial/commercial/community property use (Table 1 SCS), Table 2 Full Depth Generic SCS in a potable groundwatercondition for residential/parkland/institutional property use (Table 2 SCS), Table 3 (non-potable groundwater) SCS for residential/ parkland/ institutionalproperty use (Table 3 SCS), and Table 9 (non-potable groundwater) SCS for all type of property use (Table 9 SCS), and medium/fine textured soils . Allvalues reported in µg/g (ppm) dry weight basis, unless otherwise noted. Table 1 SCS exceedances indicated in SHADING. Table 2 SCS exceedancesindicated in THICK FRAME. Table 3 SCS exceedances indicated in BOLD. Table 9 SCS exceedances indicated in UNDERLINE. "RDL" means reportabledetection limit. "<" indicates not detected above the RDL as shown. "ppm" means parts per million. Field vapour readings shown in ppm unless otherwisenoted. Field vapour readings shown as combustible organic vapour (COV) / total organic vapour (TOV). "NV" means no value.


Table 4 - Soil Chemical AnalysesMetal and Inorganic Parameters

Sample Location

Sample ID BH1-SS1 BH1-SS3 BH1-SS5

Soil Type Topsoil and OrganicSilty Clay Organic Silty Clay Sandy Gravel

Sample Depth (mbgs) 0-0.6 1.5-2.1 3.0-3.6Field Vapour Reading 0/0 0/0 NASampling Date 23-Feb-2017 23-Feb-2017 23-Feb-2017

Latest Analyzed Date 3 and 6-Mar-2017 3 and 6-Mar-2017 3 and 6-Mar 2017


LOWER Table 1 Table 2 Table 3 Table 9RDL SCS SCS SCS SCS

Electrical Conductivity (mS/cm) 0.004 0.57 0.7 0.7 0.7 0.969 1.10 0.187Sodium Adsorption Ratio 0.1 2.4 5 5 5 0.42 0.14 0.25pH 0.10 NA NA NA NA 6.71 7.56 7.94

Antimony 1.0 1.3 7.5 7.5 1.3 <1.0 <1.0 <1.0Arsenic 1.0 18 18 18 18 1.7 <1.0 1.1Barium 1.0 220 390 390 220 72.2 26.0 16.7Beryllium 0.50 2.5 5 5 2.5 <0.50 <0.50 <0.50Boron, Hot Water Extractable 0.10 NV 1.5 1.5 1.5 0.96 0.40 <0.10Boron, Total 5.0 36 120 120 36 <5.0 <5.0 <5.0Cadmium 0.50 1.2 1.2 1.2 1.2 <0.50 <0.50 <0.50Chromium, Total 1.0 70 160 160 70 8.9 5.9 9.1Cobalt 1.0 21 22 22 22 2.7 1.7 2.2Copper 1.0 92 180 180 92 7.1 3.3 5.1Lead 1.0 120 120 120 120 11.0 1.3 1.8Mercury 0.005 0.27 1.8 1.8 0.27 0.0449 <0.0050 <0.0050Molybdenum 1.0 2 6.9 6.9 2 <1.0 2.1 <1.0Nickel 1.0 82 130 130 82 5.9 3.4 4.1Selenium 1.0 1.5 2.4 2.4 1.5 <1.0 <1.0 <1.0Silver 0.20 0.5 25 25 0.5 <0.20 <0.20 <0.20Thallium 0.50 1 1 1 1 <0.50 <0.50 <0.50Uranium 1.0 2.5 23 23 2.5 <1.0 <1.0 <1.0Vanadium 1.0 86 86 86 86 15.7 15.1 19.9Zinc 5.0 290 340 340 290 24.2 7.7 9.5Cyanide, Free 0.05 0.051 0.051 0.051 0.051 <0.050 <0.050 <0.050Chromium, VI 0.20 0.66 10 10 0.66 <1.0 <0.20 <0.20

Notes: Ontario Regulation 153/04, as amended, Table 1 Full Depth Background Site Condition Standards (SCS) forresidential/parkland/institutional/industrial/commercial/community property use (Table 1 SCS), Table 2 Full Depth Generic SCS in a potablegroundwater condition for residential/parkland/institutional property use (Table 2 SCS), Table 3 (non-potable groundwater) SCS for residential/parkland/ institutional property use (Table 3 SCS), and Table 9 (non-potable groundwater) SCS for all type of property use (Table 9 SCS), andmedium/fine textured soils . All values reported in µg/g (ppm) dry weight basis, unless otherwise noted. Table 1 SCS exceedances indicated inSHADING. Table 2 SCS exceedances indicated in THICK FRAME. Table 3 SCS exceedances indicated in BOLD. Table 9 SCS exceedancesindicated in UNDERLINE. ITALICS mean that the RDL is higher than Table 1 and Table 9 SCS. "RDL" means reportable detection limit. "<" indicatesnot detected above the RDL as shown. "ppm" means parts per million. Field vapour readings shown in ppm unless otherwise noted. Field vapourreadings shown as combustible organic vapour (COV) / total organic vapour (TOV). "NV" means no value. *To apply generic SCS, pH of soil is to bebetween 5 and 9 for surface soil (<1.5 mbg) and between 5 and 11 for subsurface soil (>1.5 mbg). "-" means not analyzed.

BH1



Sample Location


Soil Type Topsoil andSandy Silt Fill Sandy Silt Fill Sand Fill

Sample Depth (mbgs) 0-0.6 1.5-2.1 3.0-3.6Field Vapour Reading 0/0 0/0 0/0Sampling Date 23-Feb-2017 23-Feb-2017 23-Feb-2017

Latest Analyzed Date 3 and 6-Mar-2017 3 and 6-Mar-2017

3 and 6-Mar2017



Electrical Conductivity (mS/cm) 0.004 0.57 0.7 0.7 0.7 0.309 0.268 0.270Sodium Adsorption Ratio 0.1 2.4 5 5 5 <0.10 0.19 0.53pH 0.10 NA NA NA NA 7.60 7.19 7.29

Antimony 1.0 1.3 7.5 7.5 1.3 <1.0 <1.0 <1.0Arsenic 1.0 18 18 18 18 3.1 1.7 1.5Barium 1.0 220 390 390 220 55.0 44.0 29.0Beryllium 0.50 2.5 5 5 2.5 <0.50 <0.50 <0.50Boron, Hot Water Extractable 0.10 NV 1.5 1.5 1.5 0.42 0.37 0.30Boron, Total 5.0 36 120 120 36 5.3 <5.0 <5.0Cadmium 0.50 1.2 1.2 1.2 1.2 <0.50 <0.50 <0.50Chromium, Total 1.0 70 160 160 70 18.5 13.0 10.0Cobalt 1.0 21 22 22 22 5.0 3.9 3.2Copper 1.0 92 180 180 92 18.4 9.9 7.4Lead 1.0 120 120 120 120 25.8 8.0 5.8Mercury 0.005 0.27 1.8 1.8 0.27 0.179 0.0320 0.0142Molybdenum 1.0 2 6.9 6.9 2 <1.0 <1.0 <1.0Nickel 1.0 82 130 130 82 10.9 8.9 6.9Selenium 1.0 1.5 2.4 2.4 1.5 <1.0 <1.0 <1.0Silver 0.20 0.5 25 25 0.5 <0.20 <0.20 <0.20Thallium 0.50 1 1 1 1 <0.50 <0.50 <0.50Uranium 1.0 2.5 23 23 2.5 <1.0 <1.0 <1.0Vanadium 1.0 86 86 86 86 23.3 19.1 17.7Zinc 5.0 290 340 340 290 58.7 27.7 20.5Cyanide, Free 0.05 0.051 0.051 0.051 0.051 <0.050 <0.050 <0.050Chromium, VI 0.20 0.66 10 10 0.66 <0.20 <0.20 <0.20

Notes: Ontario Regulation 153/04, as amended, Table 1 Full Depth Background Site Condition Standards (SCS) forresidential/parkland/institutional/industrial/commercial/community property use (Table 1 SCS), Table 2 Full Depth Generic SCS in apotable groundwater condition for residential/parkland/institutional property use (Table 2 SCS), Table 3 (non-potable groundwater) SCSfor residential/ parkland/ institutional property use (Table 3 SCS), and Table 9 (non-potable groundwater) SCS for all type of property use(Table 9 SCS), and medium/fine textured soils . All values reported in µg/g (ppm) dry weight basis, unless otherwise noted. Table 1 SCSexceedances indicated in SHADING. Table 2 SCS exceedances indicated in THICK FRAME. Table 3 SCS exceedances indicated inBOLD. Table 9 SCS exceedances indicated in UNDERLINE. ITALICS mean that the RDL is higher than Table 1 and Table 9 SCS."RDL" means reportable detection limit. "<" indicates not detected above the RDL as shown. "ppm" means parts per million. Field vapourreadings shown in ppm unless otherwise noted. Field vapour readings shown as combustible organic vapour (COV) / total organicvapour (TOV). "NV" means no value. *To apply generic SCS, pH of soil is to be between 5 and 9 for surface soil (<1.5 mbg) and between5 and 11 for subsurface soil (>1.5 mbg). "-" means not analyzed.

