U. S. ARMY CORPS OF ENGINEERSDRAKE CHEMICAL SUPERFUND SITE182 MYRTLE STREETLOCK HAVEN, PA 17745717-748-4505 717-748-7549 FAX FIELD MEMO X0286

TO: EOCK^HAVEN REPOSITORIES:RQSS PUBLIC LIBRARY 'STEVENSON LIBRARY

' . , •' LOCK HAVM ENVIRONMENTAL ADVISORY COMM. (U S MAIL): GEORGEPRUMBOR ..::

- GREGG'CRYSTALL ' """

VIA: . HAND DELIVERYFROM: FRANK CLEAVER, USACEDATE: OCTOBER 21, 1998 : : /;RE: "STACK TESTING FOR JULY 1993 REPORT

Attached is Transmittal Number 568-Thermal Destruction Facility Compliance EmissionEvaluation Summary Report—Monthly Dioxin/Furan Sampling—July 1998.

FILE: 13590FIELD MEMO

AR32I839

A R 3 2 I 8 U O

-' DACW4593-C-0200 , _.. "TRANSMITTAL NOl 568

ITEM NO. 986 - TTHERMAL DESTRUCTION FACILITYCOMPLIANCE EMISSION EVALUATION SUMMARY REPORT

MONTHLYDIOXIN/FURANSAMPLING - JULY 1998. ATTACHED SHEET

ACTION CODE C, APPROVED, EXCEPT AS NOTED. . -RESUBMISSION REQUIRED

1. Appendix II, Page 0018: •

A. The water caught for Run I should be 3345.7 grams and not the 2934.8 gramsshown on the calculation sheet. This will impact the output data on Page 0018 forpercent moisture and subsequent calculations for stack gas flow. Also theemission rates and stack flow etc. on Tables 1 and 2 and Page 0016 will change.

B. The Delta H Value for Point 2 should be 1.36 and not 1.42.V

Page 0016, Page 0018, Table 1 and Table 2 are to be corrected accordingly andresubmitted.

AR32I8U

AirRecon®A LEVINE'FRICKE'ftECON GROUP COMPANY

.3*° OPERATING PHASE DIOXIN & FURANEMISSION EVALUATION REPORTJULY 1998 SAMPLING

FOR THE TDF OUTLET STACK @THE DRAKE CHEMICAL SUPERFUN.D SITELOCK HAVEN PA

Prepared forOHM Remediation180 Myrtle Street -Lock Haven PA 17745Attn: Gary Jones

AirRECON Project 311-81415-00-000s

Test Date: July 14, 1998

Report Date: October 6, 1998

(H:\AIRRECON\ STACK98M415-1 ..doc)

5 Johnson Drive, P.O. Box 130, Raritan, NJ 08869/0130 « n o o i o h O(90S) 526-1000 Fax (908) 526-7886 M H O d I O H C

AirRecon®Division of Levins • Fricke • Recon

TABLE OF CONTENTS

INTRODUCTION 1

SUMMARY 2

PERSONNEL & CERTIFICATIONS 5

NOMENCLATURE 6

TABLES

2

3

3 ' SUMMARY OF INCINERATOR PROCESS OPERATING DATA 4

APPENDICES

I LABORATORY DATA SUMMARYH EMISSION CALCULATIONS & ORIGINAL DATADI CALIBRATION DATAIV PROCESS INFORMATIONV SUPPLEMENTAL LABORATORY DATA SUMMARY

AR32I6U3

AirRecon®Division of Levme • Fricke • Recorr

1

INTRODUCTION

AIRRECON performed a stack emission evaluation on behalf o'f OHM REMDEIATIONSERVICES (OHM) at the Drake Chemical Superfund site located in Lock Haven PA.

OHM is performing site remediation by thermal treatment of soil contaminated with organiccompounds left from the manufacturing process formerly located at the site. After passing throughemission control, gases from the process are discharged to the atmosphere through the TDF stack.

AIRRECON is measuring dioxin/furan emissions on the TDF stack. This is the third of threemonthly test events to occur during routine remediation operations at the site.

Dioxin/furan emissions were sampled in accordance with EPA Reference Method 23 (40 CFR 60).Method 23 incorporates EPA Reference methods 1-4, which are used to determine the location oftraverse points in the stack, volumetric stack flow, gas composition (CO2/O2) and stack moisturerespectively.

SUMMARY

Sampling dates and times are summarized, along with emission data, in Table I, EmissionSummary.

Key stack and sampling conditions are summarized in Table 2, Sampling Summary.

Key process conditions are summarized in Table 3, Incinerator Process Operating Data,\

Per Section EL of the case narrative in Philip Analytical's report, samples were reanalyzed toconfirm the non-detect values found in the 2, 3, 7, 8-TCDF confinnational analysis. The re-analysiswas performed in response to instrument difficulties as explained in the same section of Philip'sreport. These data are presented as Appendix V.

