wmi monthly progress report (cover letter included)
TRANSCRIPT
1 (05V —30Waste Management of North America. Inc.Midwet.' Rtn-onTwo Westsro?!.' Corpci^te Cri*er • Suite 1000P.O. Be" 7 C 7 j
7c^^9c?: " """1 January 7, 1991Mr. Jae Lee, Remedial Project ManagerRemedial Enforcement and Response BranchMI/WI Section, 5HR-11U.S. Environmental Protection Agency, Region V230 S. Dearborn StreetChicago, Illinois 60604
Ms. Terry EvansonRemedial Project Coordinator Hagen Farm SiteWisconsin Department of Natural ResourcesP. O. Box 7921Madison, Wisconsin 53707-7921
RE: HAGEN FARM SITEMONTHLY PROGRESS REPORT FOR DECEMBER 1990.
Dear Mr. Lee and Ms. Evanson:
In accordance with Section IX, paragraph E of the Hagen Farm AdministrativeOrder by Consent, please find attached three (3) copies of the monthly progressreport for December 1990.
Please contact me if you have any questions.
Sincerely,
Dee BrncichRemedial Projects ManagerWaste Management of North America
DBrjsattachment
cc: Gerard Hamblin-WMNA (report only)Greg Asbury-Warzyn (report only)Timothy C. Wright-The Jesup Group (report only)Rich O'Hara-WMNA-EMD (report only)Ann Straw-WMNA-Legal (report only)Bill Schubert-WMNA (report only)Oliver J. Janney-The Jesup Group, Inc. (report only)Rich Kogler-WMWI (report only)Don Otter-WMWI (report only)Jane LeCapitaine-WMWI (report only)files (8.0 w/attachment, 2.1, 2.3 w/o attachment)
MONTHLY STATUS REPORTDECEMBER 1990
SITE NAME/ACTIVITY:Hagen FarmStoughton, WisconsinRemedial Investigation/Feasibility Study
PREPARED BY:Dee BrncichWaste Management of North AmericaTwo Westbrook Corporate CenterP. O. Box 7070Westchester, IL. 60153
Greg E. AsburyWarzyn Engineering, Inc.One Science CourtMadison, Wisconsin 53705
DATE:January 7,1991
PERIOD:December 1990
PROGRESS MADE THIS REPORTING PERIOD:
During December 1990 the following project activities were conducted:
The groundwater pump test was initiated on Thursday, December 13,1990 and immediately terminated due to the use of PVC glue in the pipejoints connecting the carbon units together.
The groundwater pump test was re-initiated at 12:451 p.m. on December14, 1990 following completion of replumbing activities.
The groundwater pump test was performed for approximately 32 hoursand then permanently terminated at 10:05 p.m. on December 15, 1990due to the apparent breakthrough of the largest carbon column availableat the site.
Drilling activities continued on the downgradient plume characterizationsoil borings.
The Monthly Agency Status Report for November was submitted for^ Agency review.
DATA TRANSMITTED WITH REPORT:
Pumping Test-water quality results (does not include results formanganese, and TCL semi-volatiles at 25.0 hours [See Table 3-WorkPlan Addendum]). RAW data submitted with full report to follow.
Contaminant Characterization Investigation-water quality results (doesnot include results from borings TB-5 or TB-6).
ANTICIPATED PROBLEMS AND RECOMMENDED SOLUTIONS:None
DOCUMENTS SUBMITTED:
None
UPCOMING ACTIVITIES PLANNED:
Complete downgradient soil borings to characterize groundwater qualityat distance and depth.
Summarize the results of the groundwater pump testing.
PERSONNEL CHANGES:
None
TRAVEL MEETINGS:
None
CONTRACT LABORATORY:
Round 4 groundwater monitoring well survey will be conducted at thecompletion of the current field construction program.
SCHEDULE:Attached is a project schedule listing for near-term activities showingthe current breakdown of anticipated dates.
HAGENFAKMRI/FSNEAR-TERM SCHEDULE
January February ' March
3.23
33
Activity
Hydrogeologic Investigation WaterLevels
Contaminant Characterization
Evaluate Pump Test DataTVfiatflhflifv AnfllvsiR
1 2 3 4 1 2 3 4 1 2 3 4X
^ Sofl Boring Construction
Field Sample Analysis/Interpretation
EPA/WDNR Concurrence
Monitoring Well Construction
Round 4 Sampling
* Indicates a non-schedulable activity
Pagel
Explanation of Sample DescriptionsFor the Pumping Test Water Quahty Results
Sample Description
HF-RW1
Step Test After 15000 #CU
HF-PTBT-3.5Q
HF-PTOT-0.1
HF-PTBT-1.0
HF-PTBT-5.N
HF-PTBT-5NDUP
HF-PTBT-5FB
HF-PTBT-10N
HF-PTA15-25Q&N
Explanation
Hagen Farm-recovery well (BeforePumping Test)
Sample taken from effluent of 15000 Ibcarbon unit
Hagen Farm-Pumping Test-BeforeTreatment-3.5 hours from start of test
Hagen Farm-Pumping Test-BeforeTreatment 0.1 hours from start of test
Hagen Farm-Pumping Test-BeforeTreatment 1.0 hours from start of test
Hagen Farm-Pumping Test-BeforeTreatment 5.0 hours from start of test
Hagen Farm-Pumping Test-BeforeTreatment Field Blank taken 5.0 hoursfrom start of test - duplicate sample
Hagen Farm-Pumping Test-beforeTreatment Field blank taken 5.0 hoursfrom start of testHagen Farm-Pumping Test-beforeTreatment-10.0 hours from start of test
Hagen Farm-Pumping Test-After 15,000 Ib.carbon units-25.0 hours from start of test
HF-PTA2-25Q&N Hagen Farm-Pumping Test-After 2,000 Ib.carbon units - 25.0 hours from start of test
Page 2
Sample Description
HF-PTBT-32.5
HF-PTBA15-32.5
HF-PTA2-32.5
HF-PTA2-32.5DUP
Explanation
Hagen Farm-Pumping Test-BeforeTreatment-32^ hours from start of test(immediately prior to termination of test)
Hagen Farm-Pumping Test-After 15,000 Ib.carbon unit-32^ hours from start of test(immediately prior to termination of test).
Hagen Farm-Pumping Test-After 2,000 Ib.carbon units-32.5 hours from start of test(immediately prior to termination of test).
Hagen Farm-Pumping Test-After 2,000 Ib.carbon units-32.5 hours from start of test(immediately prior to termination of test) -Duplicate,
TK/mpb[mpb-112-76]13452.80-MD
MADISONONE SCIENCE COURT
P.O. BOX 5385MADBON. Wl 5370$
mRZYN FAX (606) 23 1-4777
ANALYTICAL LABORATORY RESULTSWI LAB CERTIFICATION IDS: 113138300
Project: Hagen Farms
Location: Town of Dunkirk, Wisconsin
Project #: 13452.85Date Sampled: 11/30/90Ck'dijuJ App'd:Date Issued: lf/*«/?o
Lab No.Sample Description
ArsenicBariumCadmiumChromium, TotalIronLeadMagnesium \Mercury
2033-001HF-RW1
0.0740.46<0.0002<0.000225.2<0.00350.7<0.0002
Results are reported in mg/L. .
Method Reference: EPA-600, "Methods for Chemical Analysis of Water andWastes", March, 1984.
MADISONONE SCIENCE COURT
P.O. BOX 5585MADISON. Wl 53705
FAX <fiC8) 23 1-4777
ANALYTICAL LABORATORY RESULTSWI LAB CERTIFICATION ID#: 113138300
Project: Hagen Farms
Location: Town of Dunkirk, Wisconsin
Project I: 13452.85Date Sampled: 11/30/90Ck'd:jw App'd:Date Issued:
Lab No.Sample Description
Alkalinity, BicarbonateAlkalinity, TotalBiochemical Oxygen DemandChemical Oxygen DemandConductivity 0 25-C (umhos/cm)Nitrogen, Nitrate+NitritePhosphorus, TotalSolids, Total DissolvedSolids, Total Suspended
2023-001HF-RW1
6276272787
1140<0.10 (1)0.24
64742
Results are reported in mg/L unless otherwise stated.
(1) Elevated detection limit necessary to overcome interference.
Method Reference: EPA-600, "Methods for Chemical Analysis of Water andWastes", March, 1984.
mRZYN
MADISONONE SCIENCE COURT
P.O. BOX 5385MAD (SON. Wl 557«
(608) W-4W7FAX C606) 23M777
ANALYTICAL LABORATORY RESULTSWI LAB CERTIFICATION IDS: 113138300
Project: Hagen Farms
Location: Town of Dunkirk, Wisconsin
Project I: 13452.85Date Sampled: 11/30/90Ck'd: jfiiXAppDate Issued:
Lab No.Sample Description
Total Organic Carbon
2023-001HF-RW1
18
Results are reported in mg/L.
Method Reference: EPA-600, "Methods for Chemical Analysis of Water andWastes", March, 1984.
Method 415.1: Total Organic Carbon
IBSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO
Lab Name: COMPUCHEM.RTP__________
Lab Code: COMPU Case No.: 22001
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
% Moisture: not dec. ___ dec. ___
Extraction: (SepF/Cont/Sonc) SEPF
GPC Cleanup: (Y/N) E_
Contract: 248901
SAS No.: _ _____
HF-RW1
SDG No.:
Lab Sample ID: 385139____
Lab File ID: GH085139A06
Date Received: 12/01/90
Date Extracted: 12/03/90
Date Analyzed: 3-2/10/90
Dilution Factor: 1.0____
CAS NO. COMPOUND'CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L
108-95-2——————Phenol_________________111-44-4——————bis (2-Chloroethyl) Ether___95-57-8———————2-Chlorophe'nol ________541-73-1—————l;3-Dichlorobenzene______106-46-7—————1,4-Dichlorobenzene______100-51-6——————Benzyl Alcohol___________95-50-1———————1,2-Dichlorobenzene______95-48-7———————2-Methylphenol__________39638-32-9————bis(2-Chloroisopropyl)Ether106-44-5——————4-Methylphenol___________621-64-7——————N-Nitroso-Di-n-Propylamine__67-72-1——————Hexachloroethane_____'98-95-3———————Nitrobenzene____________78-59-1———————Isophorone____________•_88-75-5————————2-Nitrophenol____________105-67-9—————2,4-Dimethylphenol______65-85-0——————Benzoic Acid___________111-91-1——————bis(2-Chloroethoxy)Methane__120-83-2—————2,4-Dichlorophenol______120-82-1——————1,2,4-Trichlorobenzene____91-20-3———————Naphthalene______:______106-47-8—————4-Chloroaniline_________87-68-3———————Hexachlorobutadiene______59-50-7———————4-Chloro-3-Methylphenol___91-57-6———————2-Methylnaphthalene______77-47-4———————Hexachlorocyclopentadiene__88-06-2———————2,4,'6-Trichlorophenol_____95-95-4————————2,4,5-Trichlorophenol_____91-58-7———————2-Chloronaphthalene______88-74-4———————2-Nitroaniline__________131-11^-3——————Dimethyl Phthalate_______208-96-8——————Acenaphthylene___________606-20-2——————2,6-Dinitrotoluene_______
102010103101010101010101010103
1001010103101010101020201010101010
FORM I SV-1 1/87 Rev.