BH2



Sample Location


Soil Type Topsoil andClayey Silt Fill

Gravelly SandFill Silt

Sample Depth (mbgs) 0-0.6 2.3-2.9 4.6-5.1Field Vapour Reading 0/1 0/1 0/0Sampling Date 23-Feb-2017 23-Feb-2017 23-Feb-2017

Latest Analyzed Date 3 and 6-Mar-2017

3 and 6-Mar-2017

3 and 6-Mar2017



Electrical Conductivity (mS/cm) 0.004 0.57 0.7 0.7 0.7 0.154 0.228 0.419Sodium Adsorption Ratio 0.1 2.4 5 5 5 0.56 1.39 1.51pH 0.10 NA NA NA NA 7.75 7.77 7.74

Antimony 1.0 1.3 7.5 7.5 1.3 <1.0 <1.0 <1.0Arsenic 1.0 18 18 18 18 2.8 2.0 1.3Barium 1.0 220 390 390 220 47.4 36.5 22.6Beryllium 0.50 2.5 5 5 2.5 <0.50 <0.50 <0.50Boron, Hot Water Extractable 0.10 NV 1.5 1.5 1.5 <0.10 0.12 <0.10Boron, Total 5.0 36 120 120 36 6.0 <5.0 <5.0Cadmium 0.50 1.2 1.2 1.2 1.2 <0.50 <0.50 <0.50Chromium, Total 1.0 70 160 160 70 15.9 12.6 8.5Cobalt 1.0 21 22 22 22 5.8 4.2 3.0Copper 1.0 92 180 180 92 13.5 9.2 6.2Lead 1.0 120 120 120 120 10.2 9.5 2.3Mercury 0.005 0.27 1.8 1.8 0.27 0.0144 0.0158 <0.0050Molybdenum 1.0 2 6.9 6.9 2 <1.0 <1.0 <1.0Nickel 1.0 82 130 130 82 13.4 8.9 5.8Selenium 1.0 1.5 2.4 2.4 1.5 <1.0 <1.0 <1.0Silver 0.20 0.5 25 25 0.5 <0.20 <0.20 <0.20Thallium 0.50 1 1 1 1 <0.50 <0.50 <0.50Uranium 1.0 2.5 23 23 2.5 <1.0 <1.0 <1.0Vanadium 1.0 86 86 86 86 23.7 23.5 17.2Zinc 5.0 290 340 340 290 38.4 28.7 13.2Cyanide, Free 0.05 0.051 0.051 0.051 0.051 <0.050 <0.050 <0.050Chromium, VI 0.20 0.66 10 10 0.66 0.32 <0.20 <0.20

Notes: Ontario Regulation 153/04, as amended, Table 1 Full Depth Background Site Condition Standards (SCS) forresidential/parkland/institutional/industrial/commercial/community property use (Table 1 SCS), Table 2 Full Depth Generic SCS ina potable groundwater condition for residential/parkland/institutional property use (Table 2 SCS), Table 3 (non-potablegroundwater) SCS for residential/ parkland/ institutional property use (Table 3 SCS), and Table 9 (non-potable groundwater) SCSfor all type of property use (Table 9 SCS), and medium/fine textured soils . All values reported in µg/g (ppm) dry weight basis,unless otherwise noted. Table 1 SCS exceedances indicated in SHADING. Table 2 SCS exceedances indicated in THICK FRAME.Table 3 SCS exceedances indicated in BOLD. Table 9 SCS exceedances indicated in UNDERLINE. ITALICS mean that the RDLis higher than Table 1 and Table 9 SCS. "RDL" means reportable detection limit. "<" indicates not detected above the RDL asshown. "ppm" means parts per million. Field vapour readings shown in ppm unless otherwise noted. Field vapour readings shownas combustible organic vapour (COV) / total organic vapour (TOV). "NV" means no value. *To apply generic SCS, pH of soil is tobe between 5 and 9 for surface soil (<1.5 mbg) and between 5 and 11 for subsurface soil (>1.5 mbg). "-" means not analyzed.

BH3



Sample Location

Sample ID BH4 SS2 BH4 SS4 BH4 SS7

Soil TypeSandy

Silt/Silty SandFill

SandySilt/Silty Sand

Fill andGravelly Sand

Silt

Sample Depth (mbgs) 0.8-1.4 2.3-2.9 4.6-5.1Field Vapour Reading 0/0 0/0 0/0Sampling Date 24-Feb-2017 24-Feb-2017 24-Feb-2017


6 and 7-Mar-2017

6 and 7-Mar-2017




Antimony 1.0 1.3 7.5 7.5 1.3 <1.0 <1.0 <1.0Arsenic 1.0 18 18 18 18 1.7 1.8 1.3Barium 1.0 220 390 390 220 37.1 45.2 31.0Beryllium 0.50 2.5 5 5 2.5 <0.50 <0.50 <0.50Boron, Hot Water Extractable 0.10 NV 1.5 1.5 1.5 0.18 <0.10 <0.10Boron, Total 5.0 36 120 120 36 <5.0 <5.0 <5.0Cadmium 0.50 1.2 1.2 1.2 1.2 <0.50 <0.50 <0.50Chromium, Total 1.0 70 160 160 70 10.3 4.9 8.8Cobalt 1.0 21 22 22 22 3.3 1.6 2.7Copper 1.0 92 180 180 92 9.0 3.3 5.9Lead 1.0 120 120 120 120 11.4 2.1 4.3Mercury 0.005 0.27 1.8 1.8 0.27 0.0278 <0.0050 0.0084Molybdenum 1.0 2 6.9 6.9 2 <1.0 <1.0 <1.0Nickel 1.0 82 130 130 82 6.9 3.2 5.6Selenium 1.0 1.5 2.4 2.4 1.5 <1.0 <1.0 <1.0Silver 0.20 0.5 25 25 0.5 <0.20 <0.20 <0.20Thallium 0.50 1 1 1 1 <0.50 <0.50 <0.50Uranium 1.0 2.5 23 23 2.5 <1.0 <1.0 <1.0Vanadium 1.0 86 86 86 86 18.6 11.9 15.8Zinc 5.0 290 340 340 290 26.4 9.3 17.0Cyanide, Free 0.05 0.051 0.051 0.051 0.051 <0.050 <0.050 <0.050Chromium, VI 0.20 0.66 10 10 0.66 0.33 <0.20 <0.20


BH4



Sample Location

Sample ID BH5 SS2 BH5 SS3 BH5 SS4

Soil Type Silty Sand Fill Silty Sand Fill Fine Sand

Sample Depth (mbgs) 0.7-1.3 1.5-2.1 2.3-2.9Field Vapour Reading 0/0 0/0 0/0Sampling Date 24-Feb-2017 24-Feb-2017 24-Feb-2017


6 and 7-Mar-2017

6 and 7-Mar-2017




Antimony 1.0 1.3 7.5 7.5 1.3 <1.0 <1.0 <1.0Arsenic 1.0 18 18 18 18 1.4 1.2 1.1Barium 1.0 220 390 390 220 21.6 18.5 14.0Beryllium 0.50 2.5 5 5 2.5 <0.50 <0.50 <0.50Boron, Hot Water Extractable 0.10 NV 1.5 1.5 1.5 0.23 0.22 0.13Boron, Total 5.0 36 120 120 36 <5.0 <5.0 <5.0Cadmium 0.50 1.2 1.2 1.2 1.2 <0.50 <0.50 <0.50Chromium, Total 1.0 70 160 160 70 8.0 7.5 5.7Cobalt 1.0 21 22 22 22 3.1 2.9 2.5Copper 1.0 92 180 180 92 9.1 5.9 3.7Lead 1.0 120 120 120 120 5.7 5.8 1.9Mercury 0.005 0.27 1.8 1.8 0.27 0.0133 0.0090 <0.0050Molybdenum 1.0 2 6.9 6.9 2 <1.0 <1.0 <1.0Nickel 1.0 82 130 130 82 5.9 5.5 4.5Selenium 1.0 1.5 2.4 2.4 1.5 <1.0 <1.0 <1.0Silver 0.20 0.5 25 25 0.5 <0.20 <0.20 <0.20Thallium 0.50 1 1 1 1 <0.50 <0.50 <0.50Uranium 1.0 2.5 23 23 2.5 <1.0 <1.0 <1.0Vanadium 1.0 86 86 86 86 15.8 14.9 11.0Zinc 5.0 290 340 340 290 18.4 19.4 9.7Cyanide, Free 0.05 0.051 0.051 0.051 0.051 <0.050 <0.050 <0.050Chromium, VI 0.20 0.66 10 10 0.66 <0.20 <0.20 <0.20


BH5


Table 5 - Soil Chemical AnalysesPolychlorinated Biphenyls

Sample Location BH3 BH5

Sample ID BH3-SS1 BH5 SS1

Soil Type Topsoil andSandy Silt Fill

Topsoil andSandy Silt Fill

Sample Depth (mbgs) 0-0.6 0-0.6Field Vapour Reading 0/1 0/0Sampling Date 23-Feb-2017 24-Feb-2017Latest Analyzed Date 6-Mar-2017 6-Mar-2017Laboratory ID L1894670-20 L1895710-9Certificate of Analysis No. L1894670 L1895710


Total PCBs 0.020 0.30 0.35 0.35 0.30 < 0.020 <0.040

Notes: Ontario Regulation 153/04, as amended, Table 1 Full Depth Background Site Condition Standards (SCS) forresidential/parkland/institutional/industrial/commercial/community property use (Table 1 SCS), Table 2 Full DepthGeneric SCS in a potable groundwater condition for residential/parkland/institutional property use (Table 2 SCS),Table 3 (non-potable groundwater) SCS for residential/ parkland/ institutional property use (Table 3 SCS), and Table9 (non-potable groundwater) SCS for all type of property use (Table 9 SCS), and medium/fine textured soils . Allvalues reported in µg/g (ppm) dry weight basis, unless otherwise noted. Table 1 SCS exceedances indicated inSHADING. Table 2 SCS exceedances indicated in THICK FRAME. Table 3 SCS exceedances indicated in BOLD.Table 9 SCS exceedances indicated in UNDERLINE. "RDL" means reportable detection limit. "<" indicates notdetected above the RDL as shown. "ppm" means parts per million. Field vapour readings shown in ppm unlessotherwise noted. Field vapour readings shown as combustible organic vapour (COV) / total organic vapour (TOV)."NV" means no value.