/1R32I8UU

AirRecon®Division of Levine * FricKe • Recon

' 2

TABLE 1: EMISSIONS SUMMARY

RUN

DATE

TIME

1

07/14/98

0810-1135

2

07/14/98

1231-1606

3

07/14/98

1727-2052

TOTAL DIOXINS / FURANS1 ' ' : . : ' !: • . '. : ;

ng/dscm @ 7% 02* 0.25

D10X1NS / FURAN

ng/dscm

GRAMS/SECOND

POUNDS/HOUR

6.9E-3

5.7E-11

4.5E-10

0.19 0.24

5 as 2,3,7,8-TCDD: :,-::",; ;: ; : ; - : : ;

6. 1 E-3

4.6E-11

3.6E-10

6.3E-3

4.6E-11 •

3.7E-10

Corrected to 7% Oa using CCb as defined in the Trial Bum Plan

TABLE 2 : SAMPLING SUMMARY

Standard Conditions are 68°F, 29.92 "Hg.

AirRecon®Division "of Levine • Fricke • Recoji

3

RUN

SAMPLING TIME (min)

SAMPLE GAS VOLUME (dscm)

SAMPLE GAS VOLUME (dscf)

MOISTURE (%vo!)

OXYGEN (%vol, dry)

CARBON DIOXIDE {% vol, dry)

AVERAGE STACK TEMP (°F)

% ISOK1NETIC

AVG. STACK VELOCITY (ft/sec)

STACK FLOW RATE (dscm/min)

STACK FLOW RATE (dscfm)

1

180

3.03

107

56.4

9.2

11.6

185

91.2

28.6

491

, 17,400

2

192

3.08

109

59.1

9.7

11.3

184

95.8

27.7

447

15,800

3

192

3.10

110

59.6. _. ., , ^,

8.8

• 11.9

185

97.4

27.8

443

15,600

AR32I8U6

AirRecon®Division of Levme • FncKe"- Recoti"

4

PERSONNEL AND CERTIFICATIONS

FIELD SAMPLING PERFORMED BY:

Thomas F. Mattel

Peter F. Marshall

LABORATORY WORK PERFORMED BY:

' Philip Analytical

CALCULATIONS & REPORT PREPARATON PERFORMED BY:

Thomas F. Mattel

TESTING WAS OBSERVED BY:

Chris McBride Focus Environmental

AirRECON PERSONNEL CERTIFICATIONI certify that, to the best of my knowledge and ability, the work on this project was reported truly,accurately and completely.

SUBMITTED BY:Thomas F. MattelManager, Special Projects

REVIEWED BY;Frank W. SwetitsDirector,AirRECON Division

TFM/sas (HAAffiRECONX STACK.9SV 1415-l.DOC)

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AR32I81*8

AirRecon®Division of Levme • Fricke * Recorr

SELECTED NOMENCLATURETime • military time . -min * minutes°F » degrees Fahrenheit°C « degrees Centigrade"HjO a inches water (pressure or vacuum)"Hg s inches mercury (pressure Or vacuum)mm Hg s millimeters of mercury (pressure or vacuum)psig s pounds of pressure per square inch-gagesq ft * square feetin K inchesmicron = 10-6 metersft/sec s feet per secoridft/min » feet per minuteacfm s cubic feet per minute of total gas flow at flawing conditionsscfra s cubic feet per minute of total gas flow at 7QoF, 29.92"Hgdscfm " dry cubic feet per minute of dry gas flow at 70oF, 29.92"HgIb/hr • pounds per hourBtu/hr • British thermal units per hourX • volume per cent when referred to gases and water vapor% vol s volume per cent% wgt s weight percent .ppmv * volumes of gaseous contaminants per million volumes of total gasgrains = grains x 15.4ug * micrograms = 10-6 grainsma 3 milligrams * 10" gramsgrains/dscf = grains of pollutants per cubic foot of dry stack gas at 70°F, 29.92 "Hggr/dscf • grains/dscfug/nr a micrograms of pollutants per cubic meter of total stack gas at 25oC, 760 mm Hgmg/l * milligrams/liter of liquid = ppm by weight if specific gravity of liquid = 1.0C a elemental carbonCQ2 * carbon dioxideH s elemental hydrogenHS » molecular hydrogenH20 a waterM 3 elemental nitrogenN2 a molecular nitrogenMOx s HO +• M02 s nitrogen oxides * nitric oxide plus nitrogen dioxide reported as equivalent nitrogendioxideS a elemental sulfurSt32 s sulfur .dioxide$03 « sulfur trioxideSQ4 2 sulfateH2$04 = sulfuric acidHjS a hydrogen sulfideCl » elemental chlorine or chlorideCl2 * molecular chlorineHCl a hydrogen chlorideF s elemental fluorine or fluorideCH4 s methane0 » elemental oxygen ,Og 3 molecular oxygenA a argon< a less than; represents the minimum detectability limits< s equal to or less thanHD » none detected