1CSEMIVOIATILE ORGANICS ANALYSIS DATA SHEET
Name: COMPUCHEM,RTP__________
EPA SAMPLE NO,
Code: COMPU Case No.: 22001
tetrix: (soil/water) WATER
Sample wt/vol: .000 (g/mL) ML
**evel: (low/med) LOW
t Moisture: not dec. ___ dec. ___
Sxtraction: (SepF/Cont/Sonc) ?EPF
5PC Cleanup: (Y/N) H_ pH: ___
Contract: 248901
SAS No.: _____
HF-RW1
SDG No.:
Lab Sample ID: 385139____
Lab File ID: GH085139A06
Date Received: 12701/90
Date Extracted: 12/03/90
Date Analyzed: 12/10/90
Dilution Factor: 1.0____
CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L
99-09-2———————3-Nitroaniline_________83-32-9——————Acenaphthene___________51-28-5——————2,4-Dinitrophenol______100-02-7——————4-Nitrophenol__________132-64-9——————Dibenzofuran___________121-14-2——————2,4-Dinitrotoluene______84-66-2———————Diethylphthalate________7005-72-3—————4-Chlorophenyl-phenylether_86-73-7———————Fluorene______________"100-01-6—————4-Nitroaniline_________534-52-1——————4,6-Dinitro-2-Methylphenol_86-30-6——————N-Nitrosodiphenylamine (1),101-55-3—————4-Bromophenyl-phenylether_118-74-1——————Hexachlorobenzene_______87-86-5———————Pentachlorophenol_______85-01-8———————Phenanthrene___________120-12-7——————Anthracene_____________84-74-2———————Di-n-Butylphthalate_____206-44-0—————Fluoranthene__________129-00-0—————Pyrene_______________85-68-7———————Butylbenzylphthalate_____91-94-1——————3,3' -Dichlorobenzidine___56-55-3——————Benzo (a) Anthracene______218-01-9——————Chrysene_______________117-81-7——————bis (2-Ethylhexyl) Phthalate117-84-0——————Di^n-Octyl Phthalate____'_205-99-2——————Benzo'(b) Fluoranthene_____207-08-9——————Benzo(k)Fluoranthene_____50-32-8———————Benzo (a) Pyrene__________193-39-5——————Indeno (l, 2,3-cd) Pyrene___53-70-3———————Dibenz(a,h)Anthracene____191-24-2——————Benzo (g ,h, i) Perylene_____
2010401010101010101030101010201010101010101010101010101010101010
(1) - Cannot be separated from Diphenylamine
FORM I SV-2 1/87 Rev
SUMMARY OF ORGANIC QUALIFIER DEFINITIONS
Laboratory Qualifiers
U Tne_mater1al was analyzed for, but not detected.
J Indicates an estimated value. This flag 1s used either whenestimating a concentration for tentatively Identified compounds wherea 1:1 response 1s assumed, or when the quality control criteria arenot met.
B This flag 1s used when the analyte 1s found In the associated blank aswell as 1n the sample. It Indicates possible blank contamination andwarns the data user to take appropriate action. This flag must beused for a tentatively Identified compound as well as for a positivelyIdentified target compound.
C (For Pest1c1de/PCB data). The associated value was confirmed usingdual column verification.
E The compound was quantItated above the linear calibration range.
D The compound was quant Itated from an analysis at a secondary dilutionfactor.
X The associated value was quant Itated manually.
I The tentatively Identified compound Is an 1somer1c-type of thecompound reported.
C The tentatively identified compound refers to a class of compounds,
A The tentatively identified compound Is an aldol-type compound.
Data Validation Qualifiers
U The material was analyzed for, but was not detected. The associatednumerical value 1s the sample quantltatlon limit.
UJ The material was analyzed for, but was not detected. The associatednumerical value 1s an estimated quantity because quality controlcriteria were not met.
0 The associated numerical value 1s an estimated quantity.
R The data are unusable (compound may or may not be present).Resampling"and/or reanalysis 1s necessary for verification.
[jlv-601-11]
SUMMARY OF INORGANIC QUALIFIER DEFINITIONS
Laboratory Qualifiers
U The*material was analyzed for, but was not detected.
K The associated value was greater than or equal to the Instrumentdetection limit, but less than the contract required detection limit.
E Indicates the value reported 1s estimated due to the presence of anInterference.
M Duplicate Injection precision for furnace analyses was not met.
* Duplicate analysis 1s not within control limits.
+ Correlation coefficient for the MSA Is less than 0.995.
S The associated value was determined by the method of standardadditions.
N Indicates the spike sample recovery Is not within control limits.
W Post-digestion spike for Furnace AA analysis 1s out of control limits(85-115X), while sample absorbance Is less than 50X of the spikeabsorbance.
Data Validation Qualifiers
U The material was analyzed for, but was not detected above the level ofthe associated value. The associated value 1s either the samplequantltatlon limit or the sample detection limit.
UJ Sample was analyzed, but not detected. The associated value 1s anestimated quantity because quality control criteria were not met.
R The data are unusable (compound may or may not be present).Resampling and/or reanalysls 1s necessary for verification.
J The associated numerical value Is an estimated quantity becausequality control criteria were not met.
[jlv-601-11]
MADISONONE SCIENCE COURT
P.O. BOX 5385MAD CON, WI 53705
FAX(608)23M777
Volatile Organic Compound ResultsWI Lab Certification IDS: 113138300Project: Hagen FarmsLocation: Town of Dunkirk, WisconsinCi: 13452.85
Page * Of %Ck*d:jwJ App'dDate
Compound
ReportableDetectionLimit(UG/L)
2024-001(1)HF-RW111/30/90
Benzene°romodichloromethaneomoform
BromomethaneCarbon TetrachlorideChlorobenzeneChlorodibromomethaneChloroethane2-Chloroethylvinyl Ether1.2-Dichlorobenzene1.3-Di chlorobenzene1.4-Di chlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroetheneci s-1,2-Di chloroethenetrans-1.2-Dichloroethene1.2-Dicnloropropanecis-l,3-Dich1oropropenetrans-1,3-Di chloropropeneV,hy1 Benzene
Siethylene Chloride1,1,2,2-Tetrachloroeth aneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenesMethyl Ethyl Ketone (MEK)Methyl Isobutyl Ketone (MIBK)TetrahydrofuranStyrene *"° ,
20020010001000200200200600500020020020020020060060060020020020020010002002002002002005000600600600
400020004000200
XXXXXXXXXXXXXXXXXXXX1250XXXXXXXXX11300
XX14100X
MADISONONE SCIENCE COURT
P.O. BOX 5385MADISON. WI 53705
C6C8) HI-4747FAXCfiC6)23M7T7
Volatile Organic Compound ResultsWI Lab Certification ID*: 113138300Project: Hagen FarmsLocation: Town of Dunkirk, WisconsinCf: 13452.85
Page Of "**Date Issued:
X * Analyzed, but not detected.(1) Sample chromatogram contains unidentified compounds.Method Reference: SW846, "Test Methods for Evaluating Solid
Waste", September, 1986. Methods 8010and 8020 with modifications. •
MADISONONE SCIENCE COURT
P.O. BOX 5385MADISON, Wl 53705
ANALYTICAL LABORATORY RESULTSWI LAB CERTIFICATION ID#: 113138300
Project: Hagen Farms Project #: 13452.85Date Sampled: 12/12/90
Location: Town of Dunkirk, Wisconsin Ck'd:<na ApDate Issued:
Lab No. 2093-001Sample Step Test AfterDescription ISOOOff CU
Arsenic 0.041Barium 0.02Cadmium <0.0002Chromium, Total 0.0005Lead <0.003Mercury <0.0002
Results are reported in ntg/L.
Method Reference: EPA-600, "Methods for Chemical Analysis of Water andWastes", March, 1984.
mRZYN
MADISONONE SCIENCE COURT
P.O. BOX 5385MADISON, VI »705
<&» 231-4747FAX (606) 231-4777
Volatile Organic Compound ResultsWI Lab Certification IDS: 113138300Project: Hagen Farm SiteLocation: Dunkirk, WisconsinC#: 13452.85
Compound
BenzeneBromodi chloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzene .ChlorodibfomomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1, 2-Di chlorobenzene1.3-Dichlorobenzene1.4-Dichlbrobenzene1.1-Dichlproethane1.2-Dichloroethane1.1-Dichloroethenecis-l,2-Dichloroethenetrans-l,2-Dichloroethene1.2-Dichloropropanecis-l,3-D1chloropropenetrans-l,3-DichloropropeneEthyl BenzeneMetnylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-TrichloroethaneTrjchloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenes -*StyreneMethyl ethyl ketoneMethyl isobutyl ketoneTetrahydrofuranX • Analyzed, but not detected.
Page » Of >Ck?d:JU^App'dDate Issued: i/3/9l
ReportableDetectionLimit(ug/D
1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.003.0010.010.010.010.0
2093-001Step TestAfter15000? CU12/13/90
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX,xXXXXX
2093-002TripBlank12/12/90
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
Method Reference: SW846, "Test Methods for Evaluating Solid Waste ,September, 1986. Methods 8010 and 8020with modifications.
IXORGANICS ANALYSIS DATA SHEET
SAMPLE NO.