Table 6 - Soil Chemical AnalysesOrganochloride Pesticides and Herbicides

Sample Location BH1 BH2 BH3Sample ID BH1-SS1 BH2-SS1 BH3-SS1

Soil TypeTopsoil andOrganic Silty

Clay

Topsoil and SandySilt Fill

Topsoil and SandySilt Fill

Sample Depth (mbgs) 0-0.6 0-0.6 0-0.6Field Vapour Reading 0/0 0/0 0/1Sampling Date 23-Feb-2017 23-Feb-2017 23-Feb-2017Latest Analyzed Date 3-Mar-2017 3-Mar-2017 3-Mar-2017Laboratory ID L1894670-1 L1894670-11 L1894670-20Certificate of Analysis No. L1894670 L1894670 L1894670


Aldrin 0.020 0.05 0.05 0.05 0.05 <0.020 <0.020 <0.020gamma-hexachlorocyclohexane 0.010 0.01 0.063 0.063 0.01 <0.010 <0.010 <0.010a-chlordane 0.020 NV NV NV NV <0.020 <0.020 <0.020Chlordane (Total) 0.028 0.05 0.05 0.05 0.05 <0.028 <0.028 <0.028g-chlordane 0.020 NV NV NV NV <0.020 <0.020 <0.020op-DDD 0.020 NV NV NV NV <0.020 <0.020 <0.020pp-DDD 0.020 NV NV NV NV <0.020 <0.020 <0.20Total DDD 0.028 0.05 3.3 3.3 0.05 <0.028 <0.028 <0.20o,p-DDE 0.020 NV NV NV NV <0.020 <0.020 <0.020pp-DDE 0.020 NV NV NV NV <0.020 <0.020 <0.020Total DDE 0.028 0.05 0.33 0.33 0.05 <0.028 <0.028 <0.028op-DDT 0.020 NV NV NV NV <0.020 <0.020 <0.20pp-DDT 0.020 NV NV NV NV <0.020 <0.020 <0.20Total DDT 0.028 1.4 1.4 1.4 1.4 <0.028 <0.028 <0.28Dieldrin 0.020 0.05 0.05 0.05 0.05 <0.020 <0.020 <0.020Endosulfan I 0.020 NV NV NV NV <0.020 <0.020 <0.020Endosulfan II 0.020 NV NV NV NV <0.020 <0.020 <0.020Endosulfan (Total) 0.028 0.04 0.04 0.04 0.04 <0.028 <0.028 <0.028Endrin 0.020 0.04 0.04 0.04 0.04 <0.020 <0.020 <0.020Heptachlor 0.020 0.05 0.15 0.15 0.05 <0.020 <0.020 <0.020Heptachlor Epoxide 0.020 0.05 0.05 0.05 0.05 <0.020 <0.020 <0.020Hexachlorobenzene 0.010 0.01 0.52 0.52 0.02 <0.010 <0.010 <0.010Hexachlorobutadiene 0.010 0.01 0.014 0.014 0.01 <0.010 <0.010 <0.010Hexachloroethane 0.010 0.01 0.071 0.07 NV <0.010 <0.010 <0.010Methoxychlor 0.020 0.05 0.13 0.13 0.05 <0.020 <0.020 <0.020Bromoxynil 0.080 NV NV NV NV <0.080 <0.080 <0.0802,4-D 0.080 NV NV NV NV <0.080 <0.080 <0.080Dicamba 0.080 NV NV NV NV <0.080 <0.080 <0.080Dinoseb 0.080 NV NV NV NV <0.080 <0.080 <0.080MCPA 0.300 NV NV NV NV <0.30 <0.30 <0.30Mecoprop 0.300 NV NV NV NV <0.30 <0.30 <0.30Picloram 0.080 NV NV NV NV <0.080 <0.080 <0.0802,4,5-T 0.080 NV NV NV NV <0.080 <0.080 <0.0802,4,5-TP 0.080 NV NV NV NV <0.080 <0.080 <0.080

Notes: Ontario Regulation 153/04, as amended, Table 1 Full Depth Background Site Condition Standards (SCS) forresidential/parkland/institutional/industrial/commercial/community property use (Table 1 SCS), Table 2 Full Depth Generic SCS in a potable groundwatercondition for residential/parkland/institutional property use (Table 2 SCS), Table 3 (non-potable groundwater) SCS for residential/ parkland/ institutionalproperty use (Table 3 SCS), and Table 9 (non-potable groundwater) SCS for all type of property use (Table 9 SCS), and medium/fine textured soils . Allvalues reported in µg/g (ppm) dry weight basis, unless otherwise noted. Table 1 SCS exceedances indicated in SHADING. Table 2 SCS exceedancesindicated in THICK FRAME. Table 3 SCS exceedances indicated in BOLD. Table 3 SCS exceedances indicated in UNDERLINE. "RDL" meansreportable detection limit. "<" indicates not detected above the RDL as shown. "ppm" means parts per million. Field vapour readings shown in ppmunless otherwise noted. Field vapour readings shown as combustible organic vapour (COV) / total organic vapour (TOV). "NV" means no value.

RDL


Table 7 - Ontario Regulation 558/00 Leachate AnalysesWaste Classification

Sample IDBH1-SS1, SS2, SS3,SS4. SS5, SS6, SS7

(COMPOSITE)

BH2-SS1, SS2, SS3,SS4, SS5, SS6, SS7

(COMPOSITE)BH4 SS9

Sampling Date 23-Feb-2017 28-Feb-17 24-Feb-2017Laboratory ID L1894670-29 L1896353-1 L1895710-8Certificate of Analysis No. L1894670 L1896353 L1895710

Cyanide, Weak Acid Diss 0.10 20 <0.10 <0.10 <0.10Fluoride (F-) 10 150 <10 <10 <10Nitrate + Nitrite 2.8 1000 <4.0 <4.0 <4.0

Arsenic (As) 0.05 2.5 <0.050 <0.050 <0.050Barium (Ba) 0.5 100 <0.50 <0.50 <0.50Boron (B) 2.5 500 <2.5 <2.5 <2.5Cadmium (Cd) 0.01 0.5 <0.0050 <0.0050 <0.0050Chromium (Cr) 0.05 5 <0.050 <0.050 <0.050Lead (Pb) 0.05 5 0.057 <0.050 <0.050Mercury (Hg) 0.0001 0.1 <0.00010 <0.00010 <0.00010Selenium (Se) 0.25 1 <0.025 <0.025 <0.025Silver (Ag) 0.01 5 <0.0050 <0.0050 <0.0050Uranium (U) 0.25 10 <0.25 <0.25 <0.25

Aroclor 1242 0.0002 NV <0.00020 <0.00020 <0.00020Aroclor 1248 0.0002 NV <0.00020 <0.00020 <0.00020Aroclor 1254 0.0002 NV <0.00020 <0.00020 <0.00020Aroclor 1260 0.0002 NV <0.00020 <0.00020 <0.00020

PCBs 0.0004 0.3 <0.00040 <0.00040 <0.00040

1,1-Dichloroethylene 0.025 1.4 <0.025 <0.025 <0.0251,2-Dichlorobenzene 0.025 20 0.065 <0.025 <0.0251,2-Dichloroethane 0.025 0.5 <0.025 <0.025 <0.0251,4-Dichlorobenzene 0.025 0.5 <0.025 <0.025 <0.025Benzene 0.025 0.5 <0.025 <0.025 <0.025Carbon Tetrachloride 0.025 0.5 <0.025 <0.025 <0.025Chlorobenzene 0.025 8 <0.025 <0.025 <0.025Chloroform 0.1 10 <0.10 <0.10 <0.10Dichloromethane 0.5 5 <0.50 <0.50 <0.50Methyl Ethyl Ketone 1 200 <1.0 <1.0 <1.0Tetrachloroethylene 0.025 3 <0.025 <0.025 <0.025Trichloroethylene 0.025 5 <0.025 <0.025 <0.025Vinyl Chloride 0.05 0.2 <0.050 <0.050 <0.050