Front-half (dry catch particulate) s particulate matter collected in/on nozzle, probe, cyclone, flaskheated hoser and filter of ERA sampling train

Back-half (wet catch particulate) = material collected in impingers after filter of EPA sampling train

Organic wet catch s residue after low temperature (70°F) evaporation of ether/chloroform used to extractsoluble materials from the wet catch

Aqueous wet catch * residue after high temperature (220°F) evaporation of water left afterether/chloroform extraction

Combustibles ^ volatfles * loss on heating 3 550°C after drying 3 100°C

Ash s residue after heating a550°C

AirRecon®Division of Levine • Fricke • Recon

0007

APPENDIX I

LABORATORY DATA

SUMMARY

'1R32I850

PROJECT NARRATIVE

PHILIP Analytical Services (Burlington ON) . 0 f) 0 &Philip Project: AN98Q2S1 . - u U 3Philip Submission #:8G0533

Client: Levine-Fricke-ReconClient Project: 311-81415

L SAMPLE RECEIPT/ANALYSIS

a) Sample Listing

Philip 0> Client Date Date Date RunSample ID Sampled Received Prepped Date

PCDD/F(t>B5) via EPA Method 23 - Primary Column Analysis033622 98 Method Blank 98/07/14 98/07/16 98/07/22 98/07/3003362398 Blank 98/07/14 98/07/16 98/07/22 98/07/30 ...033624 98 Run#l 98/07/14 98/07/16 98/07/22 98/07/30 -033625 98 Run 22 98/07/14 98/07/16 98/07/22 98/07/3003362698 Run #3 98/07/14 98/07/16 98/07/22 98/07/30 '033627.98 Blank Toluene 98/07/14 98/07/16 98/07/21 98/07/30 .:03362898 Run # 1 Toluene 98/07/14 98/07/16 98/07/22 98/07/3003362998 Run #2 Toluene 98/07/14 98/07/16 98/07/22 98/07/31033630 98 Run S3 Toluene 98/07/14 98/07/16 98/07/22 98/07/312,3,7,8 TCDF(DB225) via EPA Method 23 - Primary Column Analysis03362398 Blank 98/07/14 98/07/16 98/07/22 98/08/1703362498 Run 31 98/07/14 98/07/16 98/07/22 98/08/17 .;....033625 9,8 Run £2 98/07/14 98/07/16 98/07/22 98/08/17033626 98 Run #3 98/07/14 98/07/16 98/07/22 98/08/17

Run Date is defined as the date of injection of the last calibration standard (12 hour or less) prior to thesamples analyzed within, that run sequence. Therefore the time of calibration injection that defines therun date is always within 12 hours of the time of sample injection.

b) Shipping Problems: none encountered

c) Documentation Problems; none encountered

a SAMPLE PREP:

No problems encountered

UL SAMPLE ANALYSIS:

See also comments within the appropriate Certificate of Analysis.

a) Hold Times; all within recommended hold times

RR32I85

0009b) Instrument Calibration: all within control limits -Note that during the confirmation run, the instrument failed before the post run calibration was injected.The standard was reinjected the following morning and this standard met the continuing calibrationcriteria. No maintenance on the instrument was performed and this was simply a rerun of the standard.Therefore the data quality should not be impacted.The samples will be reanalysed to confirm the non-detects found in the confirmational analysis.

c) Surrogate/Internal Recoveries; except where noted otherwise, all within control limits

IV.DATA QUALITY ASSESSMENT.\11 samples for PCDD/F were analysed via EPA Method 23.All data quality objectives for the method were met. All data contained herein was reviewedby the laboratory prior to release to Recon for review and deemed valid.

1 certify that this data package is in compliance with the terms and conditions of the contract,both technically and for completeness, for other than the conditions detailed above.En addition, I certify, that to the best of my knowledge and belief, the data as reported are true and accurate.Release of the data contained in this data package has been authorized by the cognizant laboratoryofficial or his/her designee, as verified by this signature.

Ada Blythe, Project Manager Date

AR32I852

0010PHILIP SERVICES

Certificate of AnalysisCLIENT INFORMATION LABORATORY INFORMATION

Attention: Tom Mattel Contact: Ron McLeodClient Name: Levine-Fricke-Recon Project: AN980282Project: 31L-81415 Date Received: 98/077 L6Project Desc: OHM/Drake Oper. Stack Test 3 Date Reported: 98/08/11

Address: P.O.Box 130,5 Johnson Dr. Submission No.: 8G0533Raritan, N.I Sample No.: 033622-03363008869-0317

Fai Number: 908-526-7886Phone Number: 908-526-1000

•NOTES: "-' - not analysed '<'*«less than .\fetftod Detection Limit (,\>fDL) '.Y4' = no data availableLOQ can by determined for all analytes by multiplying the appropriate MDL X 3.33

Solids data is based on dry weight except for biota analyses.Organic analyses are not corrected for extraction recovery standards except for isotope

. dilution methods. (Le. CARB-t29 P.±H. all PCDD/FandDSD/DBF analyses)

Methods used by PASC are based upon those found in 'Standard Methods for the Examination of Water andWastewater1, Nineteenth Edition. Other methods are based on the principles of MISA or EPA methodologies.New York State: ELAP Identification Number 10756. _. .