Lab Name: COMPUCHEM,RTP__________
Lab Code: COMPU Case No.: 22145
Matrix: (soil/water) WATER
Sample wt/vol: 1000 (g/mL) ML
Level: (low/med) LOW
% Moisture: _____ decanted: (Y/N) N
Concentrated Extract Volume: 1000(ul)
Injection Volume: l.Ofull
G^_ Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
Contract: 248901
SAS No.: _____
2093-001
SDG No.:
Lab Sample ID: 389062____
Lab File ID: GJ089062B06
Date Received: 1-2/17/90
Date Extracted: 12/19/90
Date Analyzed: 12/21/90
Dilution Factor: 1.0____
CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L
108-95-2 ————111-44-4 ————oe:_e;"7_o__. _ __
541-73-1 ————106-46-7 ————
95-50-1 —————95-48-7 —————1QtZ.tO *>*) Q _JSoJo— J^ y— ——106-44-5 ————f ^ ^ ^ * ^621—64—7 ————o/ /^i— JL— — —yo— yo— j— — ~" — •—78-59-1 —————oo— /D— o— — • — —105-67-9 ————65-85-0 —————111-91-1 ————
01-20—3 —————^ **- «* w w
106-47-8 ————a*? /;o ^o / oo— J— — — — —59-50-7 —————91-57-6 —————^^ A » Jl.77-47-4 —————
95-95-4 —————on RO—-; — __88-74-4 —————131-11-3 ————
606-20-2 ————
—— Phenol—— bis (2-Chloroethyl) Ether—— 2-Chlorophenol
f O UJL^ll^UJtUUCilACSilC
t -» <^^^>J.lXVJ J. UUC»l4C<dlIS
—— Benzyl Alcohol—— 1 , 2-Dichlorobenzene—— 2 -Methylphenol—— bis (2-Chloroisopropyl) Ether _—— 4 -Methylphenol—— N-Nitroso-Di-n-Propylamine __—— Hexachloroethane
Al J* 1— J. UJJUildiVvAiC
—— Isophorone—— 2 -Nitrophenol—— 2 , 4-Dimethylphenol
j?uiii£iuxv nv»xu—— bis ( 2 -Chloroethoxy) Methane __—— 2 , 4-Dichlorophenol
f £ / ** Ai. ^>IlXOJtwJJ6Il£cllQ
—— Naphthalene—— 4-Chloroaniline—— Hexachlorobutadiene—— 4-Chloro-3-Methylphenol—— 2-Methylnaphthalene—— Hcxachlorocyclopentadiene—— 2 , 4 ', 6-Trichlorophenol—— 2 , 4 , 5-Trichlorophenol—— 2-Chloronaphthalene—— 2-Nitroaniline—— Dimethyl Phthalate
«ii->»-.4nj[-m <»ii_y ^uiif^—— 2 , 6-Dinitrotoluene
. 6201010101010101010101010101010
10010101010101010101020201010101010
Juuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu
FORM I X-l 3/90
99-09-2———————3-Nitroaniline83-32-9———————Acenaphthene51-28-5———————2,4-Dinitrophenol100-02-7———'——4-Nitrophenol132-64-9——————Dibenzofuran121-14-2——————2,4-Dinitrotoluene84-66-2———————Diethylphthalate7005-72-3—————4-Chlorophenyl-phenylether86-73-7———'————Fluorene100-01-6——————4-Nitroaniline534-52-1——————4,6-Dinitro-2-Methylphenol86-30-6———————N-Nitrosodiphenylamine (1)101-55-3——————4-Bromophenyl-phenylether118-74-1——————Hexachlorobenzene87-86-5———————Pentachlorophenol85-01-8———————Phenanthrene120-12-7——————Anthracene84-74-2———————Di-n-Butylphthalate206-44-0——————Fluoranthene129-00-0——————Pyrene85-68-7———————Butylbenzylphthalate91-94-1———————3,3'-Dichlorobenzidine56-55-3———————Benzo( a) Anthracene218-01-9——————Chrysene117-81-7——————bis (2-Ethylhexyl) Phthalate117-84-0——————Di-n-Octyl Phthalate205-99-2——————Benzo(b) Fluoranthene207-08-9——————Benzo (k) Fluoranthene50-32-8———————Benzo (a) Pyrene193-39-5——————Indeno (1,2,3-cd) Pyrene53-70-3———————Dibenz(a,h)Anthracene191-24-2——————Benzo(g,h,i)Perylene
20104010101010101010301010-10 '201010101010101010101010io1010101010
uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu
FORM I X-2 3/90
METHOD REFERENCE
To determine the concentration of Semi-Volatile organic compounds in aqueousmatrix CompuChem employs the methods as outlined in SW-846 for sample preparation(Method 3S10) and analysis (Method 8270). These methods are approved forobtaining data to satisfy the requirement of 40CFR part 261, Identification andListing of Hazardous Waste.
METHOD SUMMARY
Surrogates are added to an aliquot (usually 1-liter) of aqueous sample. The sampleIs extracted at a pH of greater than 11 and then at a pH of less than 2 using aseparatory funnel. The solvent used is methylene chloride. The extracts are driedand concentrated for analysis.
Analysis is performed by separation of the components by gas chromatographyfollowed by qualitative and quantitative identification by mass spectrometry usinginternal standard technique.
MADISONONE SCIENCE COURT
P.O. BOX 5585MADISON. Wl 53705
(606) 23I.-4747FAX C6C6) 2JM777
Volatile Organic Compound ResultsWI Lab Certification IDS: 113138300Project: Hagen Farm RI/FSLocation: Town of Dunkirk, WisconsinC#: 13452.85
Page 1 Of *Ck?d:$WApp'dDate Issued:
Compound
ReportableDetectionLimit
2099-001(1}HF-PTBT-3.5Q12/14/90
BenzeneBromod1chloromethaneBromoformBromomethaneCarbon TetrachlorldeChlorobenzeneChlorodlbromomethaneChloroethane2-Chloroethylvlnyl EtherChloroformChloromethane1.2-D1chlorobenzene1.3-D1chlorobenzene1.4-Dlchlorobenzene1.1-D1ch1oroethane1.2-D1chloroethane1.1-D1chloroethene .cis-lt2-D1chloroethenetrans-l,2-D1chloroethene1.2-D1cnloropropanec1s-l,3-D1chloropropenetrans-l,3-D1chloropropeneEthyl BenzeneMetnylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trlchloroethane1.1.2-TrlchloroethaneTrlchloroetheneTrlchlorofluoromethaneVinyl ChlorideXylenes
1001001001001001001001001000100100100100100100100100100100100100100100500100100100100100100100100300
XXXXXXXXXXXXXXXXXXXXXX668XXXXXXXXX
8130
Tetrahydrofuran 5000 11800
mRZYN
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PageCkfd:Date Issued
(1) Sample chromatogram contains unidentified compounds.X - analyzed, but not detected.
Method reference: SW846, "Test Methods for Evaluating SolidWaste", September, 1986. Methods 8010and 8020 with modifications.
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Paqe 1 Of1*Ck d:jw App'dDate Issued:.iJ
Compound
ReportableDetectionLimit(ug/L)
2104-001HF-PTBT-0.112/14/90
BenzeneBromochloromethaneBromodi chloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethanel,2-Dibromo-3-Chloropropane1, 2-D1chlorobenzene1.3-Dichlorobenzene1.4-Di chlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroetheneci s-1,2-Di chloroethenetrans-l,2-Dichloroethene1.2-Dicnloropropaneci s-1,3-Dichioropropenetrans-l,3-Dich1oropropeneEthyl BenzeneMethylene Chloride1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trichloroethane1.1.2-Trichloroethane ;;Trichloroethene •Tri chlorof1uoromethaneVinyl ChlorideXylenesStyrene yMethyl ethyl ketone (MEK)Methyl isobutyl ketone (MIBK)Tetrahydrofuran
250250250250250•25025025025025002502505002502502502502502502502502502502502501250250250250250250250250250250750
250625025002500
XXXXXXXXXXXXXXXXXXXXXXXX958XXXXXX3CXXX
11100
XXX
14900
MADISONONE SCIENCE COURT
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Page * Of bCkfd:.*Date Issued
Compound
BenzeneBromodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodibromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-Di chlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-1,2-Dichloroethenetrans-l,2-Dichloroethene1.2-Dichloropropanecis-l,3-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trichloroethane1.1.2-TrichloroethaneTrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenesStyreneMethyl ethyl ketone (MEK)Methyl isobutyl ketone (MIBK)Tetrahydroftiran
ReportableDetectionLimit(ug/L)
SO,SO,SO,5050.50,50,50.050050.050,50,50,50.50.50.50,50.50,50,50,50.50.025050.050.050,50.50.50,50,50.01500
5001250050005000
2104-002HF-PTBT-1.012/14/90
XXXXXXXXXXXXXXXXXXXXXX
1020XXXXXXXXX
10500
XXX
14300
2104-003HF-PTBT-5.N12/14/90
XXXXXX 'XXXXXXXXXXXXXXXX778XXXXXXXXX
8220
XXX
12000
mRZYN
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Page 3 Of <•Ck*d:jw ApDate Issued
Compound
ienzeneBromodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorod i bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-Dichlorobenzene1.3-Di chlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-1,2-Dichloroethenetrans-1,2-DichloroetheneJ,2-Dichloropropanecis-l,3-Dichioropropenetrans-l,3-DichloropropeneEthyl BenzeneMetnylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1,1,1-Tri chloroethane
" 1,1,2-Tri chloroethaneTrichloroetheneTrichlorofluoromethaneVinyl ChlorideXylenesStyreneMethyl ethyl ketone (HEK)Methyl isobutyl ketone (MIBK)Tetrahydrofuran
ReportableDetectionLimit(ug/L)
50.050.050,50.50,50.50,50.050050.050,50,50.50.50,50,50,50.50,50,50,50.50.025050.050.050,50,50,50,50.50.1500
5001250050005000
2104-004HF-PTBT-10N12/14/90
X.XXXXXXXXXXXXXXXXXXXXX
683XXXXXXXXX
7450
XXX
11200
2104-005HF-PTBT-5NDUP12/14/90WKMCHKV
XXXXXXXXXXXXXXXXXXXXXX
844XXXXXXXXX
9020
XXX
12500
WJRZYN
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e i Ofd:;rvxJ
Date Issued
Compound
BenzeneBromochloromethaneBromodi chloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodibromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethanel,2-Dibromo-3-Chlorqpropane1.2-Di chlorobenzene1.3-Dichlorobenzene1,4 -Di chlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-l,2-Dichloroethenetrans-l,2-Dichlorbethene1.2-Di chloropropanecis-l,3-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMetnylene Chloride1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethanetetrachloroetheneToluene1.1.1-Trichloroethane1.1.2-Trichloroethane •'** .TrichloroetheneTrichlorofluoromethaneVinyl ChlorideXylenes
'•*StyreneMethyl ethyl ketone (MEK)Methyl isobutyl ketone (MIBK)Tetrahydrofuran
ReportableDetectionLimit
1.001.001.001.001.001.001.001.001.0010.01.001,002.001.001*001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.00.1.001.001.004.001.0025.010.010.0
2104-006HF-PTBT-5FB12/14/90
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
mRZYN
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Page f OfCk d:^»«^>Date Issued: h-J-
Compound
ReportableDetectionLimit(ug/L)
2104-007TRIPBLANK12/12/90
BenzeneBromochloromethaneBromodi chloromethaneBromoformBromomethaneCarbon Tetrachl'orideChlorobenzeneChlorodibromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethanel,2-Dibromo-3-ChToropropane1.2-01Chlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Di chloroethane1.2-Dichloroethane1.1-Dichloroethenecis-1,2-Dichloroethenetrans-l,2-Dichloroethene1.2-Dicnloropropanecis-l.S-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,1,2-Tetrachloroethane1,1,2,2-Tetrachl oroethaneTetrachloroetheneToluene1.1.1-Trichloroethane .,1.1.2-Trichloroethane "s /TrichloroetheneTrichlorofluoromethaneVinyl ChlorideXylenes
^StyreneMethyl ethyl ketorie (MEK)Methyl isobutyl ketone (MIBK)Tetrahydrofuran
1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003.00
1.0025.010.010.0
XXXX.XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
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Page t Of 6Ck'dyw*7 App'd:Date Issued:jt/z«
X - analyzed, but not detected.