Acenaphthene 0.005 NV <0.0050 <0.0050 <0.0050Acenaphthylene 0.005 NV <0.0050 <0.0050 <0.0050Anthracene 0.005 NV <0.0050 <0.0050 <0.0050Benzo(a)anthracene 0.005 NV <0.0050 <0.0050 <0.0050Benzo(a)pyrene 0.001 0.001 <0.0010 <0.0010 <0.0010Benzo(b)fluoranthene 0.005 NV <0.0050 <0.0050 <0.0050Benzo(g,h,i)perylene 0.005 NV <0.0050 <0.0050 <0.0050Benzo(k)fluoranthene 0.005 NV <0.0050 <0.0050 <0.0050Chrysene 0.005 NV <0.0050 <0.0050 <0.0050Dibenzo(ah)anthracene 0.005 NV <0.0050 <0.0050 <0.0050Fluoranthene 0.005 NV <0.0050 <0.0050 <0.0050Fluorene 0.005 NV <0.0050 <0.0050 <0.0050Indeno(1,2,3-cd)pyrene 0.005 NV <0.0050 <0.0050 <0.0050Naphthalene 0.005 NV <0.0050 <0.0050 <0.0050Phenanthrene 0.005 NV <0.0050 <0.0050 <0.0050Pyrene 0.005 NV <0.0050 <0.0050 <0.0050Quinoline 0.005 NV <0.0050 <0.0050 <0.0050

DL Schedule4 Leachate

Notes: Ontario Regulation 558/00, Schedule 4 Leachate Criteria. All results reported in mg/L except for Ignitability and flammability whichhave no units. "RDL" means reportable detection limit. "<" indicates not detected above RDL as shown. Schedule 4 exceedancesindicated in BOLD . "NV" means no value. "NA" means not applicable / not analyzed. "NI/NF means Not Ignitable/Not Flammable.


APPENDIX B

LABORATORY CERTIFICATE OF ANALYSIS(GROUNDWATER)


13-APR-18


Date Received:AMEC Foster Wheeler (Markham)

50 Vogell RoadUnit 3&4Richmond Hill ON L4B 3K6

ATTN: KIM GILDERFINAL 19-APR-18 14:28 (MT)Report Date:

Version:



____________________________________________

Mary-Lynn PikeClient Services Supervisor

ADDRESS: 95 West Beaver Creek Road, Unit 1, Richmond Hill, ON L4B 1H2 Canada | Phone: +1 905 881 9887 | Fax: +1 905 881 8062



17-638033C of C Numbers:Legal Site Desc:

19-APR-18 14:28 (MT)ANALYTICAL REPORT

L2080099 CONT’D....

2PAGE of

* Please refer to the Reference Information section for an explanation of any qualifiers noted.

Job Reference: TT16302720

Summary of Guideline Exceedances

GuidelineALS ID Client ID Grouping Analyte Result Guideline Limit Unit

Ontario Toronto Sanitary Discharge Sewer By-Law 100-2016 (FEB 4,2016) - Ontario Toronto Sanitary Discharge Sewer By-Law

Ontario Toronto Sanitary Discharge Sewer By-Law 100-2016 (FEB 4,2016) - Ontario Toronto Storm Sewer By-Law

L2080099-1

L2080099-2

L2080099-1

L2080099-2

BH-1

BH-5

BH-1

BH-5

Total Suspended Solids

Phosphorus, Total

Aluminum (Al)-TotalManganese (Mn)-Total



Phosphorus, Total

Arsenic (As)-TotalChromium (Cr)-TotalCopper (Cu)-TotalLead (Pb)-TotalManganese (Mn)-TotalNickel (Ni)-TotalZinc (Zn)-Total


Phosphorus, Total

Copper (Cu)-TotalManganese (Mn)-TotalZinc (Zn)-Total

mg/L

mg/L

mg/Lmg/L

mg/L

mg/L

mg/L

mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L

mg/L

mg/L

mg/Lmg/Lmg/L

350

10

505

350

15

0.4

0.020.080.040.120.050.080.04

15

0.4

0.040.050.04

952000

408

93.721.8

2180

952000

408

0.0550.1880.430.18121.80.2750.66

2180

3.64

0.0551.930.130

Physical Tests

Anions and Nutrients

Total Metals

Physical Tests

Physical Tests


Total Metals

Physical Tests


Total Metals


L2080099 CONT’D....

3PAGE of



Physical Tests - WATER

Guide Limit #1: Ontario Toronto Sanitary Discharge Sewer By-LawGuide Limit #2: Ontario Toronto Storm Sewer By-Law

pH


6.00-11.5350

6.0-9.5

15

L2080099-1 L2080099-213-APR-18 13-APR-18

BH-1 BH-5

pH units

mg/L

Lab IDSample Date

Sample ID

Guide LimitsUnit #1 #2Analyte

Analytical result for this parameter exceeds Guide Limits listed. See Summary of Guideline Exceedances.Detection Limit for result exceeds Guideline Limit. Assessment against Guideline Limit cannot be made.

7.91 7.43

952000 2180DLHC DLHC


L2080099 CONT’D....

4PAGE of



Anions and Nutrients - WATER


Fluoride (F)

Total Kjeldahl Nitrogen

Phosphorus, Total

10

100

10

-

-

0.4

L2080099-1 L2080099-213-APR-18 13-APR-18

BH-1 BH-5

mg/L

mg/L

mg/L

Lab IDSample Date

Sample ID



<0.20 <0.20

6.1 <1.5

408 3.64

DLM DLM

DLM DLM

DLM DLHC


L2080099 CONT’D....

5PAGE of



Cyanides - WATER


Cyanide, Total 2 0.02

L2080099-1 L2080099-213-APR-18 13-APR-18

BH-1 BH-5

mg/L

Lab IDSample Date

Sample ID



<0.0020 0.0113


L2080099 CONT’D....

6PAGE of



Bacteriological Tests - WATER


E. Coli - 200

L2080099-1 L2080099-213-APR-18 13-APR-18

BH-1 BH-5

CFU/100mL

Lab IDSample Date

Sample ID



<2 0DLM


L2080099 CONT’D....

7PAGE of



Total Metals - WATER


Aluminum (Al)-Total

Antimony (Sb)-Total

Arsenic (As)-Total

Cadmium (Cd)-Total

Chromium (Cr)-Total

Cobalt (Co)-Total

Copper (Cu)-Total

Lead (Pb)-Total

Manganese (Mn)-Total

Mercury (Hg)-Total

Molybdenum (Mo)-Total

Nickel (Ni)-Total

Selenium (Se)-Total

Silver (Ag)-Total

Tin (Sn)-Total

Titanium (Ti)-Total

Zinc (Zn)-Total

50

5

1

0.7

4

5

2

1

5

0.01

5

2

1

5

5

5

2

-

-

0.02

0.008

0.08

-

0.04

0.12

0.05

0.0004

-

0.08

0.02

0.12

-

-

0.04

L2080099-1 L2080099-213-APR-18 13-APR-18

BH-1 BH-5

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

Lab IDSample Date

Sample ID



93.7 17.8

<0.010 <0.0010

0.055 0.0048

0.00176 0.000350

0.188 0.0297

0.165 0.0529

0.43 0.055

0.181 0.0400

21.8 1.93

<0.00010 0.000020

<0.0050 <0.00050

0.275 0.0473

<0.0050 0.00102

<0.0050 <0.00050

<0.010 <0.0010

0.881 0.752

0.66 0.130

DLHC DLHC

DLHC DLHC

DLHC DLHC

DLHC DLHC

DLHC DLHC

DLHC DLHC

DLHC DLHC

DLHC DLHC

DLHC DLHC

DLM

DLHC DLHC

DLHC DLHC

DLHC DLHC

DLHC DLHC

DLHC DLHC

DLHC DLHC

DLHC DLHC


L2080099 CONT’D....

8PAGE of



Speciated Metals - WATER


Chromium, Hexavalent 2 0.04

L2080099-1 L2080099-213-APR-18 13-APR-18

BH-1 BH-5

mg/L

Lab IDSample Date

Sample ID



<0.0010 <0.0010


L2080099 CONT’D....

9PAGE of



Aggregate Organics - WATER


BOD

Oil and Grease, Total

Animal/Veg Oil & Grease

Mineral Oil and Grease

Phenols (4AAP)

300

-

150

15

1.0

15

-

-

-

0.008

L2080099-1 L2080099-213-APR-18 13-APR-18

BH-1 BH-5

mg/L

mg/L

mg/L

mg/L

mg/L

Lab IDSample Date

Sample ID



<3.0 <3.0

<4.0 <2.0

<4.0 <2.0

<2.0 <1.0

0.0012 <0.0010

BODL BODL

DLIS

DLIS


L2080099 CONT’D....