All work recorded herein has been done in accordance with normal professional standards using accepted testingmethodologies, quality assurance and quality control procedures except where otherwise agreed to by the clientand testing company in writing. Any and all use of these test results shall be limited to the actual cost of thepertinent analysis done. There is no other'warranty expressed or implied. Your samples will be retained atPASC for a period of three weeks from receipt of data or as per contract.

COMMENTS; Revision 98/10/01: DB225 data

KS Not Spiked

AR32I853s* \ortli

UU111(]/5/98 . ^PASC- Certificate of Analysis *>&

Method - - - -Client ID: - Blank Blank Runtfl Run #2 Run #3Lab.Vo.: 03362298 03362398 03362498 03362598 03362698 .

Date Sampled: 98/07/14 98/07/14 98/07/14 98/07/14 98/07/14Component - Units — _ . . _

2.3.7,S_-Cl4-Dibenzo-p-<lioxin ' ng " <0.0016 0.0092 . 0,00.96 0,0094 . .0,0100.I,2,3,7,8-C15-Dibenzo-p-dioxin ";" ng \ O.QQ16 ' . . 0.0024 0.0028 " 0.0026 <0.0027 -l-2.3,4,7,8-C16-Dibenzo-p-dioxin ' ng O.0025. . <0.0021 " .0.0062 . 0,0025 -0.0044.l,2,3,6.7,8-C16-Dibenzo-p-dioxin ng O.0021 <0.0018 „ "0.0120 0.0098 0.01101,2,3,7.8, 9-C16-Dibenzo-p-dioxin ng <0.0023 0.0049 . ,0.0150 0.0098 0.01101,2,3,4,6, 7,8-Cl7-Dibenzo-p-dioxin ng 'O.0028 "' 0^0170 " 0.0440 0.0250 0.03901,2,3,4,6,7,8,9-ClS-Dibenzo-p-dioxin ng 0.0072 ... -0.0440 . . 0.0790 0.0210 0,07602J,7,8-CI4-Dibenzofiiran(DB5) ng O.002 ' 0.0110 0.0160 0.0230 0.0190l,2,3,7,S-C15-Dibenzofuran ng <L0018 _ 0.0029 ..." 0-0041 .. 0.0055 0,0056 . .2J,4,7,8-C15-Dibenzofuran ' ng <0.0019 " ~~ "0.0060 " 0.0073 ..0.0076 0.0083L2,3,4,7?8-CI6-Dibenzofiiran _ ng <0.0019 0.0086 0.0110 .0.0084 ' 0.0100l,2,3,6,7,8-CI6-Dibenzofuran "" "~ ng " "<OTOO"l7' "0.0043 "" " 0.0056, 0'.0041 " ". 0:0046 ,Z-S e -CIfi-Dibenzofiiran ng <0.0023 0.0029 ,0,0058.. 0.0032 0.0045l,2.3.7-,8,9-C16-Dibenzofuran - ng O.0023 <0,0023 <0.0021 . O.0023 O.0021i,2,3,4,6,7,8-C17-Dibenzofuran _ . ng <0.0024 <0.011 <0.014" O.OQ5 <0_OU1.2,3,4,7,8, 9-C17-Dibenzofuran ng <0.003 <0;0032 <0.0038 <0.0028 <0,00251.2,3,4,6,7,8,9-C18-Dibenzo'l:Qran" " " " " ng "<0~OQ37 " """OTOOSO-.r^aOlTO"1 " ""0.0048 " 0.0150

Total Cl4-DibenzoTp-dioxins ng <0.0016 / 0.0092 ": 0.1900. 0!l500 0.1900Total Cl5-Dibenzo-p-dioxins ng <0.0016 "0.0160 .0.1500 0,1400 0.1500Total C16-Dibenzo-p-dioxins ng <0,0023. (X0190. 0.3100 .... .0 300 ...0 900Total C17-Dibenzo-p-dioxins ng <0.0028 0.0350 : 0.0940 0.0500,. - 0,0840CIS-Dibenzo-p-dioxin ng 0.0072 0.0440 . ._.. O."0790 .0.0210 0.0760

Total CI4-Dibenzoforans " '. ng <0.0036" ""..0.0740 " " 0,0950""- 0.1100 0.1300Total C15-Dibenzofiirans ng O.0018 0.0330 . .-0,0510.." 0:0450 . Q.0580Total, CI6-Dibenzofiirans " " " "":v ng " <0"002"~ - 0.0280" """"07(3260 -. 0.0220"." 0.0330..Total C17-Dibenzoturans - ng <0.0027 <0.012 .<d,01*5 <0.0055 <0.012C18-DibenzofUran ng O.0037 _ 0,0080 "0.0170.. 0.0048.' 0.0150