Method reference: SW846. "Test Methods for Evaluating SolidWaste*, September, 1986. Methods 8010and 8020 with modifications.
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VI Lab Certification ID?: 113138300 Ck7d:^WAp|Project: Hagen Farm RI/FS Date IssuedLocation: Town of Dunkirk, WisconsinC#: 13452.85
Compound
ReportableDetectionLimit(ug/L)
2100-001 2100-002HF-PTA15 HF-PTA2-25Q -25Q12/15/90 12/15/90
BenzeneBromodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1»2-Di chlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroetheneci s-1,2-Dichloroethenetrans-l,2-Dichloroethene1.2-Dicnloropropanecis-l,3-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMetnylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneTo!uene1.1.1-Tri chloroethane1.1.2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl ChlorideXylenes
1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.003.00
XXXXXXXXXXXXXXXXXXXXXX
1.89XXXXXXXXX
12 .8
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
Tetrahydrofuran 10.0 101
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Volatile Organic .Compound Results Page *• Of3
VI Lab Certification IDS: 113138300 Ck7d:*WAp|Project: Hagen Farm RI/FS Date Issued:Location: Town of Dunkirk, WisconsinC#: 13452.85
Compound
ReportableDetectionLimit(ug/L)
2100-003HF-PTTRIPBLANK12/15/90
BromodlchloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-Dichlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-01chloroethane1.2-Dichloroethane1.1-Di chloroethenecis-1,2-Dichloroethenetrans-1.2-Dichloroethene1.2-Dichloropropanecis-l,3-Dichloropropenetrans-1,3-PichloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneTo!uene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenes
1.001.001.001.001.001.00•1.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.003.00
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
Tetrahydrofuran 10.0
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e 2> Ofd: vJ
Date Issued
X'- analyzed, but not detected.
Method reference: SW846. "Test Methods for Evaluating SolidWasteV September, 1986. Methods §010and 8020 with modifications.
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ANALYTICAL LABORATORY RESULTSWI LAB CERTIFICATION IDS: 113138300
Project: Hagen Farms
Location: Town of Dunkirk, Wisconsin
Project f: 13452.85Date Sampled: 12/15/90Ck'dr'-wj App'd:Date Issued:
Lab No.Sample Description
ArsenicBariumCadmiumChromium, TotalLeadMercury
2103-001HF-PTBT-25N
0.0510.26<0.00020.0004<0.003<0.0002
2103-002HF-PTA2-25N
0.0150.18<0.00020.0002<0.003<0.0002
Results are reported in mg/L.
Method Reference: EPA-600, "Methods for Chemical Analysis of Water andWastes", March, 1984.
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Page ' Of /Ck7d:^W App'd:Date Issued:i/3/<)l
Compound
ReportableDetectionLimit(ug/L)
2103-001HF-PTBT-25N12/15/90
BenzeneBromodi chloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-Di chlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroetheneci s-1,2-Di chloroethenetrans-l,2-Dichloroethene1.2-Dichloropropanecis-l,3-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneTo!uene1.1.1-Tri chloroethane1.1.2-TrichloroethaneTrichloroetheneTrichlorofluoromethaneVinyl ChlorideXylenesMethyl Ethyl Ketone (MEK)Methyl isobutyl Ketone (MIBK)Styrene.TetrahydrdTuran
50.050.050.050.050.050.050.050.050050.050.050.050.050.050.050.050.050.050.050.050.050.050.025050.050.050.050.050.050.050.050.01500
125050050.05000
XXXXXXXXXXXXXXXXXXXXXX449XXXXXXXXX5780
XXX7780
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Page * OfCk*d:Date Issued: i/s/<ii
Compound
ReportableDetectionLimit(ug/L)
2103-002HF-PTA2-25N12/15/90
BenzeneBromodichloromethaneBromoformBromomethaneCarbon TetrachlorldeChlorobenzeneChlorodlbromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-01chlorobenzene1.3-01chlorobenzene1.4-Di chlorobenzene1.1-Dlchloroethane1.2-Dlchloroethane1.1-01chloroetheneds-l,2-D1chl oroethenetrans-l,2-D1chloroethene1.2-Dlcnloropropanec1s-l,3-D1chloropropenetrans-l,3-D1chloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trlchloroethane1.1.2-TrlchloroethaneTrlchloroetheneTr1chlorof1uoromethaneVinyl Chloride " tXylenesMethyl Ethyl Ketone (MEK)Methyl Isobutyl Ketone (MIBK)Styrene ^Tetrahydrofuran
1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001,001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.004.00
25.010.01.0020.0
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
XXXX
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Volatile Organic Compound Results Page3 Of/WI Lab Certification IDS: 113138300 Ckrd:**/APIProject: Hagen Farm Site Date IssuedLocation: Town of Dunkirk, WisconsinC#: 13452.85
Compound
ReportableDetectionLimit
2103-003HF-PTA15-25N12/15/90
BenzeneBromodichloromethaneBromoformBromomethaneCarbon TetrachlorldeChlorobenzeneChlorodlbromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane *1.2-D1chlorobenzene1.3-Dlchlorobenzene1.4-D1chlorobenzene1.1-01chloroethane1.2-D1chloroethane1.1-D1chloroethenecis-l,2-D1chloroethenetrans-1,2-D1chloroethene1.2-D1chloropropanecis-l",3-D1chloropropenetrans-l,3-D1chloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tr1chloroethaneTrlchloroetheneTrlchlorofluoromethane.sVinyl Chloride "^ /XylenesMethyl Ethyl Ketone (MEK)Methyl Isobutyl Ketone (MIBK)Styrene ,Tetrahydrofuran
00000000
1.001.001.001.0010,01.001.001.001.001.001.00.00.00.00
1111.001.001.001.001.005.001.001.001.001.001.001.001,001,003.00
25.010.01.0050.0
XXXXXXXXXXXXXXXXXXXXXX1.37XXXXXXX
- XX13.6
XXX87.6
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Volatile Organic Compound Results Page 4 Of/VI Lab Certification ID#: 113138300 CkTd:ju*.Project: Hagen Farm Site Date IssuedLocation: Town of Dunkirk, Wisconsin«: 13452.85
Compound
BenzeneBromodi chlorometh aneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-D1chlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-l,2-Dichloroethenetrans-K2-Dichl oroethene1.2-Dicnloropropanecis-l,3-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethanetetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTrichlorof1uoromethaneVinyl Chloride -v ,,XylenesMethyl Ethyl Ketone (MEK)Methyl isobutyl Ketone (HIBK)StyreneTetrahydrofuran
ReportableDetectionLimit(ug/L)
1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.003.00
25.010.01.0010.0
2103-004TRIP BLANK12/12/90
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
WARZYN
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Volatile Organic Compound ResultsWI Lab Certification IDS: 113138300Project: Hagen Farm SiteLocation: Town of Dunkirk, WisconsinC#: 13452.85
PageCkrd:Date Issued
X - Analyzed, but not detected.
Method Reference: SW846. "Test Methods for Evaluating SolidWaste'1, September, 1986. Methods 8010and 8020 with modifications.