10PAGE of



Volatile Organic Compounds - WATER


Benzene

Chloroform

1,2-Dichlorobenzene

1,4-Dichlorobenzene


Dichloromethane


Ethylbenzene


Tetrachloroethylene

Toluene

Trichloroethylene

o-Xylene

m+p-Xylenes

Xylenes (Total)



10

40

50

80

4000

2000

140

160

1400

1000

16

400

-

-

1400

-

-

2

2

5.6

6.8

5.6

5.2

-

2

17

4.4

2

7.6

-

-

4.4

-

-

L2080099-1 L2080099-213-APR-18 13-APR-18

BH-1 BH-5

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

Lab IDSample Date

Sample ID



<0.50 <0.50

<1.0 <1.0

<0.50 <0.50

<0.50 <0.50

<0.50 <0.50

<2.0 <2.0

<0.50 <0.50

<0.50 <0.50

<0.50 <0.50

<0.50 <0.50

<0.50 <0.50

<0.50 <0.50

<0.50 <0.50

<1.0 <1.0

<1.1 <1.1

85.3 93.1

96.7 96.8


L2080099 CONT’D....

11PAGE of



Polycyclic Aromatic Hydrocarbons - WATER


Acenaphthene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene


Benzo(e)pyrene

Benzo(ghi)perylene


Chrysene

Dibenz(a,h)acridine

Dibenz(a,j)acridine

Dibenzo(a,h)anthracene

Dibenzo(a,i)pyrene

7H-Dibenzo(c,g)carbazole

1,3-Dinitropyrene

1,6-Dinitropyrene

1,8-Dinitropyrene

Fluoranthene

Fluorene


Naphthalene

Perylene

Phenanthrene

Pyrene




Total PAHs

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

5

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

2

L2080099-1 L2080099-213-APR-18 13-APR-18

BH-1 BH-5

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

ug/L

Lab IDSample Date

Sample ID



<0.010 <0.010

<0.010 0.013

<0.010 0.048

<0.010 0.032

<0.010 0.044

<0.050 <0.050

<0.010 0.019

<0.010 0.011

<0.010 0.051

<0.050 <0.050

<0.050 <0.050

<0.010 <0.010

<0.050 <0.050

<0.050 <0.050

<1.0 <1.0

<1.0 <1.0

<1.0 <1.0

<0.010 0.102

<0.010 <0.010

<0.010 0.019

<0.010 0.014

0.047 0.015

<0.010 0.059

<0.010 0.098

68.1 68.8

87.2 73.2

74.5 66.7

<1.7 <1.7

R


L2080099 CONT’D....

12PAGE of



Phthalate Esters - WATER


Bis(2-ethylhexyl)phthalate

Surrogate: 2-fluorobiphenyl


12

-

-

8.8

-

-

L2080099-1 L2080099-213-APR-18 13-APR-18

BH-1 BH-5

ug/L

%

%

Lab IDSample Date

Sample ID



<2.0 <2.0

81.0 80.0

111.4 82.6

HSED


L2080099 CONT’D....

13PAGE of



Semi-Volatile Organics - WATER


3,3’-Dichlorobenzidine

Di-n-butylphthalate



2

80

-

-

0.8

15

-

-

L2080099-1 L2080099-213-APR-18 13-APR-18

BH-1 BH-5

ug/L

ug/L

%

%

Lab IDSample Date

Sample ID



<0.40 <0.40

<1.0 <1.0

81.0 80.0

111.4 82.6

HSED

HSED


L2080099 CONT’D....

14PAGE of



Phenolics - WATER


Pentachlorophenol

Surrogate: 2,4,6-Tribromophenol

5

-

2

-

L2080099-1 L2080099-213-APR-18 13-APR-18

BH-1 BH-5

ug/L

%

Lab IDSample Date

Sample ID



<0.50 <0.50

76.0 86.2

HSED


L2080099 CONT’D....

15PAGE of



Polychlorinated Biphenyls - WATER


Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Total PCBs


-

-

-

-

1

-

-

-

-

-

0.4

-

L2080099-1 L2080099-213-APR-18 13-APR-18

BH-1 BH-5

ug/L

ug/L

ug/L

ug/L

ug/L

%

Lab IDSample Date

Sample ID



<0.030 <0.020

<0.030 <0.020

<0.030 <0.020

<0.030 <0.020

<0.060 <0.040

60.5 75.1

HSED

HSED

HSED

HSED

HSED


L2080099 CONT’D....

16PAGE of



Organic Parameters - WATER


Nonylphenol

Nonylphenol Diethoxylates

Total Nonylphenol Ethoxylates

Nonylphenol Monoethoxylates

20

-

200

-

1

-

10

-

L2080099-1 L2080099-213-APR-18 13-APR-18

BH-1 BH-5

ug/L

ug/L

ug/L

ug/L

Lab IDSample Date

Sample ID



<1.0 <1.0

<0.10 <0.10

<2.0 <2.0

<2.0 <2.0


HSED High sediment content in submitted water sample. Analysis could only proceed using aqueous fraction after decanting. Results may be biased low and may be inappropriate for regulatory

Qualifiers for Individual Parameters Listed:


19-APR-18 14:28 (MT)

L2080099 CONT’D....

17PAGE ofJob Reference: TT163027

20


R

BODL

DLM

DLHC

DLIS

or compliance purposes.

The ion abundance ratio(s) did not meet the acceptance criteria. Value is an estimated maximum.

Limit of Reporting for BOD was increased to account for the largest volume of sample tested.


Detection Limit Raised: Dilution required due to high concentration of test analyte(s).

Detection Limit Adjusted: Insufficient Sample

19-APR-18 14:28 (MT)

L2080099 CONT’D....

18PAGE of

625-33DCBENZIDINE-WT

625-BIS-2-PHTH-WT

625-DNB-PHTH-WT

625-PAH-LOW-WT

625-PCP-WT

BOD-WT

CN-TOT-WT

CR-CR6-IC-WT

EC-WW-MF-WT

3,3-Dichlorobenzidine


Di-n-Butyl Phthalate

EPA 8270 PAH (Low Level)

Pentachlorophenol

BOD

Cyanide, Total

Chromium +6

E. Coli

Methods Listed (if applicable):ALS Test Code Test Description

Water

Water

Water

Water

Water

Water

Water

Water

Water

SW846 8270

SW846 8270

SW846 8270

SW846 8270

SW846 8270

APHA 5210 B

ISO 14403-2

EPA 7199

SM 9222D

Method Reference** Matrix

Aqueous samples are extracted and extracts are analyzed on GC/MSD.



Aqueous samples are extracted and extracts are analyzed on GC/MSD. Depending on the analytical GC/MS column used benzo(j)fluoranthene may chromatographically co-elute with benzo(b)fluoranthene or benzo(k)fluoranthene.

This analysis is carried out using procedures adapted from APHA Method 5210B - "Biochemical Oxygen Demand (BOD)". All forms of biochemical oxygen demand (BOD) are determined by diluting and incubating a sample for a specified time period, and measuring the oxygen depletion using a dissolved oxygen meter. Dissolved BOD (SOLUBLE) is determined by filtering the sample through a glass fibre filter prior to dilution. Carbonaceous BOD (CBOD) is determined by adding a nitrification inhibitor to the diluted sample prior to incubation.

Total cyanide is determined by the combination of UV digestion and distillation. Cyanide is converted to cyanogen chloride by reacting with chloramine-T, the cyanogen chloride then reacts with a combination of barbituric acid and isonicotinic acid to form a highly colored complex.

When using this method, high levels of thiocyanate in samples can cause false positives at ~1-2% of the thiocyanate concentration. For samples with detectable cyanide analyzed by this method, ALS recommends analysis for thiocyanate to check for this potential interference

This analysis is carried out using procedures adapted from "Test Methods for Evaluating Solid Waste" SW-846, Method 7199, published by the United States Environmental Protection Agency (EPA). The procedure involves analysis for chromium (VI) by ion chromatography using diphenylcarbazide in a sulphuric acid solution. Chromium (III) is calculated as the difference between the total chromium and the chromium (VI) results.


A 100 mL volume of sample is filtered through a membrane, the membrane is placed on mFC-BCIG agar and incubated at 44.5 –0 .2 °C for 24 – 2 h. Method ID: WT-TM-1200


Reference Information19-APR-18 14:28 (MT)

L2080099 CONT’D....

19PAGE of

F-IC-N-WT

HG-T-CVAA-WT

MET-T-CCMS-WT

NP,NPE-LCMS-WT

OGG-SPEC-CALC-WT

OGG-SPEC-WT

P-T-COL-WT

PAH-EXTRA-WT

PAH-SUM-CALC-WT

PCB-WT

PH-WT

PHENOLS-4AAP-WT

Fluoride in Water by IC

Total Mercury in Water by CVAAS

Total Metals in Water by CRC ICPMS

Nonylphenols and Ethoxylates by LC/MS-MS

Speciated Oil and Grease A/V Calc

Speciated Oil and Grease-Gravimetric

Total P in Water by Colour

Sanitary Sewer Use By-Law Additional PAH

TOTAL PAH’s


pH

Phenol (4AAP)


Water

Water

Water

Water

Water

Water

Water

Water

Water

Water

Water

Water

EPA 300.1 (mod)

EPA 1631E (mod)

EPA 200.2/6020A (mod)

J. Chrom A849 (1999) p.467-482

CALCULATION

APHA 5520 B

APHA 4500-P PHOSPHORUS

SW846 8270

CALCULATION

EPA 8082

APHA 4500 H-Electrode

EPA 9066

Method Reference** Matrix

Inorganic anions are analyzed by Ion Chromatography with conductivity and/or UV detection.