Total PCDD/F. ------ - ng OGo72 o.2T M".0 " "0..77 1.0

2,3,7,8-TCDF (DB225)" """ " " """ ~""ng "- \ <0.0083 <0r008.5 <0.011 <6.0U,

Client:Levine-Fricke-Recon Project:311-81415

AR32I851+

001?PASC - Certificate of Analysis _ " Pa§e 7 of

Blank Run 31 Run #2 Run #3Client ID: Toluene Toluene Toluene TolueneLab\'o.: . 03362798 03362898 03162998 03363098

Daze Sampled: 98/07/14 98/07/14 98/07/14 98/07/14Component Units

ng O.0018 <0.002 . <Q,;OQ19 <0.0018ng <0.0015 <0.0018 «X0014 <0.0018

lJU,4,7,8-C16-Dibenzo-p-dIoxiii ng <0.0022 <Q.a02 <01Q023 . <0,C026ia,3,6J.S-C16-Dibenzo-p-dioxin ng <0.0018 <0.0017 <0.0019 <0.00221 Jl,3,7»8,9-Cl6-Dibenz£>-p-dioxin ng <0,002 . <0.00 1 9 «X002 1 O.G023U.3.4.6 ,8-C17-Dibenzo-p-dioxin ng 0.0022 0.0033 0,QQ44 0,0030l ,3.4,6,7,8,9-C18-Dibenzo-p-dLoxin ng 0.0058 0.0058 0,0120 0:00662.3.7,8-CU-Dibenzofuran (DBS) ng O.Q021 <0.0017 O.0024 0.0031U2,3,7,8-C15-DibenzoRiran ng <0.0013 O.0018 O.0019 <0;00172,3,4,7,8-C15-Dibenzoftiran ng <0.0016 <0.0025 <0,002 <0:00171.2,3,4.7.8-C16-Diben2ofuraE ng <0.0017 <0.0017 0.0023 <0.0018l,2J,6.7.S-C16-Dibenzoairan ng <0.0015 <0,0015 <0.0024 0.0016Z.3.4.6,7,S-C16-Dibenzofuran _ng <0-,0021 <0.0021 <0.0024 <0.00221 .2,3 J.8,9-CI6-Dibenzofuran ng <0,002l <0.0021 <0.0024 <OX0221 ,3 A6»7.$-C17-Dibenzofuran ng <0.0022 <O.OQ2 Q.0038 <Q.Q0221.2,3,4,7,S,9-C17-Dibenzofiiran ng <0.0028 <0.0025 <0,QG34 <Q.0023U,3,4,6,7,S,9.-ClS-Diben2ofuran ng <0.0025 <0.0022 0.0047 Q.0029

Total Cl4-Dibenzo-p-dioxins ng O.OOI8 <0.002 <O.U019 <0,0018™ )tal C15-Dibenzo-p-dioxins ng <0.0015 <0.0018 <0,0014 <O.OQ18. otal C16-Dibenzo-p-dio:dns ng O.002 <0.0019 <0.0021 <0.0023'"olal C17-Dibenzo-p-dioxins ng 0.0022 0.0033 . Q.QQ44._. ..A003.Q .(Jl8-Dibenzo-p-diaxin ng 0.0058 0.0058 TS.0120 0.006§

1 ical C14-Dibenzofurans . ng 0.0026 0.0023 0,0028 . O.Q079local C15-Dibenzoftinms ng O.0016 O.0024 0.0031 0.0030Total Cl6-Dibtfnzofunms ~ ng <0.0018 <0.0018 0.0052 0,0020Total Cl7-Dibenzofiinms ng <0.0025 <0.0022 - . 0.0042 <0,0024ClS-Dibenzofiiran ng <0,0025 <0.0022 QJ3047 ' 0,0029

Total PCDD/F ng 0.011 0.011 0,036 .0.025

2.3.7,8-TCDF (DB225) ng -

Client:Levine-Fricke-Recon Project:3U-8l415

UR32I855

ln/5/98' "J '" " ~ PASC - Certificate of Analysis '" ' ' Page s of <>

Blank" Blank - Blank Blank Blank Blank;-. '- .. - Client ID: Spike #1 Spike #1 Spike'#1 Spike #2 Spike #2 Spike #2

LabXq.: 033622MS -033622MS 033622MS . 033622MS 033622MS 033.622MSUnits; ng found ng spiked % Recoveries ng found ng spiked % Recoveries