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Page J OfCk'd ^Date Issued:i*/
Compound
ReportableDetectionLimit(ug/L)
2117-001HF-PTBT-32 512/i5/90
BenzeneBromodi chloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-Dichlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-1,2-D1chloroethenetrans-1.2-Dichloroethene1.2-Di cnloropropanecis-l,3-Dichloropropenetrans-l,3-D1chloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenes ** ;StyreneMethyl ethyl ketone (MEK)Methyl isobutyl ketone (MIBK)Tetrahydr^furan
25025025025025025025025025002502502502502502502502502502502502502502501250250250250250250250250250750
250625025002500
XXXXXXXXXXXXXXXXXXXXXX
412XXXXXXXXX
4850
XXX
7840
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Page * OfCk*d:Date Issued
Compound
BenzeneBromodi chloromethaneBromoformBromomethaneCarbon TetrachlorldeChlorobenzeneChlorodlbromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-D1chlorobenzene1.3-D1chlorobenzene1.4-Dlchlorobenzene1.1-Dichloroethane1.2-Dichloroethaneltl-D1chloroethenewcis-l,2-Dichloroethenetrans-l;2-D1chloroethene112-Di cnloropropanecis-l,3-D1chloropropenetrans-l»3-DichloropropeneEthyl BenzeneMetnylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trlchloroethane1.1.2-TrlchloroethaneTrichloroethene
, Tr1chlorofluoromethane"~V1nyl ChlorideXylenesStyreneMethyl ethyl ketone (MEK)Methyl isobutyl ketone (MIBK)Tetrahydrofuran
ReportableDetectionLimit
1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.003.00
1.0025.010.010.0
2117-002HF-PTA15-32.512/15/90
XXXXXXXXXXXXXXXX 'XXXXXX1.45XXXXXXXXX15.7
XXX
100
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Page 3Ck*d:Date Issued
Compound
BenzeneBromodi chloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1»2-Di chlorobenzene1.3-Di chlorobenzene1.4-Dichlorobenzene1.1-D1chloroethane1.2-Dichloroethane1.1-Dichloroethenecl s-1,2-Dichloroethenetrans-1,2-D1chloroethene1.2-Dichloropropanecis-l,3-Dichloropropenetrans-1,3-DichloropropeneEthyl BenzeneMetnylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTrichlorofluoromethaneVinyl ChlorideXylenes "* ,•StyreneMethyl ethyl ketone (MEK)Methyl isobutyl ketone (MIBK)Tetrahydrofuran
ReportableDetectionLimit(ug/L)
1,001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.004.00
1.0025.010.010.0
2117-003 2117-004HF-PTA2 HF-PTA2-32.5 -32.5 DUP12/15/90 12/15/90
XXXXXXXX
•XXXXXXXXXXXXXXXXXXXXXXXXX
XXXX
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
XXXX
MADISONONE SCIENCE COURT
P.O. BOX 5585MADISON, wi 53705
<6C8) »M747FAX C6C8) »I-4777
Volatile Organic Compound ResultsWI Lab Certification ID*: 113138300Project: Hagen Farm RI/FSLocation: Town of Dunkirk, WisconsinC#: 13452.85
^ OfCk7d:aWApp'Date Issued:
Compound
BenzeneBromodi chloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-Dichlorobenzene1.3-Di chlorobenzene1.4-D1chlorobenzene1.1-Dlchloroethane1.2-D1chloroethane1.1-Dichloroethenecis-1,2-D1chloroethenetrans-1.2-Di chloroethene1.2-Dicnloropropanecls-1,3-Di chloropropenetrans-l,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trichloroethane1.1.2-Tr1chloroethaneTr'i chl oroetheneTrichlorofluoromethaneVinyl ChlorideXylenes '* •StyreneMethyl ethyl ketone (MEK)Methyl isobutyl ketone (MIBK)Tetrahydro/uran
ReportableDetectionLimit
1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.003.00
1.0025.010.010.0
2117-005TRIPBLANK12/15/90
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
MADISONONE SCIENCE COURT
P.O. BOX 5J85MADISON, wi 53705
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Volatile Organic Compound ResultsWI Lab Certification ID#: 113138300Project: Hagen Farm RI/FS Date Issued:Location: Town of Dunkirk, WisconsinCf: 13452.85
X - analyzed, but not detected.
Method reference: SW846, "Test Methods for Evaluating SolidWaste*, September, 1986. Methods 8010and 8020 with modifications.
Explanation of Sample Descriptionsfor the Contaminant Characterization Investigation
Water Quality Results
Description
HF-GWDTB01-22HF-GWDTB01-91HF-GWDTB01-37HF-GWDTB01-57HF-GWDTB01-79HF-GWDTB01-97HF-GWDTB01-117HF-GWDTB01-137
HF-GWDTB02-27HF-GWDTB02-37HF-GWDTB02-57HF-GWDTB02-74HF-GWDTB02-78HF-GWOTB02-94HF-GWDTB02-97HF-TB01HF-FB01
HF-GWOTB03-27HF-GWDTB03-47HF-GWDTB03-67HF-GWDTB03-87HF-GWOTB03-92HF-GWDTB03-107HF-GWDTB03-127HF-GWDTB03-147HF-FB02HF-FB03HF-TB02
HF-GWDTB04-47HF-GWOTB04-60HF-GWDTB04-75HF-GWDTB04-92HF-GWDTB04-104HF-GWOTB04-122HF-GWOTB04-134HF-GWDTB04-93HF-TB04
Explanation
HagenHagenHagenHagenHagenHagenHagenHagen
HagenHagenHagenHagenHagenHagenHagenHagenHagen
HagenHagenHagenHagenHagenHagenHagenHagenHagenHagenHagen
HagenHagenHagenHagenHagenHagenHagenHagenUagen
FarmFarmFarmFarmFarmFarmFarmFarm
FarmFarmFarmFarmFarmFarmFarmFarmFarm
FarmFarmFarmFarmFarmFarmFarmFarmFarmFarmFarm
FarmFarmFarmFarmFarmFarmFarmFarmFarm
- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater
- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater
.-------
-------
TestTestTestTestTestTestTestTest
TestTestTestTestTestTestTest
BoringBoringBoringBoringBoringBoringBoringBoring
BoringBoringBoringBoringBoringBoringBoring
11tlflfl11fl1111
1212121212#212
- 22- 22- 37- 57- 79- 97- 117
feetfeetfeetfeetfeetfeet
Duplicate
feet- 137 feet
- 27- 37- 57- 74- 78- 94- 97
feetfeetfeetfeetfeetfeetfeet
- Trip Blank 11- Field Blank
- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Field Blank- Field Blank
11--------
TestTestTestTestTestTestTestTest
BoringBoringBoringBoringBoringBoringBoringBoring
1313131313131313
- 27- 47- 67- 87- 87- 107- 127- 147
feetfeetfeetfeetfeetfeetfeetfeet
Duplicate
1213
- Trip Blank 12
- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater- Groundwater
--------
TestTestTestTestTestTestTestTest
BoringBoringBoringBoringBoringBoringBoringBoring
141414#414#414#4
- 47- 60- 75- 92- 104- 122- 134- 134
feetfeetfeetfeetfeetfeetfeetfeet Duplicate
- Trip Blank #4
[sss-101-98b]
WJRZYN
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PAGE 1 OF *CK'D^wJAPP'D:DATE ISSUED:*!*
COMPOUND
REPORTABLEDETECTIONLIMIT
1946-001 1946-002HF-GWDTB01-22 HF-GWDTB01-9111/12/90 11/12/90
BENZENEBROMOCHLOROMETHANEBROMODICHLOROMETHANEBROMOFORMBROMOMETHANECARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANEl,2-DIBROMO-3-CHLOROPROPANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE,1,1-DICHLOROETHANE1,2-DICHLOROETHANE1.1-DICHLOROETHENECIS-1,2-DICHLOROETHENETRANS-1.2-DICHLOROETHENE1.2-DICHLOROPROPANECIS-1,3-DICHLOROPROPENETPANS-1,3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1,2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE .,1.1.2-TRICHLOROETHANE '* .TRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENES
1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.00'1.001.001.003.00
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
BMQL
XXXXXXXXXXXXXXXXXXXXXXXXXXXX•XXXXXXX
BMQL
TETRAHYDROFURAN 20.0
mRZYN
MADISONONE SCIENCE COIKT
P.O. BOX 5J65MADISON. Wl 53705
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PAGECK'DDATE ISSUED
IMPOUND
BENZENEBROMOCHLOROMETHANEBROMODICHLOROMETHANEBROMOFORMBROMOMETHANE
. CARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DIBROMO-3-CHLOROPROPANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE
^4,1-DICHLOROETHANE1,2-DICHLOROETHANE1.1-DICHLOROETHENECIS-1,2-DICHLOROETHENETRANS-1.2-DICHLOROETHENE1.2-DICHLOROPROPANE
. CIS-1.3-DICHLOROPROPENETRANS-1,3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1,2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE .v1.1.2-TRICHLOROETHANETRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENES
REPORTABLEDETECTIONLIMIT(UG/L)
1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003.00
1946-003HF-GWDTB01-3711/12/90
TETRAHYDROFURAN 20.0
MADISONONE SCIENCE COU'XT
P.O. BOX 5365MADISON, wi 53705
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PAGE 3 OF JCK'D: APP'DDATE ISSUED:
BMQL - DETECTED, VALUE BELOW METHOD QUANTITATION LIMIT.X - ANALYZED, BUT NOT DETECTED.
,ETHOD REFERENCE: SW846, "TEST METHODS FOR EVALUATING SOLIDWASTE", SEPTEMBER, 1986. METHODS 8010AND 8020 WITH MODIFICATIONS.
WARZYN'
MADISONONE SOENCZ COCST
P.O. BOX 5185MADISON, wi 33705
<6C8> 231-4747FAXC6CB)23M777
VOLATILE ORGANIC XOMPOUND RESULTS PAGE 1 OF £WI LAB CERTIFICATION IDS: 113138300 CK'D:*wJAPIPROJECT: HAGEN FARM RIFS DATE ISSUED:LOCATION: STOUGHTON, WISCONSINC#: 13452.89
•OMPOUNO
REPORTABLEDETECTIONLIMIT(UG/L)
1952-001HF-GWDTB01-5711/13/90
BENZENEBROHOCHLOROHETHANEBROHODICHLOROMETHANEBROMOFORM -BROHOMETHANE .CARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DIBROMO-3-CHLOROPROPANE1.2-DICHLOROBENZENE1.3-DICHLORQBENZENE1.4-DICHLOROBENZENE
v >,1-DICHLOROETHANEM.2-DICHLOROETHANE
1.1-DICHLOROETHENECIS-1,2-DICHLOROETHENETRANS-1,2-DICHLOROETHENE1.2-DICHLOROPROPANECIS-1,3-DICHLOROPROPENETRANS-1,3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1,2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANE
- TETKACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE .,1.1.2-TRICHLOROETHANE *'TRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENES
1.00000000
1.001.001.001.001.0010.01.00
00000000
1.001.001.001.001.001.001.001.00
.1.001.005.001.001.001.001.001.001.001.001.001.003.00
XXXXXXXXXXXXXXXXXXXXXXXXXXXXX\XXXXX
TETRAHYDROFURAN 20,0
MADISON
P.O. BOX 5585MADISON, wi 53705
(6CS) 2J1-4747FAX(6C6)23M777
VOLATILE ORGANIC"COMPOUND RESULTS PAGE OF WI LAB CERTIFICATION ID*: 113138300 CK'D: JuwAPP'D:PROJECT: HAGEN FARM RIFS DATE ISSUED:LOCATION: STOUGHTON, WISCONSINC#: 13452.89
BMQL - DETECTED, VALUE BELOW METHOD QUANTITATION LIMIT.X « ANALYZED, BUT NOT DETECTED.