Water samples undergo a cold-oxidation using bromine monochloride prior to reduction with stannous chloride, and analyzed by CVAAS.

Water samples are digested with nitric and hydrochloric acids, and analyzed by CRC ICPMS.

Method Limitation (re: Sulfur): Sulfide and volatile sulfur species may not be recovered by this method.


Water sample are filtered with direct injection and analyzed by LCMS/MS.

Sample is extracted with hexane, sample speciation into mineral and animal/vegetable fractions is achieved via silica gel separation and is then determined gravimetrically.

The procedure involves an extraction of the entire water sample with hexane. Sample speciation into mineral and animal/vegetable fractions is achieved via silica gel separation and is then determined gravimetrically.

This analysis is carried out using procedures adapted from APHA Method 4500-P "Phosphorus". Total Phosphorus is deteremined colourimetrically after persulphate digestion of the sample.

Total PAH represents the sum of all PAH analytes reported for a given sample. Note that regulatory agencies and criteria differ in their definitions of Total PAH in terms of the individual PAH analytes to be included.

PCBs are extracted from an aqueous sample at neutral pH with aliquots of dichloromethane using a modified separatory funnel technique. The extracts are analyzed by GC/MSD.

Water samples are analyzed directly by a calibrated pH meter.

Analysis conducted in accordance with the Protocol for Analytical Methods Used in the Assessment of Properties under Part XV.1 of the Environmental Protection Act (July 1, 2011). Holdtime for samples under this regulation is 28 days



GLOSSARY OF REPORT TERMS

Surrogates are compounds that are similar in behaviour to target analyte(s), but that do not normally occur in environmental samples. For applicable tests, surrogates are added to samples prior to analysis as a check on recovery. In reports that display the D.L. column, laboratory objectives for surrogates are listed there.mg/kg - milligrams per kilogram based on dry weight of samplemg/kg wwt - milligrams per kilogram based on wet weight of samplemg/kg lwt - milligrams per kilogram based on lipid-adjusted weight mg/L - unit of concentration based on volume, parts per million.< - Less than.D.L. - The reporting limit.N/A - Result not available. Refer to qualifier code and definition for explanation.


Application of guidelines is provided "as is" without warranty of any kind, either expressed or implied, including, but not limited to fitness for a particular purpose, or non-infringement. ALS assumes no responsibility for errors or omissions in the information.

19-APR-18 14:28 (MT)

L2080099 CONT’D....

20PAGE of

SOLIDS-TSS-WT

TKN-WT

VOC-ROU-HS-WT

XYLENES-SUM-CALC-WT

Suspended solids





Water

Water

Water

Water

APHA 2540 D-Gravimetric

APHA 4500-Norg D

SW846 8260

CALCULATION

Method Reference**

**ALS test methods may incorporate modifications from specified reference methods to improve performance.

Matrix

An automated method is used to distill the sample. The distillate is then buffered to pH 9.4 which reacts with 4AAP and potassium ferricyanide to form a red complex which is measured colorimetrically.

A well-mixed sample is filtered through a weighed standard glass fibre filter and the residue retained is dried in an oven at 104–1°C for a minimum of four hours or until a constant weight is achieved.

This analysis is carried out using procedures adapted from APHA Method 4500-Norg "Nitrogen (Organic)". Total Kjeldahl Nitrogen is determined by sample digestion at 380 Celsius with analysis usingan automated colorimetric method.

Aqueous samples are analyzed by headspace-GC/MS.






17-638033



Client:

Contact:

AMEC Foster Wheeler (Markham)50 Vogell Road Unit 3&4Richmond Hill ON L4B 3K6KIM GILDER

Report Date: 19-APR-18Workorder: L2080099


625-33DCBENZIDINE-WT

625-BIS-2-PHTH-WT

625-DNB-PHTH-WT

625-PAH-LOW-WT

Water

Water

Water

Water

R4016836

R4016836

R4016836

R4015829

Batch

Batch

Batch

Batch

LCS

LCSD

MB

LCS

LCSD

MB

LCS

LCSD

MB

LCS

WG2751726-2

WG2751726-3

WG2751726-1

WG2751726-2

WG2751726-3

WG2751726-1

WG2751726-2

WG2751726-3

WG2751726-1

WG2751726-2

WG2751726-2

WG2751726-2

WG2751726-2








Surrogate: 2-fluorobiphenyl


Di-n-butylphthalate

Di-n-butylphthalate

Di-n-butylphthalate



Acenaphthene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene


Benzo(ghi)perylene

59.4

63.9

<0.40

113.0

115.5

105.7

<2.0

89.2

113.0

109.2

108.3

<1.0

89.2

113.0

98.1

100.7

104.0

98.1

97.1

88.2

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

7.3

8.8

0.8

50

50

50

50-140

50-140

50-150

50-140

50-140

50-140

60-130

50-140

50-140

%

%

ug/L

%

%

%

ug/L

%

%

%

%

ug/L

%

%

%

%

%

%

%

%

59.4

115.5

109.2

0.4

40-130

2

40-130

40-130

1

40-130

40-130

13


Client:

Contact:




625-PAH-LOW-WT Water

R4015829BatchLCS

LCSD

MB

WG2751726-2

WG2751726-3

WG2751726-1

WG2751726-2


Chrysene


Fluoranthene

Fluorene


Naphthalene

Perylene

Phenanthrene

Pyrene

Acenaphthene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene


Benzo(ghi)perylene


Chrysene


Fluoranthene

Fluorene


Naphthalene

Perylene

Phenanthrene

Pyrene

Acenaphthene

Anthracene

Benzo(a)anthracene

Benzo(a)pyrene


100.2

103.3

88.9

86.8

101.1

89.8

101.7

88.8

100.2

86.8

99.1

103.0

104.5

98.7

98.6

86.2

101.3

102.8

88.2

86.8

102.8

82.6

103.7

89.3

100.6

86.5

<0.010

<0.010

<0.010

<0.010

<0.010

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

1.0

2.3

0.4

0.6

1.5

2.2

1.1

0.4

0.8

0.1

1.7

8.3

2.0

0.6

0.4

0.3

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

50-140

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

ug/L

ug/L

ug/L

ug/L

ug/L

98.1

100.7

104.0

98.1

97.1

88.2

100.2

103.3

88.9

86.8

101.1

89.8

101.7

88.8

100.2

86.8

0.01

0.01

0.01

0.01

0.01

0.01

13


Client:

Contact:




625-PAH-LOW-WT

625-PCP-WT

BOD-WT

CN-TOT-WT

Water

Water

Water

Water

R4015829

R4016836

R4016693

R4016563

Batch

Batch

Batch

Batch

MB

LCS

LCSD

MB

DUP

LCS

MB

DUP

LCS

WG2751726-1

WG2751726-2

WG2751726-3

WG2751726-1

WG2751178-2

WG2751178-3

WG2751178-1

WG2753618-3

WG2753618-2

WG2751726-2

L2079155-2

L2079981-2

Benzo(ghi)perylene


Chrysene


Fluoranthene

Fluorene


Naphthalene

Perylene

Phenanthrene

Pyrene



Pentachlorophenol

Pentachlorophenol

Pentachlorophenol

Surrogate: 2,4,6-Tribromophenol

BOD

BOD

BOD

Cyanide, Total

<0.010

<0.010

<0.010

<0.010

<0.010

<0.010

<0.010

<0.010

<0.010

<0.010

<0.010

73.7

78.3

100.2

109.8

<0.50

73.6

3.7

112.6

<2.0

0.0040

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

17-APR-18

9.2

1.6

0.2

50

20

20

50-140

85-115

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

ug/L

%

mg/L

%

mg/L

mg/L

100.2

3.8

0.0040

0.01

0.01

0.01

0.01

0.01

0.01

0.01

0.01

0.01

0.01

0.01

40-130

40-130

0.5

40-150

2

13


Client:

Contact:




CN-TOT-WT

CR-CR6-IC-WT

EC-WW-MF-WT

F-IC-N-WT

HG-T-CVAA-WT

Water

Water

Water

Water

Water

R4016563

R4015666

R4012914

R4016577

R4014547

Batch

Batch

Batch

Batch

Batch

LCS

MB

MS

DUP

LCS

MB

MS

DUP

MB

DUP

LCS

MB

MS

DUP

LCS

WG2753618-2

WG2753618-1

WG2753618-4

WG2751913-4

WG2751913-2

WG2751913-1

WG2751913-5

WG2751289-3

WG2751289-1

WG2752640-14

WG2752640-12

WG2752640-11

WG2752640-15

WG2751892-3

WG2751892-2

L2079981-2

WG2751913-3

WG2751913-3

L2080105-6

WG2752640-13

WG2752640-13

L2080005-5

Cyanide, Total

Cyanide, Total

Cyanide, Total





E. Coli

E. Coli

Fluoride (F)

Fluoride (F)

Fluoride (F)

Fluoride (F)