Component

Internal Recoveries2.3,7,8 T4CDF-i3C-12 "" .'. " ''" V"'"" ". ,T ----- -^• - - _ _ 5g2.3,7,SrT4CDD-13C-12 *"" " "- " ~r ~ . ' :" "72 - ' __ " , •/ 74I,2,3,7,S-P5CDF-13C-12 " " . . : " - . . . . " " -: , . . . .88 - "T. . - "" " ". " - ." 77i.2,3,7,8-P5CDD-13C-12 " - . - - ; . . - " ioi* - 1 0 6I,2,3,6,7,8-H6CDF-13C-12 "'' - 74 • -- -- ' 74,i.2,3,6J,8-H6CDD-13C-12 " " . '" - ". " "-" : "". "= ~ -j$: _. , 831,2,3,4,6,7,8-H7CDF-13C-12 - . . . . . . 65 ..':._.... -- .- 66 "1,2,3,4,6,7,8-H7CDD-13C-12 " - " - 74 " 75OCDD-I3C-12 .. . . ..: . _- . .. ... . .- /. . ...' 9a:_"-' ; - - 99 'Alternatel,2,3,7,S,9-H6CDF-L3C-12 , - 78" "V -. - 81

2,3,.7,8-C14-Dibenzofuran(DB5)_ "2.4" " 2 . 5 ' 96..: ".. 2.4 . 2.5 982,3,7,8-Cl4-D:benzo-p-dioxin --•----• -^5 ;----2;5 . .' ..IQ6. 2.6 2.5 106I.2,3,7;S-C15-Dibenzofuran 2.4 2.5. -.-.--,' . ..96 - 2.6. " 2.5 ' 1022,3.4,7,8-C15-Dibenzoniran"* " 2.5 " "" 2.5" " "". ' 100 " " "~ 3,1 " 2.5 124l.2.3.77S-C15-Dibenzo-p-dioxin " " 2:3"""" 2.5 = ""91 ^ 2.3. 2,5 . - . 93l,2.3,4!7.8-C16-Dibenzofuran "" 2-4 2.5 ' . . 96-' 2,4 - 2.5 , 981.2,3.6,7,8-C16-Dibenzofuran 2 . 5 " " 2.5 . 1100 2.6 2.5 1042.3,4,6J,8-C16-Diben2oftiran- "" " 2.7 2.5 : " 106 " ' '2.9 2.5 " 115i,2,3,7,8,9-C16-Dibenzofuran 2.4 2.5 . . .95 1 2.5 2.5 98. .2,3.4 J,8-C16-Dibenzo-p-dioxin 2.7 2 J . . . . 106 2.9 2.5 11812,3.6.7,8-C16-Dibenzo-p-dioxin 3.0 2.5 120 2.9 2.5 11.5":.2,3.7,S,9-C16-Dibenzo-p-dioxin 2.8 2,5 114 3.0 , 2.5 118u2,3,4,6.7,8-C17-Dibenzofuran 2.6 .' 2,5 ' ' ' 106 ' 2.7 ' 2.5 109 "1.2,3,4.7.8.9-C17-Dibenzoairan 2.4 . . ..2,5 . . .,,-95.. ...... 2.4 . .2.5. .. 98 . '. =U2,3,4,6,7,8-CI7-Dibenzo-p-dioxin 2.4 2.5 . ' 95 ./.." 2.5.. .. - 2.5 99 .I,2,3,4.6,7,8,9-C18-Dibenzofuran . ..4.5. .... 5;0._ _. _. . .,81., _...: ' . 4J 5,0 , 911.2.3,4,6J,8T9-C18-Dibenzo-p-dioxin 4.8 5,0 . ^5 ".. . . - 4.9 .. .510 98

ClientLevine-Fricke-Recon Project:311-81415

AR32I856

10/5/98 PASC - Summary of Analysis Pre, Dates Page Ms-9 of 90014

Batch Code: 0722MC01 0722MC01PCDD/F(DB5) 03362298 . 03361998

033623 98 033630 98 .033624 98033625 98033626 9S03362798 . .033628 98

Run Date 98/07/30 98/07/31Date of Sample Prep, 98/07/22 98/07/22

Batch Code: 0722MC01 0722MC012.3,7.8-TCDF (DB225) 033623 58. 033623 98

033624 98 033624 98033625 98 033625 9803362698 03362698

Run Date 98/08/17 98/08/18Date of Sample Prep ' 98/07/22 98/07/22

Client:Levine-Fricke-Recon Project: 311 -81415

AH32 I 857

AirRecon®Division "of Levins * Frfcke • Recon

0015

APPENDIX II

EMISSION CALCULATIONS

& ORIGINAL DATA

AR32I858

0016OHM/Drake Drake Chemical, Operational Phase Test, 7/14/98 . .. •

RunMeter Volume (DSCM) (A)

13.03

Stack Flowrate (DSCM/MIN) (XJ 491 .48Stack Carbon Dioxide (%, dry) (C)

(0)Dioxms/Furans (nanograms)

Result2,3,7.8-CI4-Dibenzofuran (DB225) <0.00851 ,2,3,7.8-ClS-Dibenzofuran 0.00412,3,4,7.8-CI5-Dibenzofuran 0.00731,2,3,4,7.8-CIS-Dibenzofuran 0.01 11 ,2,3,6.7, 8-C16-Dibenzofuran 0.00562,3,4,6(7,8-CI6-Dibenzofuran 0.00581 12t3.7.8.9-C16-Dibenzoftiran <0.0021l,213.4.8.7.8-O7-Dibenzofuran <0,0141 ,2,3,4.7,8.9-C17-Dibenzofuran <0.0038Cl8-Dibenzofuran 0.0,1 7