REFERENCE: SW846, "TEST METHODS FOR EVALUATING SOLIDWASTE*f SEPTEMBER, 1986. METHODS 8010AND 8020 WITH MODIFICATIONS.
MADISONONE SCIENCE COLTTT
P.O. BOX 5385MADISON, Wl 5J705
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PAGE ' Of CK'D:4Uu'APP'DDATE ISSUED :
COMPOUND
REPORTABLEDETECTIONLIMIT(UG/L)
1957-001HF-GWDTB01-7911/14/90
BENZENEBROMOCHLOROMETHANEBROMOOICHLOROMETHANEBROMOFORMBROMOMETHANE
• CARBON TETRACHLORIDECHLOROBENZENECHLOROOIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DIBROMO-3-CHLOROPROPANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE
v 1,1-DICHLOROETHANE^-a,2-DICHLOROETHANE
1.1-DICHLOROETHENECIS-1,2-DICHLOROETHENETRANS-1.2-DICHLOROETHENE1.2-DICHLOROPROPANECIS-1,3-DICHLOROPROPENE
. TRANS-1,3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1,2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE1.1.2-TRICHLOROETHANE -vTRICHLOROETHENETRICHLOROFLUOROHETHANEVINYL CHLORIDEXYLENES
TETRAHYDROftjRAN
1.001.001.00i;ooi.ooi.ooi.ooi.ooi.oo10.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001,001.001,001.001.003.00
250
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
923
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PAGE*- OF5CK'D** **' APP'D"DATE*ISSUED:*/*-
OMPOUND
BENZENEBROMOCHLOROMETHANEBROMODICHLOROMETHANEBROMOFORMBROMOMETHANE .CARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANEl,2-DIBROMO-3-CHLOROPROPANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE
v 1,1-DICHLOROETHANEMf2-DICHLOROETHANE
1.1-DICHLOROETHENECIS-1.2-DICHLOROETHENETRANS-1.2-DICHLOROETHENE1.2-DICHLOROPROPANECIS-1, 3-DICHLOROPROPENETRANS-1.3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1, 2-TETRACHLOROETHANE1,1,2 , 2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE .,1.1.2-TRICHLOROETHANE " .TRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENES
REPORTABLEDETECTIONLIMIT(UG/L)
1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.00-1.001.001.003.00
1957-002HF-GWDTB01-9711/14/90
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
TETRAHYDROFURAN 50.0 157
MADISONONE SCIENCE COURTP.O. BOX 5565
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BMQL - DETECTED, VALUE BELOW METHOD QUANTITATION LIMIT.X - ANALYZED, BUT NOT DETECTED.
Si THOD REFERENCE: SW846, "TEST METHODS FOR EVALUATING SOLIDWASTE*, SEPTEMBER, 1986. METHODS 8010AND 8020 WITH MODIFICATIONS.
P.O. BOX 5535MADISON. V[ 53705
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Volatile Organic Compound ResultsWI Lab Certification ID#: 113138300Project: Hagen Farms RI/FSLocation: Stoughton, WisconsinCf: 13452.98
Page! Of3Ckfd:jW App'dDate Issued: u
Compound
ReportableDetectionLimit(ug/L)
2047-001HF-GWOTB01-11712/6/90
Bromodi chloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChlorbethane2-Chloroethylvinyl EtherChloroformChloromethane1.2-01chlorobenzene1.3-Dichlorobenzene1.4-Dlchlorobenzene1.1-Dichloroethane1.2-DichToroethane1.1-Dichloroetheneci s-1,2-Di chloroethene
\_/trans-l,2-Dichloroethene1.2-Dicnloropropanecis-1,3-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenesTetrahydrofuran
1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001,001.001.001.001.001.003.0020.0
XXXXXXXX .XXXXXXXXXXXXXXXXXXXXXXXXXX
WJRZYNi*.O. DUA «oJ
MADISON. Wl 53705C6C8) 2JM747
FAXC606)23M77?
Volatile Organic Compound ResultsWI Lab Certification IDS: 113138300Project: HagenTarms RI/FSLocation: Stoughton, Wisconsintt: 13452.98
PageCk*dDate Issued: \T_-ZC-
Compound
ReportableDetectionLimit(ug/L)
2047-002HF-GWDTB01-13712/6/90
BenzeneBromodi chloromethane
BromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromometh aneChloroethane2-Chloroethylvinyl Ether
• ChloroformChloromethane1.2-Dichlorobenzene1.3-Di chlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroetheneci s-1,2-Di chloroethenetrans-l,2-Dichloroethene1.2-Di chloropropane
^ cis-lf3-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMetnylene Chloride1,1,2,2-Tetrachl oroethaneTetrachloroetheneTo!uene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenesTetrahydrofuran
10.010.010.010.010.010.010.010.010010.010.010.010.010.010.010.010.010.010.010.010.010.010.050.010.010.010.010.010.010.010.010.030.0200
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
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Page 3 Of 3Ck*dDate
X - analyzed, but not detected.
Method reference: SW846, "Test Methods for Evaluating SolidWaste", September, 1986. Methods 8010and 8020 with modifications.
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PAGE 1 OF CZ-CK'D:jdWAPPDATE ISSUED:
COMPOUND.= »==r«CX=
N—<-• *
BENZENEBROMOCHLOROMETHANEBROMODICHLOROMETHANEBROMOFORMBROMOMETHANE
- CARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DIBROMO-3-CHLOROPROPANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENEM-DICHLOROETHANE
^,2-DICHLOROETHANE1.1-DICHLOROETHENECIS-1,2-DICHLOROETHENETRANS-1.2-DICHLOROETHENE1.2-DICHLOROPROPANECIS-1,3-DICHLOROPROPENETRANS-1.3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1,2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE1.1.2-TRICHLOROETHANE -vTRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENES
TETRAHYDROFtlRAN
REPORTABLEDETECTIONLIMIT(UG/L)
1964-001HF-GWDTB02-2711/15/90
1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003.00
20,0
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
mRZYN
MADISON'ONE SCIENCE COURT
P.O. BOX 53-85MADISON. Wl 53705
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BMQL - DETECTED, VALUE BELOW METHOD QUANTITATION LIMIT.X « ANALYZED, BUT NOT DETECTED.
METHOD REFERENCE: SWS46, "TEST METHODS FOR EVALUATING SOLIDWASTE6, SEPTEMBER, 1986. METHODS 8010AND 8020 WITH MODIFICATIONS.
WiRZYN
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PAGE l OF 3CK'D:JWAPP'DDATE ISSUED: »
"OMPOUND
BENZENEBROMOCHLOROMETHANEBROMODICHLOROMETHANEBROMOFORMBROMOMETHANECARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DIBROMO-3-CHLOROPROPANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE
v>,l-DICHLOROETHANEM.2-DICHLOROETHANE
1.1-DICHLOROETHENECIS-1.2-DICHLOROETHENETRANS-1.2-DICHLOROETHENE1.2-DICHLOROPROPANECIS-1 ,3-DICHLOROPROPENETRANS-1 ,3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1,2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRlCHLOROETHANE .,1.1.2-TRICHLOROETHANE " .TRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENES
REPORTABLEDETECTIONLIMIT(UG/L)
1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003.00
1971-001HF-GWDTB02-37
11/16/90
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
TETRAHYDROFURAN 20.0
MADISONONE SCIENCE COURT
P.O. BOX 5385MADISON. Wl 53705
(6C8) »l-47«7FAX(6CB)23M777
VOUTILE ORGANIC-COMPOUND RESULTSWI LAB CERTIFICATION IDS: 113138300PROJECT: HAGEN FARM RI/FSLOCATION: STOUGHTON, WISCONSINC#: 13452.89 •
PAGE *- OFCK'D:4vDATE ISSUED
COMPOUND
REPORTABLEDETECTIONLIMIT(UG/L)
- 1971-002HF-GWDTB02-57
11/16/90
BROMOCHLOROMETHANEBROMODICHLOROMETHANEBROMOFORMBROMOMETHANECARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANE 'CHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DIBROMO-3-CHLOROPROPANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE1.1-DICHLOROETHANE1.2-DICHLOROETHANE1.1-DICHLOROETHENECIS-1,2-DICHLOROETHENETRANS-1,2-DICHLOROETHENE1.2-DICHLOROPROPANECIS-1,3-DICHLOROPROPENETRANS-1,3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1f2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE1.1.2-TRICHLOROETHANETRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENES
1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003.00
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
TETRAHYDROFURAN 20.0
WARZYN
MADISONONE SC1ENCI COURTP.O. 3OX 5J3S
MAD BOS. wi 5J705(6CS) 23M747
FAX(6CS)23M777
VOLATILE ORGANIC COMPOUND RESULTS PAGE * OF3WI LAB CERTIFICATION ID#: 113138300 CK'Dt^APP'D:PROJECT: HAGEN FARM RI/FS DATE ISSUED: a|tt.LOCATION: STOUGHTON, WISCONSINC#: 13452.89
BMQL - DETECTED, VALUE BELOW METHOD QUANTITATION LIMIT.X « ANALYZED, BUT NOT DETECTED.
REFERENCE: SW846, "TEST METHODS FOR EVALUATING SOLIDWASTE*, SEPTEMBER, 1986. METHODS 8010AND 8020 WITH MODIFICATIONS.