Mercury (Hg)-Total

86.1

<0.0020

82.7

<0.0010

107.6

<0.0010

102.1

0

0

0.127

99.2

<0.020

97.5

<0.000010

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

15-APR-18

15-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

16-APR-18

N/A

0.0

0.1

N/A

20

65

20

20

80-120

70-130

80-120

70-130

90-110

75-125

%

mg/L

%

mg/L

%

mg/L

%

CFU/100mL

CFU/100mL

mg/L

%

mg/L

%

mg/L

<0.0010

0

0.128

<0.000010

0.002

0.001

1

0.02

RPD-NA

RPD-NA

13


Client:

Contact:




HG-T-CVAA-WT

MET-T-CCMS-WT

Water

Water

R4014547

R4014387

Batch

Batch

LCS

MB

MS

DUP

LCS

WG2751892-2

WG2751892-1

WG2751892-4

WG2751704-4

WG2751704-2

L2080005-6

WG2751704-3

Mercury (Hg)-Total

Mercury (Hg)-Total

Mercury (Hg)-Total

Aluminum (Al)-Total

Antimony (Sb)-Total

Arsenic (As)-Total

Cadmium (Cd)-Total

Chromium (Cr)-Total

Cobalt (Co)-Total

Copper (Cu)-Total

Lead (Pb)-Total



Nickel (Ni)-Total

Selenium (Se)-Total

Silver (Ag)-Total

Tin (Sn)-Total

Titanium (Ti)-Total

Zinc (Zn)-Total

Aluminum (Al)-Total

Antimony (Sb)-Total

Arsenic (As)-Total

Cadmium (Cd)-Total

Chromium (Cr)-Total

Cobalt (Co)-Total

Copper (Cu)-Total

Lead (Pb)-Total


103.0

<0.000010

98.3

0.074

<0.0010

<0.0010

0.000063

<0.0050

<0.0010

<0.010

<0.00050

0.120

0.00322

<0.0050

<0.00050

<0.00050

<0.0010

0.0035

<0.030

98.3

102.8

98.5

100.2

98.3

98.5

97.7

96.9

99.7

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

8.8

N/A

N/A

12

N/A

N/A

N/A

N/A

3.0

3.5

N/A

N/A

N/A

N/A

N/A

N/A

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

20

80-120

70-130

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

80-120

%

mg/L

%

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

%

%

%

%

%

%

%

%

%

0.081

<0.0010

<0.0010

0.000071

<0.0050

<0.0010

<0.010

<0.00050

0.124

0.00311

<0.0050

<0.00050

<0.00050

<0.0010

<0.0030

<0.030

0.00001

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

13


Client:

Contact:




MET-T-CCMS-WT Water

R4014387BatchLCS

MB

MS

WG2751704-2

WG2751704-1

WG2751704-5 WG2751704-6


Nickel (Ni)-Total

Selenium (Se)-Total

Silver (Ag)-Total

Tin (Sn)-Total

Titanium (Ti)-Total

Zinc (Zn)-Total

Aluminum (Al)-Total

Antimony (Sb)-Total

Arsenic (As)-Total

Cadmium (Cd)-Total

Chromium (Cr)-Total

Cobalt (Co)-Total

Copper (Cu)-Total

Lead (Pb)-Total



Nickel (Ni)-Total

Selenium (Se)-Total

Silver (Ag)-Total

Tin (Sn)-Total

Titanium (Ti)-Total

Zinc (Zn)-Total

Aluminum (Al)-Total

Antimony (Sb)-Total

Arsenic (As)-Total

Cadmium (Cd)-Total

Chromium (Cr)-Total

Cobalt (Co)-Total

Copper (Cu)-Total

Lead (Pb)-Total


101.6

96.4

99.1

100.6

100.6

95.2

96.5

<0.0050

<0.00010

<0.00010

<0.0000050

<0.00050

<0.00010

<0.0010

<0.000050

<0.00050

<0.000050

<0.00050

<0.000050

<0.000050

<0.00010

<0.00030

<0.0030

100.3

104.1

101.0

100.6

N/A

97.8

95.5

96.2

102.9

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

80-120

80-120

80-120

80-120

80-120

80-120

80-120

70-130

70-130

70-130

70-130

-

70-130

70-130

70-130

70-130

%

%

%

%

%

%

%

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

%

%

%

%

%

%

%

%

%

MS-B

0.005

0.0001

0.0001

0.000005

0.0005

0.0001

0.001

0.00005

0.0005

0.00005

0.0005

0.00005

0.00005

0.0001

0.0003

0.003

13


Client:

Contact:




MET-T-CCMS-WT

NP,NPE-LCMS-WT

OGG-SPEC-WT

Water

Water

Water

R4014387

R4017397

R4015030

Batch

Batch

Batch

MS

DUP

LCS

MB

MS

LCS

LCSD

MB

WG2751704-5

WG2752829-3

WG2752829-2

WG2752829-1

WG2752829-4

WG2751687-2

WG2751687-3

WG2751687-1

WG2751704-6

L2080616-1

L2080616-1

WG2751687-2


Nickel (Ni)-Total

Selenium (Se)-Total

Silver (Ag)-Total

Tin (Sn)-Total

Titanium (Ti)-Total

Zinc (Zn)-Total

Nonylphenol



Nonylphenol



Nonylphenol



Nonylphenol








107.4

93.2

100.7

99.5

102.0

99.5

95.0

<1.0

<2.0

<0.10

60.0

96.5

98.0

<1.0

<2.0

<0.10

74.4

59.1

91.2

89.8

85.0

84.4

81.2

<2.0

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

N/A

N/A

N/A

6.2

4.6

30

30

30

40

40

70-130

70-130

70-130

70-130

70-130

70-130

70-130

75-125

75-125

75-125

50-150

50-150

50-150

70-130

70-130

%

%

%

%

%

%

%

ug/L

ug/L

ug/L

%

%

%

ug/L

ug/L

ug/L

%

%

%

%

%

%

%

mg/L

LCS-L

<1.0

<2.0

<0.10

89.8

85.0

1

2

0.1

2

RPD-NA

RPD-NA

RPD-NA

13


Client:

Contact:




OGG-SPEC-WT

P-T-COL-WT

PAH-EXTRA-WT

Water

Water

Water

R4015030

R4016267

R4015906

Batch

Batch

Batch

MB

DUP

LCS

MB

MS

LCS

LCSD

MB

WG2751687-1

WG2753164-3

WG2753164-2

WG2753164-1

WG2753164-4

WG2751726-2

WG2751726-3

WG2751726-1

L2080596-1

L2080596-1

WG2751726-2


Phosphorus, Total

Phosphorus, Total

Phosphorus, Total

Phosphorus, Total

Benzo(e)pyrene

1,3-Dinitropyrene

1,6-Dinitropyrene

Dibenz(a,h)acridine

1,8-Dinitropyrene

Dibenz(a,j)acridine


Dibenzo(a,i)pyrene

Benzo(e)pyrene

1,3-Dinitropyrene

1,6-Dinitropyrene

Dibenz(a,h)acridine

1,8-Dinitropyrene

Dibenz(a,j)acridine


Dibenzo(a,i)pyrene

Benzo(e)pyrene

1,3-Dinitropyrene

<1.0

0.0588

96.6

<0.0030

97.5

88.7

58.3

62.2

136.9

50.6

91.5

126.6

92.8

87.3

56.4

60.4

134.0

48.7

97.4

121.0

88.6

<0.050

<1.0

16-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

1.6

1.6

3.4

3.1

2.2

3.7

6.3

4.5

4.7

20

50

50

50

50

50

50

50

50

80-120

70-130

50-150

50-150

50-150

50-150

50-150

50-150

50-150

50-150

mg/L

mg/L

%

mg/L

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

ug/L

ug/L

0.0579

88.7

58.3

62.2

136.9

50.6

91.5

126.6

92.8

1

0.003

0.05

1

13


Client:

Contact:




PAH-EXTRA-WT

PCB-WT

PH-WT

PHENOLS-4AAP-WT

Water

Water

Water

Water

R4015906

R4016493

R4012327

Batch

Batch

Batch

MB

LCS

LCSD

MB

DUP

LCS

WG2751726-1

WG2752164-2

WG2752164-3

WG2752164-1

WG2751317-3

WG2751317-1

WG2752164-2

WG2751317-2

1,6-Dinitropyrene

Dibenz(a,h)acridine

1,8-Dinitropyrene

Dibenz(a,j)acridine


Dibenzo(a,i)pyrene


Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260


pH

pH

<1.0

<0.050

<1.0

<0.050

<0.050

<0.050

92.5

75.8

88.1

74.2

85.1

77.4

88.1

78.6

98.1

<0.020

<0.020

<0.020

<0.020

67.2

7.16

6.98

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

18-APR-18

14-APR-18

14-APR-18

2.1

0.0

5.8

14

0.04

50

50

50

50

0.2

65-130

65-130

65-130

65-130

6.9-7.1

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

%

%

%

%

%

ug/L

ug/L

ug/L

ug/L

%

pH units

pH units

75.8

88.1

74.2

85.1

7.20

1

0.05

1

0.05

0.05

0.05

40-130

0.02

0.02

0.02

0.02

50-150

J

13


Client:

Contact:




PHENOLS-4AAP-WT

SOLIDS-TSS-WT

TKN-WT

VOC-ROU-HS-WT

Water

Water

Water

Water

R4015713

R4016316

R4014897

R4015576

Batch

Batch

Batch

Batch

DUP

LCS

MB

MS

DUP

LCS

MB

DUP

LCS

MB

MS

DUP

WG2752055-11

WG2752055-10

WG2752055-9

WG2752055-12

WG2752448-3

WG2752448-2

WG2752448-1

WG2751895-3

WG2751895-2

WG2751895-1

WG2751895-4

WG2750133-4

L2079879-1

L2079879-1

L2079504-4

L2079638-1

L2079638-1

WG2750133-3

Phenols (4AAP)

Phenols (4AAP)

Phenols (4AAP)

Phenols (4AAP)









1,2-Dichlorobenzene

1,4-Dichlorobenzene

Benzene

Chloroform


Dichloromethane

0.0054

110.6

<0.0010

105.2

2550

98.2

<2.0

0.19

99.0

<0.15

104.7

<0.50

<0.50

<0.50

210

<1.0

<0.50

<5.0

16-APR-18

16-APR-18

16-APR-18

16-APR-18

18-APR-18

18-APR-18

18-APR-18

16-APR-18

16-APR-18

16-APR-18

16-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

7.8

8.1

N/A

N/A

N/A

N/A

2.0

N/A

N/A

N/A

20

20

20

30

30

30

30

30

30

30

85-115

75-125

85-115

75-125

70-130

mg/L

%

mg/L

%

mg/L

%

mg/L

mg/L

%

mg/L

%

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

0.0058

2760

<0.15

<0.50

<0.50

<0.50

214

<1.0

<0.50

<6.0

0.001

2

0.15

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

RPD-NA

13


Client:

Contact:




VOC-ROU-HS-WT Water

R4015576BatchDUP

LCS

MB

WG2750133-4

WG2750133-1

WG2750133-2

WG2750133-3Ethylbenzene

m+p-Xylenes

o-Xylene

Tetrachloroethylene

Toluene


Trichloroethylene


1,2-Dichlorobenzene

1,4-Dichlorobenzene

Benzene

Chloroform


Dichloromethane

Ethylbenzene

m+p-Xylenes

o-Xylene

Tetrachloroethylene

Toluene


Trichloroethylene


1,2-Dichlorobenzene

1,4-Dichlorobenzene

Benzene

Chloroform


Dichloromethane

Ethylbenzene

m+p-Xylenes

o-Xylene

Tetrachloroethylene

136

11.6

2.43

<0.50

18.7

<0.50

<0.50

106.6

105.9

116.6

109.4

110.0

107.1

112.0

99.7

102.0

95.4

96.2

102.4

109.9

101.8

<0.50

<0.50

<0.50

<0.50

<1.0

<0.50

<2.0

<0.50

<1.0

<0.50

<0.50

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

1.9

1.2

0.4

N/A

2.1

N/A

N/A

30

30

30

30

30

30

30

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

70-130

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%

%

%

%

%

%

%

%

%

%

%

%

%

%

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

139

11.7

2.44

<0.50

19.0

<0.50

<0.50

0.5

0.5

0.5

0.5

1

0.5

2

0.5

1

0.5

0.5

RPD-NA

RPD-NA

RPD-NA

13


Client:

Contact:




VOC-ROU-HS-WT Water

R4015576BatchMB

MS

WG2750133-2

WG2750133-5 WG2750133-3

Toluene


Trichloroethylene




1,2-Dichlorobenzene

1,4-Dichlorobenzene

Benzene

Chloroform


Dichloromethane

Ethylbenzene

m+p-Xylenes

o-Xylene

Tetrachloroethylene

Toluene


Trichloroethylene

<0.50

<0.50

<0.50

97.2

90.3

102.3

105.6

108.9

N/A

95.6

94.2

119.8

N/A

101.1

98.6

94.0

102.3

100.4

88.2

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

17-APR-18

50-150

50-150

50-150

-

50-150

50-150

50-150

-

50-150

50-150

50-150

50-150

50-150

50-150

ug/L

ug/L

ug/L

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

%

MS-B

MS-B

0.5

0.5

0.5

70-130

70-130

13


Page 13 of




J

LCS-L

MS-B

RPD-NA


Lab Control Sample recovery was below ALS DQO. Reference Material and/or Matrix Spike results were acceptable. Non-detected sample results are considered reliable. Other results, if reported, have been qualified.Matrix Spike recovery could not be accurately calculated due to high analyte background in sample.

Relative Percent Difference Not Available due to result(s) being less than detection limit.


Legend:






Client:

Contact:


13

APPENDIX C

WATER WELL RECORD SEARCH RESULTS

Appendix C: Water Well Record Search Results within 500 mTT163027 - West Don STS

WELL_ID DATE COMPLETED FINAL STATUS PRIMARY USE6928905 2005-03-28 Observation Wells #N/A7282457 2017-01-07 Test Hole Test Hole7281554 2016-08-11 Observation Wells Monitoring6905023 1955-08-15 Water Supply Irrigation7169974 2011-08-12 Test Hole Test Hole6905216 1930-11-01 Abandoned-Supply #N/A6905091 1955-10-18 Water Supply Irrigation7188672 2012-04-19 #N/A #N/A7261486 2016-02-16 Observation Wells Monitoring7173302 2011-11-20 Abandoned-Other Monitoring7182697 2012-04-18 Observation Wells #N/A7207326 2013-03-27 #N/A #N/A7241378 2015-04-21 Abandoned-Other #N/A7182696 2012-04-27 Observation Wells Monitoring and Test Hole7274930 Observation Wells Other7135521 2009-11-20 Abandoned-Other #N/A7224951 2014-06-20 Observation Wells Monitoring7246544 2015-07-06 Observation Wells Monitoring7173301 2011-11-10 Abandoned-Other Monitoring7135515 2009-11-20 Abandoned-Other #N/A7147068 2010-05-13 Abandoned-Other #N/A7271384 2015-04-17 #N/A #N/A7250788 2015-06-29 #N/A #N/A7236212 2014-09-30 #N/A #N/A7259686 2016-01-12 #N/A #N/A7241111 2015-04-22 #N/A #N/A7200790 2013-04-19 Observation Wells Monitoring7261485 2016-02-16 Observation Wells Monitoring7284162 2017-02-01 Test Hole Test Hole6928733 2004-09-17 Test Hole Not Used7261487 2016-02-16 Observation Wells Monitoring7245193 2015-05-11 Monitoring and Test Hole Monitoring and Test Hole7246545 2015-07-06 Observation Wells Monitoring7246542 2015-07-06 Observation Wells Monitoring7246543 2015-07-06 Observation Wells #N/A

APPENDIX D

REPORT LIMITATIONS

Limitations

1. The work performed in the preparation of this report and the conclusions presented are subject to the

following:

(a) The Standard Terms and Conditions which form a part of our Professional Services Contract;

(b) The Scope of Services;

(c) Time and Budgetary limitations as described in our Contract; and

(d) The Limitations stated herein.

2. No other warranties or representations, either expressed or implied, are made as to the professional services

provided under the terms of our Contract, or the conclusions presented.

3. The conclusions presented in this report were based, in part, on visual observations of the site and attendant

structures. Our conclusions cannot and are not extended to include those portions of the site or structures

which were not reasonably available, in Wood’s opinion, for direct observation.

4. The environmental conditions at the site were assessed, within the limitations set out above, having due

regard for applicable environmental regulations as of the date of the inspection. A review of compliance by

past owners or occupants of the site with any applicable local, provincial or federal by-laws, orders-in-

council, legislative enactments and regulations was not performed.

5. The site history research included obtaining information from third parties and employees or agents of the

owner. No attempt has been made to verify the accuracy of any information provided, unless specifically

noted in our report.

6. Where testing was performed, it was carried out in accordance with the terms of our contract providing for

testing. Other substances, or different quantities of substances testing for, may be present on site and may

be revealed by different of other testing not provided for in our contract.

7. Because of the limitations referred to above, different environmental conditions from those stated in our

report may exist. Should such different conditions be encountered, Wood must be notified in order that it

may determine if modifications to the conclusions in the report are necessary.

8. The utilization of Wood’s services during the implementation of any remedial measures will allow Wood to

observe compliance with the conclusions and recommendations contained in the report. Wood’s

involvement will also allow for changes to be made as necessary to suit field conditions as they are

encountered.

9. This report is for the sole use of the party to whom it is addressed unless expressly stated otherwise in the

report or contract. Any use which any third party makes of the report, in whole or in part, or any reliance

thereon, or decisions made based on any information of conclusions in the report, is the sole responsibility

of such third party. Wood accepts no responsibility whatsoever for damages or loss of any nature or kind

suffered by any such third party as a result of actions taken or not taken or decisions made in reliance on the

report or anything set out therein.

10. This report is not to be given over to any third party for any purpose whatsoever without the written

permission of Wood.

11. Provided that the report is still reliable, and less than 12 months old, Wood will issue a third-party reliance

letter to parties client identifies in writing, upon payment of the then current fee for such letters. All third

parties relying on Wood’s report, by such reliance agree to be bound by our proposal and Wood’s standard

reliance letter. Wood’s standard reliance letter indicates that in no event shall Wood be liable for any

damages, howsoever arising, relating to third-party reliance on Wood’s report. No reliance by any party is

permitted without such agreement.

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