2.3.7.8-a4-Dibenzo-p-dJoxin 0.00961 ,2,3,7,8-CI5-D(benzo-p-dioxin 0.00281 .S J.S-CIS-Oibenzo-p-dioxin 0.00621.2,3,6,7,8-CI6-Dibenzo-p-dioxin 0.0121,2,3.7,8,9-Cl6-Dibenzo-p-dioxirT 0.0151 .SAe.T.S-Ctf-Dibenzo-p-dioxin 0.044Cl8-Dibenzo-p-dioxin 0.079

Total PCDD/F as 2,3,7,8- TCDD (nanograms)(G)

11.60TEQ

(E) (F)as 2,3,7, 8

TEF TGDD0.1 0.0000000.05 0.0002050.5 0.0036500.1" 0.0011000.1 '0.0005600.1 0.0005800.1 0.0000000.01 0.0000000.01 0.0000000.001 0.000017

1 . 0.009600.5 0.001400.1 0.000620.1 0.001200.1 0.001500.01 0.000440.001 0.00008

2.10E-02Total PCDD/F as 2.3.7.8- TCDD (nanograms/DSCM)(H) 6.92E-03Total PCDD/F as 2,3,7.8- TCDD (grams/second){J) 5.67E-1 1Total PCDD/F as 2.3.7.8- TCDD (pounds/hour)(K) 4.50E-10

Total CI4-DibenzofuransTotal CIS-DibenzoftiransTotal CI6-DifaenzofuransTotal CI7-DibenzofuransCI8-DibenzofuranTotal C14-Dibenzo-p-dioxinsTotal CI5-Dibenzo-p-dioxinsTotal CI6-Dibenzo-p-dioxinsTotal Cl7-Dibenzo-p-dioxinsCI8-Dibenza-p-dioxin

Total Nanograms(l)Total Nanograms/DSCM@ 7% 02(M)*

0.0950.0510.0260.0000.0170.190.15 -0.310.0940,079

1.010.25

(D)

Result<0.0110.00550.00760.00840.00410.0032<0.0023<0.0050<0.00280,0048 ,

0.00940.00260.00250.00980.00980.0250.021

-

•

23.08447.2711.30

TEQ(E) (F)

as 2,3,7,8TEF TCDD0.1 0.0000000.05 0,0002750.5 0.0038000.1 0.0008400.1 0.0004100.1 0.0003200,1 0.0000000.01 0.0000000.01 Q.OOOOOO0.001 0.000005

1 Q.Q09400.5 0.001300.1 0.000250.1 0.000980.1 0.000980.01 0.000250.001 0.00002

1.88E-026.11E-034.55E-113.61E-10

0.11,0.0450.0220.0000.00480.150.140.230.0500.021

0.770.19

(D)

Result<0.0110.00560.00830.0100,00460.0045<0.0021O.0110.00250.015

0.010<0.00270.00440.0110.0110.0390,076

3 M3.10 ^442.6111.90 :

TEQ(E) (F)

as 2,3,7.8TEF TCDD0.1 0.0000000.05" 0.0002800.5 0.00415Q0.1 .0.0010000.1 0.0004600,1 0.0004500.1 0.0000000.01 0.0000000.01 0.0000000.001 0.000015

1 0.010000.5 0.000000.1 0.000440.1 0.001100,1 O.OOtlO0.01.. . 0.00030.001 O.OOGM

1.95E-026.27E-034.63E-113.67E.-.10

0.130,0580,0330,0000.0150.190.150.290.0840.076

1.030.24

Zero values were used in calculations for TEQs of non-detect congenersF = (DXE) Zero values were used in calculations for non-detect total homologue valuQ s jSum p%; *Ai * = calculated using CO2 as defined in the Trial Burn PlanH » (Sum F){8)(0.01667 minutes/second)(1E-9 grams/nanogram) / (A)K » (Sum F)(B)(60 minutes / hour)(2.205 E-9 pounds/nanogram) / (A)M = (L)(8.5%COa)/{C)

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•AR32I862

GROUP COMPANY(P(4ef

Az3 .. DATE^M?O H M / D R A K E O P E R A T I O N A L S T A C K T E S T

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0048

APPENDIX V

SUPPLEMENTAL LABORATORY

DATA SUMMARY

AH.i2i889

047PHILIP SERVICES

SUPPLEMENTARY DATA PACKAGEFOR 2,3,7,8-TCDF DB225 RE-ANALYSIS DATA

XEVINE-FRICKE-RECON" : -Project : 311-81415

Philip Analytical Services Corporation5555 North Service RoadBurlington, Ontario L7L 5H7

Submission #8G0533

Prepared by: Ancy Sebastian - CSRApproved by: Dr. Ron McLeod-Principal Scientist Initial

- - - AR32I890• "• " - - - - - - PHJUP ANALYTICAL SERVICES CORPORATION .