MADISONONE SCIENCE COURT
P.O. BOX 5385MADISON, wi 537Q5
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^COMPOUND
REPORTABLEDETECTIONLIMIT(UG/L)
1977-001 1977-002HF-GWDTB02-78 HF-FB0111/19/90 11/19/90
BENZENEBROMODICHLOROMETHANEBROMOFORMBROMOMETHANECARBON TETRACHLORIOECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE.2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE1,1-DICHLOROETHANE
^yl,2-DICHLOROETHANE1.1-DICHLOROETHENECIS-1.2-DICHLOROETHENETRANS-1,2-DICHLOROETHENE1.2-DICHLOROPROPANECIS-1,3-DICHLOROPROPENETRANS-1.3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1,2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE1.1.2-TRICHLOROETHANETRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENES
1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003.00
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
TETRAHYDROfURAN 20.0
MADISONONE SCIENCE COURTP.O. BOX 5385
MADISON, VI 53705(6C8J ZJM747
FAX (6C8) 2514777
VOLATILE ORGANIC-COMPOUND RESULTS PAGE* OFWI LAB CERTIFICATION IDS: 113138300 CK'DwPROJECT: HAGEN FARM RIFS DATE ISSUEDLOCATION: STOUGHTON, WISCONSINCl: 13452.89
COMPOUND
BENZENEBROMODICHLOROMETHANEBROMOFORMBROMOMETHANECARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENC1.1-DICHLOROETHANE1.2-DICHLOROETHANE1.1-DICHLOROETHENE *
-1 ,2-DICHLOROETHENETRANS-1, 2-DICHLOROETHENE1.2-DICHLOROPROPANECIS-1, 3-DICHLOROPROPENETRANS-1 ,3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1 , 1 , 1 , 2-TETRACHLOROETHANE1 , 1 ,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE1.1.2-TRICHLOROETHANETRICHLOROETHENETRICHLOROFLUOROMETHANE - ,VINYL CHLORIDEXYLENES
REPORTABLEDETECTIONLIMIT(UG/L)
1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001,001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003,00
1977-003HF-TB0111/19/90
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
TETRAHYDROFURAN 20.0
MADISONONE SCIENCE COURT
P.O. BOX 3585MADISON, Wl 55T05
VOLATILE ORGANIC COMPOUND RESULTS PAGE 3WI LAB CERTIFICATION I0#: 113138300 CK'D: APP'D:V1CGPROJECT: HAGEN FARM RIFS DATELOCATION: STOUGHTON, WISCONSINC#: 13452.89
BMQL - DETECTED, VALUE BELOW METHOD QUANTITATION LIMIT.X - ANALYZED, BUT NOT DETECTED.
REFERENCE: sws46, -TEST METHODS FOR EVALUATING SOLIDWASTEfi, SEPTEMBER. 1986. METHODS 8010AND 8020 WITH MODIFICATIONS.
WAKZYN
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Page I Of ICkrd: W App'dDate Issued:i-j
Compound
ReportableDetectionLimit(ug/L)
2069-001HF-GWDTB02-7412/11/90
BenzeneBromochloromethaneBromod1chloromethane
v JSromoformBromomethaneCarbon TetrachlorldeChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethanel,2-Dibromo-3-Chloropropane1, 2-D1chlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-1,2-Di chloroethenetrans-1,2-Dichloroethene1t2-D1chloropropane^ cis-l,3-Dichloropropenetrans-1,3-Di chloropropeneEthyl BenzeneMethylene Chloride1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trichloroethane1.1.2-Trichloroethane
. TrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenesTetrahydrofuran
1*001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.00000000
1.001.001.001.005.001.001.001.001.001.001.001.001.001.003.00
10.0
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
X * analyzed, but not detected.Method reference: SW846, "Test Methods for Evaluatin<
Waste", September, 1986. Methods 1and 8020 with modifications.
I Solidtoio
Volatile Organic Compound ResultsWI Lab Certification ID3: 113138300Project: Hagen Farm RI/FSLocation: Town-"of Dunn, WisconsinCl: 13452.98
• Page l Ofpk rf *•Date Issued'
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Compound
ReportableDetectionLimit(ug/L)
2062-001(1)HF-GWDTB02-9412/10/90
BenzeneBromochl oromethane3romodi chl oromethane
BromomethaneCarbon TetrachlorideChl orobenzeneChl orodibromomethaneChl oroethane2-Chloroeth/l vinyl EtherChloroformChl oromethanel,2-Dibromo-3-Chloropropane1 , 2-Di chl orobenzene1,3-Dichl orobenzene1 , 4-Di chl orobenzene1 , 1 -D1 chl oroethane1, 2-Di chl oroethane1.1-Dichloroethenecis-1, 2-Dichloroethenetrans-1, 2-Di chl oroethene1.2-Dichloropropanecis-1, 3-Dichloropropenetrans-1 ,3-Dichl oropropeneEthyl BenzeneMetnylene Chloride1,1,1 , 2-Tetrachl oroethane1,1,2, 2-Tetrachl oroethaneTetrachl oroetheneTo! uene1 , 1 , 1-Tri chl oroethane1 , 1 , 2-Tri chl oroethaneTrichloroetheneTri chl orof 1 uoromethaneVinyl ChlorideXyl enes
1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.000000
1.001.005.001.001.001.001.001.001.001.001.001.003.00
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
Tetrahydrofuran 10.0
MADISONONE SCIENCE COURT
P.O. BOX 5385MADBON. -m 53705
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Volatile Organic Compound Results Paqe Of *-WI Lab Certification ID#: 113138300 £k d: App'd:Project: Hagen Farm RI/FS Date Issued:Location: Town of Dunn, WisconsinC#: 13452.98
X « analyzed, but not detected.(1) Sample chromatogram contains unidentified compounds.Method reference: SW846, "Test Methods for Evaluating Solid
Waste*, September, 1986. Methods 8010and 8020 with modifications.
WARZYN
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COMPOUND
PAGE t OF 'DATE ISSUED: ,i,»-
REPORTABLEDETECTIONLIMIT(UG/L)
1982-001HF-GWDTB02-9711/20/90
1.00BROMODICHLOROMETHANEBROMOFORMBROMOMETHANECARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE1.1-DICHLOROETHANE1.2-DICHLOROETHANE1.1-DICHLOROETHENECIS-1.2-DICHLOROETHENE
WTRANS-1,2-DICHLOROETHENE1.2-DICHLOROPROPANE 'CIS-1,3-DICHLOROPROPENETRANS-1,3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1,2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE1.1.2-TRICHLOROETHANETRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENESTETRAHYDROFURAN
1.001.001.001.001.00J.OO1.0010.01.001.001.001.001.001,001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003.00
20.0
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
X « ANALYZED, BUT NOT DETECTED.
METHOD REFERENCE: SW846, "TEST METHODS FOR EVALUATING SOLIDWASTE", SEPTEMBER, 1986. METHODS 8010AND 8020 WITH MODIFICATIONS.
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Page ICkYd :
OfApp'd:
Date Issued:rt//t/54v
Compound
ReportableDetectionLimit(ug/L)
2002-001 2002-002HF-GWDTB03-67 HF-FB0211/27/90 11/27/90
v janzene^IJromodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodibromomethaneChloroethane2-Chloroethylvinyl Ether1.2-Di chlorobenzene1.3-Di chlorobenzene1.4-Di chlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroetheneci s-1,2-Di chloroethenetrans-1.2-Dicnloroethene1.2-Di cnloropropane:i s-1,3-Di ch1oropropenerans-1,3-Di chl oropropeneEthyl BenzeneMetnylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-TrichloroethaneTrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenes
1.001.005.005.001.001.001.003.0025.01.001.001.001.001.003.003.003.001.001.001.001.005.001.001.001.001.001.001.003.003.003.00
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
XXXXXXXXXXXXXXXXXXXXX6.76XXXXXXXXX
Tetrahydrofuran 20.0
MAXHSONONE SCIENCE COURT
P.O. BOX 5385MADBON, wi 53705
FAX<606)23M777
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e 2- Ofd:j*«v
Date Issued:t*//*/>>
Compound
ReportableDetectionLimit(ug/L)
2002-003HF-GWDTB03-8711/27/90
Benzene, omodi chloromethaneX^omoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodibromomethaneChloroethane2-Chloroethylvinyl Ether1.2-Di chlorobenzene1.3-Di chlorobenzene1.4-Di chlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecls-1,2-Di chloroethenetrans-1.2-Dichloroethene1.2-Di chloropropanecis-1,3-Di chloropropene*rans-l,3-Dichloropropene
v/hyl BenzeneHetnylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTri chlorofluoromethaneVinyl ChlorideXylenes
1.001.005.005.001.001.001.003.0025.01.001.001.001.001.003.003.003.001.001.001.001.005.001.001.001.001.001.001.000000
3.00
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
Tetrahydrofuran 20.0
MADISONONE SCIENCE COURT
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3 Of-
Compound
ReportableDetectionLimit(ug/L)
2002-004HF-GWDTB03-9211/27/90
Benzene, -omodi chloromethaneroraoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodibromomethaneChloroethane2-Chloroethylvinyl Ether1.2-Dichlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-l,2-Dichloroethenetrans-1.2-Dichloroethene1.2-D1cnloropropanecis-l,3-Dichloropropene>ans-l,3-Di chloropropene
v thyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trichloroethane1.1.2-Tri chloroethaneTrichloroethene.Trichlorof1uoromethaneVinyl ChlorideXylenes
1.001.005.005.001.001.001.003.0025.01.001.001.001.001.003.003.003.001.001.001.001.005.001.001.001.001.001.001.003.003.003.00
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
Tetrahydrofuran 20.0
W^RZYN
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Page H OfCk?d:-jwDate Issued:)1/'*/
Compound
Benzenev^romodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorod i bromomethane
. Chloroethane- 2-Chloroethylvinyl Ether1.2-Di chlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-l,2-Dichloroethenetrans-1.2-Di chloroethene1.2-Dichloropropanecis-1,3-Di chloropropene
£rans-l, 3-Di chl oropropeneEthyl BenzeneMetnylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trichloroethane1.1.2-Tri chloroethaneTrichloroetheneTrichlorofluoromethaneVinyl ChlorideXylenes
ReportableDetectionLimit(ug/L)
1.001.005.005.001.001.001.003.0025.01.001.001.001,001.003.003.003.001.001.001.001.005.001.001.001.001.001.001.003.003.003.00
2002-005 2HF-FB03 H11/27/90 1
XXXXXXXXXXXXXXXXXXXXX
5.85XXXXXXXXX
:002-006(1)IF-TB021/27/90
XXXXXXXX-xXXXXXXXXXXXXXXXXXXXXXX
Tetrahydrofuran 20.0
mRZYN
Volatile Organic Compound Results Page^Of/ rf\/ —— ~WI Lab Certification ID#: 113138300 Ck?d:^juu App'd: |^X
MADISONONE SCIENCE COURT
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' C608) 231-4747FAX (608) 23M777
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X • analyzed, but not detected.(1) Sample chromatogram contains unidentified compounds.thod reference: SW846, "Test Methods for Evaluating Solid
Waste", September, 1986. Methods 8010and 8020 with modifications.
mRZYN
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PAGE I OF*CK'D:4WAPDATE ISSUED
COMPOUND
V 3ENZENEMJROMODICHLOROMETHANEBROMOFORMBROMOMETHANECARBON TETRACHLORIDECHLOROBENZENECHLORODIBROMOMETHANECHLOROETHANE2-CHLOROETHYLVINYL ETHERCHLOROFORMCHLOROMETHANE1.2-DICHLOROBENZENE1.3-DICHLOROBENZENE1.4-DICHLOROBENZENE1.1-DICHLOROETHANE1.2-DICHLOROETHANE1,1-DICHLOROETHENECIS-1,2-DICHLOROETHENETRANS-1.2-DICHLOROETHENE^,2-DICHLOROPROPANECIS-1,3-DICHLOROPROPENETRANS-1,3-DICHLOROPROPENEETHYL BENZENEMETHYLENE CHLORIDE1,1,1,2-TETRACHLOROETHANE1,1,2,2-TETRACHLOROETHANETETRACHLOROETHENETOLUENE1.1.1-TRICHLOROETHANE1.1.2-TRICHLOROETHANETRICHLOROETHENETRICHLOROFLUOROMETHANEVINYL CHLORIDEXYLENESTETRAHYDROFURAN
REPORTABLEDETECTIONLIMIT
1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003.0020.0
1998-001(1)HF-GWDTB03-2711/26/90
1998-002(1)HF-GWDTB03-4711/26/90
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
X - ANALYZED, BUT NOT DETECTED.
METHOD REFERENCE: SW846, "TEST METHODS FOR EVALUATING SOLIDWASTE", SEPTEMBER, 1986. METHODS 8010 AND8020 WITH MODIFICATIONS.
(1) SAMPLE CHROMATOGRAM CONTAINS UNIDENTIFIED COMPOUNDS.
mRZYN
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Compound
ReportableDetectionLimit(ug/L)
2007-001HF-GWDTB03-10711/28/90
v anzene^tfromodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl Ether1,2-Di bromo-3-Chloropropane1,2-D i chlorobenzene1(3-D1chlorobenzene1,4-Di chlorobenzene1.1-Dichloroethane .1.2-01chloroethane1,1-Dichloroethenecis-1,2-Dichloroethenetrans-l,2-Dichloroethene\2-Dicnloropropane
^-«ds-l,3-Dichioropropenetrans-l,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trichloroethane1.1.2-Tri chloroethaneTrichloroetheneTrichlorofluoromethaneVinyl ChlorideXylenesTetrahydrof uran - * •»
1.001.005.005.001.001.001.003.0025.02.001.001.001.001.001.003.003.003.001.001.001.001.005.001.001.001.001.001.001.003.003.003.00
20.0
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
X - analyzed, but not detected.
Method reference: SW846, "Test Methods for Evaluating SolidWaste", September, 1986. Methods 8010and 8020 with modifications.
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OfApp'd
Date Issued:
Compound
ReportableDetectionLimit(ug/L)
2007-002HF-GWDTB03-12711/28/90
BenzeneV jromodichloromethane^-Bromoform
BromomethaneCarbon TetrachlorideChlorobenzeneChlorod1bromomethaneChloroethane2-Chloroethylvinyl Ether1,2-DIbromo-3-Chl oropropane1.2-Di chlorobenzene1.3-Dichlorobenzene1.4-Di chlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-l,2-Dichloroethenetrans-1.2-Dichloroethene1.2-D1cnloropropanev:1 s-1,3-Di chl oropropene
^trans-l,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-TrichloroethaneTrichloroetheneTri chlorofluoromethaneVinyl ChlorideXylenesTetrahydrofuran
1.001.005.005.001.001.001.003.0025.02.001.001.001.001.0000000000
1.001.001.001.005.001.001.001.001.001.001.003.003.003.00
20.0
X = analyzed, but not detected.Method reference: SW846, "Test Methods for Evaluating Solid
Waste", September, 1986. Methods 8010and 8020 with modifications.
mRZYN
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Page < Of >CkTd:awu> App'd: »yDate Issued:i*/|T/?0
Compound
ReportableDetectionLimit
2016-001HF-GWDTB03-14711/29/90
yizenex^omodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorod i bromomethaneCM oroethane2-Chloroethylvinyl Ether1.2-Di chlorobenzene1.3-Dichlorobenzene1.4-Dlchlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-l,2-Dichloroethenetrans-1.2-Di chloroethene1.2-D1cnloropropane'•is-l.S-Di chl oropropene•ans-1,3-Di chloropropene'thvl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTrlchldrofluoromethaneVinyl ChlorideXylenesTetrahydrofuran
Vth
1.001.005.005.001.001.001.003.0025.01.001.001.001.001.003.003.003.001.001.001.001.005.001.001.001.001.001.001.003.003.003.00
20.0
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
X « analyzed, but not detected.Method reference: SW846, "Test Methods for Evaluating Solid
Waste", September, 1986. Methods 8010and 8020 with modifications.
WRZYN
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Volatile Organic Compound Results Page ( OfWI Lab Certification ID#: 113138300 Ckrd:<j ,Project: Hagen Farm RI/FS Date IssuedLocation: Stoughton, WisconsinC#: 13452.98 "
Compound
ReportableDetectionLimit(ug/L)
2090-OOim-HF-GWDTB04-7512/13/90
BenzeneBromochloromethaneBromod i chloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethanel,2-Dibromo-3-Chloropropane1.2-Dichlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1.1-Dichloroethenecis-l,2-Dichloroethenetrans-1,2-Dichloroethene1.2-Dichloropropanecis-l,3-Dichloropropenetrans-1,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tri chloroethaneTrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenes
1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.003.00
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
Tetrahydrofuran 10.0
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X - analyzed, but not detected.(1) Sample chromatogram contains unidentified compounds.Method reference: SW846, "Test Methods for Evaluating Solid
Waste*, September. 1986. Methods 8010and 8020 with modifications.
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Of3App'd:
Date Issued:, r/tPag?
Compound
^-BenzeneBromochloromethaneBromodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorod i bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethanel,2-Dibromo-3-Chloropropane1.2-D1chlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane,1-Dichl oroethene
ci s-1,2-Di chloroethenetrans-l,2-D1chloroethene1.2-Di chloropropanecis-l,3-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Tri chloroethane1.1.2-Tri chloroethane ^TrichloroetheneTri chlorof1uoromethaneVinyl ChlorideXylenes
ReportableDetectionLimit(ug/L)
1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.004.00
2122-001 2122-002 2122-003HF-GWD HF-GWD HF-GWDTB04-134 TB04-93 TB04-12212/18/90 12/18/90 12/18/90
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX '
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
Tetrahydro£uran 10.0
WiRZYN
MADISONONE SCIENCE COURT
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FAX (608) 231-4777
Volatile Organic Compound ResultsWI Lab Certification ID#: 113138300Project: Hagen Farm RI/FSLocation: Stoughton, WisconsinC#: 13452.98
Page *• Of 3Ck'd:-*'*-'App'd:Date Issued: i
Compound
BenzeneBromochloromethaneBromodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodibromomethaneChl oroethane2-Chloroethyl vinyl EtherChloroformChloromethanel,2-Dibromo-3-Chloropropane1 , 2-Dichl orobenzene1,3-Dichlorobenzene1 , 4 -Di chl orobenzene1.1-Dichloroethane1.2-Dichloroethane1,1-Dichloroethenecis-l,2-Dichloroethenetrans-l,2-Dichloroethene1 , 2 -Di cnl oropropanecis-l,3-Dichloropropenetrans-l,3-DichloropropeneEthyl BenzeneMethyl ene Chloride1,1,1 ,2-Tetrachl oroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1,1,1 -Tr i chl oroethane1,1,2-Trichl oroethaneTrichloroetheneTri chl orof 1 uoromethane" * . -Vinyl ChlorideXylenes
ReportableDetectionLimit
2122-004 2122-005HF-GWD HF-GWD 2122-006TB04-104 TB04-92 HF-TB0412/18/90 12/18/90 12/18/90
1.001.001.001.001.001.001.001.001.0010.01.001.002.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.004.00
XXXXXXXXXXXXXXXXXXaXXXXXXXXXXXXXXXXX
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
XXXXXXXXXXXXXXXXXXXXXXXXXXX .XXXXXXXXX
Tetrahydrofuran 10.0
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Volatile Organic Compound Results Page 3 of3WI Lab Certification ID#: 113138300 Ck'd: App'd:Project: Hagen Farm RI/FS Date Issued: iLocation: Stoughton, Wisconsin«: 13452.98
X - analyzed, but not detected.
Method reference: SW846, "Test Methods for Evaluating SolidWaste* , September, 1986. Methods 8010and 8020 with modifications.
mRZYN
MADISONONE SCIENCE COURT
P.O. BOX 5585MADISON, WI 53705
FAX (608) Z3M777
Volatile Organic Compound ResultsWI Lab Certification ID#: 113138300Project: Hagen Farm RI/FSLocation: Stoughton, WisconsinC#: 13452.98
Page I Of *-Ck'diJW-' App'd:Date Issued: 1/3/7 /
Compound
BenzeneBromodichloromethaneBromoformBromomethaneCarbon TetrachlorideChlorobenzeneChlorodi bromomethaneChloroethane2-Chloroethylvinyl EtherChloroformChloromethane1, 2-Di chlorobenzene1.3-Dichlorobenzene1.4-Dichlorobenzene1.1-Dichloroethane1.2-Dichloroethane1,1-Dichloroethenecis-1,2-Di chloroethenetrans-1,2-Dichloroethene1, 2-Di chloropropanec1s-l,3-Dichloropropenetrans-1,3-DichloropropeneEthyl BenzeneMethylene Chloride1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1.1.1-Trichloroethane1.1.2-TrichloroethaneTrichloroetheneTrlchlorofluoromethaneVinyl Chloride /-?Xylenes
ReportableDetectionLimit(ug/L)
1.001.001.001.001.001.001.001.0010.01.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.003.00
2142-001 2142-002HF-GWD HF-GWDTB05-60 TB05-4712/20/90 12/20/90
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
Tetrahydrofuran 10.0
mRZYN
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Paget, Of *Ck7d: W App'd:>iTADate Issued: i
X - analyzed, but not detected.
Method reference: SW846, "Test Methods for Evaluating SolidWaste*, September, 1986. Methods 8010and 8020 with modifications.