5555 North Service"Road,Burtingion.Ontario,Canada -L7L5H7 Tel:<9O5> i32-S788 F xgo 552-9169

0048

CASE NARRATIVE

PROJECT NARRATIVE - SUPPLEMENTARY PACKAGE 0049

PHILIP Analytical Services (Burlington ON)Philip Project: AN980281Philip Submission #:8G0533

Client: Levine-Fricke-Recon . ', .Client Project: 311-81415 :

L SAMPLE RECEIPT/ANALYSIS

a) Sample Listing " ' - ' _ ' '

PhUip ID Client Date Date Date RunSample ID Sampled Received Prepped Date

Re-Analysis Data2,3,7,8 TCDF(DB225) via EPA Method 23 - Confirming Column Analysis033623'?8 Blank 98/07/14 98/07/16 98/07/22. 98/08/18033624'98 Run*!' ""98/07/14 98/07/16 98/Q7/22 . 98/08/18033625 98 Run#2 '_ " .".''98/07/14 98/07/16, W07/22.. 9&/08/18033626:98 Run #3 ." 1 . ..98/07/14 98/07/16 98/07/22 98/08/18

Run Date is defined as the date of injection of the last calibration standard (12 hour or less) prior to thesamples analyzed within that run sequence. Therefore the time of calibration injection that defines therun date is always within 12 hours of the time of sample injection.

b) Shipping Problems: none encountered ............ . " .

c) Documentation Problems: none encountered

IL SAMPLE PREP:

No problems encountered

EL SAMPLE ANALYSIS:These extracts were re-analyzed to coiifirnithe absence of measurable 2,3,7,8-TCDF as determinedin earlier runs from August 17th. The sampK extfacts were re-injected since the post-run calibrationon the earlier runs (Aug 17th) Med to inject 'The continuing calibration from the following morning didshow the system to be in control, nevertheless, we proceeded to re-analyze the extractsto ensure complete control of an analytical sequence for the 2,3,7,8-TCDF confirmations.AH the data from the earlier DBS and DB225 analytical runs have been reported underseparate cover. • ". • . ' '^ "

a) Hold Times: all within recommended hold, times

b) Instrument Calibration: all within control limits

c) Surrogate/Internal Recoveries: except where noted otherwise, all within control limits

IV. DATA QUALITY ASSESSMENTAll samples for PCDD/F were analysed via EPA Method 23, .All data quality objectives for the method were met. All data contained herein was reviewedby the laboratory prior to release to Recon for review and deemed valid.

I certify that this data package is in compliance with the terms and conditions of the contract,both technically and for completeness, for other than the conditions detailed above.In addition, I certify, that to the best of my knowledge and belief, the data as reported are true and accurate.Release of the data contained in this data package has been authorized by the cognizant laboratoryofficial or his/her designee, as verified by this signature.

Ronald A. McLeod, Principal Sci, Ph.D, C.Chem Date

AR32I893

. PASC- Certificate of Analysis Page2of3

Client ID: Blank -Run #1 Run #2 Run #3 -:051Lab No.: 033623 98 ,031624.98 Q33625.98.,033626 98

• ' Date Sampled: 98/07/14 98/07/14 98/07/14 98/07/14Component Units

Original Analysis _........ _ _ _ _ _ ^_^__......_.2,3,7",8-TCDF (DB225) Pg' <8.3 <8-5 <11 <H .Internal Recoveries . . % . , . . . . . v . •2,3,7,8-TCDF-13C12 . . :_ . " " 82 ."/75 " 59 , .' 71Repeat Analysis2,3,7,8-TCDF(DB225) " ——— - pg -——-^0 :<18 <21 ,..<19...Internal Recoveries ; % : .. . . . . - . , . - - -2,3,7.8-TCDF-13C12 __ -,...... J87 ._.- 82 6° *"

ClientLevine-Fricke-Recon Projects 11-81415

AR32I89U

10/2/98 PASC - Summary of Analysis Pre. Dates Pa§e MS-B of 3

Batch Code: 0722MC01 0722MC01PCDD/FCDB5) 03362298 033,62998 . . . . . . . . . . . , . .-0052

03362398 03363098033624 98 . .033625.98 . .... ___.033626 98 . ...03362798 ... . __ .__ .. _ . . _ . _03362898 .. . ._. .. : _.

Run Date 98/07/30 .98/07/31Date of Sample Prep 98/07/22 98/07/22

Batch Code: 0722MC01 0722MC012,3,7,8-TCDF (DB225) 03362398 03362398 . . . . . . . . . . . .

033624 98 033624 98 '.' .... 1 . .03362598 0336259803362698 03362698 .

Run Date 98/08/17 98/08/18Date of Sample Prep 98/07/22 98/07/22

Client:Levine-Fricke-Recon Projects 11-81415MR32I895